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37 III. EXPERIMENTAL PROCEDURE Experimental procedure pertaining to the study “Fabrication and Enhancement of Plasma Treated Cotton, Tencel Cotton and Modal Cotton with Anti-bacterial and Mosquito Repellent Finish” are discussed under the following headings and expressed in Figure – 1.

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III. EXPERIMENTAL PROCEDURE Experimental procedure pertaining to the study “Fabrication and Enhancement of Plasma Treated Cotton, Tencel Cotton and Modal Cotton with Anti-bacterial and Mosquito Repellent Finish” are discussed

under the following headings and expressed in Figure – 1.

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FIGURE – 1 EXPERIMENTAL DESIGN

PHASE – III

Anti-bacterial Evaluation

Mosquito Repellent Evaluation

Physical, Mechanical Comfort and Absorbent Properties

Agar Diffusion Parallel Streak Test (AATCC 147-2004, AATCC 100-2004)

Excito Chamber Method

(Product Development)

Wear Study

Evaluation

Bacterial Reduction Evaluation

PHASE – II Pilot Study

Selection of Herbs and Optimization of the Parameters

Selection of Herbs

Phytochemical Analysis

Functional Finishes

Anti-bacterial Finish

Mosquito Repellent Finish

Optimization Parameters

Application of Finishing Techniques

FT-IR

PHASE – I Survey

Consumer and Market

Selection of Yarn (Cotton, Tencel Cotton and Modal Cotton)

Selection of Fabric Formation (100 per cent Cotton, 50/50 Tencel Cotton, 50/50 Modal Cotton)

Pre-treatments (Scouring and Bleaching)

Application of Value Added Finish (Plasma Application)

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Phase – I

The phase – I consisted of two surveys (market and consumer),

selection of yarn, selection of fabric formation, pre-treatments and application

of value added finish was done, the details are discussed below.

3.1 Conduct of Survey

The survey can be useful to collect data on phenomena that cannot be

directly observed. A questionnaire is a research instrument consisting of a

series of questions and other prompts for the purpose of gathering information

from respondents (Gupta, 2008). Hence the investigator prepared the

questionnaire to collect information from the market and the consumer

regarding the awareness, preference, rating and recommendation of

eco-friendly textile products. The survey may focus on factual information

about individuals or it might aim to collect the requirements of the consumer.

A special purpose survey is that by which data obtained are useful in

analyzing a particular problem only (Gupta, 2008).

3.1.1 Selection of Area and Sample

A sample may be defined as a selected number of units from a

population to represent it. The sample was used to make inference about a

population (Anderson et al., 2012). Sampling saves on cost and time

(Parasuraman et al., 2009). By studying the sample it was hoped to draw valid

conclusion about the larger grouping using simple random sampling method.

And this method was selected for this study. For market survey fifty textile

shops were selected in and around Coimbatore city and for the consumer

survey fifty adolescent girls were selected who were using healthcare

products. The elicited information was used for selection of fabrics and

finishes for this study.

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3.1.2 Selection of the Tool

The various methods of data gathering involved the use of appropriate

recording forms. These are called tools or instruments of data collection.

A research tool plays a major role in any worthwhile research as it is the sole

factor in determining the sound data and in arriving at a perfect conclusion

about the problem or study in hand, which ultimately helps in providing

suitable remedial measures to the problem concerned. Interview method was

selected for gathering information regarding the study.

3.1.3 Conduct of Surveys

For this study, two types of surveys were conducted namely, Market

and Consumer Survey.

3.1.3.1 Market Survey

A market survey is an objective and systematic collection, recording,

analysis and interpretation of data about existing or potential markets for a

product and service. Hence, the market survey was carried out in fifty textile

shops to know about the demand for the existing textile products. The

questionnaire was framed with the following requirements such as different

types of yarn, fabric formation, finishing, its durabilities, cost performance,

types of finishes, hazardous of synthetic finishes, disposable and degradable

qualities of the textile material available. The prepared interview schedule was

used to conduct the survey (Appendix –XXX).

3.1.3.2 Consumer Survey

Consumer surveys can provide information on when, where, why, how

and for which attitudes affect shopping habits. The survey also invites

consumers to share their perspectives regarding the current and future

economic health of business district. For this study, the consumer survey was

conducted from the adolescent 100 girls to gather information regarding the

special finishes like herbal anti-bacterial and mosquito repellent finishes. The

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schedule was framed to get information about the wearers need and their

requirements for healthcare textile products (Appendix – XX and XX). Then

the elicited information about existing products was utilized for further study.

We have removed the section (Pre-Testing of interview schedule) as this

section was not necessary because we have conducted a thorough survey of

consumer, covering major area of Coimbatore city involving 100 adolescent

girls. Detailed information on the region and information involving the basis for

the selection of the region in Coimbatore city and the choice of consumer

have been provided in chapter-III.

3.1.4 Final Conduct of Survey

The interview schedule is the data collection instruments for the

conduct of interviews. It can be highly structured or unstructured depending

on the nature of the interviews (Hall, 2004). Hence, the investigator planned to

conduct a face to face interview to collect data from the selected shops and

adolescent girls regarding health care product.

3.1.5 Consolidation and Analysis of Data

The next step in the process of research after the collection of data is

the organization, analysis and interpretation of data and formulation of

conclusions and generalizations get a meaningful picture out of the

information collected. This is a list of items of information to be obtained from

documents, records and other materials. In order to secure measurable data,

the items included in the schedule are limited to those that can be uniformly

secured from the large number of case histories or other records which will be

consolidated and analyzed systematically from the data. The consolidated

data shows that the consumer requirements of the textile related aspects such

as healthcare products and special finishes from the shops and consumers

fondness of textile products which are environmentally safe finish, cost

effective, good mosquito repellent, and non toxic properties. Hence, the

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investigator considered to finish with herbal extracts and convert into

healthcare textile products.

Justification of the selection of sample number for market and consumer survey Market survey

The fifty shops chosen represented a reasonable broad spectrum of

consumers in different regions of Coimbatore city. As our department in

Avinashilingam Institute for Home Science and Higher Education for Women

specializes in home science, through prior surveys and research carried out

by colleagues over a number of years, we found that a survey of about fifty

shops is a reasonable representation for market research and analysis. In

addition, these shops represented a broad regional base in the Coimbatore

city, such as Gandhipuram, Town Hall, Saibaba Colony and R.S Puram.

Customers in these areas vary in their social, economical and educational

backgrounds. These reasons justify our choosing of fifty shops in different

areas in Coimbatore for the market survey.

Consumer Survey

We decided to carryout survey of 100 adolescent girls based on our

earlier activities carried in our department over few decades. Our department

specializes in home economics and consumer science and has carried out

many such projects. Results and understanding from such studies showed

that the acceptability of women’s healthcare products is basically through

penetration into the segment of the population that is dominated by college

going adolescent girls. Although it is worthy to have a large population for

such survey, our earlier research activities in our department have shown that

decent size of the population could be 100 provided the survey is

geographically distribution and spread. As is evident from our study, our

survey was reasonably distributed in the city of Coimbatore involving

Gandhipuram, Town Hall, Saibaba Colony and R.S Puram.

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3.2 Selection of Yarn

Based on the finding of the survey cotton, tencel and modal were

selected for the study.

Cotton has the excellent properties such as absorbency,

biodegradable, breathable, drape, easily sterilized, high wet-strength,

insulating properties, non-allergic, renewable resource, softness and water

retaining capacity (Gopalakrishnan and Aravindan, 2005). The cotton fabric

has good property of withstanding severe treatment, especially during dyeing

and finishing (Barker and Midgley, 2007).

The selected yarns such as cotton (40 Ne), tencel (40 Ne) and modal

(40 Ne) were procured from the local yarn merchants. The yarn was

converted into plain-woven fabric. Twenty metres of cotton, tencel cotton and

modal cotton were produced from the power loom (Appendix – IV).

Tencel is made with wood pulp cellulose from the eucalyptus tree. It is

extremely absorbent irritation free, naturally prevents the growth of bacteria,

and is 100% biodegradable (Storeg, 2006). Modal is a processed bio-based

textile made from reconstituted cellulose from beech trees and is soft, smooth

and breathes well, cool to touch and high absorbent, like cotton. It drapes well

and keeps its shape, even when it was wet. One of the advantages of modal

over cotton is resistant to shrinkage. Modal is about 50% more hygroscopic

per unit volume than cotton (Mishra, 2003) (Plates – 1a and 1b).

The use of blends of fabrics has tremendously increased even in India.

The price structure and multi fibre policy of Government have increased the use

of cellulosic mixed fabrics. Hence due to the above properties and according to

the consumer requirements the following yarn was selected. Cotton, Tencel

cotton and modal yarns were used for the study.

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3.3 Fabric Formation

The most widely used methods of making fabrics are always weaving

(Kathleen et al., 2007). The fabric forming process contributes to the fabric’s

appearance and texture, performance and cost. In woven fabrics generally

two or more sets of yarns are interlaced at right angles to each other. Many

different interlacing patterns give interest to the fabric (Kadoph et al., 2002).

Similarly cotton yarn runs in the warp directions whereas modal runs in

the weft directions for modal cotton fabric (Plate – 1c).

3.4 Pre-treatment of Fabrics

Pre-treatments are essential for successful finishing. It is applied

before the final finishes are given because it contains impurities

(Garg et al., 2005). Pre-treatment improves the usability of fabrics and

therefore improves the quality. It is very essential before application of special

finishes.

The term ‘pre-treatment’ summarizes all types of basic finishes such as

desizing, scouring, mercerizing and bleaching on fibre, yarn and fabric

(Smith, 2006). The aim of the preparation process is improving the quality by

removing impurities and foreign matter thoroughly and uniformly from the

fabric (Anthappan et al., 2006). For this study scouring and bleaching process

was done on 100% cotton, 50 : 50% Tencel cotton and 50 : 50 modal cotton.

Twenty meters of cotton, tencel cotton and modal cotton fabrics were

subjected to scouring and bleaching process.

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a. Cotton

c. Moda

SE

n Yarn

al Yarn

PLATE

ELECTION

E – 1 OF YARN

d.

b. Tence

. Weaving

el Yarn

Machine

45

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3.4.1 Scouring

Scouring is an important operation by which natural impurities such as

greases, waxes, fats, and acquired impurities from the fabric are removed

(NIIR Board, 2004). The following are the recipe for scouring.

Weight of the fabric - 1000 grams

Water - 10 liters

Sodium carbonate - 20 grams

Sodium hydroxide - 30 grams

Wetting agent

( Monopal soap) - 10 drops

Temperature - 80°C

Time - 60 minutes

The selected woven fabrics (cotton, Tencel cotton, Modal cotton) were

scoured in a bath contained ten litres of water, 20 grams of sodium carbonate

and 30 grams of sodium hydroxide and a few drops of wetting agent or

Monopal soap along with the fabric and were boiled for one hour. Then the

fabric was rinsed thoroughly in running water and dried in the shade. The

process was followed for modal cotton and Tencel cotton fabrics in the same

manner.

3.4.2 Bleaching

Bleaching is to impart perfect whiteness to the fabric by removing the

natural coloring matter from the fabric (Patel et al., 2006). In one word, to

bleach it as well as to eliminate any accessory impurities by which they may

become contained and more or less solid, during such operations as spinning

and weaving (Tailfer, 2008). Hence the following recipe was adapted for

scouring and bleaching of selected cotton, modal cotton and Tencel cotton

fabrics.

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Recipe for Bleaching

Weight of the fabric - 1000 grams

Distilled water - 10 liters

Sodium bicarbonate - 20 grams

Hydrogen peroxide - 20 grams

Wetting agent - 10 drops

Temperature - 80°C

Time - 60 minutes

The selected fabric was bleached in a bath contained ten litres of

distilled water, 30 grams of sodium bicarbonate and 20 grams of hydrogen

peroxide along with the fabric boiled for one hour. The fabric then was taken

and rinsed thoroughly in running water and dried in the shade. The process

was followed for cotton, modal cotton and Tencel cotton fabrics.

3.5 Plasma Treatment

The plasma technology can enhance the function of the textile and

garment such as crease resistance, UV protection and offer hydrophillic or

hydrophobic properties including anti-bacterial activity, stain resistance with

excellent hand feel, rapid drying and breathability features (Vohrer, 2009).

According to Sujatha (2010) plasma treatment is an alternative to wet

chemical fabric treatment and pretreatment process which tend to alter fabric

mechanical properties and are environmentally hazardous. Hence the

investigator decided to apply plasma on selected fabrics.

3.5.1 Selection of Gas

Plasma is an ionized gas with equal density of positive and negative

charges which exists over an extremely wide range of temperature and

pressure. The plasma gas particles etch on the fabric surface in nano scale so

as to modify the functional properties of the fabric (Muguntharajan, 2009).

Plasma treatment depends on the choice of working gas and plasma density

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and energy. Air, oxygen, argon, fluorine, helium, carbon dioxide or their

mixtures can be used as plasma medium. The process result is affected by

the type of the gas used (Pastore and Kiekens, 2001).

Oxygen plasma shows a fast etching rate by exhibiting a progressively

pilled and etched pattern only after 10 minutes of accumulated exposure

whereas argon plasma treatment shows a relatively slower etching rate and

the etched pattern appears after almost 40 minutes of accumulated exposure.

Oxygen plasma results in shrinkage causing the corncob structure

perpendicular to the fibre axis. Oxygen plasma causes more severe effects

with fire increased the depth as well as the size of the microspores etched by

the plasma increase. The dominant weight loss during plasma treatment is

mainly due to surface etching of the fibre of the fabric surface (McCord, 2003).

Hence the investigator selected oxygen gas for plasma application in the

selected cellulosic fabrics. Five meters of cotton, tencel cotton and modal

cotton fabrics were used for plasma treatment.

3.5.2 Parameters of Plasma Application Plasma Reactor

The plasma reactor supplied by M/s HydoPneoVac, Bangalore with the

chamber dimensions of 40 cm x 40 cm x 48 cm was used in the decision

process (Figure – 2 and Plate – 2). Provisions are given to treat the fabric

samples with the dimensions of 20 cm x 20 cm, using the fabric holder placed

between the parallel plates of the capacitor. The reactor is fabricated with

provisions for the inlet of gases, vacuum pump fitted to create ambient

atmosphere for treatment. The distance between the plates, voltage and

pressure applied in the reactor were optimized based on the weight loss

obtained in the scoured samples (control), which are free from any added

impurities or polymeric coating over the surface of the fibres.

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SCHEMATIC D

P

FIGURE

IAGRAM O

PLATEPLASMA CH

E - 2 OF PLASMA

E – 2 HAMBER

A REACTOOR

49

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3.5.3 Application Method

Optimization of various process conditions of the plasma reactor was

carried out using a Gray cotton fabric and weight loss on desizing (removal of

starch from gray fabric) was considered as the response variable.

The distance between the capacitor plates of the plasma reactor

decides the mean distance between the fabric and the ionized particles

present in the reactor. Higher the distance lower the capacitance value and

hence lower would be the plasma efficiency. As the distance between the

plates increased from 3.0 to 3.8 cm (while keeping 5 minutes, 600 V and

0.1 bars), the weight loss of the control samples decreased gradually from

4.82 to 4.00%, confirming the effect of the distance on capacitance and the

charged particles produced in the reactor. However, 3.2 cm was selected for

decision of the samples since at the lowest level, difficulties were observed in

placing the samples inside the reactor. The weight loss is obviously due to the

removal of the natural impurities present in the fabric, by converting them into

the soluble components (Nalankilli et al., 2008).

The capacity of a parallel plate capacitor is inversely related to the

applied voltage, and for the plasma produced inside the reactor also. As the

voltage was doubled from 600 V to 1200 V (while keeping the sample for

5 minutes, plate distance 3.0 cm and pressure 0.1 bar) the weight loss of the

control sample decreased by 40% from 6.61 to 3.91% and hence 600 V was

maintained for desizing of cotton samples.

The pressure applied inside the plasma reactor must be matched to

the characteristic structure of the textile material to be plasma treated (Abbot

and Robinso, 1977). In the low pressure regions, the mean free path in the

gas phase exceeds the typical distance in textile material and the very low

pressure causes a relatively low radical concentration per unit volume. In the

medium and high pressure ranges, the mean free path in the gas phase is

much lower than textile distances. Most of the collisions happen with other

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gas particles and reduce the lifetime of the radicals so that the particles do not

reach the reaction sites inside the voluminous fabric. As the pressure

decreased inside the chamber from 0.2 to 0.01 bars, while keeping the

sample for 5 minutes, plate distance 3.0 cm and 600 V the efficiency of the

plasma treatment increased by 33%, in terms of weight loss from 4.90 to

7.33%, confirming the theory postulated in the earlier reports.

TABLE – III DETAILS ABOUT THE PARAMETERS OF PLASMA APPLICATION

S.No. Criteria Parameters

1. Gas Oxygen

2. Inter-electrode spacing 3.5 cm

3. Plasma current 2.1 MA

4. Plasma power 600 W

5. Exposure time 2 minutes

6. Pressure 1.5 x 10-2 bar

From the Table – IV, it is clear that the plasma application was done

using oxygen with inter-electrode spacing of 3.5 cm. The plasma current and

power used were 2.1 mA and 600 W respectively. The exposure time was

2 minutes with pressure of 1.5 x 10-1 mbar. Thus the above parameters were

used in this study. After plasma treatment the fabrics underwent finishing

process on 5 metres of cotton, tencel cotton and modal cotton material.

Phase – II

The phase – II consisted of pilot study, selection of herbs and

optimization of the parameters, phytochemical analysis, selection of functional

finishes, anti-bacterial finish, mosquito repellent finish, optimization

parameters and finishing technique.

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3.6 Pilot Study

A pilot study was conducted with six different medicinal plant namely

Turmeric (Curcuma longa), Lemon (Citrus limon), Aloe vera (Barbados aloe),

Eucalyptus oil (Eucalyptus globulus), Guava leaves (Psidium guajava), Prickly

chaff flower (Achyranthes aspera) to select the best herbs. These six plants

were selected after a thorough study from the related literature. From the

above plants two of the plants Psidium guajava and Achyranthes aspera has

superior anti-bacterial property and Phyllanthus niruri, Vetiveria zizanioides

had more mosquito repellent property. Hence the above said four herbs were

selected for this study.

3.7 Selection of Finishes

From the survey the consumers' requirements such as special finishes

like anti-bacterial and mosquito repellent herbal finishes on the needed

garments. Hence mosquito repellent and anti-bacterial finishes were selected

for this study.

3.8 Selection of Herbs

A review of literature on the anti-microbial activity of plants and plant

derived products revealed that may significant contributions have been made

on the bioactivities of medicinal plants. Herbal spices are important sources of

anti-bacterial and mosquito repellent properties. Therefore based on the

literature survey the following herbs were selected such as guava leaves

(Psidium guajava), prickly chaff flower (Achyranthes aspera), keelanelli

(Phyllanthus niruri) and vetiver roots (Vetiveria zizanioides) from the pilot and

literature survey.

3.8.1 Collection and Storage of Natural Herbs

The collected leaves were dried under shade. After drying, the grinding

was carried out to break down the leaves into a fine powder

(Thilagavathi et al., 2007). The powdered guava leaves (Psidium guajava),

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prickly chaff flower (Achyranthes aspera), keelanelli (Phyllanthus niruri) and

Vetiver root (Vetiveria zizanioides) were stored in air tight container separately

(Plates – 3a to 3h).

3.9 Selection of Extraction Procedure

Extraction refers to the separating of a desired material by physical or

chemical means with the aid of a solvent. The extraction of a selected natural

source can be carried out by various methods like aqueous, alkaline, acidic or

alcoholic methods. In case of alkaline and acidic extractions, solutions of any

alkali or acids used. In alcoholic extraction, alcohols like ethanol or methanol

are extensively used for the extraction process. Alcoholic extraction using

ethanol is more effective to extract the active ingredients of the natural

sources. Hence, the herbal powder was subjected to alcoholic extraction

(Plates – 4a to 4c).

3.9.1 Solvent Extraction of Herbs

Extraction was carried out by dissolving 6 grams of the herbal powders

of guava leaf (Psidium guajava), prickly chaff flower (Achyranthes aspera),

keelanelli (Phyllanthus niruri) and vetiver root (Vetiveria zizanioides) in 100 ml

consisting of 80% ethanol and distilled water. The containers were closed and

kept for overnight under shaking condition for proper dissolving of the

compounds into solvent. Then the extract was filtered using Whatman no. 1

filter paper, the filtrate was collected and evaporated at room temperature.

Recipe for Herbal Extraction

Powder : 6 gm

Ethanol : 100 ml consist of 80% ethanol and

balance distilled water

Time : 24 hours

Temperature : Room temperature

Weight of the fabric : 1000 gms

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a. Guava

c. Vetiver

e. G

g.

a Leaves (P

Roots (Vet

Guava Lea

Vetiver Ro

SE

Pisidium gu

tiveria zizan

ave Powder

oot Powder

PLATE

LECTION O

uajava)

nioides)

r

r

E – 3 OF HERBS

b. (Achy

d. Keela

f. Prick

h

S

Prickly Chayranthes a

anelli (Phyl

kly Chaff F

. Keelanell

aff Flower aspera Linn

yllanthus ni

lower Pow

i Powder

54

n.)

iruri)

wder

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EX

a. and b.

PLATEXTRACTION

Herbal Ext

c. Citric

E – 4 N METHOD

traction So

Acid

olution

55

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3.10 Phytochemical Analysis

The portion of the dry extract was subjected to the phytochemical

screening (Trease,and Evans,(1985) and Harbourne,(1998). Phytochemical

screening was performed to test alkaloids, phenols, flavonoids, triterpenoids

and tannins.

3.10.1 Phytochemical Screening of the Herbal Extract

The selected herbal extracts were tested for the presence of some

active chemical compounds such as alkaloides, flavanoids, phenolics,

tannins, saponins and terpenoids. The analysis was conducted as per the

methods (Khandewal, 2002).

3.10.1.a. Identification of Alkaloids

To 5 grams of the each plant sample added 50 ml of 5% HCl and

heated in a boiling water bath for one hour and filtered separately. To the

filtrate added 5 ml of dilute ammonia and 5 ml of chloroform. The ethanol

layer was taken for the following tests.

3.10.1.b. Dragendroffs Test

To one ml of the ethanol layer 1 ml of Dragendroff’s reagent was

added. Formation of orange precipitate indicated the presence of alkaloids.

3.10.1.c. Wagner’s Test

One ml of the ethanol layer was treated with few ml of Wagner’s

reagent. Formation of reddish brown precipitate indicated the presence of

alkaloids.

3.10.1.d. Identification of Flavanoids

The following tests were carried out to assess the presence of

flavanoids in the selected herbs.

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3.10.1.e. Shinoda Tests

To 5 grams of the each herbal extracts added 50 ml of ethanol and

heated in a boiling water bath. For ethanolic extract, 8-9 drops of

concentrated HCl and some magnesium fillings were added. After 10-15

minutes at room temperature red colour formation indicated the presence of

flavanoids.

3.10.1.f. Decolorization Test

Each herbal extract was reduced to dryness in the boiling water bath

separately. The residue was treated with dilute NaOH followed by addition of

dilute HCl. Yellow solution with NaOH which turns colourless with dilute HCl

indicated the presence of flavanoids.

3.10.1.g. Ammonia Test

Filter paper strips were dipped in the ethanolic extract and

ammoniated. The filter paper changed its colour to yellow indicated the

presence of flavonoids. Added 10 ml of concentrated H2SO4 to the above

yellow coloured filter paper. Disappearance of the yellow colour confirmed the

presence of flavanoids.

3.10.1.h. Identification of Terpenoids

To 0.5 grams of the herbal extracts add 2 ml of chloroform. The

chloroform extracts added 5 ml of concentrated H2SO4 along the sides of the

test tube. Reddish brown colouration in the interphase indicated the presence

of terpenoids.

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TABLE – IV PHYTOCHEMICAL TEST SCREENING

S.No. Plant

extract (Ethanol)

Code

Alkaloids Flavanoids Terpenoids

Dragendorff test

Wagner’s test

H2SO4 test

NaOH test

Shinoda test

Liebermann – Burchard

test

1. Psidium gujava leaves

PG + - - + - -

2. Achyranthes aspera leaves

AA + - - - - -

3. Phyllanthus niruri leaves

PN + - - + - + (Sterol)- Terpenoid

4. Vetiveria zizanioides root

VZ + - + + - -

(+) Presence (-) Absence

The presence of different phytochemical components in the leaves of

guava, prickly chaff flower, keelanelli and vetiver root extracts were identified

using standard phytochemical screening test. From the Table – IV, it was

understood that different phytochemicals were evident in the selected herbal

powders. The major components present in the selected herbal extracts were

alkaloids, steriods and flavanoids. These components have been found to

possess anti-bacterial and anti-viral activity.

3.10.2 Spectroscopic Study – FTIR Analysis

The FTIR spectral analysis was carried out to identify the functional

groups present in Pisidium gujava, Acharanthus aspera Linn., Vetiveria

zizanioides and Phyllanthus niruri.

Spectra were collected on a bench FTS 3000 MX spectrometer

(Varian Instruments, Randolph, MA) equipped with KBr beam splitter.

Fourier transform infrared spectroscopy (FTIR) was an analytical tool to

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identify the nature of chemicals present in the herbal powder. It also helps to

know to what extent the molecules of the finishing chemicals are attached

with fibre molecules of the specimen. The samples were analyzed for their

variations in chemical groups using FTIR spectroscopy. The same test was

carried out by Usha et al. (2010). Infrared spectroscopy was used to identify

and quantitatively analyze chemical compounds, mixtures, extent of reaction,

and molecular structure. Different chemical compounds absorb infrared

radiation at frequencies corresponding to their own molecular vibration

frequencies. According to Kale and Balaskar (2010), Infrared (IR)

spectroscopy is a chemical analysis technique which measures the absorption

of different IR frequencies by a sample positioned in the path of an IR beam.

The main goal of the IR spectroscopic analysis was to determine the chemical

functional groups in the sample.

3.11 Optimization Procedure

After extraction of herbs the optimization was done to get accurate

values by doing many combination and composition of herbs. The optimized

parameters were selected for time, temperature and other criteria’s before

finishing on the fabric for anti-bacterial and mosquito repellent activity.

3.11.1 Optimization Parameters for Finishing

The three fabric samples, cotton, Tencel cotton and modal cotton were

padded with different concentrations, temperature and time to find out the

optimized parameters for time 3, 5, 10 minutes to finish the herbal sources on

the three fabrics. For temperature 40°C, 50°C, 60°C and 80°C were set for

treating the fabric for effective finishing.

The concentration was considered as an important aspect in curing the

fabric during the finishing process. To optimize the concentration 4, 6, 8 and

10 grams of herbal powder was dissolved in 100 ml of 80% ethanol and

distilled water. Citric acid was considered as an important aspect in binding

the herbs on the fabric in the finishing process. Thilagavathi and Kannian

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(2008) suggested that citric acid gives good result as a mordant. Hence the

investigator was selected citric acid as a binder for optimizing the

concentration of binder, 6, 7, 8, 9% of citric acid was mixed with herbal extract

and finished on the selected fabrics. The bacteria grow at neutral pH.

However the growth of bacteria is hindered in acidic or alkaline pH. After a

thorough investigation the optimized parameters such as time, temperature,

concentration, binder concentration and pH were 15 minutes, 80°C, 6 g, 9%

and pH 4-5 respectively. This optimized parameter were used for this study is

given in Table – V.

TABLE – V

OPTIMIZED PARAMETERS

S.No. Criteria Pilot study Selected parameters

1. Herbal solution

4, 6, 8 and 10 g / 100 ml of 80% of ethanol

6 g / 100 ml of 80% of ethanol

2. Citric acid 6, 7, 8 and 9% 9%

3. Time 15 minutes 15 minutes

4. Temperature 80°C 80°C

5. pH 4-8 4.5

3.11.2 Method of Finishing

There are basically three types of method viz., (i) pad application,

(ii) exhaust application and (iii) spray method (Gauraw, 2013). Among these

methods pad-dry cure method gives best result and the finishing agent

impregnated thoroughly. Hence pad-dry-cure method is selected for the study.

3.11.3 Padding Mangle Method

Natural finishing has become a part of human life since the time

immemorial. India has a rich cultural heritage and the tradition of using

finishes obtained from natural sources. There is an increasing realization in

the textile industry as well as among the textile consumers to develop and

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demand eco-friendly methods of finishing textiles (Pardeshi and

Manjrekar, 2003). The durability of the finishing can be enhanced when the

herbal extracts were applied to the fabric directly by pad-dry-cure method

(Kumar, 2007).

Application of finishes in padding mangle is more convenient and many

of the problems related to exhaust techniques can be avoided primarily in

padding stage. In padding technique, the fabric was passed through two iron

rollers revolving at different speeds in the opposite direction (Sampath, 2003).

The bleached and plasma treated fabric was finished with optimized

parameters (Saini, 2004). The extracted solution was poured inside the

padding mangle and the fabric was passed inside the machine for 30 minutes.

The fabric cured inside the dry oven for 15 minutes at 80°C for the good

penetration of the finishing agents. Then the fabric was removed from the

curing chamber and the fabric was washed thoroughly and dried in shade.

TABLE FABRIC SAMPLE PREPARATION FOR FINISHING USING PADDING MANGLE

S.No. Particulars Parameters

1. Finishing solution Material liquor ratio (MLR) 1 : 20

2. Binder solution 9 : 1

3. Curing temperature 80°C – 100°C

4. Curing time 2 minutes

For this study, the above described padding mangle was selected. The

fabric was immersed in the prepared anti-bacterial and mosquito repellent

solution in the ratio of 1 : 20 of the material liquor ratio of three times with the

binder in the ratio of 9 : 1 for the effective penetration into the fabric. Then the

fabric was passed through the padding mangle (Plate – 5) between the rollers

for uniform application of the solution. The fabric is dried in the open air under

the shade at room temperature and cured at 80°C – 100°C for two minutes for

cotton, modal cotton and tencel cotton for permanent impregnation.

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PADD

PLATEING MANG

E – 5 GLE MACHIINE

62

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Two groups of fabric samples were used in this study, the first group of

samples was plasma treated fabrics (100% cotton, (50 : 50) Tencel : cotton,

(50 : 50) modal : cotton) was finished with guava extract and prickly chaff

flower extract separate bath. In the second group of samples, untreated

(plasma) fabrics (100% cotton, (50 : 50) Tencel : cotton, (50 : 50) modal :

cotton) were finished with similar guava extracts and prickly chaff flower

extracts separately for anti-bacterial activity. For mosquito repellant finish the

keelanelli and vetiver extracts were finished separately with the same

parameters in two different bath. All the samples were padded with 8% citric

acid in a padding mangle at different pressure condition and rpm with 100%

wet pickup followed by drying and curing at 160°C for 5 minutes. The above

finishes were done on cotton, tencel cotton and modal cotton fabrics.

Phase – III

The phase – III is consisted of evaluation and comparison of properties

of unfinished, finished and finished on plasma treated samples. The

evaluation was done to find out the physical, mechanical, comfort and

absorbency properties. The changes occurred during finishes and

composition with unfinished and plasma treated samples.

3.12 Evaluation of Fabrics

Textile testing as a whole refers to the vigorous testing done on textile

materials which may be inside the laboratory as well as in its natural setting,

or in the day-to-day uses, using various testing equipments (Jewel, 2005).

It plays a crucial role in gauging product quality, ensuring regulatory

compliance and assessing the performance of textile materials.

3.12.1 Physical Properties

The finished fabrics were evaluated for physical properties namely

weight, thickness and count.

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3.12.1.a. Fabric Weight – ASTM D 3776-96

Fabric weight is the relative weight of the fabric and expressed as the

weight of a particular size piece, in grams per square meter or ounces per

square yard. The investigator cuts the samples from unfinished, finished and

plasma treated finished fabrics by using GSM Die Cutter (Plates – 6a and 6b)

and weighed round the fabric using a digital weighing balance. Five readings

were noted for each and the individual mean was calculated.

Grams per square meter (GSM) = square of Area

(g)fabric the of Weightx square metre

Square meter = 100 cm x 100 cm = 10000 cm2

Area of square = Length x Breadth square units.

The same procedure was followed to find out the fabric weight of

unfinished, finished and finished with plasma samples used in the present

study. Fabric weights were carefully recorded and using the above formula.

The mean difference will be calculated.

3.12.1.b. Fabric Thickness – ASTM D 3883-2004

Thickness is defined as the distance between the upper and lower

surface of the material measured under a standard pressure using the

thickness gauge. The thickness of a fabric is one of its basic properties, giving

information on its warmth, heaviness or stiffness in use. Thickness

measurements are rarely used as they are very sensitive to the pressure used

in the measurement. Fabric weight per unit is used commercially as an

indicator of thickness (Basu and Chellamani, 2006).

The Fabric Thickness Tester (Plate – 6c) a handy instrument was used

to find out the thickness of the sample. The fabric is kept between two plane

parallel places and a known arbitrary pressure is applied between the plates

and maintained. Then the distance between the plates is noted from the dial

gauge. Ten readings were taken at random, and the mean was calculated to

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find out the thickness of the original, finished and plasma treated finished

fabrics. This was repeated for 10 times to find out the accurate value.

3.12.1.c. Fabric Count – ASTM D 1059-01

The determination of fabric count measures the number of warp yarns

per inch and number of weft yarns per inch (Angappan and

Gopalakrishnan, 2002). The fabric count is the number of warp and weft yarns

per unit distance. The fabric is kept without tension and is free from folds and

wrinkles. The determination of the number of threads per inch may be made

by counting glass (pick glass). The counting glass is a small magnifying glass

on a stand over a square exactly one inch way. The number of threads in the

field directly gives the number of threads per inch. This is the method

generally used for fabric count. The number of ends and picks per inch were

counted in five different places and recorded for the unfinished, finished and

plasma treated finished samples. This was repeated for 10 times to find out

the exact value from average.

The fabric count is the number of warp yarn per inch and the number of

weft yarn per inch. In the woven fabric, the warp yarns are referred to as ends

and weft yarns as picks. Therefore, a fabric is described in terms of “ends and

picks”. Pick glass / magnifying glass (Plate – 6d) was used to find out the

fabric count of the samples. The glass was placed randomly at different

places and the number of repeats was found by analyzing the weave. Five

readings were taken and recorded for all the samples to find out whether

there was any shrinkage or elongation during the finishing treatment for 10

times to find out the accurate answer.

3.12.2. Mechanical Properties

Mechanical properties of the finished fabrics were evaluated by

strength, elongation and abrasion resistance method.

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3.12.2.a. Fabric Tensile Strength – ASTM D 5034

The maximum tensile stress required to rupture a fabric is expressed in

kilogram. The Eureka cloth tensile strength tester was used to measure the

strength and elongation. The fabric was cut into 30 cm x 7.5 cm using

template and placed in between the clamps. The load was applied to the

sample. When the sample was torn, the movement of the lower clamp was

reversed. The strength in kilogram was noted from the dial. Ten readings

were taken for concordance (ASTM TM 5035-03, 2005) (Plate – 6e).

3.12.2.b. Fabric Elongation – ASTM D 5034

Elongation is the increase in length of a specimen during a tension test,

expressed in units of length of the fabric when loaded. The Eureka model

tensile strength tester was used for the study. The rate of traverse and

capacity of the machine was 48 cm per minute and 90 kg respectively. The

gauge length was kept at 25 cm. The dial of the machine was calibrated in

pounds and kilograms.

Ten samples from each of the fabrics with a minimum length of

33.02 cm and a width of 3.81 cm were cut from the warp and weft directions

separately. Each sample was ravelled out to 2.54 cm width and 30.48 cm

length of yarns of the two sides. Each sample was clamped firmly between

the two jaws. Care was taken to ensure that the sample was perpendicular to

the load. The load was applied to the sample which was broken. The dial

reading of elongation in centimeters was noted. Ten readings were noted for

each sample and the mean value was calculated (ASTM TM 5035-03, 2005)

for all three groups of fabrics to find out the reaction of finishes.

3.12.2.c. Fabric Abrasion Resistance – ASTM D 4158

Abrasion is one aspect of wear and is rubbing away of the component

fibres and yarns of the fabric. Abrasion may be classified as plane or flat

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abrasion, edge abrasion or flex abrasion (Jewel, 2005). Abrasion is the

wearing a way of any part of a material by rubbing against another surface.

The Martindale Abrasion Tester (Plate – 6f) is a useful instrument for

determining the resistance to abrasion of all clothes. The severity of the

abrasion varies with the nature of the radiation. Five samples were cut in

random from each of the samples using a template dimension. The initial

weight of the sample was taken accurately using an electronic weighing

balance. Then the sample was mounted on sample holders with 200 gms

weight. The rubs were standardized to 34 revolutions. The samples were

made to rub against the abrasive surface. After 34 revolutions the samples

were removed and the final weight of each sample was taken. The weight loss

due to abrasion was calculated. The same procedure was repeated for all the

samples. The mean value of the five readings for each of the sample is

calculated. The loss in weight of each material was recorded separately to

find out the abrasion resistance of the original, finished and plasma treated

finished fabrics.

Abrasion is measured by a straight line which becomes a gradually

widened ellipse, until it forms another straight line in the opposite direction

and traces the same figure against under known condition of pressure and

abrasion (ASTM Standards, 2005). Abrasion is the wearing a way of any part

of a material by rubbing against another surface (ASTM, 2000). Abrasion is

one of the major criteria to assess the durability of the fabric and this was

repeated for 10 times.

3.12.3. Comfort Properties

This property was evaluated to find out the comfortability of the fabric

before and after finishing of 3 groups of fabrics. It includes fabric stiffness,

crease recovery and air permeability.

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3.12.3.a. Fabric Stiffness – BS 3356 – 1990

Fabric stiffness is explained as a combined effect of elastic property

and mass per unit area (Chaudhuri, 2001). Stiffness is the ability of a textile

fabric to resist changes in shape due to bending deformation. The bending

properties like stiffness, drape, handle and crease recovery is the prime

parameters of evaluating the fabric.

Stiffness is the ability of a material to resist deformation. Bending

length is the length of a fabric that will bend on its own weight, to a definite

extent. It is a measure of the stiffness that determines the draping quality.

The Shirley stiffness tester was used to determine the stiffness of the

fabrics. A scale of 15 cm length and 2.5 cm width formed the templates. Ten

samples were cut at random both in the warp and weft directions from each of

the fabrics from 3 groups of fabrics. Each fabric along with the scale was

mounted on a horizontal platform. The scale was moved along with the

sample slowly until the fabric fell to the edge of the platform and the tip of the

fabric coincided with the index line, which was viewed in the mirror. The

bending length was recorded from the scale marked opposite to the zero on

the side of the platform. Ten readings were taken and the mean value

calculated (ASTM TM 1388-02-2005) (Plate – 6g).

3.12.3.b. Fabric Air Permeability – (ASTM D 737 – 04)

Air permeability of a fabric is the volume of air measured in cubic cm

passed per second through 1 sq.cm. for the fabric at a pressure of one cm.

Head of water.

The Air Permeability Tester (Plate – 6h) consists of a circular clamp to

hold the specimen and a spring loaded clamp to press the specimen while

testing, the room atmospheric air was drawn through the specimen by means

of a suction pump. The rate of air flow was adjusted to desired pressure drop

across the fabric which was indicated on drought gauge graduated from

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c

e. Tensil

a. GSM C

c. Thicknes

le StrengthTesting M

g. Stiffness

FA

Cutter

ss Guage

h and ElongMachine

s Tester

PLATE

ABRIC EVA

gation

E – 6 ALUATION

b.

f. Abra

h. A

. Weighing

d. Pick G

asion Resis

Air Permeab

g Balance

Glass

stance Tes

bility Teste

69

ster

er

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0.25 mm. The rate of air flow was read from the Rotameters. They were

calibrated to indicate air flow in cubic centimeter per second at 27°C and

760 mm of mercury. The area of the sample exposed to air was one inch in

diameter. From the reading Rotameter air permeability was calculated using

the following formula :

Air permeability = sq.cm.)sec / (cc / air to exposed sample of Area

flow air of rate Average

Then the mean was calculated and analyzed for three groups of fabrics

performed for ten times.

3.12.4 Absorbency Properties (AATCC 79 : 2007)

The wettability and absorbency tests include drop, sinking and vertical

wicking test. This test was conducted to find out the absorbency property of

three groups of fabrics to know the absorbency quality for the wear.

3.12.4.a. Drop Test

The drop test is a count of the number of drops required to penetrate

through to the under scale of the fabric when all the drops fall on the same

spot (AATCC Technical Manual, 2008). A burette filled with distilled water was

clamped in a stand. The stand was mounted in an embroidery frame and was

placed at the base of the stand. The distance between the sample and the

burette nozzle was kept constant. The nozzle of the burette was opened just

to allow a drop of water to fall on the sample. The stopwatch was started

simultaneously and it was stopped when the drop of water was fully absorbed

into the material. The time taken for this was noted. The same procedure was

carried out for the unfinished and finished and plasma treated finished

samples. The mean value was calculated to get accurate value (Plate – 7a).

3.12.4.b. Sinking Test

Sinking time test is a simple test that helps to measure the wettability of

a fabric (AATCC, 2008). In this method, each fabric was cut into a number of

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equal sized squares of 1” x 1” and added to a 1000 ml beaker which was filled

with distilled water. The stop watch was started when the fabric struck the

surface of water and stopped when the last corner was sunk below the water

surface. The test was repeated 10 times for all the fabrics and the mean time

for the sinking was calculated and recorded (Plate – 7b).

3.12.4.c. Vertical Wicking Test (AATCC – 197)

The Vertical Wicking Method measures the rapidity of absorption. Ten

samples were cut into size of 11 inches in length and 1 inch width from each

sample. One end of the sample strip was pasted with a glass rod which was

placed on heavy wooden blocks and the other end was allowed to immerse in

a tray of distilled water. The rise of the water level in the strip was noted by

keeping the length of the fabric as 5 cms constant. The same procedure was

repeated for all the samples. The mean values of ten readings were

calculated and recorded. The vertical wicking of each material was recorded

carefully to find the absorbency of original, finished and plasma treated

finished fabrics. The mean values of ten readings were calculated and

recorded (Plate – 7c).

3.12.5 Anti-bacterial Assessment Test (Qualitative Test)

The anti-bacterial activity of the fabric was assessed using standard

AATCC 100 and 147 test methods. The activity was evaluated by both

qualitative and quantitative test methods. For qualitative assessment used

Agar diffusion and parallel streak method (AATCC 147-2000). Percentage

reduction test was used for quantitative assessment.

3.12.5.a. Agar Diffusion Test Anti-bacterial activity by well diffusion method (Rojas et al., 2006)

The anti-bacterial activity of the Herbal ethanolic extraction (guava

leave and prickly chaff flower) was evaluated by the Agar well diffusion

method. Sterile nutrient plates were prepared. The plates were allowed to

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a.

. Drop Test

ABSO

t Machine

c. V

PLATEORBENCY P

Vertical Wi

E – 7 PROPERTI

b. S

cking Test

IES

Sinking Te

t

est Method

72

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solidify for 5 minutes and wells of 6 mm were punctured using a well borer.

0.1% inoculum suspension of Staphylococcus aureus (ATCC 6538) and

Escherichia coli (ATCC 8739) were swabbed uniformly over the surface of the

agar. 100 µl of each herbal extract was loaded into the well and the plates

were kept in incubation at 37ºC for 24 hours. The anti-bacterial activity was

evaluated in terms of zone of inhibition, measured and recorded in

millimeters. All the unfinished, finished and plasma treated finished fabric was

evaluated for the above test.

3.12.5.b. Parallel Streak Test

The agar diffusion test has a long-standing traditional place in

microbiology analysis. This method can be recommended as a quick and

preliminary qualitative method (Hipler and Peter, 2006 and Mercy and

Thambidurai, 2009).

Mullar Huton agar media was prepared and sterilized at 121°C at

15 lbs for 15 minutes. In these sterile media five parallel streaks of the

respective test organisms were streaked. The unfinished, furnished and

plasma treated finished fabric samples were cut to a size of 21 inch and

placed perpendicular on the streaked lines. Then the plates were incubated at

37°C for 24 hours. The anti-bacterial activity was evaluated in terms of zone

of inhibition, measured and recorded in millimeters. This test followed for

three groups of fabrics.

3.12.6 Anti-bacterial Assessment Test (Quantitative Test) 3.12.6.a. AATCC Test Method 100 – 2004 Anti-bacterial Activity of Herbal Extract Finished Fabrics by AATCC Test Method 100 - 2004

All the finished fabrics were subjected to determine anti-bacterial

activity. About 1.0 ml of 12 hours test bacteria (E. coli and S. aureus) were

inoculated as droplets over the 3 swatches (test fabrics about 50 mm) using a

micropipette. After all the samples were inoculated, the flask was incubated at

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37 ± 2°C for 18 h before being assayed for bacterial population density. The

bacterial population density was determined by extracting the bacteria from

the fabric by adding 100 ml of distilled water to each flask and shaken using

an orbital shaker for 1 minute. Then aliquots were serially diluted and pour

plated to determine the bacterial density. The difference in the number of

viable bacteria was evaluated on the basis of the percentage reduction.

Percentage reduction was calculated using the following formula.

R = (B – A) / B x 100

Where, R is percentage reduction; A is the number of bacteria recovered from

the inoculated treated test specimen swatches in the jar incubated over the

desired contact period (18 hours); B is the number of bacteria recovered from

the inoculated treated test specimen swatches in the jar immediately after

inoculation (at ‘0’ contact time) (Plates – 8a to 8g).

3.12.6.b. Wash Durability Testing (AATCC 124-1996)

The samples were washed with 5% neutral soap solution for

20 minutes and dried. The washed samples were tested for the retention of

anti-bacterial activity after every 5 launderings for 20 washes using standard

procedures. The anti-bacterial assessed by quantitative method bacterial

reduction test (AATCC test method 100-2004) the results were compared with

the unwashed fabric sample.

3.12.6.c. AATCC Test Method 124-1996 Appearance of Fabrics after Repeated Home laundering Hand Wash

Dissolve 20.0 ± 0.1 g of 1993 AATCC Standard Reference Detergent

(Tide) in 7.57 ± 0.06 L (2.00 ± 0.02 gal) of water at 40°C in a 9.5 L and then

add the three fabric test specimens. Wash for 2.0 ± 0.1 minutes with no

twisting or wringing. Rinse once using 7.57 ± 0.06 L (2.00 ± 0.02 gal) of water

at 41 ± 3°C (105 ± SF). Remove the specimens and to drip dry.

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PLATE – 8 ANTI-BACTERIAL ACTIVITY TEST AATCC – 100 METHOD

a. Control (E. coli and S. aureus)

b. Cotton AATCC 100 (E. coli) c. Cotton AATCC 100 (S. aureus)

d. Tencel Cotton AATCC 100 (E. coli)

e. Tencel Cotton AATCC 100 (S. aureus)

f. Modal Cotton 100 (E. coli) g. Modal Cotton AATCC 100 (S. aureus)

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Machine Wash

Use a specified water level, the selected water temperature of the

washing cycle and a rinse temperature of less than 29°C. Add 66 ± 0.1 g of

1993 AATCC Standard Reference Detergent TIDE, a commonly used

detergent, may be used. In case of dispute the affected parties should use

1993 AATCC Standard Reference Detergent. Add test specimens and

enough ballast to make a 1.8 ± 0.06 kg load. Set the washer for the selected

washing cycle and time. Normal or Cotton Sturdy are recommended. Remove

the specimens and drip dry.

Drip Dry

Hang each dripping wet fabric specimen by two corners with the fabric

length in the vertical direction. Allow the specimens to hang in still air at room

temperature until it dries.

TABLE – VI WASHING MACHINE CONDITIONS

Normal/Collon Sturdy Delicate Permanent Press

Water Level 18 ± 1 gal 18 ± 1 gal 18 ± 1 gal

Agitator Speed 179 ± 2 spm 119 ± 2 spm 179 ± 2 spm

Washing Time 12 minutes 8 minutes 10 minutes

Spin Speed 645 ± 15 rpm 430 ± 15 rpm 430 ± 15 rpm

Final Spin Cycle 6 minutes 4 minutes 4 minutes

Ballast: In a vessel that travels on the water, the ballast will remain below the water

level, to counteract the effects of weight above the water level

3.12.7 Mosquito Repellency Test

There are different types of testing methods for evaluation of mosquito

repellent textiles, such as cone test, cylinder test, field test and excito-

repellency standard test systems. Among the standard tests listed, Excito-

chamber standard test was carried out to study mosquito repellent activity.

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3.12.8 Testing of Mosquito Repellency

The mosquito repellent efficiency of the finished fabric was tested using

the modified excito chamber method. There have been numerous attempts to

accurately measure the behavioral responses of mosquitoes to insecticides

using various types of excito-repellency test systems. The test method

adapted in the present study for testing the mosquito repellent property is

modified in the fabric inside the excito chamber method.

Repellency is known to play an important role in preventing the vector

born diseases by reducing man-vector contact. Synthetic chemicals and

insecticides used for control of vectors are causing irreversible damage to the

eco-system, as some of them are non-degradable in nature. The

phytochemical derived from plant resources can act as larvicides, insect

growth regulators, repellents and ovipositional attract, having deterrent

activities observed by different researchers (Plate – 9a and 9b).

3.12.9 Mosquito Collection

Anopheles mosquitoes were identified based on morphological keys

and they were collected during the evening hours. All mosquitoes were

starved of blood and sugar of 4 hours before the tests.

3.12.10 Repellency Behavioural Tests

Specially designed two extra repellency test chambers were used to

evaluate the efficiency of repellent activity. The wooden outer chamber of

excito-repellency testing device measures 34 cm × 32 cm × 32 cm and faces

the front panel with the single escape portal. The box is composed of a rear

door cover, an inner Plexiglas glass panel with a rubber latex-sealed door, a

Plexiglas holding frame, a screened inner chamber, an outer chamber, a front

door, and an exit portal slot. Mosquitoes were deprived of all nutrition and

water for a minimum of 4 hours before exposure.

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PLATE – 9 MOSQUITO REPELLENCY TESTING METHOD

a. Excito Chamber 1

b. Excito Chamber 2

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Laboratory tests were performed during day light hours only and each

test was repeated four times. Observations were taken at one-minute interval

of 30 minutes. After each test was completed, the number of escaped

specimens and those remaining in the chamber were recorded separately for

each exposure chamber, external holding cage, and paired control chamber.

Escaped specimens and those remaining in the chamber, for the treated

samples, were held separately in small holding containers with food and

water.

3.13 Scanning Electron Microscopy Analysis

Scanning Electron Microscopic analysis was done to study the surface

morphology of the fabrics. The surface morphology of the finished and plasma

treated finished cotton Tencel cotton and modal cotton fabrics with guava leaf

(Psidium guajava), prickly chaff flower (Achyranthes aspera), keelanelli

(Phyllanthus niruri) and vetiver (Vetiveria zizanioides) treated fabric was

studied (JEOL/EO JSM 6390). Metal coating was used as the conducting

material to analyze the sample. The SEM working on an accelerating voltage

range from 0.5-20KV and the specimen size is 8 mm to 150 mm for finishing

fabric.

3.14 Wear study

The wear study was conducted through selected adolescent girls who

worn the herbal anti-bacterial armpit pad. A total of 18 armpit pads were

stitched from the unfinished, finished and plasma treated fabrics of cotton,

tencel cotton and modal cotton finished with guava leave and prickly chaff

flower extracts. Subjective evaluation was mainly carried out to know to judge

the comfort and odour. The respondents were asked to use the armpit pads

for 7 hours from 10 am to 5 pm on alternate days after every subsequent

wash with a neutral soap. The respondent’s opinion was collected to record

the comfortness and odour retention after repeated use and wash.

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Three cushion covers were constructed from the plasma treated and

the vetiver and keelanelli finished cotton, tencel cotton and modal cotton and

from the plasma untreated and finished vetiver and keelanelli on cotton, tencel

cotton and modal cotton. Six cushion cover was constructed was used for

performance study. Three personnel’s were selected based on the

convenience sampling. They were asked to use the cushion cover for three

hours from 6 to 9 pm when they are taking rest on the bed for 10 days. The

performance of finish was noted by using the prepared questionnaire.

Respondents opinion were recorded. The procedure was followed for both the

plasma treated and untreated cushion covers.

3.15 Statistical Analysis of the Test Results

The findings of the fabric properties of unfinished cotton, tencel cotton

and modal cotton, fabrics which was herbal finished such as guava leaf

(Psidium guajava), prickly chaff flower (Achyranthes aspera), keelanelli

(Phyllanthus niruri) and vetiver (Vetiveria zizanioides) and plasma treated

finished cotton, tencel cotton and modal cotton fabrics were analyzed using

standard deviation and one way ANOVA to determine whether there is any

difference between the samples.

Conclusion Summary of Experimental Procedure

As is evident from the detailed discussion on the experimental

methodology and procedure followed in the research work, the investigative

part of the thesis work can be grouped into three phases as shown in

Figure – 1.

Phase – I of the study dealt with the consumer survey that focused on

understanding the consumer awareness on the use of health care products

which contains anti-bacterial finishes. The outcome of the survey revealed

that there is not much awareness on the advantages on the use of health care

products that contain anti-bacterial finishes. This result shows that there is a

need to have greater understanding on the development of such products in a

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cost effective manner. The development of cost effective health care products

will result in greater acceptance of these products and will lead to penetration

of such products in the market. Having gained this understanding, the thesis

focused on developing natural and herbal based finishes that can be applied

to natural fibre blends.

Phase – II of the work focused on selected of herbs such as

anti-bacterial and mosquito repellence which could impart functional effects

such as anti-bacterial and mosquito repellence to the fabric. The details of the

materials used and the finishing treatments are given in above Table – XXXX.

Two finishing procedures were followed. Procedure one involved the

direct application of herbs such as Pisidium guajava (Guava), Achyranthes

aspera (prickly chaff flower), Phyllanthus niruri (keelanelli) and Vetiveria

zizanioides (vetiver) on to the fabric material made from cotton, Tencel/cotton

and Modal/cotton. The second procedure involved plasma pre-treatment to

the three fabric materials and subsequent to the plasma pre-treatment, fabrics

were subjected to anti-bacterial and mosquito repellent finishes.

In summary, these experimental set-ups help to understand :

a. The effect of natural herbs on functionalities such as anti-bacterial and

mosquito repellent properties;

b. The influence of plasma pre-treatment on these finishes.

Overall, 21 different types of fabrics which include natural herbs treated

fabrics without any pretreatment and plasma pre-treated fabrics with

subsequent natural herb treatments were investigated as shown in

Table – XXXXX.

Phase – III of the experimental work focused on the evaluation of

anti-bacterial and mosquito repellent properties and basic characteristics of

the fabric before and after treatments as shown in Table –XXXXXXX.

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3.16 Nomenclature

The nomenclature used for samples are given in Table – VII.

TABLE – VII NOMENCLATURE

S.No. Nomenclature Fabric samples

1. A Original cotton

2. AG1 Guava finished cotton

3. AG2 Plasma treated guava finished cotton

4. AP1 Prickly chaff flower finished cotton

5. AP2 Plasma treated prickly chaff flower finished cotton

6. B Original tencel cotton

7. BG1 Guava finished tencel cotton

8. BG2 Plasma treated guava finished tencel cotton

9. BP1 Prickly chaff flower finished tencel cotton

10. BP2 Plasma treated prickly chaff flower finished tencel cotton

11. C Original modal cotton

12. CG1 Guava finished modal cotton

13. CG2 Plasma treated guava finished modal cotton

14. CP1 Prickly chaff flower finished Tencel cotton

15. CP2 Plasma treated prickly chaff flower finished modal cotton

16. A1 Vetiver and keelanelli finished cotton

17. A2 Plasma treated veiver and keelanelli finished cotton

18. B1 Vetiver and keelanelli finished tencel cotton

19. B2 Plasma treated vetiver and keelanelli finished tencel cotton

20. C1 Vetiver and keelanelli finished modal cotton

21. C2 Plasma treated vetiver and keelanelli finished modal cotton