lab trial with liquid microtracer step 5. appearance of liquid microtracer retrieved from the feed...

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Lab Trial with liquid Microtracer Step 5. Appearance of liquid Microtracer retrieved from the feed and collec-ted on the bottom of plastic container (Nd-magnet is attached underneath)

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Page 1: Lab Trial with liquid Microtracer Step 5. Appearance of liquid Microtracer retrieved from the feed and collec-ted on the bottom of plastic container (Nd-magnet

Lab Trial with liquid Microtracer

Step 5. Appearance of liquid Microtracer retrieved from the feed and collec-ted on the bottom of plastic container (Nd-magnet is attached underneath)

Page 2: Lab Trial with liquid Microtracer Step 5. Appearance of liquid Microtracer retrieved from the feed and collec-ted on the bottom of plastic container (Nd-magnet

Lab Trial with liquid Microtracer

Step 6. Transfer of dispersion of collected liquid Microtracer in aqueous surfactant solution from the plastic container, to the beaker with ABC-coated Nd magnet on the bottom

Page 3: Lab Trial with liquid Microtracer Step 5. Appearance of liquid Microtracer retrieved from the feed and collec-ted on the bottom of plastic container (Nd-magnet

Lab Trial with liquid Microtracer

Step 7.Transfer of ABC-coated Nd-magnet covered with liquid Microtracer from the beaker

Page 4: Lab Trial with liquid Microtracer Step 5. Appearance of liquid Microtracer retrieved from the feed and collec-ted on the bottom of plastic container (Nd-magnet

Lab Trial with liquid Microtracer

Step 8. Transfer of ABC- coated Nd-magnet with attached liquid mic-rotracer into vial for treatment with hydrochloric acid solution

Page 5: Lab Trial with liquid Microtracer Step 5. Appearance of liquid Microtracer retrieved from the feed and collec-ted on the bottom of plastic container (Nd-magnet

Lab Trial with liquid Microtracer

Step 9.Analytical determination of Co(2+) concentration in retrieved portion of liquid tracer

Stages: 1. Dissolving attached liquid tracer in HCl ; 2. Addition diethylamine and ammonium thiocyanate in DMSO;

3. Determination of optical density at 667 nm

Calibration curve for determination of Co(2+) in Liquid Microtracer

R2 = 0.9985

0

0.1

0.2

0.3

0.4

0 50 100

Concentration of Co (2+) , mg/1000 ml

Ab

so

rba

nc

e a

t 6

67

n

m

Absorbance spectrum of analysed sample

0

0.05

0.1

0.15

0.2

550 600 650 700 750

Wavelength, nm

Op

tical

den

sit

y

Page 6: Lab Trial with liquid Microtracer Step 5. Appearance of liquid Microtracer retrieved from the feed and collec-ted on the bottom of plastic container (Nd-magnet

Field trial with liquid Microtracer

Validating mixing for liquid feed (500 kg Trial with liquid pig feed manufacturer –Micro Tracers Services, Europe)

Page 7: Lab Trial with liquid Microtracer Step 5. Appearance of liquid Microtracer retrieved from the feed and collec-ted on the bottom of plastic container (Nd-magnet

Field trial with liquid Microtracer

Page 8: Lab Trial with liquid Microtracer Step 5. Appearance of liquid Microtracer retrieved from the feed and collec-ted on the bottom of plastic container (Nd-magnet

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Page 9: Lab Trial with liquid Microtracer Step 5. Appearance of liquid Microtracer retrieved from the feed and collec-ted on the bottom of plastic container (Nd-magnet

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