general reference materials for food, industry and occupational hygiene.pdf
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General reference materials for food,industry and occupational hygiene
2003/2004
LGC Promochem offices
Edition 2003/2004
United Kingdom
LGC PromochemQueens RoadTeddingtonMiddlesexTW11 0LYUnited Kingdom
Tel: +44 (0)20 8943 7565Fax: +44 (0)20 8943 7554Email: [email protected]
Italy
LGC Promochem S.R.LVia Venezia, 2320099 Sesto San GiovanniMilanItaly
Tel: +39 02 2412 6830Fax: +39 02 2412 6831Email: [email protected]
France
LGC Promochem SARL6, Rue Alfred KastlerB.P.8307667123 MolsheimFrance
Tel: +33 (0)3 88 04 82 82Fax: +33 (0)3 88 04 82 90Email: [email protected]
Poland
LGC Promochem Sp. z o.o ul. M. Konopnickiej 1Dziekanów Lesny05-092 LomiankiPoland
Tel: +48 (0)22 751 31 40Fax: +48 (0)22 751 58 45Email: [email protected]
Germany
LGC Promochem GmbHMercatorstrasse 5146485 WeselGermany
Tel: +49 (0)281 9887 250Fax: +49 (0)281 9887 259Email: [email protected]
Spain
LGC Promochem SLPerú, 104 - Nave 308018 BarcelonaSpain
Tel: +34 93 308 4181Fax: +34 93 307 3612Email: [email protected]
India
LGC Promochem India Private LimitedPO Box 8061No. 142, 3rd Floor, 5th CrossRajmahal Vilas ExtensionBangalore 560 080India
Tel: +91 080 2361 4774 1256 Fax: +91 080 2361 3859Email: [email protected]
Sweden
LGC Promochem ABBox 1737SE-501 17 BoråsSweden
Tel: +46 (0)33 20 90 65Fax: +46 (0)33 20 90 79Email: [email protected]
If you are unsure of your local office, please email: [email protected]
Contents
www.lgcpromochem.com Edition 2003/2004 1
Contents
Introduction
Introduction
Einleitung
Introduction
Introducción
About the reference materials producers
About reference materials
About reference materials applications
About Quality Control Materials (QCRMs)
About proficiency testing (PT)
Relevant literature
Relevant training courses
General ordering information
4
5
6
7
8
9
9
9
10
11
11
12
Food and agriculture
Dairy products 13
Meat 17
FishShellfishShellfish toxins: Diarrhetic (DSP), Paralytic (PSP), Amnesic (ASP)Fish
22222628
Cereals and cropsWheatCornRyeRiceRapeseedGenetically modified crops
32323333333435
Vegetable matterFruit and vegetablesVegetable oils
363638
MycotoxinsSingle compoundsMulticomponent standard solutions
393940
Quality control reference materials from LGC 41
Food Authenticity 42
Lipid Standards 43
Food and drink productsProcessed foodDrinksFood additivesDye standardsAlcoholic and low alcohol beverageAlcohol
49495152535454
Animal food products 55
Fertilizers 56
PlantsTrees and bushesGrasses and cropsAquatic plantsMiscellaneous
5858606162
Contents
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Industrial raw materials and products
Solid fuels 64
Oils and liquid fuels 68
Conostan® Oil Analysis StandardsSingle element standards in oilMulti-element standards in oilSulphur in mineral oilChlorine in oilElement blank oilsPremiSolvTM ICP solventPartiStanTM particle standards- Compliant with ISO 11171:1999FTIR Operational Test StandardProficiency test program - Oil analysisCONOSTAN D-Series® Element (metallo-organic) Standards: D-3, D-12, D-19 (JOAP)Conostan® elements in oil custom standard request form
757577808081818182828385
Ores 86
Refractories and carbides 91
Cement 92
Glass and ceramics 94
Plastics 99
Metals 99
Miscellaneous 105
Occupational hygiene
Filter media 106
Paint and industrial sludges 108
Asbestos 110
Ash and particulate 111
Dust and Fumes 114
Aldehydes/Ketones-DNPH standards 116
Pure materials
Elemental analysis 119
Stochiometry 121
Organo-metallic compounds 122
Speciation 122
Isotopes 123
Standards for spectroscopyNIST Standard Reference Materials® (SRMs®)ULTRA Scientific’s certified ICP/AA standardsULTRA Scientific's EnviroConcentrateTM kits for ICPULTRA Scientific’s certified standards for atomic absorption spectroscopyULTRA Scientific's EnviroConcentratesTM for atomic absorption spectroscopy
125125125134136140
Multielement standardsEPA Method 200.7EPA Method 6010AStandards for ICP/MS
144144146147
Ion chromatography standards 148
CERTAN® - The ampoule in the bottle 150
Introduction
4 Edition 2003/2004 www.lgcpromochem.com
Introduction
About the catalogue
“Reference materials for food, industry and occupational hygiene 2003/2004” is the first cataloguefrom LGC Promochem offering a comprehensive selection of more than 1000 reference materials andstandards exclusively intended for these diverse fields of analysis
For food analysts the range includes food and beverage matrices certified for nutritional and otheranalytes as well as pure standards such as food additives and colourings. Of particular interest is thenew selection of mycotoxins standards.
The industrial chapter features materials for a wide spectrum of industries from mining to textiles andfrom plastics to cement. For the first time Conostan® Oil Analysis Standards, focussed on lubricant/oilanalysis and condition monitoring is included.
The products described in this catalogue are sourced from national and international bodies, as wellas commercial organisations. A certificate of analysis normally accompanies each sample. Howeverthe appearance and content of these certificates will vary according to producer.
About LGC Promochem
LGC Promochem is Europe’s leading supplier of reference materials. We work closely with leadingmanufacturers worldwide to offer laboratories across Europe improved access to reference materialsdesigned to suit an increasingly large range of analyses.
Our network of offices in Europe and India together with our long experience in selling referencematerials allows LGC Promochem to work in partnership with our customers to provide fast deliverytogether with good technical advice as well as dealing with complicated import and export regulations.
LGC Promochem is an authorised distributor of BCR® reference materials. We currently stock morethan 2000 units of certified BCR® reference materials under controlled conditions.
Einleitung
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Einleitung
Über den Katalog
“Reference materials for food, industry and occupational hygiene 2003/2004” ist der erste Katalog vonLGC Promochem mit einer umfassenden Auswahl von mehr als 1000 Referenzmaterialien für dieBereiche Lebensmittel, Industrie und Arbeitshygiene.
Für den Bereich der Lebenmittelanalytik reicht die Produktpalette von Matrixreferenzmaterialien wieLebensmittel und Getränke, bis hin zu reinen Verbindungen wie Fettsäuren oder auch Zusatzstoffe fürLebensmittel. Besonders interessant sind einige neue Mykotoxin-Standards.
Die Referenzmaterialien für die Industrie umfassen Matrixmaterialien aus dem Bergbau, sowieTextilien, Kunststoffe, Zement und viele mehr. Neu in unserem Lieferprogramm sind die Conostan®
Öl-Standards.
Die in diesem Katalog beschriebenen Produkte stammen von nationalen und internationalenEinrichtungen, wie auch von kommerziellen Anbietern. Jedes Produkt wird in der Regel mit einemZertifikat geliefert. Aussehen und Inhalte der Zertifikate sind je nach Hersteller unterschiedlich
Über LGC Promochem
LGC Promochem ist der führende Lieferant von Referenzmaterialien in Europa. Wir arbeiten eng mitden weltweit führenden Herstellern zusammen, um den europäischen Laboratorien einen leichtenZugriff auf Referenzmaterialien zu ermöglichen.
Das Netzwerk an Niederlassungen in Europa und Indien verbunden mit langjähriger Erfahrung imVertrieb von Referenzmaterialien hat LGC Promochem zum Partner unserer Kunden werden lassen,der neben optimierter Lieferzeit und technischer Beratung auch komplizierte Einfuhrvorgängeübernimmt.
LGC Promochem ist autorisierter Distributor für BCR®-Referenzmaterialien. Zur Zeit lagern bei unsunter kontrollierten Bedingungen mehr als 2000 Einheiten zertifizierter BCR®-Referenzmaterialien.
Introduction
6 Edition 2003/2004 www.lgcpromochem.com
Introduction
Au sujet du catalogue
Le catalogue intitulé : ”Reference materials for food, industry and occupational hygiene 2003/2004” deLGC Promochem est la première version regroupant une sélection complète de plus de 1000matériaux de référence et standards exclusivement destinés aux analyses dans ces domaines.
En ce concerne la gamme qui se destine aux analyses alimentaires, celle-ci comprend des matricesalimentaires et des boissons certifiées en analytes et nutriments ainsi que des substances pures deréférence comme des additifs et des colorants.
Le chapitre comprenant des références se destinant à l’analyse industrielle se caractérise par un trèslarge éventail d’industries, à savoir de l’extraction minière au domaine textile ou de l’industrie duplastique à celle des ciments. Nous présentons pour la première fois la gamme de standardsanalytiques d’huiles de base Conostan®.
Les produits décrits dans ce catalogue sont issus d’organismes nationaux et internationaux reconnusainsi que de sociétés commerciales. Un certificat d’analyses est généralement fourni avec chaqueéchantillon. Cependant selon le producteur, la présentation du certificat et son contenu peuventvarier.
Au sujet de LGC Promochem
LGC Promochem est le principal fournisseur européen de matériaux de référence. Nous travaillons enétroite collaboration avec les principaux producteurs mondiaux afin d’offrir aux laboratoires européensle meilleur accès possible à tout type de matériaux de référence destinés à correspondre à unnombre grandissant d’analyses.
Le réseau européen de bureaux LGC Promochem ainsi que notre expérience dans la distribution dematériaux de référence permettent d’assurer des livraisons plus rapides, un support technique endirect sans oublier une assistance lors d’importations soumises à contrôles.
LGC Promochem est un distributeur officiel des matériaux de référence du BCR®. Nous stockonsactuellement plus de 2000 unités de matériaux de référence certifiés du BCR® dans des conditionscontrôlées.
Introducción
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Introducción
Acerca de este catálogo
“Materiales de referencia para la alimentación, la industria y la higiene en el trabajo 2003/2004” es elprimer catálogo de LGC Promochem, que ofrece una amplia selección de más de 1000 materiales ynormas de referencia destinados exclusivamente a estos campos de análisis.
Para los analistas de alimentos, la variedad incluye matrices de referencia de comida y bebidacertificadas para análisis nutricionales y de otro tipo, además de normas de pureza, como loscolorantes y los aditivos alimentarios. Cabe destacar la nueva selección de normas de micotoxinas.
El capítulo industrial describe materiales para una amplio segmento de industrias, desde la minera ala textil, y desde el plástico a las cementeras. Se incluye por primera vez la gama Conostan® denormas analíticas basadas en el aceite.
Los productos descritos en este catálogo se han obtenido de organismos nacionales einternacionales, así como de organizaciones comerciales. Cada una de las muestras suele iracompañada de un certificado de análisis. Sin embargo, la presentación y el contenido de estoscertificados variarán según el fabricante.
Acerca de LGC Promochem
LGC Promochem es el primer proveedor de materiales de referencia en Europa. Trabajamos enestrecha colaboración con fabricantes líderes en el ámbito internacional para ofrecer a loslaboratorios de toda Europa un mejor acceso a materiales de referencia diseñados para adaptarse auna diversidad de análisis que se amplía constantemente.
Nuestra red de oficinas en Europa e India, junto con nuestra larga experiencia en la venta demateriales de referencia, permite a LGC Promochem trabajar conjuntamente con sus clientes paraproporcionar una rápida entrega, además de un buen asesoramiento técnico y cumplir con loscomplicados reglamentos sobre importación y exportación.
LGC Promochem es distribuidor autorizado de materiales de referencia BCR®. Actualmente tenemosalmacenadas más de 2000 unidades de materiales de referencia certificados BCR® en condicionescontroladas.
Reference Materials
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Reference Materials
About the reference materials producers
BCR®
BCR reference materials are the product of both research funding and direct action programmes ofthe European Commission, in which new or improved measurement or testing methods aredeveloped. These programmes are aimed at improving, harmonising or standardising measurementsand testing in the European Union. BCR is part of the Institute for Reference Materials andMeasurements (IRMM) in Belgium.
LGC
LGC has a long history in the development and validation of analytical methods and the referencematerials production facility at LGC, complements this expertise. In addition LGC offers a range ofchemical and bio-analytical laboratory services across a variety of sectors including: food andagriculture, environment, life sciences, chemicals and forensic science. LGC plays a pivotal role in anumber of programmes with both government and industry intended improve analytical standards andperformance.
The National Institute of Standards and Technology (NIST)
NIST produces standard reference materials (SRMs). Based in the United States, NIST has providedreference materials to industry and commerce for nearly 100 years. NIST collaborates with companiesto provide academia and industry with SRMs for expanding areas such as air and water pollution,which are international issues.
ULTRA ScientificTM
ULTRA ScientificTM is recognized as a leader in the chemical standards industry and LGCPromochem is working in close partnership with ULTRA to ensure that the requirements for highquality environmental standards are satisfied. ULTRA’s organic and inorganic calibration standardsare widely used in the analysis of drinking water, waste water, soils, sediments, foods, cosmetics andother products.Their manufacturing, quality control and distribution system is registered to the International ISO 9001standard. ULTRA was among the first standards manufacturers to have its quality control laboratoryaccredited to the ISO Guide 25 standard.
CerilliantTM Corporation
CerilliantTM Corporation is a leading supplier of chemical standards for environmental analysis andforensic drug testing and for providing custom chemical synthesis. They were the first to produce 13Clabeled chlorinated Dioxins and Furans in cooperation with Cambridge Isotope Laboratories to meetthe increasing demand for isotope-labeled reference materials. From raw materials analysis tocontinuing shelf-life studies, Cerilliant’s ISO 9001 system requires multiple checks to ensure productconformance.
CONOSTAN® Oil Analysis Standards
CONOSTAN® is a pioneer and global leader in the development, manufacturing, and marketing of oilanalysis reference materials/standards. The pioneering innovation continues with introductions ofstandards for lubricant product analysis that are benchmarks for quality, accuracy, precision, andtraceability. Their quality program is certified under ISO 9001:2000.
Others
Materials from the following organisations are also included in this catalogue:
- Agricultural Research Centre, Finland
- Institute of Nuclear Chemistry and Technology, Poland
- International Atomic Energy Agency, Austria
- National Research Centre for Certified Reference Materials, China
- National Food Administration, Sweden
- R. T. Corporation, USA
- Swedish Meats R&D, Sweden
About reference materials
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About reference materialsIt is important to differentiate between reference materials and certified reference materials.
Reference materials (RMs) are defined by the International Organisation for Standardisation (ISO)Guide 30 as: a material or substance, one or more of whose property values are sufficientlyhomogeneous and well established to be used for the calibration of an apparatus, the assessment ofa measurement method or for assigning values to materials.
The ISO Guide defines a certified reference material (CRM) as: a reference material accompanied bya certificate, one or more of whose property values are certified by a procedure which establishes itstraceability to an accurate realisation of the unit in which the property values are expressed, and forwhich each certified value is accompanied by an uncertainty at a stated level of confidence.
Reference materials may also be categorised as either pure materials, used to make standardsolutions to calibrate instruments, or as matrix reference materials used to validate test methods (thematrix should be as similar as possible to the samples being analysed).
A standard solution is required to calibrate the response of a measuring instrument. A matrixreference material is used to assess the suitability of a complete analytical measurement process. Byusing a suitable matrix reference material the problems encountered with routine samples due tospeciation, extraction efficiency, completeness of matrix dissolution and possible interference can bereplicated. With these conditions if the reference material results agree with the certificate value thenthe results obtained on the samples will be accurate.
When selecting a reference material for a particular application the analyst must consider thefollowing factors before selecting a material:
- Matrix match and potential interferences- Analytes- Measurement range- Measurement uncertainties- Certification procedures used by the producer- Documentation supplied with the material (e.g. certificate or report)
About reference materials applicationsFood safety, product quality, occupational protection and law enforcement are all dependent onreliable chemical measurements to ensure correct and accurate decisions are made. Referencematerials are instrumental in ensuring the reliability of these measurements and thus avoiding the useof poor quality data as the basis of decision making.
Reference materials have a wide variety of applications examples including:- Method validation- Instrument calibration- Establishing traceability- Assistance with quality control- Qualitative verification- As check samples to assess the performance of an analyst
About Quality Control Materials (QCRMs)QCRMs are a new product range from LGC and have been developed for use in routine analysis. TheQCRM range offers the ideal solution for independently produced materials to meet UKAS and ISO17025 accreditation requirements for traceability and comparability of results. Applications includechecking results for bias, establishing QC charts with traceable reference values and action limits,estimating the uncertainty of an analytical method, training new analysts, monitoring continuing staffcompetence and saving time associated with the production of in-house QC materials.
QCRMs have been priced to allow routine use in the analysis that forms the bulk of daily laboratoryanalysis. Full documentation and instructions are provided with each QCRM.
Currently available QCRMs are: Meat Paste (1), Flour (1), Chocolate (1), Fish Paste (1), Fish Paste(2), Animal Feed (1), Landfill Leachate (1), Landfill Leachate (2), Contaminated Soil (1).
The QCRM range is planned for expansion to meet customers’ needs for particular materials. If thereare particular materials or applications that you would like developed or if you have any other queriesregarding the QCRM range please contact the production team on:
Tel +44 (0)20 8943 7514 Fax +44 (0)20 8943 7314
About proficiency testing (PT)
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About proficiency testing (PT)Proficiency testing (PT) is a powerful quality assurance tool for laboratories undertaking analyticalmeasurements. A PT scheme provider distributes test materials on a regular basis to participatinglaboratories for independent testing.The results are returned to the organiser of the scheme whomakes an analysis of the results and provides a report to all the participants.
There are a number of benefits of taking part in a PT scheme:
- Provides laboratories with a mechanism to compare their measurements with others
- Enables laboratories to demonstrate the quality of their results to third parties e.g. customers,regulators and accreditation bodies
- Facilitates the monitoring of trends, over time, in the quality of measurements
- Assists the evaluation of methods and instrumentation
- Helps and educates laboratory staff and their customers
The PT group at LGC is an accredited PT scheme provider, offering a range of PT schemes acrossdifferent measurement sectors. As international experts in many aspects of PT, LGC can provide arange of consultancy and training services for PT providers, participants and participant customers.
Current PT schemes available from LGC include:
BAPS
Chemical, microbiological and sensory analysis of a range of beers. Jointly operated with BrewingResearch International.
CONTEST
Analysis of contaminated soils for a wide range of metals and inorganic/organic contaminants.
CRYPTS
Counting of cryptosporidium oocysts in drinking water. Jointly operated with the Scottish ParasiteDetection Laboratory under licence from the UK Drinking Water Inspectorate.
DAPS
Scheme for the alcoholic drinks industry (except beer) for the analysis of alcoholic strength and a widerange of other parameters in fermented worts, distilled spirits, wine, liquors etc.
LGC PC1
Analysis of raw sugar used in soft drink production in association with PepsiCo BeveragesInternational.
MAPS
Analysis of malt and barley used by the malting, brewing and distilling industries. Jointly operated withGreencore Malting Group.
PHARMASSURE
Measurement of a range of parameters in pharmaceutical and medicinal products.
Quartz
Measurement of a range of prescription and illicit drugs in post-mortem human blood.
SODAS
Analysis of carbonated and still soft drinks for a number of different analytes.
OIL ANALYSIS
Analysis of important properties of lubricants (new & used/in-service) such as: wear & additive metals,particles, viscosity.
Relevant literature
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TOYTEST
Toy safety testing to the European Standard EN71.
Each scheme is run on an international basis. All schemes are managed in accordance with ISO/IECGuide 43:1 and ILAC Guide G13:2000. The scientific integrity and content is assured by a SteeringGroup for each scheme, consisting of experts in the sector. All schemes are fully confidential, withparticipants only being identified by a unique identification number. The operation of each scheme isdocumented in a scheme protocol that is available on request.
For further information, please contact:
Proficiency Testing GroupLGC Tel: +44 (0)20 8943 8494Queens Road Fax: +44 (0)20 8943 0654Teddington, Middlesex Email: [email protected] 0LY, UK Web: www.lgc.co.uk
Relevant literatureApplications of Reference Materials in Analytical Chemistry VAMV. Barwick, S. Burke, R. Lawn, P. Roper and R. Walker RSC
Reference Materials in Analytical Chemistry – A Guide for Selection and UseA. Zschunke published by Springer-Verlag
Reference Materials for Chemical Analysis – Certification, Availability and Proper UsageM. Stoeppler, W.R. Wolf, P.J. Jenks published by Wiley-VCH
Proficiency Testing in Analytical Chemistry, R. Lawn, M. Thompson and R. Walker published by TheRoyal Society of Chemistry
Relevant training coursesA range of training courses are available from LGC to help laboratory managers and analystsdemonstrate competence in, and keep abreast of, quality assurance issues and practices. LGC’sanalytical quality training programme includes a range of training courses:
- Using reference materials in analytical measurements- Using proficiency testing in the analytical laboratory- Method validation- Principles and practice of measurement uncertainty in chemical testing laboratories- ISO/IEC 17025 implementation- Quality systems in testing laboratories- Statistics for analytical chemists- Further statistical tools for analytical chemists
The majority of the courses are run in South West London at Teddington. In addition, LGC canprovide training for groups of staff at your own site, where the courses can be customised to meetyour exact needs.
For further information, please contact:
Lorraine DidinalLGC Training Centre Tel: +44 (0)20 8943 7314Queens Road Fax: +44 (0)20 8943 7631Teddington, Middlesex Email: [email protected] 0LY, UK Web: www.lgc.co.uk
General ordering information
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General ordering informationPrices and delivery procedures are shown in the price list that accompanies this catalogue, or areavailable from your local LGC Promochem sales office. For products requiring special deliveryprocedures (cooled shipping, special licensing, controlled substances, etc) additional charges will beapplied.
Please check with your local LGC Promochem sales office for detailed procedures and transportcharges where applicable.
Unless otherwise agreed in advance and in writing, orders are accepted only against LGCPromochem’s standard terms and conditions of sale.
Once delivered to the customer, reference substances are not returnable. For this reason it is veryimportant for users to be certain that the product ordered meets their needs.
LGC Promochem’s technical staff is available to advise on the use and suitability of a particularproduct. Customers requiring assistance with the use or application of a particular referencesubstance should contact their local LGC Promochem office, contact details are provided at thebeginning of this catalogue.
For further information please contact any of the offices listed on page 4 or visit our websitewww.lgcpromochem.com.
Dairy products
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Dairy productsCode Product Unit
LGC7104 (RM) Sterilised cream - Proximates and nutrient elementsAssessed values
Ca ............................. 845 mg/kg P................................823 mg/kg Total fat.................. 22.7 g/100 gK ............................. 1160 mg/kg Zn ...............................3.1 mg/kg Ash......................... 0.58 g/100 gMg............................... 84 mg/kg Moisture..................70.2 g/100 gNa ............................. 505 mg/kg Nitrogen..................0.40 g/100 g
Indicative values for Cl, Lactose
5 x 170 g
LGC7106 (RM) Processed cheese - ProximatesAssessed values
Moisture ................. 46.1 g/100 g Total fat ..................27.0 g/100 gNitrogen ................. 2.98 g/100 g Ash ...........................5.3 g/100 g
5 x 220 g
BCR-063R Skim milk powder - Major and trace elementsNatural elemental levels in milk.
Certified values
Ca ............................. 13.49 g/kg I ................................0.81m g/kg Na ............................... 4.37 g/kgCl ................................ 9.94 g/kg K................................17.68 g/kg P ............................... 11.10 g/kgCu .......................... 0.602m g/kg Mg .............................1.263 g/kg Pb .............................. 18.5µg/kgFe............................. 2.32m g/kg N (total)........................62.3 g/kg Zn............................. 49.0m g/kg
Indicative values for Mo, N(Kjeldahl), Se
50 g
BCR-150 Spiked skim milk powder - Trace elementsMilk spiked with Cd, Cu, Fe and Hg.
Certified values
Cd ............................. 21.8 µg/kg Fe .............................11.8 mg/kg I ................................ 1.29 mg/kgCu ............................ 2.23 mg/kg Hg................................9.4 µg/kg Pb ............................ 1.00 mg/kg
Indicative values for Co, Mn, Ni, Se, Tl, Zn
23 g
BCR-151 Spiked skim milk powder - Trace elementsMilk spiked with Cd, Cu, Fe and Hg.
Certified values
Cd ........................... 101.0 µg/kg Fe .............................50.1 mg/kg I ................................ 5.35 mg/kgCu ............................ 5.23 mg/kg Hg...............................101 µg/kg Pb ........................... 2002 mg/kg
Indicative values for Co, Mn, Ni, Se, Tl, Zn
23 g
BCR-421 Milk powder - VitaminsSpiked spray-dried powder.
Certified values
B1 (thiamin) .............. 6.51 mg/kg B12 ..........................0.034 mg/kg E (tocopherol) ............. 99 mg/kgB2 (riboflavin)............ 14.5 mg/kg C (total ascorbate).....769 mg/kg Folate (total)............. 1.42 mg/kgB6 (total pyridoxine) .. 6.66 mg/kg D3 (cholecalciferol)..0.143 mg/kg Niacin.......................... 68 mg/kg
50 g
NIST-1549 Non-fat milk powder - Trace elementsCertified values
Ca ...................................1.30 % Fe .............................1.78 mg/kg P .....................................1.06 %Cd ........................ 0.0005 mg/kg Hg.........................0.0003 mg/kg Pb .......................... 0.019 mg/kgCl ....................................1.09 % K..................................... 1.69 % S ...................................0.351 %Cr ......................... 0.0026 mg/kg Mg ................................ 0.120 % Se ............................ 0.11 mg/kgCu .............................. 0.7 mg/kg Mn ............................0.26 mg/kg Zn............................. 46.1 mg/kgI ................................ 3.38 mg/kg Na................................. 0.497 %
Indicative values for Ag, Al, As, Br, Co, F, Mo, Rb, Sb, Sn
100 g
NIST-RM 8435 Whole milk powder - Trace elements, proximates and nutrientsReference values for major, minor and trace constituent elements, proximates, fatty acids, calories and selectedvitamins.Indicative values for additional elements, fatty acids and vitamins
40 g
NIST-1846 Whole milk powder - Trace elements, proximates and nutrientsCertified values
Vitamin A (as trans-retinol) ......................5.84 mg/kg Vitamin B6 ................................................. 8.4 mg/kgVitamin E (as α–tocopherol) .....................271 mg/kg Niacin ...................................................... 63.3 mg/kgVitamin C ................................................1146 mg/kg Iodine ...................................................... 1.11 mg/kgVitamin B2 ................................................17.4 mg/kg
Indicative values for proximates, calories, additional vitamins, minerals and trace elements
10 x 30 g
Dairy products
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Code Product Unit
ARC/CL1 Skim milk powder - Trace elementsA homogeneous spray-dried milk powder containing 2.0% fat.
Certified values
Ca ............................ 13.00 mg/g Hg...................................<1 ng/g Pb .................................. 16 ng/gCd .................................. <5 ng/g Mg ..............................1.23 mg/g Se .................................. 82 ng/gCu ............................... 0.59 µg/g Mn ...............................0.44 µg/g Zn.............................. 41.68 µg/gFe................................ 4.54 µg/g Mo ...............................0.49 µg/g
50 g
IAEA-153 Milk powder - Trace elementsCertified values
Br ............................. 12.3 mg/kg K............................17620 mg/kg P ........................... 10100 mg/kgCa ......................... 12870 mg/kg Mg ...........................1060 mg/kg Rb ............................... 14 mg/kgFe............................. 2.53 mg/kg Na............................4180 mg/kg Zn............................. 39.6 mg/kg
Indicative values for Cu, Mn, Mo, Sr
50 g
IAEA-155 Whey powder - Trace elementsCertified values
Br ............................. 39.1 mg/kg Hg.........................0.0026 mg/kg Pb .......................... 0.104 mg/kgCd .......................... 0.016 mg/kg Mg ...........................3190 mg/kg Rb ............................ 39.2 mg/kgCl .......................... 69200 mg/kg Mn ..............................9.3 mg/kg Sc........................... 0.028 mg/kgCo ........................ 0.0427 mg/kg Na.............................15.8 mg/kg Se .......................... 0.064 mg/kgCr ............................. 0.59 mg/kg Ni ..............................0.54 mg/kg Zn............................. 34.3 mg/kgCs .......................... 0.086 mg/kg P............................16210 mg/kg
Indicative values for Al, As, B, Ca, Cu, Fe, K, S, Sr
50 g
BCR-282 Whole milk powder - Aflatoxin M1 (very low level)Certified value
Aflatoxin M1 ......... <0.05 µg/kg (probable content is in the range 0.01 to 0.02 µg/kg)
25 g
BCR-283 Whole milk powder - Aflatoxin M1 (low level)Certified value
Aflatoxin M1 .............. 0.09 µg/kg
25 g
BCR-187 Natural milk powder - PesticidesCompound Certified value Uncertainty
µg/kg µg/kg
HCB ................................................................... 1.50............................ 0.2alpha-HCH ........................................................... 1.8.......................... 0.14gamma-HCH........................................................ 5.7............................ 0.74,4'-DDE .............................................................. 6.6............................ 0.6
20 g
BCR-188 Milk powder (spiked) - PesticidesCompound Certified value Uncertainty
µg/kg µg/kg
HCB ................................................................... 37.4............................ 2.7alpha-HCH ......................................................... 20.0............................ 0.9beta-HCH........................................................... 12.0............................ 1.2gamma-HCH...................................................... 45.4............................ 2.9beta-Heptachlor epoxide.................................... 32.0............................ 1.84,4'-DDE ............................................................ 51.3............................ 3.5Dieldrin............................................................... 36.1............................ 2.4Endrin .................................................................. 6.2............................ 0.94,4’-DDT ............................................................ 69.0............................ 4.6
20 g
BCR-450 Natural milk powder - PCBsCompound Certified value Uncertainty
µg/kg µg/kg
PCB 52 .............................................................. 1.16.......................... 0.17PCB 118 .............................................................. 3.3............................ 0.4PCB 153 ............................................................ 19.0............................ 0.7PCB 156 ............................................................ 1.62............................ 0.2PCB 170 .............................................................. 4.8............................ 0.6PCB 180 ............................................................ 11.0............................ 0.7
20 g
BCR-532 (RM) Unspiked milk powder - PCDDs and PCDFs (blank)Non certified values
ng/kg ng/kg ng/kg
2,3,7,8-TCDD...................... 0.10 1,2,3,7,8,9-HxCDD..............0.16 1,2,3,4,7,8-HxCDF.............. 0.341,2,3,7,8-PeCDD ................ 0.29 2,3,7,8-TCDF.......................0.16 1,2,3,6,7,8-HxCDF.............. 0.341,2,3,4,7,8-HxCDD ............. 0.17 1,2,3,7,8-PeCDF ...................0.1 2,3,4,6,7,8-HxCDF.............. 0.391,2,3,6,7,8-HxCDD ............. 0.43 2,3,4,7,8-PeCDF .................0.67
60 g
Dairy products
www.lgcpromochem.com Edition 2003/2004 15
Code Product Unit
BCR-533 (RM) Spiked milk powder - PCDDs and PCDFs (lower level)Non certified values
ng/kg ng/kg ng/kg
2,3,7,8-TCDD...................... 0.42 1,2,3,7,8,9-HxCDD..............0.47 1,2,3,4,7,8-HxCDF.............. 1.061,2,3,7,8-PeCDD ................ 0.86 2,3,7,8-TCDF.......................0.39 1,2,3,6,7,8-HxCDF.............. 1.031,2,3,4,7,8-HxCDD ............. 0.56 1,2,3,7,8-PeCDF ...................0.1 2,3,4,6,7,8-HxCDF.............. 1.221,2,3,6,7,8-HxCDD ............. 1.27 2,3,4,7,8-PeCDF .................1.96
60 g
BCR-534 (RM) Spiked milk powder - PCDDs and PCDFs (higher level)Non certified values
ng/kg ng/kg ng/kg
2,3,7,8-TCDD...................... 0.65 1,2,3,7,8,9-HxCDD..............0.80 1,2,3,4,7,8-HxCDF.............. 1.751,2,3,7,8-PeCDD ................ 1.44 2,3,7,8-TCDF.......................0.65 1,2,3,6,7,8-HxCDF.............. 1.551,2,3,4,7,8-HxCDD ............. 0.80 1,2,3,7,8-PeCDF .................0.15 2,3,4,6,7,8-HxCDF.............. 1.901,2,3,6,7,8-HxCDD ............. 1.92 2,3,4,7,8-PeCDF .................3.16
60 g
BCR-607 Natural spray dried milk powder - PCDDs and PCDFsCompound Certified value Uncertainty
ng/kg ng/kg
2,3,7,8-TCDD..................................................... 0.25.......................... 0.031,2,3,7,8-PeCDD ............................................... 0.79.......................... 0.041,2,3,4,7,8-HxCDD ............................................ 0.42.......................... 0.071,2,3,6,7,8-HxCDD ............................................ 0.98.......................... 0.111,2,3,7,8,9-HxCDD ............................................ 0.34.......................... 0.052,3,7,8-TCDF..................................................... 0.05.......................... 0.031,2,3,7,8-PeCDF.............................................. 0.054........................ 0.0132,3,4,7,8-PeCDF................................................ 1.81.......................... 0.131,2,3,4,7,8-HxCDF............................................. 0.94.......................... 0.041,2,3,6,7,8-HxCDF............................................. 1.01.......................... 0.092,3,4,6,7,8-HxCDF............................................. 1.07.......................... 0.05
100 g
IAEA-152 Milk powder - Radioactive isotopesCertified values134Cs...........................764 Bq/kg 40K ............................. 539 Bq/kg137Cs.........................2129 Bq/kg 90Sr ............................. 7.7 Bq/kg
250 g
IAEA-321 Milk powder - Radioactive isotopesCertified values134Cs..........................15.5 Bq/kg 40K ............................. 552 Bq/kg137Cs..........................72.6 Bq/kg 90S .............................. 3.3 Bq/kg
250 g
IAEA-154 Whey powder - Radioactive isotopesCertified values134Cs.........................1355 Bq/kg 40K ........................... 1575 Bq/kg137Cs.........................3749 Bq/kg 90S .............................. 6.9 Bq/kg
250 g
BCR-519 Anhydrous butter fat - Triglycerides
Triglyceride contents of an anhydrous butter fat with additional value for free cholesterol.
Compound Certified value Uncertaintymass fraction (%) mass fraction (%)
Cholesterol.............................................. 0.30......................................................... 0.03C24 ......................................................... 0.05......................................................... 0.02C26 ......................................................... 0.25......................................................... 0.03C28 ......................................................... 0.59......................................................... 0.04C30 ......................................................... 1.15......................................................... 0.05C32 ......................................................... 2.43......................................................... 0.12C34 ......................................................... 5.64......................................................... 0.18C36 ......................................................... 10.47....................................................... 0.19C38 ......................................................... 12.53....................................................... 0.22C40 ......................................................... 10.03....................................................... 0.16C42 ......................................................... 6.69......................................................... 0.10C44 ......................................................... 6.11......................................................... 0.08C46 ......................................................... 6.86......................................................... 0.08C48 ......................................................... 8.69......................................................... 0.15C50 ......................................................... 11.40....................................................... 0.24C52 ......................................................... 10.96....................................................... 0.25C54 ......................................................... 5.89......................................................... 0.13
2 amp.
Dairy products
16 Edition 2003/2004 www.lgcpromochem.com
Code Product Unit
NIST-2387 Peanut butter - Fat, fatty acids, trace elements and tocopherolsThis Standard Reference Material (SRM) is intended primarily for use in validating methods for determiningproximates, fatty acids, calories, vitamins, elements, amino acids, and aflatoxins in peanut butter and similarmatrices.
Certified concentrations for fat and selected fatty acids
Mass fraction (%)Fat (extractable) 51.6 ± 1.4
Fat (sum of fatty acids) ............................. 49.8 ± 1.9
Saturated fat ............................................. 10.4 ± 0.2
Monounsaturated fat ................................. 24.4 ± 0.9
Polyunsaturated fat ................................... 13.2 ± 0.4
Mass fraction (%) Mass fraction (%)(as the triglyceride) (as the fatty acid)
Tetradecanoic acid (C14:0) .................................................................. 0.025 ± 0.002 ..................... 0.024 ± 0.002(Myristic acid)Hexadecanoic acid (C16:0) ...................................................................... 5.18 ± 0.15 ......................... 4.94 ± 0.15(Palmitic acid)(Z)-9-Hexadecenoic acid (C16:1 n-7) ................................................... 0.046 ± 0.011 ..................... 0.044 ± 0.010(Palmitoleic acid)Octadecanoic acid (C18:0) ....................................................................... 2.23 ± 0.08 ......................... 2.13 ± 0.08(Stearic acid)(Z)-9-Octadecenoic acid (C18:1 n-9) ...................................................... 24.43 ± 0.94 ....................... 23.38 ± 0.90(Oleic acid)(Z)-11-Octadecenoic acid (C18:1 n-7) .................................................. 0.266 ± 0.017 ..................... 0.255 ± 0.016(Vaccenic acid)(Z,Z)-9,12-Octadecadienoic acid (C18:2 n-6) ......................................... 13.75 ± 0.43 ....................... 13.15 ± 0.41(Linoleic acid)(Z,Z,Z)-9,12,15-Octadecatrienoic acid (C18:3 n-3)............................... 0.031 ± 0.001 ..................... 0.030 ± 0.001(Linolenic acid)Eicosanoic acid (C20:0)........................................................................ 0.739 ± 0.030 ..................... 0.710 ± 0.029(Arachidic acid)(Z)-11-Eicosenoic acid (C20:1 n-9)....................................................... 0.669 ± 0.032 ..................... 0.643 ± 0.031(Gondoic acid)Docosanoic acid (C22:0) .......................................................................... 1.88 ± 0.08 ......................... 1.81 ± 0.08(Behenic acid)Tetracosanoic acid (C24:0)................................................................... 0.808 ± 0.045 ..................... 0.781 ± 0.044
Certified concentration values for elements and tocopherol
Mass fraction (mg/kg) Mass fraction (mg/kg)
Ca ............................................................... 411 ± 18 K.............................................................. 6070 ± 200Cu ........................................................... 4.93 ± 0.15 Na............................................................ 4890 ± 140fe............................................................... 16.4 ± 0.8 Zn.............................................................. 26.3 ± 1.1Mg............................................................. 1680 ± 70 δ -Tocopherol .................................................. 10 ± 3Mn............................................................. 16.0 ± 0.6 γ - + β -Tocopherol...................................... 100 ± 19P ............................................................... 3378 ± 92 α -Tocopherol.............................................. 108 ± 11
Reference values for proximates, caloric content, fatty acids, amino acids, water-soluble vitamins and aflatoxins
3 x 170 g
BCR-599 Ewes'/Goats' curd - Adulteration with cow's milkTwo freeze dried curd materials made from a mixture of ewes’ and goats’ milk intended to detect adulteration bycows’ milk in cheeses made from ewes’ milk, goats’ milk and mixtures of the two.
Unadulterated material 0% cows’ milk
Adulterated material 1% cows’ milk
set (2)
BCR-122 Margarine - VitaminsCertified values
D3 (cholecalciferol).................................0.125 mg/kg
E (tocopherol) ...........................................241 mg/kg
200 g
BCR-492-3 Lyophilized skimmed milk powder - OxytetracyclineSet of BCR-492 and BCR-493
BCR-492
Certified value
Oxytetracyline ............ 307 µg/kg
BCR-493
Certified value
Oxytetracyline ............ <10 µg/kg
set
Meat
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MeatCode Product Unit
LGC7000 Beef/pork meat - Proximates and trace elementsComposed of 45% beef, 10% pork, 10% rusk, 4% fat, 0.5% emulsifier. Made up to 100% with water.
Certified values
Ca ............................. 253 mg/kg Zn .............................14.2 mg/kg Ash......................... 0.78 g/100 gK ............................. 1590 mg/kg Moisture..................66.5 g/100 g Nitrogen ................. 1.96 g/100 gNa ........................... 1360 mg/kg Fat ..........................12.4 g/100 g
200 g
LGC7001 Pork meat - Proximates and trace elementsComposed of 50% pork leg, 12% rusk, 4% chicken fat, 0.5% emulsifier. Made up to 100% with water.
Certified values
Ca ............................. 319 mg/kg Zn .............................12.2 mg/kg Ash......................... 0.90 g/100 gK ............................. 1860 mg/kg Moisture..................68.6 g/100 g Nitrogen ................. 1.97 g/100 gNa ........................... 1510 mg/kg Fat ............................7.8 g/100 g
200 g
LGC7112 Pig liver paste - Trace elementsComposed of 99.5% pig's liver and 0.5% stabiliser.
Certified values
Ca ............................ 48.9 mg/kg K..............................2770 mg/kg P ............................. 3430 mg/kgCd ............................ 0.25 mg/kg Mg .............................167 mg/kg Se ............................ 0.19 mg/kgCo .......................... 0.061 mg/kg Mn ............................3.04 mg/kg Zn............................. 43.0 mg/kgCu ............................. 117 mg/kg Na..............................822 mg/kg
150 g
LGC7150 (RM) Processed meat - Proximates and hydroxyprolineA pork based processed meat.
Assessed values
Moisture ................. 65.3 g/100 g Total fat ...................15.0 g/100g Hydroxyproline ....... 0.17 g/100 gNitrogen ................. 1.78 g/100 g Ash .........................3.37 g/100 g
5 x 250 g
LGC7151 (RM) Processed meat - Proximates, salt and nitrateA pork-based processed meat.
Assessed values
Moisture ................................................ 63.6 g/100 g Ash........................................................ 5.18 g/100 gNitrogen ................................................ 1.93 g/100 g Salt (calculated from chloride content).. 4.32 g/100 gTotal fat................................................. 14.6 g/100 g Nitrate....................................................... 185m g/kg
5 x 250 g
LGC7152 (RM) Processed meat - Proximates, soya and caseinAssessed values
Moisture ................. 61.0 g/100 g Total Fat .................15.0 g/100 gNitrogen ................. 2.38 g/100 g Ash .........................4.67 g/100 g
5 x 250 g
LGC7200 (RM) Beef, raw - Meat speciesRump steak from Scottish Aberdeen Angus cattle, aged 20 months, purchased from an organic farm. The cattlehad been fed grass rich in clover.
This material is intended for use as a reference standard for species identification analytical methods.
The species content of the material was checked using both an immunoassay test and DNA analysis.
Assessed value
Beef - raw.................100 % Beef
Indicative value for moisture
30 g
LGC7201 (RM) Beef, cooked - Meat speciesRump steak from Scottish Aberdeen Angus cattle, aged 20 months, purchased from an organic farm. The cattlehad been fed grass rich in clover.
This material is intended for use as a reference standard for species identification analytical methods.
The species content of the material was checked using both an immunoassay test and DNA analysis.
Assessed value
Beef - cooked...........100 % Beef
Indicative value for moisture
30 g
LGC7202 (RM) Lamb, raw - Meat speciesSuffolk-cross leg of lamb, aged 9 months, was purchased from an organic meat supplier.
This material is intended for use as a reference standard for species identification analytical methods.
The species content of the material was checked using both an immunoassay test and DNA analysis.
Assessed value
Lamb - raw.............100 % Lamb
Indicative value for moisture
30 g
Meat
18 Edition 2003/2004 www.lgcpromochem.com
Code Product Unit
LGC7203 (RM) Lamb, cooked - Meat speciesSuffolk-cross leg of lamb, aged 9 months, was purchased from an organic meat supplier.
This material is intended for use as a reference standard for species identification analytical methods.
The species content of the material was checked using both an immunoassay test and DNA analysis.
Assessed value
Lamb - cooked.......100 % Lamb
Indicative value for moisture
30 g
LGC7204 (RM) Pork, raw - Meat species'Free range' Land Race/Large White Cross pork leg steak, aged approximately 5 months at slaughter, waspurchased from an organic meat supplier.
This material is intended for use as a reference standard for species identification analytical methods.
The species content of the material was checked using both an immunoassay test and DNA analysis.
Assessed value
Pork - raw ............... 100 % Pork
Indicative value for moisture
30 g
LGC7205 (RM) Pork, cooked - Meat species'Free range' Land Race/Large White Cross pork leg steak, aged approximately 5 months at slaughter, waspurchased from an organic meat supplier.
This material is intended for use as a reference standard for species identification analytical methods.
The species content of the material was checked using both an immunoassay test and DNA analysis.
Assessed value
Pork - cooked.......... 100 % Pork
Indicative value for moisture
30 g
LGC7206 (RM) Chicken, raw - Meat species'Free range' Ross whole chickens, aged 42 to 45 days at slaughter, were purchased from an organic meatsupplier.
This material is intended for use as a reference standard for species identification analytical methods.
The species content of the material was checked using both an immunoassay test and DNA analysis.
Assessed value
Chicken - raw.....100 % Chicken
Indicative value for moisture
30 g
LGC7207 (RM) Chicken, cooked - Meat species'Free range' Ross whole chickens, aged 42 to 45 days at slaughter, were purchased from an organic meatsupplier.
This material is intended for use as a reference standard for species identification analytical methods.
The species content of the material was checked using both an immunoassay test and DNA analysis.
Assessed value
Chicken - cooked.............................. 100 % Chicken
Indicative value for moisture
30 g
LGC7208 (RM) Turkey, raw - Meat speciesOrganic turkeys were purchased from a local butcher's shop.
This material is intended for use as a reference standard for species identification analytical methods.
The species content of the material was checked using both an immunoassay test and DNA analysis.
Assessed value
Turkey - raw........................................ 100 % Turkey
Indicative value for moisture
30 g
LGC7209 (RM) Turkey, cooked - Meat speciesOrganic turkeys were purchased from a local butcher's shop.
This material is intended for use as a reference standard for species identification analytical methods.
The species content of the material was checked using both an immunoassay test and DNA analysis.
Assessed value
Turkey - cooked .................................. 100 % Turkey
Indicative value for moisture
30 g
BCR-185R Bovine liver - Trace elementsCertified values
As.............................. 33.0 µg/kg Mn ..........................11.07 mg/kg Zn........................... 138.6 mg/kgCd .............................. 544 µg/kg Pb...............................172 µg/kgCu ............................. 277 mg/kg Se.............................1680 µg/kg
15 g
Meat
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Code Product Unit
BCR-186 Pig kidney - Trace elementsCertified values
As................................. 63 µg/kg Fe ..............................299 mg/kg Pb .............................. 306 µg/kgCd ............................ 2710 µg/kg Hg.............................1970 µg/kg Se .......................... 10300 µg/kgCu ............................ 31.9 mg/kg Mn ..............................8.5 mg/kg Zn.............................. 128 mg/kg
Indicative values for Ca, Cl, Cr, I, K, Mg, Na, Ni, P
15 g
BCR-384 Pork muscle - Major nutrientsCertified values
K ................................. 15.5 g/kg Na.............................2.8 g/100 g Fat.......................... 10.8 g/100 gMg............................... 1.00 g/kg N (Kjeldahl).............13.7 g/100 g Ash at 550°C............ 4.6 g/100 g
Indicative values for Ca, Cl, P
50 g
BCR-487 Pig liver - VitaminsCertified values
B1 (thiamin) ................................................8.6 mg/kg B12 ........................................................... 1.12 mg/kgB2 (riboflavin) .........................................106.8 mg/kg Folate (total) ............................................ 13.3 mg/kgB6 (total pyridoxine)..................................19.3 mg/kg
15 g
BCR-411 Bovine muscle - DiethylstilbestrolCertified value
Diethylstilbestrol.......... >0.5 µg/L
5 g
BCR-412 Bovine muscle - DiethylstilbestrolCertified value
Diethylstilbestrol.......... >0.1 µg/L
5 g
BCR-474/475 Bovine liver - TrenboloneSet of 2 x 2.8 g lyophylised liver powder
Certified values
BCR-474
17alpha-Trenbolone.. <0.5 µg/kg
BCR-475
17alpha-Trenbolone.... 7.6 µg/kg
set
BCR-648-9 Bovine liver - ClenbuterolSet of 2 x 10 g lyophilised bovine liver
Certified values
BCR-648
Clenbuterol ............... <0.5 µg/kg
BCR-649
Clenbuterol ................. 1.2 µg/kg
set
NIST-1577b Bovine liver - Trace elementsCertified values
Ag .......................... 0.039 mg/kg K................................... 0.994 % Pb .......................... 0.129 mg/kgCd ............................ 0.50 mg/kg Mg .............................601 mg/kg Rb ............................ 13.7 mg/kgCa ............................. 116 mg/kg Mn ............................10.5 mg/kg S ...................................0.785 %Cl ..................................0.278 % Mo ..............................3.5 mg/kg Se ............................ 0.73 mg/kgCu ............................. 160 mg/kg Na................................. 0.242 % Sr ........................... 0.136 mg/kgFe.............................. 184 mg/kg P..................................... 1.10 % Zn.............................. 127 mg/kg
Indicative values for Al, As, Br, Co, Hg, Sb, V
50 g
NIST-RM 8414 Bovine muscle powder - Trace elements (not certified)Reference values for Al, As, B, Br, Ca, Cd, Cl, Co, Cr, Cu, Fe, Hg, I, K, Mg, Mn, Mo, N, Na, Ni, P, Pb, Rb, S, Se,Sr, Zn
Indicative values for Ba, Cs, F, Sb, V
2 x 25 g
NIST-1546 Meat homogenate - NutrientsCertified values
Ca .............................................................323 mg/kg Hexadecanoic acid (C16:0)........................ 45.6 g/kgFe.............................................................11.4 mg/kg Octadecenoic acid (C18:1) ........................ 21.7 g/kgNa ...........................................................9990 mg/kg (Z)-9-Octadecanoic acid (C18:0)................ 21.7 g/kgDecanoic acid (C10:0) ..............................0.171 g/kg Eicosanoic acid ....................................... 0.31 5 g/kgDodecanoic acid (C12:0) ..........................0.133 g/kg Cholesterol ............................................... 0.750 g/kgTetradecanoic acid (C14:0) ........................2.53 g/kg
Indicative values for additional fatty acids, proximates, calories, water-soluble vitamins, sucrose, minerals, traceelements
4 x 85 g
Meat
20 Edition 2003/2004 www.lgcpromochem.com
Code Product Unit
NRMGBW08551 Pork liver - Trace elementsCertified values
Al............................... 0.044 µg/g K..................................... 1.15 % Na .................................0.233 %Cd ............................. 0.067 µg/g Mg ................................747 µg/g Pb ............................... 0.54 µg/gCa ................................ 197 µg/g Mn ...............................8.32 µg/g Se ............................... 0.94 µg/gCu ............................... 17.2 µg/g Mo .................................3.8 µg/g Zn................................. 172 µg/gFe..................................0.105 % N................................... 10.86 %
Indicative values for Co, Cr, P
25 g
NRMGBW08552 Pork muscle - Trace elementsCertified values
Br .................................. 6.2 µg/g K................................... 0.813 % P ...................................0.813 %Ca ................................ 147 µg/g Mg ................................988 µg/g Rb ............................... 42.7 µg/gCl ..................................0.187 % Mn ...............................0.48 µg/g Se ............................... 0.49 µg/gCu ............................... 3.88 µg/g N................................... 12.27 % Zn................................ 94.2 µg/gFe................................ 43.6 µg/g Na................................. 0.202 %
Indicative values for Ba, Co, Cr, Cs, Hg, Mo, Pb, Sr
20 g
SMRD 2000 Fresh meat - Proximates and trace elementsCertified values
Ash......................... 2.65 g/100 g Hydroxyproline......0.133 g/100 g K ............................. 1859 mg/kgMoisture ................. 68.8 g/100 g Starch.....................3.85 g/100 g Ca ............................ 70.3 mg/kgFat.......................... 14.3 g/100 g NaCl .......................2.19 g/100 g Fe............................. 6.33 mg/kgNitrogen ................. 1.63 g/100 g Na............................8533 mg/kg P ............................. 1075 mg/kg
190 g
SMRD 2000 Fresh Meat - Proximates and trace elements 6 x 190 g
BCR-430 Pork fat - Organochlorine pesticidesThe sample is a homogeneous pork fat obtained from pigs fed with organochlorine pesticides.
Compound Certified value Uncertaintyµg/g µg/g
HCB ................................................................. 0.392........................ 0.026alpha-HCH ....................................................... 0.140........................ 0.012beta-HCH......................................................... 0.259........................ 0.021gamma-HCH...................................................... 0.50.......................... 0.03beta-Hepo ........................................................ 0.109........................ 0.009Dieldrin............................................................. 0.124........................ 0.011Endrin .............................................................. 0.020........................ 0.004
3 g
BCR-163 Beef/pork fat blend - Fatty acidsThe entire fatty acid (methyl ester) profile was determined but certified values are only given for the majorcomponents (>2%) and indicative values are given for all minor components.
Methyl esters(mass fraction fatty acid methyl ester/total fatty acid methyl ester)Certified values
14:0 n-Tetradecanoic acids .................. 2.29 g/100 g 18:1 n-Octadecenoic acids ................. 38.34 g/100 g16:0 n-Hexadecanoic acid .................. 25.96 g/100 g 18:2 n-Octadecadienoic acids............... 7.05 g/100 g16:1 n-Hexadecanoic acids .................. 2.58 g/100 g 18:3 n-Octadecatrienoic acids ............... 0.86 g/100g18:0 n-Octadecenoic acids ................. 18.29 g/100 g
Sterols(mass fraction in fat)Certified value
Cholesterol........ 133.6 mg/100 g
Indicative values for additional methyl esters of fatty acids
2 amp.
IRMM-444 Pork fat - PCBs (blank)Certified values
PCB 28 ........................ <2 µg/kg PCB 118.......................<2 µg/kg PCB 180 ...................... <2 µg/kgPCB 52 ........................ <2 µg/kg PCB 138.......................<2 µg/kg PCB sum.................... <14 µg/kgPCB 101 ...................... <2 µg/kg PCB 153.......................<2 µg/kg
5 g
IRMM-445 Pork fat - PCBs (low level)Compound Certified value Uncertainty
µg/kg µg/kg
PCB 28 .............................................................. 14.8............................ 1.3PCB 52 .............................................................. 12.9............................ 0.9PCB 101 ............................................................ 12.5............................ 1.2PCB 118 ............................................................ 12.7............................ 1.3PCB 138 ............................................................ 14.6............................ 1.6PCB 153 ............................................................ 13.1............................ 1.1PCB 180 ............................................................ 12.6............................ 0.9PCB sum............................................................... 93............................... 7
5 g
Meat
www.lgcpromochem.com Edition 2003/2004 21
Code Product Unit
IRMM-446 Pork fat - PCB (high level)Compound Certified value Uncertainty
µg/kg µg/kg
PCB 28 .............................................................. 29.6............................ 2.1PCB 52 .............................................................. 25.5............................ 1.8PCB 101 ............................................................... 30............................... 4PCB 118 ............................................................ 30.2............................ 2.7PCB 138 ............................................................... 32............................... 4PCB 153 ............................................................ 30.8............................ 2.4PCB 180 ............................................................ 29.8............................ 2.5PCB sum............................................................. 207............................. 11
5 g
BCR-444 Porcine muscle - Chloramphenicol (blank)Certified value
Chloramphenicol....... <0.2 µg/kg
7 g
BCR-445 Porcine muscle - Chloramphenicol (positive)Certified value
Chloramphenicol......... 8.9 µg/kg
7 g
Fish
22 Edition 2003/2004 www.lgcpromochem.com
FishCode Product Unit
Shellfish
LGC7160 Crab paste - Trace elementsPrepared from frozen crab meat with 40% brown crab meat, 40% white crab meat, 0.5% stabiliser and water.
Certified values
As................................ 11 mg/kg Cu.............................10.4 mg/kg Na ........................... 2170 mg/kgCa ........................... 2150 mg/kg Hg...........................0.096 mg/kg Ni ............................. 0.23 mg/kgCd ............................ 1.85 mg/kg K..............................1980 mg/kg P ............................. 2965 mg/kgCo .......................... 0.059 mg/kg Mg .............................348 mg/kg V ............................ 0.084 mg/kgCr ............................. 0.29 mg/kg Mn ............................1.77 mg/kg Zn............................. 53.6 mg/kg
Indicative values for Al, Mo, Pb, Se, Sr
200 g
BCR-278R Mussel tissue - Trace elementsCertified values
As............................. 6.07 mg/kg Cu.............................9.45 mg/kg Pb ............................ 2,00 mg/kgCd .......................... 0.348 mg/kg Hg...........................0.196 mg/kg Se ............................ 1.84 mg/kgCr ............................. 0.78 mg/kg Mn ............................7.69 mg/kg Zn............................. 83.1 mg/kg
8 g
BCR-668 Mussel tissue - Trace elementsCertified values
Ce ............................ 88.7 mg/kg La .............................80.3 mg/kg Tb............................. 1.62 mg/kgDy............................. 8.88 mg/kg Lu ...........................0.389 mg/kg Th............................. 10.7 mg/kgEr ............................. 4.47 mg/kg Nd.............................54.5 mg/kg Tm.......................... 0.480 mg/kgEu ............................ 2.79 mg/kg Pr..............................12.3 mg/kg U .............................. 55.9 mg/kgGd .......................... 12.95 mg/kg Sm............................11.2 mg/kg Y............................... 58.9 mg/kg
Indicative values for : As, Cd, Co, Cr, Cr, Cs, Ho, Fe, Mo, Sc, Yb and Zn
10 g
BCR-682 Mussel tissue - PCBsCertified values
PCB 28 ..................... 0.30 µg/kg PCB 138......................4.6 µg/kg PCB 170 ................... 0.17 µg/kgPCB 52 ..................... 0.78 µg/kg PCB 149......................5.7 µg/kg PCB 180 ................... 0.77 µg/kgPCB 118 ..................... 2.6 µg/kg PCB 153......................9.2 µg/kg
70 g
BCR-477 Mussel tissue - Butyltin compoundsCompound Certified value Uncertainty
mg/kg mg/kg
Tributyltin (TBT) ................................................. 2.20.......................... 0.19Dibutyltin (DBT) ................................................. 1.54.......................... 0.12Monobutyltin (MBT)............................................ 1.50.......................... 0.28
14 g
NIST-2976 Mussel tissue -Trace elements and methylmercuryCertified values
As.............................................................13.3 mg/kg Pb............................................................ 1.19 mg/kgCd ............................................................0.82 mg/kg Se............................................................ 1.80 mg/kgCu ............................................................4.02 mg/kg Zn............................................................. 137 mg/kgFe..............................................................171 mg/kg Methylmercury (total)................................ 61.0 µg/kg
Indicative values for: Ag, Al, Br, Ca, Ce, Cl, Co, Cr, Cs Eu, K, Mg, Mn, Na, Ni, P, Pb, Rb, S, Sc, Sn, Sr, Th, Tl
25 g
NRMGBW08571 Mussel - Trace elementsCertified values
As.................................. 6.1 µg/g F ...................................221 µg/g Ni ................................ 1.03 µg/gCa .................................0.111 % Hg..............................0.067 µg/g Pb ............................... 1.96 µg/gCd ................................. 4.5 µg/g K................................... 0.424 % Se ............................... 3.65 µg/gCo ............................... 0.94 µg/g Mg ................................ 0.197 % Sr ................................ 12.8 µg/gCr ................................ 0.57 µg/g Mn ...............................10.2 µg/g Zn................................. 138 µg/gCu ................................. 7.7 µg/g Na................................. 0.582 %
Indicative values for Al, Au, Mo, P
12 g
Fish
www.lgcpromochem.com Edition 2003/2004 23
Code Product Unit
NIST-2977 Mussel tissue - Organics and trace elementsStandard Reference Material® NIST-2744 is intended for use in evaluating analytical methods for thedetermination of selected polycyclic aromatic hydrocarbons (PAHs), polychlorinated biphenyl (PCB) congeners,chlorinated pesticides, methylmercury, and inorganic constituents in marine bivalve mollusk tissue and similarmatrices. All the constituents for which certified and reference values are provided are naturally present in thefreeze-dried mussel tissue homogenate.
Certified concentrations for selected PAHs
Mass fraction Mass fractionµg/kg (dry mass basis) µg/kg (dry mass basis)
Fluorene................................................ 10.24 ± 0.43 Benzo(a)pyrene....................................... 8.35 ± 0.72Phenanthrene ........................................... 35.1 ± 3.8 Perylene .................................................. 3.50 ± 0.76Fluoranthene............................................. 38.7 ± 1.0 Benzo(ghi)perylene ................................. 9.53 ± 0.43Pyrene....................................................... 78.9 ± 3.5 Indeno(1,2,3-cd)pyrene........................... 4.84 ± 0.81Benzo(a)anthracene ............................. 20.34 ± 0.78 Dibenzo(a,h)anthracene.......................... 1.41 ± 0.19Benzo(b)fluoranthene ........................... 11.01 ± 0.28 Benzo(b)chrysene ................................... 1.07 ± 0.15Benzo(e)pyrene ........................................ 13.1 ± 1.1 Picene ..................................................... 2.29 ± 0.27
Certified concentrations for selected PCB congeners
Mass fractionµg/kg (dry mass basis)
PCB 8................2,4'-Dichlorobiphenyl ..................................................... 2.1 ± 0.15PCB 18..............2,2’,5-Trichlorobiphenyl ............................................... 2.65 ± 0.30PCB 28..............2,4,4'-Trichlorobiphenyl ............................................... 5.37 ± 0.44PCB 31..............2,4',5-Trichlorobiphenyl ............................................... 3.92 ± 0.24PCB 44..............2,2',3,5'-Tetrachlorobiphenyl ....................................... 3.25 ± 0.63PCB 52..............2,2',5,5'-Tetrachlorobiphenyl ....................................... 8.37 ± 0.54PCB 66..............2,3',4,4'-Tetrachlorobiphenyl ....................................... 3.64 ± 0.32PCB 87..............2,2',3,4,5'-Pentachlorobiphenyl ................................... 2.15 ± 0.10PCB 95..............2,2',3,5,6'-Pentachlorobiphenyl ................................... 5.39 ± 0.59PCB 99..............2,2’,4,4’,5-Pentachlorobiphenyl ................................... 1.59 ± 0.20PCB 101............2,2',4,5,5'-Pentachlorobiphenyl+PCB 90..............2,2’,3,4’,5-Pentachlorobipheny..................................... 11.2 ± 1.2lPCB 105............2,3,3',4,4-Pentachlorobiphenyl .................................... 3,76 ± 0.49PCB 110............2,3,3',4',6-Pentachlorobiphenyl .................................. 4.03 ± .0.20PCB 118............2,3',4,4',5-Pentachlorobiphenyl ..................................... 10.5 ± 1.0PCB 128............2,2',3,3,4,4'-Hexachlorobiphenyl ................................. 2.49 ± 0.28PCB 138............2,2',3,4',5'-Hexachlorobiphenyl+PCB 163............2,3,3',4',5,6-Hexachlorobiphenyl+PCB 164............2,3,3',4',5',6-Hexachlorobiphenyl................................... 16.6 ± 1.6PCB 149............2,2',3,4',5',6-Hexachlorobiphenyl................................. 9.23 ± 0.12PCB 151............2,2',3,4,4',5-Hexachlorobiphenyl ................................. 3.07 ± 0.18PCB 153............2,2',4,4',5,5'-Hexachlorobiphenyl................................... 14.1 ± 1.0PCB 156............2,3,3',4,4',5-Hexachlorobiphenyl ............................. 0.960 ± 0.085PCB 170............2,2',3,3',4,4',5-Heptachlorobiphenyl ............................ 2.95 ± 0.23PCB 180............2,2',3,4,4',5,5'-Heptachlorobiphenyl ............................ 6.79 ± 0.67PCB 183............2,2',3,4,4',5',6-Heptachlorobiphenyl ............................ 1.33 ± 0.10PCB 187............2,2',3,4,5,5',6-Heptachlorobiphenyl+PCB 159............2,3,3',4,5,5'-Hexachlorobiphenyl+PCB 182............2,2',3',4,4',5,6'-Hexachlorobiphenyl ............................. 4.76 ± 0.38PCB 194............2,2',3,3',4,4',5,5'-Octachlorobiphenyl....................... 0.897 ± 0.042
Certified concentrations for selected chlorinated pesticides
Mass fraction Mass fractionµg/kg (dry mass basis) µg/kg (dry mass basis)
cis-Chlordane (alpha-Chlordane)............ 1.42 ± 0.13 2,4'-DDD ................................................. 3.32 ± 0.29trans-Nonachlor ...................................... 1.43 ± 0.10 4,4’-DDD ................................................. 4.30 ± 0.38Dieldrin.................................................... 6.04 ± 0.52 4,4'-DDT.................................................. 1.28 ± 0.184,4’-DDE ................................................... 12.5 ± 1.6
Certified concentration of methylmercury
Mass fraction
µg/kg (dry mass basis)
Methylmercury........................................... 36.2 ± 1.7
Certified concentration for trace elements
Mass fraction Mass fraction Mass fractionmg/kg (dry mass basis) mg/kg (dry mass basis) mg/kg (dry mass basis)
Cd ........................ 0.179 ± 0.003 Pb.............................2.27 ± 0.13 Ni ........................... 46.06 ± 0.24Cu ............................ 9.42 ± 0.52 Mn ..........................23.93 ± 0.29 Sr ............................... 69.3 ± 4.2
Reference concentrations for PAHs.
Reference concentrations and informational values for inorganic constituents.
10 g
Fish
24 Edition 2003/2004 www.lgcpromochem.com
Code Product Unit
NIST-2978 Mussel tissue - Organics and trace elementsStandard Reference Material® NIST-2978 is intended for use in evaluating analytical methods for thedetermination of selected polycyclic aromatic hydrocarbons (PAHs), polychlorinated biphenyl (PCB) congenersand chlorinated pesticides in marine bivalve mollusk tissue and similar matrices. All the constituents for whichcertified and reference values are provided are naturally present in the freeze-dried mussel tissue.
Certified concentrations for selelcted PAHs
Mass fraction Mass fractionµg/kg (dry mass basis) µg/kg (dry mass basis)
Fluoranthene............................................... 166 ± 12 Perylene .................................................. 4.09 ± 0.32Pyrene......................................................... 256 ± 21 Benzo(ghi)perylene .................................. 19.7 ± .4.4Benzo(k)fluoranthene ............................... 24.1 ± 3.4 Indeno(1,2,3-cd)pyrene............................. 12.2 ± 2.9Benzo(e)pyrene ........................................ 89.3 ± 6.3
Certified concentrations for selected PCB congeners Mass fraction(µg/kg (dry mass basis)
PCB 28..............2,4,4'-Trichlorobiphenyl ............................................... 7.91 ± 0.90PCB 31..............2,4',5-Trichlorobiphenyl ............................................. 21.40 ± 0.43PCB 44..............2,2',3,5'-Tetrachlorobiphenyl ..................................... 11.80 ± 0.64PCB 49..............2,2’,4,5’-Tetrachlorobiphenyl ..................................... 16.84 ± 0.86PCB 52..............2,2',5,5'-Tetrachlorobiphenyl ......................................... 17.7 ± 2.8PCB 66..............2,3',4,4'-Tetrachlorobiphenyl ......................................... 18.4 ± 1.5PCB 87..............2,2',3,4,5'-Pentachlorobiphenyl ................................... 10.2 ± 0.29PCB 95..............2,2',3,5,6'-Pentachlorobiphenyl ..................................... 20.8 ± 2.1PCB 99..............2,2’,4,4’,5-Pentachlorobiphenyl ................................. 18.84 ± 0.44PCB 101............2,2',4,5,5'-Pentachlorobiphenyl+PCB 90..............2,2’,3,4’,5-Pentachlorobiphenyl ..................................... 35.9 ± 1.6PCB 105............2,3,3',4,4-Pentachlorobiphenyl .................................. 10.85 ± 0.45PCB 110............2,3,3',4',6-Pentachlorobiphenyl ................................. 35.34 ± 0.71PCB 118............2,3',4,4',5-Pentachlorobiphenyl ..................................... 35.1 ± 1.0PCB 128............2,2',3,3,4,4'-Hexachlorobiphenyl ................................. 5.25 ± 0.17PCB 138............2,2',3,4,4',5'-Hexachlorobiphenyl+PCB 163............2,3,3',4',5,6-Hexachlorobiphenyl+PCB 164............2,3,3',4',5',6-Hexachlorobiphenyl................................... 35.7 ± 1.5PCB 149............2,2',3,4',5',6-Hexachlorobiphenyl............................... 34.73 ± 0.69PCB 151............2,2',3,4,4',5-Hexachlorobiphenyl ............................... 10.92 ± 0.25PCB 153............2,2',4,4',5,5'-Hexachlorobiphenyl................................... 56.9 ± 3.5PCB 156............2,3,3',4,4',5-Hexachlorobiphenyl ................................. 1.97 ± 0.11PCB 180............2,2',3,4,4',5,5'-Heptachlorobiphenyl ............................ 7.81 ± 0.63PCB 183............2,2',3,4,4',5',6-Heptachlorobiphenyl ............................ 5.25 ± 0.15PCB 187............2,2',3,4,5,5',6-Heptachlorobiphenyl+PCB 159............2,3,3',4,5,5'-Hexachlorobiphenyl+PCB 182............2,2',3',4,4',5,6'-Heptachlorobiphenyl.............................. 16.7 ± 1.3
Certified concentrations for selected chlorinated pesticides
Mass fraction Mass fractionµg/kg (dry mass basis) µg/kg (dry mass basis)
Oxychlordane.......................................... 2.13 ± 0.27 2,4’-DDE ................................................. 4.41 ± 0.56cis-Chlordane (alpha-Chlordane).......... 15.56 ± 0.83 4,4’-DDE ................................................... 37.5 ± 1.5trans-Chlordane (gamma-Chlordane)... 11.38 ± 0.56 2,4'-DDD ................................................... 10.5 ± 1.0cis-Nonachlor.......................................... 8.23 ± 0.56 4,4’-DDD ................................................... 38.8 ± 2.3trans-Nonachlor ........................................ 11.5 ± 1.0 2,4'-DDT...................................................... 9.2 ± 1.6Dieldrin...................................................... 6.3 ± 0.67 4,4'-DDT.................................................. 3.84 ± 0.28
Reference concentrations PAHs and PCBs
10 g
BCR-542 Mussel - dc-SaxitoxinCompound Certified value Uncertainty
(mg/kg) (mg/kg)
Saxitotin·2HCl .................................................. <0.07DC-Saxitoxin·2HCl............................................. 1.59.......................... 0.20
These reference materials are “dual usage” materials and require special export/import documents under theauthority of IRMM.
15 g
BCR-543 Mussel - dc-SaxitoxinMussel material BCR-543 is intended to serve as an analytical blank or as a material enriched with the saxitoxinenrichment solution (*BCR-663). As an analytical blank it may serve- to establish recovery values for a method of analysis at various levels of contamination- to check the specific background level of the laboratories methods.BCR-543 enriched with saxitoxin enrichent solution (*BCR-663) may be used to validate the laboratory’s ownmethods.
Compound Certified value Uncertainty(mg/kg) (mg/kg)
Saxitoxin·2HCl ................................................. <0.07Saxitoxin·2HCl ................................................... 0.48.......................... 0.06DC-Saxitoxin·2HCl........................................... <0.04
These reference materials are “dual usage” materials and require special export/ import documents under theauthority of IRMM.
*BCR-663 cannot yet be sold as it is restricted by the Chemical Weapon Convention.
15 g
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www.lgcpromochem.com Edition 2003/2004 25
Code Product Unit
NRCCRM-MUS-b Mussel tissue - Domoic acid (amnesic toxin)A homogenized slurry of mussel tissue (Mytilus edulis).
Certified values
Domoic acid ................... 36 µg/gEpidomoic acid ............. 3.0 µg/g
8 g
NRCCRM-MUS-b Mussel tissue - Domoic acid (amnesic toxin) 4 x 8 g
NRMGBW08572 Prawn - Trace elementsCertified values
Al...................................0.131 % F ..................................5.31 µg/g Na .................................0.381 %As................................ 1.42 µg/g Fe ................................19.8 µg/g P ...................................0.845 %Ba ............................... 4.29 µg/g Hg..............................0.201 µg/g Pb ............................. 0.298 µg/gCa .................................0.304 % K................................... 0.597 % Se ............................... 1.52 µg/gCd ............................. 0.023 µg/g Mg ................................ 0.160 % Sr ................................ 40.6 µg/gCr ................................ 0.24 µg/g Mn ...............................1.96 µg/g Zn................................ 60.8 µg/gCu ............................... 4.66 µg/g N..................................... 14.3 %
Indicative values for Br, Co, S, Ti
8 g
NIST-1566b Oyster Tissue - Trace elements and methyl mercuryThis Standard Reference Material® (SRM®) is intended primarily for use in evaluating analytical methods andinstruments used for the determination of the concentrations of selected elements and proximates, selected fattyacids, total dietary fiber, as well as the calorific content in marine bivalve tissue, foods, or similar materials. A unitof NIST-1566b contains approximately 25 g of freeze-dried oyster tissue.
Certified values
Ca ............................................... 0.0838 ± 0.0020 % Pb............................................. 0.308 ± 0.009 mg/kgCl ................................................... 0.514 ± 0.010 % Mn .................................................. 18.5 ± 0.2 mg/kgMg............................................... 0.1085 ± 0.0023 % Hg (total) .............................. 0.0371 ± 0.0013 mg/kgK ..................................................... 0.652 ± 0.009 % Methylmercury (as Hg) ......... 0.0132 ± 0.0007 mg/kgNa ............................................... 0.3297 ± 0.0053 % Ni.................................................. 1.04 ± 0.09 mg/kgS ................................................. 0.6887 ± 0.0140 % Rb............................................. 3.262 ± 0.145 mg/kgAl...................................................197.2 ± 6.0 mg/kg Se................................................. 2.06 ± 0.15 mg/kgAs..................................................7.65 ± 0.65 mg/kg Ag............................................. 0.666 ± 0.009 mg/kgCd .................................................2.48 ± 0.08 mg/kg Th......................................... 0.0367 ± 0.0043 mg/kgCo .............................................0.371 ± 0.009 mg/kg V............................................... 0.577 ± 0.023 mg/kgCu ...................................................71.6 ± 1.6 mg/kg Zn.................................................. 1 424 ± 46 mg/kgFe..................................................205.8 ± 6.8 mg/kg
Indicative values for proximates, nitrogen, total dietary fiber, selected fatty acids (as triglycerides) and calories
25 g
NRCLUTS-1 Non-defatted Lobster Hepatopancreas - Trace elements and methyl mercuryPrepared from edible grade lobster tomalley. Except for the addition of some water and a small quantity ofantioxidant the sample is natural biological material containing 55 % lipids on a dry weight basis.
Certified values (As bottled)
Ag ..........................................................0.580 mg/kg K............................................................... 948 mg/kgAs.............................................................2.83 mg/kg Mg ........................................................... 89.5 mg/kgCa .............................................................203 mg/kg Mn ........................................................... 1.20 mg/kgCd ............................................................2.12 mg/kg Ni........................................................... 0.200 mg/kgCo ..........................................................0.051 mg/kg Pb.......................................................... 0.010 mg/kgCr ...........................................................0.079 mg/kg Se.......................................................... 0.641 mg/kgCu ............................................................15.9 mg/kg Sr............................................................. 2.46 mg/kgFe.............................................................11.6 mg/kg Zn............................................................ 12.4 mg/kgHg ........................................................0.0167 mg/kg Methylmercury (as Hg) ........................ 0.0094 mg/kg
Certified values (Dry weight)
Ag ............................................................3.89 mg/kg K............................................................. 6360 mg/kgAs.............................................................19.0 mg/kg Mg ............................................................ 601 mg/kgCa ...........................................................1360 mg/kg Mn ........................................................... 8.02 mg/kgCd ............................................................14.2 mg/kg Ni............................................................. 1.34 mg/kgCo ............................................................0.34 mg/kg Pb.......................................................... 0.069 mg/kgCr .............................................................0.53 mg/kg Se............................................................ 4.30 mg/kgCu .............................................................107 mg/kg Sr............................................................. 16.5 mg/kgFe.............................................................77.8 mg/kg Zn............................................................ 82.9 mg/kgHg ..........................................................0.112 mg/kg Methylmercury (as Hg) .......................... 0.063 mg/kg
6 x 10 g
NRCTORT-2 Lobster hepatopancreas - Trace elements and methyl mercuryPartially defatted lobster (Homarus americanus) hepatopancreas prepared from edible grade lobster tomalley.
Certified values
As.............................................................21.6 mg/kg Mo ........................................................... 0.95 mg/kgCd ............................................................26.7 mg/kg Ni............................................................. 2.50 mg/kgCo ............................................................0.51 mg/kg Pb............................................................ 0.35 mg/kgCr .............................................................0.77 mg/kg Se............................................................ 5.63 mg/kgCu .............................................................106 mg/kg Sr............................................................. 45.2 mg/kgFe..............................................................105 mg/kg V.............................................................. 1.64 mg/kgHg ............................................................0.27 mg/kg Zn............................................................. 180 mg/kgMn............................................................13.6 mg/kg Methylmercury (as Hg) .......................... 0.152 mg/kg
Indicative values for Sn
35 g
Fish
26 Edition 2003/2004 www.lgcpromochem.com
Code Product Unit
Shellfish toxins
Not all hazardous substances found in foodstuffs are anthropogenic, and the shellfish toxins are acase in point. These toxins, which are produced by algae, accumulate in various seafoods, and aregenerally classified as follows:Paralytic shellfish poisoning (PSP), has been known for centuries, and has caused many fatalities.The toxins, a mixture of tetrahydropurines are named Saxitoxins after the basic toxin first isolated in1957. They cause respiratory paralysis.
The toxins Okadaic acid and Dinophysistoxin are less dangerous and are known as Diarrehticshellfish poisons or DSP toxins.
In 1989 Quilliam and Wright reported on the difficulties of isolating and identifying the cause of the„Prince-Edward-Island-Disease“. In this case more than 100 people became violently ill after eatingmussels. The survivors suffered from loss of memory. The toxin - Domoic acid - is known to be anAmnesic shellfish poison (ASP).
Diarrhetic shellfish poisons (DSP)
NRCCRM-OA-b Okadaic acid standard solution certifiedEach ampoule contains approximately 0.5 mL of solution with 30.0 ± 0.9 µmoles/L (at 20 °C) of Okadaic acid inmethanol.
0.5 mL
NRCCRM-OA-b Okadaic acid standard solution certified 4 x 0.5 mL
Paralytic shellfish poisons (PSP)
NRCCRM-STXdiAc Saxitoxin diacetate solutionEach ampoule contains approximately 0.2 mL of solution with 480 ± 20 µmoles/L of saxitoxin diacetate in filteredand aqueous 0.1M acetic acid.
0.2 mL
NRCCRM-STXdiAc Saxitoxin diacetate solution 4 x 0.2 mL
NRCCRM-STX-d Saxitoxin dihydrochloride solutionEach ampoule contains approximately 0.5 mL of solution with 65 ± 3 µmoles/L (at 20°C) of saxitoxin in filtered andaqueous 0.003 M hydrochloric acid.
0.5 mL
NRCCRM-STX-d Saxitoxin dihydrochloride solution 4 x 0.5 mL
NRCCRM-dcSTX Decarbamoylsaxitoxin solutionEach ampoule contains approximately 0.5 mL of solution with 65 ± 2 µmoles/L (at 20°C) of decarbamoylsaxitoxinin filtered and aqueous 0.003 M hydrochloric acid.
0.5 mL
NRCCRM-dcSTX Decarbamoylsaxitoxin solution 4 x 0.5 mL
NRCCRM-NEO-b Neosaxitoxin solutionEach ampoule contains approximately 0.5 mL of solution with 65 ± 2 µmoles/L (at 20°C) of neosaxitoxin in filteredand aqueous 0.003 M hydrochloric acid.
0.5 mL
NRCCRM-NEO-b Neosaxitoxin solution 4 x 0.5 mL
NRCCRM-GTX14b Gonyautoxins-1 and -4 solutionEach ampoule contains approximately 0.5 mL of solution with 106 ± 5 µmoles/L (at 20°C) of GTX1 and 35 ± 2µmoles/L (at 20°C) of GTX4 in filtered and aqueous 0.003 M hydrochloric acid plus 0.01 M acetic acid.
0.5 mL
NRCCRM-GTX14b Gonyautoxins-1 and -4 solution 4 x 0.5 mL
NRCCRM-GTX23b Gonyautoxins-2 and -3 solutionEach ampoule contains approximately 0.5 mL of solution with 118 ± 5 µmoles/L (at 20°C) of GTX2 and 39 ± 2µmoles/L (at 20°C) of GTX3 in filtered and aqueous 0.003 M hydrochloric acid plus 0.01 M acetic acid.
0.5 mL
NRCCRM-GTX23b Gonyautoxins-2 and -3 solution 4 x 0.5 mL
NRCCRM-GTX5b Gonyautoxins-5 solutionEach ampoule contains approximately 0.5 mL of solution with 65 ± 3 µmoles/L (at 20°C) of GTX5 in filtered andaqueous acetic acid.
0.5 mL
NRCCRM-GTX5b Gonyautoxins-5 solution 4 x 0.5 mL
Fish
www.lgcpromochem.com Edition 2003/2004 27
Code Product Unit
Amnesic shellfish poisons (ASP)
NRCCRM-DA-d Domoic acid solutionSolvent: Acetonitrile/Water (1:9, v/v)
Certified values
Domoic acid +............. 89 ± 0.9 µg/g...............87.7 ± 0.9 µg/mL (at 22°C)............ µmoles/L (at 22°C)Epidomoic acid
Pure domoic acid in solution has been found to gradually isomerize, especially to the C5’-diastereomer, epidomoicacid; therefore, a mixture will inevitably result on long-term storage of any standard.
The densitiy of the solution is 0.9853 at 22°C.
0.5 mL
NRCCRM-DA-d Domoic acid solution 4 x 0.5 mL
Fish
28 Edition 2003/2004 www.lgcpromochem.com
Code Product Unit
Fish
LGC7101 Mackerel paste - Proximates and nutrientsPrepared from whole mackerel fillets (including skin) mixed with water and 2% sodium caesinate.Certified values
Cl ............................ 1500 mg/kg Moisture...................64.5 g/100g Ash......................... 0.83 g/100 gK ............................. 1850 mg/kg Nitrogen...................2.25 g/100gNa ........................... 1320 mg/kg Total fat ...................20.4 g/100g
Indicative values for Ca, Mg, P, Zn
200 g
BCR-422 Cod muscle - Trace elements and methyl mercuryCertified values
As............................. 21.1 mg/kg Hg...........................0.559 mg/kg Se ............................ 1.63 mg/kgCd .......................... 0.017 mg/kg I ................................4.95 mg/kg Zn............................. 19.6 mg/kgCu ............................ 1.05 mg/kg Mn ..........................0.543 mg/kgFe............................. 5.46 mg/kg Pb...........................0.085 mg/kg
7 g
BCR-463 Tuna fish - Total mercury and methyl mercuryCertified values
Methylmercury.......... 3.04 mg/kgTotal mercury........... 2.85 mg/kg
15 g
BCR-464 Tuna fish - Total mercury and methyl mercuryCertified values
Methylmercury.......... 5.50 mg/kgTotal mercury........... 5.24 mg/kg
15 g
BCR-349 Cod liver oil - PCBsCompound Certified value Uncertainty
µg/kg µg/kg
PCB 28 ................................................................. 68............................... 7PCB 52 ............................................................... 149............................. 20PCB 101 ............................................................. 370............................. 17PCB 118 ............................................................. 454............................. 31PCB 153 ............................................................. 938............................. 40PCB 180 ............................................................. 280............................. 22
Indicative values for PCB 44, PCB 128, PCB 138+PCB 163, PCB 194
2 g
BCR-598 Cod liver oil - Organochlorine pesticidesCompound Certified Value Uncertainty
µg/kg µg/kg
Hexachlorobenzene........................................... 55.7............................... 2alpha-HCH ............................................................ 42............................... 3beta-HCH.............................................................. 16............................... 3gamma-HCH......................................................... 23............................... 4gamma-Chlordane............................................... 6.9............................ 1.6alpha-Chlordane ................................................ 24.4............................ 1.8Oxychlordane........................................................ 11............................ 1.8trans-Nonachlor .................................................... 39............................... 4Dieldrin.................................................................. 59............................... 44,4’-DDE ................................................... 0.61 x 103................. 0.04 x 103
2,4’-DDD ............................................................... 30............................... 44,4’-DDD ................................................... 0.40 x 103................. 0.03 x 103
4,4’-DDT ................................................. 0.179 x 103............... 0.018 x 103
5 g
BCR-350 Mackerel oil - PCBsCompound Certified value Uncertainty
µg/kg µg/kg
PCB 28 .............................................................. 22.5............................ 4.0PCB 52 ................................................................. 62............................... 9PCB 101 ............................................................. 164............................... 9PCB 118 ............................................................. 142............................. 20PCB 153 ............................................................. 317............................. 20PCB 180 ............................................................... 73............................. 13
Indicative values for PCB44, PCB128, PCB138+PCB163
2 g
BCR-719 Canned fresh chub - PCBsThe material consists of approx. 70 g of minced sterilised muscle of chub to which butylhydroxy toluene (BHT)was added as an antioxidant.
Certified values
PCB 77 .......... 0.196 x 103 ng/kg PCB 126....................20.0 ng/kgPCB 81 ..................... 13.6 ng/kg PCB 169....................1.80 ng/kg
70 g
Fish
www.lgcpromochem.com Edition 2003/2004 29
Code Product Unit
BCR-718 Canned fresh herring - PCBsThe material consists of approx. 70 g of minced sterilised muscle of herring to which butylhydroxy toluene (BHT)was added as an antioxidant.
Certified values
PCB 28 ..................... 0.41 µg/kg PCB 118....................1.78 µg/kg PCB 153 ................... 4.62 µg/kgPCB 52 ..................... 1.00 µg/kg PCB 128....................0.62 µg/kg PCB 156 ................... 0.19 µg/kgPCB 101 ................... 2.12 µg/kg PCB 138....................2.97 µg/kg PCB 170 ................... 0.35 µg/kgPCB 105 ................... 0.63 µg/kg PCB 149....................2.58 µg/kg PCB 180 ................... 0.80 µg/kg
70 g
BCR-627 Tuna fish tissue - As speciesCertified values
Arsenobetaine..........................................52 µmol/kg total As ...................................................... 4.8 mg/kgDimethylarsinic acid...................................2 µmol/kg
see also arsenobetaine standard solution (BCR-626)
10 g
MURST-ISS-A2 Antarctic krill - Trace elementsPrepared from three catches made by Italian, American and Japanese expeditions.
Certified values
As............................. 5.02 mg/kg Fe .............................56.6 mg/kg Se ............................ 7.37 mg/kgCd ............................ 0.73 mg/kg Mn ............................4.12 mg/kg Zn............................. 66.0 mg/kgCo .......................... 0.110 mg/kg Ni ..............................1.28 mg/kgCu ............................ 65.2 mg/kg Pb.............................1.11 mg/kg
Indicative values for Ag, Al, Br, Ca, Cl, Cr, Hg, I, K, Mg, Na, Rb, Sc, Sn, Sr, V
0.5 g
NIST-1588a Cod liver oil - OrganicsSet of 5 x 1.2 mL
This Standard Reference Material® (SRM®) is intended for use in developing and validating analytical methods forthe determination of chlorinated biphenyls and chlorinated pesticides in cod liver oil or in other similar lipophilicmatrices. The certified values for the PCB congeners and the chlorinated pesticides are based on the agreementof results from two or more independent analytical techniques. NIST-1588 was analysed for selected PCBcongeners and chlorinated pesticides using gas chromatography with electron capture detector (GC-ECD) on twocolumns with different selectivity and using GC with mass spectrometry (GC/MS). The concentration of alpha-tocopherol was determined using two methods based on normal-phase and reversed phase liquidchromatography. Fluorescence detection was used for both methods.
Certified concentrations (mass fractions) for selected PCB congeners
µg/kg
PCB 28 ................2,4,4'-Trichlorobiphenyl ............................................. 28.32 ± 0.55PCB 31 ................2,4',5-Trichlorobiphenyl ............................................... 8.33 ± 0.28PCB 44 ................2,2',3,5'-Tetrachlorobiphenyl ......................................... 35.1 ± 1.4PCB 49 ................2,2',4,5'-Tetrachlorobiphenyl ..................................... 29.90 ± 0.84PCB 52 ................2,2',5,5'-Tetrachlorobiphenyl ......................................... 83.3 ± 2.3PCB 66 ................2,3',4,4'-Tetrachlorobiphenyl ......................................... 54.7 ± 1.5PCB 87 ................2,2',3,4,5'-Pentachlorobiphenyl ..................................... 56.3 ± 1.1PCB 95 ................2,2',3,5,6'-Pentachlorobiphenyl ..................................... 36.5 ± 1.1PCB 101 ..............2,2',4,5,5'-Pentachlorobiphenyl ................................... 126.5 ± 4.3PCB 105 ..............2,3,3',4,4-Pentachlorobiphenyl ...................................... 60.2 ± 2.3PCB 110 ..............2,3,3',4',6-Pentachlorobiphenyl ..................................... 76.0 ± 2.0PCB 118 ..............2,3',4,4',5-Pentachlorobiphenyl ................................... 176.3 ± 3.8PCB 128 ..............2,2',3,3,4,4'-Hexachlorobiphenyl ................................... 47.0 ± 2.4PCB 138 ..............2,2',3,4',5'-Hexachlorobiphenyl+PCB 163 ..............2,3,3',4',5,6-Hexachlorobiphenyl+PCB 164 ..............2,3,3',4',5',6-Hexachlorobiphenyl................................... 263.5±9.1PCB 149 ..............2,2',3,4',5',6-Hexachlorobiphenyl................................. 105.7 ± 3.6PCB 151 ..............2,2',3,4,4',5-Hexachlorobiphenyl ................................... 54.8 ± 2.1PCB 153 ..............2,2',4,4',5,5'-Hexachlorobiphenyl................................. 273.8 ± 7.7PCB 156 ..............2,3,3',4,4',5-Hexachlorobiphenyl ................................... 27.3 ± 1.8PCB 170 ..............2,2',3,3',4,4',5-Heptachlorobiphenyl .............................. 46.5 ± 1.1PCB 180 ..............2,2',3,4,4',5,5'-Heptachlorobiphenyl ............................ 105.0 ± 5.2PCB 183 ..............2,2',3,4,4',5',6-Heptachlorobiphenyl .......................... 31.21 ± 0.62PCB 187 ..............2,2',3,4,5,5',6-Heptachlorobiphenyl+PCB 159 ..............2,3,3',4,5,5'-Hexachlorobiphenyl+PCB 182 ..............2,2',3',4,4',5,6'-Hexachlorobiphenyl ........................... 35.23 ± 0.83PCB 194 ..............2,2',3,3',4,4',5,5'-Octachlorobiphenyl......................... 15.37 ± 0.61PCB 201 ..............2,2',3,3',4,4',5,5',6-Nonachlorobiphenyl..................... 12.18 ± 0.46
Certified concentrations (mass fractions) for selected chlorinated pesticides
µg/kg µg/kg
2,4'-DDE ................................................... 22.0 ± 1.0 gamma-HCH............................................. 24.9 ± 1.74,4'-DDE ..................................................... 651 ± 11 alpha-HCH ................................................ 85.3 ± 3.42,4'-DDD ................................................... 36.3 ± 1.4 Heptachlor epoxide ................................... 31.6 ± 1.54,4'-DDD ..................................................... 254 ± 11 cis-Chlordane.......................................... 167.0 ± 5.02,4'-DDT.................................................. 156.0 ± 4.4 cis-Nonachlor ............................................ 94.8 ± 2.84,4'-DDT...................................................... 524 ± 12 trans-Nonachlor....................................... 214.6 ± 7.9Hexachlorobenzene................................ 157.8 ± 5.0 Dieldrin.................................................... 155.9 ± 4.5
Reference concentration (mass fraction) for alpha-tocopherol and additional PCB congeners.
Information concentrations (mass fractions) for dibenzo-p-dioxins and octachlorodibenzofuran.
set (5)
Fish
30 Edition 2003/2004 www.lgcpromochem.com
Code Product Unit
NIST-1946 Lake Superior fish tissue - Organic contaminantsThis Standard Reference Material (SRM) is a frozen fish tissue homogenate, which was prepared from laketrout (Salvelinus namaycush namaycush) collected from Lake Superior (U.S./Canada), and is intended primarilyfor use in evaluating analytical methods for the determination of polychlorinated biphenyl (PCB) congeners,chlorinated pesticides, fatty acids (including omega-3 fatty acids), extractable fat, methylmercury, total mercuryand selected trace elements in fish tissue and similar matrices.
Certified concentrations for selected PCB congeners Mass fractionµg/kg (dry mass basis)
PCB 44..............2,2',3,5'-Tetrachlorobiphenyl ....................................... 4.66 ± 0.86PCB 49..............2,2',4,5'-Tetrachlorobiphenyl ........................................ 3.80 ±0.39PCB 52..............2,2',5,5'-Tetrachlorobiphenyl ........................................... 8.1 ± 1.0PCB 66..............2,3',4,4'-Tetrachlorobiphenyl ......................................... 10.8 ± 1.9PCB 70..............2,3',4',5-Tetrachlorobiphenyl ......................................... 14.9 ± 0.6PCB 74..............2,4,4',5-Tetrachlorobiphenyl ........................................ 4.83 ± 0.51PCB 77..............3,3',4,4'-Tetrachlorobiphenyl ................................... 0.327 ± 0.025PCB 87..............2,2',3,4,5'-Pentachlorobiphenyl ....................................... 9.4 ± 1.4PCB 95..............2,2',3,5',6-Pentachlorobiphenyl ..................................... 11.4 ± 1.3PCB 99..............2,2',4,4',5-Pentachlorobiphenyl ..................................... 25.6 ± 2.3PCB 101............2,2',4,5,5'-Pentachlorobiphenyl ..................................... 34.6 ± 2.6PCB 105............2,3,3',4,4'-Pentachlorobiphenyl ..................................... 19.9 ± 0.9PCB 110............2,3,3',4',6-Pentachlorobiphenyl ..................................... 22.8 ± 2.0PCB 118............2,3',4,4',5-Pentachlorobiphenyl ..................................... 52.1 ± 1.0PCB 126............3,3',4,4',5-Pentachlorobiphenyl ............................... 0.380 ± 0.017PCB 128............2,2',3,3',4,4'-Hexachlorobiphenyl................................... 22.8 ± 1.9PCB 138............2,2',3,4,4',5'-Hexachlorobiphenyl..................................... 115 ± 13PCB 146............2,2',3,4',5,5'-Hexachlorobiphenyl................................... 30.1 ± 3.5PCB 149............2,2',3,4',5',6-Hexachlorobiphenyl................................... 26.3 ± 1.3PCB 153............2,2',4,4',5,5'-Hexachlorobiphenyl....................................... 170 ± 9PCB 156............2,3,3',4,4',5-Hexachlorobiphenyl ................................. 9.52 ± 0.51PCB 169............2,2',3,4,4',5'-Hexachlorobiphenyl............................. 0.106 ± 0.014PCB 170............2,2',3,3',4,4',5-Heptachlorobiphenyl .............................. 25.2 ± 2.2PCB 180............2,2',3,4,4',5,5'-Heptachlorobiphenyl .............................. 74.4 ± 4.0PCB 183............2,2',3,4,4',5',6-Heptachlorobiphenyl .............................. 21.9 ± 2.5PCB 187............2,2',3,4',5,5',6-Heptachlorobiphenyl .............................. 55.2 ± 2.1PCB 194............2,2',3,3',4,4',5,5'-Octachlorobiphenyl............................. 13.0 ± 1.3PCB 195............2,2',3,3',4,4',5,6-Octachlorobiphenyl ........................... 5.30 ± 0.45PCB 206............2,2',3,3',4,4',5,5',6-Nonachlorobiphenyl....................... 5.40 ± 0.43PCB 209............Decachlorobiphenyl..................................................... 1.30 ± 0.21
Certified concentrations for selected chlorinated pesticides
Mass fraction Mass fractionµg/kg (wet- mass basis) µg/kg (wet- mass basis)
Hexachlorobenzene................................ 7.25 ± 0.83 trans-Nonachlor......................................... 99.6 ± 7.6alpha-HCH .............................................. 5.72 ± 0.65 Dieldrin...................................................... 32.5 ± 3.5gamma-HCH........................................... 1.14 ± 0.18 Mirex ....................................................... 6.47 ± 0.77Heptachlor epoxide................................. 5.50 ± 0.23 4,4'-DDE...................................................... 373 ± 48Oxychlordane............................................ 18.9 ± 1.5 2,4'-DDD ................................................. 2.20 ± 0.25cis-Chlordane (alpha-Chlordane).............. 32.5 ± 1.8 4,4'-DDD ................................................... 17.7 ± 2.8trans-Chlordane ...................................... 8.36 ± 0.91 4,4'-DDT.................................................... 37.2 ± 3.5cis-Nonachlor............................................ 59.1 ± 3.6
Certified concentrations for fat and selected fatty acids Mass fraction (%)(wet- mass basis)
Fat (Extractable) ............................................................................................ 10.17 ± 0.48Fat (Sum of Fatty Acids) .................................................................................. 8.76 ± 0.17
Mass fraction (%) (as the triglycerdide) (wet- mass basis)
Tetradecanoic acid (C14:0) ......................................................................... 0.316 ± 0.009(Myristic acid)Hexadecanoic acid (C16:0) ............................................................................. 1.22 ± 0.04(Palmitic acid)(Z)-9-Hexadecenoic acid (C16:1)................................................................. 0.816 ± 0.026(Palmitoleic acid)Octadecanoic acid (C18:0) .......................................................................... 0.263 ± 0.011(Stearic acid)(Z)-9-Octadecenoic acid (C18:1) ..................................................................... 2.64 ± 0.08(Oleic acid)c(Z,Z)-9,12-Octadecadienoic acid (C18:2) .................................................... 0.348 ± 0.023(Linoleic acid)(Z,Z,Z)-9,12,15-Octadecatrienoic acid (C18:3)............................................ 0.221 ± 0.025(Linolenic acid)Eicosanoic acid (C20:0)........................................................................... 0.0100 ± 0.0012(Arachidic acid)(Z)-11-Eicosenoic acid (C20:1).................................................................... 0.132 ± 0.012(Z,Z)-11,14-Eicosadienoic acid (C20:2)................................................... 0.0990 ± 0.0043(Z,Z,Z,Z,Z)-5,8,11,14,17-Eicosapentaenoic acid (C20:5) (EPA) ................. 0.296 ± 0.019(Z,Z,Z,Z,Z)-7,10,13,16,19-Docosapentaenoic acid (C22:5) (DPA).............. 0.335 ± 0.026(Z,Z,Z,Z,Z,Z)-4,7,10,13,16,19-Docosahexaenoic acid (C22:6) (DHA)............. 0.92 ± 0.10
Certified concentrations for methylmercury, total mercury, arsenic and iron
Mass fraction Mass fractionmg/kg (wet- mass basis) mg/kg (wet- mass basis)
Methylmercury..................................... 0.394 ± 0.015 As........................................................ 0.277 ± 0.010Hg (Total)............................................ 0.433 ± 0.009 Fe............................................................ 4.00 ± 0.32
Reference concentrations for PCBs, pesticides, fatty acids, proximates and caloric content.
5 x 10 g
Fish
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Code Product Unit
IAEA-352 Tuna fish - Radioactive isotopesCertified values137Cs............................2.7 Bq/kg 210Pb ........................... 0.6 Bq/kg 90Sr..............................0.2 Bq/kg40K..............................391 Bq/kg 210Po ........................... 2.2 Bq/kg
100 g
IAEA-MA-B3/R Fish flesh - Radioactive isotopesCertified values137Cs..........................14.2 Bq/kg 40K ............................. 272 Bq/kg
50 g
NRCDOLT-3 Dogfish liver - Trace elementsCertified values
Ag ................. 1.20 ± 0.07 mg/kg Cu....................31.2 ± 1.0 mg/kg Pb ............. 0.319 ± 0.045 mg/kgAl..................... 24.7 ± 1.9 mg/kg Fe ....................1484 ± 57 mg/kg Se ................. 7.06 ± 0.48 mg/kgAs.................... 10.2 ± 0.5 mg/kg Hg..................3.37 ± 0.14 mg/kg Zn.................... 86.6 ± 2.4 mg/kgCd ................... 19.4 ± 0.6 mg/kg Ni ...................2.72 ± 0.35 mg/kg
Indicative value for Cr, Sn, Methylmercury
25 g
NRCDORM-2 Dogfish muscle - Trace elementsCertified values
Ag .......................... 0.041 mg/kg Cr..............................34.7 mg/kg Ni ............................. 19.4 mg/kgAl.............................. 10.9 mg/kg Cu.............................2.34 mg/kg Pb .......................... 0.065 mg/kgAs............................. 18.0 mg/kg Fe ..............................142 mg/kg Se ............................ 1.40 mg/kgCd .......................... 0.043 mg/kg Hg.............................4.64 mg/kg Zn............................. 25.6 mg/kgCo .......................... 0.182 mg/kg Mn ............................3.66 mg/kg Methylmercury.......... 4.47 mg/kg
Indicative values for Sn, Tl
40 g
NRCCARP-2 Fish (common carp) - Dioxins, furans and PCBsPrepared from common carp (Cyprinus carpio) collected near the warm water discharge of the Consumer’s PowerPlant in Saginaw Bay, Lake Huron, Canada
Certified values
PCB18 ...................... 27.3 µg/kg PCB118......................148 µg/kg PCB194 .................... 10.9 µg/kgPCB28 ...................... 34.0 µg/kg PCB128.....................20.4 µg/kg PCB206 ...................... 4.4 µg/kgPCB44 ...................... 86.6 µg/kg PCB153......................105 µg/kgPCB52 ....................... 138 µg/kg PCB180.....................53.3 µg/kg
Reference Values
2,3,7,8-TCDF............................................18.2 ng/kg 1,2,3,6,7,8-HxCDD..................................... 5.8 ng/kg1,2,3,7,8-PCDF...........................................5.6 ng/kg 1,2,3,7,8,9-HxCDD................................... 0.78 ng/kg2,3,7,8-TCDD..............................................7.4 ng/kg 1,2,3,4,6,7,8-HpCDD ................................. 6.4 ng/kg1,2,3,7,8-PCDD ..........................................5.3 ng/kg OCDD ........................................................ 9.4 ng/kg1,2,3,4,7,8-HxCDD .....................................1.6 ng/kg
Other reference concentrations for selected PCB congeners and pesticides are given in the certificate.
6 x 10 g
Cereals and crops
32 Edition 2003/2004 www.lgcpromochem.com
Cereals and cropsCode Product Unit
Wheat
LGC7003 White bread flour - Nutrients and trace elementsCertified values
Ash...................................0.84% Ca............................1120 mg/kg Na ............................... 39 mg/kgFat......................................1.7% Fe ................................23 mg/kg Zn................................ 12 mg/kgN ......................................2.43% K..............................1720 mg/kg
25 g
BCR-189 Wholemeal flour - Trace elementsCertified values
Cd ............................. 71.3 µg/kg Mn ............................63.3 mg/kg Zn............................. 56.5 mg/kgCu .............................. 6.4 mg/kg Pd...............................379 µg/kgFe............................. 68.3 mg/kg Se...............................132 µg/kg
Indicative values for Ca, Cl, Cr, Hg, K, Mg, Na, Ni, P
25 g
NIST-1567a Wheat flour - Trace elementsMilled from a blend of Hard Red Spring and Hard Red Winter wheat.
Certified values
Al................................... 5.7 µg/g K................................... 0.133 % P ...................................0.134 %Ca .................................0.191 % Mg ................................ 0.040 % Rb ............................... 0.68 µg/gCd ............................. 0.026 µg/g Mn .................................9.4 µg/g S ...................................0.165 %Cu ................................. 2.1 µg/g Mo ...............................0.48 µg/g Se ................................. 1.1 µg/gFe................................ 14.1 µg/g Na..................................6.1 µg/g Zn................................ 11.6 µg/g
Indicative values for As, Br, Cl, Co, Hg, I, Pb, Sn, U, V, W
80 g
NIST-RM 8437 Hard red spring wheat flour - Trace elementsReference concentration values for major, minor and trace elements.Indicative values for additional elements.
2 x 25 g
BCR-382 Wheat flour - Major nutrientsCertified values (percentage by dry mass)
Ash.................................................................... 0.9% N (Kjeldahl) .......................................................2.1%Fat..................................................................... 1.3% Dietary fibre (AOAC 1985/1988) .......................3.3%
Indicative values for starch, starch & sugars and dietary fibre (Englyst)
100 g
BCR-121 Wholemeal flour - VitaminsCertified values
B1 (thiamin) .............................................4.63 mg/kg Folate (total) .............................................. 0.5 mg/kgB6 (total pyridoxine) .................................4.10 mg/kg
50 g
BCR-563 Common wheat flour - PropertiesCertified parameters determined according to ISO and ICC standard: Protein content, Ash content, Fallingnumber / s, Zeleny sedimentation, Chopin Alveograph, Brabender Farinograph, Brabender Extensograph.
360 g
NIST-RM 8436 Durum wheat flour - Trace elements and nutritional propertiesReference concentration values for major, minor and trace elements, proximates, total dietary fibre and calories.Indicative values for additional elements and one fatty acid.
50 g
NIST-RM 8437 Hard red spring wheat flour - Trace elementsReference concentration values for major, minor and trace elements.Indicative values for additional elements.
2 x 25 g
NIST-RM 8438 Soft winter wheat flour - Trace elementsReference concentration values for major, minor and trace elements.Indicative values for additional elements
2 x 50 g
NIST-RM 8418 Wheat gluten - Trace elements and nutritional propertiesReference concentration values for major, minor and trace elements, proximates, calories and fatty acid.Indicative values for additional elements fatty acids and total dietary fibre.
50 g
NRMGBW08503 Wheat flour - Trace elementsCertified values
As................................ 0.22 µg/g Fe ................................39.8 µg/g Pb ............................... 0.35 µg/gCa ................................ 441 µg/g K................................... 0.198 % Zn................................ 22.7 µg/gCd ............................. 0.031 µg/g Mg ................................551 µg/gCu ............................... 4.40 µg/g Mn ...............................19.6 µg/g
Indicative values for N, P, Se, Na
20 g
Cereals and crops
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Code Product Unit
BCR-396 Wheat flour - Deoxynivalenol (DON) blankCertified value
DON...................... < 0.05 mg/kg
150 g
BCR-471 Wheat - Ochratoxin A (blank)Certified value
Ochratoxin A ............ < 0.6 µg/kg
55 g
BCR-472 Wheat - Ochratoxin A (medium level)Certified value
Ochratoxin A ............... 8.2 µg/kg
55 g
NIST-RM 8441 Wheat - HardnessSet of 50 x 20 g
Determination of hardness of bulk or single kernel wheat. Ten separate lots of wheat of varying hardness. Fivesamples of each wheat .
set (50)
Corn
BCR-377 Maize flour - Deoxynivalenol (blank)Certified value
DON....................... <0.05 mg/kg
150 g
BCR-378 Maize flour - Deoxynivalenol (medium level)Certified value
DON......................... 0.43 mg/kg
150 g
NIST-RM 8432 Corn starch - Trace elements and nutritional properitiesReference concentration values for major, minor and trace elements, proximates, total dietary fibre and calories.
Indicative values for additional elements, ash and fatty acids.
50 g
NIST-RM 8433 Corn bran - Trace elements and nutritional propertiesReference concentration values for major, minor and trace elements, proximates, total dietary fibre and calories.
Indicative values for additional elements, fat and fatty acids.
50 g
NIST-RM 8412 Corn (Zea Mays) stalk - Trace elementsReference concentration values for major, minor and trace elements. Indicative values for additional elements.
34 g
NIST-RM 8413 Corn (Zea Mays) kernel - Trace elementsReference values for Al, Ca, Cl, Cu, F, I, K, Mg, Mn, N, Se, Zn
47 g
Rye
BCR-381 Rye flour - Major nutrientsCertified values (percentage by dry mass)
Ash.................................................................... 0.9% N (Kjeldahl) .......................................................1.3%Fat..................................................................... 1.1% Dietary fibre (AOAC 1985/1988) .......................8.2%
Indicative values for starch, starch & sugars, dietary fibre (Englyst)
100 g
IAEA-V-8 Rye flour - Trace elementsCertified values
Br ............................. 0.38 mg/kg Fe ...............................4.1 mg/kg P ............................... 592 mg/kgCa ............................. 149 mg/kg K..............................1925 mg/kg Rb ............................ 0.48 mg/kgCl .............................. 570 mg/kg Mg .............................121 mg/kg Zn............................. 2.53 mg/kgCu ............................ 0.95 mg/kg Mn ............................2.06 mg/kg
Indicative values for Cd, Co, Na
50 g
Rice
BCR-465 Rice flour - Amylose (low level)Certified value
Amylose ................. 15.4 g/100 g
10 g
BCR-466 Rice flour - Amylose (medium level)Certified value
Amylose ................. 23.1 g/100 g
10 g
Cereals and crops
34 Edition 2003/2004 www.lgcpromochem.com
Code Product Unit
BCR-467 Rice flour - Amylose (high level)Certified value
Amylose ................. 27.7 g/100 g
10 g
NIST-1568a Rice Flour - Trace elementsProduced from 100% long grain rice from Arkansas.
Certified values
Al................................... 4.4 µg/g Hg....................................0.0058 P ...................................0.134 %As................................ 0.29 µg/g K................................. 0.1280 % Rb ............................... 6.14 µg/gCa ...............................0.0118 % Mg ............................... 0.056 % S ...................................0.120 %Cd ............................. 0.022 µg/g Mn ...............................20.0 µg/g Se ............................... 0.38 µg/gCu ................................. 2.4 µg/g Mo ...............................1.46 µg/g Zn................................ 19.4 µg/gFe.................................. 7.4 µg/g Na..................................6.1 µg/g
Indicative values for Br, Cl, Co, I, Pb, Sb, Sn, U, V, W
80 g
NRMGBW08508 Rice - Trace elementsCertified values
Cu ................................. 3.6 µg/g Fe ................................43.2 µg/g Mg............................... 28.4 µg/gF.................................. 18.0 µg/g Hg..............................0.038 µg/g
40 g
NRMGBW08510 Rice - Trace elementsCertified values
Cu ................................. 3.6 µg/g Fe ................................43.2 µg/g Mg............................... 28.4 µg/gF.................................. 18.0 µg/g Hg..............................0.038 µg/g
40 g
NRMGBW08511 Rice - Cadmium (medium level)Certified value
Cd ............................. 0.504 µg/g
40 g
NRMGBW08512 Rice - Cadmium (low level)Certified value
Cd ........................... 0.0069 µg/g
40 g
Rapeseed
BCR-190R Rapeseed (colza) - Total glucosinolate and sulphurCertified values
Total glucosinolate..................................23 mmol/kg S................................................................. 4.72 g/kg
20 g
BCR-366R Rapeseed (colza) - Total glucosinolate and sulphurCertified values
Total glucosinolate...............................11.9 mmol/kg S................................................................. 3.31 g/kg
20 g
BCR-367R Rapeseed (colza) - Total glucosinolate and sulphurCertified values
Total glucosinolate................................102 mmol/kg S................................................................. 10.5 g/kg
Indicative values for individual glucosinolates
20 g
BCR-446 Rapeseed - Oil content (low)Certified values
“As is” oil ............................................. 39.49 g/100 gMoisture and volatiles ........................... 7.01 g/100 gDry basis oil ........................................ 42.48 g/100 g
153 g
BCR-447 Rapeseed - Oil content (medium)Certified values
“As is” oil ............................................. 41.99 g/100 gMoisture and volatiles ........................... 7.42 g/100 gDry basis oil ........................................ 45.36 g/100 g
153 g
BCR-448 Rapeseed - Oil content (high)Certified values
“As is” oil ............................................. 45.43 g/100 gMoisture and volatiles ........................... 7.68 g/100 gDry basis oil ........................................ 49.21 g/100 g
153 g
Cereals and crops
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Code Product Unit
Genetically modified crops
IRMM-410S0 - IRMM-410S5
Dried soya bean powder with different mass fractions of genetically modified (“Roundup ReadyTM”)soya beans, intended for validation of the polymerase chain reaction (PCR) screening method for thedetection of GM food.
IRMM-410S0 Genetically modified soya beans (0%)Certified mass fraction GMO < 0.03%
1 g
IRMM-410S1 Genetically modified soya beans (0.1%)Certified mass fraction GMO: 0.1 %
1 g
IRMM-410S2 Genetically modified soya beans (0.5%)Certified mass fraction GMO: 0.5%
1 g
IRMM-410S3 Genetically modified soya beans (1%)Certified mass fraction GMO: 1%
1 g
IRMM-410S4 Genetically modified soya beans (2%)Certified mass fraction GMO: 2%
1 g
IRMM-410S5 Genetically modified soya beans (5%)Certified mass fraction GMO: 5%
1 g
IRMM-413-0 - IRMM-413-5
Dried maize powder with different mass fractions (<0.02, 0.1, 0.5, 1, 2, 5 %) of genetically modifiedmaize (MON810), intended for the validation of methods for the detection of genetically modified food.As DNA and/or protein based GMO quantification may depend on varieties, one has to be careful todraw quantitative conclusions from measurements of unknown samples.
IRMM-413-0 Genetically modified MON-810 maize powder (0%)Certified mass fraction GMO <0.02 %
1 g
IRMM-413-1 Genetically modified MON-810 maize powder (0.1%)Certified mass fraction GMO: 0.1% ± 0.03
1 g
IRMM-413-2 Genetically modified MON-810 maize powder (0.5%)Certified mass fraction GMO: 0.50 % ± 0.04
1 g
IRMM-413-3 Genetically modified MON-810 maize powder (1%)Certified mass fraction GMO: 1 % ± 0.05
1 g
IRMM-413-4 Genetically modified MON-810 maize powder (2%)Certified mass fraction GMO: 2% ± 0.1
1 g
IRMM-413-5 Genetically modified MON-810 maize powder (5%)Certified mass fraction GMO: 5% ± 0.2
1 g
Vegetable matter
36 Edition 2003/2004 www.lgcpromochem.com
Vegetable matterCode Product Unit
Fruit and vegetables
LGC7111 Potato powder - Sulphur dioxideCertified value
SO2 ........................ 357.5 mg/kg
200 g
LGC7162 Strawberry leaves - Trace elementsThe raw material was collected from a private farm in the Czech Republic. The mixture was cut and jet milled topass a 250 µm nylon sieve. The resulting powder was homogenised, separated in 20 g portions and placed in60mL bottles.
Certified Values
Ca .......................... 1.53 g/100 g As .............................0.28 mg/kg Pb .............................. 1.8 mg/kgMg........................ 0.377 g/100 g Ba..............................107 mg/kg Mn............................. 171 mg/kgN ............................ 2.01 g/100 g Cd.............................0.17 mg/kg Hg .......................... 0.027 mg/kgP .......................... 0.260 g/100 g Co.............................0.47 mg/kg Ni ............................... 2.6 mg/kgK ............................ 1.96 g/100 g Cr..............................2.15 mg/kg Sr ................................ 64 mg/kgS .......................... 0.174 g/100 g Fe ..............................818 mg/kg Zn................................ 24 mg/kg
20 g
BCR-515 Carrot - Dietary fibreCertified using five different methods of dietary fibre analysis
Certified values
AOAC 1990........................................... 31.1 g/100 g AOAC 1992 MES-TRIS......................... 29.5 g/100 gEnglyst (GC) ......................................... 27.1 g/100 g Englyst (colorimetry) ............................. 25.2 g/100 gUppsala................................................. 29.8 g/100 g
25 g
ARC/CL4 Carrot powder - Total dietary fibre and trace elementsPrepared from normal commercially available carrot flakes used by the Finnish food industry.
Certified values
Total dietary fibre ...........10.93% Fe ................................12.6 µg/g Mo............................... 49.5 ng/gB ................................. 10.1 µg/g K.................................10.2 mg/g Na ................................ 485 µg/gCa .............................. 1700 µg/g Mg ................................350 µg/g Zn.................................. 6.9 µg/gCd ............................... 68.6 ng/g Mn ...............................4.90 µg/g
60 g
BCR-383 Haricots verts (beans) - Major nutrientsCertified values
N(Kjeldahl) .............................................. 1.1 g/100 g Ca............................................................ 2.9 g/100 gDietary fibre (AOAC 1985/1988)........... 11.9 g/100 g K.............................................................. 7.8 g/100 gAsh at 550°C............................................ 2.4 g/100g Na.......................................................... 0.08 g/100 g
Indicative values for glucose, fructose, sucrose, starch + sugars, dietary fibre (Englyst)
100 g
BCR-514 Haricots beans - Dietary fibreCertified using five different methods of dietary fibre analysis
Certified values
AOAC 1990........................................... 25.6 g/100 g AOAC 1992 MES-TRIS......................... 25.9 g/100 gEnglyst (GC) ......................................... 19.8 g/100 g Englyst (colorimetry) ............................. 20.1 g/100 gUppsala................................................. 23.7 g/100 g
25 g
BCR-431 Brussels sprout - VitaminsCertified values
C (total ascorbate) .. 4830 mg/kgNiacin.......................... 43 mg/kg
20 g
BCR-485 Mixed vegetables - VitaminsCertified values
B1 (thiamin) .............. 3.07 mg/kg trans-α-carotene.......10.5 mg/kg total-β-carotene........ 25.6 mg/kgB6 (total pyridoxine).... 4.8 mg/kg trans-β-carotene.......23.7 mg/kg lutein ........................ 12.5 mg/kgfolate (total) .............. 3.15 mg/kg total-α-carotene..........9.8 mg/kg lutein+zeaxanthin..... 22.3 mg/kg
25 g
BCR-517 Full fat soya - Dietary fibreCertified using five different methods of dietary fibre analysis
Certified values
AOAC 1990........................................... 12.6 g/100 g AOAC 1992 MES-TRIS......................... 12.4 g/100 gEnglyst (GC) ......................................... 11.9 g/100 g Englyst (colorimetry) ............................. 12.3 g/100 gUppsala................................................. 12.8 g/100 g
25 g
Vegetable matter
www.lgcpromochem.com Edition 2003/2004 37
Code Product Unit
BCR-516 Apple - Dietary fibreCertified using five different methods of dietary fibre analysis
Certified values
AOAC 1990......................................... 16.46 g/100 g AOAC 1992 MES-TRIS......................... 14.9 g/100 gEnglyst (GC) ......................................... 13.7 g/100 g Englyst (colorimetry) ............................. 13.4 g/100 gUppsala.................................................. 16.2 g/100g
25 g
BCR-679 White cabbage - Trace elementsCertified values
As................................ 7.0 µg/kg Fe ..............................55.0 µg/kg Sr ............................. 11.8 mg/kgB .............................. 27.7 mg/kg Hg................................6.3 µg/kg Tl............................... 2.98 µg/kgBa ............................ 10.3 mg/kg Mo ............................14.8 mg/kg Zn............................. 79.7 mg/kgCd ............................ 1.66 mg/kg Ni ..............................27.0 mg/kgCu ............................ 2.89 mg/kg Sb..............................20.6 µg/kg
15 g
BCR-401 Peanut butter (blank) - Aflatoxin B1Certified values
Aflatoxin B1............... <0.2 µg/kg Aflatoxin G1...............<0.1 µg/kg Total Aflatoxins ......... <0.5 µg/kgAflatoxin B2............... <0.1 µg/kg Aflatoxin G2...............<0.1 µg/kg
50 g
BCR-262 Defatted peanut meal (blank) - Aflatoxin B1Certified value
Aflatoxin B1.................. <3 µg/kg
100 g
BCR-264 Defatted peanut meal (high level) - Aflatoxin B1Certified value
Aflatoxin B1................ 206 µg/kg
150 g
IC-INCT-TL-1 Tea leaves - Trace elementsThe material was prepared from black tea, usually packed in tea bags.
Certified values
Al.............................. 0.229 wt % Eu...........................0,050 mg/kg Sc........................... 0.266 mg/kgAs........................... 0.106 mg/kg Hg...........................0.005 mg/kg Sm ......................... 0.177 mg/kgBa ............................ 43.2 mg/kg K.................................1.70 wt % Sr ............................. 20.8 mg/kgBr ............................. 12.3 mg/kg La .............................1.00 mg/kg Tb........................... 0.026 mg/kgCa ............................ 0.582 wt % Lu ...........................0.016 mg/kg Th........................... 0.034 mg/kgCd .......................... 0.030 mg/kg Mg ............................0.224 wt % Tl............................ 0.063 mg/kgCl .............................. 573 mg/kg Mn ............................0.157 wt % V .............................. 1.97 mg/kgCo .......................... 0.387 mg/kg Na.............................24.7 mg/kg Yb........................... 0.118 mg/kgCr ............................. 1.91 mg/kg Ni ..............................6.12 mg/kg Zn............................. 34.7 mg/kgCs ............................ 3.61 mg/kg Pb.............................1.78 mg/kgCu ............................ 20.4 mg/kg Rb.............................81.5 mg/kg
Indicative values for B, Fe, Hf, Nd, P, Sb, Se, Ta, Ti and Tm
50 g
NRMGBW07605 Tea - Trace elementsCertified values
As................................ 0.28 µg/g Cu................................17.3 µg/g Pb ................................. 4.4 µg/gB .................................... 15 µg/g Eu..............................0.018 µg/g Rb .................................. 74 µg/gBa .................................. 58 µg/g F ...................................320 µg/g S ...................................0.245 %Be ............................. 0.034 µg/g Fe .................................264 µg/g Sb ............................. 0.056 µg/gBi............................... 0.063 µg/g K..................................... 1.66 % Sc.............................. 0.085 µg/gBr .................................. 3.4 µg/g Mg .................................. 0.17 % Sm ............................ 0.085 µg/gCa ...................................0.43 % Mn ..............................1240 µg/g Sr ................................ 15.2 µg/gCd ............................. 0.057 µg/g Mo .............................0.038 µg/g Th.............................. 0.061 µg/gCe ................................. 1.0 µg/g N..................................... 3.32 % Ti.................................... 24 µg/gCo ............................... 0.18 µg/g Na...................................44 µg/g Y.................................. 0.36 µg/gCr .................................. 0.8 µg/g Ni ...................................4.6 µg/g Yb.............................. 0.044 µg/gCs ............................... 0.29 µg/g P.................................2840 µg/g Zn................................ 26.3 µg/g
Indicative values for Ag, Al, Dy, Gd, Hf, Hg, Ho, Li, Lu, Nd, Pr, Se, Si, Tb, V
35 g
SLV FUNGUS Edible fungus (C.tubaeformis) - Trace elementsCertified values
Cd .......................... 0.437 mg/kg Cu.............................34.4 mg/kg Ni ........................... 0.381 mg/kgCo .......................... 0.073 mg/kg Fe ..............................101 mg/kg Pb ............................ 1.43 mg/kgCr ........................... 0.223 mg/kg Mn ............................49.9 mg/kg Zn............................. 55.0 mg/kg
7 g
IAEA-359 Cabbage - Trace elementsCertified values
Al................................ 0.1 mg/kg Fe ..............................148 mg/kg Ni ............................. 1.05 mg/kgBa ............................... 11 mg/kg Hg...........................0.013 mg/kg Se ............................ 0.12 mg/kgCa ......................... 18500 mg/kg K............................32500 mg/kg Sr ............................. 49.2 mg/kgCd ............................ 0.12 mg/kg Mg ...........................2160 mg/kg Zn............................. 38.6 mg/kgCr ............................... 1.3 mg/kg Mn ............................31.9 mg/kgCu ............................ 5.67 mg/kg Na..............................580 mg/kg
30 g
Vegetable matter
38 Edition 2003/2004 www.lgcpromochem.com
Code Product Unit
BCR-400 Red ceramic tile (Tomato paste colour)100 mm x 100 mm
A ceramic tile the colour of which is defined by Hunter L, a and b values. Each tile is individually certified. The tileis intended for the purpose of calibration and does not represent a standard tomato paste colour.Nominal Hunter values: L 26, a 33, b 14.5
tile
Vegetable oils
LGC7120 (RM) Corn oil - BHA and BHTCommercial corn oil with added BHA and BHT
Assesed values
BHA ......................... 49.4 mg/kg BHT ..........................49.7 mg/kg
5 x 25 mL
LGC7122-23 Olive oil - TocopherolLGC7122
Certified value
alpha-tocopherol ...... 72.1 mg/kg
LGC7123
Certified value
alpha-tocopherol .... 173.6 mg/kg
2 x 25 mL
BCR-458 Coconut oil - PAHs (doped)Compound Certified value Uncertainty
µg/kg µg/kg
Pyrene.................................................................. 9.4............................ 1.5Chrysene.............................................................. 4.9............................ 0.4Benzo(k)fluoranthene ........................................ 1.87.......................... 0.18Benzo(a)pyrene ................................................. 0.93.......................... 0.09Benzo(ghi)perylene............................................ 0.97.......................... 0.07Indeno(1,2,3-cd)pyrene...................................... 1.00.......................... 0.07
45 g
BCR-459 Coconut oil - PAHs (blank)Compound Certified value Compound Certified value
µg/kg µg/kg
Pyrene................................................................ <0.9 Benzo(a)pyrene.................................................. <0.3Chrysene............................................................ <0.6 Benzo(ghi)perylene ............................................ <0.2Benzo(k)fluoranthene ........................................ <0.2 Indeno(1,2,3-cd)pyrene...................................... <0.2
45 g
NIST-1563 Coconut oil - Cholesterol and fat-soluble vitaminsThis Standard Reference Material (SRM) is intended primarily for use in the development and validation ofanalytical methods for the determination of cholesterol, fat-soluble vitamins, fat, and fatty acids in a lipid matrix.NIST-1563 consists of ten ampoules per unit: five ampoules of natural coconut oil (1563-1) and five ampoules offortified coconut oil (1563-2). Each ampoule contains approximately 4 mL of oil.
Mass fraction Concentration(mg/kg) (mg/L)
Cholesterol...........................................638 ± 8 ............................... 585 ± 6dl-alpha-Tocopheryl acetate ................158 ± 6 ............................... 145 ± 6
Reference values for fat and fatty acids, cholesterol and vitamins
set (10)
BCR-537 Plastic film A - Overall migration in olive oilTotal immersion in olive oil for 10 days at 40°C
Certified value: 8.3 mg/dm2
film
BCR-538 Plastic film B - Overall migration in olive oilSingle sided cell in olive oil for 10 days at 40°C
Certified value: 5.7 mg/dm2
film
BCR-539 Plastic film C - Overall migration in olive oilPouch in olive oil for 10 days at 40°C
Certified value: 6.1 mg/dm2
film
BCR-593 Plastic film E120 cm x 20 cm
Directive 90/128/EEC on plastic materials and articles intended for food contact regulates the limits of overallmigration of specific substances into foodstuff. BCR-593 has been prepared to check the performance of thestandard test procedure of film thickness, required for the evaluation of migration tendency.
Certified values
Fat soluble fluorescent additive (1,4-diphenyl-1,3-butadiene) .................................... 12.58 mg/kgFilm thickness............................................................................................................. 149.7 µm
film
Mycotoxins
www.lgcpromochem.com Edition 2003/2004 39
MycotoxinsCode Product Unit
Single compounds
B-MYC0340 3-Acetyl-deoxynivalenol (3-AcDON) 100 µg/mL in acetonitrile 5 mL
B-MYC0340-C 3-Acetyl-deoxynivalenol 5 mg
B-MYC0360 15-Acetyl-deoxynivalenol (15-AcDON) 100 µg/mL in acetonitrile 5 mL
B-MYC0360-C 15-Acetyl-deoxynivalenol 5 mg
CSIR-MYC 024 Acgroclavine 10 mg
CSIR-MYC 025 Acroclavine I 10 mg
B-MYC0200 Aflatoxin B1 2 µg/mL in acetonitrile 5 mL
B-MYC0220 Aflatoxin B2 0.5 µg/mL in acetonitrile 5 mL
B-MYC0240 Aflatoxin G1 2 µg/mL in acetonitrile 5 mL
B-MYC0260 Aflatoxin G2 0.5 µg/mL in acetonitrile 5 mL
B-MYC0280 Aflatoxin M2 0.5 µg/mL in acetonitrile 5 mL
BCR-423 (RM) Aflatoxin M1 standard solution9.93 µg/mL in chloroform
2.5 mL
RH36976 Aflatoxin M1 0.5 µg/mL in methanol OEKANAL® 2 mL
CSIR-MYC 005 Austdiol 10 mg
CSIR-MYC 006 Austocystin A 10 mg
CSIR-MYC 026 Chanoclavine I 10 mg
CSIR-MYC 007 Cytochalasin B 10 mg
CSIR-MYC 008 Cytochalasin H 10 mg
CSIR-MYC 009 Cytochalasin J 10 mg
B-MYC0320 Deoxynivalenol (DON) 100 µg/mL in acetonitrile 5 mL
B-MYC0320-C Deoxynivalenol 5 mg
CSIR-MYC 027 Dimer epoxyagroclavine-I-tartrate 10 mg
CSIR-MYC 028 Elymoclavine 10 mg
CSIR-MYC 030 Epoxyagroclavine-I-tartrate 10 mg
B-MYC0400 Fumonisin B1 50 µg/mL in acetonitrile/water (1:1) 5 mL
B-MYC0400-C Fumonisin B1 5 mg
B-MYC0420 Fumonisin B2 50 µg/mL in acetonitrile/water (1:1) 5 mL
CSIR-MYC 013 Gliotoxin 10 mg
CSIR-MYC 029 Meleagrin 10 mg
B-MYC0480 Nivalenol 100 µg/mL in acetonitrile 5 mL
B-MYC0480-C Nivalenol 5 mg
B-MYC0490 Ochratoxin A 10 µg/mL in acetonitrile 5 mL
B-MYC0490-C Ochratoxin A 5 mg
CSIR-MYC 015 Ochratoxin B 10 mg
B-MYC0500 Patulin 100 µg/mL in acetonitrile 5 mL
Mycotoxins
40 Edition 2003/2004 www.lgcpromochem.com
Code Product Unit
CSIR-MYC 017 Secalonic acid D 10 mg
CSIR-MYC 019 Tenuazonic acid-Ca salt 10 mg
CSIR-MYC 020 Tenuazonic acid-Cu salt 10 mg
CSIR-MYC 021 Verruculogen 10 mg
B-MYC0600 Zearalenon 100 µg/mL in acetonitrile 5 mL
B-MYC0600-C Zearalenone 5 mg
Multicomponent standard solutions
B-MYC0300 Aflatoxin MixtureAflatoxin B1................... 2 µg/mL Aflatoxin G1...................2 µg/mLAflatoxin B2................ 0.5 µg/mL Aflatoxin G2................0.5 µg/mL
5 mL
B-MYC0440 Fumonisin Mixture50 mg/L of each analyte in acetonitrile/water (1:1)
Fumonisin B1 Fumonisin B2
5 mL
B-MYC0700 Trichothecene Mixture100 µg/mL of each analyte in acetonitrile
3-Acetyl-deoxynivalenol (3-AcDON) Deoxynivalenol (DON)15-Acetyl-deoxynivalenol (15-AcDON) Nivalenol
5 mL
Quality control reference materials from LGC
www.lgcpromochem.com Edition 2003/2004 41
Quality control reference materials from LGCCode Product Unit
LGCQC1001 Meat paste 1This material is a blend of beef and pork meat .
Reference values
Ash......................... 0.78 g/100 g Ca..............................253 mg/kg Na ........................... 1360 mg/kgMoisture ................. 66.5 g/100 g K..............................1590 mg/kg Zn............................. 14.2 mg/kgTotal Fat................. 12.4 g/100 g N.............................1.96 g/100 g
10 x 200 g
LGCQC1002 Flour 1This material is a commercially produced white bread flour.
Reference values
Ash......................... 0.84 g/100 g Ca............................1120 mg/kg Fe................................ 23 mg/kgFat............................ 1.7 g/100 g K..............................1720 mg/kg Zn................................ 12 mg/kgN ............................ 2.43 g/100 g Na................................39 mg/kg
10 x 25 g
LGCQC1003 Chocolate 1This material comprises milk chocolate that has been ground and thoroughly mixed.
Reference values
Lactose ................................................... 7.8 g/100 g N............................................................ 1.25 g/100 gSucrose................................................. 44.8 g/100 g Butyric Acid in Fat ................................... 0.8 g/100 gTotal fat................................................. 29.5 g/100 g
10 x 15 g
LGCQC1004 Fish paste 1This material comprises whole mackerel fillets that have been thoroughly blended, after addition of water andsodium.
Reference values
Ash......................... 0.83 g/100 g N.............................2.25 g/100 g Cl ............................ 1500 mg/kgMoisture ................. 64.5 g/100 g Na............................1320 mg/kgTotal Fat................. 20.4 g/100 g K..............................1850 mg/kg
10 x 200 g
LGCQC1005 Fish paste 2This material comprises a thoroughly mixed blend of white and brown crab meat.
Reference values
As............................. 11.0 mg/kg Cu.............................10.4 mg/kg Na ........................... 2170 mg/kgCa ........................... 2150 mg/kg Hg.............................0.10 mg/kg Ni ............................. 0.23 mg/kgCd .............................. 1.9 mg/kg K..............................1980 mg/kg P ............................. 2960 mg/kgCo ............................ 0.06 mg/kg Mg .............................348 mg/kg V .............................. 0.08 mg/kgCr ............................... 0.3 mg/kg Mn ..............................1.8 mg/kg Zn............................. 53.6 mg/kg
10 x 200 g
LGCQC1050 Animal feed 1This material comprises a commercially produced feeding stuff that has been ground to pass a 1mm sieve andthoroughly mixed.
Reference values
Ash........................... 8.1 g/100 g Cl ............................0.66 g/100 g Mn............................. 128 mg/kgCrude fibre ............... 7.5 g/100 g Cu................................34 mg/kg Na .......................... 0.44 g/100 gMoisture ................... 5.8 g/100 g Fe ..............................248 mg/kg N ............................ 2.72 g/100 gOil ............................ 7.8 g/100 g K.............................1.07 g/100 g P ............................ 0.72 g/100 gCa .......................... 1.05 g/100 g Mg ..........................0.60 g/100 g Zn.............................. 136 mg/kg
10 x 50 g
Food Authenticity
42 Edition 2003/2004 www.lgcpromochem.com
Food AuthenticityIsotopic analyses are now official or standard methods in Europe and beyond for routine use in foodauthenticity testing. Thus, the use of nuclear magnetic resonance (NMR) spectrometry based on thesite-specific natural isotope fractionation (SNIF) is prescribed for instance by EC Regulation No.2676/90 on analytical methods for wine quality control. These methods are based on themeasurement of stable isotope content (deuterium, 13C, 18O, etc.) of the products or of a specificcomponent such as an ingredient or target molecule of the product. The determinations, carried outusing NMR and/or Isotopic Ratio Mass Spectrometry (IRMS), provide information on the botanical andgeographical orign of the food product. In order to enable a clear comparision of results the followingcertified reference materials have been developed.
Code Product Unit
BCR-123A and BCR-123B
Quantitative analysis of deuterium in ethanol by NMR spectrometry based on the site-specific naturalisotope fractionation (SNIF) is of considerable importance for the detection of wine enrichment. Thistechnique is prescribed by EC regulation No. 2676/90 on analytical methods for wine quality control.BCR-123 consists of a set of 3 sealed NMR tubes containing forms of ethanol with a range of sitespecific isotopic ratios, to which tetramethylurea internal standard and the C6F6 lock substance havebeen added.
BCR-123A Ethanol - D/H isotopic determination 3 tubes
BCR-123B Ethanol - D/H isotopic determination 3 tubes
BCR-660 Alcoholic solution - Isotope ratiosCertified values
Parameter value uncertainty
(D/H)I by 2H-NMR................................... 102.90 ppm........................ ±0.16(D/H)II by 2H-NMR.................................. 131.35 ppm........................ ±0.23R by 2H-NMR ................................................... 2.567...................... ±0.005δ13CVPDB by IRMS........................................ -2.672%...................... ±0.009(D/H) w of water (IRMS)........................... 148.68ppm........................ ±0,14Alcoholic grade tD.......................................... 11.96%..................... ±0.06(1)
(1) in v/v %
450 mL
Lipid Standards
www.lgcpromochem.com Edition 2003/2004 43
Lipid StandardsCode Product Unit
U-FLSA-098 Arachidonic acid (90%) 100 mg
U-FLSA-101 Arachidonic acid (99%) 100 mg
U-FLSA-107 Arachidonic acid methyl ester (90%) 100 mg
U-FLSA-110 Arachidonic acid methyl ester (99%) 100 mg
U-FLSA-115 Butanedioic acid (Succinic acid) 1 g
U-FLSA-132 Butanedioic acid dimethyl ester 1 g
U-FLSA-002 Butanoic acid (Butyric acid) 1 g
U-FLSA-017 Butanoic acid methyl ester 1 g
U-FLSA-121 Decanedioic acid (Sebacic acid) 500 mg
U-FLSA-138 Decanedioic acid dimethyl ester 500 mg
U-FLSA-005 Decanoic acid (Capric acid) 1 g
U-FLSA-020 Decanoic acid methyl ester 1 g
U-FLSA-100 Docosahexenoic acid 100 mg
U-FLSA-109 Docosahexenoic acid methyl ester 100 mg
U-FLSA-011 Docosanoic acid (Behenic acid) 1 g
U-FLSA-026 Docosanoic acid methyl ester 1 g
U-FLMS-018 1-Docosanol (Behenyl Alcohol) 100 mg
U-FLSA-006 Dodecanoic acid (Lauric acid) 1 g
U-FLSA-021 Dodecanoic acid methyl ester 1 g
U-FLSA-091 11,14-Eicosadienoic acid 100 mg
U-FLSA-094 11,14-Eicosadienoic acid methyl ester 100 mg
U-FLSA-010 Eicosanoic acid (Arachidic acid) 1 g
U-FLSA-025 Eicosanoic acid methyl ester 1 g
U-FLMS-016 1-Eicosanol (Arachidyl Alcohol) 500 mg
U-FLSA-097 11,14,17-Eicosatrienoic acid 100 mg
U-FLSA-106 11,14,17-Eicosatrienoic acid methyl ester 100 mg
U-FLSA-072 11-Eicosenoic acid 100 mg
U-FLSA-086 11-Eicosenoic acid methyl ester 100 mg
U-FLSA-066 Elaidic acid 100 mg
U-FLSA-080 Elaidic acid methyl ester 100 mg
U-FLSA-073 Erucic acid 100 mg
U-FLSA-087 Erucic acid methyl ester 100 mg
U-FLSA-113 Ethanedioic acid (Oxalic acid) 1 g
U-FLSA-130 Ethanedioic acid dimethyl ester 1 g
U-FLSA-001 Ethanoic acid (Acetic acid) 1 g
U-FLSA-016 Ethanoic acid methyl ester 1 g
U-FLSA-036 Hendecanoic acid (Undecylic acid) 100 mg
Lipid Standards
44 Edition 2003/2004 www.lgcpromochem.com
Code Product Unit
U-FLSA-051 Hendecanoic acid methyl ester 100 mg
U-FLSA-041 Heneicosanoic acid 100 mg
U-FLSA-056 Heneicosanoic acid methyl ester 100 mg
U-FLMS-017 1-Heneicosanol 100 mg
U-FLSA-059 Heptacosanoic acid methyl ester 50 mg
U-FLMS-023 1-Heptacosanol 50 mg
U-FLSA-039 Heptadecanoic acid (Margaric acid) 100 mg
U-FLSA-054 Heptadecanoic acid methyl ester 100 mg
U-FLMS-013 1-Heptadecanol 100 mg
U-FLSA-118 Heptanedioic acid (Pimelic acid) 1 g
U-FLSA-135 Heptanedioic acid dimethyl ester 1 g
U-FLSA-034 Heptanoic acid (Heptylic acid) 100 mg
U-FLSA-049 Heptanoic acid methyl ester 100 mg
U-FLSA-013 Hexacosanoic acid (Cerotic acid) 100 mg
U-FLSA-028 Hexacosanoic acid methyl ester 100 mg
U-FLMS-022 1-Hexacosanol (Cerotyl Alcohol) 50 mg
U-FLSA-008 Hexadecanoic acid (Palmitic acid) 1 g
U-FLSA-023 Hexadecanoic acid methyl ester 1 g
U-FLMS-012 1-Hexadecanol (Cetyl Alcohol) 1 g
U-FLSA-117 Hexanedioic acid (Adipic acid) 1 g
U-FLSA-134 Hexanedioic acid dimethyl ester 1 g
U-FLSA-003 Hexanoic acid (Caproic acid) 1 g
U-FLSA-018 Hexanoic acid methyl ester 1 g
U-FLSA-147 homo gamma-Linolenic acid 100 mg
U-FLSA-148 homo gamma-Linolenic acid methyl ester 100 mg
U-FLSA-089 Linoleic acid 100 mg
U-FLSA-092 Linoleic acid methyl ester 100 mg
U-FLSA-090 Linolelaidic acid 100 mg
U-FLSA-093 Linolelaidic acid methyl ester 100 mg
U-FLSA-095 Linolenic acid 100 mg
U-FLSA-104 Linolenic acid methyl ester 100 mg
U-FLSA-096 gamma Linolenic acid 100 mg
U-FLSA-105 gamma-Linolenic acid methyl ester 100 mg
U-FLSA-031 Methanoic acid (Formic acid) 1 g
U-FLSA-046 Methanoic acid methyl ester 1 g
U-FLBA-021 2-Methylbutanoic acid (Anteisovaleric acid) 50 mg
U-FLBA-030 2-Methylbutanoic acid methyl ester 50 mg
U-FLBA-034 10-Methyldodecanoic acid methyl ester 50 mg
Lipid Standards
www.lgcpromochem.com Edition 2003/2004 45
Code Product Unit
U-FLBA-038 18-Methyleicosanoic acid methyl ester 25 mg
U-FLBA-004 10-Methylhendecanoic acid (Isolauric acid) 50 mg
U-FLBA-014 10-Methylhendecanoic acid methyl ester 50 mg
U-FLBA-007 16-Methylheptadecanoic acid (Isostearic acid) 10 mg
U-FLBA-017 16-Methylheptadecanoic acid methyl ester 10 mg
U-FLBA-002 6-Methylheptanoic acid (Isocaprylic acid) 50 mg
U-FLBA-012 6-Methylheptanoic acid methyl ester 50 mg
U-FLBA-027 14-Methylhexadecanoic acid (Anteisomargaric acid) 10 mg
U-FLBA-036 14-Methylhexadecanoic acid methyl ester 10 mg
U-FLBA-022 4-Methylhexanoic acid (Anteisoheptylic acid) 50 mg
U-FLBA-031 4-Methylhexanoic acid methyl ester 50 mg
U-FLBA-008 18-Methylnonadecanoic acid (Isoarachidic acid) 25 mg
U-FLBA-018 18-Methylnonadecanoic acid methyl ester 25 mg
U-FLBA-003 8-Methylnonanoic acid (Isocapric acid) 50 mg
U-FLBA-013 8-Methylnonanoic acid methyl ester 50 mg
U-FLBA-028 16-Methyloctadecanoic acid (Anteisononadecylic acid) 25 mg
U-FLBA-037 16-Methyloctadecanoic acid methyl ester 25 mg
U-FLBA-032 6-Methyloctanoic acid methyl ester 50 mg
U-FLBA-006 14-Methylpentadecanoic acid (Isopalmitic acid) 10 mg
U-FLBA-016 14-Methylpentadecanoic acid methyl ester 10 mg
U-FLBA-001 4-Methylpentanoic acid (Isocaproic acid) 50 mg
U-FLBA-011 4-Methylpentanoic acid methyl ester 50 mg
U-FLBA-026 12-Methyltetradecanoic acid (Anteisopentadecylic acid) 10 mg
U-FLBA-035 12-Methyltetradecanoic acid methyl ester 10 mg
U-FLBA-015 12-Methyltridecanoic acid methyl ester 10 mg
U-FLSA-062 Myristoleic acid 100 mg
U-FLSA-076 Myristoleic acid methyl ester 100 mg
U-FLSA-074 Nervonic acid 100 mg
U-FLSA-088 Nervonic acid methyl ester 100 mg
U-FLSA-040 Nonadecanoic acid (Nonadecylic acid) 100 mg
U-FLSA-055 Nonadecanoic acid methyl ester 100 mg
U-FLMS-015 1-Nonadecanol 100 mg
U-FLSA-120 Nonanedioic acid (Azelaic acid) 500 mg
U-FLSA-137 Nonanedioic acid dimethyl ester 500 mg
U-FLSA-035 Nonanoic acid (Pelargonic acid) 100 mg
U-FLSA-050 Nonanoic acid methyl ester 100 mg
U-FLSA-014 Octacosanoic acid (Montanic acid) 100 mg
U-FLSA-029 Octacosanoic acid methyl ester 100 mg
Lipid Standards
46 Edition 2003/2004 www.lgcpromochem.com
Code Product Unit
U-FLMS-024 1-Octacosanol 50 mg
U-FLSA-127 Octadecanedioic acid 50 mg
U-FLSA-144 Octadecanedioic acid dimethyl ester 50 mg
U-FLSA-009 Octadecanoic acid (Stearic acid) 1 g
U-FLSA-024 Octadecanoic acid methyl ester 1 g
U-FLMS-014 1-Octadecanol (Stearyl Alcohol) 1 g
U-FLSA-067 cis-11-Octadecenoic acid 100 mg
U-FLSA-081 cis-11-Octadecenoic acid methyl ester 100 mg
U-FLSA-068 trans-11-Octadecenoic acid (Vaccenic acid) 100 mg
U-FLSA-082 trans-11-Octadecenoic acid methyl ester 100 mg
U-FLSA-119 Octanedioic acid (Suberic acid) 500 mg
U-FLSA-136 Octanedioic acid dimethyl ester 500 mg
U-FLSA-004 Octanoic acid (Caprylic acid) 1 g
U-FLSA-019 Octanoic acid methyl ester 1 g
U-FLSA-065 Oleic acid 100 mg
U-FLSA-079 Oleic acid methyl ester 100 mg
U-FLSA-064 Palmitelaidic acid 100 mg
U-FLSA-078 Palmitelaidic acid methyl ester 100 mg
U-FLSA-063 Palmitoleic acid 100 mg
U-FLSA-077 Palmitoleic acid methyl ester 100 mg
U-FLSA-058 Pentacosanoic acid methyl ester 50 mg
U-FLMS-021 1-Pentacosanol 50 mg
U-FLSA-038 Pentadecanoic acid (Pentadecylic acid) 100 mg
U-FLSA-053 Pentadecanoic acid methyl ester 100 mg
U-FLSA-033 Pentanoic acid (Valeric acid) 100 mg
U-FLSA-048 Pentanoic acid methyl ester 100 mg
U-FLSA-071 Petroselinic acid 100 mg
U-FLSA-085 Petroselinic acid methyl ester 100 mg
U-FLBA-042 Phytanic acid (3,7,11,15-Tetramethylhexadecanoic acid) 25 mg
U-FLBA-043 Phytanic acid methyl ester (Methyl-3,7,11,15-tetramethylhexadecanoate) 25 mg
U-FLMS-035 Phytol (tech) (3,7,11,15-Tetramethyl-2-hexadecen-1-ol ) 1 g
U-FLSA-114 Propanedioic acid (Malonic acid) 1 g
U-FLSA-131 Propanedioic acid dimethyl ester 1 g
U-FLSA-032 Propanoic acid (Propionic acid) 1 g
U-FLSA-047 Propanoic acid methyl ester 1 g
U-FLSA-070 Ricinelaidic acid 100 mg
U-FLSA-084 Ricinelaidic acid methyl ester 100 mg
U-FLSA-069 Ricinoleic acid 100 mg
Lipid Standards
www.lgcpromochem.com Edition 2003/2004 47
Code Product Unit
U-FLSA-083 Ricinoleic acid methyl ester 100 mg
U-FLSA-012 Tetracosanoic acid (Lignoceric acid) 100 mg
U-FLSA-027 Tetracosanoic acid methyl ester 100 mg
U-FLMS-020 1-Tetracosanol (Lignoceryl Alcohol) 50 mg
U-FLSA-125 Tetradecanedioic acid 100 mg
U-FLSA-142 Tetradecanedioic methyl ester 100 mg
U-FLSA-007 Tetradecanoic acid (Myristic acid) 1 g
U-FLSA-022 Tetradecanoic acid methyl ester 1 g
U-FLMS-010 1-Tetradecanol (Myristyl Alcohol) 1 g
U-FLSA-015 Triacontanoic acid (Mellisic acid) 100 mg
U-FLSA-030 Triacontanoic acid methyl ester 100 mg
U-FLMS-026 1-Triacontanol (Melissyl Alcohol) 50 mg
U-FLSA-057 Tricosanoic acid methyl ester 100 mg
U-FLMS-019 1-Tricosanol 100 mg
U-FLSA-037 Tridecanoic acid (Tridecylic acid) 100 mg
U-FLSA-052 Tridecanoic acid methyl ester 100 mg
U-FLPK-001 Unsaturated fatty acids & methyl estersEach kit contains 25 mg each of twenty compounds.
cis-9-Tetradecenoic acid (Myristoleic acid)cis-9-Hexadecenoic acid (Palmitoleic acid)trans-9-Hexadecenoic acid (Palmitelaidic acid)cis-9-Octadecenoic acid (Oleic acid)trans-9-Octadecenoic acid (elaidic acid)cis-9-cis-12-Octadecadienoic acid (Linoleic acid)trans-9-trans-12-Octadecadienoic acid (Linolelaidic acid)cis-9-cis-12-cis-15-Octadecenoate acid (Linolenic acid)cis-11-Eicosenoic acid (Gondonic acid)cis-13-Docosenoic acid (Erucic acid)Methyl cis-9-Tetradecanoate (Methyl myristoleate)Methyl cis-9-Hexadecenoate (Methyl palmitoleate)Methyl trans-9-Hexadecenoate (Methyl palmitelaidate)Methyl cis-9-Octadecenoate (Methyl oleate)trans-9-Octadecenoate (Methyl eleidate)Methyl cis-9-cis-12-Octadecadienoate (Methyl linoleate)Methyl trans-9-cis-12-Octadecadienoate (Methyl linelaidate)Methyl cis-9-cis-12-cis-15-Octadecatrienoate (Methyl linolenate)Methyl cis-11-Eicosenoate (Methyl gondonate)Methyl cis-13-Docosenoate (Methyl erucate)
kit
U-FLPK-003 Fatty acids and methyl esters kitEach kit contains 25 mg each of sixteen compounds.
Nonanoic acid Methyl nonanoateUndecanoic acid Methyl undecanoateTridecanoic acid Methyl tridecanoatePentadecanoic acid Methyl pentadecanoateHeptadecanoic acid Heptadecanoic acid methyl esterNonadecanoic acid (Nonadecylic acid) Nonadecanoic acid methyl esterHeneicosanoic acid Heneicosanoic acid methyl esterTricosanoic acid Tricosanoic acid methyl ester
kit
U-FLPK-004 Fatty acids and methyl esters kitEach kit contains 100 mg each of twenty compounds.
Hexanoic acid (Caproic acid) Hexanoic acid methyl esterOctanoic acid (Caprylic acid) Octanoic acid methyl esterDecanoic acid (Capric acid) Decanoic acid methyl esterDodecanoic acid (Lauric acid) Dodecanoic acid methyl esterTetradecanoic acid (Myristic acid) Tetradecanoic acid methyl esterHexadecanoic acid (Palmitic acid) Hexadecanoic acid methyl esterStearic acid Octadecanoic acid methyl esterEicosanoic acid (Arachidic acid) Eicosanoic acid methyl esterDocosanoic acid (Behenic acid) Docosanoic acid methyl esterTetracosanoic acid (Lignoceric acid) (25 mg) Tetracosanoic acid methyl ester (25 mg)
kit
Lipid Standards
48 Edition 2003/2004 www.lgcpromochem.com
Code Product Unit
U-FLPK-005 Volatile fatty acidsEach kit contains 1 gm each of ten compounds plus 5 mL of a mixture.
Methanoic acid (Formic acid) Isovaleric acidAcetic acid Hexanoic acid (Caproic acid)Propanoic acid (Propionic acid) Heptanoic acidButanoic acid (Butyric acid) Octanoic acid (Caprylic acid)Isobutyric acid 0.1% C1-C5 Acids test solution in H2O (5 mL)Pentanoic acid (Valeric acid)
kit
Food and drink products
www.lgcpromochem.com Edition 2003/2004 49
Food and drink productsCode Product Unit
Processed food
LGC7103 Sweet digestive biscuit - Proximates and elementsAssessed values
Moisture ................... 2.8 g/100 g Fructose .................0.24 g/100 g Mn.............................. 5.9 mg/kgNitrogen ................. 1.06 g/100 g Sucrose ..................16.6 g/100 g Na ........................... 6300 mg/kgTotal fat.................. 20.9 g/100 g Chloride ....................0.55 mg/kg P ............................... 870 mg/kgAsh.......................... 2.08 g/100g K..............................1530 mg/kg Zn............................... 5.8 mg/kg
Indicative values for glucose, starch, Ca and Mg
50 g
LGC7107 (RM) Madeira cake - ProximatesLemon Madeira cake were prepared by a UK food company. Each cake, weighing approx. 160 g, was sealed in acan.
Assessed values
Moisture ................. 25.9 g/100 g Total fat ..................13.4 g/100 g Sucrose.................. 28.1 g/100 gNitrogen ................. 0.66 g/100 g Ash .........................1.76 g/100 g Lactose .................... 0.9 g/100 g
Indicative value for starch content
160 g
LGC7105 (RM) Rice pudding - Proximates and elementsCertified values
Moisture ................. 71.3 g/100 g Sucrose ....................7.2 g/100 g Mn.............................. 0.7 mg/kgN ............................ 0.17 g/100 g Ca................................78 mg/kg Na ............................. 344 mg/kgTotal fat.................... 8.4 g/100 g K................................558 mg/kg P ............................... 346 mg/kgAsh......................... 0.22 g/100 g Mg ...............................30 mg/kg Zn............................... 1.5 mg/kg
5 x 200 g
LGC7016 Chocolate confectionery - Sugars, nitrogen and fatsCertified values
Lactose .................... 7.8 g/100 g Total fat ..................29.5 g/100 g Nitrogen ................. 1.25 g/100 gSucrose.................. 44.8 g/100 g Butyric acid in fat ......0.8 g/100 g
Indicative values for fructose and glucose
15 g
BCR-518 Bran breakfast cereal - Dietary fibreCertified using five different methods of dietary fibre analysis
Certified values
AOAC 1990........................................... 30.2 g/100 g AOAC 1992 MES-TRIS......................... 30.5 g/100 gEnglyst (GC) ......................................... 24.1 g/100 g Englyst (colorimetry) ............................. 25.0 g/100 gUppsala................................................. 27.6 g/100 g
25 g
BCR-191 Brown bread - Trace elementsCertified values
Cd ............................. 28.4 µg/kg Fe .............................40.7 mg/kg Pb .............................. 187 µg/kgCu .............................. 2.6 mg/kg Mn ............................20.3 mg/kg Zn............................. 19.5 mg/kg
Indicative values for As,Ca, Cl, Cr, Hg, K, Mg, Na, Ni, P, Se
40 g
NIST-1845 Whole egg powder - CholesterolCertified value
Cholesterol................. 19.0 mg/g
35 g
NIST-RM 8415 Whole egg powder - Trace elementsReference concentration values are given for major, minor and trace constituent elements, proximates, caloriesand fatty acids. Information concentration values are given for additional elements, fatty acids and water solublevitamins
35 g
NIST-2383 Baby food composite - Carotenoids and vitaminsCertified values
trans-Retinol ............ 0.80 mg/kg α-Tocopherol ............25.0 mg/kg β-Cryptoxanthin........ 1.38 mg/kgδ-Tocopherol ............ 1.51 mg/kg Lutein........................1.16 mg/kg Total α-carotene ...... 0.83 mg/kgγ-Tocopherol ............ 5.51 mg/kg Zeaxanthin................0.86 mg/kg Total β–carotene...... 3.12 mg/kg
Indicative values for other vitamins and carotenoids, proximates, cholesterol, calories, minerals and traceelements
4 x 70 g
Food and drink products
50 Edition 2003/2004 www.lgcpromochem.com
Code Product Unit
NIST-1548a Typical diet - Trace elementsA unit of NIST-1548a consists of two bottles, each containing approximately 6.5 g of the freeze-dried homogenateof mixed diet foods.
Certified values
Al.............................. 72.4 mg/kg Cu.............................2.32 mg/kg Ni ........................... 0.369 mg/kgAs............................. 0.20 mg/kg Fe .............................35.3 mg/kg P ............................. 3486 mg/kgCa ........................... 1967 mg/kg I ..............................0.759 mg/kg S ............................. 1928 mg/kgCd .......................... 0.035 mg/kg Mg .............................580 mg/kg Se .......................... 0.245 mg/kgCl .......................... 12078 mg/kg Mn ............................5.75 mg/kg Sn ............................ 17.2 mg/kgCs ........................ 0.0098 mg/kg Na............................8132 mg/kg Zn............................. 24.6 mg/kg
Indicative values for Ash, carbohydrate, fat, N, protein, dietary fibre, calories, B, Ba, Br, Co, Hg, Mo, Sb, Sc, Si,Sr, Ti
set (2)
NIST-1544 Diet composite - Fatty acids and cholesterolCertified values
Cholesterol.............. 0.1483 g/kg Palmitic acid ................5.77 g/kg Linoleic acid ................ 6.56 g/kgLauric acid .................. 1.31 g/kg Stearic acid..................2.00 g/kgMyristic acid ................ 1.01 g/kg Oleic acid...................11.64 g/kg
Indicative values for protein, moisture, total fat, ash, carbohydrate, calories, remaining fatty acids, Ca, K, Na
4 x 15 g
ARC/CL2 Total diet - Trace elementsCertified values
Ca .............................. 2.86 mg/g K.................................9.42 mg/g Ni ................................. 271 ng/gCd .................................. 21 ng/g Mg ................................785 µg/g Pb .................................. 43 ng/gCu ............................... 3.18 µg/g Mn ...............................12.9 µg/g Se ................................ 181 ng/gFe................................ 30.4 µg/g Mo ................................262 ng/g Zn................................ 28.9 µg/gHg ................................. 6.6 ng/g Na...............................7.87 mg/g
20 g
SLV DIET A Simulated diet A - Trace elementsA mixture of rye/wheat flour, potatoes, skim milk powder and lean beef.
Certified values
Ca ........................... 1576 mg/kg K............................11222 mg/kg Pb .......................... 0.041 mg/kgCd .......................... 0.029 mg/kg Mg .............................814 mg/kg Zn............................. 95.0 mg/kgCu ............................ 2.60 mg/kg Mn ............................5.69 mg/kgFe............................. 81.2 mg/kg Na............................1613 mg/kg
Indicative values for Al, As, Co, Hg, Ni, Rb, S
10 g
SLV DIET B Simulated diet B - Trace elementsA mixture of rye/wheat flour, pig kidney, skim milk powder and lean beef.
Certified values
Ca ........................... 2018 mg/kg Fe ..............................111 mg/kg Na ........................... 2365 mg/kgCd .......................... 0.099 mg/kg K..............................9142 mg/kg Pb .......................... 0.059 mg/kgCr ........................... 0.149 mg/kg Mg .............................749 mg/kg Zn............................. 91.9 mg/kgCu ............................ 6.64 mg/kg Mn ............................6.36 mg/kg
Indicative values for Al, As, Co, Hg, Ni, Rb, Se
10 g
SLV DIET C Simulated diet C - Trace elementsA mixture of reindeer liver, skim milk powder, lean beef and rye/wheat flour.
Certified values
Ca ........................... 1059 mg/kg Fe ..............................142 mg/kg Na ............................. 697 mg/kgCd .......................... 0.205 mg/kg K..............................4886 mg/kg Ni ........................... 0.108 mg/kgCr ........................... 0.054 mg/kg Mg .............................620 mg/kg Pb .......................... 0.114 mg/kgCu ............................ 20.8 mg/kg Mn ............................9.58 mg/kg Zn............................. 40.6 mg/kg
Indicative values for Al, As, Co, Hg, Rb, Se
10 g
SLV DIET D Simulated diet D - Trace elementsA mixture of skim milk powder, reindeer liver, rye/wheat flour and potatoes.
Certified values
Ca ............................. 510 mg/kg Fe ..............................199 mg/kg Ni ........................... 0.100 mg/kgCd .......................... 0.478 mg/kg K..............................7088 mg/kg Pb .......................... 0.218 mg/kgCo .......................... 0.072 mg/kg Mg .............................676 mg/kg Zn............................. 37.2 mg/kgCr ........................... 0.036 mg/kg Mn ............................10.2 mg/kgCu ............................ 40.8 mg/kg Na..............................485 mg/kg
Indicative values for Al, As, Hg, Rb, Se
10 g
Food and drink products
www.lgcpromochem.com Edition 2003/2004 51
Code Product Unit
SLV DIET E Simulated diet E - Trace elementsA mixture of white wine, potatoes, reindeer liver and rye/wheat flour.
Certified values
Ca ............................. 268 mg/kg Fe ..............................216 mg/kg Ni ........................... 0.124 mg/kgCd .......................... 0.536 mg/kg K..............................5985 mg/kg Pb .......................... 0.273 mg/kgCo .......................... 0.083 mg/kg Mg .............................649 mg/kg Zn............................. 39.5 mg/kgCr ........................... 0.061 mg/kg Mn ............................11.0 mg/kgCu ............................ 46.5 mg/kg Na..............................436 mg/kg
Indicative values for Al, As, Hg, Rb, Se
10 g
SLV DIET F Simulated diet F - Trace elementsA mixture of white wine, potatoes, rye/wheat flour and reindeer liver.
Certified values
Ca ............................. 262 mg/kg Fe ..............................349 mg/kg Na ............................. 758 mg/kgCd .......................... 0.877 mg/kg K..............................5966 mg/kg Ni ........................... 0.102 mg/kgCo .......................... 0.136 mg/kg Mg .............................647 mg/kg Pb .......................... 0.439 mg/kgCu ............................ 72.7 mg/kg Mn ............................11.1 mg/kg Zn............................. 55.8 mg/kg
Indicative values for Al, As, Cr, Hg, Rb, Se
10 g
Drinks
LGC7130 Soft drink - SweetenersKnown weights of saccharin and aspartame were added to a simulated soft drink.
Certified values
Saccharin..................... 77 mg/lL Aspartame...................620 mg/L
5 x 20 mL
LGC7131 Soft drink - SweetenersKnown weights of saccharin and Acesulfame-K were added to a simulated soft drink.
Certified values
Saccharin...................... 76 mg/LAcesulfame-K ............. 349 mg/L
5 x 20 mL
LGC7140 (RM) Soft drink - ColoursKnown weights of three food colours were added to a diluted solution of commercial soft drink concentrate.
Certified values
Ponceau 4R (E124) ....................................18.7 mg/l Tartrazine (E102) ...................................... 29.9 mg/LSunset yellow (E110) ................................ 19.6 mg/L
5 x 60 mL
LGC7011 Orange juiceCertified values
Degrees Brix ....................... 1.26 Refractive index...............1.3348
3 mL
LGC7012 Orange juiceCertified values
Degrees Brix ..................... 12.72 Refractive index...............1.3521
3 mL
LGC7013 Orange juiceCertified values
Degrees Brix ..................... 22.07 Refractive index...............1.3673
3 mL
LGC7014 Orange juiceCertified values
Degrees Brix ..................... 55.55 Refractive index...............1.4320
3 mL
LGC7015 Orange juiceCertified values
Degrees Brix ..................... 64.73 Refractive index...............1.4529
3 mL
For refractive index standards see our catalogue “Reference materials for physical properties”
LGC provides two proficiency testing schemes for the soft drinks industry; SODAS (analysis of softdrinks) and LGC-PCI (sugar analysis) – see section “About proficiency testing (PT)” of this catalog forfurther details.
Food and drink products
52 Edition 2003/2004 www.lgcpromochem.com
Code Product Unit
Food additives
LGC7300 2,6-Di-tert-butyl-4-methylphenol (BHT)Certified purity..................99.8%
500 mg
LGC7301 2-tertiary-butyl-4-methoxyphenolCertified purity..................99.2%
500 mg
LGC7302 SaccharinCertified purity.................99.6 %
500 mg
LGC7305 Potassium sorbateCertified purity.................99.8 %
500 mg
IPO F 010 Benzoic acid 250 mg
IPO F 170 Sorbic acid 250 mg
U-FLPK-007 Antioxidant food additives kitEach kit contains 1 g each of thirteen compounds.
Ascorbic acidAscorbyl palmitateBHA (2 & 3-t-Butyl-4-methoxyphenol)BHT (2,6-di-tert-Butyl-4-methylphenol)t-ButylhydroquinoneEthoxyquin (1,2-Dihydro-6-ethoxy-2,2,4-trimethylquinoline)Erythorbic acid (Isoascorbic acid)Dilaurel thiodipropionate4-Hydroxymethyl-2,6-di-t-butylphenolL-GlycinePropyl gallateThiodipropionic acidTHBP (2,4,5-Trihydroxybutyrophenone)
kit
U-FLPK-002 Antimicrobial food additives kitEach kit contains 1 g each of thirteen compounds.
Acetic acid Propanoic acid (Propionic acid)Benzoic acid Propyl parabenButyl paraben Sodium benzoateOctanoic acid (Caprylic acid) Sodium nitrateEthyl paraben Sodium nitriteMethyl paraben Sorbic acidPotassium sorbate
kit
NRMGBW10001 Amaranth colourCertified purity.................97.2 %
300 mg
NRMGBW10002 Ponceau 4RCertified purity.................93.3 %
300 mg
NRMGBW10003 TartrazineCertified purity.................99.3 %
300 mg
NRMGBW10004 Brilliant BlueCertified purity..................97.3%
300 mg
NRMGBW10005 Sunset YellowCertified purity.................97.3 %
300 mg
Food and drink products
www.lgcpromochem.com Edition 2003/2004 53
Code Product Unit
Dye standards
IBPO010 - IBPO008Dye standards from the Institute of Dyes and Organic Products (IBPO) Poland
The following standards of dyes, used in the food and pharmaceutical industry , are listed withcommon description, E code and colour index number (C.I.) for an easy assignment.
The IBPO is accredited by the Polish Centre for Testing and Certification according to the standardPN-EN 45001 and ISO/IEC Guide 25:1990.
Each colour reference standard is supplied with a detailed certificate of analysis which includes dyecontent value determined by spectrophotometry and values of impurities.
Black
IBPO010 Brilliant Black PNC.I.28440 - E 151
1 g
Blue
IBPO015 Brilliant Blue FCFC.I.42090 - E 133
1 g
IBPO002 IndigotineC.I.73015 - E 132
1 g
IBPO012 Patent Blue VC.I.42051 - E 131
1 g
Brown
IBPO017 Brown HTC.I.20285 - E 155
1 g
Green
IBPO016 Brilliant Green BSC.I.44090 - E 142
1 g
Red
IBPO014 Allura Red ACC.I.16035 - E 129
1 g
IBPO005 AmaranthC.I.16185 - E 123
1 g
IBPO003 AzorubinC.I.14720 - E 122
1 g
IBPO011 ErythrosineC.I.45430 - E 127
1 g
IBPO004 Ponceau 4RC.I.16255 - E 124
1 g
IBPO013 Red 2 GC.I.18050 - E 128
1 g
Yellow
IBPO007 Quinoline YellowC.I.47005 - E 104
1 g
IBPO009 Sunset Yellow FCFC.I.15985 - E 110
1 g
IBPO008 TartrazineC.I.19140 - E 102
1 g
Food and drink products
54 Edition 2003/2004 www.lgcpromochem.com
Code Product Unit
Alcoholic beverage
LGC5000 Brandy - AlcoholCertified value................39.98 mL/100 mL (at 20°C)
5 x 50 mL
LGC5100 Whisky - CongenersCertified values
Methanol ................................................. 8.2 g/100 L 2-Methylbutan-1-ol ................................ 19.6 g/100 LEthyl acetate ......................................... 27.0 g/100 L 3-Methylbutan-1-ol ................................ 51.4 g/100 LPropan-1-ol ........................................... 67.4 g/100 L 2+3-Methylbutan-1-ol ............................. 70.1g/100 L2-Methylpropan-1-ol .............................. 65.0 g/100 L
Indicative values for acetaldehyde, butan-1-ol, furfural
5 x 10 mL
LGC5001 Wine - Alcohol (5%)Certified value
Alcohol .............................. 5.04 ml/100 mL (at 20°C)
5 x 250 mL
LGC5002 Wine - Alcohol (10 %)Certified value
Alcohol ..........................................10.25 % (at 20°C)
5 x 250 mL
LGC5003 Wine - Alcohol (15 %)Certified value
Alcohol ..........................................14.66 % (at 20°C)
5 x 250 mL
LGC5004 Lager shandy - AlcoholCertified value..................1.02 mL/100 mL (at 20°C)
5 x 330 mL
LGC5005 Lager - AlcoholCertified value..................4.75 mL/100 mL (at 20°C)
5 x 440 mL
LGC provides three proficiency testing schemes for the alcoholic beverage industry; BAPS (analysisof beer), MAPS (analysis of malted and unmalted barley) and DAPS (analysis of alcoholic beveragesother than beer) – see section “About proficiency testing (PT)” of this catalog for further details.
Low alcohol beverage
Related to the labelling of 'alcohol free' or 'de-alcoholised' and 'low alcohol' beverages according toDirective 90/496/EC.
BCR-651 Beer - Alcohol (low level)Certified value
Ethanol................................................. 0.505 % (v/v)
10 mL
BCR-652 Beer - Alcohol (very low level)Certified value
Ethanol................................................. 0.051 % (v/v)
10 mL
BCR-653 Wine - Alcohol (low level)Certified value
Ethanol................................................. 0.539 % (v/v)
10 mL
Alcohol
LGC5404 Ethanol/water - 5% EthanolCertified value
Ethanol.................................... 5 mL/100 mL at 20°C
5 x 50 mL
LGC5405 Ethanol/water - 15% EthanolCertified value
Ethanol.................................. 15 mL/100 mL at 20°C
5 x 50 mL
LGC5406 Ethanol/water - 40% EthanolCertified value
Ethanol.................................. 40 mL/100 mL at 20°C
5 x 50 mL
Animal food products
www.lgcpromochem.com Edition 2003/2004 55
Code Product Unit
LGC5407 Ethanol/water - 70% EthanolCertified value
Ethanol.................................. 70 mL/100 mL at 20°C
5 x 50 mL
LGC5408 Ethanol/water - 90% EthanolCertified value
Ethanol.................................. 90 mL/100 mL at 20°C
5 x 50 mL
STA 003 N-N TetramethyllureaUsed as an internal standard in SNIF analysis (see above). D/H nominal values have been determined at 76.7,61.4 and 45.05 MHz for deuterium.
500 ml
Animal food productsCode Product Unit
LGC7176 Canned pet food - ProximatesFish recipe cat food
Certified values
Moisture ................. 84.1 g/100 g Fat ..........................4.46 g/100 gNitrogen ................. 1.32 g/100 g Ash .........................2.20 g/100 g
Indicative values for Cl, K, Na
200 g
LGC7172 (RM) Dairy cattle feed - Proximates and elementsDairy cattle nuts from a commercial animal feed manufacturer.
Assessed values
Ca .......................... 1.05 g/100 g K.............................1.07 g/100 g Moisture ................... 5.8 g/100 gCl ........................... 0.66 g/100 g Mg ..........................0.60 g/100 g Nitrogen ................. 2.72 g/100 gCu ............................... 34 mg/kg Mn .............................128 mg/kg Oil ............................ 7.8 g/100 gK ............................ 1.07 g/100 g P.............................0.72 g/100 g Ash........................... 8.1 g/100 gFe.............................. 248 mg/kg Zn ..............................136 mg/kg Crude fibre ............... 7.5 g/100 g
5 x 50 g
LGC7173 (RM) Poultry feed - Proximates and elementsPlease ask for details.
5 x 50 g
BCR-115 Animal feed - PesticidesCompound Certified value Uncertainty
mg/kg mg/kg
HCB ............................................................... 0.0194...................... 0.0014beta-HCH......................................................... 0.023........................ 0.003gamma-HCH.................................................. 0.0218...................... 0.0020Heptachlor ....................................................... 0.019...................... 0.0015gamma-Chlordane........................................... 0.048........................ 0.005Dieldrin............................................................. 0.018........................ 0.003alpha-Endosulfan............................................. 0.046........................ 0.004Endrin .............................................................. 0.046........................ 0.0062,4'-DDT........................................................... 0.046........................ 0.0054,4'-DDE .......................................................... 0.047........................ 0.004
30 g
BCR-375 Compound feed - Aflatoxin B1 (blank)Certified value
Aflatoxin B1.................. <1 µg/kg
50 g
BCR-376 Compound feed - Aflatoxin B1 (low level)Certified value
Aflatoxin B1................. 9.3 µg/kg
50 g
Fertilizers
56 Edition 2003/2004 www.lgcpromochem.com
FertilizersCode Product Unit
BCR-032 Moroccan phosphate rock - Trace elementsCertified values
As.................................. 9.5 µg/g Cr..................................257 µg/g Ni ................................ 34.6 µg/gB ................................. 22.6 µg/g Cu................................33.7 µg/g Ti.................................. 171 µg/gCd ............................... 20.8 µg/g Hg...................................55 ng/g V .................................. 153 µg/gCo ............................... 0.59 µg/g Mn ...............................18.8 µg/g Zn................................. 253 µg/g
100 g
BCR-033 Super-phosphate - ConstituentsCertified values
P2O5 .......................... 193.4 g/kg SiO2 .............................29.2 g/kg Fe2O3 ............................ 4.0 g/kgSO4 ........................... 428.0 g/kg F ..................................16.5 g/kg MgO .............................. 2.1 g/kgCaO .......................... 314.8 g/kg Al2O3............................11.0 g/kg
100 g
BCR-113 Potassium chloride - Elemental compositionCertified values
Ca ............................... 1.03 g/kg K................................502.5 g/kg Na ............................... 15.3 g/kgCl .............................. 478.0 g/kg Mg ...............................0.24 g/kg
Water soluble
K .............................. 501.3 g/kg
100 g
BCR-114 Potassium sulphate - Elemental compositionCertified values
Ca ................................. 9.4 g/kg K................................418.0 g/kg SO4 .............................. 533 g/kgCl ................................ 18.5 g/kg Na................................11.0 g/kg
Water soluble
K .................................. 17.6g/kg
100 g
BCR-178 Calcium ammonium nitrate - Elemental compositionCertified values
Ca ............................. 88.82 g/kg NO3-N......................130.15 g/kgNH4-N...................... 130.44 g/kg Total-N.....................260.19 g/kg
100 g
BCR-179 Urea - CompositionCertified values
Total-N .................... 465.35 g/kg Uric-N ........................460.9 g/kg Biuret ........................ 10.37 g/kg
100 g
NIST-120c Phosphate rock, Florida - ConstitutentsCertified values
Al2O3 ...............................1.30 % MnO.............................. 0.027 % U3O8............................0.0135 %Fe2O3 ..............................1.08 % Na2O............................... 0.52 % V2O3 ..............................0.016 %K2O ...............................0.147 % TiO2 .............................. 0.103 %
Values for the AFPC-method-Dependent concentrations also available
90 g
NIST-193 Potassium nitrate - Nitrogen and potassiumCertified values
K ...................................38.66 % N................................... 13.85 %
90 g
NIST-194 Ammonium dihydrogen phosphate - Nitrogen and phosphorousCertified values
N ...................................12.15 % P................................... 26.92 %
90 g
NIST-200a Potassium dihydrogen phosphate - Phosphorous and potassiumCertified values
K .................................28.375 % P............................... 22.7352 %
90 g
NIST-694 Phosphate rock, western - ConstituentsCertified values
Al2O3 .................................1.8 % K2O................................. 0.51 % SiO2.................................11.2 %CaO ................................43.6 % MgO................................ 0.33 % U ...............................0.01414 %CdO ..............................0.015 % MnO............................ 0.0116 % V2O5 ..............................0.031 %F........................................3.2 % Na2O............................. 0.086 %Fe2O3 ..............................0.79 % P2O5................................ 30.2 %
Indicative values for, Cr2O3 , ZnO, TiO2
90 g
Fertilizers
www.lgcpromochem.com Edition 2003/2004 57
Code Product Unit
NRMGBW06501 Urea - NitrogenCertified values
Biuret ...............................1.39% N.................................... 46.30%
Indicative values for B, Ca, Fe, Mn
35 g
NRMGBW06502 Ammonium dihydrogen phosphate - Nitrogen and phosphorousCertified values
P ...................................26.85 % N................................... 12.08 %
Indicative values for Ca, Fe, Mg
30 g
NRMGBW06503 Potassium sulphate - PotassiumCertified values
K ...................................44.79 %
Indicative values for Ca, Fe, Mg, Mn
40 g
Plants
58 Edition 2003/2004 www.lgcpromochem.com
PlantsCode Product Unit
Trees and bushes
BCR-062 Olive leaves (Olea europea) - Trace elementsCertified values
Al............................... 450 mg/kg Hg.............................0.28 mg/kg Zn............................. 16.0 mg/kgCd ............................ 0.10 mg/kg Mn ............................57.0 mg/kgCu ............................ 46.6 mg/kg Pb.............................25.0 mg/kg
Indicative values for Ag, As, Au, B, Br, CaO, Ce, Cl, Co, Cr, Cs, Eu, F, FeeO3, K2O, La, MgO, Mo, N, Na2O, Ni,P2O5, Rb, S, Sb, Sc, Se, Sn, Tb, TiO2, Tl, U
25 g
BCR-100 Beech leaves - Trace elementsCertified values
Al............................... 0.435 g/kg Cr.............................0.0080 g/kg N ............................... 26.29 g/kgCa ............................... 5.30 g/kg K..................................9.94 g/kg P ................................. 1.55 g/kgCl ................................ 1.49 g/kg Mg .............................0.878 g/kg S ................................. 2.69 g/kg
Indicative values for Cd, Cu, Fe, Mn, Mo, Pb, Zn
30 g
BCR-101 Spruce needles - Trace elementsCertified values
Al............................... 0.173 g/kg Mg .............................0.619 g/kg P ................................. 1.69 g/kgCa ............................... 4.28 g/kg Mn .............................0.915 g/kg S ................................. 1.70 g/kgCl .............................. 0.688 g/kg N................................18.89 g/kg Zn............................ 0.0353 g/kg
Indicative values for Cd, Cr, Cu, Fe, K, Mo, Pb
30 g
NIST-1575A Pine needles - Trace elements and minor constituentsCertified values
P ...................................0.107 % Ba...............................6.0 mg/kg Fe................................ 46 mg/kgK ...................................0.417 % Cd...........................0.233 mg/kg Hg ........................ 0.0399 mg/kgCa ...................................0.25 % Cl ...............................421 mg/kg Rb ............................ 16.5 mg/kgAl............................... 580 mg/kg Cu.....................................2.g/kg Zn................................ 38 mg/kg
50 g
NIST-1515 Apple leaves - Trace elementsDried leaves from Golden Delicious and Rome varieties.
Certified values
Al............................... 286 mg/kg Fe ................................83 mg/kg Ni ............................. 0.91 mg/kgAs........................... 0.038 mg/kg Hg...........................0.044 mg/kg P ...................................0.159 %B ................................. 27 mg/kg K..................................... 1.61 % Pb .......................... 0.470 mg/kgBa ............................... 49 mg/kg Mg ................................ 0.271 % Rb ............................ 10.2 mg/kgCa .................................1.526 % Mn ...............................54 mg/kg Se .......................... 0.050 mg/kgCd .......................... 0.013 mg/kg Mo ..........................0.094 mg/kg Sr ................................ 25 mg/kgCl .............................. 579 mg/kg N..................................... 2.25 % V .............................. 0.26 mg/kgCu ............................ 5.64 mg/kg Na.............................24.4 mg/kg Zn............................. 12.5 mg/kg
Indicative values for Au, Br, Ce, Co, Cr, Eu, Gd, I, La, Nd, S, Sb, Sc, Sm, Sn, Tb, Th, U, W, Yb
50 g
NIST-1547 Peach leaves - Trace elementsDried leaves from the Coronet variety.
Certified values
Al............................... 249 mg/kg Fe ..............................218 mg/kg Ni ............................. 0.69 mg/kgAs........................... 0.060 mg/kg Hg...........................0.031 mg/kg P ...................................0.137 %B ................................. 29 mg/kg K..................................... 2.43 % Pb ............................ 0.87 mg/kgBa ............................. 124 mg/kg Mg ................................ 0.432 % Rb ............................ 19.7 mg/kgCa ...................................1.56 % Mn ...............................98 mg/kg Se .......................... 0.120 mg/kgCd .......................... 0.026 mg/kg Mo ..........................0.060 mg/kg Sr ................................ 53 mg/kgCl .............................. 360 mg/kg N..................................... 2.94 % V .............................. 0.37 mg/kgCu .............................. 3.7 mg/kg Na................................24 mg/kg Zn............................. 17.9 mg/kg
Indicative values for Br, Ce, Co, Cr, Eu, Gd, I, La, Nd, S, Sb, Sc, Sm, Sn, Tb, Th, U, Yb
50 g
NRMGBW08501 Peach leaves - Trace elementsCertified values
As................................ 0.34 µg/g Fe .................................431 µg/g Pb ............................... 0.99 µg/gBa ............................... 18.4 µg/g Hg..............................0.046 µg/g Sr ................................ 61.6 µg/gCd ............................. 0.018 µg/g K..................................... 2.17 % Zn................................ 22.8 µg/gCs ............................... 10.4 µg/g Mg .................................. 0.47 %Cr ................................ 0.94 µg/g Mn ...............................75.4 µg/g
Indicative values for B, Co, Se
30 g
Plants
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Code Product Unit
NRMGBW07604 Poplar leaves - Trace elementsCertified values
Al...................................0.104 % Eu..............................0.009 µg/g Pb ................................. 1.5 µg/gAs................................ 0.37 µg/g F .....................................22 µg/g Rb ................................. 7.6 µg/gB .................................... 53 µg/g Fe .................................274 µg/g S .....................................0.35 %Ba .................................. 26 µg/g Hg..............................0.026 µg/g Sb ............................. 0.045 µg/gBe ............................. 0.021 µg/g K..................................... 1.38 % Sc.............................. 0.069 µg/gBi............................... 0.027 µg/g La ................................0.26 µg/g Se ............................... 0.14 µg/gBr .................................. 7.2 µg/g Li..................................0.84 µg/g Si.....................................0.71 %Ca ...................................1.81 % Mg .................................. 0.65 % Sm ............................ 0.038 µg/gCd ............................... 0.32 µg/g Mn ..................................45 µg/g Sr ................................. 154 µg/gCe ............................... 0.49 µg/g Mo ...............................0.28 µg/g Th................................ 0.07 µg/gCo ............................... 0.42 µg/g N..................................... 2.56 % Ti................................. 20.4 µg/gCr ................................ 0.55 µg/g Na.................................200 µg/g Yb.............................. 0.018 µg/gCs ............................. 0.053 µg/g Ni ...................................1.9 µg/g Y................................ 0.145 µg/gCu ................................. 9.3 µg/g P.................................1680 µg/g Zn................................... 37 µg/g
Indicative values for Ag, Cl, Dy, Gd, Hf, Nd, U, V
35 g
NRMGBW07602 Bush branches and leaves - Trace elementsCertified values
Ag ............................. 0.027 µg/g Eu..............................0.037 µg/g Rb ................................. 4.2 µg/gAl...................................0.214 % F .....................................24 µg/g S .....................................0.32 %As................................ 0.95 µg/g Fe ...............................1020 µg/g Sb ............................. 0.045 µg/gB .................................... 34 µg/g Hf.................................0.14 µg/g Sc................................ 0.31 µg/gBa .................................. 19 µg/g K..................................... 0.85 % Se ............................. 0.184 µg/gBe ............................. 0.056 µg/g La ................................1.23 µg/g Si.....................................0.58 %Bi............................... 0.027 µg/g Li....................................2.4 µg/g Sm ............................... 0.19µg/gBr .................................. 2.4 µg/g Mg ................................ 0.287 % Sr ................................. 345 µg/gCa ...................................2.22 % Mn ..................................58 µg/g Th................................ 0.37 µg/gCd ............................... 0.14 µg/g Mo ...............................0.26 µg/g Ti.................................... 95 µg/gCe ................................. 2.4 µg/g N..................................... 1.20 % V ................................... 2.4 µg/gCo ............................... 0.39 µg/g Na................................... 1.10 % Yb.............................. 0.063 µg/gCr .................................. 2.3 µg/g Ni ...................................1.7 µg/g Zn................................ 20.6 µg/gCs ............................... 0.27 µg/g P...................................830 µg/gCu ................................. 5.2 µg/g Pb..................................7.1 µg/g
Indicative values for Cl, Nd, Tb, U, W, Y
35 g
NRMGBW07603 Bush branches and leaves - Trace elementsCertified values
Ag ............................. 0.049 µg/g F .....................................23 µg/g Rb ................................. 4.5 µg/gAl.....................................0.20 % Fe ..............................1070 µg/g S .....................................0.73 %As................................ 1.25 µg/g Hf.................................0.14 µg/g Sb ............................. 0.095 µg/gB .................................... 38 µg/g K..................................... 0.92 % Sc................................ 0.32 µg/gBa .................................. 18 µg/g La ................................1.25 µg/g Se ............................... 0.12 µg/gBe ............................. 0.051 µg/g Li....................................2.6 µg/g Si.....................................0.60 %Bi............................... 0.023 µg/g Mg .................................. 0.48 % Sm .............................. 0.19 µg/gBr .................................. 3.0 µg/g Mn ..................................61 µg/g Sr ................................. 246 µg/gCa ...................................1.68 % Mo ...............................0.28 µg/g Tb.............................. 0.025 µg/gCe ................................. 2.2 µg/g N..................................... 1.50 % Th................................ 0.36 µg/gCo ............................... 0.41 µg/g Na................................... 1.96 % Ti.................................... 95 µg/gCr .................................. 2.6 µg/g Nd..................................1.0 µg/g V ................................... 2.4 µg/gCs ............................... 0.27 µg/g Ni ...................................1.7 µg/g Y.................................. 0.68 µg/gCu ................................. 6.6 µg/g P.................................1000 µg/g Yb.............................. 0.063 µg/gEu ............................. 0.039 µg/g Pb...................................47 µg/g Zn................................... 55 µg/g
Indicative values for Cd, Cl, Dy, Gd, Hf, Ho, Lu, Pr, Sn, U, W
35 g
IC-CTA-OTL1 Oriental tobacco leaves - Trace elementsProduced in Poland from oriental tobacco leaves grown in Bulgaria, and air dried before processing.
Certified values
Al................................ 1740 µg/g Cu................................14.1 µg/g Rb ............................... 9.79 µg/gAs.............................. 0.539 µg/g Eu..............................0.038 µg/g S ................................ 7.32 mg/gBa ............................... 84.2 µg/g La ................................1.44 µg/g Se ............................. 0.153 µg/gBr ................................ 9.28 µg/g Li.....................................23 µg/g Sm ............................ 0.229 µg/gCa .............................. 31.7 mg/g K.................................15.6 mg/g Sr ................................. 201 µg/gCd ............................... 1.12 µg/g Mg ..............................4470 µg/g Tb.............................. 0.032 µg/gCe ............................... 2.69 µg/g Mn ................................412 µg/g Th.............................. 0.348 µg/gCo ............................. 0.879 µg/g Ni .................................6.32 µg/g V ................................. 3.08 µg/gCr ................................ 2.59 µg/g P.................................2892 µg/g Zn................................ 49.9 µg/gCs ............................. 0.177 µg/g Pb................................4.91 µg/g
Uncertified values for trace elements Au, CI, Fe, Hf, Hg, Mo, Na, Sb, Sc, U and Yb
50 g
Plants
60 Edition 2003/2004 www.lgcpromochem.com
Code Product Unit
IC-CTA-VTL2 Virginia tobacco leaves - Trace elementsProduced in Poland from Virginia Tobacco leaves grown in Bulgaria, and air dried before processing.
Certified values
As.............................. 0.969 µg/g Fe ...............................1083 µg/g Pb ............................... 22.1 µg/gBa ............................... 42.7 µg/g Hf...............................0.118 µg/g Rb ............................... 48.6 µg/gBr .................................. 4.3 µg/g Hg..............................0.048 µg/g Sb ............................. 0.312 µg/gCa .............................. 3.60 wt % K................................1.03 wt. % Sm ............................ 0.157 µg/gCd ............................... 1.52 µg/g La ................................1.01 µg/g Sr ................................. 110 µg/gCe ............................... 1.91 µg/g Li..................................23.0 µg/g Tb.............................. 0.022 µg/gCl ............................. 0.743 wt % Mg ...........................0.510 wt. % Th.............................. 0.378 µg/gCo ............................. 0.429 µg/g Mn ...............................79.7 µg/g U ............................... 0.163 µg/gCr ................................ 1.87 µg/g Mo ...............................2.01 µg/g V ................................. 4.00 µg/gCs ............................. 0.515 µg/g Ni .................................1.98 µg/g W .............................. 0.233 µg/gCu ............................... 18.2 µg/g P.................................2204 µg/g Zn................................ 43.3 µg/g
Informational values for AI, Eu, Na, S, Sc, Se, Si, Ta, Ti and Yb
25 g
IC-INCT-TL-1 Tea leaves - Trace elementsThe material was prepared from black tea, usually packed in tea bags.
Certified values
Al.............................. 0.229 wt % Eu...........................0,050 mg/kg Sc........................... 0.266 mg/kgAs........................... 0.106 mg/kg Hg...........................0.005 mg/kg Sm ......................... 0.177 mg/kgBa ............................ 43.2 mg/kg K.................................1.70 wt % Sr ............................. 20.8 mg/kgBr ............................. 12.3 mg/kg La .............................1.00 mg/kg Tb........................... 0.026 mg/kgCa ............................ 0.582 wt % Lu ...........................0.016 mg/kg Th........................... 0.034 mg/kgCd .......................... 0.030 mg/kg Mg ............................0.224 wt % Tl............................ 0.063 mg/kgCl .............................. 573 mg/kg Mn ............................0.157 wt % V .............................. 1.97 mg/kgCo .......................... 0.387 mg/kg Na.............................24.7 mg/kg Yb........................... 0.118 mg/kgCr ............................. 1.91 mg/kg Ni ..............................6.12 mg/kg Zn............................. 34.7 mg/kgCs ............................ 3.61 mg/kg Pb.............................1.78 mg/kgCu ............................ 20.4 mg/kg Rb.............................81.5 mg/kg
Indicative values for B, Fe, Hf, Nd, P, Sb, Se, Ta, Ti and Tm
50 g
NRMGBW07605 Tea - Trace elementsCertified values
As................................ 0.28 µg/g Cu................................17.3 µg/g Pb ................................. 4.4 µg/gB .................................... 15 µg/g Eu..............................0.018 µg/g Rb .................................. 74 µg/gBa .................................. 58 µg/g F ...................................320 µg/g S ...................................0.245 %Be ............................. 0.034 µg/g Fe .................................264 µg/g Sb ............................. 0.056 µg/gBi............................... 0.063 µg/g K..................................... 1.66 % Sc.............................. 0.085 µg/gBr .................................. 3.4 µg/g Mg .................................. 0.17 % Sm ............................ 0.085 µg/gCa ...................................0.43 % Mn ..............................1240 µg/g Sr ................................ 15.2 µg/gCd ............................. 0.057 µg/g Mo .............................0.038 µg/g Th.............................. 0.061 µg/gCe ................................. 1.0 µg/g N..................................... 3.32 % Ti.................................... 24 µg/gCo ............................... 0.18 µg/g Na...................................44 µg/g Y.................................. 0.36 µg/gCr .................................. 0.8 µg/g Ni ...................................4.6 µg/g Yb.............................. 0.044 µg/gCs ............................... 0.29 µg/g P.................................2840 µg/g Zn................................ 26.3 µg/g
Indicative values for Ag, Al, Dy, Gd, Hf, Hg, Ho, Li, Lu, Nd, Pr, Se, Si, Tb, V
35 g
BCR-683 Wood - PCP and PAHsCompound Certified value Uncertainty
mg/kg mg/kg
Pentachlorophenol............................................... 3.6............................ 0.5Benzo(a)anthracene ............................................ 6.5............................ 0.7Benzo(a)pyrene ................................................... 3.4............................ 0.4Benzo(e)pyrene ................................................... 9.3............................ 1.0Benzo(b)fluoranthene .......................................... 5.8............................ 0.6Benzo(k)fluoranthene ........................................ 2.58.......................... 0.29
60 g
Grasses and crops
BCR-129 Hay powder - Trace elementsCertified values
Ca ................................. 6.4 g/kg Mg ...............................1.45 g/kg S ................................. 3.16 g/kgI .............................. 0.167 mg/kg N..................................37.2 g/kg Zn............................ 0.0321 g/kgK ................................. 33.8 g/kg P..................................2.36 g/kg Kjeldahl-N ................... 34.2 g/kg
Indicative values for Cu, Fe, Mo, Se
30 g
IAEA-V-10 Hay - Trace elementsCertified values
Ba ................................. 6 mg/kg Cu...............................9.4 mg/kg P ............................. 2300 mg/kgBr .................................. 8 mg/kg Fe ..............................185 mg/kg Pb .............................. 1.6 mg/kgCa ......................... 21600 mg/kg Hg...........................0.013 mg/kg Rb .............................. 7.6 mg/kgCd ............................ 0.03 mg/kg Mg ...........................1360 mg/kg Sc........................... 0.014 mg/kgCo ............................ 0.13 mg/kg Mo ..............................0.9 mg/kg Sr ................................ 40 mg/kgCr ............................... 6.5 mg/kg Ni ...................................4 mg/kg Zn................................ 24 mg/kg
Indicative values for Al, K, Mn, Na
50 g
Plants
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Code Product Unit
NIST-2695 Vegetation - FluorideTwo samples of timothy grass with fluoride concentrations above natural levels.
Low level
Certified value
Fluoride....................... 64.0 µg/g
High level
Certified value
Fluoride........................ 277 µg/g
2 x 25 g
IAEA-373 Grass - Radioactive isotopesCertified values134Cs.........................1167 Bq/kg 40K ............................. 432 Bq/kg127Cs.......................12350 Bq/kg 90Sr .......................... 1312 Bq/kg
200 g
NIST-RM 8412 Corn (Zea Mays) stalk - Trace elementsReference concentration values for major, minor and trace elements. Indicative values for additional elements.
34 g
NIST-RM 8413 Corn (Zea Mays) kernel - Trace elementsReference values for Al, Ca, Cl, Cu, F, I, K, Mg, Mn, N, Se, Zn
47 g
IAEA-V-9 Cellulose (cotton) - Trace elementsCertified values
Ba ................................. 9 mg/kg Hg.............................0.06 mg/kg Ni ............................. 0.09 mg/kgCa ............................. 240 mg/kg Mg ...............................53 mg/kg Pb ............................ 0.25 mg/kgCl .............................. 600 mg/kg Mn ............................0.15 mg/kg Sr ............................. 0.65 mg/kgCr ............................. 0.11 mg/kg Mo ..........................0.034 mg/kgCu ............................ 0.59 mg/kg Na................................56 mg/kg
Indicative values for Al, Br, Fe, V
25 g
BCR-402 White clover - Trace elementsCollected from an area with soil especially rich in selenium, resulting in a high selenium content
Certified values
As........................... 0.093 mg/kg Mo ............................6.93 mg/kgCo .......................... 0.178 mg/kg Se.............................6.70 mg/kg
Indicative values for Cr, Fe, Ni, Zn
25 g
IAEA-156 Clover - Radioactive isotopesCertified values134Cs...........................132 Bq/kg 40K ............................. 657 Bq/kg137Cs...........................264 Bq/kg 90Sr ........................... 14.8 Bq/kg
250 g
Aquatic plants
BCR-060 Aquatic plant (Lagarosiphon major) - Trace elementsCertified values
Al............................. 4180 mg/kg Hg.............................0.34 mg/kg Zn.............................. 313 mg/kgCd ............................ 2.20 mg/kg Mn ...........................1759 mg/kgCu ............................ 51.2 mg/kg Pb.............................63.8 mg/kg
Indicative values for Ag, As, Au, B, Br, CaO, Ce, Cl, Co, Cr, Cs, Eu, F, FeeO3, K2O, La, MgO, Mo, N, Na2O, Ni,P2O5, Rb, S, Sb, Sc, Se, SiO2, Sn, Ta, Tb, TiO2, Tl, U, V, W
25 g
BCR-596 Aquatic plant (trapa natans) - ChromiumCertified value
Cr ............................. 36.3 mg/kg
25 g
BCR-279 Sea lettuce (ulva lactuca) - Trace elementsCertified values
As............................. 3.09 mg/kg Cu...........................13.14 mg/kg Se .......................... 0.593 mg/kgCd .......................... 0.274 mg/kg Pb...........................13.48 mg/kg Zn............................. 51.3 mg/kg
Indicative values for B, C, Ca, Cl, Cr, Fe, Hg, I, K, Mg, Mn, N, P
35 g
BCR-670 Aquatic plant (Lemna minor) - Trace elementsCertified values
Ce .............................. 987 µg/kg La ...............................487 µg/kg Tb.............................. 14.0 µg/kgDy.............................. 78.9 µg/kg Lu ..............................6.33 µg/kg Th............................... 159 µg/kgEr .............................. 44.0 µg/kg Nd...............................473 µg/kg Tm............................. 5.70 µg/kgEu ............................ 23.2 µg/kg Pr................................121 µg/kg U ................................ 81.7µg/kgGd ............................. 97.8 µg/kg Sc ...............................191 µg/kg Y................................. 462 µg/kgHo ............................. 15.8 µg/kg Sm.............................94.2 µg/kg Yb.............................. 39.9 µg/kg
Indicative values for : As, Cd, Cr, Cs, Cu, Fe, Mo, Ni, Pb, Sb, Se and Zn
10 g
Plants
62 Edition 2003/2004 www.lgcpromochem.com
Code Product Unit
IAEA-140OC Fucus (sea plant homogenate) - Organic contaminantsCertified values
beta-HCH..................................................... 4.6 ng/g Indeno(1,2,3-cd)pyrene................................. 33 ng/g4,4’-DDE ...................................................... 1.2 ng/g UVF equval. Chrysene.............................. 3500 ng/g4,4’-DDD .................................................... 0.72 ng/g UVF equival. ROPME oil......................... 29000 ng/g4,4’-DDT ...................................................... 2.2 ng/g Resolved Aliphatics................................. 13000 ng/gDieldrin......................................................... 1.7 ng/g Unresolved Aliphatics ............................. 26000 ng/gHCB ............................................................. 1.3 ng/g Total Aromatics ......................................... 5800 ng/galpha-HCH ................................................... 1.4 ng/g Resolved Aromatics .................................... 350 ng/ggamma-HCH................................................. 11 ng/g Unresolved Aromatics............................... 8100 ng/gHeptachlor ...................................................... 3 ng/g Fluorene....................................................... 6.5 ng/gHeptachlor epoxide.................................... 0.79 ng/g Benzo(b)fluoranthene.................................... 37 ng/gAldrin.......................................................... 0.76 ng/g Perylene .......................................................... 5 ng/gEndrin ........................................................ 0.71 ng/g 1-Methylnaphthalene..................................... 13 ng/galpha-Endosulfan......................................... 0.9 ng/g 2-Methylnaphthalene..................................... 16 ng/galpha-Chlordane .......................................... 1.4 ng/g PCB 18......................................................... 1.5 ng/gAroclor 1254 ................................................. 25 ng/g PCB 28......................................................... 1.7 ng/gAroclor 1260 ................................................. 12 ng/g PCB 31......................................................... 1.8 ng/gTotal Aliphatics ....................................... 27000 ng/g PCB 44............................................................ 2 ng/gn-C17 .......................................................... 890 ng/g PCB 49......................................................... 1.6 ng/gPristane......................................................... 50 ng/g PCB 52......................................................... 3.8 ng/gn-C18 ............................................................ 99 ng/g PCB 66....................................................... 0.89 ng/gPhytane......................................................... 56 ng/g PCB 70......................................................... 1.8 ng/gSum n Alkanes (C14-C34)...................... 11000 ng/g PCB 77....................................................... 0.19 ng/gPhenanthrene ............................................... 76 ng/g PCB 87......................................................... 1.6 ng/g2-Methylphenanthrene .................................. 19 ng/g PCB 99......................................................... 0.9 ng/g1-Methylphenanthrene .................................. 11 ng/g PCB 101....................................................... 2.4 ng/gAnthracene ................................................... 14 ng/g PCB 105..................................................... 0.49 ng/gChrysene....................................................... 40 ng/g PCB 118.......................................................... 1 ng/gFluoranthene................................................. 88 ng/g PCB 138....................................................... 1.7 ng/gPyrene........................................................... 67 ng/g PCB 149....................................................... 1.2 ng/gBenzo(k)fluoranthene ................................... 19 ng/g PCB 153....................................................... 1.7 ng/gBenzo(a)anthracene ..................................... 25 ng/g PCB 156..................................................... 0.17 ng/gBenzo(e)pyrene ............................................ 26 ng/g PCB 170..................................................... 0.21 ng/gBenzo(a)pyrene ............................................ 20 ng/g PCB 180..................................................... 0.43 ng/gNaphthalene ................................................. 17 ng/g PCB 187..................................................... 0.38 ng/gBenzo(ghi)perylene....................................... 20 ng/g
35 g
IAEA-140TM Fucus (sea plant homogenate) - Trace elements and methylmercuryCertified values
As............................. 44.3 mg/kg K............................31100 mg/kg Sb .......................... 0.103 mg/kgBr .............................. 567 mg/kg Li...............................2.29 mg/kg Sr .............................. 750 mg/kgCa ......................... 12730 mg/kg Mg ...........................9070 mg/kg Th........................... 0.299 mg/kgCd .......................... 0.537 mg/kg Mn ............................56.1 mg/kg U .............................. 0.73 mg/kgCo .......................... 0.876 mg/kg Mo ............................2.65 mg/kg V .............................. 3.67 mg/kgCr ............................. 10.4 mg/kg Na..........................32000 mg/kg Zn............................. 47.3 mg/kgCu ............................ 5.05 mg/kg Ni ..............................3.79 mg/kg Methylmercury.. 0.000626 mg/kgFe............................ 1256 mg/kg Pb.............................2.19 mg/kgHg .......................... 0.038 mg/kg Rb.............................16.4 mg/kg
Indicative values for Ag, Al, Ba, Ce, Cs, Hf, La, Sc, Se, Sm
14 g
NIES03 Chlorella (green algae) - Trace elementsCertified values
Ca ...................................0.49 % Fe ................................. 0.185 % Mn.................................. 69 µg/gCo ............................... 0.87 µg/g K..................................... 1.24 % Sr ................................... 40 µg/gCu ................................. 3.5 µg/g Mg .................................. 0.33 % Zn................................ 20.5 µg/g
Indicative values for Cd, P, Pb, Sc
36 g
Miscellaneous
LGC7162 Strawberry leaves - Trace elementsThe raw material was collected from a private farm in the Czech Republic. The mixture was cut and jet milled topass a 250 µm nylon sieve. The resulting powder was homogenised, separated in 20 g portions and placed in60mL bottles.
Certified Values
Ca .......................... 1.53 g/100 g As .............................0.28 mg/kg Pb .............................. 1.8 mg/kgMg........................ 0.377 g/100 g Ba..............................107 mg/kg Mn............................. 171 mg/kgN ............................ 2.01 g/100 g Cd.............................0.17 mg/kg Hg .......................... 0.027 mg/kgP .......................... 0.260 g/100 g Co.............................0.47 mg/kg Ni ............................... 2.6 mg/kgK ............................ 1.96 g/100 g Cr..............................2.15 mg/kg Sr ................................ 64 mg/kgS .......................... 0.174 g/100 g Fe ..............................818 mg/kg Zn................................ 24 mg/kg
20 g
Plants
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Code Product Unit
NIST-1570a Spinach leaves - Trace elementsCertified values
Al............................... 310 mg/kg Hg...........................0.030 mg/kg Se .......................... 0.117 mg/kgAs........................... 0.068 mg/kg K................................... 2.903 % Sr ............................. 55.6 mg/kgB .............................. 37.6 mg/kg Mn ............................75.9 mg/kg Th............................. 0.48 mg/kgCd ............................ 2.89 mg/kg N..................................... 5.90 % V ............................ 0.835 mg/kgCa .................................1.527 % Na................................. 1.818 % Zn............................. 30.9 mg/kgCo ............................ 0.39 mg/kg Ni ..............................2.14 mg/kgCu ............................ 12.2 mg/kg P................................... 0.518 %
Indicative values for Ba, Br, Ce, Cl, Cs, I, La, Mg, Mo, S, Sc, Sm, Sr, U
60 g
NIST-1573a Tomato leaves - Trace elementsCertified values
Al............................... 598 mg/kg Cu.............................4.70 mg/kg P ...................................0.216 %As........................... 0.112 mg/kg Hg...........................0.034 mg/kg Rb .......................... 14.89 mg/kgB .............................. 33.3 mg/kg K..................................... 2.70 % Sb .......................... 0.063 mg/kgCd ............................ 1.52 mg/kg Mn .............................246 mg/kg Se .......................... 0.054 mg/kgCa ...................................5.05 % N..................................... 3.03 % V .............................. 0.57 mg/kgCo ............................ 0.57 mg/kg Na..............................136 mg/kg Zn................................ 82 mg/kgCr ............................. 1.99 mg/kg Ni ..............................1.59 mg/kg
Indicative values for Eu, Gd, Mg, Pb, S, Sc, Sm, Sr, Th, U
50 g
IC-INCT-MPH-2 Mixed polish herbs - Trace elementsFresh herbs collected in a non contaminated rural area were collected, mixed and processed as for drugproduction by Herbapol S.A.
Certified values
Al............................... 670 mg/kg Eu...........................0.016 mg/kg S ............................. 0.241 wt %As........................... 0.191 mg/kg Hf............................0.236 mg/kg Sb .......................... 0.066 mg/kgBa ............................ 32.5 mg/kg Hg...........................0.018 mg/kg Sc........................... 0.123 mg/kgBr ............................. 7.71 mg/kg K.................................1.91 wt % Sm ......................... 0.094 mg/kgCa .............................. 1.08 wt % La ...........................0.571 mg/kg Sr ............................. 37.6 mg/kgCd .......................... 0.199 mg/kg Lu ...........................0.009 mg/kg Ta........................... 0.019 mg/kgCe ............................ 1.12 mg/kg Mg ............................0.292 wt % Tb........................... 0.014 mg/kgCl ............................. 0.284 wt % Mn .............................191 mg/kg Th........................... 0.154 mg/kgCo .......................... 0.210 mg/kg Nd...........................0.457 mg/kg V ............................ 0.952 mg/kgCr ............................. 1.69 mg/kg Ni ..............................1.57 mg/kg Yb........................... 0.053 mg/kgCs .......................... 0.076 mg/kg Pb.............................2.16 mg/kgCu ............................ 7.77 mg/kg Rb.............................10.7 mg/kg
Indicative values for P, Fe, Mo, Na, Ti, Tl, U and W
50 g
BCR-482 Lichen - Trace elementsCertified values
Al............................. 1103 mg/kg Cr..............................4.12 mg/kg Ni ............................. 2.47 mg/kgAs............................. 0.85 mg/kg Cu.............................7.03 mg/kg Pb ............................ 40.9 mg/kgCd ............................ 0.56 mg/kg Hg.............................0.48 mg/kg Zn........................... 100.6 mg/kg
15 g
IAEA-336 Lichen - Trace elementsCertified values
As............................. 0.63 mg/kg Fe ..............................430 mg/kg Se ............................ 0.22 mg/kgBa .............................. 6.4 mg/kg Hg...............................0.2 mg/kg Sm ......................... 0.106 mg/kgBr ............................. 12.9 mg/kg K..............................1840 mg/kg SR.............................. 9.3 mg/kgCe ............................ 1.28 mg/kg La .............................0.66 mg/kg Th............................. 0.14 mg/kgCo ............................ 0.29 mg/kg Mn ...............................63 mg/kg Zn............................. 30.4 mg/kgCs ............................ 0.11 mg/kg Na..............................320 mg/kgCu .............................. 3.6 mg/kg Sb...........................0.073 mg/kg
Indicative values for Al, Cd, Cl, Cr, Eu, Lu, Nd, P, Pb, Rb, Sc, Tb, V, Yb
20 g
BCR-302 Microcrystalline cellulose (water content above saturated solutions)Intended to check the correct application of the COST procedure for determination of water sorption isotherms offood. Water contents at ten water activities are given.
20 g
BCR-273 Single cell protein - Major elementsCertified value
Ca ............................. 11.97 g/kg K..................................2.22 g/kg P ................................. 26.8 g/kgFe.............................. 156 mg/kg N................................121.6 g/kg
Indicative values for Mg, N(Kjeldahl), Na, S
10 g
BCR-274 Single cell protein - Trace elementsCertified values
As............................... 132 µg/kg Cu..............................13.1 µg/kg Se ............................ 1.03 mg/kgCd ................................ 30 µg/kg Mn ............................51.9 mg/kg Zn................................ 42.7 µg/gCo ................................ 39 µg/kg Pb.................................44 µg/kg
Indicative values for F, I, Ni
10 g
Solid fuels
64 Edition 2003/2004 www.lgcpromochem.com
Solid fuelsCode Product Unit
BCR-180 Gas coal - Elements, ash and gross calorific valueA high volatile, weakly coking coal of moderately high ash content.
Certified values
As............................. 4.23 mg/kg Hg...........................0.123 mg/kg V .............................. 19.3 mg/kgC ............................... 760.1 g/kg Mn ............................34.3 mg/kg Zn............................. 27.4 mg/kgCd .......................... 0.212 mg/kg N..................................14.4 g/kg Ash.............................. 99.0 g/kgCl .............................. 593 mg/kg Pb.............................17.5 mg/kg GCV ........................31.89 MJ/kgH ................................. 50.4 g/kg Se.............................1.32 mg/kg
Indicative values for Al, B, Ba, Br, Ce, Co, Cr, Cu, Fe, K, La, Na, Ni, Rb, Sc, Th, Ti, Vol. matter
20 g
BCR-181 Coking coal - Elements, ash and gross calorific valueA high volatile, strongly coking coal of low ash and moderate sulphur content.
Certified values
As............................. 27.7 mg/kg Hg...........................0.138 mg/kg Zn............................... 8.4 mg/kgC ............................... 849.9 g/kg N..................................17.8 g/kg Ash.............................. 18.5 g/kgCd .......................... 0.051 mg/kg Pb.............................2.59 mg/kg GCV ........................35.43 MJ/kgCl ................................ 1.38 g/kg Se.............................1.15 mg/kgH ................................. 54.0 g/kg V...............................12.0 mg/kg
Indicative values for Al, B, Br, Ce, Co, Cr, Cu, Fe, K, La, Mn, Na, Ni, Rb, Sc, Th, Ti, Vol. matter
20 g
BCR-182 Steam coal - Elements, ash and gross calorific valueA medium volatile coal of high ash content.
Certified values
C ............................... 732.9 g/kg Mn .............................195 mg/kg Zn............................. 33.3 mg/kgCd .......................... 0.057 mg/kg N................................16.36 g/kg Ash............................ 122.7 g/kgCl ................................ 3.70 g/kg Se.............................0.68 mg/kg GCV ........................29.68 MJ/kgHg .......................... 0.040 mg/kg V...............................24.3 mg/kg
Indicative values for Al, As, B, Br, Ce, Co, Cr, Cu, Fe, H, K, La, Mn, Na, Ni, Pb, Rb, Sc, Th, Ti, Vol. matter
20 g
BCR-065 Coal - Sulphur, ash and gross calorific valueCertified values
S ................................... 8.3 g/kg Ash ..............................39.1 g/kg GCV ......................34.915 MJ/kg
150 g
BCR-331 Low volatile steam coal - SulphurCertified value
S ................................. 4.99 g/kg
20 g
BCR-332 High volatile industrial coal - SulphurCertified value
S ................................. 9.61 g/kg
20 g
BCR-333 Coking steam coal - SulphurCertified value
S ............................... 13.44 g/kg
20 g
BCR-334 Anthracite - SulphurCertified value
S ............................... 16.09 g/kg
20 g
BCR-335 Flame coal - SulphurCertified value
S ................................. 50.8 g/kg
20 g
BCR-336 High volatile steam coal - SulphurCertified value
S ............................... 32.90 g/kg
20 g
BCR-460 Coal - FluorineCertified value
F................................ 225 mg/kg
Indicative value for Cl
40 g
NIST-1630A Bitiminous coal - Chlorine and sulphurCertified values
Cl ............................ 1144 mg/kgS ...................................1.462 %
Indicative values for Hg, Furnace ash, HHV2
50 g
Solid fuels
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Code Product Unit
NIST-2682b Coal (sub-bituminous) - Sulphur, mercury and heat of combustionCertified values
S ................................................................ 0.4917 % Heat of combustion ................................25.66 MJ/kgHg ...........................................................108.8 µg/kg
Indicative values for Ash content, Gross calorific value
50 g
NIST-2683b Coal (bituminous) - SulphurCertified value
S ...................................1.955 %
Indicative value for Furnace ash
50 g
NIST-2684b Coal (bituminous) - Sulphur, mercury and heat of combustionCertified values
S .................................................................. 3.076 % Heat of combustion ................................28.56 MJ/kgHg .............................................................97.4 µg/kg
Indicative values for Ash content, Gross calorific value
50 g
NIST-2692b Coal (bituminous) - Sulphur and mercuryCertified values
S .................................................1.170 % ± 0.020 % Hg........................................ 133.3 µg/kg ± 4.1 µg/kg
Reference values (dry basis) for ash content (mass fraction) and gross calorific value
50 g
NIST-2685 Coal (bituminous) - Sulphur and mercuryCertified values
S ...................................4.730 % Hg............................146.2 µg/kg
Indicative values for Ash content, Gross calorific value
50 g
NIST-1632c Coal (bituminous) - ElementsCertified values
H ......................................5.11% Ba.............................41.1 mg/kg Selenium................ 1.326 mg/kgS ...................................1.462 % Co.............................3.48 mg/kg Sodium................... 298.8 mg/kgPotassium...................0.1100 % Mn ..........................13.04 mg/kg Strontium ................. 63.8 mg/kgChlorine ......................0.1139 % Hg.........................0.0938 mg/kg Thorium.................... 1.40 mg/kgSb .......................... 0.461 mg/kg Rb.............................7.52 mg/kg Zinc .......................... 12.1 mg/kg
Indicative values for Carbon (total), N , Si, Al, As, B, Br, Ca, Cd, Ce, Cr, Cs, Co, Eu, Fe, Hf, Mg, Ni, Pb, Sm,Sc,Ti, U, V, Ash
50 g
NIST-1635 Coal - Trace elementsCertified values
As............................. 0.42 mg/kg Fe ................................. 0.239 % Se .............................. 0.9 mg/kgCd ............................ 0.03 mg/kg Mn ............................21.4 mg/kg Th............................. 0.62 mg/kgCr ............................... 2.5 mg/kg Ni ..............................1.74 mg/kg U .............................. 0.24 mg/kgCu .............................. 3.6 mg/kg Pb...............................1.9 mg/kg V ................................ 5.2 mg/kgF............................... 25.9 mg/kg S................................. 0.3616 % Zn............................... 4.7 mg/kg
Indicative values for Al, Ce, Co, Eu, Ga, Hf, Hg, Na, Sb, Sc, Ti
75 g
NRMGBW11101c Coal - Elements and propertiesCertified values
C .................................................................. 74.33 % Ash.................................................................9.23 %H .................................................................... 4.54 % Volatile matter ..............................................32.88 %N .................................................................... 1.39 % Relative density (20°C) ...................................... 1.41S .................................................................... 0.49 % Gross calorific value...............................30.05 MJ/kg
50 g
NRMGBW11102c Coal - Elements and propertiesCertified values
C .................................................................. 46.54 % Ash...............................................................40.64 %H .................................................................... 3.05 % Volatile matter ..............................................23.18 %N .................................................................... 0.86 % Relative density (20°C) ...................................... 1.73S .................................................................... 1.40 % Gross calorific value...............................18.72 MJ/kg
50 g
NRMGBW11103b Coal - Elements and propertiesCertified values
C .................................................................. 76.80 % Ash...............................................................17.39 %H .................................................................... 1.40 % Volatile matter ................................................6.59 %N .................................................................... 0.54 % Relative density (20°C) ...................................... 1.86S .................................................................... 0.36 % Gross calorific value...............................26.84 MJ/kg
50 g
Solid fuels
66 Edition 2003/2004 www.lgcpromochem.com
Code Product Unit
NRMGBW11104b Coal - Elements and propertiesCertified values
C .................................................................. 68.58 % Ash...............................................................26.35 %H .................................................................... 0.68 % Volatile matter ................................................5.94 %N .................................................................... 0.21 % Relative density (20°C) ...................................... 2.10S .................................................................... 1.01 % Gross calorific value...............................23.03 MJ/kg
50 g
NRMGBW11105a Coal - Elements and propertiesCertified values
C .................................................................. 76.45 % Ash...............................................................13.88 %H .................................................................... 3.33 % Volatile matter ..............................................11.80 %N .................................................................... 1.17 % Relative density (20°C) ...................................... 1.49S .................................................................... 1.73 % Gross calorific value...............................29.89 MJ/kg
50 g
NRMGBW11107b Coal - Elements and propertiesCertified values
C .................................................................. 78.57 % Ash.................................................................8.43 %H .................................................................... 4.54 % Volatile matter ..............................................28.89 %N .................................................................... 1.41 % Relative density (20°C) ...................................... 1.39S .................................................................... 0.88 % Gross calorific value...............................31.94 MJ/kg
50 g
NRMGBW11108b Coal - Elements and propertiesCertified values
C .................................................................. 72.28 % Ash...............................................................11.08 %H .................................................................... 4.60 % Volatile matter ..............................................33.52 %N .................................................................... 1.32 % Relative density (20°C) ...................................... 1.42S .................................................................... 1.93 % Gross calorific value...............................29.61 MJ/kg
50 g
NRMGBW11109b Coal - Elements and propertiesCertified values
C .................................................................. 68.69 % Ash...............................................................13.89 %H .................................................................... 4.50 % Volatile matter ..............................................34.08 %N .................................................................... 1.18 % Relative density (20°C) ...................................... 1.45S .................................................................... 3.04 % Gross calorific value...............................28.32 MJ/kg
50 g
NRMGBW11110b Coal - Elements and propertiesCertified values
C .................................................................. 58.75 % Ash...............................................................29.71 %H .................................................................... 2.64 % Volatile matter ..............................................11.21 %N .................................................................... 0.92 % Relative density (20°C) ...................................... 1.72S .................................................................... 4.70 % Gross calorific value...............................23.00 MJ/kg
50 g
NRMGBW11111a Coal - Elements and propertiesCertified values
C .................................................................. 78.60 % Ash.................................................................9.99 %H .................................................................... 4.53 % Volatile matter ..............................................25.22 %N .................................................................... 1.37 % Relative density (20°C) ...................................... 1.38S .................................................................... 1.38 % Gross calorific value...............................32.12 MJ/kg
50 g
NRMGBW11112a Coal - Elements and propertiesCertified values
C .................................................................. 69.05 % Ash...............................................................21.26 %H .................................................................... 3.04 % Volatile matter ..............................................11.86 %N .................................................................... 1.03 % Relative density (20°C) ...................................... 1.58S .................................................................... 2.20 % Gross calorific value...............................26.96 MJ/kg
50 g
NRMGBW11113a Coal - Elements and propertiesCertified values
C .................................................................. 49.98 % Ash...............................................................40.62 %H .................................................................... 2.22 % Volatile matter ..............................................10.69 %N .................................................................... 0.64 % Relative density (20°C) ...................................... 1.85S .................................................................... 3.40 % Gross calorific value...............................19.21 MJ/kg
50 g
NIST-2775 Foundry coke - SulphurCertified value
S .................................0.5816 %
Indicative values for Furnace ash, Volatile matter
50 g
NIST-2776 Foundry coke - Sulphur, ash and volatile matterCertified values
S ...................................0.825 %Furnace ash....................8.06 %Volatile matter.................0.98 %
50 g
Solid fuels
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Code Product Unit
NIST-2718 Green petroleum coke - Trace elementsCertified values
Al.............................. 16.5 mg/kg Fe ..............................290 mg/kg S ........................... 47032 mg/kgCa ............................. 174 mg/kg Ni ............................139.1 mg/kg V ............................... 302 mg/kg
Indicative values for C, Co, H, N, Na, Si, Ash, Volatile matter, Gross calorific value
50 g
NIST-2719 Calcinated petroleum coke - Trace elementsCertified values
Al.............................. 58.9 mg/kg Fe ...........................201.6 mg/kg S ............................. 8877 mg/kgCa ............................ 57.7 mg/kg Ni ...............................204 mg/kg V .............................. 58.6 mg/kg
Indicative values for C, Co, H, N, Na, Si, Ash, Volatile content, Gross calorific value
50 g
NRMGBW11106a Metallurgy coke - Phosphorous, sulphur and ashCertified values
P ...................................0.034 %S .....................................0.58 %Ash...............................13.05 %,
Indicative values for Volatile matter, Calorific value
90 g
NJV 94-1 Energy peat (Carex) - Trace elementsMilled peat from Sweden with an approximate composition of 80:20 Carex: Sphagnum.
Certified values
Al...................................0.090 % Fe ................................... 0.39 % Pb .............................. 2.4 mg/kgCa ...................................1.02 % Mg ................................ 0.077 % S .....................................0.29 %Cd .......................... 0.062 mg/kg Mn .............................. 0.0036 % Zn.................................. 9 mg/kgCl ..................................0.028 % N..................................... 2.09 % Ash..................................4.07 %Cu .............................. 2.0 mg/kg P................................... 0.045 % Calorific value ...........22.3 MJ/kg
Indicative values for As, C, Cr, H, K, Na, Si, Ti, Volatile matter
50 g
NJV 94-2 Energy peat (sphagnum) - Trace elementsSod peat from Sweden with an approximate composition of 90:10 Sphagnum: Peat wool.
Certified values
Al...................................0.095 % Fe ................................... 0.13 % Pb ............................ 10.1 mg/kgCa ...................................0.12 % Mg .................................. 0.11 % S ...................................0.217 %Cd ............................ 0.16 mg/kg Mn .............................. 0.0008 % Zn.................................. 9 mg/kgCl ..................................0.061 % N..................................... 1.10 % Ash..................................1.57 %Cu .............................. 1.7 mg/kg P................................... 0.024 % Calorific value ...........21.8 MJ/kg
Indicative values for C, Cr, H, K, Na, Si, Ti, Volatile matter
50 g
NJV 94-3 Energy forest (salix) - Trace elementsSalix cultivated in Sweden.
Certified values
Ca ...................................0.44 % Mg ................................ 0.034 % Zn................................ 75 mg/kgCd .............................. 1.8 mg/kg Mn ................................ 0.006 % Ash..................................1.56 %Cu .............................. 4.0 mg/kg N..................................... 0.37 % Calorific value ...........19.5 MJ/kgFe................................0.0026 % P..................................... 0.05 %K .....................................0.20 % S................................... 0.028 %
Indicative values for Al, C, Cl, H, Na, Si, Pb, Volatile matter
50 g
NJV 94-4 Energy grass (phalaris arudinaceae L.) - Trace elementsSpring harvested reed canary grass (Phalaris arudinaceae L.) from Sweden.
Certified values
Al.....................................0.18 % Fe ................................. 0.106 % S ...................................0.132 %As............................... 0.4 mg/kg K..................................... 0.38 % Si.......................................2.1 %Ca ...................................0.21 % Mg ................................ 0.088 % Zn................................ 42 mg/kgCd ............................ 0.09 mg/kg Mn ................................ 0.016 % Ash..................................6.87 %Cl ..................................0.058 % N..................................... 1.04 % Calorific value ...........18.5 MJ/kgCr ............................... 3.4 mg/kg P................................... 0.109 %Cu .............................. 6.8 mg/kg Pb...............................2.1 mg/kg
Indicative values for C, H, Na, Ti, Volatile matter
50 g
NJV 94-5 Wood fuel - Trace elementsPine wood waste from a saw mill in Sweden with a composition of approximately 70:30 bark: chip
Certified values
Al...................................0.026 % Fe ................................. 0.007 % Pb ............................ 0.68 mg/kgAs............................... 0.8 mg/kg K..................................... 0.09 % S ...................................0.018 %Ca ...................................0.35 % Mg ................................ 0.030 % Zn................................ 38 mg/kgCd ............................ 0.27 mg/kg Mn ................................ 0.021 % Ash...................................1.22%Cr ............................... 0.8 mg/kg Na................................. 0.004 % Calorific value ...........20.6 MJ/kgCu .............................. 2.2 mg/kg P................................... 0.021 %
Indicative values for C, Cl, H, N, Si, Ti, Volatile matter
50 g
Oils and liquid fuels
68 Edition 2003/2004 www.lgcpromochem.com
Oils and liquid fuelsCode Product Unit
LGC3000 Gas oil - SulphurCertified value
S ...................................0.010 %
50 mL
LGC3001 Gas oil - SulphurCertified value
S ...................................0.047 %
50 mL
LGC3002 Gasoline - BenzeneCertified value
Benzene..........................0.76 %
5 x 5 mL
LGC3003 Gasoline - BenzeneCertified value
Benzene..........................5.37 %
5 x 5 mL
BCR-672 - BCR-107
In addition to national regulations, a Council Directive (93/12/EEC) specifies the maximum permissiblesulphur content of gas oils intended for combustion. These materials provide a means of checkinganalytical processes and of calibrating automatic equipment in the range 0.02 to 1.0% S in gas oil.
BCR-672 Gas oil - SulphurCertified value
S .................................0.0203 %
8 mL
BCR-671 Gas oil - SulphurCertified value
S .................................0.0452 %
8 mL
BCR-104R Gas oil - SulphurCertified value
S .................................0.1019 %
8 mL
BCR-105 Gas oil - SulphurCertified value
S ...................................0.363 %
25 g
BCR-106 Gas oil - SulphurCertified value
S ...................................0.502 %
25 g
BCR-107 Gas oil - SulphurCertified value
S ...................................1.040 %
25 g
BCR-395 Gas oilIntended for verifying manual and automatic cold filter plugging point (CFPP) apparatus in relation to the methodEN 116
Certified value
CFPP ............................... -5.8°C
jar
SS99859-0 Gas oil - Total sulphurASTM D4294-IP336: D2622, Total S in the range 0.12 to 0.97%m/m
50 mL
LGC6147 Waste oil - PCBsAssessed values
PCB 28 .................... 0.27 mg/kg PCB 118.....................8.5 mg/kg PCB 156 .................... 1.5 mg/kgPCB 52 ...................... 5.8 mg/kg PCB 128.....................2.1 mg/kg PCB 170 .................. 0.92 mg/kgPCB 101 .................. 10.9 mg/kg PCB 138.....................8.0 mg/kg PCB 180 .................... 2.3 mg/kgPCB 105 .................... 2.8 mg/kg PCB 153.....................7.2 mg/kg
5 x 5 mL
BCR-420 Waste mineral oil - PCBs (low level)Certified values
PCB 28 .................... 0.61 mg/kg PCB 118...................1.69 mg/kg PCB 180 ................ 0.195 mg/kgPCB 101 .................. 1.45 mg/kg PCB 153...................0.92 mg/kg
7.5 g
Oils and liquid fuels
www.lgcpromochem.com Edition 2003/2004 69
Code Product Unit
BCR-449 Waste mineral oil - PCBs (high level)Certified values
PCB 28 ................... 0.80 mg/kg PCB 118...................46.6 mg/kg PCB 170 .................... 6.6 mg/kgPCB 52 ..................... 31.4mg/kg PCB 128...................12.5 mg/kg PCB 180 .................. 10.4 mg/kgPCB 101 .................. 57.2 mg/kg PCB 153...................39.0 mg/kgPCB 105 .................. 17.4 mg/kg PCB 156.....................6.9 mg/kg
50 g
RTC-CRM920 Transformer oil - PCBsCertified value
Aroclor 1260 ............ 35.2 mg/kg
10 mL
NIST-1818a Lubricating base oil - ChlorineSet of 5 x 20 mL ampoules
Certified values
I Cl............................ 31.6 mg/kgII Cl........................... 60.0 mg/kgIII Cl.......................... 78.2 mg/kgIV C........................ 154.4 mg/kgV Cl ........................ 234.0 mg/kg
set (5)
NIST-1819a Lubricating base oil - SulphurNIST-1819a consists of five lubricating base oils at different sulphur concentrations.
Certified values
I S........................... 423.5 mg/kgII S.......................... 741.1 mg/kgIII S.......................... 4022 mg/kgIV S ......................... 4689 mg/kgV S .......................... 6135 mg/kg
set (5)
NIST-1836 Lube base oil - NitrogenSet of 4 x 5 mL vials
Certified values
I N .............................. 9.0 mg/kgII N ........................... 50.9 mg/kgIII N ........................ 113.3 mg/kgIV N........................ 166.2 mg/kg
set (4)
SS99863-0 Lube oil - Trace elementsI ASTM-IP method ICP, Ca in the range 0.029 to 0.486 % m/m
II ASTM-IP method ICP, Mg in the range 0.001 to 0.124 %m/m
III ASTM-IP method ICP, P in the range 0.026 to 0.131 %m/m
IV ASTM-IP method ICP, Zn in the range 0.030 to 0.149 %m/m
50 mL
NIST-1848 Lubricating oil additive packageCertified values
B ...................................0.137 % Mg ................................ 0.821 % Zn.....................0.873 ± 0.022 %Ca .................................0.359 % P................................... 0.788 %Cl ................................0.0927 % S................................. 2.3270 %
Indicative values for H, N, Si, total base number by ASTM D 2896, total base number by ASTM D 4739*
100 g
NIST-1634c Fuel oil - Trace elementsCertified values
As......................... 0.1426 mg/kg Ni ............................17.54 mg/kg V ............................ 28.19 mg/kgCo ........................ 0.1510 mg/kg Se.........................0.1020 mg/kg
Indicative values for Ba, Cl, Na, S
100 mL
SS99860-0 Fuel oil - Vanadium and nickelI ASTM-IP method IP288, V in the range 71.5 to 129.1 µg/g
II ASTM-IP method IP288, Ni in the range 26.6 to 44.2 µg/g
50 mL
SS99861-0 Fuel oil - Aluminium and siliconI ASTM-IP method IP377, Al in the range 7.2 to 31.9 mg/kg,
II ASTM-IP method IP377, Si in the range 13.3 to 70.4 mg/kg
100 mL
SS99862-0 Fuel oil - Total sulphurASTM D4294-IP336: D2622, Total S in the range 2.04 to 3.27 %m/m
50 mL
Oils and liquid fuels
70 Edition 2003/2004 www.lgcpromochem.com
Code Product Unit
NIST-1580 Shale oil - PAHsSet of 5 x 2 mL ampoules
Certified values
Benzo[a]pyrene........... 21 mg/kg o-Cresol.....................385 mg/kg Pyrene....................... 104 mg/kgBenzo[e]pyrene........... 18 mg/kg Phenol .......................407 mg/kg 2,6-Dimethylphenol ... 175 mg/kgFluoranthene............... 54 mg/kg Perylene .....................3.4 mg/kg Benzo[f]quinoline ........ 16 mg/kg
set (5)
NIST-1582 Petroleum crude oil - PAHsSet of 5 x 2 mL
Certified values
Benzo[a]anthracene... 3.0 mg/kg Fluoranthene ..............2.5 mg/kg Phenanthrene ........... 101 mg/kgBenzo[e]pyrene.......... 1.1 mg/kg Perylene ......................31 mg/kg Dibenzothiophene....... 33 mg/kg
set (5)
NIST-2721 Crude oil (light-sour) - Sulphur and mercuryCertified values
S .................................1.5832 % Hg.................................53 ng/kg
5 x 10 mL
NIST-2722 Crude oil (heavy-sweet) - Sulphur and mercuryCertified values
S ...............................0.21037 % Hg...............................144 ng/kg
5 x 10 mL
NIST-1616a Kerosine - SulphurCertified value
S ...............................0.01462 %
100 mL
NIST-1617a Kerosine - SulphurCertified value
S ...............................0.17307 %
100 mL
NIST-2298 Reformulated gasoline - SulphurCertified value
S ................................... 4.7 µg/g
5 x 20 mL
NIST-2299 Reformulated gasoline - SulphurCertified value
S ................................. 13.6 µg/g
5 x 20 mL
SS99857-0 Kerosine - NaphthalenesASTM D1840, Napthalenes in the range 1.69 to 4.23 %vol
50 mL
SS99858-0 Kerosine - Total sulphurASTM D429-IP336, Total S in the range 0.02 to 0.15 %m/m
50 mL
NIST-1623c Residual fuel oil - SulphurCertified value
S .................................0.3806 %
100 mL
NIST-1619b Residual fuel oil - SulphurCertified value
S .................................0.6960 %
100 mL
NIST-1621e Residual fuel oil - SulphurCertified value
S .................................0.9480 %
100 mL
NIST-1622e Residual fuel oil - SulphurCertified value
S .................................2.1468 %
100 mL
NIST-2717a Residual fuel oil - SulphurCertified value
S .................................2.9957 %
100 mL
NIST-1620c Residual fuel oil - SulphurCertified value
S ...................................4.561 %
100 mL
Oils and liquid fuels
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Code Product Unit
IRMM-441 and IRMM-442
High purity n-heptane and isooctane intended for use as a primary standard in the octane rating ofmotor and aviation fuels as specified in ASTM test methods (see Volume 05.04, Annual Book ofASTM Standards) and in evaluating ASTM methods for chemical analysis of fuels by gaschromatography (D2268).
IRMM-441 n-Heptanen-Heptane
Certified value: Purity by difference 99.985%
Impurities
Certified values
Total organics (other than n-Heptane)......... 0.012 % Water ...........................................................0.003 %Isooctane ..................................................... 0.007 % Pb............................................................... <0.5 µg/L
100 mL
IRMM-442 IsooctaneIsooctane
Certified value: Purity by difference 99.985%
Impurities
Certified values
Total organics (other than Isooctane) ........... 0.011% Water ...........................................................0.004%,n-Heptane .................................................... 0.002 % Pb.................................................................. <1 µg/L
100 mL
NIST-1815a n-HeptaneCertified purity.............99.987 %
100 mL
NIST-1816a Isooctane (2,2,4-Trimethylpentane)Certified purity.............99.987 %
100 mL
NIST-2713 Reference fuel - LeadCertified value
Pb ............................ 19.4 mg/kg
6 x 20 mL
NIST-2714 Reference fuel - LeadCertified value
Pb ............................ 28.1 mg/kg
6 x 20 mL
NIST-2724b Diesel fuel oil - SulphurCertified value
S ...............................0.04265 %
10 x 10 mL
NIST-2890 Water saturated octanolNIST-2890 is a solution of water saturated 1-octanol which is certified for its water content.
Certified values
Water ......................... 47.3 mg/g Water.....................39.24 mg/mL
5 x 2 mL
NIST-RM 8505 Crude oil - Vanadium (not certified)Reference value
V ............................... 390 mg/kg
275 mL
NIST-RM 8506a Transformer oil - Water (not certified)A unit of NIST-RM 8506a consists of five ampoules with each ampoule containing 9.5 mL of petroleum electricalinsulating oil.The first coulometric value is the NIST result corrected for the coulometrically detected material present in the oilthat reacts with iodine but is not water (interfering substances). Because the correction is new, two additionaluncorrected values determined by the coulometric method in ASTM Standard D 1533-99 are provided: the NISTresult, and a consensus result obtained from an interlaboratory study conducted among 14 laboratories fromindustry. The volumetric reference value, which has not been corrected for interfering substances, is significantlydifferent from the coulometric results. Applying the coulometrically determined correction for interferingsubstances does not resolve this difference. The basis of the difference between coulometric and volumetricresults in this material has not been fully resolved.
Reference values for water content
NIST coulometric mass concentration of water, ASTM method minus interferences ...... 12.1 mg/kg ± 1.9 mg/kg
(NIST coulometric mass concentration of water, ASTM method..................................... 18.3 mg/kg ± 1.9 mg/kg)
(Consensus coulometric mass concentration of water, ASTM method: .......................... 21.2 mg/kg ± 1.7 mg/kg)
NIST volumetric mass concentration of water, modified ASTM method: ......................... 34.5 mg/kg ± 2.2 mg/kg
set (5)
Oils and liquid fuels
72 Edition 2003/2004 www.lgcpromochem.com
Code Product Unit
NIST-RM 8507 Mineral oil - Water (not certified)Set of 5 x 10 mL
Reference value
Water .......................... 47 mg/kg
set (5)
NIST-RM 8509 Methanol - WaterSet of 5 x 5 mL
Reference value
Water .......................... 93 mg/kg
Indicative values for Ag, Al, Cr, Cu, Fe, Mg, Mn, Mo, Na, Ni, Pb, S, Si, Sn, Ti, V, Zn
set (5)
NIST-RM 8510 Methanol - WaterSet of 5 x 5 mL
Reference value
Water ........................ 325 mg/kg
set (5)
NIST-1083 Oil (base oil) - Wear metalsIndicative values for Ag, Al, Cr, Cu, Fe, Mg, Mn, Mo, Na, Ni, Pb, S, Si, Sn, Ti, V, Zn
150 mL
NIST-1084a Oil - Wear metalsSet of 5 x approx. 1.6 g of the oil blend
Certified values
Ag .......................... 101.4 mg/kg Mg ............................99.5 mg/kg Sn ............................ 97.2 mg/kgCr ............................. 98.3 mg/kg Mo ..........................100.3 mg/kg Ti............................ 100.4 mg/kgCu .......................... 100.0 mg/kg Ni ..............................99.7 mg/kg V .............................. 95.9 mg/kgFe............................. 98.9 mg/kg Pb...........................101.1 mg/kg
Indicative values for Al, S, Si
set (5)
NIST-1085b Oil - Wear metalsA unit of NIST-1085b consists of 10 ampoules: five 5 mL amber borosilicate ampoules, each containingapproximately 1.2 g of a blend of 21 constituent elements in a base oil at a nominal concentration of 300 mg/kg;and five ampoules, each containing approximately 1.2 g of a matching base oil intended for use as an analyticalblank and for matrix matching.
Certified values
Ag ......................... 304.6 mg/kg Mg ..........................297.3 mg/kg Pb .......................... 297.7 mg/kgBa .......................... 300.1 mg/kg Mn ..........................300.7 mg/kg Sn .......................... 299.4 mg/kgCd .......................... 302.9 mg/kg Mo ..........................300.6 mg/kg V ............................ 297.8 mg/kgCr ........................... 302.9 mg/kg Na...........................305.2 mg/kg Zn.................. 296.8 ± 6.8 mg/kgCu .......................... 295.6 mg/kg Ni ............................295.9 mg/kg
Indicative values for Al, As, Cl, Fe, P, Si, Ti
5 x 1.2 g
NIST-1829 Reference fuel - AlcoholsCertified values
Methanol ...................................................... 0.335 % Methanol and t-butanol .....................10.33 + 6.63 %Ethanol......................................................... 11.39 %
set (6)
NIST-1837 Reference fuel - Methanol and t-butanolCertified values
Methanol and t-butanol ..................... 10.33 + 6.63 %
set (5)
NIST-1838 Reference fuel - EthanolCertified value
Ethanol..........................11.39 %
5 x 20 mL
NIST-1839 Reference fuel - MethanolCertified value
Methanol .......................0.335 %
set (5)
NIST-2286 Ethanol in gasoline - Oxygen and oxygenateSet of 3 x 20 mL
Certified values
Oxygenate.......................5.73 % Oxygen ........................... 2.02 %
set (3)
NIST-2287 Ethanol in gasoline - Oxygen and oxygenateSet of 3 x 20 mL
Certified values
Oxygenate.....................10.07 % Oxygen ........................... 3.53 %
set (3)
Oils and liquid fuels
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Code Product Unit
NIST-2288 t-Amyl methyl ether in gasoline - Oxygen and oxygenateSet of 3 x 20 mL
Certified values
Oxygenate.....................12.78 % Oxygen ........................... 2.02 %
set (3)
NIST-2289 t-Amyl methyl ether in gasoline - Oxygen and oxygenateSet of 3 x 20 mL
Certified values
Oxygenate.....................17.30 % Oxygen ........................... 2.73 %
set (3)
NIST-2290 Ethyl t-butyl ether in gasoline - Oxygen and oxygenateSet of 3 x 20 mL
Certified values
Oxygenate.....................12.78 % Oygen............................. 2.01 %
set (3)
NIST-2291 Ethyl-t-butyl ether in gasoline - Oxygen and oxygenateSet of 3 x 20 mL
Certified values
Oxygenate.....................17.18 % Oxygen ........................... 2.70 %
set (3)
NIST-2292 Methyl t-butyl ether in gasoline - Oxygen and oxygenateA unit of NIST-2292 consists of two 20 mL ampoules ot the methyl-t-butyl ether in reference gasoline solutioneach containing 18 mL, and one 20 ml ampoule containing 18 mL of the reference gasoline, intended for use as ameasurement blank.
Certified values
Oxygenate.....................10.96 % Oxygen ........................... 2.00 %
set (3)
NIST-2293 Methyl t-butyl ether in gasoline - Oxygen and oxygenateA unit of NIST-2292 consists of two 20 mL ampoules ot the methyl-t-butyl ether in reference gasoline solutioneach containing 18 mL, and one 20 ml ampoule containing 18 mL of the reference gasoline, intended for use as ameasurement blank.
Certified values
Oxygenate.....................14.86 % Oxygen ........................... 2.71 %
set (3)
NIST-2294 Reformulated gasoline - Sulphur, benzene, MTBE and tolueneCertified values
S (total) .................... 40.9 mg/kg MTBE ........................... 10.97 %Benzene..........................1.03 % Toluene .......................... 8.29 %
Indicative values for a wide range of additional constituents
2 x 20 mL
NIST-2295 Reformulated gasoline - Sulphur, benzene, MTBE and tolueneCertified values
S (total) ..................... 308 mg/kg MTBE ........................... 14.54 %Benzene......................... .0.99 % Toluene .......................... 7.89 %
Indicative values for a wide range of additional constituents
2 x 20 mL
NIST-2296 Reformulated gasoline - Sulphur, benzene, MTBE and tolueneCertified values
S (total) .................... 40.0 mg/kg MTBE ........................... 13.02 %Benzene..........................1.01 % Toluene .......................... 8.02 %
Indicative values for a wide range of additional constituents
2 x 20 mL
NIST-2297 Reformulated gasoline - Sulphur, benzene, MTBE and tolueneCertified values
S (total) .................. 303.7 mg/kg MTBE ............................. 9.91 %Benzene..........................1.04 % Toluene .......................... 8.27 %
Indicative values for a wide range of additional constituents
2 x 20 mL
NRMGBW11201 Petroleum - Trace metalsCertified values
Fe.................................. 7.7 µg/g Mn ...............................2.69 µg/g Ni ................................ 15.4 µg/gMg............................... 1.39 µg/g Na................................11.2 µg/g
Indicative values for As, K
20 mL
NRMGBW11202 Petroleum -Trace elementsCertified values
Ca ............................... 2.57 µg/g Fe ................................19.5 µg/g V ................................. 2.28 µg/gCo ............................... 4.87 µg/g Ni ....................................99 µg/g
Indicative value for Pb
20 mL
Oils and liquid fuels
74 Edition 2003/2004 www.lgcpromochem.com
Code Product Unit
SS99864-0 Gasoline - LeadIP270 Pb in the range 0.0015 to 0.170 g/L, Pb X-ray in the range 0.0013 to 0.175 g/L
5 x 5 mL
SS99865-0 Gasoline - BenzeneASTM D3606, Benzene in the range 1.82 to 2.94 %vol
5 x 5 mL
Multi-test verification materials (MTVMs)
The Multi-Test Verification Materials (MTVMs) are unique because, unlike most other certifiedreference materials, they enable a laboratory to use a single sample to validate different tests andinstrumentation. Each unit is supplied with certified data for multiple types of internationally acceptedtest methods.
SS99850-0 SETA MTVM KerosineDistillation IBP (method D86-IP123) 140-170 °C, 100 mLDistillation 10 % (method D86-IP123) 159-188 °C, 100 mLDistillation 50 % (method D86-IP123) 192-218 °C, 100 mLDistillation 90 % (method D86-IP123) 234-247 °C, 100 mLDistillation FBP (method D86-IP123) 248-263 °C, 100 mLDistillation residue (method D86-IP123) 1.10-1.24 %vol, 100 mLDistillation loss (method D86-IP123) 0.30-0.49 %vol, 100 mLFlashpoint (method IP170) 36.7-57.5 °C, 85 mLFreezing point (method D2386-IP16) –51.2 to -43.4°C, 25 mLAniline point (method D611) 55.0-59.0 °C, 10 mLAromatics FIA (method D1319-IP156) 18.1-22.7 %vol, 0.75 mLSmoke rate (method D1322) 20.7-24.2 mm, 20 mL
500 mL
SS99851-0 SETA MTVM Gas oilDensity at 15 °C (method D1298-IP160) 0.8252-0.8481 kg/L, 200 mLDistillation IBP (method D86-IP123) 160-223 °C, 100 mLDistillation 10 % (method D86-IP123) 187-254 °C, 100 mLDistillation 50 % (method D86-IP123) 240-290 °C, 100mLDistillation 90 % (method D86-IP123) 304-341 °C, 100 mLDistillation FBP (method D86-IP123) 347-367 °C, 100 mLDistillation residue (method D86-IP123) 1.27-1.42 %vol, 100 mLDistillation loss (method D86-IP123) 0.20-0.36 %vol, 100 mLFlashpoint (method D93-IP34) 51.7-103°C, 75 mLCloud point (method D2500-IP219) –15.9 to –3.8 °C, 38 mLCFPP (method IP309) –28.0 to –5.4 °C, 45 mLPour point (method D97-IP15) –26.9 to –7.6 °C, 38 mLKin. Visc. (40 °C) (method D445-IP71) 2.15-3.70 mm2/s, up to 40 mL
500 mL
SS99852-0 SETA MTVM Fuel oilDensity at 15 °C (method D1298-IP160) 0.9313-0.9909 kg/L, 200 mLPour point (method D97-IP15) –10.7 to 17.2 °C, 38 mLKin. Visc. (50 °C) (method D445-IP71) 38.9-993.3 mm2/s, up to 500 mLKin. Visc. (80 °C) (method D445-IP71) 13.7-130 mm2/s, up to 500 mLKin. Visc. (100 °C) (method D445-IP71) 8.4-53.8 mm2/s, up to 500 mLConradson carbon (method D189-IP13) 9.3-17.3 %m/m, 5 mL
500 mL
SS99853-0 SETA MTVM lubricating oilKin. Visc. (40 °C) (method D445-IP71) 55.7-111.1 mm2/s, up to 500mLKin. Visc. (100 °C) (method D445-IP71) 7.7-14.7 mm2/s, up to 500mLViscosity index (method D2270-IP226) 102.0-149.5, up to 500 mLPour point (method D97-IP15) –34.9 to –20.5 °C, 38 mLFlashpoint (method D93-IP34) 198-213 °C, 75 mLCold cranking sim. (method IP383) 1676-3462 mPa.s, 5 mL
500 mL
SS99854-0 SETA MTVM motor gasolineMotor octane no. (method D2700) 85.7-87.8Research octane no. (method D2699) 97-99.9Density at 15 °C (method D1298-IP160) 0.7214-0.7823 kg/L, 200 mLDistillation IBP (method D86-IP123) 26.0-32.0 °C, 100 mLDistillation 70 °C (method D86-IP123) 15.0-48.8 %vol, 100 mLDistillation 100 °C (method D86-IP123) 23.4-71.2 %vol, 100 mLDistillation 140 °C (method D86-IP123) 51.1-90.4 %vol, 100 mLDistillation FBP (method D86-IP123) 170-218 °C, 100mLAromatics FIA (method D1319-IP156) 27.7-45.2 %vol, 0.75 mLOlefins FIA (method D1319-IP156) 7.6-23.6 %vol, 0.75 mLSaturates FIA (method D1319-IP156) 40.7-55.0 %vol, 0.75 mL
500 mL
SS99856-0 SETA MTVM bitumenSoftening point (method IP58) 36.8-44 °C, 7.5 mLNeedle penetration (method IP49) 184-200 °C, 130 mL
500 mL
Conostan® Oil Analysis Standards
www.lgcpromochem.com Edition 2003/2004 75
Conostan® Oil Analysis StandardsReference materials for lubricant/oil analysis include: Element (metallo-organic) standards andassociated blank oils and solvent (for ICP application), Particle Counting (contamination) standardsfor Automatic Particle Counters, and FTIR Operational Test Standard. A proficiency test program foranalysis of important properties of lubricants (new & used) such as: wear & additive metals, particles,and viscosity is offered (see “About proficiency testing (PT)” section – OIL ANALYSIS).
Element (Metallo-organic) Standards (see JOAP Military Spectrometric Standards, page 83)
CONOSTAN® Division is the world's leading manufacturer and marketer of Elements (metallo-organic)in Oil standards and related spectroscopy products. CONOSTAN's industry leading position is derivedfrom superior product chemistry, manufacturing technology, and blending techniques. CONOSTANproducts are used extensively in the calibration and operation of analytical instruments for theanalysis of elements in oil and other organic fluids. CONOSTAN is the only source of multi-elementmetallo-organic standards in the history of the National Institute of Standards & Technology (NIST),for example, NIST-1085b is CONOSTAN S-21:300, Code CON-S214300 and CON-S218300. Thevariety of products afford convenience as reference and routine analytical materials for ICP, DCP,Rotating Disk Electrode (RDE), XRF, AA, and other analytical spectrometer techniques. CONOSTAN®
products are optimized for:
- Compatability: 33 elements can be combined over an extensive concentration range
- Solubility: CONOSTAN® element standards are soluble in CONOSTAN® PremiSolv™ ICP solvent,CONOSTAN® base oils, ketones, such as 4-methyl-2-pentanone (MIBK), as well as in paraffinic andaromatic hydrocarbons, such as mineral oil, xylene, and kerosene.
- Volatility: CONOSTAN® element standards are made in ultra-pure, highly processed hydrocarbon oilonly; no solubilizers are used. These element standards are extremely stable to volatile loss.
- Viscosity: Viscosity range at room temperature is ideal for instrumental applications.
- Instrumental Response: Excellent analytical response over a wide range of analytical applications.
- Shelf life: All CONOSTAN element standards and spectroscopy products have a one year minimumshelf life from the date of shipment.
Single element standards in oil
Single-element CONOSTAN® standards are especially useful for atomic absoption and X-rayfluorescence determinations. The matrix oil for these standards is high purity hydrocarbon oil with a17 cSt viscosity at 40°C and flash point of 175°C (20 Base Oil). They are available at the followingmetal concentrations.The 1000 and 5000 ppm standards can be used as a source of single-element calibration standard foryour specific applications using all types of spectroscopic methods of analysis.Cobalt 1000 & 5000 ppm, yttrium 1000 & 5000 ppm, and scandium 2000 ppm are often used as aninternal standards for inductive coupled plasma (ICP) analysis.Stock concentrations are listed in the table below. Concentrations not listed in the table below areavailable as custom single element standards on request.
Code Product Unit
CON-Al1000 Aluminium in 20 base oil, 1000 µg/g Al:1000 ppm 50 g
CON-Al5000 Aluminium in 20 base oil, 5000 µg/g Al:5000 ppm 50 g
CON-Sb1000 Antimony in 20 base oil, 1000 µg/g Sb:1000 ppm 50 g
CON-Sb5000 Antimony in 20 base oil, 5000 µg/g Sb:5000 ppm 50 g
CON-As100 Arsenic in 20 base oil, 100 µg/g As:100 ppm 100 g
CON-Ba1000 Barium in 20 base oil, 1000 µg/g Ba:1000 ppm 50 g
CON-Ba5000 Barium in 20 base oil, 5000 µg/g Ba:5000 ppm 50 g
CON-Be1000 Beryllium in 20 base oil, 1000 µg/g Be:1000 ppm 50 g
CON-Be5000 Beryllium in 20 base oil, 5000 µg/g Be:5000 ppm 50 g
CON-Bi1000 Bismuth in 20 base oil, 1000 µg/g Bi:1000 ppm 50 g
CON-Bi5000 Bismuth in 20 base oil, 5000 µg/g Bi:5000 ppm 50 g
Conostan® Oil Analysis Standards
76 Edition 2003/2004 www.lgcpromochem.com
Code Product Unit
CON-B1000 Boron in 20 base oil, 1000 µg/g B:1000 ppm 50 g
CON-B5000 Boron in 20 base oil, 5000 µg/g B:5000 ppm 50 g
CON-Cd1000 Cadmium in 20 base oil, 1000 µg/g Cd:1000 ppm 50 g
CON-Cd5000 Cadmium in 20 base oil, 5000 µg/g Cd:5000 ppm 50 g
CON-Ca1000 Calcium in 20 base oil, 1000 µg/g Ca:1000 ppm 50 g
CON-Ca5000 Calcium in 20 base oil, 5000 µg/g Ca:5000 ppm 50 g
CON-Cr1000 Chromium in 20 base oil, 1000 µg/g Cr:1000 ppm 50 g
CON-Cr5000 Chromium in 20 base oil, 5000 µg/g Cr:5000 ppm 50 g
CON-Co1000 Cobalt in 20 base oil, 1000 µg/g Co:1000 ppm 50 g
CON-Co5000 Cobalt in 20 base oil, 5000 µg/g Co:5000 ppm 50 g
CON-Cu1000 Copper in 20 base oil, 1000 µg/g Cu:1000 ppm 50 g
CON-Cu5000 Copper in 20 base oil, 5000 µg/g Cu:5000 ppm 50 g
CON-In1000 Indium in 20 base oil, 1000 µg/g In:1000 ppm 50 g
CON-In5000 Indium in 20 base oil, 5000 µg/g In:5000 ppm 50 g
CON-Fe1000 Iron in 20 base oil, 1000 µg/g Fe:1000 ppm 50 g
CON-Fe5000 Iron in 20 base oil, 5000 µg/g Fe:5000 ppm 50 g
CON-La1000 Lanthanum in 20 base oil, 1000 µg/g La:1000 ppm 50 g
CON-La5000 Lanthanum in 20 base oil, 5000 µg/g La:5000 ppm 50 g
CON-Pb1000 Lead in 20 base oil, 1000 µg/g Pb:1000 ppm 50 g
CON-Pb5000 Lead in 20 base oil, 5000 µg/g Pb: 5000 ppm 50 g
CON-Li1000 Lithium in 20 base oil, 1000 µg/g Li:1000 ppm 50 g
CON-Li5000 Lithium in 20 base oil, 5000 µg/g Li:5000 ppm 50 g
CON-Mg1000 Magnesium in 20 base oil, 1000 µg/g Mg:1000 ppm 50 g
CON-Mg5000 Magnesium in 20 base oil, 5000 µg/g Mg:5000 ppm 50 g
CON-Mn1000 Manganese in 20 base oil, 1000 µg/g Mn:1000 ppm 50 g
CON-Mn5000 Manganese in 20 base oil, 5000 µg/g Mn:5000 ppm 50 g
CON-Hg100 Mercury in 20 base oil, 100 µg/g Hg:100 ppm 100 g
CON-Mo1000 Molybdenum in 20 base oil, 1000 µg/g Mo:1000 ppm 50 g
CON-Mo5000 Molybdenum in 20 base oil, 5000 µg/g Mo:5000 ppm 50 g
CON-Ni1000 Nickel in 20 base oil, 1000 µg/g Ni:1000 ppm 50 g
CON-Ni5000 Nickel in 20 base oil, 5000 µg/g Ni:5000 ppm 50 g
CON-P1000 Phosphorus in 20 base oil, 1000 µg/g P:1000 ppm 50 g
CON-P5000 Phosphorus in 20 base oil, 5000 µg/g P:5000 ppm 50 g
CON-K1000 Potassium in 20 base oil, 1000 µg/g K:1000 ppm 50 g
CON-K5000 Potassium in 20 base oil, 5000 µg/g K:5000 ppm 50 g
CON-Sc2000 Scandium in 20 base oil, 2000 µg/g Sc:2000 ppm 50 g
CON-Se100 Selenium in 20 base oil, 100 µg/g Se:100 ppm 100 g
CON-Si1000 Silicon in 20 base oil, 1000 µg/g Si:1000 ppm 50 g
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Code Product Unit
CON-Si5000 Silicon in 20 base oil, 5000 µg/g Si:5000 ppm 50 g
CON-Ag1000 Silver in 20 base oil, 1000 µg/g Al:1000 ppm 50 g
CON-Ag5000 Silver in 20 base oil, 5000 µg/g Ag:5000 ppm 50 g
CON-Na1000 Sodium in 20 base oil, 1000 µg/g Na:1000 ppm 50 g
CON-Na5000 Sodium in 20 base oil, 5000 µg/g Na:5000 ppm 50 g
CON-Sr1000 Strontium in 20 base oil, 1000 µg/g Sr:1000 ppm 50 g
CON-Sr5000 Strontium in 20 base oil, 5000 µg/g Sr:5000 ppm 50 g
CON-Sn1000 Tin in 20 base oil, 1000 µg/g Sn:1000 ppm 50 g
CON-Sn5000 Tin in 20 base oil, 5000 µg/g Sn:5000 ppm 50 g
CON-Ti1000 Titanium in 20 base oil, 1000 µg/g Ti:1000 ppm 50 g
CON-Ti5000 Titanium in 20 base oil, 5000 µg/g Ti:5000 ppm 50 g
CON-W1000 Tungsten in 20 base oil, 1000 µg/g W:1000 ppm 50 g
CON-W5000 Tungsten in 20 base oil, 5000 µg/g W:5000 ppm 50 g
CON-V1000 Vanadium in 20 base oil, 1000 µg/g V:1000 ppm 50 g
CON-V5000 Vanadium in 20 base oil, 5000 µg/g V:5000 ppm 50 g
CON-Y1000 Yttrium in 20 base oil, 1000 µg/g Y:1000 ppm 50 g
CON-Y5000 Yttrium in 20 base oil, 5000 µg/g Y:5000 ppm 50 g
CON-Zn1000 Zinc in 20 base oil, 1000 µg/g Zn:1000 ppm 50 g
CON-Zn5000 Zinc in 20 base oil, 5000 µg/g Zn:5000 ppm 50 g
Multi-element standards in oil
Multi-element Conostan® standards are especially useful for ICP, RDE, and DCPanalysis of metals in oil. They are available in high purity hydrocarbon oil solutions andare blended to approximately 70 cSt viscosity at 40°C and flash point of 215°C (75Base Oil). They contain equal amounts of each element.Concentrations not listed are available as custom multi-element standards onrequest. You may create your own S-21 and S-12 standards by adding additionalelements to the stocked product standards, listed as follows.
CON-S21410 Multi-element standard in 75 base oil: S-21:10 ppmAg .................................. 10 µg/g Cu...................................10 µg/g P .................................... 10 µg/gAl.................................... 10 µg/g Fe ...................................10 µg/g Pb .................................. 10 µg/gB .................................... 10 µg/g Mg ..................................10 µg/g Si.................................... 10 µg/gBa .................................. 10 µg/g Mn ..................................10 µg/g Sn .................................. 10 µg/gCa .................................. 10 µg/g Mo ..................................10 µg/g Ti.................................... 10 µg/gCd .................................. 10 µg/g Na...................................10 µg/g V .................................... 10 µg/gCr ................................... 10 µg/g Ni ....................................10 µg/g Zn................................... 10 µg/g
100 g
CON-S21810 Multi-element standard in 75 base oil: S-21:10 ppm 200 g
CON-S21430 Multi-element standard in 75 base oil: S-21:30 ppmAg .................................. 30 µg/g Cu...................................30 µg/g P .................................... 30 µg/gAl.................................... 30 µg/g Fe ...................................30 µg/g Pb .................................. 30 µg/gB .................................... 30 µg/g Mg ..................................30 µg/g Si.................................... 30 µg/gBa .................................. 30 µg/g Mn ..................................30 µg/g Sn .................................. 30 µg/gCa .................................. 30 µg/g Mo ..................................30 µg/g Ti.................................... 30 µg/gCd .................................. 30 µg/g Na...................................30 µg/g V .................................... 30 µg/gCr ................................... 30 µg/g Ni ....................................30 µg/g Zn................................... 30 µg/g
100 g
CON-S21830 Multi-element standard in 75 base oil: S-21:30 ppm 200 g
Conostan® Oil Analysis Standards
78 Edition 2003/2004 www.lgcpromochem.com
Code Product Unit
CON-S21450 Multi-element standard in 75 base oil: S-21:50 ppmAg .................................. 50 µg/g Cu...................................50 µg/g P .................................... 50 µg/gAl.................................... 50 µg/g Fe ...................................50 µg/g Pb .................................. 50 µg/gB .................................... 50 µg/g Mg ..................................50 µg/g Si.................................... 50 µg/gBa .................................. 50 µg/g Mn ..................................50 µg/g Sn .................................. 50 µg/gCa .................................. 50 µg/g Mo ..................................50 µg/g Ti.................................... 50 µg/gCd .................................. 50 µg/g Na...................................50 µg/g V .................................... 50 µg/gCr ................................... 50 µg/g Ni ....................................50 µg/g Zn................................... 50 µg/g
100 g
CON-S21850 Multi-element standard in 75 base oil: S-21:50 ppm 200 g
CON-S214100 Multi-element standard in 75 base oil: S-21:100 ppmAg ................................ 100 µg/g Cu.................................100 µg/g P .................................. 100 µg/gAl.................................. 100 µg/g Fe .................................100 µg/g Pb ................................ 100 µg/gB .................................. 100 µg/g Mg ................................100 µg/g Si.................................. 100 µg/gBa ................................ 100 µg/g Mn ................................100 µg/g Sn ................................ 100 µg/gCa ................................ 100 µg/g Mo ................................100 µg/g Ti.................................. 100 µg/gCd ................................ 100 µg/g Na.................................100 µg/g V .................................. 100 µg/gCr ................................. 100 µg/g Ni ..................................100 µg/g Zn................................. 100 µg/g
100 g
CON-S218100 Multi-element standard in 75 base oil: S-21:100 ppm 200 g
CON-S214300 Multi-element standard in 75 base oil: S-21:300 ppmAg ................................ 300 µg/g Cu.................................300 µg/g P .................................. 300 µg/gAl.................................. 300 µg/g Fe .................................300 µg/g Pb ................................ 300 µg/gB .................................. 300 µg/g Mg ................................300 µg/g Si.................................. 300 µg/gBa ................................ 300 µg/g Mn ................................300 µg/g Sn ................................ 300 µg/gCa ................................ 300 µg/g Mo ................................300 µg/g Ti.................................. 300 µg/gCd ................................ 300 µg/g Na.................................300 µg/g V .................................. 300 µg/gCr ................................. 300 µg/g Ni ..................................300 µg/g Zn................................. 300 µg/g
100 g
CON-S218300 Multi-element standard in 75 base oil: S-21:300 ppm 200 g
CON-S214500 Multi-element standard in 75 base oil: S-21:500 ppmAg ................................ 500 µg/g Cu.................................500 µg/g P .................................. 500 µg/gAl.................................. 500 µg/g Fe .................................500 µg/g Pb ................................ 500 µg/gB .................................. 500 µg/g Mg ................................500 µg/g Si.................................. 500 µg/gBa ................................ 500 µg/g Mn ................................500 µg/g Sn ................................ 500 µg/gCa ................................ 500 µg/g Mo ................................500 µg/g Ti.................................. 500 µg/gCd ................................ 500 µg/g Na.................................500 µg/g V .................................. 500 µg/gCr ................................. 500 µg/g Ni ..................................500 µg/g Zn................................. 500 µg/g
100 g
CON-S218500 Multi-element standard in 75 base oil: S-21:500 ppm 200 g
CON-S214900 Multi-element standard in 75 base oil: S-21:900 ppmAg ................................ 900 µg/g Cu.................................900 µg/g P .................................. 900 µg/gAl.................................. 900 µg/g Fe .................................900 µg/g Pb ................................ 900 µg/gB .................................. 900 µg/g Mg ................................900 µg/g Si.................................. 900 µg/gBa ................................ 900 µg/g Mn ................................900 µg/g Sn ................................ 900 µg/gCa ................................ 900 µg/g Mo ................................900 µg/g Ti.................................. 900 µg/gCd ................................ 900 µg/g Na.................................900 µg/g V .................................. 900 µg/gCr ................................. 900 µg/g Ni ..................................900 µg/g Zn................................. 900 µg/g
100 g
CON-S218900 Multi-element standard in 75 base oil: S-21:900 ppm 200 g
CON-S12410 Multi-element standard in 75 base oil: S-12:10 ppmAg .................................. 10 µg/g Fe ...................................10 µg/g Pb .................................. 10 µg/gAl.................................... 10 µg/g Mg ..................................10 µg/g Si.................................... 10 µg/gCr ................................... 10 µg/g Na...................................10 µg/g Sn .................................. 10 µg/gCu .................................. 10 µg/g Ni ....................................10 µg/g Ti.................................... 10 µg/g
100 g
CON-S12810 Multi-element standard in 75 base oil: S-12:10 ppm 200 g
CON-S12430 Multi-element standard in 75 base oil: S-12:30 ppmAg .................................. 30 µg/g Fe ...................................30 µg/g Pb .................................. 30 µg/gAl.................................... 30 µg/g Mg ..................................30 µg/g Si.................................... 30 µg/gCr ................................... 30 µg/g Na...................................30 µg/g Sn .................................. 30 µg/gCu .................................. 30 µg/g Ni ....................................30 µg/g Ti.................................... 30 µg/g
100 g
CON-S12830 Multi-element standard in 75 base oil: S-12:30 ppm 200 g
CON-S12450 Multi-element standard in 75 base oil: S-12:50 ppmAg .................................. 50 µg/g Fe ...................................50 µg/g Pb .................................. 50 µg/gAl.................................... 50 µg/g Mg ..................................50 µg/g Si.................................... 50 µg/gCr ................................... 50 µg/g Na...................................50 µg/g Sn .................................. 50 µg/gCu .................................. 50 µg/g Ni ....................................50 µg/g Ti.................................... 50 µg/g
100 g
CON-S12850 Multi-element standard in 75 base oil: S-12:50 ppm 200 g
Conostan® Oil Analysis Standards
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Code Product Unit
CON-S124100 Multi-element standard in 75 base oil: S-12:100 ppmAg ................................ 100 µg/g Fe .................................100 µg/g Pb ................................ 100 µg/gAl.................................. 100 µg/g Mg ................................100 µg/g Si.................................. 100 µg/gCr ................................. 100 µg/g Na.................................100 µg/g Sn ................................ 100 µg/gCu ................................ 100 µg/g Ni ..................................100 µg/g Ti.................................. 100 µg/g
100 g
CON-S128100 Multi-element standard in 75 base oil: S-12:100 ppm 200 g
CON-S124300 Multi-element standard in 75 base oil: S-12:300 ppmAg ................................ 300 µg/g Fe .................................300 µg/g Pb ................................ 300 µg/gAl.................................. 300 µg/g Mg ................................300 µg/g Si.................................. 300 µg/gCr ................................. 300 µg/g Na.................................300 µg/g Sn ................................ 300 µg/gCu ................................ 300 µg/g Ni ..................................300 µg/g Ti.................................. 300 µg/g
100 g
CON-S128300 Multi-element standard in 75 base oil: S-12:300 ppm 200 g
CON-S124500 Multi-element standard in 75 base oil: S-12:500 ppmAg ................................ 500 µg/g Fe .................................500 µg/g Pb ................................ 500 µg/gAl.................................. 500 µg/g Mg ................................500 µg/g Si.................................. 500 µg/gCr ................................. 500 µg/g Na.................................500 µg/g Sn ................................ 500 µg/gCu ................................ 500 µg/g Ni ..................................500 µg/g Ti.................................. 500 µg/g
100 g
CON-S128500 Multi-element standard in 75 base oil: S-12:500 ppm 200 g
CON-S124900 Multi-element standard in 75 base oil: S-12:900 ppmAg ................................ 900 µg/g Fe .................................900 µg/g Pb ................................ 900 µg/gAl.................................. 900 µg/g Mg ................................900 µg/g Si.................................. 900 µg/gCr ................................. 900 µg/g Na.................................900 µg/g Sn ................................ 900 µg/gCu ................................ 900 µg/g Ni ..................................900 µg/g Ti.................................. 900 µg/g
100 g
CON-S128900 Multi-element standard in 75 base oil: S-12:900 ppm 200 g
AM Special
This multi-element standard is used in determination of additive elements in lubricantoils by ICP, RDE, and DCP analysis of metals in oil. [Concentrations not listed areavailable as custom multi-element standards on request. You may create your ownAM Special standards by adding additional elements to the stocked product standards,listed as follows]
CON-AM4900 Multi-element standard AM-special in 75 base oil: AM Special 900 ppmBa ................................ 900 µg/g Mg ................................900 µg/g Zn................................. 900 µg/gCa ................................ 900 µg/g P...................................900 µg/g
100 g
CON-AM8900 Multi-element standard AM-special in 75 base oil: AM Special 900 ppm 200 g
CON-AM41000 Multi-element standard AM-special in 75 base oil: AM Special 1000 ppmBa .............................. 1000 µg/g Mg ..............................1000 µg/g Zn............................... 1000 µg/gCa .............................. 1000 µg/g P.................................1000 µg/g
100 g
CON-AM81000 Multi-element standard AM-special in 75 base oil: AM Special 1000 ppm 200 g
Custom Multi-Element Standards in Mineral Oil
Customized standards can be prepared if your spectrometric analysis of metalsrequires a specific combination of elements and concentrations. Custom standardsallow testing for unusual combinations and concentrations of elements with minimalspectral interference and repeatable results. Both single element and multi-elementcustom standards are available. Any element available (All except S, Cl, As, Hg, andSe) can be combined to prepare multi-element custom standards. Create your ownS-21, S-12, and AM Special standards by adding additional elements to the stockedproduct standards. Popular additions to S-21 are potassium, lithium, and antimony.Standards are designated, for example, by S-21+K+Sb:100 ppm, AM Special+Fe:900 ppm, S-12+Mo:100 ppm, etc. Custom standards are available in 100 g, 200 g, and400 g. Custom standards are prepared and shipped within two business days of orderreceipt by CONOSTAN®.
Conostan® Oil Analysis Standards
80 Edition 2003/2004 www.lgcpromochem.com
Code Product Unit
Sulphur in mineral oil
Sulphur and chlorine calibration standards are specifically designed for analysis of sulphur andchlorine in a wide variety of petroleum products by XRF, ICP and other analytical techniques. Allstandards are prepared on a weight/weight basis in high purity hydrocarbon oil with a 70 cSt viscosityat 40°C (75 Base Oil). Stock concentrations are listed in the table below. Concentrations not listed inthe table below are available as custom standards on request.
CON-Sblank Sulphur in mineral oil, blank S:blank 100 g
CON-S50 Sulphur in mineral oil, 50 µg/g S:50 ppm; 0.005 wt% 100 g
CON-S100 Sulphur in mineral oil, 100 µg/g S:100 ppm; 0.01 wt% 100 g
CON-S250 Sulphur in mineral oil, 250 µg/g S:250 ppm; 0.025 wt% 100 g
CON-S500 Sulphur in mineral oil, 500 µg/g S:500 ppm; 0.05 wt% 100 g
CON-S750 Sulphur in mineral oil, 750 µg/g S:750 ppm; 0.075 wt% 100 g
CON-S1000 Sulphur in mineral oil, 1000 µg/g S:1000 ppm; 0.1 wt% 100 g
CON-S2500 Sulphur in mineral oil, 2500 µg/g S:2500 ppm; 0.25 wt% 100 g
CON-S5000 Sulphur in mineral oil, 5000 µg/g S:5000 ppm; 0.5 wt% 100 g
CON-S7500 Sulphur in mineral oil, 7500 µg/g S:7500 ppm; 0.75 wt% 100 g
CON-S10000 Sulphur in mineral oil, 10000 µg/g S:10000 ppm; 1.0 wt% 100 g
CON-S15000 Sulphur in mineral oil, 15000 µg/g S:15000 ppm; 1.5 wt% 100 g
CON-S20000 Sulphur in mineral oil, 20000 µg/g S:20000 ppm; 2.0 wt% 100 g
CON-S25000 Sulphur in mineral oil, 25000 µg/g S:25000 ppm; 2.5 wt% 100 g
CON-S30000 Sulphur in mineral oil, 30000 µg/g S:30000 ppm; 3.0 wt% 100 g
CON-S40000 Sulphur in mineral oil, 40000 µg/g S:40000 ppm; 4.0 wt% 100 g
CON-S50000 Sulphur in mineral oil, 50000 µg/g S:50000 ppm; 5.0 wt% 100 g
Chlorine in oil
CON-Cl-blank Chlorine in oil, blank Cl:blank 100 g
CON-Cl10 Chlorine in oil, 10 µg/g Cl:10 ppm; 0.001 wt% 100 g
CON-Cl100 Chlorine in oil, 100 µg/g Cl:100ppm; 0.01 wt% 100 g
CON-Cl500 Chlorine in oil, 500 µg/g Cl:500 ppm; 0.05 wt% 100 g
CON-Cl1000 Chlorine in oil, 1000 µg/g Cl:1000 ppm; 0.1 wt% 100 g
CON-Cl5000 Chlorine in oil, 5000 µg/g Cl:5000 ppm; 0.5 wt% 100 g
CON-Cl10000 Chlorine in oil, 10000 µg/g Cl:10000 ppm; 1.0 wt% 100 g
CON-Cl50000 Chlorine in oil, 50000 µg/g Cl:50000 ppm; 5.0 wt% 100 g
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Code Product Unit
Element blank oils
Blank oils may be used as a “zero“ point standard or for diluting calibration standards forspectrometric analysis of metals in oil.
CON-EBO204 20 Blank oilViscosity
40 °C (104 °F).............14-18 cSt 100 °C (212 °F) ............. 3-4 cSt Any trace metal ......... <0.10 ppm
100 g
CON-EBO2016 20 Blank oil 400 g
CON-EBO754 75 Blank oilViscosity
40 °C (104 °F).............65-72 cSt 100 °C (212 °F) ....... 8.1-8.7 cSt Any trace metal ......... <0.10 ppm
100 g
CON-EBO7516 75 Blank oil 400 g
PremiSolvTM ICP solvent
PremiSolv™ ICP solvent is a superior product vs. low odor kerosene or xylene for useas a diluent and “zero” point standard in ICP/DCP analysis of metals in oil and otherorganic fluids. PremiSolv™ ICP solvent features:
- Extremely low odour: No sulphur/aromatic odor for increased worker comfort andless occupational exposure
- Extremely low toxicity compared to kerosene or xylene.- Non-hazardous for shipping/disposal.- Supplied with certificate of analysis listing the concentration of 33 different metals
and sulphur.
CON-PSOLV4 PremiSolvTM ICP solvent 3.78 L
CON-PSOLV19 PremiSolvTM ICP solvent 18.9 L
PartiStanTM particle standards- Compliant with ISO 11171:1999
Automatic particle counters (APC), using a laser source, are used for measurement of contaminationin lubrication products, especially hydraulic fluids. These products are necessary for instrumentcalibration and verification of performance, and may, also, be used for non-laser based particlecounting instruments.
PartiStan™ Particle Standard Features:
- Traceable to NIST SRM 2806.- ISO 11171 compliant, Per Annex F; uses ISO medium test dust.- Certificate of analysis for 4-30 um(c) (micrometers, certified).- Maintain conformance to ISO programs (ISO 4402 is obsolete).- Independent of APC manufacturer.
Routine Products Usage:
- PartiStan™ 2806.- Sizing calibration (Clause 6, ISO 11171).- Verification fluid for APC performance.
- PartiStan™ SCF (Super Clean Fluid).- APC system cleaning.- Test sample dilution.
- PartiStan™ Calibration Kits - All fluids for ISO 11171 APC calibration.- PartiStan™ UFTD.
- Ultra fine test dust suspensions for ISO 11171 - Annexes A,B,C, & E.
CON-PS2806 PartiStanTM 2806 - 2.8 mg/L ISO Medium Test Dust suspension in Super Clean Fluid 400 mL
CON-PSSCF PartiStanTM SCF - Super Clean Fluid 400 mL
CON-PSCK PartiStanTM APC calibration kits various
CON-PSUFTD PartiStanTM UFTD - Ultra Fine test dust suspension in Super Clean Fluid 400/250 mL
Conostan® Oil Analysis Standards
82 Edition 2003/2004 www.lgcpromochem.com
Code Product Unit
FTIR Operational Test Standard
The CONOSTAN® FTIR Operational Test Standard is a petroleum-based fluid similar to routine oilsamples that are analyzed by Fourier Transform Infrared (FTIR) spectroscopy as part of a condition-monitoring program. The product looks and handles like the used oil samples routinely tested, andflows through the system to monitor the cell and tubing in addition to providing a known spectrum andtest values. The CONOSTAN® FTIR Operational Test Standard validates FTIR instrumentperformance and handling procedures to ensure repeatability and reproducibility for fluid conditionmonitoring programs. Additionally, it may be used to supplement the ASTM E-1421 FTIR performancetest using polystyrene and is recommended in the pending ATSM draft practice for used oil analysisby FTIR.
An automated method has been implemented by Digilab (formerly Bio-Rad) for their line of oilanalyzers and oil analysis systems. An installation floppy disk, provided, contains the analyticalmethods and information necessary to perform these tests. Automated methods for other FTIRspectrometers are under development, owners should contact their respective manufacturers orCONOSTAN® for information on availability.
CON-FTIR-OTSPE FTIR operation test standard for Perkin-Elmer FTIR oil analysis systemsCall for availability
100 g
CON-FTIR-OTSBR FTIR operation test standard for Digilab FTIR oil analysis systemsCall for availability
100 g
Proficiency test program - Oil analysis
Programme includes:
- Elemental spectroscopy- Particle counting- Viscosity measurement
Get and remain on target with a program that tests your systems and processes. Aimfor an accurately known “bull’s-eye“ where you can learn if you are off target and thenadvance toward excellence- not a program that tests your ability to be average. Testsample values are certified and based on NIST traceable measurements. Metalssample: wear, additive, contaminants-16 each, selected from list of 22. Particlesample: based on ISO 11171/ISO Medium Test Dust. Viscosity sample: valuesdetermined per D-2162. Monthly and quarterly sample distributions available.
CON-PTSQ-Set Quarterly proficiency test subscription for metals, particle counting, and viscosityIndividual types available – please call
5 - 15 g
CON-PTSM-Set Monthly proficiency test subscription for metals, particle counting, and viscosityIndividual types available – please call
5 - 15 g
Conostan® Oil Analysis Standards
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Code Product Unit
CONOSTAN D-Series® Element (metallo-organic) Standards: D-3, D-12, D-19 (JOAP)
The CONOSTAN D-Series® standards are specially designed for military laboratories required toconform to the JOAP (Joint Oil Analysis Program –U.S.) program for emission spectrometers. Thesestandards should not be used unless the laboratory instrument is JOAP certified. Refer to anduse CONOSTAN® multi-element standards, otherwise.
D-3 series (Note: U.S. Dept. Of Defense NSN # equivalent shown with productidentity)
CON-D38100 CONOSTAN D-Series® Standard: D-3:100 (NSN 9150-01-283-0249)B .................................. 100 µg/g Mo ................................100 µg/g Zn................................. 100 µg/g
200 g
D-12 series (Note: U.S. Dept. Of Defense NSN # equivalent shown with product identity)
CON-D1285 CONOSTAN D-Series® Standard: D-12:5 ppm (NSN: 9150-01-307-3343)Ag .................................... 5 µg/g Fe .....................................5 µg/g Pb .................................... 5 µg/gAl...................................... 5 µg/g Mg ....................................5 µg/g Si...................................... 5 µg/gCr ..................................... 5 µg/g Na.....................................5 µg/g Sn .................................... 5 µg/gCu .................................... 5 µg/g Ni ......................................5 µg/g Ti...................................... 5 µg/g
200 g
CON-D12810 CONOSTAN D-Series® Standard: D-12:10 ppm (NSN: 9150-00-179-5145)Ag .................................. 10 µg/g Fe ...................................10 µg/g Pb .................................. 10 µg/gAl.................................... 10 µg/g Mg ..................................10 µg/g Si.................................... 10 µg/gCr ................................... 10 µg/g Na...................................10 µg/g Sn .................................. 10 µg/gCu .................................. 10 µg/g Ni ....................................10 µg/g Ti.................................... 10 µg/g
200 g
CON-D12830 CONOSTAN D-Series® Standard: D-12:30 ppm (NSN: 9150-00-179-5144)Ag .................................. 30 µg/g Fe ...................................30 µg/g Pb .................................. 30 µg/gAl.................................... 30 µg/g Mg ..................................30 µg/g Si.................................... 30 µg/gCr ................................... 30 µg/g Na...................................30 µg/g Sn .................................. 30 µg/gCu .................................. 30 µg/g Ni ....................................30 µg/g Ti.................................... 30 µg/g
200 g
CON-D12850 CONOSTAN D-Series® Standard: D-12:50 ppm (NSN: 9150-00-179-5143)Ag .................................. 50 µg/g Fe ...................................50 µg/g Pb .................................. 50 µg/gAl.................................... 50 µg/g Mg ..................................50 µg/g Si.................................... 50 µg/gCr ................................... 50 µg/g Na...................................50 µg/g Sn .................................. 50 µg/gCu .................................. 50 µg/g Ni ....................................50 µg/g Ti.................................... 50 µg/g
200 g
CON-D128100 CONOSTAN D-Series® Standard: D-12:100 ppm (NSN: 9150-00-179-5142)Ag ................................ 100 µg/g Fe .................................100 µg/g Pb ................................ 100 µg/gAl.................................. 100 µg/g Mg ................................100 µg/g Si.................................. 100 µg/gCr ................................. 100 µg/g Na.................................100 µg/g Sn ................................ 100 µg/gCu ................................ 100 µg/g Ni ..................................100 µg/g Ti.................................. 100 µg/g
200 g
CON-D128300 CONOSTAN D-Series® Standard: D-12:300 ppm (NSN: 9150-00-179-5141)Ag ................................ 300 µg/g Fe .................................300 µg/g Pb ................................ 300 µg/gAl.................................. 300 µg/g Mg ................................300 µg/g Si.................................. 300 µg/gCr ................................. 300 µg/g Na.................................300 µg/g Sn ................................ 300 µg/gCu ................................ 300 µg/g Ni ..................................300 µg/g Ti.................................. 300 µg/g
200 g
D-19 series (Note: U.S. Dept. Of Defense NSN # equivalent shown with productidentity)
CON-D19-0 CONOSTAN D-Series® Standard (blank): D-19:0 (NSN:9150-00-179-5137) 100 g
CON-D1945 CONOSTAN D-Series® Standard: D-19:5 ppm (no NSN number; not offered by U.S.Dept. Of Defense; see CON-D19 Set, below)Ag .................................... 5 µg/g Fe .....................................5 µg/g Si...................................... 5 µg/gAl...................................... 5 µg/g Mg ....................................5 µg/g Sn .................................... 5 µg/gB ...................................... 5 µg/g Mn ....................................5 µg/g Ti...................................... 5 µg/gBa .................................... 5 µg/g Mo ....................................5 µg/g V ...................................... 5 µg/gCd .................................... 5 µg/g Na.....................................5 µg/g Zn..................................... 5 µg/gCr ..................................... 5 µg/g Ni ......................................5 µg/gCu .................................... 5 µg/g Pb.....................................5 µg/g
100 g
CON-D19410 CONOSTAN D-Series® Standard: D-19:10 ppm (no NSN number; not offered by U.S.Dept. Of Defense; see CON-D19 Set, below)Ag .................................. 10 µg/g Fe ...................................10 µg/g Si.................................... 10 µg/gAl.................................... 10 µg/g Mg ..................................10 µg/g Sn .................................. 10 µg/gB .................................... 10 µg/g Mn ..................................10 µg/g Ti.................................... 10 µg/gBa .................................. 10 µg/g Mo ..................................10 µg/g V .................................... 10 µg/gCd .................................. 10 µg/g Na...................................10 µg/g Zn................................... 10 µg/gCr ................................... 10 µg/g Ni ....................................10 µg/gCu .................................. 10 µg/g Pb...................................10 µg/g
100 g
Conostan® Oil Analysis Standards
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Code Product Unit
CON-D19430 CONOSTAN D-Series® Standard: D-19:30 ppm (no NSN number; not offered by U.S.Dept. Of Defense; see CON-D19 Set, below)Ag .................................. 30 µg/g Fe ...................................30 µg/g Si.................................... 30 µg/gAl.................................... 30 µg/g Mg ..................................30 µg/g Sn .................................. 30 µg/gB .................................... 30 µg/g Mn ..................................30 µg/g Ti.................................... 30 µg/gBa .................................. 30 µg/g Mo ..................................30 µg/g V .................................... 30 µg/gCd .................................. 30 µg/g Na...................................30 µg/g Zn................................... 30 µg/gCr ................................... 30 µg/g Ni ....................................30 µg/gCu .................................. 30 µg/g Pb...................................30 µg/g
100 g
CON-D19450 CONOSTAN D-Series® Standard: D-19:50 ppm (no NSN number; not offered by U.S.Dept. Of Defense; see CON-D19 Set, below)Ag .................................. 50 µg/g Fe ...................................50 µg/g Si.................................... 50 µg/gAl.................................... 50 µg/g Mg ..................................50 µg/g Sn .................................. 50 µg/gB .................................... 50 µg/g Mn ..................................50 µg/g Ti.................................... 50 µg/gBa .................................. 50 µg/g Mo ..................................50 µg/g V .................................... 50 µg/gCd .................................. 50 µg/g Na...................................50 µg/g Zn................................... 50 µg/gCr ................................... 50 µg/g Ni ....................................50 µg/gCu .................................. 50 µg/g Pb...................................50 µg/g
100 g
CON-D194100 CONOSTAN D-Series® Standard: D-19:100 ppm (no NSN number; not offered by U.S.Dept. Of Defense; see CON-D19 Set, below)Ag ................................ 100 µg/g Fe .................................100 µg/g Si.................................. 100 µg/gAl.................................. 100 µg/g Mg ................................100 µg/g Sn ................................ 100 µg/gB .................................. 100 µg/g Mn ................................100 µg/g Ti.................................. 100 µg/gBa ................................ 100 µg/g Mo ................................100 µg/g V .................................. 100 µg/gCd ................................ 100 µg/g Na.................................100 µg/g Zn................................. 100 µg/gCr ................................. 100 µg/g Ni ..................................100 µg/gCu ................................ 100 µg/g Pb.................................100 µg/g
100 g
CON-D194300 CONOSTAN D-Series® Standard: D-19:300 ppm (no NSN number; not offered by U.S.Dept. Of Defense; see CON-D19 Set, below)Ag ................................ 300 µg/g Fe .................................300 µg/g Si.................................. 300 µg/gAl.................................. 300 µg/g Mg ................................300 µg/g Sn ................................ 300 µg/gB .................................. 300 µg/g Mn ................................300 µg/g Ti.................................. 300 µg/gBa ................................ 300 µg/g Mo ................................300 µg/g V .................................. 300 µg/gCd ................................ 300 µg/g Na.................................300 µg/g Zn................................. 300 µg/gCr ................................. 300 µg/g Ni ..................................300 µg/gCu ................................ 300 µg/g Pb.................................300 µg/g
100 g
CON-D194500 CONOSTAN D-Series® Standard: D-19:500 ppm (no NSN number; not offered by U.S.Dept. Of Defense; see CON-D19 Set, below)Ag ................................ 500 µg/g Fe .................................500 µg/g Si.................................. 500 µg/gAl.................................. 500 µg/g Mg ................................500 µg/g Sn ................................ 500 µg/gB .................................. 500 µg/g Mn ................................500 µg/g Ti.................................. 500 µg/gBa ................................ 500 µg/g Mo ................................500 µg/g V .................................. 500 µg/gCd ................................ 500 µg/g Na.................................500 µg/g Zn................................. 500 µg/gCr ................................. 500 µg/g Ni ..................................500 µg/gCu ................................ 500 µg/g Pb.................................500 µg/g
100 g
CON-D194700 CONOSTAN D-Series® Standard: D-19:700 ppm (no NSN number; not offered by U.S.Dept. Of Defense; see CON-D19 Set, below)Ag ................................ 700 µg/g Fe .................................700 µg/g Si.................................. 700 µg/gAl.................................. 700 µg/g Mg ................................700 µg/g Sn ................................ 700 µg/gB .................................. 700 µg/g Mn ................................700 µg/g Ti.................................. 700 µg/gBa ................................ 700 µg/g Mo ................................700 µg/g V .................................. 700 µg/gCd ................................ 700 µg/g Na.................................700 µg/g Zn................................. 700 µg/gCr ................................. 700 µg/g Ni ..................................700 µg/gCu ................................ 700 µg/g Pb.................................700 µg/g
100 g
CON-D194900 CONOSTAN D-Series® Standard: D-19:900 ppm (no NSN number; not offered by U.S.Dept. Of Defense; see CON-D19 Set, below)Ag ................................ 900 µg/g Fe .................................900 µg/g Si.................................. 900 µg/gAl.................................. 900 µg/g Mg ................................900 µg/g Sn ................................ 900 µg/gB .................................. 900 µg/g Mn ................................900 µg/g Ti.................................. 900 µg/gBa ................................ 900 µg/g Mo ................................900 µg/g V .................................. 900 µg/gCd ................................ 900 µg/g Na.................................900 µg/g Zn................................. 900 µg/gCr ................................. 900 µg/g Ni ..................................900 µg/gCu ................................ 900 µg/g Pb.................................900 µg/g
100 g
CON-D19 Set CONOSTAN D-Series® Standards: D-19:Set (NSN: 9150-01-355-1178)Each set includes
CON-D19/0A............... 4 x 100 g CON-D19/50A .............1 x 100 g CON-D19/100A........... 3 x 100 gCON-D19/5A............... 1 x 100 g CON-D19/500A ...........1 x 100 g CON-D19/300A........... 2 x 100 gCON-D19/10A............. 1 x 100 g CON-D19/700A ...........1 x 100 gCON-D19/30A............. 1 x 100 g CON-D19/900A ...........1 x 100 g
set
www.lgcpromochem.com Edition 2003/2004 85
Please photocopy this form for your use
CONOSTAN® elements in oil custom standard request formCONOSTAN® custom blends standards are available from LGC Promochem if your spectrometric analysis of metals in oilrequires a combination or concentration of metals not routinely available from stock.
Please request a quotation for any CONOSTAN® custom blend standard you require by filling out this form.
Please return the completed form to the LGC Promochem office which is responsible for your country.You will find the country list on page 3 of this catalogue.
Analyte Concentration Analyte Concentration
1 13
2 14
3 15
4 16
5 17
6 18
7 19
8 20
9 21
10 22
11 23
12 24
Base oil � 20 base oil � 75 base oil
Unit size � 100 g � 200 g � 400 g
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Ores
86 Edition 2003/2004 www.lgcpromochem.com
OresCode Product Unit
BCR-010 Tin ore - TinCertified value
Sn ............................. 765.9 g/kg
225 g
BCR-026 Zinc ore (blende) - ZincCertified value
Zn.............................. 485.0 g/kg
10 g
BCR-027 Zinc ore - ZincCertified value
Zn............................. 440.1 mg/g
10 g
BCR-028 Zinc ore (blende) - ZincCertified value
Zn.............................. 511.6 g/kg
10 g
BCR-029 Zinc ore (blende) - ZincCertified value
Zn.............................. 351.8 g/kg
10 g
BCR-030 Zinc ore (calcined calamine) - ZincCertified value
Zn.............................. 491.0 g/kg
10 g
BCR-031 Zinc ore (natural silicate) - ZincCertified value
Zn.............................. 367.3 g/kg
10 g
BCR-108 Zinc ore (blende) - Trace elementsCertified values
Cd ............................... 0.79 g/kg Fe ................................72.1 g/kg Pb ............................... 9.04 g/kgCu ............................... 0.73 g/kg Hg............................0.0109 g/kgF................................ 0.063 g/kg Mg ...............................0.75 g/kg
200 g
BCR-109 Zinc ore (blende) - Trace elementsCertified values
Cd ................................. 4.6 g/kg Fe ..............................145.1 g/kg Pb ............................... 7.38 g/kgCu ............................... 9.46 g/kg Hg..........................0.00096 g/kgF................................ 0.081 g/kg Mg ...............................0.20 g/kg
200 g
BCR-110 Zinc ore (blende) - Trace elementsCertified values
Cd ............................. 10.51 g/kg Fe ..................................5.5 g/kg Pb ............................... 97.8 g/kgCu ............................. 16.28 g/kg Hg............................0.1484 g/kgF................................ 0.055 g/kg Mg ...............................1.36 g/kg
200 g
NRMGBW07237 Zinc ore - ConstituentsCertified values for 37 elements, 9 oxides
Indicative values for 4 elements
100 g
NIST-79a Fluorspar, customs grade - Calcium fluorideCertified value
CaF2............................297.39 %
120 g
NIST-180 Fluorspar, high grade - Calcium fluorideCertified value
CaF2...............................98.80%
120 g
NIST-181 Lithium ore, Spodumene - Lithium oxideCertified value
Li2O.................................6.39 %
45 g
NIST-182 Lithium ore, Petalite - Lithium oxideCertified value
Li2O.................................4.34 %
45 g
Ores
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Code Product Unit
NIST-183 Lithium ore, Lepidolite - Lithium oxideCertified value
Li2O.................................4.12 %
45 g
NIST-RM 8455 Pyrite - Bioleaching rate (not certified)Reference value
Bioleaching rate ............................... 12.4 mg Fe/L/hr
100 g
NIST-277 Tungsten concentrate - Tungsten oxideCertified value
WO3 ................................67.4 %
Indicative values for Ca, Fe, Mn, Mo, Nb, O, P, Pb, S, Si, Sn, Ta, Ti
100 g
NIST-2430 Scheelite ore - Tunsten oxideCertified values
As..................................0.002 % Mo .................................. 0.22 % S .....................................0.26 %Bi...................................0.078 % P................................... 0.017 % WO3 ............................................70.26 %
Indicative values for Al, Cu, Fe, K, Mg, Mn, Na, Ta
100 g
NRMGBW07240 Tungsten ore - ConstituentsCertified values for 38 elements, 9 oxides
Indicative values for 5 elements
100 g
NRMGBW07241 Tungsten ore - ConstituentsCertified values for 38 elements, 9 oxides
Indicative values for 5 elements
100 g
NIST-330 Copper ore mill heads - Copper, molybdenum and rheniumCertified values
Cu ...................................0.84 % Mo ................................ 0.018 % Re ............................ 0.30 mg/kg
Indicative values for Ag, Au
100 g
NIST-25d Manganese ore - ConstituentsCertified values
Mn.................................51.78 % K2O................................. 0.93 % TiO2.................................0.13 %Al2O3 ...............................5.32 % P2O5................................ 0.25 % Available oxygen...........14.28 %Fe2O3 ..............................3.92 % SiO2 ................................ 2.52 %
Indicative values for BaO, CaO, Moisture
60 g
NRMGBW07261 Manganese ore - ConstituentsCertified values
Cu .................................0.013 % Zn ................................. 0.027 % MnO2.............................67.25 %Fe....................................1.22 % Al2O3..............................................2.20 % Na2O .............................0.044 %Mn.................................45.39 % BaO ................................ 0.68 % SiO2...............................16.16 %Ni ..................................0.019 % CaO................................ 1.06 % TiO2...............................0.063 %P ...................................0.054 % K2O................................. 1.00 %S ...................................0.007 % MgO................................ 0.64 %
Indicative value for Mn(SiO32-)
100 g
NRMGBW07262 Manganese ore - ConstituentsCertified values
Cu .................................0.014 % Zn ................................. 0.029 % MnO2.............................54.38 %Fe....................................2.24 % Al2O3..............................................3.00 % Na2O .............................0.048 %Mn.................................36.99 % BaO ................................ 0.47 % SiO2...............................22.24 %Ni ..................................0.019 % CaO................................ 3.60 % TiO2.................................0.10 %P ...................................0.081 % K2O................................. 0.46 %S ...................................0.013 % MgO................................ 1.44 %
Indicative value for Mn(SiO32-)
100 g
NRMGBW07263 Manganese ore - ConstituentsCertified values
Cu .................................0.036 % Zn ................................. 0.064 % MnO2.............................48.01 %Fe..................................11.24 % Al2O3..............................................8.55 % Na2O .............................0.039 %Mn.................................32.54 % BaO ................................ 0.18 % SiO2...............................14.50 %Ni ..................................0.099 % CaO.............................. 0.083 % TiO2.................................0.43 %P ...................................0.207 % K2O................................. 0.93 %S ...................................0.019 % MgO................................ 0.11 %
Indicative value for Mn(SiO32-)
100 g
Ores
88 Edition 2003/2004 www.lgcpromochem.com
Code Product Unit
NRMGBW07264 Manganese ore - ConstituentsCertified values
Cu .................................0.028 % Zn ................................. 0.048 % MnO2.............................36.93 %Fe..................................20.99 % Al2O3..............................................8.97 % Na2O .............................0.030 %Mn.................................25.00 % BaO ................................ 0.23 % SiO2...............................10.46 %Ni ..................................0.073 % CaO.............................. 0.051 % TiO2.................................0.54 %P ...................................0.275 % K2O................................. 0.72 %S ...................................0.032 % MgO................................ 0.10 %
Indicative value for Mn(SiO32-)
100 g
NRMGBW07265 Manganese ore - ConstituentsCertified values
Cu .................................0.009 % Zn ................................. 0.018 % Mn(CO32-)......................22.46 %
Fe....................................1.40 % Al2O3..............................................1.68 % Na2O .............................0.024 %Mn.................................22.54 % BaO ................................ 0.13 % SiO2...............................14.07 %Ni ..................................0.041 % CaO.............................. 14.73 % TiO2.................................0.10 %P ...................................0.043 % K2O................................. 0.46 %S .....................................0.21 % MgO................................ 3.50 %
Indicative value for Mn(SiO32-)
100 g
NRMGBW07266 Manganese ore - ConstituentsCertified values
Cu .................................0.014 % Zn ................................. 0.020 % Mn(CO32-)......................15.69 %
Fe....................................2.07 % Al2O3..............................................2.49 % Na2O .............................0.040 %Mn.................................15.74 % BaO ................................ 0.15 % SiO2...............................15.82 %Ni ..................................0.050 % CaO.............................. 19.78 % TiO2.................................0.15 %P ...................................0.061 % K2O................................. 0.70 %S .....................................0.27 % MgO................................ 3.82 %
Indicative value for Mn(SiO32-)
100 g
NIST-690 Iron ore, Canada - ConstituentsCertified values
Fe (total)........................66.85 % CaO................................ 0.20 % Na2O .............................0.003 %P ...................................0.011 % K2O............................. 0.0030 % SiO2.................................3.71 %S ...................................0.003 % MgO................................ 0.18 % TiO2...............................0.022 %Al2O3..............................................0.18 % MnO................................ 0.23 %
100 g
NIST-691 Iron ore, reduced - ConstituentsCertified values
C .....................................0.12 % S................................... 0.005 % Na2O .............................0.186 %Co .................................0.030 % Al2O3............................... 1.22 % SiO2...................................3.7 %Cu .................................0.032 % CaO................................ 0.63 % TiO2.................................0.27 %Fe (total)..........................90.8 % MgO................................ 0.52 %P ...................................0.006 % MnO.............................. 0.043 %
100 g
NIST-692 Iron ore, Labrador - ConstituentsCertified values
Fe (total)........................59.58 % CaO.............................. 0.023 % Na2O .............................0.008 %P ...................................0.039 % K2O............................... 0.039 % SiO2...................................3.7 %S ...................................0.005 % MgO.............................. 0.035 % TiO2...............................0.045 %Al2O3 ...............................1.41 % MnO................................ 0.46 %
100 g
NIST-693 Iron ore, Nimba - ConstituentsCertified values
Fe (total)........................65.11 % CaO.............................. 0.016 % Na2O ...........................0.0028 %P ...................................0.056 % K2O............................. 0.0028 % SiO2.................................3.87 %S ...................................0.005 % MgO.............................. 0.013 % TiO2...............................0.035 %Al2O3 ...............................1.02 % MnO.............................. 0.091 %
100 g
NRMGBW07213 Iron ore - ConstituentsCertified values
Fe (total).........................67.01% CaO................................ 0.22 % SiO2.................................3.16 %S ...................................0.118 % MgO................................ 0.71 % TiO2...............................0.032 %Al2O3 ...............................1.23 % MnO................................ 0.19 %
Indicative values for C, P, CO2, FeO, H2O+
100 g
NRMGBW07218a Iron ore - ConstituentsCertified values
Fe (total)........................64.88 % Al2O3............................... 1.59 % Mn.................................0.056 %Mn.................................0.056 % CaO.............................. 0.080 % Na2O .............................0.012 %P ...................................0.055 % FeO ................................ 0.37 % SiO2.................................3.48 %S ...................................0.015 % K2O............................... 0.085 %Ti...................................0.044 % MgO.............................. 0.044 %
100 g
Ores
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Code Product Unit
NIST-69b Bauxite, Arkansas - ConstituentsCertified values
Al2O3 ...............................48.8 % MgO.............................. 0.085 % TiO2.................................1.90 %CaO ................................0.13 % MnO.............................. 0.110 % V2O5 ..............................0.028 %Cr2O3.............................0.011 % P2O5.............................. 0.118 % ZnO.............................0.0035 %Fe2O3 ..............................7.14 % SO3............................... 0.551 % ZrO2 ................................0.29 %K2O ...............................0.068 % SiO2 .............................. 13.43 % LOI*.................................27.2 %
Indicative values for Co, BaO, Na2O
LOI* Loss on Ignition
60 g
NIST-600 Bauxite, Australian - ConstituentsCertified values
Al2O3 ...............................40.0 % MnO.............................. 0.013 % V2O5 ..............................0.060 %CaO ................................0.22 % Na2O............................. 0.022 % ZnO...............................0.003 %Cr2O3.............................0.024 % P2O5.............................. 0.039 % ZrO2 ..............................0.060 %Fe2O3 ..............................17.0 % SO3............................... 0.155 % LOI*.................................20.5 %K2O .................................0.23 % SiO2 ................................ 20.3 %MgO .................................. 0.055 TiO2 ................................ 1.31 %
LOI* Loss on Ignition
90 g
NIST-696 Bauxite, Surinam - ConstituentsCertified value
Al2O3 ...............................54.5 % MgO.............................. 0.012 % TiO2.................................2.64 %CaO ..............................0.018 % MnO.............................. 0.004 % V2O5 ..............................0.072 %Cr2O3.............................0.047 % P2O5.............................. 0.050 % ZnO.............................0.0014 %Fe2O3 ..............................8.70 % SiO2 ................................ 3.79 % ZrO2 ................................0.14 %K2O ...............................0.009 % SO3................................. 0.15 % LOI*.................................29.9 %
Indicative values for Co, BaO, Na2O
LOI* Loss on Ignition
60 g
NIST-697 Bauxite, Dominican - ConstituentsCertified value
Al2O3 ...............................45.8 % MgO................................ 0.18 % TiO2.................................2.52 %CaO ................................0.71 % MnO................................ 0.41 % V2O5 ..............................0.063 %Cr2O3.............................0.100 % P2O5................................ 0.97 % ZnO...............................0.037 %Fe2O3 ..............................20.0 % SiO2 ................................ 6.81 % ZrO2 ..............................0.065 %K2O ...............................0.062 % SO3............................... 0.077 % LOI*.................................22.1 %
Indicative values for Co, BaO, Na2O
LOI* Loss on Ignition
60 g
NIST-698 Bauxite, Jamaican - ConstituentsCertified value
Al2O3 ...............................48.2 % MgO.............................. 0.058 % TiO2.................................2.38 %CaO ................................0.62 % MnO................................ 0.38 % V2O5 ..............................0.064 %Cr2O3.............................0.080 % P2O5................................ 0.37 % ZnO...............................0.029 %Fe2O3 ............................0.013 % SiO2 ................................ 0.69 % ZrO2 ...........................0.0,061 %K2O ...............................0.010 % SO3............................... 0.143 % LOI*.................................27.3 %
Indicative values for Co, BaO, Na2O
LOI* Loss on Ignition
60 g
NIST-699 Alumina (reduction grade) - Trace constituentsCertified values
CaO ..............................0.036 % MgO............................ 0.0006 % V2O5 ............................0.0005 %Cr2O3...........................0.0002 % MnO............................ 0.0005 % ZnO...............................0.013 %Fe2O3 ............................0.013 % P2O5............................ 0.0002 % LOI*.................................0.69 %Ga2O3............................0.010 % SiO2 .............................. 0.014 %Li2O...............................0.002 % Na2O............................... 0.59 %
LOI* Loss on Ignition
60 g
NRMGBW07235 Lead ore - ConstituentsCertified values for 38 elements, 9 Oxides
Indicative values for 4 elements
100 g
NRMGBW07236 Lead ore - ConstituentsCertified values for 38 elements, 9 Oxides
Indicative values for 4 elements
100 g
NIST-670 Rutile ore - ConstituentsCertified values
Cr2O3...............................0.23 % SiO2 ................................ 0.51 % V2O5 ................................0.66 %Fe2O3 ..............................0.86 % TiO2 .............................. 96.16 % ZrO2 ................................0.84 %
90 g
Ores
90 Edition 2003/2004 www.lgcpromochem.com
Code Product Unit
NRMGBW07238 Molybdenum ore - ConstituentsCertified values for 38, elements, 9 oxides
Indicative values for 3 elements
100 g
NRMGBW07239 Molybdenum ore - ConstituentsCertified values for 38, elements, 9 oxides
Indicative values for 3 elements
100 g
NIST-886 Gold ore, refractory - Trace elementsCertified values
S ...................................1.466 % Al2O3.........................8.25 mg/kg
Indicative values for C (total), SO3
200 g
NIST-1835 Borate ore - ConstituentsCertified values
F....................................0.348 % Fe2O3............................ 1.141 % Na2O .............................3.484 %Al2O3 .............................3.474 % MgO.............................. 3.411 % SO3 ...............................1.477 %B2O3 ............................18.739 % MnO............................ 0.0333 % SrO .............................0.9418 %BaO.............................0.0497 % K2O............................... 1.261 % TiO2.............................0.1332 %CaO ............................21.622 % SiO2 ............................ 18.408 % LOI*...............................25.72 %
60 g
NRMGBW03118 Graphite ore - ConstituentsCertified values
C (graphite).....................2.91 % CO2................................. 3.60 % P2O5 ................................0.13 %Fe (total)..........................6.73 % H2O
+ ............................... 2.60 % Na2O ...............................1.60 %S .....................................1.18 % K2O................................. 2.54 % SiO2...............................49.84 %Al2O3 .............................12.93 % MgO................................ 6.10 % TiO2.................................0.57 %CaO ................................9.37 % MnO.............................. 0.084 %
50 g
NRMGBW03119 Graphite ore - ConstituentsCertified values
C (graphite).....................9.91 % CO2................................. 0.67 % P2O5 ................................0.14 %Fe (total)..........................6.99 % H2O
+ ............................... 2.80 % Na2O ...............................1.56 %S .....................................2.59 % K2O................................. 2.17 % SiO2...............................49.34 %Al2O3 .............................13.03 % MgO................................ 5.35 % TiO2.................................0.64 %CaO ................................5.34 % MnO.............................. 0.054 %
50 g
NRMGBW03120 Graphite ore - ConstituentsCertified values
C (graphite)...................76.50 % H2O+ ............................... 1.98 % SiO2...............................10.34 %
Fe (total)..........................1.48 % K2O................................. 0.99 % TiO2.................................0.55 %S .....................................0.14 % MgO................................ 0.50 % Ash................................20.78 %Al2O3 ...............................5.60 % MnO.............................. 0.022 % Volatile matter.................2.72 %CaO ................................0.74 % P2O5................................ 0.16 %CO2 .................................0.28 % Na2O............................... 0.23 %
50 g
IAEA-RGTh-1 Thorium ore (with silica) - ConstituentsReference values
Th.............................. 800 mg/kg U.................................6.3 mg/kg
Indicative value for K
500 g
IAEA-RGU-1 Uranium ore (with silica) - ConstituentsReference value
U ............................... 400 mg/kg
Indicative values for K, Th
500 g
NIST-120c Phosphate rock, Florida - ConstitutentsCertified values
Al2O3 ...............................1.30 % MnO.............................. 0.027 % U3O8............................0.0135 %Fe2O3 ..............................1.08 % Na2O............................... 0.52 % V2O3 ..............................0.016 %K2O ...............................0.147 % TiO2 .............................. 0.103 %
Values for the AFPC-method-Dependent concentrations also available
90 g
NIST-694 Phosphate rock, western - ConstituentsCertified values
Al2O3 .................................1.8 % K2O................................. 0.51 % SiO2.................................11.2 %CaO ................................43.6 % MgO................................ 0.33 % U ...............................0.01414 %CdO ..............................0.015 % MnO............................ 0.0116 % V2O5 ..............................0.031 %F........................................3.2 % Na2O............................. 0.086 %Fe2O3 ..............................0.79 % P2O5................................ 30.2 %
Indicative values for, Cr2O3 , ZnO, TiO2
90 g
Refractories and carbides
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Refractories and carbidesCode Product Unit
NIST-76a Burnt refractory (Al2O3-40%) - ConstituentsCertified values
Al2O3 ...............................38.7 % Li2O .............................. 0.042 % SiO2.................................54.9 %CaO ................................0.22 % MgO................................ 0.52 % SrO ................................... 0.037Fe2O3 ..............................1.60 % Na2O........................... 0.07 % % TiO2..................................... 2.03K2O .................................1.33 % P2O5.............................. 0.120 %
Indicative value for LOI*
75 g
NIST-77a Burnt refractory (Al2O3 - 60%) - ConstituentsCertified values
Al2O3 ...............................60.2 % Li2O .............................. 0.025 % SiO2.................................35.0 %CaO ................................0.05 % MgO................................ 0.38 % SrO ................................... 0.009Fe2O3 ..............................1.00 % Na2O............................. 0.037 % TiO2.................................2.66 %K2O ...............................0.090 % P2O5.............................. 0.092 %
Indicative value for LOI*
75 g
NIST-78a Burnt refractory (Al2O3- 70%) - ConstituentsCertified values
Al2O3 .................................1.7 % Li2O ................................ 0.12 % SiO2.................................19.4 %CaO ................................0.11 % MgO................................ 0.70 % SrO .................................0.25 %Fe2O3 ................................1.2 % Na2O............................. 0.078 % TiO2.................................3.22 %K2O .................................1.22 % P2O5.................................. 1.3 %
Indicative value for LOI*
75 g
NIST-198 Silica brick - ConstituentsCertified values
Al2O3 ...............................0.16 % Li2O .............................. 0.001 % P2O5 ..............................0.022 %CaO ................................2.71 % MgO................................ 0.07 % TiO2.................................0.02 %Fe2O3 ..............................0.66 % MnO.............................. 0.008 % LOI*.................................0.21 %K2O ...............................0.017 % Na2O............................. 0.012 %
45 g
NIST-199 Silica brick - ConstituentsCertified values
Al2O3 ...............................0.48 % Li2O .............................. 0.002 % P2O5 ..............................0.015 %CaO ................................2.41 % Na2O............................. 0.015 % TiO2.................................0.06 %Fe2O3 ..............................0.74 % MgO................................ 0.13 % LOI*.................................0.17 %K2O ...............................0.094 % MnO.............................. 0.007 %
45 g
NIST-887 Cemented carbide (W83-Co25-Ti4) - CobaltCertified value
Co .................................10.35 %
Indicative value for C
100 g
NIST-888 Cemented carbide (W64-Co25-Ti4) - Cobalt and tantalumCertified values
Co ...................................24.7 % Ta ................................... 4.77 %
Indicative value for C
100 g
NIST-889 CEM carbide (W75-Co9-Ta5-Ti4) - Cobalt, tantalum and titaniumCertified values
Co ....................................... 9.50 Ta ........................................4.60 Ti......................................... 4.03
Indicative value for C
100 g
NIST-112b Silicon carbideCertified value
Al.....................................0.44 % C (free) ........................... 0.26 % Fe....................................0.13 %C (total) .........................29.43 % Ca................................... 0.04 % Silicon carbide ..............97.37 %
80 g
NIST-276b Tungsten carbide - CarbonCertified value
C .....................................6.10 %
Indicative values for C (free), O, N
75 g
Cement
92 Edition 2003/2004 www.lgcpromochem.com
CementCode Product Unit
NIST-1880a - NIST-1889a
These materials are intended for x-ray spectroscopic and chemical analysis of cements and relatedmaterials.
NIST-1880a Portland cement (formally black) - ConstituentsCertified values
Cl ..................................0.007 % MgO................................ 1.72 % SrO ...............................0.083 %Al2O3 ...............................5.18 % Mn2O3 ........................... 0.127 % TiO2.................................0.25 %CaO ..............................63.83 % Na2O............................... 0.28 % ZnO...............................0.005 %Cr2O3.............................0.007 % P2O5................................ 0.22 % LOI*..................................... 1.32Fe2O3 ..............................2.81 % SiO2 .............................. 20.31 %K2O .................................0.92 % SO3................................. 3.25 %
Indicative values for Insoluble residue, CaO (free), F,Total
4 x 5 g
NIST-1881a Portland cement - ConstituentsCertified values
Al2O3 .............................7.060 % MgO.............................. 2.981 % SO3 ...............................3.366 %CaO ..............................57.58 % Mn2O3 ........................... 0.013 % SrO ...............................0.036 %Cr2O3...........................0.0588 % Na2O............................. 0.199 % TiO2.............................0.3663 %Fe2O3 ..............................3.09 % P2O5............................ 0.1459 % ZnO................................. 0.0489K2O ...............................1.228 % SiO2 .............................. 22.26 %
Indicative values for Cl, F, LOI, Insoluble residue
4 x 5 g
NIST-1882a Calcium aluminate cement (formally orange) - ConstituentsCertified values
Al2O3 .............................39.14 % MgO................................ 0.51 % SrO ...............................0.024 %CaO ..............................39.29 % Mn2O3 ........................... 0.060 % TiO2...............................1.786 %Cr2O3.............................0.113 % Na2O............................. 0.021 % ZnO...............................0.004 %Fe2O3 ............................14.67 % P2O5.............................. 0.070 % LOI*.................................0.20 %K2O ...............................0.051 % SiO2 ................................ 4.01 %
Indicative value for Total
4 x 5 g
NIST-1883a Calcium aluminate cement (formally silver) - ConstituentsCertified values
Al2O3 .............................70.04 % K2O............................... 0.014 % SiO2.............................0.24 % %CaO ..............................29.52 % MgO................................ 0.19 %Fe2O3 ............................0.078 % Na2O............................... 0.30 %
Indicative values for Cr2O3, P2O5, SrO, TiO2, LOI*, Total
4 x 5 g
NIST-1884a Portland cement - ConstituentsCertified values
Al2O3 .............................4.264 % MgO.............................. 4.475 % SO3 ...............................2.921 %CaO ..............................62.26 % Mn2O3 ......................... 0.0853 % SrO .............................0.2984 %Cr2O3...........................0.0166 % Na2O........................... 0.2161 % TiO2...............................0.186 %Fe2O3 ............................2.695 % P2O5............................ 0.1278 %K2O ...............................0.997 % SiO2 .............................. 20.57 %
Indicative values for ZnO, F, LOI, Total, Insoluble residues, free CaO
4 x 5 g
NIST-1885a Portland cement - ConstituentsCertified values
Al2O3 .............................4.026 % MgO.............................. 4.033 % SO3 ...............................2.830 %CaO ..............................62.39 % Mn2O3 ......................... 0.0478 % SrO ...............................0.638 %Cr2O3...........................0.0195 % Na2O............................. 1.068 % TiO2...............................0.195 %Fe2O3 ............................1.929 % P2O5............................ 0.1220 %K2O ...............................0.206 % SiO2 ............................ 20.909 %
Indicative values for ZnO, F, LOI, Total, Insoluble residues, free CaO
4 x 5 g
NIST-1886a Portland cement (cranberry) - ConstituentsCertified values
Al2O3 ...............................3.99 % Mn2O3 ........................... 0.013 % SrO .................................0.11 %CaO ..............................67.43 % Na2O............................... 0.02 % TiO2.................................0.19 %Fe2O3 ..............................0.31 % P2O5.............................. 0.025 % LOI*.................................1.73 %K2O .................................0.16 % SiO2 .............................. 22.53 %MgO ................................1.60 % SO3................................. 2.04 %
Indicative values for Cl, Cr2O3, F, ZnO, Total
3 x 5 g
Cement
www.lgcpromochem.com Edition 2003/2004 93
Code Product Unit
NIST-1887a Portland cement - ConstituentsCertified values
Al2O3 .............................6.202 % Mn2O3 ......................... 0.1186 % SrO ...............................0.322 %CaO ..............................60.90 % Na2O........................... 0.4778 % TiO2.............................0.2658 %Fe2O3 ............................2.861 % P2O5.............................. 0.306 % ZnO.............................0.0667 %K2O ...............................1.100 % SiO2 ............................ 18.637 %MgO ..............................2.835 % SO3............................... 4.622 %
Indicative values for Cl, F, LOI, Total, Insoluble residues, free CaO
4 x 5 g
NIST-1888a Portland cements - ConstiutentsCertified values
Al2O3 .............................4.265 % MgO.............................. 2.982 % SO3 ...............................2.131 %CaO ..............................63.23 % Mn2O3 ......................... 0.1256 % SrO ...............................0.082 %Fe2O3 ............................3.076 % Na2O........................... 0.1066 % TiO2...............................0.263 %K2O ...............................0.526 % SiO2 .............................. 21.22 % ZnO...............................0.107 %
Indicative values for P2O3, Cr2O3, F, LOI, Total, Insoluble residues, free CaO
4 x 5 g
NIST-1889a Portland cement - ConstituentsCertified values
Al2O3 ...............................3.89 % Mn2O3 ......................... 0.2588 % SrO ...............................0.042 %CaO ..............................65.34 % Na2O............................. 0.195 % TiO2...............................0.227 %Fe2O3 ............................1.937 % P2O5.............................. 0.110 % ZnO.............................0.0048 %K2O ...............................0.605 % SiO2 .............................. 20.66 %MgO ..............................0.814 % SO3................................. 2.69 %
Indicative values for Cl, F, LOI, Total, Insoluble residues, free CaO
4 x 5 g
NRMGBW03201a Portland cement - ConstituentsCertified values
Al2O3 ...............................5.02 % MgO................................ 1.40 % L.O.I. ...............................3.39 %CaO ..............................62.34 % Na2O............................... 0.18 % Insolubile residue............0.98 %Fe2O3 ..............................3.16 % SiO2 .............................. 20.56 %K2O .................................1.15 % SO3................................. 2.29 %
25 g
NIST-2686 Portland cement clinker - Major phasesMajor phases in cement clinker
Certified values
Alite.................................58.6 % Ferrite ............................. 14.1 % Periclase ............................33 %Belite...............................23.3 % Aluminate ......................... 2.3 %
Informational values for elemental constituents expressed as the chemical forms.
3 x 10 g
NIST-2688 Portland cement clinker - Major phasesMajor phases in cement clinker
Certified values
Alite.................................66.1 % Ferrite ............................. 11.1 % Arcanite.............................1.0 %Belite...............................17.9 % Aluminate ......................... 5.0 %
Informational values for elemental constituents expressed as the chemical forms.
3 x 10 g
NIST-2687 Portland cement clinker - Major phasesMajor phases in cement clinker
Certified values
Alite.................................73.6 % Ferrite ............................... 2.2 % Arcanite.............................1.0 %Belite.................................9.1 % Aluminate ....................... 12.1 %
Informational values for elemental constituents expressed as the chemical forms.
3 x 10 g
Glass and ceramics
94 Edition 2003/2004 www.lgcpromochem.com
Glass and ceramicsCode Product Unit
BCR-126A Lead crystal glass - ConstituentsSpecially selected glass with a composition that displays many typical analytical problems.Size: 100 x 100 x 10 mm
Certified values
Al2O3 .........................................................0.128 cg/g Na2O .......................................................... 3.58 cg/gBaO...........................................................1.036 cg/g PbO.......................................................... 23.98 cg/gCaO ..........................................................1.033 cg/g Sb2O3 ....................................................... 0.290 cg/gFe2O3 ......................................................0.0055 cg/g SiO2.......................................................... 57.80 cg/gK2O ...........................................................10.00 cg/g ZnO .......................................................... 1.020 cg/gLi2O...........................................................0.495 cg/g Density(20°C)....................................... 2.9905 g/cm3
MgO ..........................................................0.512 cg/g Refractive index (20°C) at 589.3nm............. 1.55967
300 g
BCR-664 Glass - Trace elementsSize: 50 x 50 x 7 mm
Certified values
As............................... 5.9 mg/kg Cl ..............................68.4 mg/kg Pb ............................ 53.1 mg/kgBa ............................ 29.1 mg/kg Co.............................2.77 mg/kg Sb ............................ 24.3 mg/kgCd .............................. 5.7 mg/kg Cr..............................2.65 mg/kg Se .............................. 8.6 mg/kg
plate
BCR-300 (RM) Corundum (alpha-aluminia) - Lattice spacingHigh crystallinty. Content of β-alumina of about 6 mg/g. No other phase detected.
Impurities: CaO, Fe2O3, K2O, MgO, Na2O, SiO2, TiO2
Values for lattice spacing and relative intensity at five different reflections.
Available in granular form to be ground by the user.
50 g
BCR-301 (RM) MulliteHigh crystallinty. Vitreous phase 0.03 g/g. No other phase detected.
Impurities: CaO, Fe2O3, K2O, MgO, Na2O, TiO2
Values for lattice spacing and relative intensity at five different reflections.
Available in granular form to be ground by the user.
50 g
NIST-1412 Multicomponent glass - ConstituentsSet of 8 platelets (32 x 32 x 3 mm)
Certified values
Al2O3 ...............................7.52 % CdO................................ 4.38 % SiO2...............................42.38 %B2O3 ................................4.53 % K2O................................. 4.14 % SrO .................................4.55 %BaO.................................4.67 % Na2O............................... 4.69 % ZnO.................................4.48 %CaO ................................4.53 % PbO ................................ 4.40 %
Indicative values for Fe2O3, Li2O, MgO
set (8)
NIST-89 Lead-barium glass - ConstituentsCertified values
Cl ....................................0.05 % Fe2O3............................ 0.049 % PbO...............................17.50 %Al2O3 ...............................0.18 % K2O................................. 8.40 % SiO2...............................63.35 %As2O3 ..............................0.03 % MgO................................ 0.03 % SO3 .................................0.03 %As2O5 ..............................0.36 % MnO.............................. 0.088 % TiO2.................................0.01 %BaO.................................1.40 % Na2O............................... 5.70 % ZrO2 ..............................0.005 %CaO ................................0.21 % P2O5................................ 0.23 % LOI*.................................0.32 %
45 g
NIST-92 Low boron soda-lime powder - BoronCertified value
B2O3 ................................0.70 %
Indicative values for CaO, K2O, MgO, Na2O, SiO2, ZnO, LOI*
45 g
NIST-93a Borosilicate glass - Constituents32 x 6 mm wafer
Certified values
Cl ..................................0.060 % Fe2O3............................ 0.028 % Na2O ...............................3.98 %Al2O3 ...............................2.28 % FeO .............................. 0.016 % SiO2.................................80.8 %B2O3 ..............................12.56 % K2O............................... 0.014 % TiO2...............................0.014 %CaO ................................0.01 % MgO.............................. 0.005 % ZrO2 ..............................0.042 %
wafer
NIST-1411 Soft borosilicate glass - ConstituentsSet of 10 platelets (32 x 32 x 3 mm)
Certified values
Al2O3 ...............................5.68 % Fe2O3............................ 0.050 % SiO2...............................58.04 %B2O3 ..............................10.94 % K2O................................. 2.97 % SrO .................................0.09 %BaO.................................5.00 % MgO................................ 0.33 % TiO2.................................0.02 %CaO ................................2.18 % Na2O............................. 10.14 % ZnO.................................3.85 %
set (10)
Glass and ceramics
www.lgcpromochem.com Edition 2003/2004 95
Code Product Unit
NRMGBW03132 Borosilicate glass - ConstituentsCertified values
F......................................0.54 % Fe2O3.............................. 0.34 % SiO2...............................53.98 %Al2O3 .............................14.50 % K2O................................. 0.59 % TiO2.................................0.19 %B2O3 ................................8.87 % MgO................................ 4.40 % LOI*.................................0.26 %CaO ..............................16.54 % Na2O............................. 0.096 %
50 g
NIST-81a Glass sand - ConstituentsCertified values
Al2O3 ...............................0.66 % Fe2O3............................ 0.082 % ZrO2 ..............................0.034 %Cr2O3........................... 46 mg/kg TiO2 ................................ 0.12 %
75 g
NIST-165a Glass sand (low iron) - ConstituentsCertified values
Al2O3 .............................0.059 % TiO2 .............................. 0.011 %Fe2O3 ............................0.012 % ZrO2.............................. 0.006 %
75 g
NIST-1413 Glass sand (high alumina) - ConstituentsCertified values
Al2O3 ...............................9.90 % Fe2O3.............................. 0.24 % Na2O ...............................1.75 %BaO.................................0.12 % K2O................................. 3.94 % SiO2...............................82.77 %CaO ................................0.74 % MgO................................ 0.06 % TiO2.................................0.11 %
75 g
Sand No.1 Sand - ConstituentsCertified values
Al2O3 .............................0.061 % MgO.............................. <0.02 % Cr3O3...........................0.0003 %CaO .............................< 0.02 % Na2O............................. <0.02 % LOI*.................................0.12 %Fe2O3 (total Fe) .............0.014 % SiO2 .............................. 99.74 %K2O ..............................< 0.02 % TiO2 .............................. 0.026 %
*Loss on ignition
200 g
Sand No.6 Sand - ConstituentsCertified values
Al2O3 ...............................0.60 % K2O................................. 0.40 % SiO2...............................98.66 %CaO .............................< 0.02 % MgO.............................. <0.02 % TiO2...............................0.024 %Fe2O3 (total Fe) .............0.032 % Na2O............................. <0.02 % LOI*.................................0.14 %
*Loss on ignition
200 g
Sand No.8 Sand - ConstituentsCertified values
Al2O3 ...............................2.07 % K2O.............................. < 1.06 % SiO2...............................95.63 %CaO ................................0.06 % MgO................................ 0.12 % TiO2...............................0.073 %Fe2O3 (total Fe) ...............0.26 % Na2O............................... 0.20 % LOI*.................................0.48 %
*Loss on ignition
200 g
Sand No.9 Sand - ConstituentsCertified values
Al2O3 ...............................1.35 % K2O................................. 0.82 % SiO2...............................97.24 %CaO ................................0.02 % MgO................................ 0.06 % TiO2...............................0.044 %Fe2O3 (total Fe) .............0.103 % Na2O............................... 0.10 % LOI*.................................0.24 %
*Loss on ignition
200 g
NIST-620 Soda-lime flat glass - ConstituentsSet of 3 platelets (35 x 35 x 3 mm)
Certified values
Al2O3 ...............................1.80 % K2O................................. 0.41 % SO3 .................................0.28 %As2O3 ............................0.056 % MgO................................ 3.69 % TiO2...............................0.018 %CaO ................................7.11 % Na2O............................. 14.39 %Fe2O3 ............................0.043 % SiO2 .............................. 72.08 %
set (3)
NIST-621 Soda-lime container glass - ConstituentsSet of 3 disks (38 x 5 mm)
Certified values
Al2O3 ...............................2.76 % Fe2O3............................ 0.040 % SO3 .................................0.13 %As2O3 ............................0.030 % K2O................................. 2.01 % SiO2...............................71.13 %BaO.................................0.12 % Na2O............................. 12.74 % TiO2...............................0.014 %CaO ..............................10.71 % MgO................................ 0.27 % ZrO2 ..............................0.007 %
set (3)
Glass and ceramics
96 Edition 2003/2004 www.lgcpromochem.com
Code Product Unit
NIST-1830 Soda-lime float glass - ConstituentsSet of 3 platelets (38 x 38 x 6 mm)
Certified values
Al2O3 ...............................0.12 % K2O................................. 0.04 % SO3 .................................0.26 %CaO ................................8.56 % MgO................................ 3.90 % TiO2...............................0.011 %FeO...............................0.032 % Na2O............................. 13.75 %Fe2O3 ............................0.121 % SiO2 .............................. 73.07 %
3 platelets
NIST-1831 Soda lime sheet glass - ConstituentsSet of 3 platelets (37 x 37 x 3 mm)
Certified values
Al2O3 ...............................1.21 % K2O................................. 0.33 % SO3 .................................0.25 %CaO ................................8.20 % MgO................................ 3.51 % TiO2...............................0.019 %FeO...............................0.025 % Na2O............................. 13.32 %Fe2O3 ............................0.087 % SiO2 .............................. 73.08 %
3 platelets
EC 1.1 Soda lime-magnesia-silica glass - ConstituentsCertified values
Al2O3 ...............................1.08 % K2O................................. 0.59 % SiO2...............................71.97 %CaO ................................8.63 % MgO................................ 3.78 % SO3 (total S) ....................0.23 %Fe2O3(total Fe)..............0.121 % Na2O............................. 13.41 % TiO2...............................0.040 %
75x75x6 mm
NIST-1834 Fused ore glass - Constiutents30 x 3 mm disc
Certified values
Al...................................20.71 % K..................................... 0.42 % Sr ..................................0.153 %Ba .................................0.062 % Mg ................................ 0.088 % Ti.....................................1.11 %Ca ................................... 0.0955 P................................... 0.152 %Fe....................................0.32 % Si .................................. 20.19 %
Indicative values for B, Cr, Li, Na, Zr
disk
Glass No.4 Fluoride opal glass - ConstituentsReference: Glass Technol., 1962, 3 (1), 9-16, ‘the chemical analysis of a fluoride glass described as StandardGlass No. 4’.
Certified values
F......................................4.96 % K2O................................. 0.57 % TiO2...............................0.041 %Al2O3 ...............................3.02 % MgO.............................. <0.05 % ZnO.................................3.28 %B2O3 ................................0.19 % Na2O............................. 15.45 % LOI* (550°C) ...................0.22 %CaO ................................4.24 % SO3 (total S) ................. <0.05 %Fe2O3 (total Fe) .............0.099 % SiO2 .............................. 69.49 %
*Loss on ignition
25 g
Glass No.5 Soda lime-magnesia-silica glass - ConstituentsReference glass Technol.,1973, 14 (1), 5-13, ‘ The chemical analysis of a colourless soda-lime-silica glass’.
Certified values
Al2O3 ...............................1.12 % K2O................................. 0.42 % SO3 (total S)....................0.21 %CaO ................................6.55 % MgO................................ 2.75 % SiO2...............................72.74 %Fe2O3 (total Fe) .............0.043 % Na2O............................. 15.65 % TiO2...............................0.034 %
25 g
Glass No.6 Soda lime-silica glass - ConstituentsCertified values
Al2O3 ...............................1.70 % K2O................................. <0.1 % SO3 (total S)....................0.21 %CaO ................................9.97 % MgO................................ <0.1 % SiO2...............................73.06 %Fe2O3 (total Fe) .............0.034 % Na2O............................. 14.65 % TiO2.................................0.02 %
25 g
Glass No.7 Soda lime-silica glass - ConstituentsCertified values
Al2O3 ...............................1.50 % Na2O............................. 13.90 % TiO2...............................0.042 %CaO ..............................11.03 % MgO................................ 0.14 % LOI* (550°C) ...................0.07 %Fe2O3 (total Fe) .............0.044 % SO3 (total S) ................... 0.19 %K2O .................................0.43 % SiO2 .............................. 73.06 %
*Loss on ignition
25 g
Glass No.8 Lead oxide-potassium oxide-silica glass - ConstituentsCertified values
Al2O3 ...............................0.05 % Fe2O3 (total Fe)............. 0.010 % PbO...............................30.59 %As2O3 (total As)...............0.32 % K2O............................... 11.85 % SiO2...............................56.34 %B2O3 ................................0.36 % MgO.............................. <0.02 % TiO2.................................0.02 %CaO ..............................<0.02 % Na2O............................... 0.23 % LOI* (550°C) ...................0.21 %
*Loss on ignition
25 g
Glass and ceramics
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Code Product Unit
SGT 10 Soda-lime-silica container glass - Constituents40 mm diameter disc
Certified values
Al2O3 ...............................1.62 % K2O................................. 0.35 % SO3 .................................0.05 %BaO.................................0.02 % MgO................................ 1.81 % TiO2...............................0.097 %CaO ................................10.7 % Na2O............................... 12.2 % Cr3O3.............................0.020 %Fe2O3 ............................0.325 % SiO2 ................................ 72.7 %
disc
SGT 10-P Soda-lime-silica container glass - ConstituentsGlass pieces
pieces
SGT 11 Soda-lime-silica container glass - Constituents40 mm diameter disc
Certified values
Al2O3 ...............................1.83 % K2O................................. 0.69 % SO3 .................................0.06 %BaO.................................0.03 % MgO................................ 2.14 % TiO2...............................0.068 %CaO ................................10.3 % Na2O............................... 13.6 % Cr3O3.............................0.205 %Fe2O3 ............................0.342 % SiO2 ................................ 70.7 %
disc
SGT 11-P Soda-lime-silica container glass - ConstituentsGlass pieces
pieces
NIST-607 Potassium feldspar - Trace elementsCertified values
Rb ........................ 523.90 mg/kg Sr..........................65.485 mg/kg
5 g
NIST-610 and NIST-611NIST-610 and NIST-611 are the same material and therefore have the same certified values. NIST-610 consistsof glass 3 mm thick and NIST-611 is 1 mm thick.
NIST-610 Glass - Trace elementsCertified values
Fe.............................. 458 mg/kg Pb..............................426 mg/kg Th........................... 457.2 mg/kgMn............................. 485 mg/kg Rb...........................425.7 mg/kg U ............................ 461.5 mg/kgNi ........................... 458.7 mg/kg Sr............................515.5 mg/kg
Indicative values for Ag, Au, Co, Cu, K, Ti, Tl, Zn
6 wafers
NIST-611 Glass - Trace elements 6 wafers
NIST-612 and NIST-613NIST-612 and NIST-613 are the same material and therefore have the same certified values. NIST-612 consistsof glass 3 mm thick and NIST-613 is 1 mm thick.
NIST-612 Glass - Trace elementsCertified value
Ag ............................ 22.0 mg/kg Pb...........................38.57 mg/kg Th............................. 37.9 mg/kgFe................................ 51 mg/kg Rb.............................31.4 mg/kg U ............................ 37.38 mg/kgNi ............................. 38.8 mg/kg Sr..............................78.4 mg/kg
Indicative values for Au, B, Ba, Ce, Co, Cu, Dy, Er, Eu, Gd, K, La, Mn, Nd, Sm, Ti, Tl, Zn
6 wafers
NIST-613 Glass - Trace elements 6 wafers
NIST-614 and NIST-615NIST-614 and NIST-615 are the same material and therefore have the same certified values. NIST-614 consistsof wafers of glass 3 mm thick and NIST-615 is 1 mm thick.
NIST-614 Glass - Trace elementsCertified values
Ag ............................ 0.42 mg/kg Pb.............................2.32 mg/kg Th........................... 0.748 mg/kgCu ............................ 1.37 mg/kg Rb...........................0.855 mg/kg U ............................ 0.823 mg/kgK ................................. 30 mg/kg Sr..............................78.4 mg/kg
Indicative values for Au, B, Cd, Co, Eu, Fe, Ga, La, Ni, Sb, Sc, Ti, Tl
6 wafers
NIST-615 Glass - Trace elements 6 wafers
Glass and ceramics
98 Edition 2003/2004 www.lgcpromochem.com
Code Product Unit
NIST-616 and NIST-617NIST-616 and NIST-617 are the same material and therefore have the same certified values. NIST-616 consistsof wafers of glass 3 mm thick and NIST-617 is 1 mm thick.
NIST-616 Glass - Trace elementsCertified values
K ................................. 29 mg/kg Sr............................41.72 mg/kg U .......................... 0.0721 mg/kgPb ............................ 1.85 mg/kg Th .........................0.0252 mg/kg
Indicative values for Au, B, Cu, Fe, Ga, La, Rb, Sb, Sc, Ti, Tl
6 wafers
NIST-617 Glass - Trace elements 6 wafers
NIST-1872 Synthetic glass - Lead and germaniumNIST-1872 consists of three different lead-germanate glasses in rod form approximately 2 x 2 x 20 mm.
K-453
Certified values
Ge .................................28.43 % Pb................................. 54.21 %
Indicative value for O
K-491
Certified values
Ge .................................26.10 % Pb................................. 54.69 %
Indicative values for Al, Ce, Fe, O, Si, Ta, Ti, Zr
K-968
Certified values
Ge .................................25.93 % Pb................................. 54.74 %
Indicative values for Ba, Cr, Eu, Mg, Ni, O, P, Si, Th, Ti, U, Zr
set (3)
NIST-1873 Synthetic glass - Barium, silicon and zincNIST-1873 consists of three different barium-zinc-silicate glasses in rod form approximately 2 x 2 x 20mm.
K-458
Certified values
Ba .................................41.79 % Si .................................. 23.05 % Zn....................................3.01 %
Indicative value for O
K-489
Certified values
Ba .................................39.53 % Zn ................................... 2.93 %
Indicative values for Al, Ce, Fe, O, Pb, Si, Ta, Ti, Zr
K-963
Certified values
Ba .................................39.21 % Zn ................................... 2.95 %
Indicative values for Cr, Eu, Ge, Mg, O, Si
set (3)
NIST-2063a Mineral glass (for transmission electron microscope)NIST-2063a consists of a mineral glass film that has been deposited onto a 20 nm thick carbon support film on a3 mm diameter, copper transmission electron microscope grid.
Certified values
Ca .................................11.82 % Mg .................................. 7.97 % Si...................................25.34 %Fe..................................11.06 % O..................................... 43.2 %
Indicative value for Ar
glass film
Plastics
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PlasticsCode Product Unit
The „Packaging-Directive“ - EC-Directive 94/62/EEC - regulates the amount of metals such as Cd, Cr,Hg and Pb in plastics. The materials VDA 001-4 as well as BCR-680 and -681 were produced tofacilitate the implementation of this directive and to allow the effective introduction of QA-systems forelemental analysis of plastic materials.
VDA 001-4 Plastic - CadmiumFour polyethylene reference materials have been certified by IRMM on behalf of Verband der Automobilindustriee.V. (VDA).
Certified values
Sicolen Yellow 09/16493
Cd ................... 40.9 ± 1.2 mg/kg
Sicolen Orange 28/16494
Cd ................... 75.9 ± 2.1 mg/kg
Sicolen Red 39/16495
Cd ................. 197.9 ± 4.8 mg/kg
Sicolen Bordeaux 49/16496
Cd ..................... 407 ± 12 mg/kg
4 bottles
BCR-680 Polyethylene - Trace elements (high level)Certified values
As............................. 30.9 mg/kg Cl ...............................810 mg/kg Pb .......................... 107.6 mg/kgBr .............................. 808 mg/kg Cr............................114.6 mg/kg S ....................... 0.67x103 mg/kgCd .......................... 140.8 mg/kg Hg.............................25.3 mg/kg
100 g
BCR-681 Polyethylene - Trace elements (low level)Certified values
As............................. 3.93 mg/kg Cl ..............................92.9 mg/kg Pb ............................ 13.8 mg/kgBr ................................ 98 mg/kg Cr..............................17.7 mg/kg S ................................. 78 mg/kgCd ............................ 21.7 mg/kg Hg.............................4.50 mg/kg
100 g
MetalsCode Product Unit
BCR-025A Aluminium (primary ingot) - Oxygen, carbon and boron26 mm diameter x 9 mm disc
Certified values
O .............................. <0.1 mg/kg C...............................0.26 mg/kg B .............................. 1.22 mg/kg
12 g
BCR-025B Aluminium (primary ingot) - Oxygen, carbon and boron8 mm diameter x 50 mm cylinder
6 g
BCR-329 Aluminium-Magnesium alloy (3 % Mg) - BoronChips
Certified value
B .................................... 30 µg/g
50 g
BCR-330 Aluminium-Magnesium alloy (3 % Mg) - Boron55 mm diameter x 30 mm disc
Certified value
B ................................. 30 mg/kg
190 g
BCR-017A Copper - Sulphur and phosphorous42 mm diameter x 30 mm disc
Certified values
P ................................ 6.9 mg/kg S...............................10.4 mg/kg
370 g
BCR-017B Copper - Sulphur and phosphorousChips (bottle with 50 g)
50 g
Metals
100 Edition 2003/2004 www.lgcpromochem.com
Code Product Unit
BCR-022A Copper (electrolytic tough pitch) - Oxygen26 mm diameter x 9 mm disc
Certified value
Oxygen...................... 139 mg/kg
42 g
BCR-022B Copper (electrolytic tough pitch) - Oxygen9 m diameter x 50 mm rods
28 g
BCR-054R Copper - Oxygen7 m diameter x 50 mm rods
Certified value
O .............................. 0.47 mg/kg
42 g
BCR-058 Copper (continuous cast) - Oxygen7 mm diameter x 50 mm rods
Certified value
Oxygen...................... 390 mg/kg
17 g
BCR-055 Lead (refined) - Oxygen7 mm diameter x 9 mm discs
Certified value
Oxygen....................... 1.0 mg/kg
71 g
BCR-023A Molybdenum - Oxygen, nitrogen and carbon26 mm diameter x 9 mm discs
Certified values
Oxygen..................... 14.7 mg/kg Nitrogen....................<0.3 mg/kg Carbon ..................... <0.2 mg/kg
49 g
BCR-023B Molybdenum - Oxygen, nitrogen and carbon25 cubes of 1 g
25 g
BCR-099 Nickel - Oxygen and nitrogen25 cubes of 2 g
Certified values
Oxygen....................... 8.4 mg/kg Nitrogen......................1.1 mg/kg
50 g
BCR-024B Titanium - Oxygen and nitrogen25 cubes of 0.4 g
Certified values
Nitrogen .................... 117 mg/kg Oxygen ......................608 mg/kg
10 g
BCR-024C Titanium - Oxygen, nitrogen25 cubes of 0.2 g
5 g
BCR-059A Titanium alloy Ti6Al4V - Oxygen and nitrogen26 mm diameter x 9 mm discs
Certified values
Oxygen.................... 1750 mg/kg Nitrogen.....................172 mg/kg
21 g
BCR-059B Titanium alloy Ti6Al4V - Oxygen and nitrogen25 cubes of 0.2 g
5 g
BCR-318 Titanium - Hydrogen7 mm diameter x 1 mm discs (approx. 100 discs)
Certified value
Hydrogen ................. 12.2 mg/kg
20 g
BCR-275 Zirconium alloy Zircaloy-4 - Oxygen, nitrogen and carbon10 discs each 13 mm diameter x 1 mm
Certified values
O ............................. 1673 mg/kg N...............................39.0 mg/kg C ............................ 113.3 mg/kg
9 g
BCR-276 Zirconium alloy Zircaloy-4 - Oxygen, nitrogen and carbon4.5 mm diameter x 2 mm (approx. 100 cylinders)
Certified values
O ............................. 1541 mg/kg N...............................41.1 mg/kg C ............................ 107.6 mg/kg
20 g
Metals
www.lgcpromochem.com Edition 2003/2004 101
Code Product Unit
BCR-102 Tungsten carbide powder - OxygenPowder sealed under argon
Certified value
O ............................... 185 mg/kg
2-3 g
BCR-074A Electrolytic copper - Trace elementsCylinder of 40 mm diameter and 30 mm height
Certified values
Ag ............................ 12.8 mg/kg Fe .............................1.14 mg/kg Se ............................ 0.37 mg/kgAs............................. 0.78 mg/kg Mn ............................1.27 mg/kg Sn .......................... <0.07 mg/kgCd .......................... <0.02 mg/kg Ni ..............................1.04 mg/kg Zn............................. 0.46 mg/kgCo .......................... <0.05 mg/kg Pb.............................0.97 mg/kgCr ............................. <0.1 mg/kg Sb.............................0.58 mg/kg
Indicative values for Bi, Te
disc
BCR-074B Electrolytic copper - Trace elementsPair of rods of 8 mm diameter and 100 mm lenght
2 rods
BCR-074C Electrolytic copper - Trace elementsSmall pieces in a bottle containing about 50 g
50 g
BCR-075A Copper with added impurities - Trace elementsCylinder of 40 mm diameter and 30 mm height
Certified values
Ag ............................ 12.2 mg/kg Cr..............................0.89 mg/kg Sb ............................ 2.56 mg/kgAs............................. 3.74 mg/kg Fe ...............................9.0 mg/kg Se ............................ 1.26 mg/kgBi.............................. 1.44 mg/kg Mn ............................3.23 mg/kg Sn ............................ 1.09 mg/kgCd ............................ 2.57 mg/kg Ni ..............................1.45 mg/kg Te............................. 1.52 mg/kgCo ............................ 2.50 mg/kg Pb.............................3.27 mg/kg Zn............................. 3.47 mg/kg
disc
BCR-075B Copper with added impurities - Trace elementsPair of rods of 8 mm diameter and 100 mm length
2 rods
BCR-075C Copper with added impurities - Trace elementsSmall pieces in a bottle containing about 50 g
50 g
BCR-691 Copper alloys - Alloying elementsSet of five discs (one of each composition) of 35 diameter and 2 mm thickness
Certified values
Substance Quaternary bronze Brass Arsenic-Copper Lead-bronze Tin-bronze
As....................................1.94 g/kg.............. 0.99 g/kg..............46.0 g/kg ..........2.85 g/kg.............. 1.94 g/kg
Pb .....................................79 g/kg................ 3.9 g/kg..............1.75 g/kg .............92 g/kg.............. 2.04 g/kg
Sn ...................................71.6 g/kg.............. 20.6 g/kg..............2.02 g/kg ...........101 g/kg................. 70 g/kg
Zn....................................60.2 g/kg............... 148 g/kg..............0.55 g/kg ..........1.48 g/kg.............. 1.57 g/kg
Set (5)
BCR-286A Lead (electrolytically refined) - Trace elementsBlocks of 60 mm x 60 mm x 12 mm
Certified values
Ag .......................... 0.015 mg/kg Cu.............................1.49 mg/kg Sn .......................... <0.05 mg/kgAs......................... <0.002 mg/kg Ni ............................0.041 mg/kg Te............................. <0.1 mg/kgBi.............................. 21.5 mg/kg Sb.............................0.10 mg/kg Ti................................ 2.5 mg/kgCd .......................... 0.125 mg/kg Se...........................<0.05 mg/kg Zn............................. <0.1 mg/kg
600 g
BCR-286B Lead (electrolytically refined) - Trace elementsChips in bottles containing about 160 g
160 g
BCR-287A Lead (thermally refined) -Trace elementsBlocks of 60 mm x 60 mm x 12 mm
Certified values
Ag ............................ 15.2 mg/kg Cu.............................0.89 mg/kg Sn .......................... <0.05 mg/kgAs......................... <0.003 mg/kg Ni ............................0.024 mg/kg Te............................. <0.2 mg/kgBi.............................. 67.3 mg/kg Sb...........................0.040 mg/kg Ti.............................. 0.73 mg/kgCd ............................ 0.36 mg/kg Se...........................<0.05 mg/kg Zn............................. <0.1 mg/kg
600 g
BCR-287B Lead (thermally refined) -Trace elementsChips in bottles containing about 160 g
160 g
Metals
102 Edition 2003/2004 www.lgcpromochem.com
Code Product Unit
BCR-288A Lead with added impurities - Trace elementsBlocks of 60 mm x 60 mm x 12 mm
Certified values
Ag ............................ 30.5 mg/kg Cu.............................19.3 mg/kg Sn ............................ 30.6 mg/kgAs............................. 55.7 mg/kg Ni ..............................4.57 mg/kg Te............................. 32.8 mg/kgBi............................ 215.8 mg/kg Sb.............................32.5 mg/kg Ti................................ 2.3 mg/kgCd ............................ 33.3 mg/kg Se.............................<0.2 mg/kg Zn............................... 8.2 mg/kg
600 g
BCR-288B Lead with added impurities - Trace elementsChips in bottles containing about 160 g
160 g
BCR-321 Unalloyed zinc - Trace elementsDiscs of 80 mm diameter and 20 mm thickness
Certified values
Al.............................. <0.7 mg/kg Pb.............................4.85 mg/kg Tl.............................. 0.78 mg/kgIn .............................. <0.2 mg/kg Sn.............................<0.5 mg/kg
Indicative values for Cd, Cu, Fe
0.7 kg
BCR-322R Unalloyed zinc - ImpuritiesDiscs of 60 mm diameter and 30 mm thickness
Certified values
Cd .......................... 15.08 mg/kg Fe .............................19.1 mg/kg Sn .............................. 5.6 mg/kgCu ............................ 5.89 mg/kg Pb.............................15.0 mg/kg Tl.............................. 5.28 mg/kg
0.7 kg
BCR-323R Unalloyed zinc - ImpuritiesDiscs of 60 mm diameter and 30 mm thickness
Certified values
Cd ............................ 6.51 mg/kg Fe .............................11.3 mg/kg Sn ............................ 18.7 mg/kgCu ............................ 18.9 mg/kg Pb.............................48.6 mg/kg Tl.............................. 10.8 mg/kg
0.7 kg
BCR-324R Unalloyed zinc - ImpuritiesDiscs of 60 mm diameter and 30 mm thickness
Certified values
Cd ............................ 48.6 mg/kg Fe .............................58.5 mg/kg Sn .............................. 9.8 mg/kgCu ............................ 9.87 mg/kg Pb.............................26.1 mg/kg Tl.............................. 19.9 mg/kg
0.7 kg
BCR-325R Unalloyed zinc - ImpuritiesDiscs of 60 mm diameter and 30 mm thickness
Certified values
Cd ............................ 94.7 mg/kg Fe .............................56.1 mg/kg Sn ............................ 46.1 mg/kgCu ............................ 47.5 mg/kg Pb..............................142 mg/kg Tl.............................. 36.8 mg/kg
0.7 kg
BCR-326 Unalloyed zinc - ImpuritiesDiscs of 80 mm diameter and 2 mm thickness
Certified values
Cd .......................... 203.0 mg/kg Fe ...........................264.8 mg/kgCu .......................... 104.8 mg/kg Pb...........................307.0 mg/kg
Indicative value for Al
0.7 kg
BCR-327 Unalloyed zinc - ImpuritiesDiscs of 80 mm diameter and 2 mm thickness
Certified values
Cd .......................... 301.4 mg/kg Fe ...........................144.0 mg/kg Pb .......................... 409.4 mg/kg
Indicative value for Cu
0.7 kg
BCR-351 Zinc alloy ZnAl4 - Trace elementsDiscs of 80 mm diameter and 20 mm thickness
Certified values
Al................... 43.55 x 103 mg/kg Mg ..........................131.0 mg/kg Tl.............................. 0.74 mg/kgCu .......................... 12.13 mg/kg Pb.............................4.50 mg/kgIn .............................. <0.2 mg/kg Sn................................<1 mg/kg
Indicative values for Cd, In, Ni
0.7 kg
Metals
www.lgcpromochem.com Edition 2003/2004 103
Code Product Unit
BCR-352 Zinc alloy ZnAl4 - Trace elementsDiscs of 80 mm diameter and 20 mm thickness
Certified values
Al................... 41.50 x 103 mg/kg In ..............................3.02 mg/kg Sn .............................. 3.0 mg/kgCd ............................ 2.88 mg/kg Mg ..........................283.0 mg/kg Tl................................ 3.2 mg/kgCu .......................... 31.26 mg/kg Ni ..............................6.74 mg/kg
Indicative value for Pb
0.7 kg
BCR-353 Zinc alloy ZnAl4 - Trace elementsDiscs of 80 mm diameter and 20 mm thickness
Certified values
Al..................... 39.5 x 103 mg/kg In ..............................2.55 mg/kg Sn .............................. 5.6 mg/kgCd .......................... 10.44 mg/kg Mg ..........................452.5 mg/kg Tl.............................. 3.95 mg/kgCu .......................... 100.0 mg/kg Pb.............................24.4 mg/kg
0.7 kg
BCR-354 Zinc alloy ZnAl4 - Trace elementsDiscs of 80 mm diameter and 20 mm thickness
Certified values
Al................... 37.27 x 103 mg/kg In ................................9.8 mg/kg Pb ............................ 30.8 mg/kgCd ............................ 29.7 mg/kg Mg .............................602 mg/kg Sn ............................ 14.1 mg/kgCu .......................... 312.3 mg/kg Ni ..............................83.1 mg/kg Tl............................ 11.01 mg/kg
0.7 kg
BCR-355 Zinc alloy ZnAl4 - Trace elementsDiscs of 80 mm diameter and 20 mm thickness
Certified values
Al................... 34.43 x 103 mg/kg In ..............................24.6 mg/kg Pb ............................ 56.9 mg/kgCd ............................ 58.1 mg/kg Mg .............................786 mg/kg Sn ............................ 29.1 mg/kgCu ........................... 1035 mg/kg Ni ...............................268 mg/kg Tl............................ 23.25 mg/kg
0.7 kg
BCR-356 Zinc alloy ZnAl4Cu1 - Trace elementsDiscs of 80 mm diameter and 20 mm thickness
Certified values
Al................... 44.34 x 103 mg/kg Fe .............................31.5 mg/kg Ni ............................. 3.43 mg/kgCd ............................ 0.73 mg/kg In ..............................<0.2 mg/kg Pb ............................ 9.87 mg/kgCu ................. 3.944 x 103 mg/kg Mg ..........................132.3 mg/kg Tl.............................. 0.79 mg/kg
Indicative value for Sn
0.7 kg
BCR-357 Zinc alloy ZnAl4Cu1 - Trace elementsDiscs of 80 mm diameter and 20 mm thickness
Certified values
Al................. 42.270 x 103 mg/kg In ..............................3.30 mg/kg Sn ............................ 3.51 mg/kgCd ............................ 2.83 mg/kg Mg .............................273 mg/kg Tl.............................. 2.76 mg/kgCu ................ 5.849 x 103 mg/kg Ni ..............................9.82 mg/kgFe............................. 25.7 mg/kg Pb.............................13.8 mg/kg
0.7 kg
BCR-358 Zinc alloy ZnAl4Cu1 - Trace elementsDiscs of 80 mm diameter and 20 mm thickness
Certified values
Al................... 39.46 x 103 mg/kg In ..............................7.04 mg/kg Sn ............................ 7.87 mg/kgCd .......................... 10.22 mg/kg Mg .............................403 mg/kg Tl.............................. 6.09 mg/kgCu .................. 7.93 x 103 mg/kg Ni ............................26.98 mg/kgFe............................. 40.5 mg/kg Pb.............................22.5 mg/kg
0.7 kg
BCR-359 Zinc alloy ZnAl4Cu1 - Trace elementsDiscs of 80 mm diameter and 20 mm thickness
Certified values
Al................... 37.11 x 103 mg/kg In ..............................15.5 mg/kg Sn .......................... 16.93 mg/kgCd ............................ 29.8 mg/kg Mg .............................557 mg/kg Tl............................ 13.34 mg/kgCu .................. 9.89 x 103 mg/kg Ni ..............................92.6 mg/kgFe........................... 119.7 mg/kg Pb.............................36.2 mg/kg
0.7 kg
BCR-360 Zinc alloy ZnAl4Cu1 - Trace elementsDiscs of 80 mm diameter and 20 mm thickness
Certified values
Al................... 34.27 x 103 mg/kg In ..............................29.8 mg/kg Pb ............................ 73.9 mg/kgCd ............................ 59.5 mg/kg Mg .............................705 mg/kg Sn ............................ 33.0 mg/kgCu ................ 12.34 x 103 mg/kg Ni ...............................267 mg/kg Tl.............................. 25.9 mg/kg
0.7 kg
Metals
104 Edition 2003/2004 www.lgcpromochem.com
Code Product Unit
BCR-361 Zinc alloy ZnAl4Cu1 - Trace elementsDiscs of 80 mm diameter and 20 mm thickness
Certified values
Al................... 40.68 x 103 mg/kg Fe ...........................10.34 mg/kg Sn ............................ 46.3 mg/kgCu .................. 7.98 x 103 mg/kg Pb.............................5.31 mg/kg Tl.............................. 37.4 mg/kg
Indicativ values for cd, In
0.7 kg
BCR-089 Titnanium alloy Ti 6Al 4V - ImpuritiesCylinder of 40 mm diameter and 20 mm height
Certified values
Al................................. 59.7 g/kg V............................... 39.76 g/kg
disc
BCR-090A Titanium - ImpuritiesCylinder of 40 mm diameter and 20 mm height
Certified values
B ....................... 28.2 x 10-3 g/kg Cu..............................0.513 g/kg Mo............................ 0.488 g/kgCo ............................ 0.501 g/kg Fe ............................. 0.563 g/kg Ni ............................. 0.667 g/kgCr .............................. 0.533 g/kg Mn ............................ 0.314 g/kg
Indivativ values for Al, Nb, Sn, V, W, Zr
disc
BCR-090B Titanium - ImpuritiesCubes of about 0.2 g
25 g
BCR-098 Zircaloy-4 - ImpuritiesChips
Certified values
Cr ............................. 906 mg/kg Hf..............................77.6 mg/kgFe............................ 2143 mg/kg Sn..........................14600 mg/kg
10 g
LGC Promochem supplies a comprehensive range of ferrous and non-ferrous metal certifiedreference materials produced by BCR®, European Commission and National Institute of Standardsand Technology (NIST), USA. Please contact the responsible office in your country.
Miscellaneous
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MiscellaneousCode Product Unit
LGC9000 Wool worsted/polyester woven fabricWool/polyester fabric with the wool as combed fibres and the polyester as discontinuous fibres.
Certified values
Polyester .........................56.3 % Wool ............................... 43.7 %
10 x 1 g
LGC9001 Cotton/polyester woven fabricCotton/polyester fabric with the cotton as normal unmercerized fibres and the polyester as discontinuous fibres.
Certified values
Polyester .........................51.5 % Cotton............................. 48.5 %
10 x 1 g
LGC3004 Petroleum wax - OilCertified value
Oil content.......................0.54 %
5 x 1 g
NIST-2567 Catalyst package for lubricant oxidation - ASTM sequence IIIE engine testThis Standard Reference Material is specified for the use in the NIST modification to ASTM D 4742, StandardTest Method for the Oxidation Stability of Gasoline Automobile Engine Oils by Thin-Film Oxygen Uptake (TFOUT).
NIST-2567 consist of one ampoule each of the following:
- oxidised/nitrated fuel fraction
- nitro-paraffin model compound
- nitro-aromatic model compound
- metal naphthenate mixture
- distilled water
set (5)
NIST-2556 Used auto catalyst - recycled pelletCertified values
Pb ........................... 6228 mg/kg Pt ............................697.4 mg/kgPd .......................... 326.0 mg/kg Rh.............................51.2 mg/kg
70 g
NIST-2557 Used auto catalyst - recycled monolithCertified values
Pb ........................... 1131 mg/kg Pt .............................1131 mg/kgPd .......................... 233.2 mg/kg Rh...........................135.1 mg/kg
70 g
NIST-RM 8495 Northern softwood bleached kraft pulp - Properties (RM)Properties of fibres and paper sheets
10 sheets
NIST-RM 8496 Eucalyptus hardwood bleached kraft pulp - Properties (RM)Properties of fibres and paper sheets
10 sheets
NIST-154c Titanium dioxide - PurityThis Standard Reference Material® (SRM®) is intended primarily for use in the evaluation of techniques employedin the assay of titanium dioxide in the paint and ceramic industries.
Certified value
Titanium dioxide..........99.951 %
Informational values for impurities
90 g
Filter media
106 Edition 2003/2004 www.lgcpromochem.com
Filter mediaCode Product Unit
BCR-545 Glass fibre filter - ChromiumWelding dust loaded on a filter.
Certified values
Cr (VI) .........................................................40.2 g/kg total leachable Cr ....................................... 39.5 g/kg
filter
NAMI A-2 and NAMI B-2
Intended for use in conjunction with measurements of elements in air filters collected from work-roomair. The levels correspond to current threshold limit values of contaminants in workroom atmospheres.
NAMI A-2 Cellulose ester membrane filter - Metals37 mm filters
Certified values
Al..................................... 255 µg Fe ....................................593 µg Sn .................................. 42.8 µgAs................................... 8.68 µg Mg ..................................84.6 µg Ti.................................... 42.0 µgBe .................................. 1.68 µg Mn ...................................170 µg Tl.................................... 2.96 µgCd .................................. 16.9 µg Mo ..................................42.7 µg V .................................... 17.6 µgCo .................................. 42.3 µg Ni ....................................68.4 µg W ................................... 43.4 µgCr ................................... 54.3 µg Pb...................................42.0 µg Zn.................................... 256 µgCu .................................. 85.2 µg Sb...................................42.6 µg
Indicative values for B, Ba, Zr
filter
NAMI(5)/A-2 Cellulose ester membrane filter - Metals 5 filter
NAMI B-2 Cellulose ester membrane filter - Metals37 mm filters
Certified values
Al..................................... 125 µg Fe ....................................290 µg Sn .................................. 21.0 µgAs................................... 4.25 µg Mg ..................................41.4 µg Ti.................................... 20.5 µgBe .................................. 0.82 µg Mn ..................................83.1 µg Tl.................................... 1.45 µgCd .................................. 8.29 µg Mo ..................................20.9 µg V .................................... 8.60 µgCo .................................. 20.7 µg Ni ....................................33.5 µg W ................................... 21.2 µgCr ................................... 26.6 µg Pb...................................20.5 µg Zn.................................... 125 µgCu .................................. 41.7 µg Sb...................................20.8 µg
Indicative values for B, Ba, Zr
filter
NAMI(5)/B-2 Cellulose ester membrane filter - Metals 5 filter
NIST-2679a Filter media - QuartzIntended to be used to determine the levels of potentially hazardous materials in industrial atmospheres.
I
Certified value
Quartz ................................. 2 µg
Indicative value for clay
II
Certified value
Quartz ............................ 30.8 µg
Indicative value for clay
III
Certified value
Quartz ............................ 80.2 µg
Indicative value for clay
IV
Certified value
Quartz .......................... 202.7 µg
Indicative value for clay
set (4)
Filter media
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Code Product Unit
NIST-2783 Air particulate on filter media - Trace elementsThis Standard Reference Material is an air particulate sample reduced in particle size to simulate PM25 airparticulate matter (particles with an aerodynamic equivalent diameter of 2.5 µm) and deposited on apolycarbonate filter membrane. NIST-2783 included two loaded filters and two blank filters.
Certified values
Al...................................... 23210 Cu.........................................404 Ni ........................................... 68As........................................ 11.8 Fe .....................................26500 Pb ........................................ 317Ba ........................................ 335 K.........................................5280 Sb ....................................... 71.8Ca .................................... 13200 Mg ......................................8620 Ti........................................ 1490Co ......................................... 7.7 Mn ........................................320 V ......................................... 48.5Cr ......................................... 135 Na.......................................2860 Zn....................................... 1790
Indicative values for Ce, Rb, S, Sc, Si, SM, Th, U, W
4 filter
NIST-2678 Blank cellulose acetate membrane filterSet of 10 blank filters
Intended for use in evaluating the performance of air sampling filter methods.
Certified values or limits of detection for each of 30 constituent elements as well as 6 leachable anions andcations.
set (10)
NIST-2681 Blank ashless filter - Trace elementsIntended for use in evaluating the performance of air sampling filter methods.
Certified values or limits of detection for each of 30 constituent elements as well as 6 leachable anions andcations.
set(10)
RTC-CRM002 Activated charcoal filter - Trace elementsCertified values
Ag ............................... 18 mg/kg Cr...........................36339 mg/kg Cu ......................... 96935 mg/kg
Indicative values for 22 further elements
100 g
RTC-CRM004 Diatomaceous earth filter - Trace elementsCertified values
Ba ........................... 1595 mg/kg Cr.................................21 mg/kgCd ................................. 2 mg/kg Pb..........................11871 mg/kg
Indicative values for 20 further elements
100 g
Paint and industrial sludges
108 Edition 2003/2004 www.lgcpromochem.com
Paint and industrial sludgesCode Product Unit
BCR-620, BCR-621 and BCR-623
These paint reference materials are to be used in support of the EU Toy Safety Directive(88/378/EEC). The certified and indicative values are method specific and relate only to the EuropeanStandard EN71-3: 1994.
BCR-620 Mild steel coated with alkyd resin paint - Trace elementsThe material consists of a mild steel panel, size 150 x 100 mm, sprayed on one side with alkyd resin paint.
Certified values
As............................. 23.0 mg/kg Cr.................................64 mg/kg Se ............................. 240 mg/kgBa ............................. 430 mg/kg Pb..............................140 mg/kgCd ............................. 117 mg/kg Sb................................83 mg/kg
panel
BCR-621 (RM) Beechwood coated nitrocellulose paint - Trace elementsThe material consists of a beechwood panel, size 150 x 100 mm, sprayed on one side with nitrocellulose paint.
Indicative values for As, Ba, Cd, Se
panel
BCR-623 Comminuted paint from alkyd resin paint - Trace elementsCertified values
As................................ 23 mg/kg Cr................................9.4 mg/kg Se ............................... 40 mg/kgBa ............................. 105 mg/kg Pb................................19 mg/kgCd ............................ 26.0 mg/kg Sb................................14 mg/kg
2 g
NIST-2579a Set of six lead paint films (NIST-2570 - NIST-2575) - LeadA unit of NIST-2579a consists of a set of six coated polyester sheets, approximately 7.6 cm wide and 10.2 cmlong. Five of the six sheets, NIST-2571 to NIST-2575, are coated with a single, uniform paint layer. The units arecolor coded and each color indicates a different level of lead content. The paint layer and white polyester sheetare approximately 0.04 mm and 0.2 mm thick, respectively. The sixth sheet, NIST-2570, is coated with a lead-free, lacquer layer of the same thickness as the lead paint samples and is included as a blank. All sheets areover-coated with a clear, thin, plastic laminate to protect the surface from abrasion.
set (6)
NIST-2570 - NIST-2576
These items consist of one Mylarä sheet per unit. Each sheet, 7.6 cm x 10.2 cm, is coated with asingle uniform paint layer for use with portable x-ray fluorescence analysers.
NIST-2570 Lead paint film (white/blank) - LeadCertified value
Pb ........................<0.01 mg/cm2
2 sheets
NIST-2571 Lead paint film (yellow) - LeadA unit of NIST-2571 consists of a white polyester sheet, approximately 7.6 cm wide, 10.2 cm long, and 0.2 mmthick, coated with a single, yellow-colored paint layer, approximately 0.04 mm thick. A blank, SRM 2570, is alsoprovided.
Certified value
Pb ..........................3.58 mg/cm2
2 sheets
NIST-2572 Lead paint film (orange) - LeadA unit of NIST-2572 consists of a white polyester sheet, approximately 7.6 cm wide, 10.2 cm long, and 0.2 mmthick, coated with a single, orange-colored paint layer, approximately 0.04 mm thick. A blank, NIST-2570, is alsoprovided.
Certified value
Pb ........................1.527 mg/cm2
2 sheets
NIST-2573 Lead paint film (red) - LeadA unit of NIST-2573 consists of a white polyester sheet, approximately 7.6 cm wide, 10.2 cm long, and 0.2 mmthick, coated with a single, red-colored paint layer, approximately 0.04 mm thick. A blank, NIST-2570, is alsoprovided.
Certified value
Pb ........................1.040 mg/cm2
2 sheets
NIST-2574 Lead paint film (gold) - LeadA unit of NIST-2574 consists of a white polyester sheet, approximately 7.6 cm wide, 10.2 cm long, and 0.2 mmthick, coated with a single, gold-colored paint layer, approximately 0.04 mm thick. A blank, NIST-2570, is alsoprovided.
Certified value
Pb ........................0.714 mg/cm2
2 sheets
Paint and industrial sludges
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Code Product Unit
NIST-2575 Lead paint film (green) - LeadA unit of NIST-2575 consists of a white polyester sheet, approximately 7.6 cm wide, 10.2 cm long, and 0.2 mmthick, coated with a single, green-colored paint layer, approximately 0.04 mm thick. A blank, NIST-2570, is alsoprovided.
Certified value
Pb ........................0.307 mg/cm2
2 sheets
NIST-2576 Lead paint film (blue) - LeadA unit of NIST-2576 consists of a white polyester sheet, approximately 7.6 cm wide, 10.2 cm long, and 0.2 mmthick, coated with a single, blue-colored paint layer, approximately 0.04 mm thick. A blank, NIST-2570, is alsoprovided.
Certified value
Pb ..........................5.59 mg/cm2
2 sheets
NIST-2589 Powdered paint - LeadCertified value
Pb ...................................9.99 %
35 g
NIST-2580 Powdered paint - LeadCertified value
Pb ...................................4.34 %
30 g
NIST-2581 Powdered paint - LeadCertified value
Pb .................................0.449 %
35 g
NIST-2582 Powdered paint - LeadCertified value
Pb ............................. 209 mg/kg
20 g
NIST-RM 8680 Paint on fiberboard - Lead10.2 x 15.2 x 1.3 cm sheet
Indicative value for Pb
1 sheet
RTC-CRM017 Powdered paint - LeadCertified value
Pb .....................................7.4 %
20 g
RTC-CRM013 Paint chips/waste - Trace elementsCertified values
Cd ............................... 38 mg/kg Cr...............................618 mg/kg Pb ............................. 643 mg/kg
Indicative values for a further 21 elements
50 g
RTC-CRM006 Paint sludge - Trace elementsCertified values
Al................................. 73 mg/kg Cr.................................11 mg/kg Na ............................... 91 mg/kgBa ........................... 9970 mg/kg Fe ................................64 mg/kg Pb ............................. 753 mg/kgCa ............................. 111 mg/kg K..............................8710 mg/kg Zn........................ 737431 mg/kgCd ............................... 32 mg/kg Mg ...............................47 mg/kg
Indicative values for B, Cu, Mn, Ni, Se, Sn, Sr, Ti, Tl
50 g
NIST-2586 Soil containing lead from paint - Trace elementsSoil collected from urban areas where the principal source of lead is believed to be from old house lead-basedpaint.
Certified values
As............................... 8.7 mg/kg Cr...............................301 mg/kgCd ............................ 2.71 mg/kg Pb..............................432 mg/kg
Indicative values for a wide range of additional elements
55 g
NIST-2587 Soil containing lead from paint - Trace elementsSoil collected from a suburban garden known to have been contaminated by lead-based house paint.
Certified values
As............................. 13.7 mg/kg Cr.................................92 mg/kgCd ............................ 1.92 mg/kg Pb............................3242 mg/kg
Indicative values for a wide range of additional elements
55 g
Asbestos
110 Edition 2003/2004 www.lgcpromochem.com
Code Product Unit
RTC-CRM009 Plating sludge no. 1 - Trace elementsCertified values
Ag ................................. 9 mg/kg Cu........................121415 mg/kgCr ................................ 50 mg/kg Ni ...............................343 mg/kg
Indicative values for a further 22 elements
100 g
RTC-CRM010 Plating sludge no. 2 - Trace elementsCertified values
Ag ............................... 56 mg/kg Cr.................................79 mg/kg Mn............................... 17 mg/kgAl............................... 692 mg/kg Cu..........................63169 mg/kg Ni .............................. 194 mg/kgBa ............................. 175 mg/kg Fe ...........................2,699 mg/kg Zn.............................. 183 mg/kgCa ............................. 563 mg/kg Pb........................119344 mg/kg
Indicative values for Hg, Mg, Mo, Na
100 g
RTC-CRM011 Plating sludge no. 3 - Trace elementsCertified values
Cr .......................... 59225 mg/kg Ni ...........................41975 mg/kgCu ............................. 108 mg/kg Pb..............................269 mg/kg
Indicative values for a further 21 elements
100 g
RTC-CRM101 API separator sludge - PAHsCertified values
Fluorene...................... 55 mg/kg Napthalene..................97 mg/kg Pyrene......................... 17 mg/kgMethylnapthalene...... 185 mg/kg Phenanthrene............173 mg/kg
100 g
AsbestosCode Product Unit
NIST-1866a Common commercial asbestosStandard Reference Material® (SRM®) 1866a is a set of three common bulk mine-grade asbestos materials andone synthetic glass fiber material. The three asbestos types are chrysotile, grunerite (Amosite), and riebeckite(crocidolite). The optical properties of each of these materials have been characterized by polarized lightmicroscopy.
set (4)
NIST-1876b Chrysotile asbestos for TEMThis Standard Reference Material® (SRM®) is intended primarily for use in evalutating the techniques used tocount and identify chrysotile asbestos fibers in filter samples by transmission electron microscopy (TEM). NIST-1876b consists of ten 3 mm x 3 mm sections of 0.45 µm mixed-cellulose-ester (MCE) filters containing chrysotilefibers deposted by an aerosol generator.
set
NIST-RM 8411 Mixed asbestos research filterResearch Material (RM) 8411 consists of a section approximately one centimeter square of collapsed mixedcellulose ester filter with a high concentration of chrysotile asbestos and a medium concentration of grunerite(Amosite asbestos). This RM is intended for use in deviating and refining sample preparatation and analyticalprocedures for the determination of the asbestos concentration in ambient air samples by phase contrast lightmicroscopy, scanning electron microscopy, and transmission electron microscopy.
Asbestos concentration in fibers per 0.01 mm2
Section chrysotile grunerite
1................................ 97,24........................... 55.192................................ 86.73........................... 42.053.............................. 173.46........................... 57.824.............................. 115.64........................... 44.685.............................. 159.26........................... 50.736.............................. 183.97........................... 52.567.............................. 157.69........................... 49.938.............................. 162.94........................... 18.409.............................. 141.92........................... 21.0210.............................. 78.84........................... 44.6811............................ 128.78........................... 18.4012............................ 134.03........................... 36.7913............................ 139.29........................... 44.6814.............................. 99.87........................... 44.6815............................ 177.40........................... 63.0716............................ 141.92........................... 39.4217............................ 171.62........................... 49.93
1 cm2
Ash and particulate
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Ash and particulateCode Product Unit
LGC6180 (RM) Pulverised fuel ash - Extractable and total metalsCollected from a disposal site near Camarthan Bay in South Wales. Pulverised fuel ash is a waste product ofcoal-fired power stations.The extractable metal content refers to metals soluble in Aqua Regia using methods based on ISO11466 (1995).
Extractable metal content
Assessed values
Al........................... 25700 mg/kg Cr..............................43.8 mg/kg Na ........................... 1230 mg/kgAs............................. 91.7 mg/kg Cu.............................67.9 mg/kg Ni ............................. 48.4 mg/kgBa ............................. 676 mg/kg K..............................6170 mg/kg Pb ............................ 48.6 mg/kgCa ........................... 6415 mg/kg Mg ...........................3660 mg/kg V ............................... 105 mg/kgCo ............................ 18.5 mg/kg Mn .............................259 mg/kg Zn.............................. 115 mg/kg
Indicative values for B, Be, Fe, Hg, Li, Sb, Se, Ti
Total metal content
Indicative values for Al, As, Ba, Be, Ca, Co, Cr, Cu, Fe, K, Li, Mg, Mn, Mo, Na, Ni, Pb, Sb, Se, Sn, Ti, V, Zn
5 x 50 g
BCR-038 Fly ash from pulverised coal - Trace elementsCertified values
As............................. 48.0 mg/kg Cu..............................176 mg/kg Na ........................... 3740 mg/kgCd .............................. 4.6 mg/kg F ................................538 mg/kg Pb ............................. 262 mg/kgCl .............................. 323 mg/kg Fe ..........................33800 mg/kg Zn.............................. 581 mg/kgCo ............................ 53.8 mg/kg Hg.............................2.10 mg/kgCr .............................. 192 mg/kg Mn .............................479 mg/kg
Indicative values for Ni, Th, V
5 g
BCR-128 Fly ash on artificial filters - Trace elements(1 charged filter + 1 blank)Intended for the verification of the calibration in XRF- and PIXE-analysis of (air borne) dust. A filter will normallylast for at least ten measurements in a vacuum or twenty-five in air. The filter consists of a methyl cellulose filtermounted on polythene backed paper in a petrislide. Each foil contains a certified amount of BCR-038 (see above)
set
BCR-490 Fly ash - PCDDs and PCDFsCompound Certified value Uncertainty
µg/kg µg/kg
2,3,7,8-TCDD................................................... 0.169........................ 0.0121,2,3,7,8-PeCDD ............................................... 0.67.......................... 0.041,2,3,4,7,8-HxCDD ............................................ 0.95.......................... 0.111,2,3,6,7,8-HxCDD .............................................. 4.8............................ 0.41,2,3,7,8,9-HxCDD ............................................ 2.84.......................... 0.172,3,7,8-TCDF..................................................... 0.90.......................... 0.051,2,3,7,8-PeCDF................................................ 1.71.......................... 0.122,3,4,7,8-PeCDF.................................................. 1.8.......................... 0.111,2,3,4,7,8-HxCDF............................................. 2.37.......................... 0.121,2,3,6,7,8-HxCDF............................................. 2.64.......................... 0.141,2,3,7,8,9-HxCDF............................................. 0.34.......................... 0.052,3,4,6,7,8-HxCDF............................................. 2.47.......................... 0.17
30 g
BCR-615 Fly ash - PCDDs, PCDFsCertified values
2,3,7,8-T4CDD (D48) .................................... 27 pg/g 2,3,4,7,8-P5CDF (F114) .............................. 125 pg/g1,2,3,7,8-P5CDD (D54) ................................. 92 pg/g 1,2,3,4,7,8-H6CDF (F118) ........................... 203 pg/g1,2,3,4,7,8-H6CDD (D66).............................. 74 pg/g 1,2,3,6,7,8-H6CDF (F121) ........................... 204 pg/g1,2,3,6,7,8-H6CDD (D67)............................ 103 pg/g 1,2,3,7,8,9-H6CDF (F124) .......................... 13.3 pg/g1,2,3,7,8,9-H6CDD (D70)............................ 108 pg/g 2,3,4,6,7,8-H6CDF (F130) ........................... 130 pg/g1,2,3,4,6,7,8-H7CDD (D73)................0.87 x 103 pg/g 1,2,3,4,6,7,8-H7CDF (F131) .............. 0.75 x 103 pg/gO8CDD (D75).....................................1.75 x 103 pg/g 1,2,3,4,7,8,9-H7CDF (F134) .......................... 61 pg/g2,3,7,8-T4CDF (F83) ..................................... 86 pg/g O8CDF (F135) .................................. 0.29 x 103 pg/g1,2,3,7,8-P5CDF (F94) ................................ 176 pg/g
50 g
NIST-1633b Coal fly ash - Trace and constituent elementsCertified values
Al.....................................15.5 % Hg...........................0.141 mg/kg S .................................0.2075 %As........................... 136.2 mg/kg K..................................... 1.95 % Se .......................... 10.26 mg/kgBa ............................. 709 mg/kg Mg ................................ 0.482 % Si...................................23.02 %Ca ...................................1.51 % Mn ..........................131.8 mg/kg Sr ............................ 1041 mg/kgCd .......................... 0.784 mg/kg Na................................. 0.201 % Th............................. 25.7 mg/kgCr ........................... 198.2 mg/kg Nd...........................120.6 mg/kg Ti.....................................0.75 %Cu .......................... 112.8 mg/kg Ni ............................102.6 mg/kg U .............................. 8.79 mg/kgFe....................................7.78 % Pb.............................68.2 mg/kg V ............................ 295.7 mg/kg
Indicative values for Br, Ce, Co, Cs, Eu, Gd, Hf, Ho, La, Lu, Mo, P, Rb, Sb, Sc, Sm, Ta, Tb, Tl, Tm, W, Yb, Zn
75 g
Ash and particulate
112 Edition 2003/2004 www.lgcpromochem.com
Code Product Unit
NIST-2689 Coal fly ash - Constituent elementsSet of 3 x 10 g
Certified values
Al...................................12.94 % K..................................... 2.20 % P .....................................0.10 %Ca ...................................2.18 % Mg .................................. 0.61 % Si...................................24.06 %Fe(total)...........................9.32 % Na................................... 0.25 % Ti.....................................0.75 %
Indicative values for As, Ba, Be, Cd, Co, Cr, Cs, Eu, Hf, Hg, Mn, Ni, Pb, Sb, Sc, Se, Sr, Th, Zn
set (3)
NIST-2690 Coal fly ash - Constituent elementsSet of 3 x 10 g
Certified values
Al...................................12.35 % Mg .................................. 1.53 % Si...................................25.85 %Ca ...................................5.71 % Na................................... 0.24 % Ti.....................................0.52 %Fe(total)...........................3.57 % P..................................... 0.52 %K .....................................1.04 % S..................................... 0.15 %
Indicative values for As, Ba, Be, Cd, Co, Cr, Cs, Eu, Hf, Hg, Mn, Ni, Pb, Sb, Sc, Se, Sr, Th, Zn
set (3)
NIST-2691 Coal fly ash - Constituent elementsSet of 3 x 10 g
Certified values
Al.....................................9.81 % Mg .................................. 3.12 % Si...................................16.83 %Ca .................................18.45 % Na................................... 1.09 % Ti.....................................0.90 %Fe(total)...........................4.42 % P..................................... 0.51 %K .....................................0.34 % S..................................... 0.83 %
Indicative values for As, Ba, Be, Cd, Co, Cr, Cs, Eu, Hf, Hg, Mn, Ni, Pb, Sb, Sc, Se, Sr, Th, Zn
set (3)
IC-CTA-FFA-1 Fine fly ash - Constituent elementsCollected from the 3rd zone electrofilters at Kozienice power station in Poland.
Certified values for elements
Al............................. 14.87 wt. % Hf..............................6.09 mg/kg Si.............................. 22.48 wt %As............................. 53.6 mg/kg La .............................60.7 mg/kg Sm ........................... 10.9 mg/kgBa ............................. 835 mg/kg Li................................128 mg/kg Sc............................. 24.2 mg/kgCe ............................. 120 mg/kg Lu ...........................0.658 mg/kg Sr .............................. 250 mg/kgCr .............................. 156 mg/kg Mn ...........................1066 mg/kg Ta............................. 2.11 mg/kgCu ............................. 158 mg/kg Na.............................2.19 mg/kg Tb............................. 1.38 mg/kgDy............................. 9.09 mg/kg Nd.............................56.8 mg/kg Th............................. 29.4 mg/kgEr ............................. 4.52 mg/kg Ni ..............................99.0 mg/kg Tm.......................... 0.705 mg/kgEu ............................ 2.39 mg/kg P................................725 mg/kg W ............................. 10.5 mg/kgF................................ 198 mg/kg Pb..............................369 mg/kg Y............................... 45.0 mg/kgFe.............................. 4.89 wt. % Rb..............................185 mg/kg Yb............................. 4.24 mg/kgGd ............................ 10.0 mg/kg Sb.............................17.6 mg/kg Zn.............................. 569 mg/kg
Informational values for Be, Ca, Cd, Ga, In, K, Mg, Mo, Se
50 g
NRMGBW08401 Coal fly ash - MetalsCertified values
As................................ 11.4 µg/g Cr....................................60 µg/g Pb ............................... 33.8 µg/gBe ............................... 10.7 µg/g Cu...................................53 µg/g Se ............................... 1.13 µg/gCd ............................... 0.16 µg/g Fe ................................... 7.65 % V .................................... 95 µg/gCo ............................... 33.2 µg/g Mn ..............................1178 µg/g Zn................................... 61 µg/g
Indicative values for Ba, Hg
30 g
NRMGBW08403 Coal fly ash - PAHsCertified values
Anthracene .................................................. 2.0 µg/g Phenanthrene............................................... 7.1 µg/gBenzo(a)pyrene ........................................... 1.3 µg/g Pyrene............................................................. 7 µg/gFluoranthene................................................ 7.4 µg/g
Indicative values for Benzo(a)anthracene, Benzo(b)fluoranthene, Benzo(ghi)perylene, Benzo(k)fluoranthene,Chrysene + Triphenylene, Dibenzo(a,h)anthracene
10 g
NIST-1975 Diesel particulate extract - PAHsThis Standard Reference Material® (SRM®) is intended for use in evaluating analytical methods for thedetermination of selected polycyclic aromatic hydrocarbons (PAHs) in diesel particulate extracts and similarmatrices. In addition to certified and reference values for selected polycyclic aromatic hydrocarbons, referencevalues are provided for the concentrations of selected nitro-substituted PAHs, extract residue mass, andmutagenic activity.
Certified Concentrations for Selected PAHs
Mass Fraction Mass Fractionmg/kg mg/kg
Phenanthrene ......................................... 8.00 ± 0.20 Triphenylen ............................................. 2.38 ± 0.10Fluoranthene............................................. 13.5 ± 0.6 Benzo(b)fluoranthene.............................. 3.20 ± 0.10Benzo(a)anthracene ........................... 0.092 ± 0.015 Benzo(k)fluoranthene.......................... 0.174 ± 0.050Chrysene................................................. 1.95 ± 0.07 Benzo(e)pyrene................................... 0.268 ± 0.023
Reference Concentrations for PAHs, Nitro-substituted PAHs, Extract Residue Mass, Mutagenicity (revertants/ µgof organic extract).
4 x 1.2 mL
Ash and particulate
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Code Product Unit
NIST-2975 Diesel particulate matter - PAHsThis Standard Reference Material® (SRM®) is intended for use in evaluating analytical methods for thedetermination of selected polycyclic aromatic hydrocarbons (PAHs) in diesel particulate extracts and similarmatrices. In addition to certified and reference values for selected polycyclic aromatic hydrocarbons, referencevalues or informational values are provided for total extractable mass, particle-size distribution, specific surfacearea, and the concentration of 1-nitropyrene.
Certified Concentrations for Selected PAHs
Mass Fraction Mass Fractionmg/kg mg/kg
Phenanthrene ........................................... 17.0 ± 2.8 Benzo(j)fluoranthene............................... 0.82 ± 0.11Fluoranthene............................................. 26.6 ± 5.1 Benzo(k)fluoranthene.......................... 0.678 ± 0.076Pyrene..................................................... 0.90 ± 0.24 Benzo(e)pyrene....................................... 1.11 ± 0.10Benzo(a)anthracene ........................... 0.317 ± 0.066 Benzo(a)pyrene................................. 0.0522 ± 0.043Chrysene................................................. 4.56 ± 0.16 Benzo(ghi)perylene ............................. 0.498 ± 0.044Triphenylen ............................................. 5.22 ± 0.20
Reference Concentrations for PAHs, Total Extractable Mass and Particle-Size Characteristics.
1 g
NIST-1648 Urban particulate matter- Constituent elementsCertified values
Al.....................................3.42 % Fe(total) .......................... 3.91 % Se ............................... 27 mg/kgAs.............................. 115 mg/kg K..................................... 1.05 % U ................................ 5.5 mg/kgCd ............................... 75 mg/kg Na................................. 0.425 % V ............................... 140 mg/kgCr .............................. 403 mg/kg Ni .................................82 mg/kg Zn..................................0.476 %Cu ............................. 609 mg/kg Pb................................. 0.655 %
Indicative values for Ba, Br, Ce, Cl, Co, Cs, Hf, I, In, La, Mn, Th, Sb
2 g
Dust and Fumes
114 Edition 2003/2004 www.lgcpromochem.com
Dust and FumesCode Product Unit
BCR-605 Urban dust - TrimethylleadCertified value
Trimethyllead .............. 7.9 µg/kg
15 g
NIST-1649a Urban dust - Organic contaminantsStandard Reference Material® (SRM®) 1649a is an atmospheric particulate matter collected in an urban area andis intended for use in evaluating analytical methods for the determination of selected polycyclic aromatichydrocarbons (PAHs), polychlorinated biphenyls (PCB) congeners, and chlorinated pesticides in atmosphericparticulate material and similar matrices.
Certified concentrations for selected PAHs
Mass fraction ( mg/kg) Mass fraction ( mg/kg)
Phenanthrene ......................................... 4.14 ± 0.37 Benzo(a)pyrene................................... 2.509 ± 0.087Anthracene ......................................... 0.432 ± 0.082 Perylene .............................................. 0.646 ± 0.075Fluoranthene........................................... 6.45 ± 0.18 Anthanthrene....................................... 0.450 ± 0.067Pyrene..................................................... 5.29 ± 0.25 Benzo(ghi)perylene ................................. 4.01 ± 0.91Benzo(a)anthracene ............................. 2.21 ± 0.073 Indeno(1,2,3-cd)pyrene........................... 3.18 ± 0.72Chrysene............................................. 3.049 ± 0.060 Dibenz(a,j)anthracene......................... 0.310 ± 0.034Triphenylene ....................................... 1.357 ± 0.054 Dibenzo(a,c)anthracene...................... 0.200 ± 0.025Benzo(b)fluoranthene ............................. 6.45 ± 0.64 Dibenzo(a,h)anthracene...................... 0.288 ± 0.023Benzo(k)fluoranthene ......................... 1.913 ± 0.031 Pentaphene......................................... 0.151 ± 0.035Benzo(a)fluoranthene ......................... 0.409 ± 0.035 Benzo(b)chrysene ............................... 0.315 ± 0.013Benzo(e)pyrene ...................................... 3.09 ± 0.19 Picene ................................................. 0.426 ± 0.022
Certified concentrations for selected PCB congeners
Mass fraction ( µg/kg)
PCB 8................2,4’-Dichlorobiphenyl................................................. 12.28 ± 0.29PCB 18..............2,2',5-Trichlorobiphenyl ............................................. 20.44 ± 0.84PCB 28..............2,4,4'-Trichlorobiphenyl ................................................. 18.5 ± 1.2PCB 31..............2,4’,5-Trichlorobiphenyl ................................................. 17.3 ± 1.4PCB 44..............2,2',3,5'-Tetrachlorobiphenyl ......................................... 15.4 ± 1.6PCB 49..............2,2’,4,5’-Tetrachlorobiphenyl ......................................... 12.2 ± 1.5PCB 52..............2,2',5,5'-Tetrachlorobiphenyl ..................................... 24.65 ± 0.97PCB 66..............2,3',4,4'-Tetrachlorobiphenyl +
95..............2,2’,3,5’,6-Pentachlorobiphenyl ......................................... 65 ± 12PCB 87..............2,2’,3,4,5`-Pentachlorobiphenyl................................. 10.65 ± 0.62PCB 95..............2,2’,3,5’,6-Pentachlorobiphenyl ..................................... 51.6 ± 4.2PCB 99..............2,2’,4,4’,5-Pentachlorobiphenyl ................................... 9.58 ± 0.69PCB 101............2,2',4,5,5'-Pentachlorobiphenyl ..................................... 52.9 ± 1.0PCB 105............2,3,3',4,4'-Pentachlorobiphenyl ................................... 8.63 ± 0.80PCB 110............2,3,3’,4’,6-Pentachlororbiphyl........................................ 26.6 ± 1.6PCB 118............2,3',4,4',5-Pentachlorobiphenyl ..................................... 25.7 ± 1.5PCB 128............2,2',3,3',4,4'-Hexachlorobiphenyl................................. 6.35 ± 0.69PCB 138............2,2',3,4,4',5'-Hexachlorobiphenyl +
163............2,3,3',4',5,6-Hexachlorobiphenyl +164............2,3,3',4',5',6-Hexachlorobiphenyl.................................. 69.7 ± .7.5
PCB 149............2,2',3,4',5',6-Hexachlorobiphenyl................................... 75.7 ± 1.3PCB 151............2,2',3,5,5',6-Hexachlorobiphenyl ................................... 34.3 ± 3.9PCB 153............2,2',4,4',5,5'-Hexachlorobiphenyl................................... 82.5 ± 8.0PCB 156............2,3,3',4,4',5-Hexachlorobiphenyl ............................... 16.25 ± 0.77PCB 170............2,2',3,3',4,4',5-Heptachlorobiphenyl +
190............(2,3,3’,4,4’,5,5’-Heptachlorobiphenyl............................. 30.8 ± 2.2PCB 180............2,2',3,4,4',5,5'-Heptachlorobiphenyl .............................. 78.7 ± 8.2PCB 183............2,2',3,4,4',5',6-Heptachlorobiphenyl .......................... 20.34 ± 0.95PCB 187............2,2',3,4',5,5',6-Heptachlorobiphenyl +
159............2,3,3',4,5,5'-Hexachlorobiphenyl +182............2,2’,3,’,4,4’,5,6’-Heptachlorobiphenyl ............................ 40.1 ± 2.5
PCB 194............2,2’,3,3’,4,4’,5,5’-Octachlorobiphenyl ............................ 28.9 ± 3.6PCB 195............2,2’,3,3’,4,4’,5,6-Octachlorobiphenyl ........................... 9.63 ± 0.37PCB 206............2,2’,3,3’,4,4’,5,5’,6-Nonachlorobiphenyl ........................ 20.6 ± 4.6PCB 209............Decachlorobiphenyl..................................................... 8.04 ± 0.77
Certified concentrations for selected chlorinated pesticides
Chlorinated pesticides Mass fraction in µg/kg Chlorinated pesticides Mass fraction in µg/kg
Hexachlorobenzene.................................. 16.3 ± 1.8 2,4’-DDE ................................................. 5.79 ± 0.85trans-Chlordane (gamma-Chlordane)....... 40.3 ± 2.8 4,4’-DDE ................................................... 40.4 ± 1.7cis-Chlordane (alpha-Chlordane).......... 34.88 ± 0.42 4,4’-DDD ............................................... 34.01 ± 0.48trans-Nonachlor ........................................ 27.6 ± 1.6 4,4’-DDT...................................................... 212 ± 15
Reference values for PAHs, chlorinated pesticides, mutagenic anions activity, particle-size characteristics, totalorganic carbon and percent extractable mass, carbon composition.
2.5 g
BCR-723 Road dust - Palladium, platinum and rhodiumCertified values
Pd ............................... 6.0 µg/kg Pt ...............................81.3 µg/kg Rh ............................. 12.8 µg/kg
25 g
Dust and Fumes
www.lgcpromochem.com Edition 2003/2004 115
Code Product Unit
BCR-553-4 Formaldehyde-2,4-dinitrophenyl-hydrazone on filterSet of 2 x BCR 553 & 1 x BCR 554 (blank)
BCR-553 (spiked filter)
Certified value (per filter)
Formaldehyde-2,4-dinitrophenylhydrazone....................... 4.96 µg
BCR-554 (blank filter)
Certified value (per filter)
Formaldehyde-2,4-dinitrophenylhydrazone....................... < 0.1µg
set
Council directive 80/1107/EEC and national legislation prescribes that the exposure of each individualworker to certain potentially harmful vapours has to be monitored periodically. This requires “personalmonitoring” where a tube, containing a suitable sorbing agent, is attached to the worker’s clothes.After a set sampling period any harmful vapours absorbed onto the material in the tube are desorbed,either by heating or solvent extraction, and determined using gas chromatography.
BCR-112 Tenax charged tube - Aromatic hydrocarbonsCertified values (per tube)
Benzene....................... 1.053 µg Toluene ........................1.125 µg m-Xylene...................... 1.043 µg
tube
BCR-562 Charcoal charged tube - Aromatic hydrocarbonsSet of 20 tubes (6 charged, 14 blanks)
Certified values (per tube)
Benzene......................... 15.0 µg m-Xylene ........................96.4 µgToluene........................ 147.3 µg o-Xylene .........................93.0 µg
set
BCR-555 Tenax charged tube - Chlorinated hydrocarbonsStainless steel tube of 9.0 cm length and 0.25 inches outer diameter containing a single section of 250 mgTENAX GR, charged with 4 chlorinated hydrocarbons and toluene at the levels shown above.
Certified values
Dichloromethane............. 320 ng Trichloroethylene.............390 ng Toluene............................. 57 ng1,1,1-Trichloroethane...... 370 ng Perchloroethylene ...........327 ng
tube
RTC-CRM014 Baghouse dust - Trace metalsCertified values
Cd ............................. 510 mg/kg Cr............................2,228 mg/kg Pb .......................... 1,914 mg/kg
Indicative values for a further 24 elements
50 g
NIST-1878a Alpha quartzOne form of respirable silica
Certified value
Crystalline α–quartz................................... 100.00 %
5 g
NIST-1879a CristabaliteOne form of respirable silica
Certified value
Crystalline cristabolite.................................... 95.6 %
5 g
NIST-2583 Indoor dust - Trace elementsCertified values
As............................... 7.0 mg/kg Cr.................................80 mg/kg Pb ............................ 85.9 mg/kgCd .............................. 7.3 mg/kg Hg.............................1.56 mg/kg
8 g
NIST-2584 Indoor dust - Trace elementsCollected from vacuum cleaner bags used in the cleaning of interior dwelling places
Certified values
As............................. 17.4 mg/kg Cr............................135.0 mg/kg Pb ........................... 9761 mg/kgCd ............................ 10.0 mg/kg Hg.............................5.20 mg/kg
Indicative values for a wide range of additional elements
8 g
Aldehydes/Ketones-DNPH standards
116 Edition 2003/2004 www.lgcpromochem.com
Aldehydes/Ketones-DNPH standardsCode Product Unit
CERERA-012 Acetaldehyde-DNPH 10 mg
BCR-547 Acetaldehyde-2,4-dinitrophenylhydrazoneCertified purity.................98.3 %
10 mg
CERERA-024S Acetaldehyde-DNPH 500 µg/mL* in Acetonitrile 1.2 mL
CERERA-011 Acetone-DNPH 10 mg
BCR-549 Acetone-2,4-dinitrophenylhydrazoneCertified purity..............> 99.6 %
10 mg
CERERA-025S Acetone-DNPH 500 µg/mL* in Acetonitrile 1.2 mL
CERERA-021 Acetophenone-DNPH 10 mg
CERERA-026S Acetophenone-DNPH 100 µg/mL* in Acetonitrile 1.2 mL
CERERA-014 Acrolein-DNPH 10 mg
BCR-548 Acrolein-2,4-dinitrophenylhydrazoneCertified purity..............> 97.9 %
10 mg
CERERA-027S Acrolein-DNPH 500 µg/mL* in Acetonitrile 1.2 mL
CERERB-017 Benzaldehyde-DNPH 10 mg
CERERB-026S Benzaldehyde-DNPH 100 µg/mL* in Acetonitrile 1.2 mL
CERERB-023 1,4-Benzoquinone-DNPH (mono) 10 mg
CERERB-016 2-Butanone (MEK)-DNPH 10 mg
CERERB-028S 2-Butanone (MEK)-DNPH 100 µg/mL* in Methanol 1.2 mL
CERERB-018 n-Butyraldehyde-DNPH 10 mg
CERERB-029S n-Butyraldehyde-DNPH 500 µg/mL* in Acetonitrile 1.2 mL
CERERC-006 Crotonaldehyde-DNPH 10 mg
CERERC-011S Crotonaldehyde-DNPH 100 µg/mL* in Acetontrile 1.2 mL
CERERC-016 Cyclohexanone-DNPH 10 mg
CERERC-015S Cyclohexanone-DNPH 500 µg/mL* in Acetonitrile 1.2 mL
CERERD-030 2,5-Dimethylbenzaldehyde-DNPH 10 mg
CERERD-035S 2,5-Dimethylbenzaldehyde-DNPH 500 µg/mL* in Acetonitrile 1.2 mL
CERERF-003 Formaldehyde-DNPH 10 mg
BCR-546 Formaldehyde-2,4-dinitrophenylhydrazoneCertified purity................ > 0.993
10 mg
CERERF-004S Formaldehyde-DNPH 100 µg/mL* in Acetonitrile 1.2 mL
CERERF-005S Formaldehyde-DNPH 500 µg/mL* in Acetonitrile 1.2 mL
CERERG-002 Glutaraldehyde-DNPH 10 mg
BCR-550 Glutaraldehyde-2,4-dinitrophenylhydrazoneCertified purity..............> 98.1 %
10 mg
CERERH-011 Heptaldehyde-DNPH 10 mg
CERERH-012S Heptaldehyde-DNPH 500 µg/mL* in Acetonitrile 1.2 mL
CERERH-003 Hexaldehyde-DNPH 10 mg
CERERH-005S Hexaldehyde-DNPH 500 µg/mL* in Acetonitrile 1.2 mL
Aldehydes/Ketones-DNPH standards
www.lgcpromochem.com Edition 2003/2004 117
Code Product Unit
CERERI-003 Isobutyraldehyde-DNPH 10 mg
CERERI-005 Isophorone-DNPH 10 mg
CERERI-004 Isovaleraldehyde-DNPH 10 mg
CERERI-009S Isovaleraldehyde-DNPH 500 µg/mL* in Acetonitrile 1.2 mL
CERERM-002 Methacrolein-DNPH 10 mg
CERERM-022S Methacrolein-DNPH 100 µg/mL* in Acetonitrile 1.2 mL
CERERM-020 Methyl isobutyl ketone-DNPH 10 mg
CERERM-023S Methyl isobutyl ketone-DNPH 500 µg/mL* in Acetonitrile 1.2 mL
CERERM-024 Methyl isopropyl ketone-DNPH 10 mg
CERERP-005 Propionaldehyde-DNPH 10 mg
CERERP-030S Propionaldehyde-DNPH 500 µg/mL* in Acetonitrile 1.2 mL
CERERT-007 m-Tolualdehyde-DNPH 10 mg
CERERT-027S m-Tolualdehyde-DNPH 100 µg/mL* in Acetonitrile 1.2 mL
CERERT-012 o-Tolualdehyde-DNPH 10 mg
CERERT-011 p-Tolualdehyde-DNPH 10 mg
CERERV-001 Valeraldehyde-DNPH 10 mg
CERERV-002S Valeraldehyde-DNPH 500 µg/mL in Acetonitrile 1.2 mL
*as aldehyde or ketone
BCR-551-2 2,4-Dinitrophenylhydrazones in AcetonitrileEach set consists of 4 samples of BCR-551 and 1 sample of BCR-552
BCR 551 2,4-Dinitrophenylhydrazones in Acetonitrile
Compound Certified value Uncertainty(µg/mL) (µg/mL)
Formaldehyde-DNPH ........................................ 2.94.......................... 0.05Acetaldehyde-DNPH.......................................... 4.89.......................... 0.07Acrolein-DNPH ................................................ 0.483........................ 0.011Acetone-DNPH .................................................. 4.69.......................... 0.07
BCR-552 2,4-Dinitrophenylhydrazones in a solution of 2,4-Dinitrophenylhydrazine (blank)
Compound Certified value(µg/mL)
Formaldehyde-DNPH ...................................... <0.08Acetaldehyde-DNPH........................................ <0.05Acrolein-DNPH ................................................ <0.04Acetone-DNPH ................................................ <0.05
set
CERERA-020 Aldehyde/Ketone-DNPH Standard Solution(15 compounds)
15 µg/mL (as Aldehyde/Ketone) of each analyte in Acetonitrile
Acetaldehyde-DNPH Hexaldehyde-DNPHAcetone-DNPH Isovaleraldehyde-DNPHAcrolein-DNPH Propionaldehyde-DNPHBenzaldehyde-DNPH o- Tolualdehyde-DNPHn-Butyraldehyde-DNPH p-Tolualdehyde-DNPHCrotonaldehyde-DNPH m-Tolualdehyde-DNPH2,5-Dimethylbenzaldehyde-DNPH Valeraldehyde-DNPHFormaldehyde-DNPH
1.2 mL
CERERA-028 Aldehyde/Ketone-DNPH Standard Solution(13 compounds)
15 µg/mL (as Aldehyde/Ketone) of each analyte in Acetonitrile
Acetaldehyde-DNPH Formaldehyde-DNPHAcetone-DNPH Hexaldehyde-DNPHAcrolein-DNPH Methacrolein-DNPHBenzaldehyde-DNPH Propionaldehyde-DNPH2-Butanone-DNPH m-Tolualdehyde-DNPHn-Butyraldehyde-DNPH Valeraldehyde-DNPHCrotonaldehyde-DNPH
1.2 mL
Aldehydes/Ketones-DNPH standards
118 Edition 2003/2004 www.lgcpromochem.com
Code Product Unit
CERERA-013K Aldehyde/Ketone-DNPH Working Standard Solution(13 compounds)
3 µg/mL (as Aldehyde/Ketone) of each analyte in Acetonitrile
Acetaldehyde-DNPH Formaldehyde-DNPHAcetone-DNPH Hexaldehyde-DNPHAcrolein-DNPH Methacrolein-DNPHBenzaldehyde-DNPH Propionaldehyde-DNPH2-Butanone-DNPH m-Tolualdehyde-DNPHn-Butyraldehyde-DNPH Valeraldehyde-DNPHCrotonaldehyde-DNPH
5 x 1.2 mL
CERERA-037 Aldehyde/Ketone-DNPH CheckStandard Solution(13 compounds)
1 µg/mL (as Aldehyde/Ketone) of each analyte in Acetonitrile
Acetaldehyde-DNPH Formaldehyde-DNPHAcetone-DNPH Hexaldehyde-DNPHAcrolein-DNPH Methacrolein-DNPHBenzaldehyde-DNPH Propionaldehyde-DNPH2-Butanone-DNPH m-Tolualdehyde-DNPHn-Butyraldehyde-DNPH Valeraldehyde-DNPHCrotonaldehyde-DNPH
5 x 1.2 mL
CERERA-030 Aldehyde/Ketone-DNPH Calibration KIT-15Each kit contains one 3,0 mL ampoule of C1, C2, C3, C4 and C5.
Solvent: Acetonitrile
Concentrations (µg/mL) as Aldehyde or Ketone
Analytes C1 C2 C3 C4 C5
Acetaldehyde-DNPH.................................0.01 .............. 0.02.............. 0.05.............. 0.10...............0.50Acetone-DNPH .........................................0.01 .............. 0.02.............. 0.05.............. 0.10...............0.50Acrolein-DNPH .........................................0.01 .............. 0.02.............. 0.05.............. 0.10...............0.50Benzaldehyde-DNPH................................0.01 .............. 0.02.............. 0.05.............. 0.10...............0.50n-Butyraldehyde-DNPH ............................0.01 .............. 0.02.............. 0.05.............. 0.10...............0.50Crotonaldehyde-DNPH .............................0.01 .............. 0.02.............. 0.05.............. 0.10...............0.502,5-Dimethylbenzaldehyde-DNPH............0.01 .............. 0.02.............. 0.05.............. 0.10...............0.50Formaldehyde-DNPH ...............................0.01 .............. 0.02.............. 0.05.............. 0.10...............0.50Hexaldehyde-DNPH..................................0.01 .............. 0.02.............. 0.05.............. 0.10...............0.50Isovaleraldehyde-DNPH ...........................0.01 .............. 0.02.............. 0.05.............. 0.10...............0.50Propionaldehyde-DNPH ...........................0.01 .............. 0.02.............. 0.05.............. 0.10...............0.50m-Tolualdehyde-DNPH.............................0.01 .............. 0.02.............. 0.05.............. 0.10...............0.50o-Tolualdehyde-DNPH..............................0.01 .............. 0.02.............. 0.05.............. 0.10...............0.50p-Tolualdehyde-DNPH..............................0.01 .............. 0.02.............. 0.05.............. 0.10...............0.50Valeraldehyde-DNPH ...............................0.01 .............. 0.02.............. 0.05.............. 0.10...............0.50
kit
CERERA-029 Aldehyde/Ketone-DNPH Calibration KIT-4Each kit contains one 3.0 mL ampoule of C1, C2, C3, C4 and C5
Solvent: Acetonitrile
Concentrations (µg/mL) as Aldehyde or Ketone
Analytes C1 C2 C3 C4 C5
Acetaldehyde-DNPH.................................0.01 .............. 0.02.............. 0.05.............. 0.10...............0.50Acetone-DNPH .........................................0.01 .............. 0.02.............. 0.05.............. 0.10...............0.50Acrolein-DNPH .........................................0.01 .............. 0.02.............. 0.05.............. 0.10...............0.50Formaldehyde-DNPH ...............................0.01 .............. 0.02.............. 0.05.............. 0.10...............0.50
kit
Elemental analysis
www.lgcpromochem.com Edition 2003/2004 119
Elemental analysisCode Product Unit
LGC4000 - LGC4009
Produced in collaboration with the Micro and Chemical Methods Group of the Analytical Division of theRoyal Society of Chemistry.
LGC4000 Dibutyl sulphideCertified value
S .....................................21. 5%
50 mL
LGC4001 DibenzothiopheneCertified value
S ....................................17.6 %
500 mg
LGC4002 AcetanilideCertified values
C ...................................71.14 % H..................................... 6.73 % N ...................................10.33 %
1 g
NIST-141D Acetanilide - Carbon, hydrogen, nitrogen and oxygenCertified values
C .................................71.089 % N................................. 10.363 %H ...................................6.711 % O................................. 11.837 %
unit
LGC4003 Benzoic acid - OxygenCertified value
O ...................................26.24 %
1 g
LGC4004 4-Chlorobenzoic acid - ChlorineCertified value
Cl ..................................22.72 %
1 g
LGC4005 Cyclohexanone-2,4-dinitrophenylhydrazone - NitrogenCertified value
N ...................................20.11 %
1 g
LGC4006 Triphenylphosphine - PhosphorousCertified value
P ...................................11.73 %
1 g
LGC4007 Arachidic acid - Carbon and hydrogenCertified values
C ...................................76.81 % H................................... 12.96 %
1 g
LGC4008 4-Bromobenzoic acid - BromineCertified value
Br ..................................39.74 %
1 g
LGC4009 2-Iodobenzoic acid - IodineCertified value
I .....................................51.14 %
1 g
NIST-142 Anisic acid - MethoxylCertified value
CH3O-............................20.40 %
2 g
NIST-143D Cystine - Carbon, hydrogen, nitrogen, oxygen and sulphurCertified values
C ...................................29.99 % N................................... 11.66 % S ...................................26.69 %H .....................................5.03 % O................................... 26.63 %
2 g
NIST-148 Nicotinic acid - Carbon, hydrogen and nitrogenCertified values
C ...................................58.54 % H..................................... 4.09 % N ...................................11.38 %
2 g
NIST-2141 Urea - NitrogenCertified value
N .................................46.635 %
2 g
Elemental analysis
120 Edition 2003/2004 www.lgcpromochem.com
Code Product Unit
NIST-2143 p-Fluorobenzoic acid - FluorineCertified value
F....................................13.54 %
2 g
NIST-2144 m-Chlorobenzoic acid - ChlorineCertified value
Cl ..................................22.62 %
2 g
NIST-1216 Carbon modified silicon - CarbonCertified values
Level I
C .......................................0.7 %
Level II
C .....................................9.06 %
Level III
C ...................................17.04 %
Set
Stochiometry
www.lgcpromochem.com Edition 2003/2004 121
StochiometryCode Product Unit
NIST-17e Sucrose - Optical rotationIntended for use as a saccharimetry standard in calibrating polarimetric systems.
Certified purity.............99.950 %
Reference values are given for optical rotation at 3 wavelengths
60 g
NIST-40H Sodium oxalate - Reductometric valueCertified purity.............99.972 %
60 g
NIST-83D Arsenic trioxide - Reductometric valueCertified purity...........99.9926 %
60 g
NIST-84K Potassium hydrogen phthalate - Acidmetric valueCertified purity...........99.9911 %
60 g
NIST-350A Benzoic acid - Acidmetric valueCertified purity...........99.9958 %
30 g
NIST-723D Benzoic acid - Acidmetric valueCertified purity...........99.9958 %
50 g
NIST-351 Sodium carbonate - Oxidimetric valueCertified purity...........99.9796 %
50 g
NIST-951 Boric acid assay - Acidmetric and boron isotopic valuePurity...........................100.00 % Certified value
Abundance ratio
10B/11B .......................... 0.2473 10B............................. 19.827 % 11B .............................80.173 %
100 g
NIST-987 Strontium carbonate - Assay and isotopic valuesCertified values
Purity.............................99.98 % 87Sr ............................. 7.0015 % 84Sr..............................0.5574 %88Sr............................82.5845 % 86Sr ............................. 9.8566 %
1 g
NIST-999A Potassium chloride - Assay valuesCertified purity
KCl ............................99.9817 % K............................... 52.4354 % Cl ..............................47.5463 %
60 g
NRMGBW06101a Sodium carbonateCertified purity.............99.995 %
50 g
NRMGBW06102 EDTA disodium saltCertified purity.............99.979 %
25 g
NRMGBW06103a Sodium chlorideCertified purity.............99.995 %
50 g
NRMGBW06104 BenzeneCertified purity...............99.95 %
5 mL
NRMGBW06105b Potassium dichromateCertified purity.............99.984 %
50 g
NRMGBW06106a Potassium hydrogen phthalateCertified purity.............99.984 %
50 g
NRMGBW06107a Sodium oxalateCertified purity...............99.99 %
50 g
NRMGBW06108 Zinc oxide - Complexometric standardComplexometric value .......................12.280 mmol/g Certified value
50 g
NRMGBW06109 Potassium chlorideCl ................................100.00 % K................................... 99.97 % Certified purities
50 g
NRMGBW06110 Potassium iodate - OxidimetryCertified purity...............99.91 %
50 g
Organo-metallic compounds
122 Edition 2003/2004 www.lgcpromochem.com
Organo-metallic compoundsCode Product Unit
NIST-1051B Barium cyclohexanebutyrate - BariumBa ...................................28.7 % Certified value
5 g
NIST-1052B Bis(1-phenyl-1,3-butanediono) oxovanadium (IV) - VanadiumCertified value
V ...................................13.01 % Certified value
5 g
NIST-1053A Cadmium cyclohexanebutyrate - CadmiumCd ...................................24.8 % Certified value
5 g
NIST-1057B Dibutyltin bis (2-ethylhexanoate) - TinSn .................................22.95 % Certified value
5 g
NIST-1059C Lead cyclohexanebutyrate - LeadPb ...................................37.5 % Certified value
5 g
NIST-1060A Lithium cyclohexanebutyrate - LithiumLi .......................................4.1 % Certified value
5 g
NIST-1065B Nickel cyclohexanebutyrate - NickelNi ..................................13.89 % Certified value
5 g
NIST-1066 Octaphenylcyclotetrasiloxane - SiliconSi...................................14.14 % Certified value
5 g
NIST-1069B Sodium cyclohexanebutyrate - SodiumNa ...................................12.0 % Certified value
5 g
NIST-1070A Strontium cyclohexanebutyrate - StrontiumSr ....................................20.7 % Certified value
5 g
NIST-1071B Triphenyl phosphate - PhosphorousP .....................................9.48 % Certified value
5 g
NIST-1073B Zinc cyclohexanebutyrate - ZincZn..................................16.66 % Certified value
5 g
NIST-1075A Aluminium 2-ethylhexanoate - AluminiumAl.....................................8.07 % Certified value
5 g
NIST-1077A Silver 2-ethylhexanoate - SilverAg .................................42.60 % Certified value
5 g
NIST-1078B Tris (1-phenyl-1,3-butanediono) chromium (III) - ChromiumCr ......................................9.6 % Certified value
5 g
NIST-1079B Tris (1-phenyl-1,3-butanediono) iron (III) - IronFe..................................10.45 % Certified value
5 g
NIST-1080A Bis (1-phenyl-1,3-butanediono) copper (II) - CopperCu .................................16.37 % Certified value
5 g
SpeciationCode Product Unit
BCR-544 Lyophilised chromium solution - ChromiumCertified values
Cr(III) ........................... 26.8 µg/L Cr(VI)...........................22.8 µg/L Total Cr ....................... 49.4 µg/L
2 mg
BCR-626 Arsenobetaine standard solution - ArsenobetaineCertified value
Arsenobetaine [as (CH3) As+CH2COO- ] ................................................. 1031 mg/kg
10 mL
Isotopes
www.lgcpromochem.com Edition 2003/2004 123
IsotopesCode Product Unit
NIST-951 Boric acid assay - Acidmetric and boron isotopic valueCertified values
Purity...........................100.00 %
Abundance ratio
10B/11B .......................... 0.2473 10B............................. 19.827 % 11B .............................80.173 %
100 g
NIST-952 Boric acid (enriched 10B)Certified values
Purity.............................99.97 %
Abundance ratio10B/11B............................... 18.80 10B .............................. 94.949 % 11B.................................5.051 %
250 mg
NIST-975a Sodium chloride - Isotopic compositionCertified values
Absolute abundance ratio35Cl/37Cl............. 3.1279 ± 0.0047
Isotopic composition35Cl .........75.774 ± 0.028 atom% 37Cl......... 24.226 ± 0.028 atom%
Atomic weight ........................... 35.45265 ± 0.00055
250 mg
NIST-977 Sodium bromide - Isotopic compositionCertified values
Abundance ratio79Br/81Br ........................ 1.02784 79Br ............................. 50.686 % 81Br..............................49.314 %
250 mg
NIST-978A Silver nitrate - Assay/isotopic compositionCertified values
Purity.............................99.99 %
Abundance ratio107Ag/109Ag .................... 1.07638 107Ag ......................... 51.8392 % 109Ag..........................48.1608 %
250 mg
NIST-979 Chromium nitrate - Isotopic compositionCertified values50Cr ...............................4.345 % 53Cr ............................... 9.501 %52Cr .............................83.789 % 54Cr ............................... 2.365 %
250 mg
NIST-981 Lead metal, natural - Isotopic compositionCertified values204Pb............................1.4255 % 207Pb ......................... 22.0833 %206Pb..........................24.1442 % 208Pb ......................... 52.3470 %
1 g
NIST-986 Nickel - Isotopic compositionCertified values58Ni........................68.076886 % 61Ni ......................... 1.139894 % 64Ni..........................0.925546 %60Ni........................26.223146 % 62Ni ......................... 3.634528 %
500 mg
NIST-987 Strontium carbonate - Assay and isotopic valuesCertified values
Purity.............................99.98 % 87Sr ............................. 7.0015 % 84Sr..............................0.5574 %88Sr............................82.5845 % 86Sr ............................. 9.8566 %
1 g
NIST-991 Lead-206 spike - Assay/isotopic compositionCertified values
Pb ..................... 0.32261 µmol/g 206Pb ........................... 99.979 % 208Pb..............................0.013 %204Pb................................ <3ppm 207Pb ............................. 0.008 %
15 g
NIST-994 Gallium metal - Isotopic compositionCertified values
Abundance ratio69Ga/71Ga ...................... 1.5067669Ga ..........................60.1079 % 71Ga.......................... 39.8921 %
250 mg
Isotopes
124 Edition 2003/2004 www.lgcpromochem.com
Code Product Unit
NIST-997 Thallium metal - Isotopic compositionCertified values
Abundance ratio205Tl/203Tl ....................... 2.38714203Tl ...........................29.5235 % 205Tl .......................... 70.4765 %
250 mg
IAEA-305 Ammonium sulfate - Nitrogen-15Assessed values
Solution A15N..................... 39.8 activity/mL
Solution B15N................... 375.3 activity/mL
unit
IAEA-311 Ammonium sulfate - Nitrogen-15Assessed value15N..................... 2.05 activity/mL
100 mg
IAEA-303 Sodium bicarbonate - Carbon-13Assessed values
Solution A
13C .................... 93.3 activity/ml
Solution B
13C ..................... 466 activity/ml
2 x 3 mL
Standards for spectroscopy
www.lgcpromochem.com Edition 2003/2004 125
Standards for spectroscopy
Introduction
This comprehensive range of elemental standards has been compiled by selecting complementarymaterials from two sources, NIST and ULTRA Scientific Inc. Their combined range covers virtually allcalibration needs for elemental emission spectroscopy instruments.It is important to understand that there are fundamental differences between standards prepared foratomic absorption spectroscopy (AAS) and ICP and ICP-MS techniques. This is because of theintrinsic difference in the way measurement is carried out. In AAS the sample is energized bycombustion, a specific light source is passed through the flame and elements present in the sampleabsorb at a specific wavelength. With ICP and ICP-MS the sample is energized to the point where theelements in the sample emit energy at a specific wavelength. Because measurement is dependent onspecific emission there is a considerable potential for impurities to interfere with the analyte ofinterest. The distinction between AAS and ICP standards is the purity of starting materials. Typicallymaterial of 99.9 or 99.99% purity is suitable for AAS, but for critical ICP work the standards need to beproduced from a starting material that is 99.999% or better. Remember that ICP/ICP-MS standardsare perfectly suitable for AAS, but not the reverse.
NIST Standard Reference Materials® (SRMs®)
NIST Standard Reference Materials® are certified by procedures that conform with the requirementsof ISO Guides 30 to 35, and are therefore accepted as primary standards for use in atomic absorptionspectroscopy (AAS), optical emission spectroscopy (OES), inductively coupled plasma (ICP), mass[plasma] spectroscopy (MS), ion chromatography or any other analytical technique that requiresaqueous solutions of elements for calibration. These SRM Standards are the most precise andaccurate solutions available and are best used as single element solutions.
ULTRA ScientificTM certified ICP/AA standards
The ULTRA Scientific range of single and multi-element solutions in this catalogue are of the highestquality. ULTRA Scientific are one of the leading manufacturers in the US and have an ISO 9001registered quality system verified by their ISO 17025 accredited laboratory. The ICP standards areprepared from starting materials having a purity of 99.999 % (where possible), high purity acids andASTM Type I water (18 megohm). Standards are traceable to NIST Standard Reference Materials®
(SRM®) whenever possible. Solution density data are available for single element standards.
Code Product Unit
Aluminum - Al
NIST-3101A Al in 10% HNO3, 10 mg/g 50 mL
U-ICP-013 Al(NO3)3 x 9H2O in dilute HNO3, 1000 µg/mL 100 mL
U-ICP-013-5 Al(NO3)3 x 9H2O in dilute HNO3, 1000 µg/mL 500 mL
Antimony - Sb
NIST-3102A Sb in 10% HNO3 + 2% HF, 10 mg/g 50 mL
U-ICP-051 Sb-metal in dilute HNO3/C4H6O6, 1000 µg/mL 100 mL
U-ICP-051-5 Sb-metal in dilute HNO3/C4H6O6, 1000 µg/mL 500 mL
Arsenic - As
NIST-3103A As in 15% HNO3, 10 mg/g 50 mL
U-ICP-033 As2O3 in dilute HNO3, 1000 µg/mL 100 mL
U-ICP-033-5 As2O3 in dilute HNO3, 1000 µg/mL 500 mL
Barium - Ba
NIST-3104A Ba in 1% HNO3, 10 mg/g 50 mL
U-ICP-056 Ba(NO3)2 in dilute HNO3, 1000 µg/mL 100 mL
U-ICP-056-5 Ba(NO3)2 in dilute HNO3, 1000 µg/mL 500 mL
Standards for spectroscopy
126 Edition 2003/2004 www.lgcpromochem.com
Code Product Unit
Beryllium – Be
NIST-3105A Be in 10% HNO3, 10 mg/g 5 x 10 mL
U-ICP-004 Be acetate in dilute HNO3, 1000 µg/mL 100 mL
U-ICP-004-5 Be acetate in dilute HNO3, 1000 µg/mL 500 mL
Bismuth – Bi
U-ICP-083 Bi-metal in dilute HNO3, 1000 µg/mL 100 mL
U-ICP-083-5 Bi-metal in dilute HNO3, 1000 µg/mL 500 mL
Boron – B
NIST-3107 B in water, 5 mg/g 50 mL
U-ICP-005 H3BO3 in H2O tr. NH4OH, 1000 µg/mL 100 mL
U-ICP-005-5 H3BO3 in H2O tr. NH4OH, 1000 µg/mL 500 mL
Cadmium – Cd
NIST-3108 Cd in 10% HNO3, 10 mg/g 50 mL
U-ICP-048 Cd(NO3)2 x H2O in dilute HNO3, 1000 µg/mL 100 mL
U-ICP-048-5 Cd(NO3)2 x H2O in dilute HNO3, 1000 µg/mL 500 mL
Calcium – Ca
NIST-3109° Ca in 10% HNO3, 10 mg/g 50 mL
U-ICP-020 CaCO3 in dilute HNO3, 1000 µg/mL 100 mL
U-ICP-020-5 CaCO3 in dilute HNO3, 1000 µg/mL 500 mL
Cerium – Ce
NIST-3110A Ce in 10% HNO3, 10 mg/g 5 x 10 mL
U-ICP-058 Ce(NO3)3 in dilute HNO3, 1000 µg/mL 100 mL
U-ICP-058 Ce(NO3)3 in dilute HNO3, 1000 µg/mL 100 mL
Cesium – Cs
U-ICP-055 CsNO3 in dilute HNO3, 1000 µg/mL 100 mL
U-ICP-055-5 CsNO3 in dilute HNO3, 1000 µg/mL 500 mL
Chromium – Cr
NIST-3112A Cr in 10% HNO3, 10 mg/g 5 x 10 mL
U-ICP-024 Ammonium dichromate in dilute HNO3, 1000 µg/mL 100 mL
U-ICP-024-5 Ammonium dichromate in dilute HNO3, 1000 µg/mL 500 mL
Cobalt – Co
NIST-3113 Co in 10% HNO3, 10 mg/g 5 x 10 mL
U-ICP-027 Co(NO3)2 x 6H2O in dilute HNO3, 1000 µg/mL 100 mL
U-ICP-027-5 Co(NO3)2 x 6H2O in dilute HNO3, 1000 µg/mL 500 mL
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Code Product Unit
Copper – Cu
NIST-3114 Cu in 10% HNO3, 10 mg/g 5 x 10 mL
U-ICP-029 Cu(NO3)2 x 3H2O in dilute HNO3, 1000 µg/mL 100 mL
U-ICP-029-5 Cu(NO3)2 x 3H2O in dilute HNO3, 1000 µg/mL 500 mL
Dysprosium – Dy
NIST-3115A Dy in 10% HNO3, 10 mg/g 5 x 10 mL
U-ICP-066 Dy2O3 in dilute HNO3, 1000 µg/mL 100 mL
U-ICP-066-5 Dy2O3 in dilute HNO3, 1000 µg/mL 500 mL
Erbium – Er
U-ICP-068 Er2O3 in dilute HNO3, 1000 µg/mL 100 mL
U-ICP-068-5 Er2O3 in dilute HNO3, 1000 µg/mL 500 mL
Europium – Eu
NIST-3117A Eu in 10% HNO3, 10 mg/g 5 x 10 mL
U-ICP-063 Eu2O3 in dilute HNO3, 1000 µg/mL 100 mL
U-ICP-063-5 Eu2O3 in dilute HNO3, 1000 µg/mL 500 mL
Gadolinium – Gd
NIST-3118° Gd in 10% HNO3, 10 mg/g 5 x 10 mL
U-ICP-064 Gd2O3 in dilute HNO3, 1000 µg/mL 100 mL
U-ICP-064-5 Gd2O3 in dilute HNO3, 1000 µg/mL 500 mL
Gallium – Ga
NIST-3119° Ga in 10% HNO3, 10 mg/g 50 mL
U-ICP-031 Ga-metal in dilute HNO3, 1000 µg/mL 100 mL
U-ICP-031-5 Ga-metal in dilute HNO3, 1000 µg/mL 500 mL
Germanium- Ge
NIST-3120° Ge in 10% Oxalic acid, 10 mg/g 50 mL
U-ICP-032 GeO2 in H2O trace HF, 1000 µg/mL 100 mL
U-ICP-032-5 GeO2 in H2O trace HF, 1000 µg/mL 500 mL
Gold – Au
NIST-3121 Au in 5% HNO3 + 2% HF, 10 mg/g 5 x 10 mL
U-ICP-079 Au-metal in dilute HCl, 1000 µg/mL 100 mL
U-ICP-079-5 Au-metal in dilute HCl, 1000 µg/mL 500 mL
Hafnium – Hf
NIST-3122 Hf in 10% HNO3 + 2% HF, 10 mg/g 50 mL
U-ICP-072 HfOCl2 x 8H2O in dilute HCl, 1000 µg/mL 100 mL
U-ICP-072-5 HfOCl2 x 8H2O in dilute HCl, 1000 µg/mL 500 mL
Standards for spectroscopy
128 Edition 2003/2004 www.lgcpromochem.com
Code Product Unit
Holmium – Ho
U-ICP-067 Ho2O3 in dilute HNO3, 1000 µg/mL 100 mL
U-ICP-067-5 Ho2O3 in dilute HNO3, 1000 µg/mL 500 mL
Indium – In
NIST-3124A In in 10% HNO3, 10 mg/g 5 x 10 mL
U-ICP-049 In-metal in dilute HNO3 , 1000 µg/mL 100 mL
U-ICP-049-5 In-metal in dilute HNO3 , 1000 µg/mL 500 mL
Iridium – Ir
U-ICP-077 IrCl3 in dilute HCl, 1000 µg/mL 100 mL
U-ICP-077-5 IrCl3 in dilute HCl, 1000 µg/mL 500 mL
Iron – Fe
NIST-3126A Fe in 10% HNO3, 10 mg/g 50 mL
U-ICP-026 Fe(NO3)2 in dilute HNO3, 1000 µg/mL 100 mL
U-ICP-026-5 Fe(NO3)2 in dilute HNO3, 1000 µg/mL 500 mL
Lanthanum – La
NIST-3127° La in 10% HNO3, 10 mg/g 5 x 10 mL
U-ICP-057 La2O3 in dilute HNO3, 1000 µg/mL 100 mL
U-ICP-057-5 La2O3 in dilute HNO3, 1000 µg/mL 500 mL
Lead – Pb
NIST-3128 Pb in 10% HNO3, 10 mg/g 5 x 10 mL
U-ICP-082 Pb(NO3)2 in dilute HNO3, 1000 µg/mL 100 mL
U-ICP-082-5 Pb(NO3)2 in dilute HNO3, 1000 µg/mL 500 mL
Lithium – Li
NIST-3129° Li in 10% HNO3, 10 mg/g 5 x 10 mL
U-ICP-003 Li2CO3 in dilute HNO3, 1000 µg/mL 100 mL
U-ICP-003-5 Li2CO3 in dilute HNO3, 1000 µg/mL 500 mL
Lutetium – Lu
NIST-3130A Lu in 10% HNO3, 10 mg/g 5 x 10 mL
U-ICP-071 Lu2O3 in dilute HNO3, 1000 µg/mL 100 mL
U-ICP-071-5 Lu2O3 in dilute HNO3, 1000 µg/mL 500 mL
Magnesium – Mg
NIST-3131A Mg in 10% HNO3, 10 mg/g 50 mL
U-ICP-012 Mg(NO3)2 in dilute HNO3, 1000 µg/mL 100 mL
U-ICP-012-5 Mg(NO3)2 in dilute HNO3, 1000 µg/mL 500 mL
Standards for spectroscopy
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Code Product Unit
Manganese – Mn
NIST-3132 Mn in 10% HNO3 5 x 10 mL
U-ICP-025 Mn(NO3)2 in dilute HNO3, 1000 µg/mL 100 mL
U-ICP-025-5 Mn(NO3)2 in dilute HNO3, 1000 µg/mL 500 mL
Mercury – Hg
NIST-3133 Hg in 10% HNO3, 10 mg/g 5 x 10 mL
U-ICP-080 HgNO3 in dilute HNO3, 1000 µg/mL 100 mL
U-ICP-080-5 HgNO3 in dilute HNO3, 1000 µg/mL 500 mL
Molybdenum - Mo
NIST-3134 Mo in 10% HCl, 10 mg/g 5 x 10 mL
U-ICP-042 MoO2 in H2O trace NH4OH, 1000 µg/mL 100 mL
U-ICP-042-5 MoO2 in H2O trace NH4OH, 1000 µg/mL 500 mL
Neodymium - Nd
NIST-3135A Nd in 10% HNO3, 10 mg/g 5 x 10 mL
U-ICP-060 Nd2O3 in dilute HNO3, 1000 µg/mL 100 mL
U-ICP-060-5 Nd2O3 in dilute HNO3, 1000 µg/mL 500 mL
Nickel - Ni
NIST-3136 Ni in 10% HNO3, 10 mg/g 5 x 10 mL
U-ICP-028 Ni(NO3)2 in dilute HNO3, 1000 µg/mL 100 mL
U-ICP-028-5 Ni(NO3)2 in dilute HNO3, 1000 µg/mL 500 mL
Niobium - Nb
NIST-3137 Nb in 5% HNO3 + 2% HF, 10 mg/g 50 mL
U-ICP-041 Nb3O5 in H2O trace HF, 1000 µg/mL 100 mL
U-ICP-041-5 Nb3O5 in H2O trace HF, 1000 µg/mL 500 mL
Palladium - Pd
NIST-3138 Pd in 10% HNO3, 10 mg/g 5 x 10 mL
U-ICP-046 Pd-metal in dilute HNO3, 1000 µg/mL 100 mL
U-ICP-046-5 Pd-metal in dilute HNO3, 1000 µg/mL 500 mL
Phosphorus - P
NIST-3139A P in 0.8% HNO3, 10 mg/g 5 x 10 mL
U-ICP-015 NH4H2PO4 in dilute HNO3, 1000 µg/mL 100 mL
U-ICP-015-5 NH4H2PO4 in dilute HNO3, 1000 µg/mL 500 mL
Platinum - Pt
NIST-3140 Pt in 10% HCl, 10 mg/g 5 x 10 mL
U-ICP-078 Pt-metal in dilute HCl, 1000 µg/mL 100 mL
U-ICP-078-5 Pt-metal in dilute HCl, 1000 µg/mL 500 mL
Standards for spectroscopy
130 Edition 2003/2004 www.lgcpromochem.com
Code Product Unit
Potassium - K
NIST-3141A K in 1% HNO3, 10 mg/g 50 mL
U-ICP-019 KNO3 in dilute HNO3, 1000 µg/mL 100 mL
U-ICP-019-5 KNO3 in dilute HNO3, 1000 µg/mL 500 mL
Praseodymium - Pr
NIST-3142A Pr in 10% HNO3, 10 mg/g 5 x 10 mL
U-ICP-059 Pr6O11 in dilute HNO3, 1000 µg/mL 100 mL
U-ICP-059-5 Pr6O11 in dilute HNO3, 1000 µg/mL 500 mL
Rhenium – Re
NIST-3143 Re in 10% HNO3, 10 mg/g 50 mL
U-ICP-075 Re-metal in H2O, 1000 µg/mL 100 mL
U-ICP-075-5 Re-metal in H2O, 1000 µg/mL 500 mL
Rhodium – Rh
NIST-3144 Rh in 10% HCl, 10 mg/g 5 x 10 mL
U-ICP-045 RhCl3 in dilute HCl, 1000 µg/mL 100 mL
U-ICP-045 RhCl3 in dilute HCl, 1000 µg/mL 100 mL
Rubidium – Rb
NIST-3145A Rb in 1% HNO3, 10 mg/g 5 x 10 mL
U-ICP-037 RbNO3 in dilute HNO3, 1000 µg/mL 100 mL
U-ICP-037-5 RbNO3 in dilute HNO3, 1000 µg/mL 500 mL
Ruthenium – Ru
U-ICP-044 RuCl3 in dilute HCl, 1000 µg/mL 100 mL
U-ICP-044-5 RuCl3 in dilute HCl, 1000 µg/mL 500 mL
Samarium – Sm
NIST-3147A Sm in 10% HNO3, 10 mg/g 5 x 10 mL
U-ICP-062 Sm2O3 in dilute HNO3, 1000 µg/mL 100 mL
U-ICP-062-5 Sm2O3 in dilute HNO3, 1000 µg/mL 500 mL
Scandium – Sc
NIST-3148° Sc in 10% HNO3, 10 mg/g 5 x 10 mL
U-ICP-021 Sc2O3 in dilute HNO3, 1000 µg/mL 100 mL
U-ICP-021-5 Sc2O3 in dilute HNO3, 1000 µg/mL 500 mL
Selenium – Se
NIST-3149 Se in 10% HNO3, 10 mg/g 5 x 10 mL
U-ICP-034 SeO2 in dilute HNO3, 1000 µg/mL 100 mL
U-ICP-034-5 SeO2 in dilute HNO3, 1000 µg/mL 500 mL
Standards for spectroscopy
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Code Product Unit
Silicon – Si
NIST-3150 Si in water, 10 mg/g 50 mL
U-ICP-014 (NH4)2SiF6 in dilute HNO3, 1000 µg/mL 100 mL
U-ICP-014-5 (NH4)2SiF6 in dilute HNO3, 1000 µg/mL 500 mL
U-ICP-014° SiO2 in dilute NaOH, 1000 µg/mL 100 mL
U-ICP-014°-5 SiO2 in dilute NaOH, 1000 µg/mL 500 mL
Silver – Ag
NIST-3151 Ag in 10% HNO3, 10 mg/g 5 x 10 mL
U-ICP-047 AgNO3 in dilute HNO3, 1000 µg/mL 100 mL
U-ICP-047-5 AgNO3 in dilute HNO3, 1000 µg/mL 500 mL
Sodium - Na
NIST-3152A Na in 1% HNO3, 10 mg/g 50 mL
U-ICP-011 NaNO3 in dilute HNO3, 1000 µg/mL 100 mL
U-ICP-011-5 NaNO3 in dilute HNO3, 1000 µg/mL 500 mL
Strontium - Sr
NIST-3153A Sr in 10% HNO3, 10 mg/g 5 x 10 mL
U-ICP-038 SrNO3 in dilute HNO3, 1000 µg/mL 100 mL
U-ICP-038-5 SrNO3 in dilute HNO3, 1000 µg/mL 500 mL
Sulphur - S
NIST-3154 S in 0.1% H2SO4, 10 mg/g 5 x 10 mL
U-ICP-016 (NH4)2SO4 in H2O, 1000 µg/mL 100 mL
U-ICP-016-5 (NH4)2SO4 in H2O, 1000 µg/mL 500 mL
Tantalum - Ta
NIST-3155 Ta in 5% HNO3 + 2% HF, 10 mg/g 50 mL
U-ICP-073 Ta-metal in H2O trace HF, 1000 µg/mL 100 mL
U-ICP-073-5 Ta-metal in H2O trace HF, 1000 µg/mL 500 mL
Tellurium - Te
NIST-3156 Te in 20% HCl, 10 mg/g 5 x 10 mL
U-ICP-052 Te-metal in dilute HCl, 1000 µg/mL 100 mL
U-ICP-052-5 Te-metal in dilute HCl, 1000 µg/mL 500 mL
Terbium - Tb
NIST-3157A Tb in 16% HNO3, 10 mg/g 5 x 10 mL
U-ICP-065 Tb4O7 in dilute HNO3, 1000 µg/mL 100 mL
U-ICP-065-5 Tb4O7 in dilute HNO3, 1000 µg/mL 500 mL
Standards for spectroscopy
132 Edition 2003/2004 www.lgcpromochem.com
Code Product Unit
Thallium - Tl
NIST-3158A Tl in 10% HNO3, 10 mg/g 5 x 10 mL
U-ICP-081 TlNO3 in dilute HNO3, 1000 µg/mL 100 mL
U-ICP-081-5 TlNO3 in dilute HNO3, 1000 µg/mL 500 mL
Thorium - Th
NIST-3159 Th in 10% HNO3, 10 mg/g 50 mL
U-ICP-090 Th(NO3)4 x 4H2O in dilute HNO3, 1000 µg/mL 100 mL
U-ICP-090-5 Th(NO3)4 x 4H2O in dilute HNO3, 1000 µg/mL 500 mL
Thulium - Tm
NIST-3160A Tm in 10% HNO3, 10 mg/g 5 x 10 mL
U-ICP-069 Tm in dilute HNO3, 1000 µg/mL 100 mL
U-ICP-069-5 Tm in dilute HNO3, 1000 µg/mL 500 mL
Tin - Sn
NIST-3161A Sn in 5% HNO3 + 2% HF, 10 mg/g 50 mL
U-ICP-050 (NH4)2SnF6 in dilute HNO3, 1000 µg/mL 100 mL
U-ICP-050-5 (NH4)2SnF6 in dilute HNO3, 1000 µg/mL 500 mL
Titanium - Ti
NIST-3162A Ti in 10% HNO3 + 2% HF, 10 mg/g 50 mL
U-ICP-022 (NH4)2TiF6 dilute HNO3, 1000 µg/mL 100 mL
U-ICP-022-5 (NH4)2TiF6 dilute HNO3, 1000 µg/mL 500 mL
Tungsten - W
NIST-3163 W in 7% HNO3 + 4% HF, 10 mg/g 50 mL
U-ICP-074 (NH4)2WO4 in H2O trace NH4OH, 1000 µg/mL 100 mL
U-ICP-074-5 (NH4)2WO4 in H2O trace NH4OH, 1000 µg/mL 500 mL
Uranium - U
NIST-3164 U in 10% HNO3, 10 mg/g 5 x 10 mL
U-ICP-092 U3O8 in dilute HNO3, 1000 µg/mL 100 mL
U-ICP-092-5 U3O8 in dilute HNO3, 1000 µg/mL 500 mL
Vanadium - V
NIST-3165 V in 10% HNO3, 10 mg/g 5 x 10 mL
U-ICP-023 NH4VO3 in dilute HNO3, 1000 µg/mL 100 mL
U-ICP-023-5 NH4VO3 in dilute HNO3, 1000 µg/mL 500 mL
Ytterbium - Yb
NIST-3166A Yb in 16% HNO3, 10 mg/g 5 x 10 mL
U-ICP-070 Yb2O3 in dilute HNO3, 1000 µg/mL 100 mL
U-ICP-070-5 Yb2O3 in dilute HNO3, 1000 µg/mL 500 mL
Standards for spectroscopy
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Code Product Unit
Yttrium - Y
NIST-3167A Y in 10% HNO3, 10 mg/g 5 x 10 mL
U-ICP-039 Y2O3 in dilute HNO3, 1000 µg/mL 100 mL
U-ICP-039-5 Y2O3 in dilute HNO3, 1000 µg/mL 500 mL
Zinc - Zn
NIST-3168A Zn in 10% HCl, 10 mg/g 50 mL
U-ICP-030 Zn(NO3)2 x H2O in dilute HNO3, 1000 µg/mL 100 mL
U-ICP-030-5 Zn(NO3)2 x H2O in dilute HNO3, 1000 µg/mL 500 mL
Zirconium - Zr
NIST-3169 Zr in 10% HNO3 + 2% HF, 10 mg/g 50 mL
U-ICP-040 Zr(NO3)4 in dilute HNO3, 1000 µg/mL 100 mL
U-ICP-040-5 Zr(NO3)4 in dilute HNO3, 1000 µg/mL 500 mL
The ULTRA ScientificTM range of single element solutions for ICP are alsoavailable at a concentration of 10000 µg/mL in 100 mL and 500 mL units.
Standards for spectroscopy
134 Edition 2003/2004 www.lgcpromochem.com
Code Product Unit
ULTRA Scientific's EnviroConcentrateTM kits for ICP
Kit
- 20 mL of analyte solution at 10000 µg/mL- yields 2 x 100 mL 1000 µg/mL standards- 500 ml of ASTM Type I water- 100 mL pre-cleaned LDPE bottle for storage- starting material 99.999 % pure, where available- NIST traceable
Aluminum - Al
U-ECK-013 Al in dilute HNO3, 10000 µg/mL kit
Antimony - Sb
U-ECK-051 Sb in dilute HNO3, 10000 µg/mL kit
Arsenic - As
U-ECK-033 As in dilute HNO3, 10000 µg/mL kit
Barium - Ba
U-ECK-056 Ba in dilute HNO3, 10000 µg/mL kit
Beryllium - Be
U-ECK-004 Be in dilute HNO3, 10000 µg/mL kit
Boron - B
U-ECK-005 B in water with trace NH4OH, 10000 µg/mL kit
Cadmium - Cd
U-ECK-048 Cd in dilute HNO3, 10000 µg/mL kit
Calcium - Ca
U-ECK-020 Ca in dilute HNO3, 10000 µg/mL kit
Chromium - Cr
U-ECK-024 Cr in dilute HNO3, 10000 µg/mL kit
Cobalt - Co
U-ECK-027 Co in dilute HNO3, 10000 µg/mL kit
Copper - Cu
U-ECK-029 Cu in dilute HNO3, 10000 µg/mL kit
Iron - Fe
U-ECK-026 Fe in dilute HNO3, 10000 µg/mL kit
Lead - Pb
U-ECK-082 Pb in dilute HNO3, 10000 µg/mL kit
Lithium - Li
U-ECK-003 Li in dilute HNO3, 10000 µg/mL kit
Magnesium - Mg
U-ECK-012 Mg in dilute HNO3, 10000 µg/mL kit
Standards for spectroscopy
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Code Product Unit
Manganese - Mn
U-ECK-025 Mn in dilute HNO3, 10000 µg/mL kit
Mercury - Hg
U-ECK-080 Hg in dilute HNO3, 10000 µg/mL kit
Molybdenum - Mo
U-ECK-042 Mo in water with tr. NH4OH, 10000 µg/mL kit
Nickel - Ni
U-ECK-028 Ni in dilute HNO3, 10000 µg/mL kit
Phosphorus - P
U-ECK-015 P in dilute HNO3, 10000 µg/mL kit
Potassium - K
U-ECK-019 K in dilute HNO3, 10000 µg/mL kit
Selenium - Se
U-ECK-034 Se in dilute HNO3, 10000 µg/mL kit
Silicon - Si
U-ECK-014 Si in water, 10000 µg/mL kit
Silver - Ag
U-ECK-047 Ag in dilute HNO3, 10000 µg/mL kit
Sodium - Na
U-ECK-011 Na in dilute HNO3, 10000 µg/mL kit
Strontium - Sr
U-ECK-038 Sr in dilute HNO3, 10000 µg/mL kit
Thallium - Tl
U-ECK-081 Tl in dilute HNO3, 10000 µg/mL kit
Tin - Sn
U-ECK-050 Sn in water, 10000 µg/mL kit
Titanium - Ti
U-ECK-022 Ti in water with trace HF, 10000 µg/mL kit
Vanadium - V
U-ECK-023 V in dilute HNO3, 10000 µg/mL kit
Zinc - Zn
U-ECK-030 Zn in dilute HNO3, 10000 µg/mL kit
Standards for spectroscopy
136 Edition 2003/2004 www.lgcpromochem.com
Code Product Unit
ULTRA Scientific´s certified standards for atomic absorption spectroscopy
Aluminum - Al
U-IAA-213 Al in dilute HNO3, 1000 µg/mL 100 mL
Antimony - Sb
U-IAA-251 Sb in dilute HNO3, 1000 µg/mL 100 mL
Arsenic - As
U-IAA-233 As in dilute HNO3, 1000 µg/mL 100 mL
Barium - Ba
U-IAA-256 Ba in dilute HNO3, 1000 µg/mL 100 mL
Beryllium - Be
U-IAA-204 Be in dilute HNO3, 1000 µg/mL 100 mL
Bismuth - Bi
U-IAA-283 Bi in dilute HNO3, 1000 µg/mL 100 mL
Boron - B
U-IAA-205 B in water with trace NH4OH, 1000 µg/ml 100 mL
Cadmium - Cd
U-IAA-248 Cd in dilute HNO3, 1000 µg/mL 100 mL
Calcium - Ca
U-IAA-220 Ca in dilute HNO3, 1000 µg/mL 100 mL
Cerium - Ce
U-IAA-258 Ce in dilute HNO3, 1000 µg/mL 100 mL
Cesium - Cs
U-IAA-255 Cs in dilute HNO3, 1000 µg/mL 100 mL
Chromium - Cr
U-IAA-224 Cr in dilute HNO3, 10000 µg/mL 100 mL
Cobalt - Co
U-IAA-227 Co in dilute HNO3, 1000 µg/mL 100 mL
Copper - Cu
U-IAA-229 Cu in dilute HNO3, 1000 µg/mL 100 mL
Dysprosium - Dy
U-IAA-266 Dy in dilute HNO3, 1000 µg/mL 100 mL
Erbium - Er
U-IAA-268 Er in dilute HNO3, 1000 µg/mL 100 mL
Europium - Eu
U-IAA-263 Eu in dilute HNO3, 1000 µg/mL 100 mL
Standards for spectroscopy
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Code Product Unit
Gadolinium - Gd
U-IAA-264 Gd in dilute HNO3, 1000 µg/mL 100 mL
Gallium - Ga
U-IAA-231 Ga in dilute HNO3, 1000 µg/mL 100 mL
Germanium - Ge
U-IAA-232 Ge in water with trace HF, 1000 µg/mL 100 mL
Gold - Au
U-IAA-279 Au-metal in dilute HCl, 1000 µg/mL 100 mL
Hafnium - Hf
U-IAA-272 Hf in dilute HCl, 1000 µg/mL 100 mL
Holmium - Ho
U-IAA-267 Ho in dilute HNO3, 1000 µg/mL 100 mL
Indium - In
U-IAA-249 In in dilute HNO3, 1000 µg/mL 100 mL
Iridium - Ir
U-IAA-277 Ir in dilute HCl, 1000 µg/mL 100 mL
Iron - Fe
U-IAA-226 Fe in dilute HNO3, 1000 µg/mL 100 mL
Lanthanum - La
U-IAA-257 La in dilute HNO3, 1000 µg/mL 100 mL
Lead - Pb
U-IAA-282 Pb in dilute HNO3, 1000 µg/mL 100 mL
Lithium - Li
U-IAA-203 Li in dilute HNO3, 1000 µg/mL 100 mL
Lutetium - Lu
U-IAA-271 Lu in dilute HNO3, 1000 µg/mL 100 mL
Magnesium - Mg
U-IAA-212 Mg in dilute HNO3, 1000 µg/mL 100 mL
Manganese - Mn
U-IAA-225 Mn in dilute HNO3, 1000 µg/mL 100 mL
Mercury - Hg
U-IAA-280 Hg in dilute HNO3, 1000 µg/mL 100 mL
Molybdenum - Mo
U-IAA-242 Mo in water with trace NH4OH, 1000 µg/mL 100 mL
Neodymium - Nd
U-IAA-260 Nd in dilute HNO3, 1000 µg/mL 100 mL
Standards for spectroscopy
138 Edition 2003/2004 www.lgcpromochem.com
Code Product Unit
Nickel - Ni
U-IAA-228 Ni in dilute HNO3, 1000 µg/mL 100 mL
Niobium - Nb
U-IAA-241 Nb in water with trace. HF, 1000 µg/mL 100 mL
Palladium - Pd
U-IAA-246 Pd-metal in dilute HNO3, 1000 µg/mL 100 mL
Phosphorus - P
U-IAA-215 P in dilute HNO3, 1000 µg/mL 100 mL
Platinum - Pt
U-IAA-278 Pt-metal in dilute HCl, 1000 µg/mL 100 mL
Potassium - K
U-IAA-219 K in dilute HNO3, 1000 µg/mL 100 mL
Praseodymium - Pr
U-IAA-259 Pr in dilute HNO3, 1000 µg/mL 100 mL
Rhenium - Re
U-IAA-275 Re-metal in H2O, 1000 µg/mL 100 mL
Rhodium - Rh
U-IAA-245 Rh in dilute HCl, 1000 µg/mL 100 mL
Rubidium - Rb
U-IAA-237 Rb in dilute HNO3, 1000 µg/mL 100 mL
Ruthenium - Ru
U-IAA-244 Ru in dilute HCl 100 mL
Samarium - Sm
U-IAA-262 Sm in dilute HNO3, 1000 µg/mL 100 mL
Scandium - Sc
U-IAA-221 Sc in dilute HNO3, 1000 µg/mL 100 mL
Selenium - Se
U-IAA-234 Se in dilute HNO3, 1000 µg/mL 100 mL
Silicon - Si
U-IAA-214 Si in water, 1000 µg/mL 100 mL
Silver - Ag
U-IAA-247 Ag in dilute HNO3, 1000 µg/mL 100 mL
Sodium - Na
U-IAA-211 Na in dilute HNO3, 1000 µg/mL 100 mL
Strontium - Sr
U-IAA-238 Sr in dilute HNO3, 1000 µg/mL 100 mL
Standards for spectroscopy
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Code Product Unit
Sulphur - S
U-IAA-216 S in water, 1000 µg/mL 100 mL
Tantalum - Ta
U-IAA-273 Ta in trace HF, 1000 µg/mL 100 mL
Tellurium - Te
U-IAA-252 Te in dilute HCl 1000 µg/mL 100 mL
Terbium - Tb
U-IAA-265 Tb in dilute HNO3, 1000 µg/mL 100 mL
Thallium - Tl
U-IAA-281 Tl in dilute HNO3, 1000 µg/mL 100 mL
Thorium - Th
U-IAA-290 Th in dilute HNO3, 1000 µg/mL 100 mL
Thulium - Tm
U-IAA-269 Tm in dilute HNO3, 1000 µg/mL 100 mL
Tin - Sn
U-IAA-250 Sn in water, 1000 µg/mL 100 mL
Titanium - Ti
U-IAA-222 Ti in water with trace HF, 1000 µg/mL 100 mL
Tungsten - W
U-IAA-274 W in dilute HNO3 with trace NH4OH, 1000 µg/mL 100 mL
Uranium - U
U-IAA-292 U in dilute HNO3, 1000 µg/mL 100 mL
Vanadium - V
U-IAA-223 V in dilute HNO3, 1000 µg/mL 100 mL
Ytterbium - Yb
U-IAA-270 Yb in dilute HNO3, 1000 µg/mL 100 mL
Yttrium - Y
U-IAA-239 Y in dilute HNO3, 1000 µg/mL 100 mL
Zinc -Zn
U-IAA-230 Zn in dilute HNO3, 1000 µg/mL 100 mL
Zirconium - Zr
U-IAA-240 Zr in dilute HNO3, 1000 µg/mL 100 mL
Standards for spectroscopy
140 Edition 2003/2004 www.lgcpromochem.com
Code Product Unit
ULTRA Scientific's EnviroConcentratesTM for atomic absorption spectroscopy
ULTRA Scientific’s AA EnviroConcentratesTM consist of a 10 mL bottle of the selected element at aconcentration of 10000 µg/mL. Simply pipette the required amount of EnviroConcentrate and dilute tovolume. Standards are traceable to NIST Standard Reference Materials® whenever possible.
Aluminum - Al
U-IAA-013 Al in dilute HNO3, 10000 µg/mL 10 mL
Antimony - Sb
U-IAA-051 Sb in dilute HNO3, 10000 µg/mL 10 mL
Arsenic - As
U-IAA-033 As in dilute HNO3, 10000 µg/mL 10 mL
Barium - Ba
U-IAA-056 Ba in dilute HNO3, 10000 µg/mL 10 mL
Beryllium - Be
U-IAA-004 Be in dilute HNO3, 10000 µg/mL 10 mL
Bismuth - Bi
U-IAA-083 Bi in dilute HNO3, 10000 µg/mL 10 mL
Boron - B
U-IAA-005 B in water with trace NH4OH, 10000 µg/mL 10 mL
Cadmium - Cd
U-IAA-048 Cd in dilute HNO3, 10000 µg/mL 10 mL
Calcium - Ca
U-IAA-020 Ca in dilute HNO3, 10000 µg/mL 10 mL
Cerium - Ce
U-IAA-058 Ce in dilute HNO3, 10000 µg/mL 10 mL
Cesium - Cs
U-IAA-055 Cs in dilute HNO3, 10000 µg/mL 10 mL
Chromium - Cr
U-IAA-024 Cr in dilute HNO3, 10000 µg/mL 10 mL
Cobalt - Co
U-IAA-027 Co in dilute HNO3, 10000 µg/mL 10 mL
Copper - Cu
U-IAA-029 Cu in dilute HNO3, 10000 µg/mL 10 mL
Dysprosium - Dy
U-IAA-066 Dy in dilute HNO3, 10000 µg/mL 10 mL
Erbium - Er
U-IAA-068 Er in dilute HNO3, 10000 µg/mL 10 mL
Standards for spectroscopy
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Code Product Unit
Europium - Eu
U-IAA-063 Eu in dilute HNO3, 10000 µg/mL 10 mL
Gadolinium - Gd
U-IAA-064 Gd in dilute HNO3, 10000 µg/mL 10 mL
Gallium - Ga
U-IAA-031 Ga in dilute HNO3, 10000 µg/mL 10 mL
Germanium - Ge
U-IAA-032 Ge in water with trace HF, 10000 µg/mL 10 mL
Holmium - Ho
U-IAA-067 Ho in dilute HNO3, 10000 µg/mL 10 mL
Indium - In
U-IAA-049 In in dilute HNO3, 10000 µg/mL 10 mL
Iron - Fe
U-IAA-026 Fe in dilute HNO3, 10000 µg/mL 10 mL
Lanthanum - La
U-IAA-057 La in dilute HNO3, 10000 µg/mL 10 mL
Lead - Pb
U-IAA-082 Pb in dilute HNO3, 10000 µg/mL 10 mL
Lithium -Li
U-IAA-003 Li in dilute HNO3, 10000 µg/mL 10 mL
Magnesium - Mg
U-IAA-012 Mg in dilute HNO3, 10000 µg/mL 10 mL
Manganese - Mn
U-IAA-025 Mn in dilute HNO3, 10000 µg/mL 10 mL
Mercury - Hg
U-IAA-080 Hg in dilute HNO3, 10000 µg/mL 10 mL
Molybdenum - Mo
U-IAA-042 Mo in water with trace NH4OH, 10000 µg/mL 10 mL
Neodymium - Nd
U-IAA-060 Nd in dilute HNO3, 10000 µg/mL 10 mL
Nickel - Ni
U-IAA-028 Ni in dilute HNO3, 10000 µg/mL 10 mL
Niobium - Nb
U-IAA-041 Nb in water with trace HF, 10000 µg/mL 10 mL
Phosphorus - P
U-IAA-015 P in dilute HNO3, 10000 µg/mL 10 mL
Standards for spectroscopy
142 Edition 2003/2004 www.lgcpromochem.com
Code Product Unit
Potassium - K
U-IAA-019 K in dilute HNO3, 10000 µg/mL 10 mL
Praseodymium - Pr
U-IAA-059 Pr in dilute HNO3, 10000 µg/mL 10 mL
Samarium - Sm
U-IAA-062 Sm in dilute HNO3, 10000 µg/mL 10 mL
Selenium - Se
U-IAA-034 Se in dilute HNO3, 10000 µg/mL 10 mL
Silicon - Si
U-IAA-014 Si in water, 10000 µg/mL 10 mL
Silver - Ag
U-IAA-047 Ag in dilute HNO3, 10000 µg/mL 10 mL
Sodium - Na
U-IAA-011 Na in dilute HNO3, 10000 µg/mL 10 mL
Strontium - Sr
U-IAA-038 Sr in dilute HNO3, 10000 µg/mL 10 mL
Sulphur - S
U-IAA-016 S in water, 10000 µg/mL 10 mL
Tantalum - Ta
U-IAA-073 Ta in water with trace HF, 10000 µg/mL 10 mL
Tellurium - Te
U-IAA-052 Te in dilute HCl, 10000 µg/mL 10 mL
Terbium - Tb
U-IAA-065 Tb in dilute HNO3, 10000 µg/mL 10 mL
Thallium - Tl
U-IAA-081 Tl in dilute HNO3, 10000 µg/mL 10 mL
Thorium - Th
U-IAA-090 Th in dilute HNO3, 10000 µg/mL 10 mL
Tin - Sn
U-IAA-050 Sn in water, 10000 µg/mL 10 mL
Titanium - Ti
U-IAA-022 Ti in water with trace HF, 10000 µg/mL 10 mL
Tungsten - W
U-IAA-074 W in dilute HNO3 with trace NH4OH, 10000 µg/mL 10 mL
Uranium - U
U-IAA-092 U in dilute HNO3, 10000 µg/mL 10 mL
Standards for spectroscopy
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Code Product Unit
Vanadium - V
U-IAA-023 V in dilute HNO3, 10000 µg/mL 10 mL
Ytterbium - Yb
U-IAA-070 Yb in dilute HNO3, 10000 µg/mL 10 mL
Yttrium - Y
U-IAA-039 Y in dilute HNO3, 10000 µg/mL 10 mL
Zinc - Zn
U-IAA-030 Zn in dilute HNO3, 10000 µg/mL 10 mL
Zirconium - Zr
U-IAA-040 Zr in dilute HNO3,10000 µg/mL 10 mL
Multielement standards
144 Edition 2003/2004 www.lgcpromochem.com
Multielement standardsCode Product Unit
U-IQC-007 Inorganic Quality Control Standard 17 analytes in 5% HNO3
Aluminum.................. 100 µg/mL Potassium ...............1000 µg/mL Sodium...................... 100 µg/mLBarium ...................... 100 µg/mL Silicon..........................50 µg/mLBoron ........................ 100 µg/mL Silver .........................100 µg/mL
100 mL
U-IQC-019 Inorganic Quality Control Standard 219 analytes each at 100 µg/mL in dilute HNO3
Antimony Chromium Magnesium ThalliumArsenic Cobalt Manganese TitaniumBeryllium Copper Molybdenum VanadiumCadmium Iron Nickel ZincCalcium Lead Selenium
100 mL
U-IQC-026 Combined Quality Control Standard26 analytes in dilute HNO3
Aluminum.................. 100 µg/mL Beryllium....................100 µg/mL Manganese ............... 100 µg/mLBarium ...................... 100 µg/mL Cadmium...................100 µg/mL Molybdenum ............. 100 µg/mLBoron ........................ 100 µg/mL Calcium .....................100 µg/mL Nickel ........................ 100 µg/mLPotassium............... 1000 µg/mL Chromium..................100 µg/mL Selenium................... 100 µg/mLSilicon ......................... 50 µg/mL Cobalt ........................100 µg/mL Thallium .................... 100 µg/mLSilver......................... 100 µg/mL Copper.......................100 µg/mL Titanium.................... 100 µg/mLSodium...................... 100 µg/mL Iron ............................100 µg/mL Vanadium.................. 100 µg/mLAntimony................... 100 µg/mL Lead ..........................100 µg/mL Zinc ........................... 100 µg/mLArsenic...................... 100 µg/mL Magnesium................100 µg/mL
100 mL
EPA Method 200.7
U-ICM-231 EPA Method 200.7 Mixed Calibration Standard I10 Analytes in 2% HNO3
Antimony..................... 50 µg/mL Cadmium.....................20 µg/mL Selenium..................... 50 µg/mLArsenic...................... 100 µg/mL Calcium .....................100 µg/mL Silver............................. 5 µg/mLBarium ........................ 10 µg/mL Copper.........................20 µg/mLBoron .......................... 20 µg/mL Manganese..................20 µg/mL
100 mL
U-ICM-232 EPA Method 200.7 Mixed Calibration Standard II5 Analytes in 2% HNO3
Lithium ........................ 50 µg/mL Potassium .................200 µg/mL Strontium .................... 10 µg/mLMolybdenum ............. 100 µg/mL Sodium ......................100 µg/mL
100 mL
U-ICM-233 EPA Method 200.7 Mixed Calibration Standard III3 Analytes in 2% HNO3
Cobalt ......................... 20 µg/mL Phosphorus ...............100 µg/mL Vanadium.................... 20 µg/mL
100 mL
U-ICM-234 EPA Method 200.7 Mixed Calibration Standard IV5 Analytes in 2% HNO3
Aluminum.................. 100 µg/mL Silicon........................100 µg/mL Zinc ............................. 50 µg/mLChromium ................... 50 µg/mL Tin ...............................40 µg/mL
100 mL
U-ICM-235 EPA Method 200.7 Mixed Calibration Standard V6 Analytes in 2% HNO3
Beryllium ..................... 10 µg/mL Lead ..........................100 µg/mL Nickel .......................... 20 µg/mLIron............................ 100 µg/mL Magnesium................100 µg/mL Thallium ...................... 50 µg/mL
100 mL
U-ICM-642 TCLP Mercury StandardMercury ..................................20 µg/mL in 2% HNO3
100 mL
U-ICK-230A EPA Method 200.7 Calibration KitEach kit contains 100 mL of each of the following standards
ICM-231 ICM-233 ICM-235ICM-232 ICM-234 ICM-642
Kit
Multielement standards
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Code Product Unit
U-ICM-240 EPA Method 200.7 LPC Solution30 Analytes in 2% HNO3
Aluminum.................... 20 µg/mL Copper.........................20 µg/mL Potassium................. 100 µg/mLAntimony..................... 20 µg/mL Iron ..............................20 µg/mL Selenium..................... 20 µg/mLArsenic........................ 20 µg/mL Lead ............................20 µg/mL Silicon ....................... 100 µg/mLBarium ........................ 20 µg/mL Lithium.........................20 µg/mL Silver............................. 5 µg/mLBeryllium ..................... 20 µg/mL Magnesium..................20 µg/mL Sodium........................ 20 µg/mLBoron .......................... 20 µg/mL Manganese..................20 µg/mL Strontium .................... 20 µg/mLCadmium .................... 20 µg/mL Mercury........................20 µg/mL Thallium ...................... 20 µg/mLCalcium....................... 20 µg/mL Molybdenum................20 µg/mL Tin............................... 20 µg/mLChromium ................... 20 µg/mL Nickel ..........................20 µg/mL Vanadium.................... 20 µg/mLCobalt ......................... 20 µg/mL Phosphorus ...............100 µg/mL Zinc ............................. 20 µg/mL
100 mL
U-ICM-245 EPA Method 200.7 Lab Fortifying Stock Solution26 Analytes in 2% HNO3
Aluminum.................... 25 µg/mL Copper.........................25 µg/mL Selenium..................... 25 µg/mLAntimony..................... 25 µg/mL Iron ..............................25 µg/mL Silicon ......................... 25 µg/mLArsenic........................ 25 µg/mL Lead ............................25 µg/mL Silver.......................... 2.5 µg/mLBarium ........................ 25 µg/mL Lithium.........................25 µg/mL Strontium .................... 25 µg/mLBeryllium ....................... 5 µg/mL Manganese..................25 µg/mL Thallium ...................... 25 µg/mLBoron .......................... 25 µg/mL Mercury..........................5 µg/mL Tin............................... 10 µg/mLCadmium .................... 10 µg/mL Molybdenum................10 µg/mL Vanadium.................... 10 µg/mLChromium ................... 25 µg/mL Nickel ..........................25 µg/mL Zinc ............................. 25 µg/mLCobalt ......................... 10 µg/mL Phosphorus .................50 µg/mL
100 mL
U-ICM-241 EPA Method 200.7 SIC Solution IMolybdenum ..........................50 µg/mL in 2% HNO3
100 mL
U-ICM-242 EPA Method 200.7 SIC Solution II5 Analytes in 2% HNO3
Chromium ................... 20 µg/mL Copper.........................40 µg/mL Vanadium.................... 20 µg/mLCobalt ......................... 10 µg/mL Manganese..................20 µg/mL
100 mL
U-ICM-243 EPA Method 200.7 SIC Solution III3 Analytes in 2% HNO3
Aluminum.................... 30 µg/mL Iron ............................150 µg/mL Nickel .......................... 20 µg/mL
100 mL
U-ICM-237 EPA Method 200.7 Plasma Solution4 Analytes in 2% HNO3
Arsenic........................ 10 µg/mL Selenium .....................10 µg/mLLead............................ 10 µg/mL Thallium.......................10 µg/mL
100 mL
U-ICM-238 EPA Method 200.7 Tuning Solution2 Analytes in 2% HNO3
Copper ........................ 10 µg/mL Lead ............................10 µg/mL
100 mL
U-ICP-051 Sb-metal in dilute HNO3/C4H6O6, 1000 µg/mL 100 mL
U-ICM-202 EPA Method 200.7 Calibration Standard #1B5 Analytes in 5% HNO3
Arsenic.................... 1000 µg/mL Lead ........................1000 µg/mL Thallium .................. 1000 µg/mLCadmium .................. 500 µg/mL Selenium ...................500 µg/mL
100 mL
U-ICM-203 EPA Method 200.7 Calibration Standard #27 Analytes in 2% HNO3
Barium ...................... 100 µg/mL Copper.......................100 µg/mL Vanadium.................. 100 µg/mLBeryllium ................... 100 µg/mL Iron ..........................1000 µg/mLCobalt ....................... 200 µg/mL Manganese................100 µg/mL
100 mL
U-ICM-204 EPA Method 200.7 Calibration Standard #33 Analytes in water with trace hydrofluoric acid
Boron ........................ 100 µg/mL Molybdenum............1000 µg/mL Silicon ..................... 1000 µg/mL
100 mL
U-ICM-205 EPA Method 200.7 Calibration Standard #49 Analytes in 5% HNO3
Aluminum................ 1000 µg/mL Magnesium..............1000 µg/mL Silver......................... 500 µg/mLCalcium................... 1000 µg/mL Nickel ........................500 µg/mL Sodium.................... 1000 µg/mLChromium ................. 500 µg/mL Potassium ...............1000 µg/mL Zinc ........................... 500 µg/mL
100 mL
U-ICP-022 (NH4)2TiF6 dilute HNO3, 1000 µg/mL 100 mL
U-ICP-028 Ni(NO3)2 in dilute HNO3, 1000 µg/mL 100 mL
Multielement standards
146 Edition 2003/2004 www.lgcpromochem.com
Code Product Unit
U-ICM-221 EPA Method 200.7 Interference Check Std #14 Analytes in water with trace hydrofluoric acid
Boron ........................ 500 µg/mL Silicon........................230 µg/mLMolybdenum ............. 300 µg/mL Titanium ..................1000 µg/mL
50 mL
U-ICM-223 Interference Check Std #316 Analytes in 5% HNO3
Arsenic.................... 1000 µg/mL Copper.......................300 µg/mL Silver......................... 300 µg/mLBarium ...................... 300 µg/mL Lead ........................1000 µg/mL Thallium .................. 1000 µg/mLBeryllium ................... 100 µg/mL Manganese................200 µg/mL Vanadium.................. 300 µg/mLCadmium .................. 300 µg/mL Nickel ........................300 µg/mL Zinc ........................... 300 µg/mLChromium (III) ........... 300 µg/mL Potassium .............20000 µg/mL ~ob~Cobalt ....................... 300 µg/mL Selenium ...................500 µg/mL
50 mL
U-ICM-224 Interference Check Std #45 Analytes in 2% HNO3
Aluminum................ 3000 µg/mL Iron ........................12500 µg/mL Sodium.................... 2500 µg/mLCalcium................. 15000 µg/mL Magnesium..............7500 µg/mL
100 mL
U-ICP-051 Sb-metal in dilute HNO3/C4H6O6, 1000 µg/mL 100 mL
U-ICM-211 EPA Method 200.7 Spiking Standard #13 Analytes in water with trace hydrofluoric acid
Boron ........................ 500 µg/mL Molybdenum..............500 µg/mL Silicon ..................... 2000 µg/mL
50 mL
U-ICM-212 EPA Method 200.7 Spiking Standard #24 Analytes in 5% HNO3
Calcium................... 1000 µg/mL Potassium .............10000 µg/mLMagnesium ............. 2000 µg/mL Sodium ....................3000 µg/mL
50 mL
U-ICM-213 EPA Method 200.7 Spiking Standard #312 Analytes in 5% HNO3
Aluminum................ 2000 µg/mL Cobalt ........................500 µg/mL Nickel ........................ 500 µg/mLBarium .................... 2000 µg/mL Copper.......................250 µg/mL Silver........................... 50 µg/mLBeryllium ..................... 50 µg/mL Iron ..........................1000 µg/mL Vanadium.................. 500 µg/mLChromium ................. 200 µg/mL Manganese................500 µg/mL Zinc ........................... 500 µg/mL
50 mL
U-ICM-215 EPA Method 200.7 Spiking Standard #55 Analytes in 5% HNO3
Arsenic...................... 800 µg/mL Lead ........................1000 µg/mL Thallium .................. 1000 µg/mLCadmium .................. 100 µg/mL Selenium .................1000 µg/mL
50 mL
EPA Method 6010A
U-ICM-601 EPA Method 6010A Mixed Standard Solution I6 Analytes in 2% HNO3
Beryllium ..................... 50 µg/mL Lead ..........................500 µg/mL Selenium................... 200 µg/mLCadmium .................. 150 µg/mL Manganese................100 µg/mL Zinc ........................... 150 µg/mL
100 mL
U-ICM-602 EPA Method 6010A Mixed Standard Solution II5 Analytes in 2% HNO3
Barium ...................... 100 µg/mL Copper.......................100 µg/mL Vanadium.................. 100 µg/mLCobalt ....................... 100 µg/mL Iron ........................10000 µg/mL
100 mL
U-ICM-603 EPA Method 6010A Mixed Standard Solution III2 Analytes in 2% HNO3
Arsenic...................... 500 µg/mL Molybdenum..............100 µg/mL
100 mL
U-ICM-604 EPA Method 6010A Mixed Standard Solution IV8 Analytes in 2% HNO3
Aluminum.................. 200 µg/mL Lithium.......................100 µg/mL Sodium...................... 200 µg/mLCalcium................... 1000 µg/mL Nickel ..........................20 µg/mL Strontium .................... 10 µg/mLChromium ................... 20 µg/mL Potassium .................400 µg/mL
100 mL
U-ICM-605 EPA Method 6010A Mixed Standard Solution V4 Analytes in 2% HNO3
Antimony................... 200 µg/mL Silver ...........................50 µg/mLMagnesium ............. 1000 µg/mL Thallium.....................200 µg/mL
100 mL
Multielement standards
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Code Product Unit
U-ICM-607 EPA Method 6010A Mixed Standard Solution IIa5 Analytes in 2% HNO3
Barium ...................... 100 µg/mL Copper.......................100 µg/mL Vanadium.................. 100 µg/mLCobalt ....................... 100 µg/mL Iron ..........................1000 µg/mL
500 mL
U-ICP-015 NH4H2PO4 in dilute HNO3, 1000 µg/mL 100 mL
U-ICM-611 EPA Method 6010A Interference Check Std I5 Analytes in 2% HNO3 with trace hydrofluoric acid
Lithium ...................... 300 µg/mL Phosphorus .............1000 µg/mL Titanium.................. 1000 µg/mLMolybdenum ............. 300 µg/mL Strontium...................200 µg/mL
100 mL
U-ICP-051 Sb-metal in dilute HNO3/C4H6O6, 1000 µg/mL 100 mL
U-ICM-223 Interference Check Std #316 Analytes in 5% HNO3
Arsenic.................... 1000 µg/mL Copper.......................300 µg/mL Silver......................... 300 µg/mLBarium ...................... 300 µg/mL Lead ........................1000 µg/mL Thallium .................. 1000 µg/mLBeryllium ................... 100 µg/mL Manganese................200 µg/mL Vanadium.................. 300 µg/mLCadmium .................. 300 µg/mL Nickel ........................300 µg/mL Zinc ........................... 300 µg/mLChromium (III) ........... 300 µg/mL Potassium .............20000 µg/mL ~ob~Cobalt ....................... 300 µg/mL Selenium ...................500 µg/mL
50 mL
U-ICM-224 Interference Check Std #45 Analytes in 2% HNO3
Aluminum................ 3000 µg/mL Iron ........................12500 µg/mL Sodium.................... 2500 µg/mLCalcium................. 15000 µg/mL Magnesium..............7500 µg/mL
100 mL
Standards for ICP/MS
U-IMS-102 ICP/MS Calibration Standard #229 Analytes , 10 µg/mL of each analyte in 5% HNO3
Aluminum Chromium Magnesium StrontiumArsenic Cobalt Manganese ThalliumBarium Copper Nickel uraniumBeryllium Gallium Potassium VanadiumBismuth Indium Rubidium ZincCadmium Iron SeleniumCalcium, Lead SilverCesium Lithium Sodium
100 mL
U-IMS-103 ICP/MS Calibration Standard #310 Analytes, 10 µg/mL of each analyte 10% HCl
Antimony Iridium Rhodium TinGold Palladium RutheniumHafnium Platinum Tellurium
100 mL
U-IMS-104 ICP/MS Calibration Standard #412 Analytes, 10 µg/mL of each analyte in water
Boron Niobium Silicon TitaniumGermanium Phosphorus Sulfur TungstenMolybdenum Rhenium Tantalum Zirconium
100 mL
U-IMS-105 ICP/MS Calibration Standard #5Mercury ..................................10 µg/mL in 5% HNO3
100 mL
U-IMS-110 ICP/MS Tuning Solution5 Analytes, 10 µg/mL of each analyte 2% HNO3
Beryllium Indium MagnesiumCobalt Lead
100 mL
U-IMS-111 ICP/MS Internal StandardBismuth................................100 µg/mL in 2% HNO3
100 mL
U-IMS-112 ICP/MS Internal StandardIndium ..................................100 µg/mL in 2% HNO3
100 mL
U-IMS-113 ICP/MS Internal StandardScandium.............................100 µg/mL in 2% HNO3
100 mL
U-IMS-114 ICP/MS Internal StandardTerbium................................100 µg/mL in 2% HNO3
100 mL
Ion chromatography standards
148 Edition 2003/2004 www.lgcpromochem.com
Code Product Unit
U-IMS-115 ICP/MS Internal StandardYttrium .................................100 µg/mL in 2% HNO3
100 mL
U-IMS-100 ICP/MS Verification Standard9 Analytes, 10 µg/mL in 2% HNO3
Beryllium Cobalt MagnesiumBismuth Indium NickelCerium Lead Uranium
100 mL
Ion chromatography standards
Anions
Code Product Unit
ULTRA Scientific standards and NIST SRMs® are solutions prepared gravimetrically for use in ionchromatography or other techniques that require aqueous standard solutions for calibration.
The standards from ULTRA Scientific are traceable to NIST Standard Reference Materials® (SRM®)wherever possible.
U-ICC-001 Bromide (Br -), 1000 µg/mL 100 mL
NIST-3182 Chloride (Cl -), 1000 mg/kg 50 mL
U-ICC-002 Chloride (Cl -), 1000 µg/mL 100 mL
NIST-3183 Fluoride (F -), 1000 mg/kg 50 mL
U-ICC-003 Fluoride (F -), 1000 µg/mL 100 mL
NIST-3185 Nitrate (NO3-), 1000 mg/kg 5 x 10 mL
U-ICC-004 Nitrate (NO3-), 1000 µg/mL 100 mL
U-ICC-007 Nitrite (NO2-), 1000 µg/ml 100 mL
NIST-3186 Phoshate (PO43-), 1000 mg/kg 5 x 10 mL
U-ICC-005 Phoshate (PO43-), 1000 µg/mL 100 mL
NIST-3181 Sulfate (SO42-), 1000 mg/kg 5 x 10 mL
U-ICC-006 Sulfate (SO42-), 1000 µg/mL 100 mL
U-ICC-010 Bromate (BrO3-) 1000 µg/mL in water 100 mL
U-ICC-011 Chlorate (ClO3-) 1000 µg/mL in water 100 mL
U-ICC-012 Chlorite (ClO2-) 1000 µg/mL in water 100 mL
U-ICC-013 Perchlorate (ClO4-) 1000 µg/mL in water 100 mL
Anion mixtures for ion chromatography
U-ICC-200 IC Anions Mixture 1Solvent : Water
Chloride (Cl-)............... 30 µg/mL Nitrate (NO32-)............100 µg/mL Sulfate (SO4
2-)........... 150 µg/mLFluoride (F-)................. 20 µg/mL Phosphate (PO4
3-) .....150 µg/mL
100 mL
U-ICC-210 IC Anions Mixture 2Solvent : Water
Bromide .................... 400 µg/mL Fluoride (F-) ...............100 µg/mL Phosphate (PO43-)..... 600 µg/mL
Chloride (Cl-)............. 200 µg/mL Nitrate (NO32-)............400 µg/mL Sulfate (SO4
2-)........... 400 µg/mL
100 mL
Ion chromatography standards
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Code Product Unit
Cations
U-ICC-101 Ammonium (NH4+), 1000 µg/mL 100 mL
U-ICC-102 Barium (Ba2+), 1000 µg/mL 100 mL
U-ICC-103 Calcium (Ca2+), 1000 µg/mL 100 mL
U-ICC-104 Lithium (Li+), 1000 µg/mL 100 mL
U-ICC-105 Magnesium (Mg2+), 1000 µg/mL 100 mL
U-ICC-106 Potassium (K+), 1000 µg/mL 100 mL
U-ICC-107 Sodium (Na+), 1000 µg/mL 100 mL
U-ICC-108 Strontium (Sr2+), 1000 µg/mL 100 mL
Cation mixtures for ion chromatography
U-ICC-300 IC Cations Mixture 1Solvent: 2% HNO3
Ammonium (NH4+) .... 400 µg/mL Lithium (Li+) .................50 µg/mL Potassium (K+).......... 200 µg/mL
Calcium (Ca2+) ........ 1000 µg/mL Magnesium (Mg2+).....200 µg/mL Sodium (Na+) ............ 200 µg/mL
100 mL
U-ICC-310 IC Cations Mixture 2Solvent: 0.5% HNO3
Ammonium (NH4+) .... 100 µg/mL Potassium (K+) ............50 µg/mL
Lithium (Li+)................. 10 µg/mL Sodium (Na+).............100 µg/mL
100 mL
U-ICC-320 IC Cations Mixture 3Solvent: 2% HNO3
Barium (Ba2+).......... 1600 µg/mL Magnesium (Mg2+).....200 µg/mLCalcium (Ca2+) ........ 1000 µg/mL Strontium (Sr2+) .........600 µg/mL
100 mL
CERTAN® - The ampoule in the bottle
150 Edition 2003/2004 www.lgcpromochem.com
CERTAN® - The ampoule in the bottleThe CERTAN® capillary bottle is sample container with a capillary-opening. It has been specificallydeveloped for use with and storage of reference solutions. Using the CERTAN® bottle the problemsof storing volatile solutions become a thing of the past. Unopened glass ampoules provide an efficientway of storing volatile standards, but once opened are impossible to reseal and are unsuitable forfurther storage. The use of screw cap bottles for volatile standards invariably leads to losses by virtueof their construction. There is also a higher risk of contamination from the cap itself and from theinsert within the cap.
CERTAN® is the solution for solutions!
CERTAN® Advantages
- No change in concentration of standard solutions even when open- Totally secure storage, free of losses- Minimised risk of contamination- The filling and removal of aliquots can be easily achieved using a standard GC syringe- Proven usability from -30°C to +50°C- Serial filling is easy with an auto diluter- Almost impossible to spill.
CERTAN® Application Examples
- Supply and storage of LGC Promochem standard solutions- Storage of standard solutions removed from conventional glass ampoules- Storage of working stock and standard solutions- Storage of difficult samples, such as volatile halogen compounds or BTEX aromatics- Archiving of production samples and extracts- Transport and storage of ringtest samples.
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CERTAN® Principle
The properties of the patented CERTAN® capillary bottle depend on the unique way in which the glassbottle, capillary and screw cap closures have been engineered. The 1.2 mm diameter and 28 mm longcapillary works as a re-condensation zone for any of solvent vaporous. Reducing the surface areainside the cap ensures a more efficient sealing of the bottle. It also minimizes the chance ofcontamination by the cap insert.
The CERTAN® capillary bottles combines the advantages of a sealed ampoule with the flexibility of ascrew cap bottle or a septum vial.Storage tests on CERTAN® bottles at room temperature showed that after 15 months the loss byevaporation from the CERTAN® bottle was much lower then the loss by evaporation on opening aflame sealed ampoule. Both cap and insert have been manufactured in materials which have beentested to ensure they retain their sealing properties, even with such critical solvents such asDiethylether.
CERTAN® Cleaning Protocol
The CERTAN bottle can be easily cleaned using the following method:A 0.53 mm quartz capillary is inserted into the CERTAN® bottle which is then inverted over a solventcontainer similar to a wash bottle. (Refer to illustration below). Dry nitrogen from a standard gascylinder pressurizes the container forcing the cleaning solvent up the capillary tube spraying the insideof the bottle and hence thorough cleaning of the bottle should be achieved. The capillary of theCERTAN® bottle itself is simply cleaned by the action of the cleaning solvent draining through. Testsusing different cleaning solvents showed that Toluene was the most effective solvent in cleaning theCERTAN® bottles.
Once the cleaning process is complete and the cleaning solvents, is all used up, the CERTAN® bottleshould be dried by flushing with nitrogen and finally placed in a suitable flame proof oven at 400 °C forat least two hours.
Please note that the CERTAN® capillary bottles are gamma-irradiated to obtain the brown colour.However, at a temperature above 270 °C the brown colour will disappear without leaving anyresidues.
CERTAN® bottle
quartz capillary
container for used solvents
dry Nitrogen
wash bottle with solvent
152 Edition 2003/2004 www.lgcpromochem.com
Advice
The manufacturing process of the CERTAN® bottle, ensures that as far as possible the bottles arefree of any chemical contamination. However it would be good practice to rinse the bottles out with thesame solvent in which your standards are dissolved in. The bottle should also be checked for anyminute glass particles which may occasionally be found, these can be easily flushed out using drynitrogen which has been passed through an activated charcoal filter. In the same way the bottle canbe dried after rinsing with the appropriate solvent.
Care should be taken when removing aliquots from the CERTAN® bottle, ensure that there are nodroplets adhering to the end of the needle.
Prior to opening a full CERTAN® bottle, check to see if a small column of the solution has migratedinto the capillary, if so this can be returned to the bottle easily by a quick flick of the wrist, as youwould mercury in clinical thermometer.
When replacing the cap onto the CERTAN® bottle, it should be firmly tightened so that the top of thecapillary leaves a clear indentation on the insert of the cap.
We also recommend that with new CERTAN® bottles the cap be re-tightened after 30 minutes to takeup any slack caused by the initial indentation on the insert.
The CERTAN® bottle is manufactured out of high quality Duran glass, and robust in its construction.However, care should be taken when handling to avoid dropping onto hard surfaces.
CERTAN®-The ampoule in the bottle
Code Product Unit
DE-CE 01 CERTAN capillary bottle (10 x 1.5 mL) set
DE-CE 05 CERTAN capillary bottle (5 x 4.5 mL) set
DE-CE 10 CERTAN capillary bottle (5 x 10 mL) set
Racks for CERTAN®
DE-MIG 13 10 place rack for DE-CE 01 unit
DE-MIG 17 10 place rack for DE-CE 05 unit
DE-MIG 19 10 place rack for DE-CE 10 unit
DE-ENG 416 Plastic shipping container for single DE-CE 01 / DE-CE 05 bottle unit
DE-ENG 484 Plastic shipping container for single DE-CE 10 bottle unit
CERTAN® wash-bottle
DE-WB 1000 CERTAN wash bottle incl. capillary each
Trademarks
CERTAN® - LGC Promochem GmbH
BCR® - IRMM (Institute for Reference Materials and Measurement)
EnviroConcentratesTM- ULTRA Scientific, Inc.
Standard Reference Materials®, SRMs® - NIST National Institute of Standards and Technology
CONOSTAN® - Conoco Inc.
Code number index
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Codenumberindex
ARC/CL1 ....................14ARC/CL2 ....................50ARC/CL4 ....................36BCR-010.....................86BCR-017A ..................99BCR-017B ..................99BCR-022A ................100BCR-022B ................100BCR-023A ................100BCR-023B ................100BCR-024B ................100BCR-024C ................100BCR-025A ..................99BCR-025B ..................99BCR-026.....................86BCR-027.....................86BCR-028.....................86BCR-029.....................86BCR-030.....................86BCR-031.....................86BCR-032.....................56BCR-033.....................56BCR-038...................111BCR-054R ................100BCR-055...................100BCR-058...................100BCR-059A ................100BCR-059B ................100BCR-060.....................61BCR-062.....................58BCR-063R ..................13BCR-065.....................64BCR-074A ................101BCR-074B ................101BCR-074C ................101BCR-075A ................101BCR-075B ................101BCR-075C ................101BCR-089...................104BCR-090A ................104BCR-090B ................104BCR-098...................104BCR-099...................100BCR-100.....................58BCR-101.....................58BCR-102...................101BCR-104R ..................68BCR-105.....................68BCR-106.....................68BCR-107.....................68BCR-108.....................86BCR-109.....................86BCR-110.....................86BCR-112...................115BCR-113.....................56BCR-114.....................56BCR-115.....................55BCR-121.....................32BCR-122.....................16BCR-123A ..................42BCR-123B ..................42BCR-126A ..................94BCR-128...................111BCR-129.....................60BCR-150.....................13BCR-151.....................13BCR-163.....................20BCR-178.....................56BCR-179.....................56BCR-180.....................64BCR-181.....................64BCR-182.....................64BCR-184.....................19BCR-185R ..................19BCR-186.....................19BCR-187.....................14
BCR-188 .....................14BCR-189 .....................32BCR-190R ..................34BCR-191 .....................49BCR-262 .....................37BCR-264 .....................37BCR-273 .....................63BCR-274 .....................63BCR-275 ...................100BCR-276 ...................100BCR-278R ..................22BCR-279 .....................61BCR-282 .....................14BCR-283 .....................14BCR-286A.................101BCR-286B.................101BCR-287A.................101BCR-287B.................101BCR-288A.................102BCR-288B.................102BCR-300 (RM) ............94BCR-301 (RM) ............94BCR-302 .....................63BCR-318 ...................100BCR-321 ...................102BCR-322R ................102BCR-323R ................102BCR-324R ................102BCR-325R ................102BCR-326 ...................102BCR-327 ...................102BCR-329 .....................99BCR-330 .....................99BCR-331 .....................64BCR-332 .....................64BCR-333 .....................64BCR-334 .....................64BCR-335 .....................64BCR-336 .....................64BCR-349 .....................28BCR-350 .....................28BCR-351 ...................102BCR-352 ...................103BCR-353 ...................103BCR-354 ...................103BCR-355 ...................103BCR-356 ...................103BCR-357 ...................103BCR-358 ...................103BCR-359 ...................103BCR-360 ...................103BCR-361 ...................104BCR-366R ..................34BCR-367R ..................34BCR-375 .....................55BCR-376 .....................55BCR-377 .....................33BCR-378 .....................33BCR-381 .....................33BCR-382 .....................32BCR-383 .....................36BCR-384 .....................19BCR-395 .....................68BCR-396 .....................33BCR-400 .....................38BCR-401 .....................37BCR-402 .....................61BCR-411 .....................19BCR-412 .....................19BCR-420 .....................68BCR-421 .....................13BCR-422 .....................28BCR-423 (RM) ............39BCR-430 .....................20BCR-431 .....................36BCR-444 .....................21BCR-445 .....................21BCR-446 .....................34BCR-447 .....................34BCR-448 .....................34BCR-449 .....................69BCR-450 .....................14BCR-458 .....................38BCR-459 .....................38
BCR-460 .................... 64BCR-463 .................... 28BCR-464 .................... 28BCR-465 .................... 33BCR-466 .................... 33BCR-467 .................... 34BCR-471 .................... 33BCR-472 .................... 33BCR-474/475 ............. 19BCR-477 .................... 22BCR-482 .................... 63BCR-485 .................... 36BCR-487 .................... 19BCR-490 .................. 111BCR-492-3................. 16BCR-514 .................... 36BCR-515 .................... 36BCR-516 .................... 37BCR-517 .................... 36BCR-518 .................... 49BCR-519 .................... 15BCR-532 (RM) ........... 14BCR-533 (RM) ........... 15BCR-534 (RM) ........... 15BCR-537 .................... 38BCR-538 .................... 38BCR-539 .................... 38BCR-542 .................... 24BCR-543 .................... 24BCR-544 .................. 122BCR-545 .................. 106BCR-546 .................. 116BCR-547 .................. 116BCR-548 .................. 116BCR-549 .................. 116BCR-550 .................. 116BCR-551-2............... 117BCR-553-4............... 115BCR-555 .................. 115BCR-562 .................. 115BCR-563 .................... 32BCR-593 .................... 38BCR-596 .................... 61BCR-598 .................... 28BCR-599 .................... 16BCR-605 .................. 114BCR-607 .................... 15BCR-615 .................. 111BCR-620 .................. 108BCR-621 (RM) ......... 108BCR-623 .................. 108BCR-626 .................. 122BCR-627 .................... 29BCR-648-9................. 19BCR-651 .................... 54BCR-652 .................... 54BCR-653 .................... 54BCR-660 .................... 42BCR-664 .................... 94BCR-668 .................... 22BCR-670 .................... 61BCR-671 .................... 68BCR-672 .................... 68BCR-679 .................... 37BCR-680 .................... 99BCR-681 .................... 99BCR-682 .................... 22BCR-683 .................... 60BCR-691 .................. 101BCR-718 .................... 29BCR-719 .................... 28BCR-723 .................. 114B-MYC0200 ............... 39B-MYC0220 ............... 39B-MYC0240 ............... 39B-MYC0260 ............... 39B-MYC0280 ............... 39B-MYC0300 ............... 40B-MYC0320 ............... 39B-MYC0320-C............ 39B-MYC0340 ............... 39B-MYC0340-C............ 39B-MYC0360 ............... 39B-MYC0360-C............ 39
B-MYC0400................ 39B-MYC0400-C............ 39B-MYC0420................ 39B-MYC0440................ 40B-MYC0480................ 39B-MYC0480-C............ 39B-MYC0490................ 39B-MYC0490-C............ 39B-MYC0500................ 39B-MYC0600................ 40B-MYC0600-C............ 40B-MYC0700................ 40CERERA-011........... 116CERERA-012........... 116CERERA-013K ........ 118CERERA-014........... 116CERERA-020........... 117CERERA-021........... 116CERERA-024S ........ 116CERERA-025S ........ 116CERERA-026S ........ 116CERERA-027S ........ 116CERERA-028........... 117CERERA-029........... 118CERERA-030........... 118CERERA-037........... 118CERERB-016........... 116CERERB-017........... 116CERERB-018........... 116CERERB-023........... 116CERERB-026S ........ 116CERERB-028S ........ 116CERERB-029S ........ 116CERERC-006........... 116CERERC-011S ........ 116CERERC-015S ........ 116CERERC-016........... 116CERERD-030........... 116CERERD-035S ........ 116CERERF-003 ........... 116CERERF-004S......... 116CERERF-005S......... 116CERERG-002 .......... 116CERERH-003........... 116CERERH-005S ........ 116CERERH-011........... 116CERERH-012S ........ 116CERERI-003 ............ 117CERERI-004 ............ 117CERERI-005 ............ 117CERERI-009S.......... 117CERERM-002 .......... 117CERERM-020 .......... 117CERERM-022S........ 117CERERM-023S........ 117CERERM-024 .......... 117CERERP-005........... 117CERERP-030S ........ 117CERERT-007........... 117CERERT-011........... 117CERERT-012........... 117CERERT-027S......... 117CERERV-001........... 117CERERV-002S ........ 117CON-Ag1000 ............. 77CON-Ag5000 ............. 77CON-Al1000............... 75CON-Al5000............... 75CON-AM41000........... 79CON-AM4900............. 79CON-AM81000........... 79CON-AM8900............. 79CON-As100................ 75CON-B1000 ............... 76CON-B5000 ............... 76CON-Ba1000 ............. 75CON-Ba5000 ............. 75CON-Be1000 ............. 75CON-Be5000 ............. 75CON-Bi1000............... 75CON-Bi5000............... 75CON-Ca1000 ............. 76CON-Ca5000 ............. 76CON-Cd1000 ............. 76
CON-Cd5000 ............. 76CON-Cl10................... 80CON-Cl100................. 80CON-Cl1000............... 80CON-Cl10000............. 80CON-Cl500................. 80CON-Cl5000............... 80CON-Cl50000............. 80CON-Cl-blank............. 80CON-Co1000 ............. 76CON-Co5000 ............. 76CON-Cr1000 .............. 76CON-Cr5000 .............. 76CON-Cu1000 ............. 76CON-Cu5000 ............. 76CON-D12810 ............. 83CON-D128100 ........... 83CON-D12830 ............. 83CON-D128300 ........... 83CON-D1285 ............... 83CON-D12850 ............. 83CON-D19 Set ............. 84CON-D19-0 ................ 83CON-D19410 ............. 83CON-D194100 ........... 84CON-D19430 ............. 84CON-D194300 ........... 84CON-D1945 ............... 83CON-D19450 ............. 84CON-D194500 ........... 84CON-D194700 ........... 84CON-D194900 ........... 84CON-D38100 ............. 83CON-EBO2016 .......... 81CON-EBO204 ............ 81CON-EBO7516 .......... 81CON-EBO754 ............ 81CON-Fe1000.............. 76CON-Fe5000.............. 76CON-FTIR-OTSBR .... 82CON-FTIR-OTSPE .... 82CON-Hg100 ............... 76CON-In1000 ............... 76CON-In5000 ............... 76CON-K1000................ 76CON-K5000................ 76CON-La1000 .............. 76CON-La5000 .............. 76CON-Li1000 ............... 76CON-Li5000 ............... 76CON-Mg1000 ............. 76CON-Mg5000 ............. 76CON-Mn1000 ............. 76CON-Mn5000 ............. 76CON-Mo1000 ............. 76CON-Mo5000 ............. 76CON-Na1000 ............. 77CON-Na5000 ............. 77CON-Ni1000............... 76CON-Ni5000............... 76CON-P1000................ 76CON-P5000................ 76CON-Pb1000.............. 76CON-Pb5000.............. 76CON-PS2806 ............. 81CON-PSCK ................ 81CON-PSOLV19.......... 81CON-PSOLV4............ 81CON-PSSCF.............. 81CON-PSUFTD ........... 81CON-PTSM-Set ......... 82CON-PTSQ-Set ......... 82CON-S100.................. 80CON-S1000................ 80CON-S10000.............. 80CON-S12410.............. 78CON-S124100............ 79CON-S12430.............. 78CON-S124300............ 79CON-S12450.............. 78CON-S124500............ 79CON-S124900............ 79CON-S12810.............. 78CON-S128100............ 79
Code number index
154 Edition 2003/2004 www.lgcpromochem.com
CON-S12830 ..............78CON-S128300 ............79CON-S12850 ..............78CON-S128500 ............79CON-S128900 ............79CON-S15000 ..............80CON-S20000 ..............80CON-S21410 ..............77CON-S214100 ............78CON-S21430 ..............77CON-S214300 ............78CON-S21450 ..............78CON-S214500 ............78CON-S214900 ............78CON-S21810 ..............77CON-S218100 ............78CON-S21830 ..............77CON-S218300 ............78CON-S21850 ..............78CON-S218500 ............78CON-S218900 ............78CON-S250 ..................80CON-S2500 ................80CON-S25000 ..............80CON-S30000 ..............80CON-S40000 ..............80CON-S50 ....................80CON-S500 ..................80CON-S5000 ................80CON-S50000 ..............80CON-S750 ..................80CON-S7500 ................80CON-Sb1000 ..............75CON-Sb5000 ..............75CON-Sblank ...............80CON-Sc2000 ..............76CON-Se100 ................76CON-Si1000 ...............76CON-Si5000 ...............77CON-Sn1000 ..............77CON-Sn5000 ..............77CON-Sr1000...............77CON-Sr5000...............77CON-Ti1000 ...............77CON-Ti5000 ...............77CON-V1000 ................77CON-V5000 ................77CON-W1000...............77CON-W5000...............77CON-Y1000 ................77CON-Y5000 ................77CON-Zn1000 ..............77CON-Zn5000 ..............77CSIR-MYC 005 ...........39CSIR-MYC 006 ...........39CSIR-MYC 007 ...........39CSIR-MYC 008 ...........39CSIR-MYC 009 ...........39CSIR-MYC 013 ...........39CSIR-MYC 015 ...........39CSIR-MYC 017 ...........40CSIR-MYC 019 ...........40CSIR-MYC 020 ...........40CSIR-MYC 021 ...........40CSIR-MYC 024 ...........39CSIR-MYC 025 ...........39CSIR-MYC 026 ...........39CSIR-MYC 027 ...........39CSIR-MYC 028 ...........39CSIR-MYC 029 ...........39CSIR-MYC 030 ...........39DE-CE 01 .................152DE-CE 05 .................152DE-CE 10 .................152DE-ENG 416.............152DE-ENG 484.............152DE-MIG 13................152DE-MIG 17................152DE-MIG 19................152DE-WB 1000 ............152EC 1.1.........................96Glass No.4..................96Glass No.5..................96Glass No.6..................96
Glass No.7 ..................96Glass No.8 ..................96IAEA-140OC ...............62IAEA-140TM ...............62IAEA-152 ....................15IAEA-153 ....................14IAEA-154 ....................15IAEA-155 ....................14IAEA-156 ....................61IAEA-303 ..................124IAEA-305 ..................124IAEA-311 ..................124IAEA-321 ....................15IAEA-336 ....................63IAEA-352 ....................31IAEA-359 ....................37IAEA-373 ....................61IAEA-MA-B3/R............31IAEA-RGTh-1..............90IAEA-RGU-1 ...............90IAEA-V-10...................60IAEA-V-8.....................33IAEA-V-9.....................61IBPO002 .....................53IBPO003 .....................53IBPO004 .....................53IBPO005 .....................53IBPO007 .....................53IBPO008 .....................53IBPO009 .....................53IBPO010 .....................53IBPO011 .....................53IBPO012 .....................53IBPO013 .....................53IBPO014 .....................53IBPO015 .....................53IBPO016 .....................53IBPO017 .....................53IC-CTA-FFA-1...........112IC-CTA-OTL1..............59IC-CTA-VTL2..............60IC-INCT-MPH-2 ..........63IC-INCT-TL-1 ........37, 60IPO F 010....................52IPO F 170....................52IRMM-410S0...............35IRMM-410S1...............35IRMM-410S2...............35IRMM-410S3...............35IRMM-410S4...............35IRMM-410S5...............35IRMM-413-0 ................35IRMM-413-1 ................35IRMM-413-2 ................35IRMM-413-3 ................35IRMM-413-4 ................35IRMM-413-5 ................35IRMM-441 ...................71IRMM-442 ...................71IRMM-444 ...................21IRMM-445 ...................21IRMM-446 ...................21LGC3000 ....................68LGC3001 ....................68LGC3002 ....................68LGC3003 ....................68LGC3004 ..................105LGC4000 ..................119LGC4001 ..................119LGC4002 ..................119LGC4003 ..................119LGC4004 ..................119LGC4005 ..................119LGC4006 ..................119LGC4007 ..................119LGC4008 ..................119LGC4009 ..................119LGC5000 ....................54LGC5001 ....................54LGC5002 ....................54LGC5003 ....................54LGC5004 ....................54LGC5005 ....................54LGC5100 ....................54
LGC5404.................... 54LGC5405.................... 54LGC5406.................... 54LGC5407.................... 54LGC5408.................... 54LGC6147.................... 68LGC6180 (RM)......... 111LGC7000.................... 17LGC7001.................... 17LGC7003.................... 32LGC7011.................... 51LGC7012.................... 51LGC7013.................... 51LGC7014.................... 51LGC7015.................... 51LGC7016.................... 49LGC7101.................... 28LGC7103.................... 49LGC7104 (RM)........... 13LGC7105 (RM)........... 49LGC7106 (RM)........... 13LGC7107 (RM)........... 49LGC7111.................... 36LGC7112.................... 17LGC7120 (RM)........... 38LGC7122-23 .............. 38LGC7130.................... 51LGC7131.................... 51LGC7140 (RM)........... 51LGC7150 (RM)........... 17LGC7151 (RM)........... 17LGC7152 (RM)........... 17LGC7160.................... 22LGC7162.............. 36, 62LGC7172 (RM)........... 55LGC7173 (RM)........... 55LGC7176.................... 55LGC7200 (RM)........... 17LGC7201 (RM)........... 17LGC7202 (RM)........... 17LGC7203 (RM)........... 18LGC7204 (RM)........... 18LGC7205 (RM)........... 18LGC7206 (RM)........... 18LGC7207 (RM)........... 18LGC7208 (RM)........... 18LGC7209 (RM)........... 18LGC7300.................... 52LGC7301.................... 52LGC7302.................... 52LGC7305.................... 52LGC9000.................. 105LGC9001.................. 105LGCQC1001 .............. 41LGCQC1002 .............. 41LGCQC1003 .............. 41LGCQC1004 .............. 41LGCQC1005 .............. 41LGCQC1050 .............. 41MURST-ISS-A2.......... 29NAMI A-2 ................. 106NAMI B-2 ................. 106NAMI(5)/A-2 ............. 106NAMI(5)/B-2 ............. 106NIES03....................... 62NIST-1051B ............. 122NIST-1052B ............. 122NIST-1053A ............. 122NIST-1057B ............. 122NIST-1059C............. 122NIST-1060A ............. 122NIST-1065B ............. 122NIST-1066................ 122NIST-1069B ............. 122NIST-1070A ............. 122NIST-1071B ............. 122NIST-1073B ............. 122NIST-1075A ............. 122NIST-1077A ............. 122NIST-1078B ............. 122NIST-1079B ............. 122NIST-1080A ............. 122NIST-1083.................. 72NIST-1084a................ 72
NIST-1085b................ 72NIST-112b.................. 91NIST-120c............ 56, 90NIST-1216................ 120NIST-1411.................. 94NIST-1412.................. 94NIST-1413.................. 95NIST-141D ............... 119NIST-142.................. 119NIST-143D ............... 119NIST-148.................. 119NIST-1515.................. 58NIST-1544.................. 50NIST-1546.................. 20NIST-1547.................. 58NIST-1548a................ 50NIST-1549.................. 13NIST-154c................ 105NIST-1563.................. 38NIST-1566b................ 25NIST-1567a................ 32NIST-1568a................ 34NIST-1570a................ 63NIST-1573a................ 63NIST-1575A ............... 58NIST-1577b................ 19NIST-1580.................. 70NIST-1582.................. 70NIST-1588a................ 29NIST-1616a................ 70NIST-1617a................ 70NIST-1619b................ 70NIST-1620c................ 70NIST-1621e................ 70NIST-1622e................ 70NIST-1623c................ 70NIST-1630A ............... 64NIST-1632c................ 65NIST-1633b.............. 111NIST-1634c................ 69NIST-1635.................. 65NIST-1648................ 113NIST-1649a.............. 114NIST-165a.................. 95NIST-17e.................. 121NIST-180.................... 86NIST-181.................... 86NIST-1815a................ 71NIST-1816a................ 71NIST-1818a................ 69NIST-1819a................ 69NIST-182.................... 86NIST-1829.................. 72NIST-183.................... 87NIST-1830.................. 96NIST-1831.................. 96NIST-1834.................. 96NIST-1835.................. 90NIST-1836.................. 69NIST-1837.................. 72NIST-1838.................. 72NIST-1839.................. 72NIST-1845.................. 49NIST-1846.................. 13NIST-1848.................. 69NIST-1866a.............. 110NIST-1872.................. 98NIST-1873.................. 98NIST-1876b.............. 110NIST-1878a.............. 115NIST-1879a.............. 115NIST-1880a................ 92NIST-1881a................ 92NIST-1882a................ 92NIST-1883a................ 92NIST-1884a................ 92NIST-1885a................ 92NIST-1886a................ 92NIST-1887a................ 93NIST-1888a................ 93NIST-1889a................ 93NIST-193.................... 56NIST-194.................... 56NIST-1946.................. 30
NIST-1975................ 112NIST-198.................... 91NIST-199.................... 91NIST-200a.................. 56NIST-2063a................ 98NIST-2141................ 119NIST-2143................ 120NIST-2144................ 120NIST-2286.................. 72NIST-2287.................. 72NIST-2288.................. 73NIST-2289.................. 73NIST-2290.................. 73NIST-2291.................. 73NIST-2292.................. 73NIST-2293.................. 73NIST-2294.................. 73NIST-2295.................. 73NIST-2296.................. 73NIST-2297.................. 73NIST-2298.................. 70NIST-2299.................. 70NIST-2383.................. 49NIST-2387.................. 16NIST-2430.................. 87NIST-2556................ 105NIST-2557................ 105NIST-2567................ 105NIST-2570................ 108NIST-2571................ 108NIST-2572................ 108NIST-2573................ 108NIST-2574................ 108NIST-2575................ 109NIST-2576................ 109NIST-2579a.............. 108NIST-2580................ 109NIST-2581................ 109NIST-2582................ 109NIST-2583................ 115NIST-2584................ 115NIST-2586................ 109NIST-2587................ 109NIST-2589................ 109NIST-25d.................... 87NIST-2678................ 107NIST-2679a.............. 106NIST-2681................ 107NIST-2682b................ 65NIST-2683b................ 65NIST-2684b................ 65NIST-2685.................. 65NIST-2686.................. 93NIST-2687.................. 93NIST-2688.................. 93NIST-2689................ 112NIST-2690................ 112NIST-2691................ 112NIST-2692b................ 65NIST-2695.................. 61NIST-2713.................. 71NIST-2714.................. 71NIST-2717a................ 70NIST-2718.................. 67NIST-2719.................. 67NIST-2721.................. 70NIST-2722.................. 70NIST-2724b................ 71NIST-276b.................. 91NIST-277.................... 87NIST-2775.................. 66NIST-2776.................. 66NIST-2783................ 107NIST-2890.................. 71NIST-2975................ 113NIST-2976.................. 22NIST-2977.................. 23NIST-2978.................. 24NIST-3101A ............. 125NIST-3102A ............. 125NIST-3103A ............. 125NIST-3104A ............. 125NIST-3105A ............. 126NIST-3107................ 126
Code number index
www.lgcpromochem.com Edition 2003/2004 155
NIST-3108 ................126NIST-3109°...............126NIST-3110A..............126NIST-3112A..............126NIST-3113 ................126NIST-3114 ................127NIST-3115A..............127NIST-3117A..............127NIST-3118°...............127NIST-3119°...............127NIST-3120°...............127NIST-3121 ................127NIST-3122 ................127NIST-3124A..............128NIST-3126A..............128NIST-3127°...............128NIST-3128 ................128NIST-3129°...............128NIST-3130A..............128NIST-3131A..............128NIST-3132 ................129NIST-3133 ................129NIST-3134 ................129NIST-3135A..............129NIST-3136 ................129NIST-3137 ................129NIST-3138 ................129NIST-3139A..............129NIST-3140 ................129NIST-3141A..............130NIST-3142A..............130NIST-3143 ................130NIST-3144 ................130NIST-3145A..............130NIST-3147A..............130NIST-3148°...............130NIST-3149 ................130NIST-3150 ................131NIST-3151 ................131NIST-3152A..............131NIST-3153A..............131NIST-3154 ................131NIST-3155 ................131NIST-3156 ................131NIST-3157A..............131NIST-3158A..............132NIST-3159 ................132NIST-3160A..............132NIST-3161A..............132NIST-3162A..............132NIST-3163 ................132NIST-3164 ................132NIST-3165 ................132NIST-3166A..............132NIST-3167A..............133NIST-3168A..............133NIST-3169 ................133NIST-3181 ................148NIST-3182 ................148NIST-3183 ................148NIST-3185 ................148NIST-3186 ................148NIST-330 ....................87NIST-350A................121NIST-351 ..................121NIST-40H..................121NIST-600 ....................89NIST-607 ....................97NIST-610 ....................97NIST-611 ....................97NIST-612 ....................97NIST-613 ....................97NIST-614 ....................97NIST-615 ....................97NIST-616 ....................98NIST-617 ....................98NIST-620 ....................95NIST-621 ....................95NIST-670 ....................89NIST-690 ....................88NIST-691 ....................88NIST-692 ....................88NIST-693 ....................88NIST-694 ..............56, 90
NIST-696 ....................89NIST-697 ....................89NIST-698 ....................89NIST-699 ....................89NIST-69b ....................89NIST-723D................121NIST-76a ....................91NIST-77a ....................91NIST-78a ....................91NIST-79a ....................86NIST-81a ....................95NIST-83D..................121NIST-84K ..................121NIST-886 ....................90NIST-887 ....................91NIST-888 ....................91NIST-889 ....................91NIST-89 ......................94NIST-92 ......................94NIST-93a ....................94NIST-951 ..........121, 123NIST-952 ..................123NIST-975a ................123NIST-977 ..................123NIST-978A ................123NIST-979 ..................123NIST-981 ..................123NIST-986 ..................123NIST-987 ..........121, 123NIST-991 ..................123NIST-994 ..................123NIST-997 ..................124NIST-999A ................121NIST-RM 8411..........110NIST-RM 8412......33, 61NIST-RM 8413......33, 61NIST-RM 8414............20NIST-RM 8415............49NIST-RM 8418............32NIST-RM 8432............33NIST-RM 8433............33NIST-RM 8435............13NIST-RM 8436............32NIST-RM 8437............32NIST-RM 8438............32NIST-RM 8441............33NIST-RM 8455............87NIST-RM 8495..........105NIST-RM 8496..........105NIST-RM 8505............71NIST-RM 8506a..........71NIST-RM 8507............72NIST-RM 8509............72NIST-RM 8510............72NIST-RM 8680..........109NJV 94-1.....................67NJV 94-2.....................67NJV 94-3.....................67NJV 94-4.....................67NJV 94-5.....................67NRCCARP-2...............31NRCCRM-DA-d ..........27NRCCRM-dcSTX........26NRCCRM-GTX14b .....26NRCCRM-GTX23b .....26NRCCRM-GTX5b .......26NRCCRM-MUS-b .......25NRCCRM-NEO-b........26NRCCRM-OA-b ..........26NRCCRM-STX-d ........26NRCCRM-STXdiAc.....26NRCDOLT-3 ...............31NRCDORM-2..............31NRCLUTS-1................25NRCTORT-2...............25NRMGBW03118.........90NRMGBW03119.........90NRMGBW03120.........90NRMGBW03132.........95NRMGBW03201a.......93NRMGBW06101a.....121NRMGBW06102.......121NRMGBW06103a.....121NRMGBW06104.......121
NRMGBW06105b.... 121NRMGBW06106a.... 121NRMGBW06107a.... 121NRMGBW06108...... 121NRMGBW06109...... 121NRMGBW06110...... 121NRMGBW06501........ 57NRMGBW06502........ 57NRMGBW06503........ 57NRMGBW07213........ 88NRMGBW07218a...... 88NRMGBW07235........ 89NRMGBW07236........ 89NRMGBW07237........ 86NRMGBW07238........ 90NRMGBW07239........ 90NRMGBW07240........ 87NRMGBW07241........ 87NRMGBW07261........ 87NRMGBW07262........ 87NRMGBW07263........ 87NRMGBW07264........ 88NRMGBW07265........ 88NRMGBW07266........ 88NRMGBW07602........ 59NRMGBW07603........ 59NRMGBW07604........ 59NRMGBW07605.. 37, 60NRMGBW08401...... 112NRMGBW08403...... 112NRMGBW08501........ 58NRMGBW08503........ 32NRMGBW08508........ 34NRMGBW08510........ 34NRMGBW08511........ 34NRMGBW08512........ 34NRMGBW08551........ 20NRMGBW08552........ 20NRMGBW08571........ 22NRMGBW08572........ 25NRMGBW10001........ 52NRMGBW10002........ 52NRMGBW10003........ 52NRMGBW10004........ 52NRMGBW10005........ 52NRMGBW11101c ...... 65NRMGBW11102c ...... 65NRMGBW11103b...... 65NRMGBW11104b...... 66NRMGBW11105a...... 66NRMGBW11106a...... 67NRMGBW11107b...... 66NRMGBW11108b...... 66NRMGBW11109b...... 66NRMGBW11110b...... 66NRMGBW11111a...... 66NRMGBW11112a...... 66NRMGBW11113a...... 66NRMGBW11201........ 73NRMGBW11202........ 73RH36976.................... 39RTC-CRM002 .......... 107RTC-CRM004 .......... 107RTC-CRM006 .......... 109RTC-CRM009 .......... 110RTC-CRM010 .......... 110RTC-CRM011 .......... 110RTC-CRM013 .......... 109RTC-CRM014 .......... 115RTC-CRM017 .......... 109RTC-CRM101 .......... 110RTC-CRM920 ............ 69Sand No.1 .................. 95Sand No.6 .................. 95Sand No.8 .................. 95Sand No.9 .................. 95SGT 10....................... 97SGT 10-P................... 97SGT 11....................... 97SGT 11-P................... 97SLV DIET A ............... 50SLV DIET B ............... 50SLV DIET C ............... 50SLV DIET D ............... 50
SLV DIET E................ 51SLV DIET F................ 51SLV FUNGUS............ 37SMRD 2000................ 20SS99850-0 ................. 74SS99851-0 ................. 74SS99852-0 ................. 74SS99853-0 ................. 74SS99854-0 ................. 74SS99856-0 ................. 74SS99857-0 ................. 70SS99858-0 ................. 70SS99859-0 ................. 68SS99860-0 ................. 69SS99861-0 ................. 69SS99862-0 ................. 69SS99863-0 ................. 69SS99864-0 ................. 74SS99865-0 ................. 74STA 003 ..................... 54U-ECK-003............... 134U-ECK-004............... 134U-ECK-005............... 134U-ECK-011............... 135U-ECK-012............... 134U-ECK-013............... 134U-ECK-014............... 135U-ECK-015............... 135U-ECK-019............... 135U-ECK-020............... 134U-ECK-022............... 135U-ECK-023............... 135U-ECK-024............... 134U-ECK-025............... 135U-ECK-026............... 134U-ECK-027............... 134U-ECK-028............... 135U-ECK-029............... 134U-ECK-030............... 135U-ECK-033............... 134U-ECK-034............... 135U-ECK-038............... 135U-ECK-042............... 135U-ECK-047............... 135U-ECK-048............... 134U-ECK-050............... 135U-ECK-051............... 134U-ECK-056............... 134U-ECK-080............... 135U-ECK-081............... 135U-ECK-082............... 134U-FLBA-001 ............... 45U-FLBA-002 ............... 45U-FLBA-003 ............... 45U-FLBA-004 ............... 45U-FLBA-006 ............... 45U-FLBA-007 ............... 45U-FLBA-008 ............... 45U-FLBA-011 ............... 45U-FLBA-012 ............... 45U-FLBA-013 ............... 45U-FLBA-014 ............... 45U-FLBA-015 ............... 45U-FLBA-016 ............... 45U-FLBA-017 ............... 45U-FLBA-018 ............... 45U-FLBA-021 ............... 44U-FLBA-022 ............... 45U-FLBA-026 ............... 45U-FLBA-027 ............... 45U-FLBA-028 ............... 45U-FLBA-030 ............... 44U-FLBA-031 ............... 45U-FLBA-032 ............... 45U-FLBA-034 ............... 44U-FLBA-035 ............... 45U-FLBA-036 ............... 45U-FLBA-037 ............... 45U-FLBA-038 ............... 45U-FLBA-042 ............... 46U-FLBA-043 ............... 46U-FLMS-010............... 47U-FLMS-012............... 44U-FLMS-013............... 44
U-FLMS-014............... 46U-FLMS-015............... 45U-FLMS-016............... 43U-FLMS-017............... 44U-FLMS-018............... 43U-FLMS-019............... 47U-FLMS-020............... 47U-FLMS-021............... 46U-FLMS-022............... 44U-FLMS-023............... 44U-FLMS-024............... 46U-FLMS-026............... 47U-FLMS-035............... 46U-FLPK-001 ............... 47U-FLPK-002 ............... 52U-FLPK-003 ............... 47U-FLPK-004 ............... 47U-FLPK-005 ............... 48U-FLPK-007 ............... 52U-FLSA-001 ............... 43U-FLSA-002 ............... 43U-FLSA-003 ............... 44U-FLSA-004 ............... 46U-FLSA-005 ............... 43U-FLSA-006 ............... 43U-FLSA-007 ............... 47U-FLSA-008 ............... 44U-FLSA-009 ............... 46U-FLSA-010 ............... 43U-FLSA-011 ............... 43U-FLSA-012 ............... 47U-FLSA-013 ............... 44U-FLSA-014 ............... 45U-FLSA-015 ............... 47U-FLSA-016 ............... 43U-FLSA-017 ............... 43U-FLSA-018 ............... 44U-FLSA-019 ............... 46U-FLSA-020 ............... 43U-FLSA-021 ............... 43U-FLSA-022 ............... 47U-FLSA-023 ............... 44U-FLSA-024 ............... 46U-FLSA-025 ............... 43U-FLSA-026 ............... 43U-FLSA-027 ............... 47U-FLSA-028 ............... 44U-FLSA-029 ............... 45U-FLSA-030 ............... 47U-FLSA-031 ............... 44U-FLSA-032 ............... 46U-FLSA-033 ............... 46U-FLSA-034 ............... 44U-FLSA-035 ............... 45U-FLSA-036 ............... 43U-FLSA-037 ............... 47U-FLSA-038 ............... 46U-FLSA-039 ............... 44U-FLSA-040 ............... 45U-FLSA-041 ............... 44U-FLSA-046 ............... 44U-FLSA-047 ............... 46U-FLSA-048 ............... 46U-FLSA-049 ............... 44U-FLSA-050 ............... 45U-FLSA-051 ............... 44U-FLSA-052 ............... 47U-FLSA-053 ............... 46U-FLSA-054 ............... 44U-FLSA-055 ............... 45U-FLSA-056 ............... 44U-FLSA-057 ............... 47U-FLSA-058 ............... 46U-FLSA-059 ............... 44U-FLSA-062 ............... 45U-FLSA-063 ............... 46U-FLSA-064 ............... 46U-FLSA-065 ............... 46U-FLSA-066 ............... 43U-FLSA-067 ............... 46U-FLSA-068 ............... 46U-FLSA-069 ............... 46U-FLSA-070 ............... 46U-FLSA-071 ............... 46
Code number index
156 Edition 2003/2004 www.lgcpromochem.com
U-FLSA-072................43U-FLSA-073................43U-FLSA-074................45U-FLSA-076................45U-FLSA-077................46U-FLSA-078................46U-FLSA-079................46U-FLSA-080................43U-FLSA-081................46U-FLSA-082................46U-FLSA-083................47U-FLSA-084................46U-FLSA-085................46U-FLSA-086................43U-FLSA-087................43U-FLSA-088................45U-FLSA-089................44U-FLSA-090................44U-FLSA-091................43U-FLSA-092................44U-FLSA-093................44U-FLSA-094................43U-FLSA-095................44U-FLSA-096................44U-FLSA-097................43U-FLSA-098................43U-FLSA-100................43U-FLSA-101................43U-FLSA-104................44U-FLSA-105................44U-FLSA-106................43U-FLSA-107................43U-FLSA-109................43U-FLSA-110................43U-FLSA-113................43U-FLSA-114................46U-FLSA-115................43U-FLSA-117................44U-FLSA-118................44U-FLSA-119................46U-FLSA-120................45U-FLSA-121................43U-FLSA-125................47U-FLSA-127................46U-FLSA-130................43U-FLSA-131................46U-FLSA-132................43U-FLSA-134................44U-FLSA-135................44U-FLSA-136................46U-FLSA-137................45U-FLSA-138................43U-FLSA-142................47U-FLSA-144................46U-FLSA-147................44U-FLSA-148................44U-IAA-003.................141U-IAA-004.................140U-IAA-005.................140U-IAA-011.................142U-IAA-012.................141U-IAA-013.................140U-IAA-014.................142U-IAA-015.................141U-IAA-016.................142U-IAA-019.................142U-IAA-020.................140U-IAA-022.................142U-IAA-023.................143U-IAA-024.................140U-IAA-025.................141U-IAA-026.................141U-IAA-027.................140U-IAA-028.................141U-IAA-029.................140U-IAA-030.................143U-IAA-031.................141U-IAA-032.................141U-IAA-033.................140
U-IAA-034 .................142U-IAA-038 .................142U-IAA-039 .................143U-IAA-040 .................143U-IAA-041 .................141U-IAA-042 .................141U-IAA-047 .................142U-IAA-048 .................140U-IAA-049 .................141U-IAA-050 .................142U-IAA-051 .................140U-IAA-052 .................142U-IAA-055 .................140U-IAA-056 .................140U-IAA-057 .................141U-IAA-058 .................140U-IAA-059 .................142U-IAA-060 .................141U-IAA-062 .................142U-IAA-063 .................141U-IAA-064 .................141U-IAA-065 .................142U-IAA-066 .................140U-IAA-067 .................141U-IAA-068 .................140U-IAA-070 .................143U-IAA-073 .................142U-IAA-074 .................142U-IAA-080 .................141U-IAA-081 .................142U-IAA-082 .................141U-IAA-083 .................140U-IAA-090 .................142U-IAA-092 .................142U-IAA-203 .................137U-IAA-204 .................136U-IAA-205 .................136U-IAA-211 .................138U-IAA-212 .................137U-IAA-213 .................136U-IAA-214 .................138U-IAA-215 .................138U-IAA-216 .................139U-IAA-219 .................138U-IAA-220 .................136U-IAA-221 .................138U-IAA-222 .................139U-IAA-223 .................139U-IAA-224 .................136U-IAA-225 .................137U-IAA-226 .................137U-IAA-227 .................136U-IAA-228 .................138U-IAA-229 .................136U-IAA-230 .................139U-IAA-231 .................137U-IAA-232 .................137U-IAA-233 .................136U-IAA-234 .................138U-IAA-237 .................138U-IAA-238 .................138U-IAA-239 .................139U-IAA-240 .................139U-IAA-241 .................138U-IAA-242 .................137U-IAA-244 .................138U-IAA-245 .................138U-IAA-246 .................138U-IAA-247 .................138U-IAA-248 .................136U-IAA-249 .................137U-IAA-250 .................139U-IAA-251 .................136U-IAA-252 .................139U-IAA-255 .................136U-IAA-256 .................136U-IAA-257 .................137U-IAA-258 .................136U-IAA-259 .................138
U-IAA-260 ................ 137U-IAA-262 ................ 138U-IAA-263 ................ 136U-IAA-264 ................ 137U-IAA-265 ................ 139U-IAA-266 ................ 136U-IAA-267 ................ 137U-IAA-268 ................ 136U-IAA-269 ................ 139U-IAA-270 ................ 139U-IAA-271 ................ 137U-IAA-272 ................ 137U-IAA-273 ................ 139U-IAA-274 ................ 139U-IAA-275 ................ 138U-IAA-277 ................ 137U-IAA-278 ................ 138U-IAA-279 ................ 137U-IAA-280 ................ 137U-IAA-281 ................ 139U-IAA-282 ................ 137U-IAA-283 ................ 136U-IAA-290 ................ 139U-IAA-292 ................ 139U-ICC-001................ 148U-ICC-002................ 148U-ICC-003................ 148U-ICC-004................ 148U-ICC-005................ 148U-ICC-006................ 148U-ICC-007................ 148U-ICC-010................ 148U-ICC-011................ 148U-ICC-012................ 148U-ICC-013................ 148U-ICC-101................ 149U-ICC-102................ 149U-ICC-103................ 149U-ICC-104................ 149U-ICC-105................ 149U-ICC-106................ 149U-ICC-107................ 149U-ICC-108................ 149U-ICC-200................ 148U-ICC-210................ 148U-ICC-300................ 149U-ICC-310................ 149U-ICC-320................ 149U-ICK-230A.............. 144U-ICM-202................ 145U-ICM-203................ 145U-ICM-204................ 145U-ICM-205................ 145U-ICM-211................ 146U-ICM-212................ 146U-ICM-213................ 146U-ICM-215................ 146U-ICM-221................ 146U-ICM-223........ 146, 147U-ICM-224........ 146, 147U-ICM-231................ 144U-ICM-232................ 144U-ICM-233................ 144U-ICM-234................ 144U-ICM-235................ 144U-ICM-237................ 145U-ICM-238................ 145U-ICM-240................ 145U-ICM-241................ 145U-ICM-242................ 145U-ICM-243................ 145U-ICM-245................ 145U-ICM-601................ 146U-ICM-602................ 146U-ICM-603................ 146U-ICM-604................ 146U-ICM-605................ 146U-ICM-607................ 147U-ICM-611................ 147
U-ICM-642................ 144U-ICP-003 ................ 128U-ICP-003-5 ............. 128U-ICP-004 ................ 126U-ICP-004-5 ............. 126U-ICP-005 ................ 126U-ICP-005-5 ............. 126U-ICP-011 ................ 131U-ICP-011-5 ............. 131U-ICP-012 ................ 128U-ICP-012-5 ............. 128U-ICP-013 ................ 125U-ICP-013-5 ............. 125U-ICP-014 ................ 131U-ICP-014°............... 131U-ICP-014°-5............ 131U-ICP-014-5 ............. 131U-ICP-015 ........ 129, 147U-ICP-015-5 ............. 129U-ICP-016 ................ 131U-ICP-016-5 ............. 131U-ICP-019 ................ 130U-ICP-019-5 ............. 130U-ICP-020 ................ 126U-ICP-020-5 ............. 126U-ICP-021 ................ 130U-ICP-021-5 ............. 130U-ICP-022 ........ 132, 145U-ICP-022-5 ............. 132U-ICP-023 ................ 132U-ICP-023-5 ............. 132U-ICP-024 ................ 126U-ICP-024-5 ............. 126U-ICP-025 ................ 129U-ICP-025-5 ............. 129U-ICP-026 ................ 128U-ICP-026-5 ............. 128U-ICP-027 ................ 126U-ICP-027-5 ............. 126U-ICP-028 ........ 129, 145U-ICP-028-5 ............. 129U-ICP-029 ................ 127U-ICP-029-5 ............. 127U-ICP-030 ................ 133U-ICP-030-5 ............. 133U-ICP-031 ................ 127U-ICP-031-5 ............. 127U-ICP-032 ................ 127U-ICP-032-5 ............. 127U-ICP-033 ................ 125U-ICP-033-5 ............. 125U-ICP-034 ................ 130U-ICP-034-5 ............. 130U-ICP-037 ................ 130U-ICP-037-5 ............. 130U-ICP-038 ................ 131U-ICP-038-5 ............. 131U-ICP-039 ................ 133U-ICP-039-5 ............. 133U-ICP-040 ................ 133U-ICP-040-5 ............. 133U-ICP-041 ................ 129U-ICP-041-5 ............. 129U-ICP-042 ................ 129U-ICP-042-5 ............. 129U-ICP-044 ................ 130U-ICP-044-5 ............. 130U-ICP-045 ................ 130U-ICP-046 ................ 129U-ICP-046-5 ............. 129U-ICP-047 ................ 131U-ICP-047-5 ............. 131U-ICP-048 ................ 126U-ICP-048-5 ............. 126U-ICP-049 ................ 128U-ICP-049-5 ............. 128U-ICP-050 ................ 132U-ICP-050-5 ............. 132
U-ICP-051 125, 145, 146,147
U-ICP-051-5 ............. 125U-ICP-052 ................ 131U-ICP-052-5 ............. 131U-ICP-055 ................ 126U-ICP-055-5 ............. 126U-ICP-056 ................ 125U-ICP-056-5 ............. 125U-ICP-057 ................ 128U-ICP-057-5 ............. 128U-ICP-058 ................ 126U-ICP-059 ................ 130U-ICP-059-5 ............. 130U-ICP-060 ................ 129U-ICP-060-5 ............. 129U-ICP-062 ................ 130U-ICP-062-5 ............. 130U-ICP-063 ................ 127U-ICP-063-5 ............. 127U-ICP-064 ................ 127U-ICP-064-5 ............. 127U-ICP-065 ................ 131U-ICP-065-5 ............. 131U-ICP-066 ................ 127U-ICP-066-5 ............. 127U-ICP-067 ................ 128U-ICP-067-5 ............. 128U-ICP-068 ................ 127U-ICP-068-5 ............. 127U-ICP-069 ................ 132U-ICP-069-5 ............. 132U-ICP-070 ................ 132U-ICP-070-5 ............. 132U-ICP-071 ................ 128U-ICP-071-5 ............. 128U-ICP-072 ................ 127U-ICP-072-5 ............. 127U-ICP-073 ................ 131U-ICP-073-5 ............. 131U-ICP-074 ................ 132U-ICP-074-5 ............. 132U-ICP-075 ................ 130U-ICP-075-5 ............. 130U-ICP-077 ................ 128U-ICP-077-5 ............. 128U-ICP-078 ................ 129U-ICP-078-5 ............. 129U-ICP-079 ................ 127U-ICP-079-5 ............. 127U-ICP-080 ................ 129U-ICP-080-5 ............. 129U-ICP-081 ................ 132U-ICP-081-5 ............. 132U-ICP-082 ................ 128U-ICP-082-5 ............. 128U-ICP-083 ................ 126U-ICP-083-5 ............. 126U-ICP-090 ................ 132U-ICP-090-5 ............. 132U-ICP-092 ................ 132U-ICP-092-5 ............. 132U-IMS-100................ 148U-IMS-102................ 147U-IMS-103................ 147U-IMS-104................ 147U-IMS-105................ 147U-IMS-110................ 147U-IMS-111................ 147U-IMS-112................ 147U-IMS-113................ 147U-IMS-114................ 147U-IMS-115................ 148U-IQC-007................ 144U-IQC-019................ 144U-IQC-026................ 144VDA 001-4.................. 99