internal technical annex agrifood department …©e-version... · pesticide residues scope of...
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Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
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Phytocontrol Laboratoire d’analyses
INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
INTERNAL TECHNICAL ANNEX AGRIFOOD DEPARTMENT
PHYTOCONTROL ANALYTICS France
Version 24 – June 12, 2018
References : Technical annex Cofrac No 1-1904 rev. 8 Technical annex Cofrac No 1-6066 rev. 6
LABORATOIRE PHYTOCONTROL (1)
Parc Scientifique Georges Besse II
180, rue Philippe Maupas
30035 NIMES,
under the accreditation number No 1-1904
LABORATOIRE PHYTOCONTROL (2)
Parc Scientifique Georges Besse
70 allée Graham Bell
30035 NIMES,
under the accreditation number No 1-6066
BIOTECHNOLOGICAL UNIT (Phytocontrol 1) ANALYTICAL CHEMISTRY UNIT (Phytocontrol 1, Phytocontrol 2) MICROBIOLOGY UNIT (Phytocontrol 2)
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
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INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
Pesticide Residues Scope of accreditation No 1-1904
Flexible scope (FLEX3)
General scope*
Food and food products/ Foodstuffs / Physical-chemical analyses
Analysis of pesticide residues and organic contaminants in foodstuffs intended for human or animal consumption, biological matrices of animal origin - LAB GTA 26/99-2
OBJET CARACTERISTIQUE MESUREE OU RECHERCHEE PRINCIPE DE LA METHODE
Products of plant origin Products of animal origin Animal feed
Pesticide Residues
Extraction: Solid/Liquid Purification (if necessary) : Liquid-Solid (SPE) Liquid-Solid (SPE dispersive) Analysis : LC/MS-MS, GC/MS-MS, GC-MS
* FLEX3 Flexible Scope: The laboratory is recognised as competent, in the area covered by the general scope, to adopt any recognised method and to develop or implement any other method for which it has provided validation.
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
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INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
Detailed scope
Food and food products/ Foodstuffs / Physical-chemical analyses
Analysis of pesticide residues and organic contaminants in foodstuffs intended for human or animal consumption, biological matrices of animal origin - LAB GTA 26/99-2
ITEM CHARACTERISTIC MEASURED OR SOUGHT PRINCIPLE OF THE METHOD REFERENCE OF
THE METHOD
Products of plant and animal origin: Watery product, High oil content products, Acid and water-rich products, Products rich in sugar and low in water, Products low in water and fat, Spices, aromatic and medicinal plants, Alcoholic beverages,
Fruit and vegetable juices
Diquat/Paraquat
Preparation/Extraction : Solid / liquid cold extraction Purification : SPE Analysis : LC-MS/MS
In-house method MOC3/20
Non-fat products of vegetable origin :
Watery product
Products rich in starch and protein Acid products Highly-pigmented products
Determination of the content of Chlormequat and Mepiquat
Extraction: by solvent Analysis : LC-MS-MS
In-house method
MOC3/21
Products of plant origin:
Watery product Products rich in starch and protein Acid products Highly-pigmented products
Determination of residues of Dithiocarbamates
Preparation/Extraction : Hydrolysis Analysis : Determination of residual CS2 by GC-MS
In-house method
MOC3/01
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
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INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
ITEM CHARACTERISTIC MEASURED OR SOUGHT PRINCIPLE OF THE METHOD REFERENCE OF
THE METHOD
Products of plant origin: Watery product Products rich in starch and protein Acid products Highly-pigmented products
Determination of pesticides multiresidues Organophosphates: Chlorpyriphos ethyl Isofenphos methyl, Malathion, Parathion methyl, Phosalone, Pirimiphos methyl, Tolclophos methyl, Chlorfenvinphos, chlorpyriphos-methyl, dichlorfenthion, ethoprofos, fenchlorfos, fonofos Organochlorines : Chlorpropham, Procymidone, Propyzamide, Vinchlozoline, Myclobutanil, Triadimefon, Triadimenol, 2-4'DDE, 2-4'DDD, 4-4'DDE, 4-4''DDT, chlorobenzylate, fenarimol, fenhexamide, hcb, hch alpha, hch beta, hch delta, mirex oxadiazon, pentachloroanisole, tebufenpyrad Pyrethroids: Bifenthrin, Cyhalothrin Nitrogenous / miscellaneous : Bromopropylate, Cyprodinil, Diphenylamine, Pirimicarb, Propyconazole, Pyrimethanil, Fludioxonil, O-phenylphenol, Oxadixyl, Benalaxyl, bitertanol, carfentrazone-ethyl, chorthal-dimethyl, cyproconazole, dichlofop-methyl, difenoconazole, flusilasole, mepanipyrim, mepronil, penconazole, perthane, proquinazid, pyriproxyfen, tebuconazole Polychlorinated biphenyls (PCBs) : PCB 28, PCB 52, PCB 101, PCB 118, PCB 138, PCB 153, PCB 180.
Extraction : Solid/liquid cold extraction
Purification : SPE
Analysis : GC-MS GC/MS-MS
In-house method
MOC3/25
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
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INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
ITEM CHARACTERISTIC MEASURED OR SOUGHT PRINCIPLE OF THE METHOD REFERENCE OF
THE METHOD
Products of plant origin: High oil content products
Products of animal origin : Dairy products Meat products Fats Fish products Egg products
Multi-residue pesticide dosing Organophosphates: Chlorfenvinphos, Chlorpyriphos ethyl, Chlorpyrifos methyl, Coumaphos Fenitrothion, Malathion, Methidathion Parathion methyl, Parathion ethyl, Phosalone, Pirimiphos methyl Ethion, Isofenphos methyl Pyridafenthion, Tolclophos methyl Organochlorates: Aclonifen, Chlorpropham, 2,4-DDD 2,4-DDE, 4,4’-DDE, 4,4’ DDT, Dieldrin Endosulfan alpha, Endosulfan beta Endosulfan sulphate, HCB, Oxyfluorfen Procymidone, Propyzamide Vinchlozoline, Myclobutanil Carfentrazone ethyl, Cyproconazole Diclofop methyl, Difenoconazole Fenarimol, Penconazole, Tebuconazole Tebufenpyrad Pyrethroids: Bifenthrine, Cyfluthrine, Cyhalothrine Cypermethrine, Deltamethrine Fluvalinate, Tefluthrine, Tetramethrine Organonitrogen groups / other: Bromopropylate, Propyconazole Fludioxonil, Benalaxyl, Cyprodinil Diflufenican, Flusilasole, Mepronil Metalaxyl, Pirimicarb, Proquinazid, Prosulfocarb, Pyriproxifen
Extraction : Solid/liquid cold extraction Purification : SPE dispersive Analysis : GC-MS/MS
In-house method
MOC3/26
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
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INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
ITEM CHARACTERISTIC MEASURED OR SOUGHT PRINCIPLE OF THE METHOD REFERENCE OF
THE METHOD
Products of plant origin: Watery product Products rich in starch and protein Acid products Highly-pigmented products Products low in water and fat
Ethephon
Extraction : Solid/liquid cold extraction
Analysis: LC-MS-MS
In-house method
MOC3/27
Products of plant origin: Watery product, Acid and water-rich products, Products low in water and fat Products rich in sugars and low in water Alcoholic beverages, Fruit and vegetable juices, Infant nutrition
Determination of the content of fentin (expressed as triphenyltin cation), fenbutatin oxide, cyhexatin and azocyclotin.
Extraction : by solvent Purification : Liquid/solid (SPE dispersive) Analysis : LC-MS/MS
In-house method
MOC3/31
Products of plant origin: Watery product Products rich in starch and protein Acid products
Determination of the content of Maleic Hydrazide
Extraction : Solid/liquid cold extraction Analysis : LC-MS/MS
In-house method
MOC3/44
Products of plant origin: Watery product, Acid and water-rich products, Products rich in sugar and low in water, Products low in water and fat, Alcoholic beverages, Fruit and vegetable juices, Infant nutrition
Determination of the content of ethylene thiourea (ETU) and propylene thiourea (PTU)
Extraction : Solid/liquid cold extraction Purification : Liquid/liquid Analysis : LC-MS-MS
In-house method MOC3/45
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
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INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
ITEM CHARACTERISTIC MEASURED OR SOUGHT PRINCIPLE OF THE METHOD REFERENCE OF
THE METHOD
Products of plant origin: Watery product, Acid and water-rich products, Products low in water and fat Products rich in sugars and low in water Alcoholic beverages, Fruit and vegetable juices, Sodas
Determination of the content of Acetochlore, Alachlore, Benfluraline, Clomazone, Diflufenican, Ethofumesate, Etofenprox, Fenpropathrine, Fenvalerate, Fluopicolide, Hexazinone, Metolachlore, Permethrine, Pyridaben, Tefluthrine, Terbufos, Terbuthylazine, Triallate, Zoxamide.
Extraction : by solvent Purification : Liquid/solid (SPE dispersive) Analysis : GC-MS/MS
In-house method MOC3/55
Products of plant origin: Infant nutrition
Multi-residue pesticide dosing Terbufos, Fipronil, Fipronil desulfinyl, HCB, Haloxyfop 2ethylhexyl, Haloxyfop methyl, Terbufos sulfone, Heptachlor, Heptachlor epoxide cis, Heptachlor epoxide trans Endrin, Disulfoton, Dieldrin, Aldrin, Demeton S Methyl, Nitrofen
Extraction : Solid/liquid cold extraction Purification : Liquide/Solide (SPE) Analysis : GC-MS/MS
In-house method
MOC3/56
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
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INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
ITEM CHARACTERISTIC MEASURED OR SOUGHT PRINCIPLE OF THE METHOD REFERENCE OF
THE METHOD
Products of plant origin:
Infant nutrition
Multi-residue pesticide dosing Haloxyfop (free acid), Terbufos sulfoxide, Ethoprophos, Fensulfothion, Fensulfothion oxon, Fensulfothion oxon sulfone, Fensulfothion sulfone, Disulfoton sulfone, Disulfoton sulfoxide, Cadusafos
Extraction : Solid/liquid cold extraction
Analysis : LC-MS/MS
In-house method
MOC3/57
Non-fat products of plant origin : Watery product, Acid and water-rich products, Alcoholic beverages, High oil content products (oil seeds) Products low in water and fat Products Other : teas Animal feed : Fodder, oilcake Mixed feeds
Determination of the content of Glyphosate and AMPA
Extraction : Solid/liquid cold extraction Analysis : LC-MS/MS
In-house method MOC3/80
Products of plant origin: Watery product Acid and water-rich products Alcoholic beverages Fruit and vegetable juices
Determination of the content of Fosetyl-Aluminum and Phosphoric Acid
Extraction : Solid/liquid cold extraction Analysis : LC-MS/MS
In-house method
MOC3/89
Products of plant origin:
Watery product
Acid and water-rich products
Sugar-rich and water-poor products
Alcoholic beverages
Fruit and vegetable juices
Determination of the content of Chlorate and Perchlorate
Extraction : Solid/liquid cold extraction Analysis : LC-MS/MS
In-house method
MOC3/120
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
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INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
ITEM CHARACTERISTIC MEASURED OR SOUGHT PRINCIPLE OF THE METHOD REFERENCE OF
THE METHOD
Products of plant origin:
Watery product Acid and water-rich products
Multiresidue pesticide dosing Phenoxyacetic herbicides : 2.4.5 T, 2.4 D, 2.4 DB, DNOC, MCPA
Phenoxypropionic herbicides : Dichloprop P, Diclofop acid Fluazifop (free acid), Haloxyfop P Mecoprop P, Quizalofop Ureas : Amidosulfuron, Diflubenzuron Hexaflumuron, Teflubenzuron Thifensulfuron methyl, Triflumuron Nitriles : Bromoxynil, Ioxynil, Dinitrophenols : Dinoseb, dinoterb Pyridines : Triclopyr, Fluroxypyr Other : Bentazone, Dicamba, Dithianon MCPB, Orizalin
Extraction : Solid/liquid cold extraction Analysis : LC-MS/MS
In-house method
MOC3/90
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
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INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
ITEM CHARACTERISTIC MEASURED OR SOUGHT PRINCIPLE OF THE METHOD REFERENCE OF
THE METHOD
Products of plant origin: Watery product Acid and water-rich products Products rich in sugar and low in water Fruit and vegetable juices Sodas Alcoholic beverages Low water and fat products
Multi-residue pesticide dosing Benzimidazoles : Thiabendazole Ureas : Chlorotoluron, Diuron, Lufenuron Novaluron, Pencycuron Triazoles : Metconazole, Prothioconazole desthio, Etoxazole Triazines : Simazine, Terbumeton Carbamates : Benthiavalicarb isopropyl, Methomyl Oxamyl, Propoxur Organophosphores : Dimethoate, Omethoate Other : 1-naphtylacetamide, Ametoctradin Bifenazate, Carbetamide Carboxin, Chlorantraniliprole, Chloridazon, Clofentezine, Clothianidin, Cymoxanil, Dodine, Emamectin benzoate B1a, Etoxazole, Imidachlopride, Kresoxim-methyl, Mandipropamide Metamitron, Spinosad A + D Spiromesifen, Spirotetramate, Spirotetramate enol, Spirotetramate enol glucoside, Spirotetramate keto hydroxy, Spirotetramate mono hydroxy TCMTB, Thiachlopride Thiametoxam, Tricyclazole
Extraction : Solid/liquid cold extraction Analysis : LC-MS/MS
In-house method
MOC3/97
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
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INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
ITEM CHARACTERISTIC MEASURED OR SOUGHT PRINCIPLE OF THE METHOD REFERENCE OF
THE METHOD
Products of plant origin: Watery product Products rich in starch and protein Acid products Highly-pigmented products
Multi-residue pesticide dosing Benzimidazoles : Carbendazime, Thiophanate-methyl Strobilurines : Azoxystrobine, trifloxystrobine, Fluoxastrobine, picoxystrobine, pyraclostrobine Ureas : Isoproturon, linuron, metoxuron, triflusulfuron-methyl, Bensulfuron-methyl, buturon, cycluron, flufenoxuron, fluometuron, methabenzthiazuron, monolinuron, monuron, neburon Triazoles : Epoxyconazole, fenbuconazole, fetraconazole, Azaconazole, bromuconazole, paclobutrazole, triticonazole, Triazines : Cyanazine Carbamates : Iprovalicarb, thiodicarb
Pyridilmethyamines : Acetamipride Other :
Lenacil, metoxyfenoside, phenmedipham, rotenone, tebufenozide, Boscalid, butafenacil, cloquintecet, cyazofamide, desmedipham, desmetryn, dimethanamide, dimethomorphe, fenamidone, fenpyroximate, flurtamone, hexythiazox, indoxacarbe, isoporthiolane, isoxathion, metrafenone, phoxim, picolinafen, propaquizafop, pyraflufen-ethyl, spirodiclofen, spiroxamine, triflumizole, warfarine
Preparation/Extraction : Solid/liquid cold extraction
Analysis : LC-MS/MS
In-house method
MOC3/35
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
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INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
ITEM CHARACTERISTIC MEASURED OR SOUGHT PRINCIPLE OF THE METHOD
REFERENCE OF THE METHOD
Beehive products :
Honey
Royal Jelly
Pollen
Bees
Multi-residue pesticide dosing : 2,4 DDD, 2,4 DDE, 4,4 DDE, 4,4 DDT, Alachlor, Bromopropylate, Chlordane (cis+trans), Chlorobenzilate, Chlorpyriphos ethyl, Chlorpyriphos methyl, Cyhalothrine, Cymiazole, Cypermethrine, Deltamethrine, Dichlobenil, Dieldrin, Difenoconazole, Endosulfan alpha, Endosulfan beta, Endrin, Ethion, Fenitrothion, Tau-fluvalinate, HCH alpha, HCH beta, Malathion, Metolachlor, Oxadiazon, Oxyfluorfen, Parathion methyl, Permethrine, Pirimiphos methyl, Procymidone, Profenofos, Prothiofos, Quinalfos, Tebufenpyrad, Tetradifon, Trifluraline, Vinchlozoline.
Extraction : Solid/liquid cold extraction Purification : SPE dispersive Analysis : GC-MS/MS
In-house method
MOC3/76
Products of animal origin : Meat products Egg products and by-products
Fipronil, Fipronil sulfone
Preparation / Extraction : Solid/liquid cold extraction Purification : SPE Analysis : GC-MS/MS
In-house method MOC3/183
Products of animal origin : Meat products Egg products and by-products.
Amitraz (including metabolites containing the 2,4-dimethylaniline moiety expressed as amitraz)
Preparation / Extraction : Hydrolysis Solid/liquid cold extraction Purification : SPE dispersive Analysis : LC-MS/MS
In-house method MOC3/184
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
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INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
Products of plant origin: Watery product Acid and water-rich products Sugar-rich and water-poor products Products low in water and fat Alcoholic beverages Fruit and Vegetable Juices Sodas
Multi-residue pesticide dosing : 6-Benzyladenine, Acephate, Acetamipride, Ametoctradine, Amidosulfuron, Azaconazole, Azimsulfuron, Azinphos-ethyl, Azinphos-methyl, Azoxystrobine, Beflubutamide, Bensulfuronmethyl, Benthiavalicarbisopropyl, Bixafen, Boscalide, Bromacil, Bromuconazole, Bupirimate, Buprofezin, Buturon, Cadusafos, Carbendazim, Carbetamide, Carboxine, Chlorantraniliprole, Chloridazon, Chlorotoluron, Chloroxuron, Chlorsulfuron, Chromafenozide, Cinidonethyl, Cinosulfuron, Clethodim-sulfoxide, Clofentezine, Clothianidine, Cyanazine, Cyantraniliprole, Cyazofamide, Cycluron,Cyflufenamid, Cymoxanil, Cyprosulfamide, Demeton-S, Demeton-S-methylsulfone, Demeton-S-methylsulfoxide, Desmetryn, Difenamide, Diflubenzuron, Dimethenamid- P, Dimethoate, Dimethomorphe, Dinoseb, Dinoterb, Disulfoton-sulfone, Disulfoton-sulfoxide, Diuron,DMST, Dodemorphe, Dodine, Emamectine-benzoate B1a, Emamectine-benzoate B1b, Epoxiconazole, Ethametsulfuron-methyl, Ethidimuron, Ethiprole, Ethirimol, Etoxazole, Fenamidone, Fenamiphos sulfone, Fenamiphossulfoxide, Fenbuconazole, Fenchlorphos oxon, Fenoxaprop-ethyl, Fenoxycarbe, Fenpropidine, Fenpyramazine, Fenpyroximate, Fensulfothion, Fensulfothionoxon, Fensulfothion-oxonsulfone, Fensulfothionsulfone, Fenthion, Fenthion sulfone, Fenthion sulfoxide, Fenuron, Florasulam, Fluazinam, Flufenoxuron, Fluometuron, Fluopyram, Fluoxastrobine, Flupyradifurone, Flupyrsulfuron methyl, Fluquinconazole, Flurtamone, Fluxapyroxad, Foramsulfuron, Forchlorfenuron, Fosthiazate, Fuberidazole, Furametpyr, Halauxifen methyl, Halfenprox, Halosulfuronmethyl, Hexythiazox, Hydramethylnon, Imazalil, Imazamox, Imazaquin, Imazosulfuron, Imidachlopride, Indoxacarb, Iodosulfuronmethyl, Ioxynil, Iprovalicarbe, Isazofos, Isocarbophos, Isoprocarb, Isoprothiolane, Isoproturon, Isopyrazam, Isoxaben, Isoxaflutole, Isoxathion, Kresoxim-methyl, Lenacil, Linuron, Lufenurone, Mandipropamide, MCPA, Mecarbam, Mesosulfuronmethyl, Metaflumizone, Metamitron, Metconazole
Preparation/ Extraction: Solid/liquid cold extraction Purification : SPE Analysis : LC-MS/MS
In-house method MOC3/407
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
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INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
Products of plant origin: Watery product Acid and water-rich products Sugar-rich and water-poor products Products low in water and fat Alcoholic beverages Fruit and Vegetable Juices Sodas
Methabenzthiazuron, Methomyl, Methoxyfenozide, Metobromuron, Metolcarb, Metosulam, Metoxuron, Metrafenone, Metsulfuronmethyl, Mevinphos, Monalide, Monocrotophos, Monolinuron, Monuron, NAD(1-naphtyl acetamide), Napropamide, Neburon, Nicosulfuron, Norflurazon, Novaluron, Ofurace, Omethoate, Orthosulfamuron, Oxamyl, Oxasulfuron, Paclobutrazol, Paraoxon-ethyl, Pencycuron, Penflufen, Penoxsulame, Penthiopyrad, Phenmediphame, Phorate sulfone, Phorate-oxon, Phosphamidon, Phoxim, Picolinafen, Picoxystrobine, Pinoxadene, Pirimicarbdesmethyl, Promecarb, Prometon, Propamocarbe, Propaphos, Propaquizafop, Propoxur, Prothioconazoledesthio, Pyraclofos, Pyraclostrobine, Pyraflufenethyl, Pyrimidifen, Pyriofenone, Pyroquilon, Pyroxsulam, Rimsulfuron, Rotenone, Sedaxane, Silthiofam, Simazine, Spinetoram A, Spinetoram B, Spinosad A, Spinosad D, Spirodiclofen, Spiromesifen, Spirotetramate, Spirotetramate-enol, Spirotetramate-enolglucoside, Spirotetramate-keto-hydroxy, Spirotetramate-monohydroxy, Spiroxamine, Sulfosulfuron, TCMTB, Tebufenozide, Tebutam, Tebuthiuron, Teflubenzuron, Tepraloxydim, Terbumeton, Terbumeton desethyl, Tetraconazole, Thiabendazole, Thiachlopride, thiamethoxam, Thiencarbazone methyl, Thifensulfuron-methyl,Thiobencarb, Thiodicarb, Thionazin, Thiophanatemethyl, Tricyclazole, Trifloxystrobine, Triflumuron, Triflusulfuron-methyl, Triticonazole, Tritosulfuron, Vamidothion, Warfarin
Preparation/ Extraction: Solid/liquid cold extraction Purification : SPE Analysis : LC-MS/MS
In-house method MOC3/407
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
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Phytocontrol Laboratoire d’analyses
INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
Scope FLEX3
General scope*
Food and food products/ Foodstuffs / Physical-chemical analyses
Analysis of pesticide residues and organic contaminants in foodstuffs intended for human or animal consumption, biological matrices of animal origin - LAB GTA 26/99-2
OBJET CARACTERISTIQUE MESUREE OU RECHERCHEE PRINCIPE DE LA METHODE
Products of plant origin Products of animal origin Animal feed
Organic Contaminant Residues
Extraction : by solvent Purification : Liquid-Solid (SPE) Analysis : UFLC, LC-MS/MS, GC-MS/MS
* FLEX3 Flexible Scope: The laboratory is recognised as competent, in the area covered by the general scope, to adopt any recognised method and to develop or implement any other method for which it has provided validation.
Detailed scope
Food and food products/ Foodstuffs / Physical-chemical analyses
Analysis of pesticide residues and organic contaminants in foodstuffs intended for human or animal consumption, biological matrices of animal origin - LAB GTA 26/99-2
ITEM CHARACTERISTIC MEASURED OR SOUGHT PRINCIPLE OF THE METHOD REFERENCE OF
THE METHOD
Products of plant origin: Watery product, Acid and water-rich products, Alcoholic beverages, Products rich in sugar and low in water, Products low in water and fat, Fruit and vegetable juices, Sodas Products of animal origin : Dairy products Meat products Fish products
Determination of the content of DDAC and BAC (QAC Analysis)
Preparation/ Extraction : Solid/liquid cold extraction
Analysis : LC-MS-MS
In-house method
MOC3/145
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
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Phytocontrol Laboratoire d’analyses
INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
FIXED Scope
Food and food products/ Foodstuffs / Physical-chemical analyses
Analysis of pesticide residues and organic contaminants in foodstuffs intended for human or animal consumption, biological matrices of animal origin - LAB GTA 26/99-2
ITEM CHARACTERISTIC MEASURED OR SOUGHT PRINCIPLE OF THE METHOD REFERENCE OF
THE METHOD
Products of plant origin: Watery product (Water content ≥ 60%) High oil content products Acid and water-rich products Products rich in sugar and low in water Other products Alcoholic beverages Fruit and vegetable juices Sodas
Products of animal origin : Dairy products
Determination of nitrate, nitrite, chloride, bromide content
Preparation / Extraction : Water Analysis : HPLC/CI (conductivity measurement)
In-house method MOC3/02
Products of plant origin: High oil content products, Products low in water and fat (cerals and by-products, Fruits and vegetables powder) Fruit and vegetable juices, Alcoholic beverages Products rich in sugar and low in water Animal feed : Flour of animal origin Mixed feeds Raw materials of vegetable origin Products of animal origin : Dairy products including Infant nutrition Egg products Meat products Fish products
Melamine
Extraction :
Solvant
Analysis :
LC-MS/MS
In-house method MOC3/134
FIXED Scope : The laboratory is recognized as competent to perform the tests in strict compliance with the methods mentioned in the scope of accreditation. Technical changes to the operating mode are not permitted.
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
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Phytocontrol Laboratoire d’analyses
INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
Heavy Metals Scope of accreditation N°1-1904
Scope FLEX3
General scope*
# Food and food products/ Foodstuffs / Physical-chemical analyses
Analysis of metallic and mineral trace elements and their chemical species in foodstuffs intended for human or animal consumption - LAB GTA 45
ITEM CHARACTERISTIC MEASURED OR SOUGHT PRINCIPLE OF THE METHOD
Foodstuffs for humans and animals (including infant nutrition)
Metals Minerals
Mineralisation Wet process (microwave digestion in closed system) Wet process (acid digestion in open system) Analysis : ICP/MS LC-ICP/MS
* FLEX3 Flexible Scope: The laboratory is recognised as competent, in the area covered by the general scope, to adopt any recognised method and to develop or implement any other method for which it has provided validation.
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
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Phytocontrol Laboratoire d’analyses
INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
Detailed scope
# Food and food products/ Foodstuffs / Physical-chemical analyses
Analysis of metallic and mineral trace elements and their chemical species in foodstuffs intended for human or animal consumption - LAB GTA 45
ITEM CHARACTERISTIC MEASURED OR SOUGHT PRINCIPLE OF THE METHOD REFERENCE OF
THE METHOD
Foodstuffs for humans and animals (including infant nutrition)
Arsenic, Lead, Cadmium, Mercury, Antimony, Barium, Boron, Chromium, Cobalt, Copper, Tin, Manganese, Molybdenum, Nickel, Palladium, Platinium, Iridium, Lithium, Rhodium, Ruthenium, Thallium, Vanadium
Mineralisation : Wet process (microwave digestion in closed system)
Wet process (open system digestion) Analysis : ICP-MS
In-house method
MOC3/85
Dairy products including infant nutrition Aluminium
Mineralisation : Wet process (microwave digestion in closed system)
Wet process (acid digestion in open system)
Analysis : ICP-MS
In-house method
MOC3/85
Alcoholic beverages Iron
Mineralisation : Wet process (acid digestion in open system)
Analysis : ICP-MS
In-house method
MOC3/85
Cereals Fruits and vegetables Fruit and vegetable juices Medicinal plants Beehive products Fish products Dairy products including infant nutrition
Arsenic III, Arsenic V, monomethyl Arsenic, dimethyl Arsenic, Arsenocholine AsC, Arsenobetaine AsB
Mineralisation : Wet process (acid digestion in open system)
Analysis : LC-ICP/MS
In-house method MOC3/94
Fish products Fruits and vegetables Mushrooms Medicinal plants Food supplements Animal feed
Mercury II HgII, Methylmercury MeHg
Mineralisation : Wet process (acid digestion in open system)
Analysis : LC/ICP-MS
In-house method MOC3/144
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
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Phytocontrol Laboratoire d’analyses
INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
Human food : Grain products, Fatty products, Egg products, Dairy products, Meat products, Fish products, Fruits and vegetables, Sweet products, Non-alcoholic beverages, Alcoholic beverages, Spices and condiments, Aromatic and medicinal plants, Special and dietary foods, Mixed feeds, Infant nutrition Animal feed : Raw materials, Complete or complementary compound feedingstuffs
Calcium, Magnesium, Phosphorus, Potassium
Mineralisation : Wet process (open system digestion) Analysis : ICP-MS
In-house method
MOC3/152
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
Page 20 sur 67
Phytocontrol Laboratoire d’analyses
INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
Mycotoxins Scope of accreditation N°1-1904
Scope FLEX3
General scope*
Food and food products/ Foodstuffs / Physical-chemical analyses
Determination of mycotoxins and phycotoxins in food and feed - LAB GTA 21/99-1
ITEM CHARACTERISTIC MEASURED OR SOUGHT PRINCIPLE OF THE METHOD
Plant and animal products Raw material, derived and/or processed products
Determination of mycotoxins
Extraction : by solvent Purification : SPE Immunoaffinity Analysis : UFLC/LC-MS/MS
* Flexible scope FLEX3 : The laboratory is recognized as competent, in the field covered by the General scope, to adopt any recognized method and to develop or implement any other method including it will have ensured validation.
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
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Phytocontrol Laboratoire d’analyses
INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
Detailed scope
Food and food products/ Foodstuffs / Physical-chemical analyses
Determination of mycotoxins and phycotoxins in food and feed - LAB GTA 21/99-1
ITEM CHARACTERISTIC MEASURED OR SOUGHT PRINCIPLE OF THE METHOD REFERENCE OF
THE METHOD
Cereals Oilseeds Nuts Dried fruit Legumes Cereal Derivatives Products derived from oilseeds and nuts Fruit products : Compotes, Juices Alcoholic beverages Spices Coffee/Cocoa Coffee/Cocoa Products Food and drink for children Animal feed
Determination of the content of Ochratoxine A
Extraction : by solvent Purification : Immunoaffinity Analysis : UFLC
In-house method MOC3/65
Fresh fruit and fruit products including children's food (fruit-based baby food)
Determination of the content of patuline
Extraction/purification: Solvant/SPE
Analysis : LC-MS-MS
In-house method MOC3/37
Cereals Oilseeds Nuts Dried fruit Legumes Cereal Derivatives Products derived from oilseeds and nuts Fruit products : Compotes (including Infant nutrients) Food for children Animal feed
Determination of the content of aflatoxines (B1, B2, G1, G2)
Extraction : by solvent
Purification : Immunoaffinity
Analysis : UFLC
In-house method MOC3/71
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
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Phytocontrol Laboratoire d’analyses
INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
ITEM CHARACTERISTIC MEASURED OR SOUGHT PRINCIPLE OF THE METHOD REFERENCE OF
THE METHOD
Cereals Cereal by-products Fresh fruit Fruit products Infant nutrition Animal feed : Products derived from oilseeds : Oilseed cake
Determination of the content of : Deoxynivalenol (DON), Fumonisines (B1+B2, B3), HT2 toxine, T2 toxine, Zearalenone (ZEA), Aflatoxines (B1, B2, G1, G2), Ochratoxine A (OTA)
Extraction / purification: Solvant / SPE
Purification : Immunoaffinity
Analysis : UFLC
In-house method MOC3/107
Spices Dry plants Coffee and cocoa and their by-products
Determination of the content of aflatoxines (G2, G1, B2, B1) et en ochratoxine
Extraction : by solvent
Purification : Immunoaffinity
Analysis : LC-MS-MS
In-house method MOC3/108
Milk and all dairy products including infant food Dairy products containing cereals
Determination of the content of Aflatoxine M1
Extraction : by solvent
Purification : Immunoaffinity
Analysis : UFLC
In-house method MOC3/110
Cereals Determination of the content of Deoxynivalenol (DON)
Extraction : by solvent
Purification : Immunoaffinity
Analysis : UFLC
In-house method MOC3/78
Cereals, Cereal by-products Legumes (pulses) Fresh vegetables, Leafy vegetables, Animal feed, Oilcake
Determination of the content of Datura Alkaloids
Extraction : By solvent Purification : SPE Analysis : LC-MS-MS
In-house method MOC3/121
Cereals Cereal by-products Legumes (pulses) Fresh vegetables
Determination of the content of Ergot alkaloids
Extraction : by solvent Purification : SPE Analysis : UFLC
In-house method
MOC3/122
Cereals Determination of the content of Zearalenone (ZEA)
Extraction : by solvent Purification : SPE Analysis : UFLC
In-house method
MOC3/60
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
Page 23 sur 67
Phytocontrol Laboratoire d’analyses
INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
Alkaloids Scope of accreditation N°1-1904
Scope FLEX3
General scope*
Food and food products/ Foodstuffs / Physical-chemical analyses
Analysis of pesticide residues and organic contaminants in foodstuffs intended for human or animal consumption, biological matrices of animal origin - LAB GTA 26/99-2
ITEM CHARACTERISTIC MEASURED OR SOUGHT PRINCIPLE OF THE METHOD
Products of plant origin Products of animal origin Animal feed
Organic Contaminant Residues
Extraction : by solvent Purification : Liquide-Solide (SPE) Analysis : UFLC, LC-MS/MS, GC-MS/MS
* FLEX3 Flexible Scope: The laboratory is recognised as competent, in the area covered by the general scope, to adopt any recognised method and to develop or implement any other method for which it has provided validation.
Detailed scope
Food and food products/ Foodstuffs / Physical-chemical analyses
Analysis of pesticide residues and organic contaminants in foodstuffs intended for human or animal consumption, biological matrices of animal origin - LAB GTA 26/99-2
ITEM CHARACTERISTIC MEASURED OR SOUGHT PRINCIPLE OF THE METHOD REFERENCE OF
THE METHOD
Spices Piperine
Preparation/Extraction : Solid/liquid cold extraction Purification : SPE Analysis : LC-MS/MS
In-house method MOC3/51
Potato Chaconine and solanine Preparation/Extraction : Solid/liquid cold extraction Analysis : LC-MS/MS
In-house method MOC3/50
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
Page 24 sur 67
Phytocontrol Laboratoire d’analyses
INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
General scope*
Food and food products/ Foodstuffs / Physical-chemical analyses
Determination of mycotoxins and phycotoxins in food and feed - LAB GTA 21/99-1
ITEM CHARACTERISTIC MEASURED OR SOUGHT PRINCIPLE OF THE METHOD
Plant and animal products Raw material, derived and/or processed products
Determination of mycotoxins
Extraction : by solvent Purification : Immunoaffinity SPE Analysis : UFLC/LC-MS/MS
* FLEX3 Flexible Scope: The laboratory is recognised as competent, in the area covered by the general scope, to adopt any recognised method and to develop or implement any other method for which it has provided validation.
Detailed scope
Food and food products/ Foodstuffs / Physical-chemical analyses
Determination of mycotoxins and phycotoxins in food and feed - LAB GTA 21/99-1
ITEM CHARACTERISTIC MEASURED OR SOUGHT PRINCIPLE OF THE METHOD REFERENCE OF
THE METHOD
Products of plant and animal origin: Leafy vegetables Cereals and cereal by-products Aromatic and medicinal plants Food supplements Spices Honey
Echimidine, Echimidine-N-oxide, (Z)-Erucifoline, (Z)-Erucifoline-N-oxide, Europine hydrochloride, Europine-N-oxide, Heliotrine, Heliotrine-N-oxide, Indicine hydrochloride, Indicine-N-oxide, Integerrimine, Integerrimine-N-oxide, Jacobine, Jacobine-N-oxide, Lasiocarpine, Lasiocarpine-N-oxide, Lycopsamine, Lycopsamine-N-oxide, Monocrotaline, Monocrotaline-N-oxide, Retrorsine, Retrorsine-N-oxide, Senecionine, Senecionine-N-oxide, Senkirkine, Seneciphylline, Seneciphylline-N-oxide, Senecivernine, Senecivernine-N-oxide, Trichodesmine, Intermedine, Intermedine-N-oxide.
Preparation/Extraction : By solvent Purification : SPE Analysis : LC-MS/MS
In-house method MOC3/123
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
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Phytocontrol Laboratoire d’analyses
INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
GMOs Scope of accreditation N°1-1904
Scope FLEX3
General scope*
Agri-food / Vegetables / Molecular Genetics
Analysis related to genetically modified organisms - GMOs
ITEM CHARACTERISTIC MEASURED OR SOUGHT PRINCIPLE OF THE METHOD
Corn Crude and/or processed products
PCR target plant species PCR target of a GMO sequence :
- screening sequence - specific event sequence
Homogenisation / Grinding Extraction Real-time PCR (qualitative and quantitative)
Soy Crude and/or processed products
PCR target plant species PCR target of a GMO sequence : - screening sequence - specific event sequence
Homogenisation / Grinding Extraction Real-time PCR (qualitative and quantitative)
* FLEX3 Flexible Scope: The laboratory is recognised as competent, in the area covered by the general scope, to adopt any recognised method and to develop or implement any other method for which it has provided validation.
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
Page 26 sur 67
Phytocontrol Laboratoire d’analyses
INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
Detailed scope
Agri-food / Vegetables / Molecular Genetics
Analysis related to genetically modified organisms - GMOs
OBJET CARACTERISTIQUE
MESUREE OU RECHERCHEE
DOMAINE D’APPLICATION
ETENDUE DE MESURE
PRINCIPE DE LA METHODE
REFERENCE DE LA METHODE
Plant species Maize
Target plant species-specific PCR: ADH
Raw products (seeds, grains, flour, etc.) and processed products
Qualitative/quantitative
Homogenisation/ Grinding Extraction PCR in real time
In-house method adapted from standards
NF EN ISO 21569, 24276, 21570 and 21571 and
their respective amendments on MON 810, GA21, NK 603 and
MON 863 maize
MOC3/103
Plant species Maize
Target plant sequence-specific PCR P35S screening
Raw products (seeds, grains, flour, etc.) and processed products
Qualitative/quantitative
Homogenisation/ Grinding Extraction PCR in real time
In-house method adapted from standards
NF EN ISO 21569, 24276, 21570 and 21571 and
their respective amendments on MON 810, GA21, NK 603 and
MON 863 maize
MOC3/103
Plant species Maize
Target GMO sequence-specific PCR Tnos screening
Raw products (seeds, grains, flour, etc.) and processed products
Qualitative/quantitative
Homogenisation/ Grinding Extraction PCR in real time
In-house method adapted from standards
NF EN ISO 21569, 24276, 21570 and 21571 and
their respective amendments on MON 810, GA21, NK 603 and
MON 863 maize
MOC3/103
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
Page 27 sur 67
Phytocontrol Laboratoire d’analyses
INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
OBJET CARACTERISTIQUE
MESUREE OU RECHERCHEE
DOMAINE D’APPLICATION
ETENDUE DE MESURE
PRINCIPE DE LA METHODE
REFERENCE DE LA METHODE
Plant species Maize
Target GMO sequence-specific PCR Identification of specific event MON810
Raw products (seeds, grains, flour, etc.) and processed products
Qualitative
Homogenisation/ Grinding Extraction PCR in real time
Internal method adapted to the NF EN
ISO 21569,24276,21570 and 21571 standards and their respective
amendments on MON 810 maize.
MOC3/103
Plant species Maize
Target GMO sequence-specific PCR Identification of specific event MON863
Raw products (seeds, grains, flour, etc.) and processed products
Qualitative/quantitative
Homogenisation/ Grinding Extraction PCR in real time
Internal method adapted to the NF EN
ISO 21569,24276,21570 and 21571 standards and their respective
amendments on MON 810 maize.
MOC3/103
Plant species Maize
Target GMO sequence-specific PCR Identification of specific event NK603
Raw products (seeds, grains, flour, etc.) and processed products
Qualitative/quantitative
Homogenisation/ Grinding Extraction PCR in real time
Internal method adapted to NF EN ISO 21569,24276,21570 and 21571 standards and their respective
amendments on NK603 maize.
MOC3/103
Plant species Maize
Target GMO sequence-specific PCR Identification of specific event GA21
Raw products (seeds, grains, flour, etc.) and processed products
Qualitative
Homogenisation/ Grinding Extraction PCR in real time
Internal method adapted to NF EN ISO 21569,24276,21570 and 21571 standards and their respective
amendments on GA21 maize.
MOC3/103
Plant species Maize
Target GMO sequence-specific PCR Identification of specific event Bt11
Raw products (seeds, grains, flour, etc.) and processed products
Qualitative
Homogenisation/ Grinding Extraction PCR in real time
Internal method adapted from NF EN
ISO 21569,24276,21570 and 21571 and their
respective amendments on Bt11
maize.
MOC3/103
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
Page 28 sur 67
Phytocontrol Laboratoire d’analyses
INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
OBJET CARACTERISTIQUE
MESUREE OU RECHERCHEE
DOMAINE D’APPLICATION
ETENDUE DE MESURE
PRINCIPE DE LA METHODE
REFERENCE DE LA METHODE
Plant species Maize
Target GMO sequence-specific PCR Identification of specific event Mon88017
Raw products (seeds, grains, flour, etc.) and processed products
Qualitative/quantitative
Homogenisation/ Grinding Extraction PCR in real time
Internal method adapted to NF EN ISO
21569,24276,21570 and 21571 standards and their respective amendments on
maize Mon88017
MOC3/103
Plant species Maize
Target GMO sequence-specific PCR Identification of specific event T25
Raw products (seeds, grains, flour, etc.) and processed products
Qualitative
Homogenisation/ Grinding Extraction PCR in real time
Internal method adapted to the standards... Validation
according to NF EN ISO 21569,24276,21570 and
21571 standards and their respective amendments on
maize T25
MOC3/103
Plant species Maize
Target GMO sequence-specific PCR Identification of specific event TC1507
Raw products (seeds, grains, flour, etc.) and processed products
Qualitative
Homogenisation/ Grinding Extraction PCR in real time
Internal method adapted to the standards... Validation
according to NF EN ISO 21569,24276,21570 and
21571 standards and their respective amendments on
maize TC1507
MOC3/103
Plant species Soya
Target plant species-specific PCR: ADH: Lectine
Raw products (seeds, grains, flour, etc.) and processed products
Qualitative/quantitative
Homogenisation/ Grinding Extraction PCR in real time
In-house method adapted to NF EN ISO
21569,24276,21570 and 21571 standards and their respective amendments on
RRS soybeans.
MOC3/103
Plant species Soya
Target GMO sequence-specific PCR P35S screening
Raw products (seeds, grains, flour, etc.) and processed products
Qualitative/quantitative
Homogenisation/ Grinding Extraction PCR in real time
Internal method adapted to NF EN ISO
21569,24276,21570 and 21571 standards and their respective amendments on
RRS soybeans.
MOC3/103
Plant species Soya
Target GMO sequence-specific PCR TNOS screening
Raw products (seeds, grains, flour, etc.) and processed products
Qualitative/quantitative
Homogenisation/ Grinding Extraction PCR in real time
Internal method adapted to NF EN ISO
21569,24276,21570 and 21571 standards and their respective amendments on
RRS2 soybeans.
MOC3/103
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
Page 29 sur 67
Phytocontrol Laboratoire d’analyses
INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
OBJET CARACTERISTIQUE
MESUREE OU RECHERCHEE
DOMAINE D’APPLICATION
ETENDUE DE MESURE
PRINCIPE DE LA METHODE
REFERENCE DE LA METHODE
Plant species Soya
Target GMO sequence-specific PCR Identification of specific event RRS
Raw products (seeds, grains, flour, etc.) and processed products
Qualitative/quantitative
Homogenisation/ Grinding Extraction PCR in real time
Internal method adapted to NF EN ISO
21569,24276,21570 and 21571 standards and their respective amendments
on FG72 soybeans.
MOC3/103
Plant species Soya
Target GMO sequence-specific PCR Identification of specific event RRS2
Raw products (seeds, grains, flour, etc.) and processed products
Qualitative/quantitative
Homogenisation/ Grinding Extraction PCR in real time
Internal method adapted to NF EN ISO
21569,24276,21570 and 21571 standards and their respective amendments
on RRS2 soybeans.
MOC3/103
Plant species Soya
Target GMO sequence-specific PCR Identification of specific event FG72
Raw products (seeds, grains, flour, etc.) and processed products
Qualitative/quantitative
Homogenisation/ Grinding Extraction PCR in real time
Internal method adapted to NF EN ISO
21569,24276,21570 and 21571 standards and their respective amendments
on FG72 soybeans.
MOC3/103
Plant species Soya
Target GMO sequence-specific PCR Identification of specific event MON87701
Raw products (seeds, grains, flour, etc.) and processed products
Qualitative
Homogenisation/ Grinding Extraction PCR in real time
Internal method adapted to NF EN ISO
21569,24276,21570 and 21571 standards and their respective amendments on Mon87701 soybeans.
MOC3/103
Plant species Soya
Target GMO sequence-specific PCR Identification of specific event A2704-12
Raw products (seeds, grains, flour, etc.) and processed products
Qualitative
Homogenisation/ Grinding Extraction PCR in real time
Internal method adapted to NF EN ISO
21569,24276,21570 and 21571 standards and their respective amendments on A2704-12 soybeans.
MOC3/103
Plant species Soya
Target GMO sequence-specific PCR Identification of DAS-81419
Raw products (seeds, grains, flour, etc.) and processed products
Qualitative
Homogenization/ grinding
Manual and automated extraction
Real-time PCR
Internal method adapted to NF EN ISO
21569,24276,21570 and 21571 standards and their respective amendments
MOC3/103
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
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INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
OBJET CARACTERISTIQUE
MESUREE OU RECHERCHEE
DOMAINE D’APPLICATION
ETENDUE DE
MESURE
PRINCIPE DE LA METHODE
REFERENCE DE LA METHODE
Plant species Soya
Target GMO sequence-specific PCR Identification of MON87751
Raw products (seeds, grains, flour, etc.) and processed products
Qualitative
Homogenization/ grinding Manual and automated extraction Real-time PCR
Internal method adapted to NF EN ISO 21569,24276,21570 and 21571 standards and their respective
amendments MOC3/103
Plant species Soya
Target GMO sequence-specific PCR Identification of DAS-68416-4
Raw products (seeds, grains, flour, etc.) and processed products
Qualitative
Homogenization/ grinding Manual and automated extraction Real-time PCR
Internal method adapted to NF EN ISO 21569,24276,21570 and 21571 standards and their respective
amendments MOC3/103
Plant species Soya
Target GMO sequence-specific PCR Identification of DAS-44406-6
Raw products (seeds, grains, flour, etc.) and processed products
Qualitative
Homogenization/ grinding Manual and automated extraction Real-time PCR
Internal method adapted to NF EN ISO 21569,24276,21570 and 21571 standards and their respective
amendments MOC3/103
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
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INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
Allergènes Scope of accreditation N°1-1904
Scope FLEX3
General scope*
Agri-food / Vegetables / Molecular Genetics
ITEM CHARACTERISTIC MEASURED OR SOUGHT PRINCIPLE OF THE METHOD
Grain products Fruits and vegetables Sweet products Tea and infusion
Detection of specific target DNA of an allergenic protein Detection in simplex
Grinding /Homogenisation Manual extraction of DNA by silica gel column adsorption Amplification by real time PCR (qualitative method)
* FLEX3 Flexible Scope: The laboratory is recognised as competent, in the area covered by the general scope, to adopt any recognised method and to develop or implement any other method for which it has provided validation.
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
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INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
Detailed scope
Agri-food / Vegetables / Molecular Genetics
ITEM CHARACTERISTIC MEASURED OR SOUGHT PRINCIPLE OF THE METHOD REFERENCE OF THE METHOD
Cereal products: Raw material: soybeans, barley Processed products: (granules, cake, cookies) Sweet and sweetened products: (processed products): chocolate, rice and chocolate desserts, jam, cake mixtures, cake. Fruits and vegetables: Tapioca, soya milk, coconut, milk
Specific target DNA sequence: Cashew nuts: Ana o (1.010 vicilin-like protein) Almond: prunin 1 precursor Hazelnut: Cor a 1 Nuts: 2S albumin seed storage protein precursor
Grinding /Homogenisation Manual extraction of DNA by silica gel column adsorption Amplification by real time PCR (qualitative method)
In-house method MOC3/115: Grinding /Homogenisation C3/01-01. D Extraction of ADN: NucleoSpin®Plant II (Macherey-Nagel)
Real-time PCR: according to MOC3/115 ‘annex 1’
Target DNA sequence specific: Pistachio: COR gene dehydrin Pecan nuts: pec2a1a (7S vicilin)
Grinding /Homogenisation Manual extraction of DNA by silica gel column adsorption Amplification by real time PCR (qualitative method)
In-house method MOC3/115: Grinding /Homogenisation IC3/01-01.D Extraction of ADN: NucleoSpin®Plant II (Macherey-Nagel) Real-time PCR: according to MOC3/115 ‘annex 2’
Cereal products: Raw material: soybeans, barley Processed products: (granules, cake, cookies) Tea and infusion: Tea, Jasmine flower Sweet and sweetened products: cake mixtures, cake
Target DNA sequence specific for peanut: Arah 1 gene
Grinding /Homogenisation Manual extraction of DNA by silica gel column adsorption Amplification by real time PCR (qualitative method)
In-house method MOC3/115:
Grinding /Homogenisation IC3/01-01.D Extraction of ADN: NucleoSpin®Plant II
(Macherey-Nagel) Real-time PCR: according
to: according to MOC3/115
‘annex 1’
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
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INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
ITEM CHARACTERISTIC MEASURED OR SOUGHT PRINCIPLE OF THE METHOD REFERENCE OF THE METHOD
Cereal products: Raw material: soybeans, barley Processed products: (granules, cake, cookies) Sweet and sweetened products: cake mixtures, cake
Specific target DNA sequence for sesame: 2S albumin
Grinding /Homogenisation Manual extraction of DNA by silica gel column adsorption Amplification by real time PCR (qualitative method)
In-house method MOC3/115: Grinding /Homogenisation C3/01-01. D Extraction of ADN: NucleoSpin®Plant II (Macherey-Nagel) Real-time PCR: according to MOC3/115 ‘annex 1’
Cereal products: Raw material: corn flour, lupin flour, tapioca starch, chestnut flour Processed products: (granules, fondant, pancakes, muffins, cookies)
Specific target DNA sequence for Brazilian nuts: 2S albumin (ber e1)
Grinding /Homogenisation Manual extraction of DNA by silica gel column adsorption Amplification by real time PCR (qualitative method)
In-house method MOC3/115: Grinding /Homogenisation C3/01-01. D Extraction of ADN: NucleoSpin®Plant II (Macherey-Nagel) Real-time PCR: according to MOC3/115 ‘annex 1’
Cereal products: Raw material: corn flour, lupin flour, tapioca starch, chestnut flour. Processed products: (granules, fondant, pancakes, muffins, cookies)
Sweet and sweetened products: Soy yogurt, soy cream, fruit compote, vegetable drinks
Target DNA sequence specific soya: Lectine
Grinding /Homogenisation Manual extraction of DNA by silica gel column adsorption Amplification by real time PCR (qualitative method)
In-house method MOC3/115: Grinding /Homogenisation C3/01-01. D Extraction of ADN: NucleoSpin®Plant II
(Macherey-Nagel) Real-time PCR: according to
MOC3/115 ‘annex 1’
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
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INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
ITEM CHARACTERISTIC MEASURED OR SOUGHT PRINCIPLE OF THE METHOD REFERENCE OF THE METHOD
Cereal products: Raw material: corn flour, lupin flour, tapioca starch, chestnut flour. Processed products: fondant, filled pancakes, filled muffins, chocolate chip cookies, prepared baby food dishes, frozen patties, zucchini, vegetable terrine, verrine meat.
Sweet and sweetened products: Soy yogurt, soy cream, vegetable drinks
Target DNA sequence specific celery: 5.8 ribosomal RNA
Grinding /Homogenisation Manual extraction of DNA by silica gel column adsorption Amplification by real time PCR (qualitative method)
In-house method MOC3/115: Grinding /Homogenisation C3/01-01. D Extraction of ADN: NucleoSpin®Plant II (Macherey-Nagel) Real-time PCR: according to MOC3/115 ‘annex 1’
Cereal products: Raw material: corn flour, lupin flour, tapioca Processed products: fondant, pancakes, muffins Sweet and sweetened products: Turron, soy fruit cream, fruit compote, vegetable drinks
Target DNA sequence specific lupine: conglutin alpha mRNA
Grinding /Homogenisation Manual extraction of DNA by silica gel column adsorption Amplification by real time PCR (qualitative method)
In-house method MOC3/115: Grinding /Homogenisation C3/01-01. D Extraction of ADN: NucleoSpin®Plant II (Macherey-Nagel) Real-time PCR: according to MOC3/115 ‘annex 1’
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
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INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
Scope FLEX3
General scope*
Food and food products/ Allergens / Immunology
ITEM CHARACTERISTIC MEASURED OR SOUGHT PRINCIPLE OF THE METHOD
Cereal products
Alcoholic and non-alcoholic drinks
Compound feed
Meat production
Fish products
Sweet and sweetened products
Dairy products
Detection and quantification of allergenic proteins
Grinding /Homogenisation Extraction of proteins ELISA
* FLEX3 Flexible Scope: The laboratory is recognised as competent, in the area covered by the general scope, to adopt any recognised method and to develop or implement any other method for which it has provided validation.
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
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INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
Detailed scope
Food and food products/ Allergens / Immunology
ITEM CHARACTERISTIC MEASURED OR SOUGHT PRINCIPLE OF THE METHOD REFERENCE OF THE
METHOD
Cereal products
Compound products
Raw cereals and primary products: wheat, rye, barley, barley, oats, spelt and their hybrid strains, rice, sorghum, quinoa, lentils, chick peas, flour and derivatives, cereal flakes, tapioca, buckwheat, brewer's yeast, guar gum.
Mix for pastry Pizzas Spreads Cereal puree and vegetables, ravioli Breakfast cereals Sauce preparations Spices and aromatic plants
Detection and quantification of gluten
Grinding /Homogenisation Extraction of proteins ELISA
In-house method MOC3/119 according to supplier kit: R7001 RIDASCREEN® Gliadin (R. BIOPHARM)
Fish products Fresh and Canned Fish
Alcoholic beverages
Wine
Detection of histamine Grinding /Homogenisation Extraction of proteins ELISA
In-house method MOC3/135 version 1 according to supplier kit: R1601 RIDASCREEN® Histamine (R. BIOPHARM)
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
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INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
ITEM CHARACTERISTIC MEASURED OR SOUGHT PRINCIPLE OF THE METHOD REFERENCE OF THE
METHOD
Non-alcoholic beverages
Cereal products
Sweet products
Compound products
Almond milk; Soy milk; Fruit juice Raw cereals and primary products Blown cereals Cereal products containing chocolate Sorbets & water ice cream Prepared meals based on cereals and vegetables Babyfood based on cereals and vegetables
Detection and quantification of casein
Grinding /Homogenisation Extraction of proteins ELISA
In-house method MOC3/125 version 2 according to supplier R4612 RIDASCREEN®FAST Casein (R. BIOPHARM)
Cereal products
Compound products
Meat products
Dairy products
Beverages
Raw cereals and primary products Blown cereals Babyfood Chile Bolognese sauce Soup Cheese Pork ham and pork chorizo wine
Detection and quantification of egg protein
Grinding /Homogenisation Extraction of proteins ELISA
In-house method MOC3/125 according to supplier kit: R6402 RIDASCREEN®FAST Ei /Egg Protein (R. BIOPHARM)
Almond milk
Soy milk
Crude cereals and products of
primary processing - Blown
cereals
Chile
Bolognese sauce
Wine
Detection and quantification of total milk protein
Grinding /Homogenisation Extraction of proteins ELISA
In-house method MOC3/125 according to supplier kit R4652 RIDASCREEN®FAST Milk (R. BIOPHARM
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
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INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
Grain products (raw and first processing) : Corn flour, soya, quinoa, wheat semolina Grain products processed: Mini plum, Mix dry pastry, Cookies, sandwich bread, Mixed feeds: Chili con carne, Bolognese sauce, Mediterranean pizza, Doy passato BBF ; Sweet products: Organic candy, Hazelnut ice cream, Glucose syrup, Chocolate
Detection and quantification of beta-lactoglubin
Grinding /Homogenisation Extraction of proteins ELISA
In-house method MOC3/190 selon kit fournisseur R4912 RIDASCREEN® FAST β-Lactoglobulin (R. BIOPHARM)
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
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INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
Contaminants from packaging and materials Scope of accreditation N°1-1904
Scope FLEX3
General scope*
Food processing / Other foods / Physical and chemical analyses
Analysis of pesticide residues and organic contaminants in foodstuffs intended for human or animal consumption, biological matrices of animal origin - LAB GTA 26/99-2
ITEM CHARACTERISTIC MEASURED OR SOUGHT PRINCIPLE OF THE METHOD
Products of plant origin Products of animal origin Animal feed
Organic Contaminant Residues
Extraction : by solvent Purification : Liquid-Solid (SPE) Analysis : UFLC, LC-MS/MS, GC-MS/MS
* FLEX3 Flexible Scope: The laboratory is recognised as competent, in the area covered by the general scope, to adopt any recognised method and to develop or implement any other method for which it has provided validation.
Detailed scope
Food processing / Other foods / Physical and chemical analyses
Analysis of pesticide residues and organic contaminants in foodstuffs intended for human or animal consumption, biological matrices of animal origin - LAB GTA 26/99-2
ITEM CHARACTERISTIC MEASURED OR SOUGHT PRINCIPLE OF THE METHOD REFERENCE OF
THE METHOD
Products of plant origin: Watery product Acid and water-rich products Products rich in sugar and low in water Products low in water and fat Alcoholic beverages Fruit and vegetable juices Sodas Products of animal origin : Dairy products including infant nutrition
Bisphenol A
Extraction : Solid/liquid cold extraction Purification : SPE Analysis : LC-MS/MS
In-house method MOC3/62
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
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INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
ITEM CHARACTERISTIC MEASURED OR SOUGHT PRINCIPLE OF THE METHOD
REFERENCE OF THE METHOD
Products of plant origin: Alcoholic beverages, Oils
Determination of the content of Phthalates and other plasticisers: - DMP (Dimethyl phtalate) -DiBP (Di-iso-butyl phtalate) -DBP (Di-n-butyl phtalate) -BBP (Benzylbutyl phtalate) -DiPP (Di-iso-pentyl phtalate) -nPiPP (n-pentyl-iso-pentyl phthalate) -DPP (Di-n-pentyl phtalate) -DHxP (Di-n-hexyl phthalate) -DEHP (Bis(2-ethylhexyl) phtalate) -DCHP (Dicyclohexyl phtalate) -DiHpP (Di-iso-heptyl phtalate) -DnOP (Di-n-octyl phtalate) -DEHT (Bis(2-ethylhexyl) terephtalate) -DiNP (Di-iso-nonyl phtalate) -DNP (Di-n-nonyl phtalate) -DiDP (Di-iso-decyl phtalate) -DiBA (Di-iso-butyl adipate) -DBA (Di-n-butyl adipate) -DINCH (1,2-cyclohexanedicarboxylic acid, diisononyl ester) -Tributyl O-acetylcitrate - DMEP (Bis(2-methoxyethyl) phtalate) - DMiP (Dimethyl isophtalate) - DMT (Dimethyl terephthalate) - DPhP (Diphenyl phthalate) - DAP (Diallyl phthalate) - DEP (Diethyl phthalate) - TBP (tributylphosphate) - DEA (Diethyl adipate) - DEHA (Bis(2-ethylhexyl) adipate) - DVA (Divinyl adipate)
Extraction : Liquid/liquid cold extraction Analysis : GC-MS-MS
In-house method MOC3/137
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
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INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
Neoformed contaminants : Scope of accreditation N°1-1904
Scope FLEX3
General scope*
Food processing / Other foods / Physical and chemical analyses
Analysis of pesticide residues and organic contaminants in foodstuffs intended for human or animal consumption, biological matrices of animal origin - LAB GTA 26/99-2
ITEM CHARACTERISTIC MEASURED OR SOUGHT PRINCIPLE OF THE METHOD
Products of plant origin Products of animal origin Animal feed
Pesticide Residues
Extraction: Solid/Liquid Purification (if necessary) : Liquid-Solid (SPE) Liquid-Solid (SPE dispersive) Analysis : LC/MS-MS, GC/MS-MS, GC-MS
* FLEX3 Flexible Scope: The laboratory is recognised as competent, in the area covered by the general scope, to adopt any recognised method and to develop or implement any other method for which it has provided validation.
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
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INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
Detailed scope
Food processing / Other foods / Physical and chemical analyses
Analysis of pesticide residues and organic contaminants in foodstuffs intended for human or animal consumption, biological matrices of animal origin - LAB GTA 26/99-2
ITEM CHARACTERISTIC MEASURED OR SOUGHT PRINCIPLE OF THE METHOD REFERENCE OF
THE METHOD
Products of plant and animal origin: Tea, cocoa, vegetable oils, soy sauce, hydrolyzed vegetable proteins, infant milk
3-MCPD (free) 2-MCPD (free) Glycidol (free)
Preparation/Extraction: Solid / cold liquid Liquid / cold liquid Purification: Derivation Analysis : GC-MS/MS
In-house method MOC3/59
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
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INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
Scope FLEX3
General scope*
Food processing / Other foods / Physical and chemical analyses
Analysis of pesticide residues and organic contaminants in foodstuffs intended for human or animal consumption, biological matrices of animal origin - LAB GTA 26/99-2
ITEM CHARACTERISTIC MEASURED OR SOUGHT PRINCIPLE OF THE METHOD
Products of plant origin Products of animal origin Animal feed
Organic Contaminant Residues
Extraction : by solvent Purification : Liquid-Solid (SPE) Analysis : UFLC, LC-MS/MS, GC-MS/MS
* FLEX3 Flexible Scope: The laboratory is recognised as competent, in the area covered by the general scope, to adopt any recognised method and to develop or implement any other method for which it has provided validation.
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
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INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
Detailed scope
Food processing / Other foods / Physical and chemical analyses
Analysis of pesticide residues and organic contaminants in foodstuffs intended for human or animal consumption, biological matrices of animal origin - LAB GTA 26/99-2
ITEM CHARACTERISTIC MEASURED OR SOUGHT PRINCIPLE OF THE METHOD REFERENCE OF
THE METHOD
Products of vegetal origin : Spices Aromatic and medicinal plants Products rich in sugar and low in water Watery product, High oil content products, Acid and water-rich products, Products low in water and fat, Alcoholic beverages, Fruit and vegetable juices, Sodas Products of animal origin : Beehive products, Dairy products, Meat products, Fish products, Fats Animal feed : Animal feed Other : Cacao
Polycyclic aromatic hydrocarbons : Benzo(a)anthracène, Benzo(b)fluoranthène, Benzo(a)pyrène, Chrysène.
Preparation / Extraction : Liquid/liquid cold extraction Purification : SPE Analysis : GC-MS/MS
In-house method MOC3/23
Products of vegetal origin : High oil content products Cereals and by-products Cacao Products of animal origin : Dairy products Meat products Fats Fish products Infant nutrition
Polycyclic aromatic hydrocarbons: Benzo(a)anthracène, Benzo(b)fluoranthène, Benzo(a)pyrène, Benzo(k)fluoranthène, Chrysène, Dibenzo(a, e)pyrene, Dibenzo(a, l)pyrene, Fluoranthène, 5-methylchrysene, Pyrène
Extraction : Solid/liquid cold extraction Purification : SPE Analysis : UFLC
In-house method MOC3/29
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
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INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
Products of plant origin: Cereals and by-products Cacao Tea and coffee High oil content products Infant nutrition Products of animal origin : Dairy products Meat products Fats Fish products Infant nutrition Animal feed : Raw materials of vegetable origin
Polycyclic aromatic hydrocarbons: Acenaphtène, Acenaphtylène, Benzo(g,h,i)perylène, Benzo(k)fluoranthène, Benzo(j)fluoranthène, Cyclopenta(c,d)pyrene, Dibenzo(a,h)anthracène, Dibenzo(a, l)pyrene, Fluorène, Indeno(1,2,3-cd)pyrène, 5- methylchrysene. Anthracene Phenanthrene Fluoranthene Pyrene
Extraction : Solid/liquid cold extraction Purification : SPE Analysis : GC-MS/MS
In-house method MOC3/28
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
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INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
ITEM CHARACTERISTIC MEASURED OR SOUGHT PRINCIPLE OF THE METHOD REFERENCE OF
THE METHOD
Products of plant origin: Watery product and by-products, Cereals and by-products, Products rich in sugar and low in water, Nuts, Vegetable and Fruit juices, Wine, cider, beer, coffee, tea Products of animal origin : Meat products Fish products Milk, Yogurt
Determination of the content of Acrylamide
Extraction : Solid/liquid cold extraction Purification : SPE Analysis : LC-MS/MS
In-house method MOC3/129
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
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Phytocontrol Laboratoire d’analyses
INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
Dioxins and PCBs Scope of accreditation N°1-1904
FIXED Scope
Food processing / Other foods / Physical and chemical analyses
Analysis of pesticide residues and organic contaminants in foodstuffs intended for human or animal consumption, biological matrices of animal origin - LAB GTA 26/99-2
ITEM CHARACTERISTIC MEASURED OR SOUGHT PRINCIPLE OF THE METHOD REFERENCE OF
THE METHOD
Products of plant origin: High oil content products Watery product Acid and water-rich products Products rich in sugar and low in water Products low in water and fat Infant nutrition Other products: spices, coffee, tea, aromatic and medicinal plants Products of animal origin : Dairy products (cheese) Egg products Meat products Fish products Infant nutrition Animal feed : Flours of animal origin Mixed feeds Raw materials of vegetable origin Mineral Compounds
Polychlorodibenzo-p-dioxines (PCDD) : 2,3,7,8-TCDD, 1,2,3,7,8-PeCDD, 1,2,3,4,7,8-HxCDD, 1,2,3,6,7,8-HxCDD, 1,2,3,7,8,9-HxCDD, 1,2,3,4,6,7,8-HpCDD, OCDD
Polychlorodibenzofurannes (PCDF) : 2,3,7,8–TCDF, 1,2,3,7,8-PeCDF, 2,3,4,7,8-PeCDF, 1,2,3,4,7,8-HxCDF, 1,2,3,6,7,8-HxCDF, 1,2,3,7,8,9-HxCDF, 2,3,4,6,7,8-HxCDF, 1,2,3,4,6,7,8-HpCDF, 1,2,3,4,7,8,9-HpCDF, OCDF,
PCB “dioxins like” : PCB77, PCB81, PCB126, PCB169, PCB105, PCB114, PCB118, PCB123, PCB156, PCB157, PCB167, PCB189
PCB « Non dioxins Like » (indicators) : PCB28, PCB52, PCB101,
PCB138, PCB 153, PCB180
Extraction :
Under hot pressure
(PFE)
Purification:
SPE
Analysis :
GC-HRMS
Dilution isotopique
In-house method MOC3/130
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
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Phytocontrol Laboratoire d’analyses
INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
ITEM CHARACTERISTIC MEASURED OR SOUGHT PRINCIPLE OF THE METHOD REFERENCE OF
THE METHOD
Products of plant origin: High oil content products (vegetable oils) Alcoholic beverages Fruit and vegetable juices Soda Products of animal origin : Dairy products (milk, yoghurt, very fatty products) Fats Infant nutrition Animal feed : Fats
Polychlorodibenzo-p-dioxines (PCDD) : 2,3,7,8-TCDD, 1,2,3,7,8-PeCDD, 1,2,3,4,7,8-HxCDD, 1,2,3,6,7,8-HxCDD, 1,2,3,7,8,9-HxCDD, 1,2,3,4,6,7,8-HpCDD, OCDD,
Polychlorodibenzofurannes (PCDF) : 2,3,7,8–TCDF, 1,2,3,7,8-PeCDF, 2,3,4,7,8-PeCDF, 1,2,3,4,7,8-HxCDF, 1,2,3,6,7,8-HxCDF, 1,2,3,7,8,9-HxCDF, 2,3,4,6,7,8-HxCDF, 1,2,3,4,6,7,8-HpCDF, 1,2,3,4,7,8,9-HpCDF, OCDF,
PCB “dioxines like” : PCB77, PCB81, PCB126, PCB169, PCB105, PCB114, PCB118, PCB123, PCB156, PCB157, PCB167, PCB189
PCB « Non dioxines Like » (indicators) : PCB28, PCB52, PCB101, PCB138, PCB 153, PCB180
Extraction :
Liquid-Liquide
Purification:
SPE
Analysis :
GC-HRMS
Isotopic dilution
In-house method MOC3/131
FIXED Scope : The laboratory is recognized as competent to practice the methods described in strict compliance with the recognized methods mentioned in the Scope of accreditation.
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
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Phytocontrol Laboratoire d’analyses
INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
Scope FLEX3
General scope*
Food processing / Other foods / Physical and chemical analyses
Analysis of pesticide residues and organic contaminants in foodstuffs intended for human or animal consumption, biological matrices of animal origin - LAB GTA 26/99-2
ITEM CHARACTERISTIC MEASURED OR SOUGHT PRINCIPLE OF THE METHOD
Products of plant origin Products of animal origin Animal feed
Organic Contaminant Residues
Preparation/Extraction : Solid / liquid cold by solvent Purification : Liquid-Solid (SPE) Analysis : UFLC-FLD, LC-MS/MS, GC-MS/MS
* FLEX3 Flexible Scope: The laboratory is recognised as competent, in the area covered by the general scope, to adopt any recognised method and to develop or implement any other method for which it has provided validation.
Detailed scope
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
Page 50 sur 67
Phytocontrol Laboratoire d’analyses
INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
Food processing / Other foods / Physical and chemical analyses
Analysis of pesticide residues and organic contaminants in foodstuffs intended for human or animal consumption, biological matrices of animal origin - LAB GTA 26/99-2
ITEM CHARACTERISTIC MEASURED OR SOUGHT PRINCIPLE OF THE METHOD REFERENCE OF
THE METHOD
Products of plant origin: High oil content products Infant nutrition Products of animal origin : Dairy products (cheese) Egg products Meat products Fish products Infant nutrition Animal feed : Farines d’origine animales Mixed feeds Minerals compound
Polychlorodibenzo-p-dioxines (PCDD) : 2,3,7,8-TCDD, 1,2,3,7,8-PeCDD, 1,2,3,4,7,8-HxCDD, 1,2,3,6,7,8-HxCDD, 1,2,3,7,8,9-HxCDD, 1,2,3,4,6,7,8-HpCDD, OCDD Polychlorodibenzofurannes (PCDF) : 2,3,7,8–TCDF, 1,2,3,7,8-PeCDF, 2,3,4,7,8-PeCDF, 1,2,3,4,7,8-HxCDF, 1,2,3,6,7,8-HxCDF, 1,2,3,7,8,9-HxCDF, 2,3,4,6,7,8-HxCDF, 1,2,3,4,6,7,8-HpCDF, 1,2,3,4,7,8,9- HpCDF, OCDF PCB “dioxins like” : PCB77, PCB81, PCB126, PCB169, PCB105, PCB114, PCB118, PCB123, PCB156, PCB157, PCB167, PCB189 PCB “non dioxins like” (indicators) : PCB28, PCB52, PCB101, PCB138, PCB 153, PCB180
Preparation / Extraction : By solvent Purification: SPE Analysis : GC-MS/MS Isotopic dilution
In-house method
MOC3/180
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
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Phytocontrol Laboratoire d’analyses
INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
Products of plant origin: High oil content products (vegetable oils) Products of animal origin : Dairy products Fats Infant nutrition Animal feed : Fats
Polychlorodibenzo-p-dioxines (PCDD) : 2,3,7,8-TCDD, 1,2,3,7,8-PeCDD, 1,2,3,4,7,8-HxCDD, 1,2,3,6,7,8-HxCDD, 1,2,3,7,8,9-HxCDD, 1,2,3,4,6,7,8-HpCDD, OCDD Polychlorodibenzofurannes (PCDF) : 2,3,7,8–TCDF, 1,2,3,7,8-PeCDF, 2,3,4,7,8-PeCDF, 1,2,3,4,7,8-HxCDF, 1,2,3,6,7,8-HxCDF, 1,2,3,7,8,9-HxCDF, 2,3,4,6,7,8-HxCDF, 1,2,3,4,6,7,8-HpCDF, 1,2,3,4,7,8,9- HpCDF, OCDF PCB “dioxins like” : PCB77, PCB81, PCB126, PCB169, PCB105, PCB114, PCB118, PCB123, PCB156, PCB157, PCB167, PCB189 PCB “non dioxins like” (indicators): PCB28, PCB52, PCB101, PCB138, PCB 153, PCB180
Preparation / Extraction : By solvent Purification: SPE Analysis : GC-MS/MS Isotopic dilution
In-house method
MOC3/181
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
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Phytocontrol Laboratoire d’analyses
INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
Veterinary drug residues Scope of accreditation N°1-1904
Scope FLEX3
General scope*
# Food processing / Other foods / Physical and chemical analyses
Analysis of authorised or unauthorised substances for veterinary or zootechnical use (veterinary medicinal products) - LAB GTA 30/99-6
ITEM CHARACTERISTIC MEASURED OR SOUGHT PRINCIPLE OF THE METHOD
Biological matrices of animal origin Chloramphenicol
Preparation : Extraction by solvent Purification : SPE dispersive Analysis : LC-MS/MS
* FLEX3 Flexible Scope: The laboratory is recognised as competent, in the area covered by the general scope, to adopt any recognised method and to develop or implement any other method for which it has provided validation.
Detailed scope
# Food processing / Other foods / Physical and chemical analyses
Analysis of authorised or unauthorised substances for veterinary or zootechnical use (veterinary medicinal products) - LAB GTA 30/99-6
ITEM CHARACTERISTIC MEASURED OR SOUGHT PRINCIPLE OF THE METHOD REFERENCE OF
THE METHOD
Œufs Muscles Milk Honey Fish products :fish, shellfish, crustaceans
Chloramphenicol
Preparation : Extraction by solvent Purification : SPE dispersive Analysis : LC-MS/MS
In-house method MOC3/147
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
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Phytocontrol Laboratoire d’analyses
INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
Food colouring Scope of accreditation N°1-1904
FIXED Scope
Agri-food / Other foods, Beverages (excluding drinking water) and Sweet products / Physico-chemical analysis
Physico-chemical analyses for the determination of composition, quality and technological criteria, and nutritional labelling in human food and animal nutrition - LAB GTA 25/60-118
ITEM CHARACTERISTIC MEASURED OR SOUGHT PRINCIPLE OF THE METHOD REFERENCE OF
THE METHOD
Spices and condiments Mixed feeds Sauce
Dosing of dyes: Auramine, Fast garnet GBC, Oil orange SS, Para red, P-nitroaniline, Sudan blue 2, Sudan I, Sudan II, Sudan III, Sudan IV, Sudan red 7B, Sudan red G, Sudan yellow, Toluidine red, Vert de leucomalachite.
Extraction : by solvent Analysis : LC-MS/MS
In-house method MOC3/163
Non-alcoholic beverages
Dosing of dyes: E101, E110, E122, E123, E124, E129, E131, E132, E133, E151
Extraction : by solvent Analysis : UFLC-DAD
In-house method MOC3/161
FIXED Scope : The laboratory is recognized as competent to perform the tests in strict compliance with the methods mentioned in the scope of accreditation. Technical changes to the operating mode are not permitted.
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
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Phytocontrol Laboratoire d’analyses
INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
Nutritional values Scope of accreditation N°1-1904
Scope FLEX3
General scope*
Agri-food / Other foods, Dairy products, Animal feed, Fats, Beverages (excluding drinking water) and Sweet products, Grain products / Analyses physico-chemical
Physico-chemical analyses for the determination of composition, quality and technological criteria, and nutritional labelling in human food and animal feed - LAB GTA 25/60-61-81-82-118-119
ITEM CHARACTERISTIC MEASURED OR SOUGHT PRINCIPLE OF THE METHOD
Human food Animal feed Determination of the content of sodium
Preparation : Mineralisation (wet process) Analysis : ICP-MS
* FLEX3 Flexible Scope: The laboratory is recognised as competent, in the area covered by the general scope, to adopt any recognised method and to develop or implement any other method for which it has provided validation.
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
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Phytocontrol Laboratoire d’analyses
INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
Detailed scope
Agri-food / Other foods, Dairy products, Animal feed, Fats, Beverages (excluding drinking water) and Sweet products, Grain products / Analyses physico-chemical
Physico-chemical analyses for the determination of composition, quality and technological criteria, and nutritional labelling in human food and animal feed - LAB GTA 25/60-61-81-82-118-119
ITEM CHARACTERISTIC MEASURED OR SOUGHT PRINCIPLE OF THE METHOD REFERENCE OF
THE METHOD
Human food : Fruits and vegetables Mixed feeds Dairy products Fatty products Sweet products Grain products Egg products Meat products Fish products Coffee, Teas, Infusion Non-alcoholic beverages Spices and condiments Dietetic foods, diet foods, special foods Animal feed : Complete or complementary mixed feeds Raw material for anaimal nutrition
Determination of the content of total sodium and calculation of salt content
Preparation : Mineralisation (wet process) Analysis : ICP-MS
In-house method MOC3/152
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
Page 56 sur 67
Phytocontrol Laboratoire d’analyses
INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
Scope FLEX3
General scope*
Agri-food / Other aliments, Dairy products, Animal feed, Fats, Beverages (excluding drinking water) and Sweet products, Grain products / Analyses physico-chemicals
Physico-chemical analyses for the determination of composition, quality and technological criteria, and nutritional labelling in human food and animal feed - LAB GTA 25/60-61-81-82-118-119
ITEM CHARACTERISTIC MEASURED OR SOUGHT PRINCIPLE OF THE METHOD
Human food Determination of carbohydrate components
Preparation : Water extraction Analysis : Ion chromatography / Pulsed amperometry
* FLEX3 Flexible Scope: The laboratory is recognised as competent, in the area covered by the general scope, to adopt any recognised method and to develop or implement any other method for which it has provided validation.
Detailed scope
Agri-food / Other aliments, Dairy products, Animal feed, Fats, Beverages (excluding drinking water) and Sweet products, Grain products / Analyses physico-chemicals
Physico-chemical analyses for the determination of composition, quality and technological criteria, and nutritional labelling in human food and animal feed - LAB GTA 25/60-61-81-82-118-119
ITEM CHARACTERISTIC MEASURED OR SOUGHT PRINCIPLE OF THE METHOD REFERENCE OF
THE METHOD
Human food : Fruits and vegetables Mixed feeds Dairy products Sweet products Grain products Dietary foods
Determination of the content of Fructose, Glucose, Lactose, Maltose, Saccharose
Preparation : Water extraction Analysis : Ion Chromatography / Pulsed Amperometry
In-house method MOC3/168
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
Page 57 sur 67
Phytocontrol Laboratoire d’analyses
INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
Nutritional values Scope of accreditation N°1-1904
FIXED Scope
Agri-food / Other aliments, Dairy products, Animal feed, Fats, Beverages (excluding drinking water) and Sweet products, Grain products / Analyses physico-chemicals
Physico-chemical analyses for the determination of composition, quality and technological criteria, and nutritional labelling in human food and animal nutrition - LAB GTA 25/82-118
ITEM CHARACTERISTIC MEASURED OR SOUGHT PRINCIPLE OF THE METHOD REFERENCE OF
THE METHOD
Fatty products Sweet products Fat extraction for characterisation
Extraction by solvent : n-hexane / Isopropanol 3 /2 (v/v)
In-house method MOC3/160
Fatty products Sweet products
Multi-residue determination of methyl esters, fatty acids
Preparation : Methylation Analysis : GC-FID
In-house method MOC3/160
FIXED Scope : The laboratory is recognized as competent to perform the tests in strict compliance with the methods mentioned in the scope of accreditation. Technical changes to the operating mode are not permitted.
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
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Phytocontrol Laboratoire d’analyses
INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
FIXED Scope
Agri-food / Other aliments, Dairy products, Animal feed, Fats, Beverages (excluding drinking water) and Sweet products, Grain products / Analyses physico-chemicals
Physical-chemical analyses for the determination of composition, quality and technological criteria, and nutrition labelling in food and feed - GAB GTA 25/60-61-80-81-82-118-119
ITEM CHARACTERISTIC MEASURED OR SOUGHT PRINCIPLE OF THE METHOD REFERENCE OF
THE METHOD
Human food : Fruits and vegetables Dietary foods Diet foods Special power supply Mixed feeds Spices and condiments Dairy products Meat products Fish products Sweet products Coffee, tea, infusion Grain products Animal feed : Mixed feeds
Determination of water activity
Hygrometry (Principle of dew point)
In-house method MOC3/155
FIXED Scope : The laboratory is recognized as competent to perform the tests in strict compliance with the methods mentioned in the scope of accreditation. Technical changes to the operating mode are not permitted.
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
Page 59 sur 67
Phytocontrol Laboratoire d’analyses
INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
Scope FLEX3
General scope*
Agri-food / Other aliments, Dairy products, Animal feed, Fats, Beverages (excluding drinking water) and Sweet products, Grain products / Analyses physico-chemicals
Physical-chemical analyses for the determination of composition, quality and technological criteria, and nutrition labelling in food and feed - LAB GTA 25/60-118-119
ITEM CHARACTERISTIC MEASURED OR SOUGHT PRINCIPLE OF THE METHOD
Human food
Determination of content of food fiber
Preparation/Extraction: Enzymatic digestion Analysis: Gravimetry
* FLEX3 Flexible Scope: The laboratory is recognised as competent, in the area covered by the general scope, to adopt any recognised method and to develop or implement any other method for which it has provided validation.
Detailed scope
Agri-food / Other aliments, Dairy products, Animal feed, Fats, Beverages (excluding drinking water) and Sweet products, Grain products / Analyses physico-chemicals
Physical-chemical analyses for the determination of composition, quality and technological criteria, and nutrition labelling in food and feed - LAB GTA 25/60-118-119
ITEM CHARACTERISTIC MEASURED OR SOUGHT PRINCIPLE OF THE METHOD REFERENCE OF
THE METHOD
Fruits and vegetables Mixed feeds Sweet products Grain products
Determination of total dietary fibre
Preparation/Extraction: Enzymatic digestion Analysis: Gravimetry
In-house method MOC3/156
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
Page 60 sur 67
Phytocontrol Laboratoire d’analyses
INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
Scope FLEX3
General scope*
Agri-food / Other aliments, Dairy products, Animal feed, Fats, Beverages (excluding drinking water) and Sweet products, Grain products / Analyses physico-chemicals
Physico-chemical analyses for the determination of composition, quality and technological criteria, and nutritional labelling in human food and animal feed - LAB GTA 25/60-61-81-82-118-119
ITEM CHARACTERISTIC MEASURED OR SOUGHT PRINCIPLE OF THE METHOD
Human food Animal feed Determination of total fat content
Preparation : Hydrolysis Extraction by solvent Analysis: Gravimetry
* FLEX3 Flexible Scope: The laboratory is recognised as competent, in the area covered by the general scope, to adopt any recognised method and to develop or implement any other method for which it has provided validation.
Detailed scope
Agri-food / Other aliments, Dairy products, Animal feed, Fats, Beverages (excluding drinking water) and Sweet products, Grain products / Analyses physico-chemicals
Physico-chemical analyses for the determination of composition, quality and technological criteria, and nutritional labelling in human food and animal feed - LAB GTA 25/60-61-81-82-118-119
ITEM CHARACTERISTIC MEASURED OR SOUGHT PRINCIPLE OF THE METHOD REFERENCE OF
THE METHOD
Human food : Fruits and vegetables Mixed feeds Dairy products Fatty products without seeds Oilseeds Sweet products Grain products except Raw cereals Dietary foods Spices and condiments Meat products Non-alcoholic beverages Animal feed : Complete or complementary compound feedingstuffs
Determination of total fat content
Preparation : Hydrolysis Extraction by solvent Analysis: Gravimetry
In-house method MOC3/154
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
Page 61 sur 67
Phytocontrol Laboratoire d’analyses
INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
Scope FLEX3
General scope*
Agri-food / Other aliments, Dairy products, Animal feed, Fats, Beverages (excluding drinking water) and Sweet products, Grain products / Analyses physico-chemicals
Physico-chemical analyses for the determination of composition, quality and technological criteria, and nutritional labelling in human food and animal feed - LAB GTA 25/60-61-81-82-118-119
ITEM CHARACTERISTIC MEASURED OR SOUGHT PRINCIPLE OF THE METHOD
Human food Animal feed Determination of total nitrogen content
Kjeldahl : Mineralisation Distillation Titrimetry
* FLEX3 Flexible Scope: The laboratory is recognised as competent, in the area covered by the general scope, to adopt any recognised method and to develop or implement any other method for which it has provided validation.
Detailed scope
Agri-food / Other aliments, Dairy products, Animal feed, Fats, Beverages (excluding drinking water) and Sweet products, Grain products / Analyses physico-chemicals
Physico-chemical analyses for the determination of composition, quality and technological criteria, and nutritional labelling in human food and animal feed - LAB GTA 25/60-61-81-82-118-119
ITEM CHARACTERISTIC MEASURED OR SOUGHT PRINCIPLE OF THE METHOD REFERENCE OF
THE METHOD
Human food : Fruits and vegetables Mixed feeds Dairy products Fatty products Sweet products Grain products Dietary foods Spices and condiments Animal feed : Complete or complementary compound feedingstuffs
Determination of total nitrogen content and protein content calculation
Kjeldahl : Mineralisation Distillation Titrimetry
In-house method MOC3/153
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
Page 62 sur 67
Phytocontrol Laboratoire d’analyses
INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
Scope FLEX3
General scope*
Agri-food / Other aliments, Dairy products, Animal feed, Fats, Beverages (excluding drinking water) and Sweet products, Grain products / Analyses physico-chemicals
Physico-chemical analyses for the determination of composition, quality and technological criteria, and nutritional labelling in human food and animal feed - LAB GTA 25/60-61-81-82-118-119
ITEM CHARACTERISTIC MEASURED OR SOUGHT PRINCIPLE OF THE METHOD
Human food Animal feed
Determination of humidity Drying process Gravimetry
Determination of ash content Dry Mineralization Gravimetry
* FLEX3 Flexible Scope: The laboratory is recognised as competent, in the area covered by the general scope, to adopt any recognised method and to develop or implement any other method for which it has provided validation.
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
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INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
Detailed scope
Agri-food / Other aliments, Dairy products, Animal feed, Fats, Beverages (excluding drinking water) and Sweet products, Grain products / Analyses physico-chemicals
Physico-chemical analyses for the determination of composition, quality and technological criteria, and nutritional labelling in human food and animal feed - LAB GTA 25/60-61-81-82-118-119
ITEM CHARACTERISTIC MEASURED OR SOUGHT PRINCIPLE OF THE METHOD REFERENCE OF
THE METHOD
Foodstuff : Fruit and vegetables Compound foods Dairy products Non-seeded fat products oleaginous Sweet and sweetened products Cereal products except crude cereals Dietetic foods Spices and condiments Animal feed: Complete or complementary compound feedingstuffs
Determination of dry matter content or moisture content
Drying process Gravimetry
In-house method MOC3/150
Determination of ash content Dry Mineralization Gravimetry
In-house method MOC3/151
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
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INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
Scope FLEX3
General scope*
Agri-food / Other foods, Beverages (excluding drinking water) and Sweet products / Physico-chemical analyses
Physico-chemical analyses for the determination of composition, quality and technological criteria, and nutritional labelling in human food - LAB GTA 25/60-118
ITEM CHARACTERISTIC MEASURED OR SOUGHT PRINCIPLE OF THE METHOD
Human food
Determination of sulphite content
Monier-Williams optimized method: Distillation Titrimetry
* FLEX3 Flexible Scope: The laboratory is recognised as competent, in the area covered by the general scope, to adopt any recognised method and to develop or implement any other method for which it has provided validation.
Detailed scope
Agri-food / Other foods, Beverages (excluding drinking water) and Sweet products / Physico-chemical analyses
Physico-chemical analyses for the determination of composition, quality and technological criteria, and nutritional labelling in human food - LAB GTA 25/60-118
ITEM CHARACTERISTIC MEASURED OR SOUGHT PRINCIPLE OF THE METHOD REFERENCE OF
THE METHOD
Foodstuff :
Fruit and vegetables
Compound foods
Non-alcoholic beverages
Dried fruit, dried tomatoes, mustard
Determination of sulphite content
Monier-Williams optimized method: Distillation Titrimetry
In-house method MOC3/164
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
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INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
Food Microbiology Scope of accreditation N°1-6066
Scope FLEX1
Agri-food / Other foods / Microbiological analyses
Microbiological analysis of food products and environment - LAB GTA 59
ITEM CHARACTERISTIC MEASURED OR SOUGHT PRINCIPLE OF THE METHOD REFERENCE OF
THE METHOD
Products intended for human consumption, feed and environmental samples
Micro-organisms Colony counts at 30°C by deep seeding technique NF EN ISO 4833-
1
Products intended for human consumption, feed and environmental samples
Micro-organisms Colony counts at 30°C using surface seeding technique NF EN ISO 4833-
2
Products intended for human consumption or animal feed, environmental samples in the agri-food sector
Entero-bacteriaceae
Colony counts at 37°C (or 30°C)
NF ISO 21528-2
All food and feed products and samples of the production plant working environment
Entero-bacteriaceae Colony counts at 37°C
BRD 07/24-11/13
Products intended for human consumption or animal feed, environmental samples in the agri-food sector
Coliforms
Colony counts at 30°C (or 37°C)
NF ISO 4832
Products intended for human consumption or animal nutrition Thermotolerant coliforms
Colony counts at 44°C NF V08-060
Products intended for human consumption or animal nutrition
Escherichia coli - β-glucuronidase positive
Colony counts at 44°C NF ISO 16649-2
All human food products
Coliforms
Colony counts at 37°C by chromogenic medium RAPID E.coli 2
BRD 07/08-12/04
All food and feed products Escherichia coli
-β-glucuronidase positive
Colony counts at 37°C by chromogenic medium RAPID E. coli 2
BRD 07/07-12/04
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
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INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
ITEM CHARACTERISTIC MEASURED OR SOUGHT PRINCIPLE OF THE METHOD REFERENCE OF
THE METHOD
All food and feed products Enterobacteriaceae Colony counts at 37°C by chromogenic medium REBECCA™ + EB
AES 10/07-01/08
All food and feed products Escherichia coli - β - glucuronidase positive
Colony counts at 37°C by chromogenic medium REBECCA™ BASE or REBECCA™+ EB
AES 10/06-01/08
Products intended for human consumption or animal nutrition
Escherichia coli O157 Enrichment Separation / Concentration Isolation - Confirmation
NF EN ISO 16654
Products intended for human consumption or animal nutrition
Positive coagulase staphylococcus Colony counts at 37°C by chromogenic agar medium Baird Parker
NF EN ISO 6888-1
Products intended for human consumption or animal nutrition
Positive coagulase staphylococcus Aerobic colony counts at 35°C or 37°C using rabbit plasma and Fibrinogen agar media.
NF EN ISO 6888-2
Human food products and environmental sampling
Positive coagulase staphylococcus Colony counts at 37°C by specific media RAPID' Staph and confirmation
BRD 07/09-02/05
Products intended for human consumption or animal nutrition
Sulfitore-reducing bacteria Anaerobic colony counts at 46°C in anaerobic conditions
NF V08-061
Products intended for human consumption or animal feed, environmental samples in the agri-food sector
Anaerobic sulfitore-reducing bacteria
Colony counts at 37°C
NF ISO 15213
Products intended for human consumption or animal feed, environmental samples in the agri-food sector
Clostridium perfringens Colony counts at 37°C and confirmation
NF EN ISO 7937
Products intended for human consumption or animal feed, environmental samples in the agri-food sector
Presumptive Bacillus cereus Colony counts at 30°C
NF EN ISO 7932
Phytocontrol Analytics France, Parc Scientifique Georges Besse II – 180 rue Philippe Maupas – 30035 Nîmes - France Tél. +33 (0)4 34 14 70 00 - Fax. +33 (0)4 66 23 99 95 - www.phytocontrol.com - [email protected] SAS au capital de 1.000.000 euros - RCS Nîmes 490 024 049 - TVA intra FR 08 490 024 049 - APE 7120B
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INTERNAL TECHNICAL ANNEX EA3.b-1 - Version 24 – 18/06/2018
ITEM CHARACTERISTIC MEASURED OR SOUGHT PRINCIPLE OF THE METHOD REFERENCE OF
THE METHOD
All food and feed products Presumptive Bacillus cereus Enumeration at 30°C using Compass® Bacillus cereus Agar chromogenic medium
BKR 23/06-02/10
Products intended for human consumption or animal nutrition
Mesophilic lactic acid bacteria Colony counts at 30°C NF ISO 15214
Meat and meat products Pseudomonas spp Colony counts at 25°C NF EN ISO 13720 Products intended for human consumption or animal nutrition
Yeasts and moulds Colony counts at 25°C NF V08-059
Products intended for human consumption or animal nutrition
Yeasts and moulds developing on a medium with low water activity
Colony counts at 25°C NF V08-036
Products intended for human consumption or animal nutrition
Listeria monocytogenes Colony counts at 37°C and confirmation
NF EN ISO 11290-2
All feeding products and environmental samples
Listeria monocytogenes et
Listeria spp
Enumeration at 37°C by chromogenic medium ALOA COUNT™
AES 10/05-09/06
Milk powders, infant milk powder Cronobacter spp Search Isolation / Identification and Confirmation
NF EN ISO 6579-1
Products intended for human consumption or animal feed, environmental samples in the agri-food sector
Salmonella spp. of which Salmonella Typhi and Salmonella
Paratyphi
Search Isolation / Identification and Confirmation BRD 07/11-12/05
All food and feed products and samples from the production environment
Salmonella Search by Hromogenic Environment RAPID Salmonella
NF EN ISO 11290-1
All food and feed products Listeria monocytogenes Search Isolation / Identification and Confirmation
AES 10/03-09/00
Flexible Scope FLEX1: The laboratory is accredited to perform the tests according to the method described in the referential referred to in the version in force at the time of the evaluation. # Accreditation made compulsory under the French regulatory framework specified by the text cited in the document. Cofrac LAB INF 99 available at www.cofrac.fr.