,,-OHM*,

UNITED STATES ENVIRONMENTAL PROTECTION AGENCY

REGION 725 FUNSTON ROAD

KANSAS CITY, KANSAS 66115

Date:AUG 2 0 !?Gi

kzceived

AUG 2 H l9u,

Reml section

MEMORANDUM

FROM:

SUBJECT:

Chief, Laboratory Branch, ENSV

Robert MorbyChief, Superfund Branch, WSTM

TO:

ATTN:

Attached is the data transmittal for the above referenced

Complete data transmittal (completes transmittal of

--- ------------------ ) . If you have have any questions or

comments, please contact Dee Simmons at 551-5129.

Attachments

cc: Data Files

site. This should

NOTE: Please see Mary Gerken, SPFD-WSTM, if you want an electronic copy of the data.

2041433

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ENVIRONMENTAL SERVICES ASSISTANCE TEAM — Zone II

ICF Technology, Inc.

ManTech Environmental Technology, Inc

The Bionetics Corp.

ManTech Env. Tech, Inc. 25 Funston Road Kansas City, KS 66115 (913) 236-3881

ESAT Region VII

TO: Barry EvansData Review Task Monitor

THRU: Harold Brown, Ph.D.ESAT Deputy Project Officer, EPA

FROM: David J. HickeyESAT Data Reviewer

THRU: Ronald A. RossESAT Team Manager

DATE: August 1, 1991SUBJECT: Review of organic data for Tenth Street Site

TID# 07-9103-535 ASSIGNMENT# 890 ICF ACCT# 26-535-02 NSI S.O.# 1073-535ESAT Document No. ESAT-VII-535-0145

These data were reviewed primarily according to the "LaboratoryData Validation Functional Guidelines for Evaluating Organic

•Analyses," February 1988 revision with changes given in the Region VII Organic Data Review Training Manual and EPA memorandums.

The following comments and attached data sheets are a result of the ESAT review, according to EPA policies, of the following data from the contract laboratory.

CASE NO.: 6403GSITE: Tenth Street SiteREVIEWER: David J. Hickey

LABORATORY: WANTECMETHOD NO.: 3317.1AEPA ACTIVITY NO.: CS1CS MATRIX: SOIL

VOLATILES BY TCLP (SOIL)

TOTAL METALS BY TCLP (SOIL)

SMO Sample No. EPA Sample No. SMO Sample No. EPA Sample No.

6403G-001 6403G-002 6403G-003 64 03G-004 6403G-005 6403G-006 6403G-007

CS1CS001CS1CS002CS1CS003CS1CS004CS1CS004DCS1CS006CS1CS007

6403G-0086403G-0096403G-0106403G-0116403G-0126403G-0136403G-014

CS1CS001CS1CS002CS1CS003CS1CS004CS1CS004DCS1CS006CS1CS007

GENERAL

This data review assignment covers 14 SOIL samples analyzed for TCLP VOLATILES and TCLP Total Metals for SAS number 6403G. There was one field duplicate sample included with this assignment. There was 1 method blank for TCLP Volatiles, and two laboratory duplicates for TCLP Total Metals. The level of review for this package was 2.

1* Holding Times and Preservation

The samples were extracted within the specified holding time for both Volatiles and Total Metals.

2. QC/M8 Tuning

All relative ion abundances were within the established control limits.

3. Initial and Continuing Calibration

Volatiles: All criteria were within established controllimits.

Total Metals: All % recoveries were within established controllimits.

4. ICP Interference Check

Recoveries of solution AB analytes were within control limits.

5. Laboratory Control Standard

LCS results were within established control limits.

6. Internal Standard Response

Volatiles: All internal standard criteria were within controllimits.

7. ICP Serial Dilution

All results were within established control limits.

8. Blanks

Volatiles: No compounds of interest were detected in themethod blank.

Total Metals: No compounds of interest were detected in any ofthe blanks.

9. Surrogate Recovery

Volatiles: Standard recovery for 1,2-Dichloroethane-d4 wereouside (high) acceptable criteria in sample CS1CS006. The sample was not reanalyzed because the holding time had expired. No qualification was required, though, according to Regional policy.

10. Matrix Spike/Matrix Spike Duplicate Recovery

Volatiles: Matrix spike/matrix spike duplicate recoveries wereoutside (high) established control limits for two of the twenty compounds. No qualification of the samples was required, however, according to Regional policy.

Total Metals: All matrix spike recoveries were within controllimits. The narrative states, though, that spike recoveries for Barium were low and the RPD for Barium was very high. However, these alleged anomalies could not be confirmed.

11. Performance Evaluation Sample

No performance samples were included in this package.

12. Duplicates

Good agreement existed between the samples and their respective field and laboratory duplicates. In the Metals package, the first duplicate was analyzed for analytes by ICP only; the second for Mercury by cold vapor. The RPDs for all analytes were within control limits. However, it was found that the reported RPDs were not reproducible from results reported on the summary sheet. The reason for this conflict is unknown and, considering the level of review, was not investigated.

13. Compound Identification and Quantitation

Due to the requested review level, results listed on the summary forms were used for the review. With one exception, these results were not checked against the raw data for accuracy, and calculations were not verified. The exception being the calculations for laboratory duplicate RPDs were checked. All positive results found below the CRQL were raised to the CRQL according to Regional policy and coded U.

14. Summary

The laboratory was instructed to analyze the soil samples for TCLP Volatiles and TCLP Total Metals according to the SAS. QC outliers did not result in any data qualification since sample results were below the CRQL. All laboratory blanks were free of contamination. Several QC outliers were noted in both packages, but no qualification of sample data was necessary or required according to Regional policy.

ANALYSIS REQUEST REPORT VALIDATED DATA

» ,FOR ACTIVITY: CS1CS

S p F D 08/20/91 16:31:55 ALL REAL SAMPLES AND FIELD Q.C.

* FINAL REPORTFY: 91 ACTIVITY: CS1CS DESCRIPTION: TENTH STREET SITE LOCATION: COLUMBUS NEBRASKA

STATUS: ACTIVE TYPE: SAMPLING - CONTRACT LAB ANALYSIS PROJECT: A33

LABO DUE DATE IS 8/13/91. REPORT DUE DATE IS 8/27/91.

INSPECTION DATE: 6/13/91 ALL SAMPLES RECEIVED DATE: 06/14/91

ALL DATA APPROVED BY LABO DATE: 08/20/91 FINAL REPORT TRANSMITTED DATE: 08/20/91

EXPECTED LABO TURNAROUND TIME IS 60 DAYS EXPECTED REPORT TURNAROUND TIME IS 75 DmYS

ACTUAL LABO TURNAROUND TIME IS 67 DAYS ACTUAL REPORT TURNAROUND TIME IS 68 DAYS

AIRS/SAMP. SAMPLE STORET BEG. BEG. END.NO. occ M DESCRIPTION STATUS CONT. CITY STATE L0C NO DATE TIME DATE

001 S TENTH STREET SITE-DRUM SAMPLE DF-1 1 2 COLUMBUS NEBRASKA 06/13/91 / /002 s TENTH STREET SITE-DRUM SAMPLE DF-2 1 2 COLUMBUS NEBRASKA 06/13/91 / /003 s TENTH STREET SITE-DRUM SAMPLE DF-3 1 2 COLUMBUS NEBRASKA 06/13/91 / /004 s TENTH STREET SITE-DRUM SAMPLE S-1 1 2 COLUMBUS NEBRASKA 06/13/9V / /004 D s TENTH STREET SITE-DRUM SAMPLE S-1 1 2 COLUMBUS NEBRASKA 06/13/91 / /006 s TENTH STREET SITE-DRUM SAMPLE S-2 1 2 COLUMBUS NEBRASKA 06/13/91 / /007 s TENTH STREET SITE-DRUM SAMPLE S-3 1 2 COLUMBUS NEBRASKA 06/13/91 / /

END.TIME

TABLE OF CODES

SAMP. NO. = SAMPLE IDENTIFICATION NUMBER QCC = QUALITY CONTROL SAMPLE/AUDIT CODEM = MEDIA OF SAMPLE (A=AIR. T=TISSUE. H=HAZARDOUS

MATERIAL. S=SEDIMENT/SOIL, W=WATER)AIRS/STORET LOC. NO. = A SAMPLING SITE LOCATION

IDENTIFICATION NUMBER BEG. DATE = THE DATE SAMPLING WAS STARTEDBEG. TIME = THE TIME SAMPLING WAS STARTEDEND. DATE = THE DATE SAMPLING WAS ENDEDEND. TIME = THE TIME SAMPLING WAS STOPPEDA = RESERVEDB = RESERVEDPES = PESTICIDES BY CONTRACT

= DIOXINS/FURANS BY EPA E = EXPLOSIVES BY CONTRACTFLD = FIELD MEASUREMENTS BY EPAG = MINERALS & DISSOLVED MATERIALS BY EPA HER = HERBICIDES BY EPA I = ION CHROMATOGRAPHY ANALYSES BY EPA MC = METALS BY CONTRACT BNC = BASE NEUTRALS BY CONTRACT L = FISH PHYSICAL DATA BY EPA MET = METALS BY EPA N = FISH TISSUE PARAMETERS BY EPA VC = VOLATILES BY CONTRACT P = PESTICIDES BY EPAQ = FLASH POINT ANALYSES BY EPAR = RESERVEDBN = SEMIVOLATILE BY EPAT = CYANIDE PHENOL BY EPAU = RESERVEDVOA = VOLATILE ORGANICS BY EPA HC = HERBICIDES BY CONTRACT X = RESERVEDY = RESERVEDTRK = ACTIVITY TRACKING PARAMETERS BY EPA

STORET DETECTION IDENTIFIERS BlAMK = MO RFMARKSJ = DATA REPORTED BUT NOT VALID BY APPROVED QC PROCEDURES I = INVALID SAMPLE/DATA - VALUE NOT REPORTED U = LESS THAN (MEASUREMENT DETECTION LIMIT)M = DFTFCTFD BUT RELOW THE LEVEL FOR ACCURATE QUANTIFICATION 0 - PARAMEIER NOT ANALYZEDCONTRACTOR/ IN HOUSE / FIELD MEDIA GROUPS FIELD = » » * = AF.HF.SF.TF.WF.ZZCONTRACTOR = * = HA.HC.HJ,HK.HO,SC,SJ.SK.SO,SW,TC,TJ,

TK.TO.TW,WA.WC.WE.WJ.WK,WO,WW IN HOUSE = « = ALL OTHERS

VALIDATED DATA

QUALITY CONTROL AUDIT CODES A = TRUE VALUE FOR CALIBRATION STANDARD B = CONCENTRATION RESULTING FROM DUPLICATE LAB SPIKE C = MEASURED VALUE FOR CALIBRATION STANDARD D = MEASURED VALUE FOR FIELD DUPLICATEF = MEASURED VALUE FOR FIELD BLANKG = MEASURED VALUE FOR METHOD STANDARDH = TRUE VALUE FOR METHOD STANDARDK = CONCENTRATION RESULTING FROM DUPLICATE FIELD SPIKEL = MEASURED VALUE FOR LAB DUPLICATEM = MEASURED VALUE FOR LAB BLANKN = MEASURED VALUE FOR DUPLICATE FIELD SPIKEP = MEASURED VALUE FOR PERFORMANCE STANDARDR = CONCENTRATION RESULTING FROM LAB SPIKES = MEASURED VALUE FOR LAB SPIKET = TRUE VALUE OF PERFORMANCE STANDARDW = MEASURED VALUE FOR DUPLICATE LAB SPIKEY = MEASURED VALUE FOR FIELD SPIKEZ = CONCENTRATION RESULTING FROM FIELD SPIKE

MEDIA CODES A = AIRT = BIOLOGICAL (PLANT & ANIMAL) TISSUE H = HAZARDOUS MATERIALS/MAN MADE PRODUCTS S = SEDIMENT. SLUDGE 8. SOIL W = WATER

UNITSNA = NOT APPLICABLEPG = PICOGRAMS (1 X 10-12 GRAMS)NG = NANOGRAMS (1 X 10-9 GRAMS)UG = MICROGRAMS (1 X 10-6 GRAMS)MG = MILLIGRAMS (1 X 10-3 GRAMS)M3 = METER CUBED MPH = MILES PER HOURSCM = STANDARD (1 ATM, 25 C) CUBIC METER KG = KILOGRAML = LITERC = CENTIGRADE DEGREESSU = STANDARD (PH) UNITSH = NUMBERLB = POUNDSIN = INCHESM/F = MALE/FEMALEM2 = SQUARE METERID. = SPECIES IDENTIFICATIONGPM = GALLONS PER MINUTECFS = CUBIC FEET PER SECONDMGD = MILLION GALLONS PER DAY1000G= FLOW. 1000 GALLONS PER COMPOSITEUMHOS= CONDUCTIVITY UNITS (1/OHMS)NTU = TURBIDITY UNITSPC/L = PICO (1 X 10-12) CURRIES PER LITER MV = MILLIVOLT SQ FT= SQUARE FEET P/CM2= PICOGRAMS PER SQ. CENTIMETER U/CM2= MICROGRAMS PER SQ. CENTIMETER

ANALYSIS REQUEST DETAIL REPORT ACTIVITY: 1-CS1CS VALIDATED DATA

COMPOUND UNITS 001 002 003 004 004D

SM46 SILVER TCLP MG/L 5.0 U 5.0 u 5.0 U 5.0 U 5.0 U

SM47 ARSENIC TCLP MG/L 5.0 u 5.0 U 5.0 U 5.0 U 5.0 U

SM48 BARIUM TCLP MG/L 100 u 100 U 100 U 100 U 100 u

SM49 CADMIUM TCLP MG/L 1.0 u 1.0 U 1 .0 U 1.0 u 1 .0 u

SM50 CHROMIUM TCLP MG/L 5.0 u 5.0 U 5.0 U 5.0 u 5.0 u

SM51 LEAD TCLP MG/L 5.0 u 5.0 U 5.0 U 5.0 u 5.0 u

SM52 SELENIUM TCLP MG/L 1.0 u 1.0 U 1.0 U 1 .0 u 1 .0 u

SM53 MERCURY TCLP MG/L 0.2 u 0.2 u 0.2 U 0.2 u 0.2 u

SV01 VINYL CHLORIDE. TCLP MG/L 0.20 u 0.20 u 0.20 U 0.20 u 0.20 u

SV02 CHLOROFORM. TCLP MG/L 6.0 u 6.0 u 6.0 u 6.0 u 6.0 u

SV23 1,2-DICHLOROETHANE, TCLP MG/L 0.50 u 0.50 u 0.50 u 0.50 u 0.50 u

SV38 CARBON TETRACHLORIDE. TCLP MG/L 0.50 u 0.50 u 0.50 u 0.50 u 0.50 u

SV39 BENZENE, TCLP MG/L 0.50 u 0.50 u 0.50 u 0.50 u 0.50 u

SV40 CHLOROBENZENE. TCLP MG/L 100 u TOO u 100 u 100 u 100 u

SV50 1.1-DICHLOROETHYLENE. TCLP MG/L 0.70 u 0.70 u 0. 70 u 0. 70 u 0.70 u

SV51 METHYL ETHYL KETONE. TCLP MG/L 200 u 200 u 200 u 200 u 200 u

SV52 TETRACHLOROETHYLENE. TCLP MG/L 0.70 u 0.70 u 0.70 u 0. 70 u 0.70 u

SV53 TRICHLOROETHYLENE. TCLP MG/L 0.50 u 0.50 u 0.50 u 0.50 u 0.50 u

ZZOl SAMPLE NUMBER NA 001 002 003 004 004

7702 ACTIVITY CODE NA C.S1C.S CS1CS CS1CS CS1CS C.S10S

I

COMPOUND

ANALYSIS REQUEST DETAIL REPORT ACTIVITY:

UNITS 006 007

1-CS1CS VALIDATED DATA

SM46 SILVER TCLP

SM47 ARSENIC TCLP

MG/L

MG/L

5.0

5.0

U

U

5.0

5.0

,U

U--------------------- ----------—

SM48 BARIUM TCLP MG/L 100 U 100 U

SM49 CADMIUM TCLP MG/L 1 .0 u 1 .0 U.

SM50 CHROMIUM TCLP MG/L 5.0 u 5.0 u

SM51 LEAD TCLP MG/L 5.0 u 5.0 u.

SM52 SELENIUM TCLP MG/L 1 .0 u 1.0 u_____

MG/L 0.2 u 0.2 u

SV01 VINYL CHLORIDE. TCLP MG/L 0.20 u 0.20 uV __________ „__

SV02 CHLOROFORM. TCLP MG/L 6.0 u 6.0 u_____________

SV23 1.2-DICHLOROETHANE. TCLP MG/L 0.50 u 0.50 u.

SV38 CARBON TETRACHLORIDE. TCLP MG/L 0.50 u 0.50 u___ ___ _________

0.50 u 0.50 u

SV40 CHLOROBENZENE. TCLP MG/L 100 u 100 u_____________

<;V50 1.1-DICHLOROETHYLENE TCLP MG/L 0.70 u 0.70 u____________

SV51 METHYL ETHYL KETONE. TCLP MG/L 200 u 200 u_____________

SV52 TETRACHLOROETHYLENE, TCLP MG/L 0. 70 u 0.70 u_____________

SV53 TRICHLOROETHYLENE, TCLP MG/L 0.50 u 0.50 u_____ _______

ZZ01 SAMPLE NUMBER NA 006 007___________

7702 ACTIVITY CODE NA CS1CS CS1CS____________________________ ,

ACTIVITY CS1CS TENTH STREET SITE

THE PROJECT LEADER SHOULD CIRCLE ONE - STORET. AIRS, OR ARCHIVE.

CIRCLE ONE: STORET AIRS ARCHIVE

DATA APPROVED BY LABO FOR TRANSMISSION TO PROJECT LEADER ON 08/20/91 16:30:12 BY