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Integrated system and process to increase the recovery of ethanol and co-production of isoamyl alcohol TECHNOLOGY PROFILE: Higher ethanol recovery and production of isoamyl alcohol from fusel oil distillation Get to know the technology that enables higher ethanol recovery without increasing energy consumption

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Integrated system and process to increase the recovery of ethanol and co-production of isoamyl alcohol

TECHNOLOGY PROFILE:

ENERGY AND FUELS

Higher ethanol recovery and production of isoamyl alcohol from fusel oil distillationConheça a tecnologia que permite aumentar a recuperação de etanol sem aumentar o consumo energéticoConheça a tecnologia que permite aumentar a recuperação Get to know the technology that enables higher ethanol Conheça a tecnologia que permite aumentar a recuperação Get to know the technology that enables higher ethanol Conheça a tecnologia que permite aumentar a recuperação Get to know the technology that enables higher ethanol Conheça a tecnologia que permite aumentar a recuperação Get to know the technology that enables higher ethanol Conheça a tecnologia que permite aumentar a recuperação Get to know the technology that enables higher ethanol Conheça a tecnologia que permite aumentar a recuperação Get to know the technology that enables higher ethanol Conheça a tecnologia que permite aumentar a recuperação Get to know the technology that enables higher ethanol Conheça a tecnologia que permite aumentar a recuperação Get to know the technology that enables higher ethanol Conheça a tecnologia que permite aumentar a recuperação Get to know the technology that enables higher ethanol Conheça a tecnologia que permite aumentar a recuperação Get to know the technology that enables higher ethanol Conheça a tecnologia que permite aumentar a recuperação Conheça a tecnologia que permite aumentar a recuperação Conheça a tecnologia que permite aumentar a recuperação Conheça a tecnologia que permite aumentar a recuperação Conheça a tecnologia que permite aumentar a recuperação Conheça a tecnologia que permite aumentar a recuperação Conheça a tecnologia que permite aumentar a recuperação Conheça a tecnologia que permite aumentar a recuperação Conheça a tecnologia que permite aumentar a recuperação Conheça a tecnologia que permite aumentar a recuperação Conheça a tecnologia que permite aumentar a recuperação Conheça a tecnologia que permite aumentar a recuperação Conheça a tecnologia que permite aumentar a recuperação Conheça a tecnologia que permite aumentar a recuperação Conheça a tecnologia que permite aumentar a recuperação Conheça a tecnologia que permite aumentar a recuperação Conheça a tecnologia que permite aumentar a recuperação Conheça a tecnologia que permite aumentar a recuperação Conheça a tecnologia que permite aumentar a recuperação Conheça a tecnologia que permite aumentar a recuperação recovery without increasing energy consumptionde etanol sem aumentar o consumo energéticorecovery without increasing energy consumptionde etanol sem aumentar o consumo energéticorecovery without increasing energy consumptionde etanol sem aumentar o consumo energéticorecovery without increasing energy consumptionde etanol sem aumentar o consumo energéticorecovery without increasing energy consumptionde etanol sem aumentar o consumo energéticorecovery without increasing energy consumptionde etanol sem aumentar o consumo energéticorecovery without increasing energy consumptionde etanol sem aumentar o consumo energéticorecovery without increasing energy consumptionde etanol sem aumentar o consumo energéticorecovery without increasing energy consumptionde etanol sem aumentar o consumo energéticode etanol sem aumentar o consumo energéticode etanol sem aumentar o consumo energéticode etanol sem aumentar o consumo energéticode etanol sem aumentar o consumo energéticode etanol sem aumentar o consumo energéticode etanol sem aumentar o consumo energéticode etanol sem aumentar o consumo energéticode etanol sem aumentar o consumo energéticode etanol sem aumentar o consumo energéticode etanol sem aumentar o consumo energéticode etanol sem aumentar o consumo energéticode etanol sem aumentar o consumo energéticoGet to know the technology that enables higher ethanol recovery without increasing energy consumption

INTEGRATED SYSTEM FOR INCREASING ETHANOL RECOVERY ANDCO-PRODUCTION OF ISOAMYL ALCOHOL, INTEGRATED PROCESS FOR INCREASING ETHANOL RECOVERY AND CO-PRODUCTION OF ISOAMYL ALCOHOL, AND PRODUCTS THUS OBTAINED

TECHNOLOGY PROFILE

The technology enables higher ethanol recovery and production of isoamyl alcohol without major changes in the processThe growth in the demand for ethanol production enabled an increase in options for more profitable uses of by-products generated in the process, such as fusel oil. For every 1000 liters of produced ethanol, 1 to 11 liters of fusel oil are generated. However, mills have not been taking advantage of this by-product that contains not only ethanol but also isoamyl alcohol.

The technology allows the integration of a system in the conventional ethanol distillation process without changing its structure by simply attaching a new module to the existing plant. This enables fusel oil distillation increasing ethanol recovery and the production of high purity isoamyl alcohol. This kind of alcohol is often used as a reagent and solvent in the food, paint and varnishes, plasticizers and fragrance industries.

INOVA UNICAMP INNOVATION AGENCY1831 Roxo Moreira StreetPO BOX 6131Campinas, SP 13083-592Brazil

www.inova.unicamp.br

INVENTORS:

SCHOOL/INSTITUTE:School of Food Engineering - FEA - UNICAMP - University ofCampinas, Brazil

Magno José de OliveiraSchool of Food Engineering - FEA - UNICAMP - University of Campinas, Brazil

Eduardo Augusto Caldas Batista• Food Engineer - UNESP - São Paulo State University, Brazil• Master of Science in Food Engineering - UNICAMP - University of Campinas, Brazil• Ph.D. in Food Engineering - UNICAMP - University of Campinas, BrazilHe is currently a Ph.D. professor at UNICAMP - University of Campinas, Brazil, and has experience in the area of Food Engineering with emphasis on separation processes.

Antonio José de Almeida Meirelles• Food Engineer - UNICAMP - University of Campinas, Brazil• Master of Sciences in Food Engineering - UNICAMP - University of Campinas, Brazil• Ph.D. in Economic Sciences - UNICAMP - University of Campinas, Brazil• Ph.D. in Thermal Process Engineering - Martin Luther Universität, GermanyHe is currently a full professor at UNICAMP - University of Campinas, Brazil

PATENT STATUS:Patent application at the INPI - Brazilian National Institute of Industrial Property (Brazilian Patent Office).

Internal code:811_RECUPERAÇÃO

Further information:[email protected]

+55 19 3521-2607+55 19 3521-5013

OBTAINED RESULTS USING THE TECHNOLOGY:

99 99 98

93 93 99

9 6

4823048230

48322

92

ethanol ethanol isoamyl alcoholCONVENTIONAL APPLYING THE TECHNOLOGY

Recovery(%)

Product Purity (% m/m)

Fusel oil by-product (kg/h)

Steam consumption (kg/h)

CONFIGURATION

KEY BENEFITS AND ADVANTAGES OF THE TECHNOLOGY:

Increase in ethanol recovery and production of isoamyl alcohol by using only one

distillation column

Greater efficiency in the production process

maintaining ethanol purity

Solvents or alkaline agents are not used in

the purification process.

Structural changes in the ethanol distillation system

are not required

It can be applied to ethanol mills or distilled spirits

plants.

Allows for taking advantage of fusel oil

with higher profitability and energy savings

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ENERGY AND FUELS