icp test report certification packet/media/electronics...negative = absence of cr(vl) coating /...

1

ICP Test Report Certification Packet

Company name : Littelfuse, Inc. Product Series: FLQ Series Product #: FLQ Series Issue Date: August 24, 2010 It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive 2002/95/EC)-restricted substance nor such use, for materials to be used for unit parts, for packing/packaging materials, and for additives and the like in the manufacturing processes. In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing processes, are all composed of the following components.

Issued by:

(1) Parts, sub-materials and unit parts This document covers the FLQ RoHS-Compliant series products manufactured by Littelfuse, Inc. ＜ Raw Materials Used

Please see Table 1 (2) The ICP data on all measurable substances Please see appropriate pages as identifed in Table 1

Remarks：

Form 585-047 Rev. A 2/21/06

2

Table 1: List of Raw Materials covered by this report

Total Parts Raw Material Part Number Raw Material Description Page(s) 1 NA Filler- Gray-White Sand 3-10 2 NA Filler- Cream Sand 3-10 3 NA Body- White Glass Fiber Tube 3-10 4 NA Body- Green Glass Fiber Tube 3-10 5 NA Metal cap 3-10 6 648102 Yarn 11-14 7 082xxx-001 Wire- Cu Sn Plated 11-14 8 082xxx Wire-Copper Nickel Alloy (082384) 15-23 9 079xxx Wire-Cu 110 Strip w/center Sn Overlay 24-28 10 685xxx Pure Ag (685406) 29-36

Valid own

Plgase sGs

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Test Report No.:CE/2010t6157 Date:2010/08/10 Paoe :1of8LITTELFUSE INC,8FL., NO. 18,1, SEC, 2, TIDING BLVD., TAIPEI 1'14, TAIWAN,R. O. C.

Thafollowing sample(s) was/we.e submitt€d and identified by/on behalfofthe client as:

Sample DescriptionStyldltem No.Sample Receiving DateTesting Period

MIDGET FUSE

2010to7t30201 0 I 07 | 30 f O 201 ong I 1 0

In accordance with th€ RoHS Directive 2002l95/EC, and it5 amendment directive6.

with reference to lEc 62321: 2008Procedures for the Detemination of Lovets of Regulated Substances in Electrotechnic€lProducts,

(1) Determination of Cadmium by ICP-AES.(2) Determination of Lead by ICP-AES.(3) Determination of llercury by ICP-AES.(4) Determination of Hex€val€nt Chromium by W /is Specirometry.(5) Determination of Hexavalent Chromium by Spot test / boiling water e\4raction Method.(6) Determinatjon of PBB and PBDE by GC/MS.

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T€6t Requested

Teat Method

T€6t R6ult(sl Please refer to next page(s).

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Test Report No. : CE/2010t6157 Date: 2010/08/10 P a g e : 2 o f 8LITTELFUSE INC.8FL., NO, 181, SEC.2, TIDING BLVO,, TAIPEI 114, TAIWAN,R. O. C.

Test results by chemical method (Unit mg/kg)

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Teat ltem (s): Method(Refor to)

R.6ultMDLNo.1 No.2 No.3 No.4 No.5

Cadmium (Cd) ( 1 ) n.d. n.d. n.d. n-d. n.d.Lead (Pb) (2) n.d. n.d. n.d. n.d. n,d, 2Morcury (Hg) (3) n.d. n.d. n.d. n.o. n.o, 2Hexavalent Chromium Cr(Vl) by alkatinee)draction

(4) n.d. n.d. n.d. n.o, 2

Hexavalent Chrornium C(Vl) by Spot test /boiling u€ter extraclion

(s) N€gative SeeNote 4

Sum of PBB8

(6)

n.o. n.o, n.d. n.d.Monobromobiphenyl n.o. n.o, n-d. n.d.Dibromobiphenyl n.o. n.o. n.o, n .d .Tribromobiphenyl n.o. n,o, n.o. n.d.Tetrabromobiphenyl n.d, n.o. n.o. n.d.Pentabromobiphenyl n.o, n.o. n.o, n.d.Hexabromobiphenyl n.o, n.o. n.o, n.d.Hepiabromobiphenyl n.d. n.d, n.o. n.d. 5Oc'tabromobiphenyl n.o, n.o. n.d, n.d.Nonabrcmobiphenyl n.o. n.o. n.o. n.d. 5Decabromobiphenyl n.d. n.o. n.d. n.d.Sum of PBDES n.o. n.o, n.d. n.d.Monobromodiphenyl eth€r n.d. n.o. n.d. n.d.Dibromodiphenyl ether n.d. n.o, n.d. n.d.Tribromodiphenyl eth€r n.d. n-d. n.d. n.d. 5Tetrabromodiphenyl elhgr n.d. n.d. n.d. n,d, 5Pentabromodiphenyl ether n.d. n.d. n.d. n.o.H€xabromodiphenyl ether n.d. n.d. n.d. n.d, 5Heptabromodiphenyl ether n.d. n.d. n.d. n.o. 5Oclabromodiphenyl ether n.d. n.d. n.d. n.d. 5Nonabromodiphenyl ether n.d. n.d. n.d. n.d. 5Decabromodiphenyt olher n.d. n.d. n.d. n.d. 5

Mhbrd ri€ s6s crdp (s6s s )

Test Report No. : CE/2010t6157 Date : 2010/0€t/10 page:3of8LITTELFUSE INC.8FL,, NO. 181, SEC. 2, TIDING BLVD., TAIPEI ,114, TAIWAN,R. O. C.

TEST PART DESCRIPTION:N O . 1NO.2NO.3NO.4NO.5

Note :1 .

3.4.

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GRAY.WHITE SANDCREAM SANDWHITE GLASSFIBER TUBEGREEN GLASSFIBER TUBESILVER COLORED IJETAL CAP

mg/kg= ppm ; 0.1wt%= 1000ppmn.d. = Not Det€c1edMDL = Method Detection LimitSpot-testi

Negative = Absence of Cr(Vl) coating / surface layer,Positive = Prerence of Cr(Vl) coating / surface layer:(The tesled sample should be fudher vedfied by boiling-water-extraction method if the spot test result cannot boconfirmed.)

Eoil in g-lyater-extraction :Negative = Absence of Cr(Vl) coating / $rrface tayer.Positive = Presence of Cr(Vt) coating / surface layerlThe detected conc€ntration in boiling-water-extraction solution i6 equal or greater than 0.02 mg/kg with 50 cm,sample surlace area.

5. "-" = Not Regulated6. "-" = Not Conducted

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Test Report No. : CE2010t6157 Date : 2010/OCi/10 page :4 of 8LITTELFUSE INC.8FL., NO. 181, SEC,2, TIDING BLVD., TAIPEI 114, TAIWAN,R. O. C.

1 )

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These samples were dis6olved totally by pre-conditioning method accarding to below flow chart.rur tesl merod exctuded )

Name ofhe person who made measwement: Climbgr€at yangName of the person in charge of measuroment: Troy Chang

ICP.AES

Sample [,laterial DigestionAcid

S-teel, copper, aluminum, solder Aqua regia, HNO3, HCl, HF, HrO,Glass HNO3/HF

Gold, platinum, palladium, ceramic Aqua regiaSilver HNO3

Plastic HrSOr, HrOr, HNO3, HCI

Othe.s Any acid to totral digeslion

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Sample Measurement

Acid digestion by suitable aciddepended on different samptematerial (as below table)

Add appropriete amount ofdigestion reagent

Heat to appropriate

temperature to extract

Cool, flter digesbte

through filterAlkali FusionHCltodissolve

Add diphenyl.carbazide tor

color developmedt

measure the ab6otbance

at 540 nm by W-VIS

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Test Report No.: CEnO1On6157 Dete : 2010/08/10 Page :5o f8

PBBTPBDE analytical FLOW CHART

LITTELFUSE INC.8F1., NO. ,181, SEC, 2, TIDING BLVD., TAIPEI 114, TAIWAN,R. O. C.

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1) Nameofthe2) Name of the

Fhst testing process --'

Optional screen process ---.

Confirmation process - .>

pefson who made measurementt Roman wongpeason in charge of measurementt Troy Chang

Screen analysis

Sample extraclion/Soxhlel method

t

Concentrate/DiluteExhacted solution

Analy6is by GC/MS

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Test Report No. I CE/2010/76157 Date: 2010/08/10 Page r7o f8LITTELFUSE INC.8FL,, NO. 181, SEC.2, TIDING BLVD., TAIPEI '114, TAIWAN,R. O. C.

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Test Report No. : CE/2010t6157 Date : 2010/08/10 P a g e : 8 o f 8LITTELFUSE INC.8FL., NO, 181, SEC.2, TIDING BLVD,, TAIPEI 114, TAIWAN,R. O. C.

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" End of Report "

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Report No.: MX10-1742 Date：2010-08-16

It is prohibited the total or partial reproduction of this document, as well as any modification or alteration in no of its parts without the previous authorization of Intertek Testing

Services de México, S.A. de C.V. On the contrary Intertek reserves the right of coming from legal form against that (it is) they are responsible (s). The results that appear in this report belong solely to (s) shows (s) analyzed (s).

1ª. Emisión Junio 2005, 1° Revisión Junio 26, 2009. ILTA/003/GENS-F8

Intertek Testing Services de México, S.A. de C.V. Blvd. Manuel Ávila Camacho No. 182 Col. Lomas de Chapultepec

C.P. 11650, México, D.F. Tel.: 50912150 Fax: 55407863 www.intertek.com

RESULTS REPORT

INTERTEK TESTING SERVICES

DE MEXICO SA DE CV

LABORATORIO CD. DE MEXICO

DELIVER TO: Littelfuse, S.A. de C.V. Blvd. Fausto Z. Martínez 1800, Col. Magisterio Sección 38,

Piedras Negras, Coahuila

ATTENTION: Ing. Mario Falcón / Ing. Manuel Berain

http://www.itsglobal.com/

Report No.: MX10-1742 Date：2010-08-16






TEST REPORT

APPLICANT Littelfuse, S.A. de C.V. Blvd. Fausto Z. Martínez 1800, Col. Magisterio Sección 38, Piedras Negras, Coahuila Ing. Mario Falcón / Ing. Manuel Berain SAMPLE DESCRIPTION

One (1) group of submitted samples said to be : Sample Description Serie FLQ

Item No. 1) N.P. 648102 2) N.P. 082201-001

Country of Origin NP Buyer's Name NP Supplier's Name NP Date sample received 2010-08-12 Testing period 2010-08-13 to 2010-08-16 ******************************************************************************************** TEST CONDUCTED

As requested by the applicant, for details please refer to attached pages. ********************************************************************************************

CONCLUSION

Sample Number Testing item Conclusion Failed component Failed result

1

N.P. 648102 Pass

See Result summary --- ---

2

N.P. 082201-001 Pass

See Result summary --- ---

********************************************************************************************


Report No.: MX10-1742 Date：2010-08-16






TEST CONDUCTED Sample : 1) N.P. 648102 2) N.P. 082201-001

TEST RESULT SUMMARY FOR RoHS DIRECTIVE :

TESTING ITEM Ω RESULT (ppm) Limit (1) (2)

Cadmium (Cd) content ND ND 0,01% (100 ppm)

Lead (Pb) content 13,33 ND 0,1% (1000 ppm)

Mercury (Hg) content ND 0,096 0,1% (1000 ppm)

Chromium (VI) (Cr6+) ND ND 0,1% (1000 ppm) ppm = parts per million based on dry weight of sample. µg/cm2 = microgram per square centimeter. mg/kg WITH 50cm2 = milligram per kilogram with 50 square centimeter. < = less than. ND = Not detected. The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material. These Accreditations only apply for the methods listed in such. Not accredited under EMA Ω.

Prepared and checked by： For Intertek Laboratory Manager

The Official Mexican Standard NOM-008-SCFI-1993 establishes like separator decimal the comma (,).


Report No.: MX10-1742 Date：2010-08-16






NOTE :DecaBDE IN POLYMERIC APPLICATIONS IS EXEMPTED ACCORDING TO ROHS DIRECTIVE AMENDMENT 2005/717/EC.

# =ACCORDING TO IEC 62321, A POSITIVE RESULT INDICATES THE PRESENCE OF Cr(VI) COATING. IT IS THE Cr(VI) CONCENTRATION DETECTED IN THE BOILING-WATER-EXTRACTION SOLUTION AND SHOULD NOT BE INTERPRETED AS THE Cr(VI) CONCENTRATION IN THE COATING LAYER OF THE SAMPLE. REMARK : AS REQUESTED BY THE APPLICANT, COATING WITH BASE MATERIAL OF TESTED COMPONENTS OF THE SAMPLE MX10-1742-1 WERE TESTED TOGETHER. REMARK : AS REQUESTED BY THE APPLICANT, COATING WITH BASE MATERIAL OF TESTED COMPONENTS OF THE SAMPLE MX10-1742-2 WERE TESTED TOGETHER. Test method：

Sample Number Testing item Ω Testing method

Quality control Batch:

Analysis Date:

Analyzed By:

Reporting limit ppm

1,2 Chromium VI (Cr6+)

content With reference to USEPA 3060, by

EPA 7196 QHU2009-3p168 2010-08-14 JLHS,MLG 2,0



Analysis Date:

Analyzed By:

Reporting limit ppm

1 Lead (Pb) content With reference to USEPA 3052, by EPA 6010 MET2010-32p50 2010-08-16 DCL,JMR 5,0 2 Lead (Pb) content With reference to USEPA 3050-MOD, by EPA 6010 MET2010-32p51 2010-08-16 DCL,JMR 5,0



Analysis Date:

Analyzed By:

Reporting limit ppm

1 Cadmium (Cd) content With reference to USEPA 3052, by EPA 6010 MET2010-32p50 2010-08-16 DCL,JMR 2,0 2 Cadmium (Cd) content With reference to USEPA 3050-MOD, by EPA 6010 MET2010-32p51 2010-08-16 DCL,JMR 2,0



Analysis Date:

Analyzed By:

Reporting limit ppm

1 Mercury (Hg) content With reference to USEPA 7471 by USEPA 7471 MET2010-31p37,38 2010-08-16 JAPM 0,083 2 Mercury (Hg) content With reference to USEPA 7471 by USEPA 7471 MET2010-31p37,38 2010-08-16 JAPM 0,083


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Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 E-mail: [email protected] www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338

TEST REPORT NUMBER: SHAH00176744

PREPARED AND CHECKED BY: AUTHORIZED BY: FOR INTERTEK TESTING SERVICES FOR INTERTEK TESTING SERVICES LTD., SHANGHAI LTD., SHANGHAI

MYRA LV STEPHEN TSANG CHEMICAL DIVISION MANAGER GENERAL MANAGER

PAGE 1 OF 5

APPLICANT: LITTELFUSE,INC. DATE: FEB 09, 2010 800 E. NORTHWEST HWY ATTN: A.DIVIETRO/D.UNTIEDT

SAMPLE DESCRIPTION: One (1) group of submitted samples said to be Silvery color/golden color metal. Part Description : Element. Part Number : Cu 110 Strip with Center Sn Overlay(079xxx)

917-445xxxxx-P1,917-447xxxx,917-447xxxx-P1,917-447xxxxx,917-447xxxxx-P1,917-448xxxx,917-449xxxx,917-45xxxxx,917-48xxxxx-P1.

Date Sample Received : Feb.3, 2010. Date Test Started : Feb.3, 2010. ***********************************************************************

TESTS CONDUCTED: AS REQUESTED BY THE APPLICANT, FOR DETAILS REFER TO ATTACHED PAGE(S)

*********************************************************************** TO BE CONTINUED



TESTS CONDUCTED

PAGE 2 OF 5

(I) Test Result Summary :

Testing Item Result (ppm)

Heavy Metal

Cadmium (Cd) content ND Lead (Pb) content 80 Mercury (Hg) content ND Chromium VI (Cr6+) content (mg/kg with 50cm2) ND

Remarks: ppm = Parts per million based on weight of tested sample =

mg/kg ND = Not detected mg/kg with 50cm2 = milligram per kilogram with 50 square

centimetre

Responsibility Of Chemist : Dent Fang

(II) RoHS Requirement: Restricted Substances Limits Cadmium (Cd) Content 0.01% (100ppm)Lead (Pb) Content 0.1% (1000ppm)Mercury (Hg) Content 0.1% (1000ppm)Chromium VI (Cr6+) Content 0.1% (1000ppm)

The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material. ***********************************************************************

TO BE CONTINUED



TESTS CONDUCTED

PAGE 3 OF 5

(III) Test Method: Testing Item Testing Method Reporting Limit

Cadmium (Cd) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Lead (Pb) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Mercury (Hg) content

With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Chromium VI (Cr6+) content

With reference to IEC 62321 edition 1.0:2008 in annex B, by boiling water extraction and determined by UV-Vis spectrophotometer.

0.02 mg/kg with

50cm2

Remark: Reporting limit = Quantitation limit of analyte in sample

Date Sample Received : FEB.3, 2010 Testing Period : FEB.3, 2010 TO FEB.8, 2010 ***********************************************************************

TO BE CONTINUED



TESTS CONDUCTED

PAGE 4 OF 5

(IV) Measurement Flowchart:

Test For Cd/Pb/Hg/Chromium (VI) Reference Standard：IEC 62321 edition 1.0:2008

***********************************************************************

TO BE CONTINUED



TESTS CONDUCTED

PAGE 5 OF 5

***********************************************************************

END OF REPORT

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icp test report certification packet/media/electronics...negative = absence of cr(vl) coating /...

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