lab trial with liquid microtracer step 5. appearance of liquid microtracer retrieved from the feed...
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Lab Trial with liquid Microtracer
Step 5. Appearance of liquid Microtracer retrieved from the feed and collec-ted on the bottom of plastic container (Nd-magnet is attached underneath)
Lab Trial with liquid Microtracer
Step 6. Transfer of dispersion of collected liquid Microtracer in aqueous surfactant solution from the plastic container, to the beaker with ABC-coated Nd magnet on the bottom
Lab Trial with liquid Microtracer
Step 7.Transfer of ABC-coated Nd-magnet covered with liquid Microtracer from the beaker
Lab Trial with liquid Microtracer
Step 8. Transfer of ABC- coated Nd-magnet with attached liquid mic-rotracer into vial for treatment with hydrochloric acid solution
Lab Trial with liquid Microtracer
Step 9.Analytical determination of Co(2+) concentration in retrieved portion of liquid tracer
Stages: 1. Dissolving attached liquid tracer in HCl ; 2. Addition diethylamine and ammonium thiocyanate in DMSO;
3. Determination of optical density at 667 nm
Calibration curve for determination of Co(2+) in Liquid Microtracer
R2 = 0.9985
0
0.1
0.2
0.3
0.4
0 50 100
Concentration of Co (2+) , mg/1000 ml
Ab
so
rba
nc
e a
t 6
67
n
m
Absorbance spectrum of analysed sample
0
0.05
0.1
0.15
0.2
550 600 650 700 750
Wavelength, nm
Op
tical
den
sit
y
Field trial with liquid Microtracer
Validating mixing for liquid feed (500 kg Trial with liquid pig feed manufacturer –Micro Tracers Services, Europe)
Field trial with liquid Microtracer
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