laboratory report for samples received 05/11/2006 · 2020-07-03 · laboratory report chris nitchie...
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Laboratory Report
Chris Nitchie PO Number: None
Rizzo Associates LabiD: 10338
One Grant Street Date Received: 5/11/06
Framingham, MA 01701
Project: 1272420016
Attached please find results for the analysis of the samples received on the date referenced above.
Unless otherwise noted in the attached report, the analyses performed met the requirements of Resource Laboratories, LLC Quality Assurance Plan. The Standard Operating Procedures (SOP) are based upon USEPA SW-846, USEPA Methods for Chemical Analysis of Water and Wastewater, Standard Methods for the Examination of Water and Wastewater and other recognized methodologies. The results contained in this report pertain only to the samples as indicated on the chain of custody.
Resource Laboratories, LLC maintains certification with the agencies listed below.
We appreciate the opportunity to provide laboratory services. If you have any questions regarding the enclosed report, please contact the laboratory and we will be glad to assist you.
Sincerely, Resource. Laboratories, LLC
fl-1 t-a' , klA ..L-<
Susan Sylvester Date
Principal, General Manager
Total number of pages
New Hampshire Maine
Resource Laboratories, LLC Certifications
1732 NH903
Massachusetts M-NH902
124 Heritage Avenue #1 0 Portsmouth NH 03801 Voice: 603-436-2001 Fax: 603-430-2100
www. reslabs.com
Lab Number: Sample Designation: Date Sampled: Date Analyzed: Matrix: Instrument Dilution Factor: Analyst:
VOLATILE ORGANICS SW846 Method 50308/82608
dichlorodifluoromethane chloromethane vinyl chloride bromomethane chloroethane trichlorofluoromethane diethyl ether acetone 1,1-dichloroethene methylene chloride carbon disulfide methyl t-butyl ether (MTBE) trans-1 ,2-dichloroethene 1,1-dichloroethane 2-butanone (MEK) 2,2-dichloropropane cis-1 ,2-dichloroethene chloroform bromochloromethane tetrahydrofuran (THF) 1,1, 1-trichloroethane 1,1-dichloropropene carbon tetrachloride 1 ,2-dichloroethane benzene trichloroethene 1 ,2-dichloropropane bromodichloromethane dibromomethane 4-methyl-2-pentanone (MIBK) cis-1 ,3-dichloropropene toluene trans-1 ,3-dichloropropene 2-hexanone
SURROGATE STANDARDS
dibromofluoromethane toluene-DB 4-bromofluorobenzene
10338-01 B-5D-I 5/9/06 5/12/06 Water 1 LMM
Concentration
ug/L u u u u u u u u 2 u u u u
240 u u u u u
22 u u u u u u u u u u u u u u
Recovery (%)
109 104 101
Concentration Quantitation Limit
ug/L ug/L u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 5 u 2
Quantitation Limit
ug/L 2 2 2 2 2 2
10 10
1 5 2 2 2 2
10 2 2 2 2
10 2 2 2 2 2 2 2 2 2
10 2 2 2
10
Acceptance Limits
(%) 78-114
88-110 86-115
1,1 ,2-trichloroethane 1 ,3-dichloropropane tetrachloroethene dibromochloromethane 1 ,2-dibromoethane chlorobenzene 1,1, 1 ,2-tetrachloroethane ethylbenzene m&p-xylenes a-xylene styrene bromoform isopropylbenzene 1,1 ,2,2-tetrachloroethane 1 ,2,3-trichloropropane n-propylbenzene bromo benzene 1 ,3,5-trimethylbenzene 2-chlorotoluene 4-chlorotoluene tert-butylbenzene 1 ,2,4-trimethylbenzene sec-butylbenzene 1 ,3-dichlorobenzene 4-isopropyltoluene 1 A-dichlorobenzene 1 ,2-dichlorobenzene n-butylbenzene 1 ,2-dibromo-3-chloropropane 1 ,2,4-trichlorobenzene hexachlorobutadiene naphthalene 1 ,2,3-trichlorobenzene
U =Below quantitation limit
RL Resource Laboratories, LLC
Lab Number: Sample Designation: Date Sampled: Date Analyzed: Matrix: Instrument Dilution Factor: Analyst:
VOLATILE ORGANICS SW846 Method 50308/82608
dichlorodifluoromethane chloromethane vinyl chloride bromo methane chloroethane trichlorofluoromethane diethyl ether acetone 1,1-dichloroethene methylene chloride carbon disulfide methyl t-butyl ether (MTBE) trans-1 ,2-dichloroethene 1, 1-dichloroethane 2-butanone (MEK) 2,2-dichloropropane cis-1 ,2-dichloroethene chloroform bromochloromethane tetrahydrofuran (THF) 1,1, 1-trichloroethane 1,1-dichloropropene carbon tetrachloride 1 ,2-dichloroethane benzene trichloroethene 1 ,2-dichloropropane bromodichloromethane dibromomethane 4-methyl-2-pentanone {MIBK) cis-1 ,3-dichloropropene toluene trans-1 ,3-dichloropropene 2-hexanone
SURROGATE STANDARDS
dibromofluoromethane
toluene-DB
4-bromofluorobenzene
10338-02 B-6A-D 5/9/06 5/15/06 Water 10 LMM
Concentration
ug/L u u
250 u u u u u
510 u u u
56 5200
u u
3500 u u u u u u u u
69 u u u
470 u
27 u u
Recovery
(%)
106
104
97
Concentration Quantitation Limit
ug/L ug/L u 20 u 20 u 20 u 20 u 20 u 20 u 20
1700 20 940 20
u 20 u 20 u 20 u 20 u 20 u 20 u 20 u 20
u 20 u 20 u 20 u 20 u 20 u 20 u 20 u 20 u 20 u 20 u 20 u 20 u 20 u 20 u 50 u 20
Quantitation Limit
ug/L 20 20 20 20 20 20
100 100
10 50 20 20 20 20
100 20 20 20 20
100 20 20 20 20 20 20 20 20 20
100 20 20 20
100
Acceptance Limits
(%)
78-114
88-110
86-115
1,1 ,2-trichloroethane 1 ,3-dichloropropane tetrachloroethene dibromochloromethane 1 ,2-dibromoethane chlorobenzene 1,1, 1 ,2-tetrachloroethane ethylbenzene m&p-xylenes a-xylene styrene bromoform isopropyl benzene 1,1 ,2,2-tetrachloroethane 1 ,2,3-trichloropropane n-propylbenzene bromo benzene 1 ,3,5-trimethylbenzene 2-chlorotoluene 4-chlorotoluene tert-butylbenzene 1 ,2,4-trimethylbenzene sec-butylbenzene 1 ,3-dichlorobenzene 4-isopropyltoluene 1 A-dichlorobenzene 1 ,2-dichlorobenzene n-butylbenzene 1 ,2-dibromo-3-chloropropane 1 ,2,4-trichlorobenzene hexachlorobutadiene naphthalene 1 ,2,3-trichlorobenzene
U = Below quantitation limit
RL Resource Laboratories, LLC
Lab Number: Sample Designation: Date Sampled: Date Analyzed: Matrix: Instrument Dilution Factor: Analyst:
VOLATILE ORGANICS SW846 Method 50308/82608
dichlorodifluoromethane chloromethane vinyl chloride bromomethane chloroethane trichlorofluoromethane diethyl ether acetone 1,1-dichloroethene methylene chloride carbon disulfide methyl t-butyl ether (MTBE) trans-1 ,2-dichloroethene 1,1-dichloroethane 2-butanone (MEK) 2,2-dichloropropane cis-1 ,2-dichloroethene chloroform bromochloromethane tetrahydrofuran (THF) 1,1, 1-trichloroethane 1,1-dichloropropene carbon tetrachloride 1 ,2-dichloroethane benzene trichloroethene 1 ,2-dichloropropane bromodichloromethane dibromomethane 4-methyl-2-pentanone (MIBK) cis-1 ,3-dichloropropene toluene trans-1 ,3-dichloropropene 2-hexanone
SURROGATE STANDARDS
dibromofluoromethane toluene-D8
4-bromofluorobenzene
10338-03 B-8A-D 5/9/06 5/12/06 Water 1 LMM
Concentration
ug/L u u 3 u u u u u
110 u u u u
430 u u u u u
59 u u u u u
13 u u u
330 u u u u
Recovery
(%)
108 102 99
Concentration Quantitation Limit
ug/L ug/L u 2 u 2 u 2 u 2 u 2 u 2 u 2 6 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 5 u 2
Quantitation Limit
ug/L 2 2 2 2 2 2
10 10
1 5 2 2 2 2
10 2 2 2 2
10 2 2 2 2 2 2 2 2 2
10 2 2 2
10
Acceptance Limits (%)
78-114 88-110
86-115
1,1 ,2-trichloroethane 1 ,3-dichloropropane tetrachloroethene dibromochloromethane 1 ,2-dibromoethane chlorobenzene 1,1, 1 ,2-tetrachloroethane ethylbenzene m&p-xylenes a-xylene styrene bromoform isopropylbenzene 1,1 ,2,2-tetrachloroethane 1 ,2,3-trichloropropane n-propylbenzene bromo benzene 1 ,3,5-trimethylbenzene 2-chlorotoluene 4-chlorotoluene tert-butylbenzene 1 ,2,4-trimethylbenzene sec-butyl benzene 1 ,3-dichlorobenzene 4-isopropyltoluene 1 A-dichlorobenzene 1 ,2-dichlorobenzene n-butylbenzene 1 ,2-dibromo-3-chloropropane 1 ,2,4-trichlorobenzene hexachlorobutadiene naphthalene 1 ,2,3-trichlorobenzene
U = Below quantitation limit
RL Resource Laboratories, LLC
Lab Number: 10338-04 Sample Designation: B-9A-I Date Sampled: 5/9/06 Date Analyzed: 5/15/06 Matrix: Water Instrument Dilution Factor: 5 Analyst: LMM
VOLATILE ORGANICS SW 846 Method 50308/82608
Concentration Quantitation Limit Concentration Quantitation Limit
ug/L ug/L ug/L ug/L dichlorodifluoromethane u 10 1,1 ,2-trichloroethane u 10 chloromethane u 10 1 ,3-dichloropropane u 10 vinyl chloride u 10 tetrachloroethene u 10 bromomethane u 10 dibromochloromethane u 10 chloroethane 370 10 1 ,2-dibromoethane u 10 trichlorofluoromethane u 10 chlorobenzene u 10 diethyl ether u 50 1,1, 1 ,2-tetrachloroethane u 10 acetone 1300 50 ethyl benzene 40 10 1,1-dichloroethene u 5 m&p-xylenes 45 10 methylene chloride u 30 a-xylene 19 10 carbon disulfide 15 10 styrene u 10 methyl t-butyl ether (MTBE) u 10 bromoform u 10 trans-1 ,2-dichloroethene u 10 isopropylbenzene u 10 1,1-dichloroethane 670 10 1,1 ,2,2-tetrachloroethane u 10 2-butanone (MEK) 1100 50 1 ,2,3-trichloropropane u 10 2,2-dichloropropane u 10 n-propylbenzene u 10 cis-1 ,2-dichloroethene 31 10 bromo benzene u 10 chloroform u 10 1 ,3,5-trimethylbenzene u 10 bromochloromethane u 10 2-chlorotoluene u 10 tetrahydrofuran (THF) u 50 4-chlorotoluene u 10 1,1, 1-trichloroethane u 10 tert-butylbenzene u 10 1 ,1-dichloropropene u 10 1 ,2,4-trimethylbenzene u 10 carbon tetrachloride u 10 sec-butyl benzene u 10 1 ,2-dichloroethane u 10 1 ,3-dichlorobenzene u 10 benzene u 10 4-isopropyltoluene u 10 trichloroethene 18 10 1 A-dichlorobenzene u 10 1 ,2-dichloropropane u 10 1 ,2-dichlorobenzene u 10 bromodichloromethane u 10 n-butylbenzene u 10 dibromomethane u 10 1 ,2-dibromo-3-chloropropane u 10 4-methyl-2-pentanone (MIBK) 130 50 1 ,2,4-trichlorobenzene u 10 cis-1 ,3-dichloropropene u 10 hexachlorobutadiene u 10 toluene 68 10 naphthalene u 30 trans-1 ,3-dichloropropene u 10 1 ,2,3-trichlorobenzene u 10 2-hexanone u 50
SURROGATE STANDARDS Recovery Acceptance Limits
(%) (%) dibromofluoromethane 107 78-114 toluene-DB 102 88-110 4-bromofluorobenzene 99 86-115
Note: The sample pH was greater than 2, indicating inadequate preservation. U = Below quantitation limit
RL Resource Laboratories, LLC
Lab Number: Sample Designation: Date Sampled: Date Analyzed: Matrix: Instrument Dilution Factor: Analyst:
VOLATILE ORGANICS SW846 Method 50308/82608
dichlorodifluoromethane chloromethane vinyl chloride bromo methane chloroethane trichlorofluoromethane diethyl ether acetone 1, 1-dichloroethene methylene chloride carbon disulfide methyl t-butyl ether (MTBE) trans-1,2-dichloroethene 1,1-dichloroethane 2-butanone (MEK) 2,2-dichloropropane cis-1,2-dichloroethene chloroform bromochloromethane tetrahydrofuran (THF) 1, 1, 1-trichloroethane 1,1-dichloropropene carbon tetrachloride 1,2-dichloroethane benzene trichloroethene 1,2-dichloropropane bromodichloromethane dibromomethane 4-methyl-2-pentanone (MIBK) cis-1,3-dichloropropene toluene trans-1,3-dichloropropene 2-hexanone
SURROGATE STANDARDS
dibromofluoromethane
toluene-DB
4-bromofluorobenzene
10338-05 B-128-1 5/9/06 5/15/06 Water 5 LMM
Concentration
ug/L
u u
52 u
190 u u
63 270
u u u
14 2900
120 u
830 u u
51 u u u u u
36 u u u
310 u
72 u u
Recovery
(%)
106
103
99
Quantitation Limit
ug/L
10 1,1,2-trichloroethane
10 1,3-dichloropropane
10 tetrachloroethene 10 dibromochloromethane 10 1,2-dibromoethane 10 chlorobenzene 50 1,1,1,2-tetrachloroethane 50 ethyl benzene
5 m&p-xylenes 30 a-xylene 10 styrene 10 bromoform 10 isopropyl benzene
10 1, 1,2,2-tetrachloroethane 50 1,2,3-trichloropropane 10 n-propylbenzene 10 bromo benzene 10 1,3,5-trimethylbenzene 10 2-chlorotoluene 50 4-chlorotoluene 10 tert-butylbenzene 10 1,2,4-trimethylbenzene 10 sec-butylbenzene . 10 1,3-dichlorobenzene 10 4-isopropyltoluene 10 1A-dichlorobenzene 10 1,2-dichlorobenzene
10 n-butylbenzene 10 1,2-dibromo-3-chloropropane 50 1,2,4-trichlorobenzene
10 hexachlorobutadiene 10 naphthalene 10 1,2,3-trichlorobenzene 50
Acceptance Limits
(%)
78-114
88-110
86-115
Concentration Quantitation Limit
ug/L ug/L
u 10
u 10
u 10 u 10 u 10
u 10
u 10 400 10 300 10 130 10
u 10
u 10
u 10 u 10
u 10
u 10
u 10 u 10
u 10
u 10
u 10 u 10
u 10
u 10
u 10
u 10
u 10
u 10
u 10
u 10 u 10
u 30 u 10
U = Below quantitation limit
RL Resource Laboratories, LLC
Lab Number: Sample Designation: Date Sampled: Date Analyzed: Matrix: Instrument Dilution Factor: Analyst:
VOLATILE ORGANICS SW846 Method 50308/82608
dichlorodifluoromethane chloromethane vinyl chloride bromomethane chloroethane trichlorofluoromethane diethyl ether acetone 1,1-dichloroethene methylene chloride carbon disulfide methyl t-butyl ether (MTBE) trans-1 ,2-dichloroethene 1,1-dichloroethane 2-butanone (MEK) 2,2-dichloropropane cis-1 ,2-dichloroethene chloroform bromochloromethane tetrahydrofuran (THF) 1,1, 1-trichloroethane 1,1-dichloropropene carbon tetrachloride 1 ,2-dichloroethane benzene trichloroethene 1 ,2-dichloropropane bromodichloromethane dibromomethane 4-methyl-2-pentanone {MIBK) cis-1 ,3-dichloropropene toluene trans-1 ,3-dichloropropene 2-hexanone
SURROGATE STANDARDS
dibromofluoromethane toluene-DB
4-bromofluorobenzene
10338-06 NBW-L 5/9/06 5/12/06 Water 1 LMM
Concentration
ug/L u u u u u u u
100 u u u u u u u u u u u u u u u u u u u u u u u u u u
Recovery
(%)
107 102
96
Quantitation Limit
ug/L 2 1,1 ,2-trichloroethane 2 1 ,3-dichloropropane 2 tetrachloroethene 2 dibromochloromethane 2 1 ,2-dibromoethane 2 chlorobenzene
10 1,1, 1 ,2-tetrachloroethane 10 ethyl benzene
1 m&p-xylenes 5 a-xylene 2 styrene 2 bromoform 2 isopropylbenzene . 2 1,1 ,2,2-tetrachloroethane
10 1 ,2,3-trichloropropane 2 n-propylbenzene 2 bromobenzene 2 1 ,3,5-trimethylbenzene 2 2-chlorotoluene
10 4-chlorotoluene 2 tert-butylbenzene 2 1 ,2,4-trimethylbenzene 2 sec-butyl benzene 2 1 ,3-dichlorobenzene 2 4-isopropyltoluene 2 1 A-dichlorobenzene 2 1 ,2-dichlorobenzene 2 n-butylbenzene 2 1 ,2-dibromo-3-chloropropane
10 1 ,2,4-trichlorobenzene 2 hexachlorobutadiene 2 naphthalene 2 1 ,2,3-trichlorobenzene
10
Acceptance Limits (%)
78-114
88-110 86-115
Concentration Quantitation Limit
ug/L ug/L u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 5 u 2
U = Below quantitation limit
RL Resource Laboratories, LLC
Lab Number: Sample Designation: Date Sampled: Date Analyzed: Matrix: Instrument Dilution Factor: Analyst:
VOLATILE ORGANICS SW 846 Method 50308/82608
dichlorodifluoromethane chloromethane vinyl chloride bromomethane chloroethane trichlorofluoromethane diethyl ether acetone 1,1-dichloroethene methylene chloride carbon disulfide methyl t-butyl ether (MTBE) trans-1 ,2-dichloroethene 1,1-dichloroethane 2-butanone (MEK) 2,2-dichloropropane cis-1 ,2-dichloroethene chloroform bromochloromethane tetrahydrofuran (THF) 1,1, 1-trichloroethane 1,1-dichloropropene carbon tetrachloride 1 ,2-dichloroethane benzene trichloroethene 1 ,2-dichloropropane bromodichloromethane dibromomethane 4-methyl-2-pentanone (MIBK) cis-1 ,3-dichloropropene toluene trans-1 ,3-dichloropropene 2-hexanone
SURROGATE STANDARDS
dibromofluoromethane toluene-DB
4-bromofluorobenzene
10338-07 NBW-U 5/9/06 5/12/06 Water 1 LMM
Concentration
ug/L u u u u u u u
290 u u u u u u u u u u u u u u u u u u u u u u u u u u
Recovery (%)
108 102
98
Concentration Quantitation Limit
ug/L ug/L u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 5 u 2
Quantitation Limit ug/L
2 2 2 2 2 2
10 10
1 5 2 2 2 2
10 2 2 2 2
10 2 2 2 2 2 2 2 2 2
10 2 2 2
10
Acceptance Limits (%)
78-114
88-110 86-115
1,1 ,2-trichloroethane 1 ,3-dichloropropane tetrachloroethene dibromochloromethane 1 ,2-dibromoethane' chlorobenzene 1,1, 1 ,2-tetrachloroethane ethyl benzene m&p-xylenes o-xylene styrene bromoform isopropylbenzene 1,1 ,2,2-tetrachloroethane 1 ,2,3-trichloropropane n-propylbenzene bromobenzene 1 ,3,5-trimethylbenzene 2-chlorotoluene 4-chlorotoluene tert-butylbenzene 1 ,2,4-trimethylbenzene sec-butyl benzene 1 ,3-dichlorobenzene 4-isopropyltoluene 1 A-dichlorobenzene 1 ,2-dichlorobenzene n-butylbenzene 1 ,2-dibromo-3-chloropropane 1 ,2,4-trichlorobenzene hexachlorobutadiene naphthalene 1 ,2,3-trichlorobenzene
U = Below quantitation limit
RL Resource Laboratories, LLC
Lab Number: Sample Designation: Date Sampled: Date Analyzed: Matrix: Instrument Dilution Factor: Analyst:
VOLATILE ORGANICS SW846 Method 50308/82608
dichlorodifluoromethane chloromethane vinyl chloride bromo methane chloroethane trichlorofluoromethane diethyl ether acetone 1,1-dichloroethene methylene chloride carbon disulfide methyl t-butyl ether (MTBE) trans-1 ,2-dichloroethene 1,1-dichloroethane 2-butanone (MEK) 2,2-dichloropropane cis-1 ,2-dichloroethene chloroform bromochloromethane tetrahydrofuran (THF) 1,1, 1-trichloroethane 1,1-dichloropropene carbon tetrachloride 1 ,2-dichloroethane benzene trichloroethene 1 ,2-dichloropropane bromodichloromethane dibromomethane 4-methyl-2-pentanone (MIBK) cis-1 ,3-dichloropropene toluene trans-1 ,3-dichloropropene 2-hexanone
SURROGATE STANDARDS
dibromofluoromethane
toluene-DB 4-bromofluorobenzene
10338-08 ODW-L 5/9/06 5/12/06 Water 1 LMM
Concentration ug/L
u u u u u u u
27 u u u u u u u u u u u u u u u u u u u u u u u u u u
Recovery
(%)
110 103
100
Quantitation Limit ug/L
2 1,1 ,2-trichloroethane 2 1 ,3-dichloropropane 2 tetrachloroethene 2 dibromochloromethane 2 1 ,2-dibromoethane· 2 chlorobenzene
10 1,1, 1 ,2-tetrachloroethane 10 ethyl benzene
m&p-xylenes 5 a-xylene 2 styrene 2 bromoform 2 isopropyl benzene 2 1,1 ,2,2-tetrachloroethane
10 1 ,2,3-trichloropropane 2 n-propylbenzene 2 bromo benzene 2 1 ,3,5-trimethylbenzene 2 2-chlorotoluene
10 4-chlorotoluene 2 tert-butylbenzene 2 1 ,2,4-trimethylbenzene 2 sec-butyl benzene 2 1 ,3-dichlorobenzene 2 4-isopropyltoluene 2 1 A-dichlorobenzene 2 1 ,2-dichlorobenzene 2 n-butylbenzene 2 1 ,2-dibromo-3-chloropropane
10 1 ,2,4-trichlorobenzene 2 hexachlorobutadiene 2 naphthalene 2 1 ,2,3-trichlorobenzene
10
Acceptance Limits (%)
78-114
88-110 86-115
Concentration Quantitation Limit
ug/L ug/L u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 5 u 2
U = Below quantitation limit
RL Resource Laboratories, LLC
Lab Number: Sample Designation: Date Sampled: Date Analyzed: Matrix: Instrument Dilution Factor: Analyst:
VOLATILE ORGANICS SW 846 Method 50308/82608
dichlorodifluoromethane chloromethane vinyl chloride bromomethane chloroethane trichlorofluoromethane diethyl ether acetone 1,1-dichloroethene methylene chloride carbon disulfide methyl t-butyl ether (MTBE) trans-1 ,2-dichloroethene 1,1-dichloroethane 2-butanone (MEK) 2,2-dichloropropane cis-1 ,2-dichloroethene chloroform bromochloromethane tetrahydrofuran (THF) 1,1, 1-trichloroethane 1,1-dichloropropene carbon tetrachloride 1 ,2-dichloroethane benzene trichloroethene 1 ,2-dichloropropane bromodichloromethane dibromomethane 4-methyl-2-pentanone (MIBK) cis-1 ,3-dichloropropene toluene trans-1 ,3-dichloropropene 2-hexanone
SURROGATE STANDARDS
dibromofluoromethane toluene-DB
4-bromofluorobenzene
10338-09 ODW-U 5/9/06 5/12/06 Water 1 LMM
Concentration
ug/L u u u u u u u
29 u u u u u
27 u u 4 u u u u u u u u u u u u u u u u u
Recovery
(%)
108 102
99
Concentration Quantitation Limit
ug/L ug/L u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 5 u 2
Quantitation Limit
ug/L 2 2 2 2 2 2
10 10
5 2 2 2 2
10 2 2 2 2
10 2 2 2 2 2 2 2 2 2
10 2 2 2
10
Acceptance Limits
(%)
78-114 88-110
86-115
1,1 ,2-trichloroethane 1 ,3-dichloropropane tetrachloroethene dibromochloromethane 1 ,2-dibromoethane chlorobenzene 1,1, 1 ,2-tetrachloroethane ethyl benzene m&p-xylenes o-xylene styrene bromoform isopropyl benzene 1,1 ,2,2-tetrachloroethane 1 ,2,3-trichloropropane n-propylbenzene bromo benzene 1 ,3,5-trimethylbenzene 2-chlorotoluene 4-chlorotoluene tert-butylbenzene 1 ,2,4-trimethylbenzene sec-butylbenzene 1 ,3-dichlorobenzene 4-isopropyltoluene 1 A-dichlorobenzene 1 ,2-dichlorobenzene n-butylbenzene 1 ,2-dibromo-3-chloropropane 1 ,2,4-trichlorobenzene hexachlorobutadiene naphthalene 1 ,2,3-trichlorobenzene
U = Below quantitation limit
RL Resource Laboratories, LLC
Lab Number: Sample Designation: Date Sampled: Date Analyzed: Matrix: Instrument Dilution Factor: Analyst:
VOLATILE ORGANICS SW846 Method 50308/82608
dichlorodifluoromethane chloromethane vinyl chloride bromo methane chloroethane trichlorofluoromethane diethyl ether acetone 1,1-dichloroethene methylene chloride carbon disulfide methyl t-butyl ether (MTBE) trans-1 ,2-dichloroethene 1,1-dichloroethane 2-butanone (MEK) 2,2-dichloropropane cis-1 ,2-dichloroethene chloroform bromochloromethane tetrahydrofuran (THF) 1,1, 1-trichloroethane 1,1-dichloropropene carbon tetrachloride 1 ,2-dichloroethane benzene trichloroethene 1 ,2-dichloropropane bromodichloromethane dibromomethane 4-methyl-2-pentanone (MIBK) cis-1 ,3-dichloropropene toluene trans-1 ,3-dichloropropene 2-hexanone
SURROGATE STANDARDS
dibromofluoromethane toluene-D8
4-bromofluorobenzene
10338-10 P-20 5/9/06 5/12/06 Water 1 LMM
Concentration
ug/L u u
63 u u u u u 2 u u u
180 55 u u
420 u u u u u u u u
210 u u u u u u u u
Recovery
(%) 108 104
102
Concentration Quantitation Limit
ug/L ug/L u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 5 u 2
Quantitation Limit
ug/L 2 2 2 2 2 2
10 10
5 2 2 2 2
10 2 2 2 2
10 2 2 2 2 2 2 2 2 2
10 2 2 2
10
Acceptance Limits
(%) 78-114 88-110
86-115
1,1 ,2-trichloroethane 1 ,3-dichloropropane tetrachloroethene dibromochloromethane 1 ,2-dibromoethane chlorobenzene 1,1, 1 ,2-tetrachloroethane ethyl benzene m&p-xylenes a-xylene styrene bromoform isopropyl benzene 1,1 ,2,2-tetrachloroethane 1 ,2,3-trichloropropane n-propylbenzene bromo benzene 1 ,3,5-trimethylbenzene 2-chlorotoluene 4-chlorotoluene tert-butylbenzene 1 ,2,4-trimethylbenzene sec-butyl benzene 1 ,3-dichlorobenzene 4-isopropyltoluene 1 A-dichlorobenzene 1 ,2-dichlorobenzene n-butylbenzene 1 ,2-dibromo-3-chloropropane 1 ,2,4-trichlorobenzene hexachlorobutadiene naphthalene 1 ,2,3-trichlorobenzene
U = Below quantitation limit
RL Resource Laboratories, LLC
Lab Number: Sample Designation: Date Sampled: Date Analyzed: Matrix: Instrument Dilution Factor: Analyst:
VOLATILE ORGANICS SW846 Method 50308/82608
dichlorodifluoromethane chloromethane vinyl chloride bromomethane chloroethane trichlorofluoromethane diethyl ether acetone 1,1-dichloroethene methylene chloride carbon disulfide methyl t-butyl ether (MTBE) trans-1 ,2-dichloroethene 1,1-dichloroethane 2-butanone (MEK) 2,2-dichloropropane cis-1 ,2-dichloroethene chloroform bromochloromethane tetrahydrofuran (THF) 1,1, 1-trichloroethane 1,1-dichloropropene carbon tetrachloride 1 ,2-dichloroethane benzene trichloroethene 1 ,2-dichloropropane bromodichloromethane dibromomethane 4-methyl-2-pentanone (MIBK) cis-1 ,3-dichloropropene toluene trans-1 ,3-dichloropropene 2-hexanone
SURROGATE STANDARDS
dibromofluoromethane toluene-D8
4-bromofluorobenzene
10338-11 QB-4 5/9/06 5/12/06 Water 1 LMM
Concentration
ug/L u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u
Recovery (%)
107
102 101
Quantitation Limit ug/L
2 1,1 ,2-trichloroethane 2 1 ,3-dichloropropane 2 tetrachloroethene 2 dibromochlorometliane 2 1 ,2-dibromoethane 2 chlorobenzene
10 1,1, 1 ,2-tetrachloroethane 10 ethylbenzene
m&p-xylenes 5 o-xylene 2 styrene 2 bromoform 2 isopropyl benzene 2 1,1 ,2,2-tetrachloroethane
10 1 ,2,3-trichloropropane 2 n-propylbenzene 2 bromo benzene 2 1 ,3,5-trimethylbenzene 2 2-chlorotoluene
10 4-chlorotoluene 2 tert-butylbenzene 2 1 ,2,4-trimethylbenzene 2 sec-butylbenzene 2 1 ,3-dichlorobenzene 2 4-isopropyltoluene 2 1 A-dichlorobenzene 2 1 ,2-dichlorobenzene 2 n-butylbenzene 2 1 ,2-dibromo-3-chloropropane
10 1 ,2,4-trichlorobenzene 2 hexachlorobutadiene 2 naphthalene 2 1 ,2,3-trichlorobenzene
10
Acceptance Limits (%)
78-114
88-110 86-115
Concentration Quantitation Limit
ug/L ug/L u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 5 u 2
U = Below quantitation limit
RL Resource Laboratories, LLC
Lab Number: Sample Designation: Date Sampled: Date Analyzed: Matrix: Instrument Dilution Factor: Analyst:
VOLATILE ORGANICS SW846 Method 50308/82608
dichlorodifluoromethane chloromethane vinyl chloride bromo methane chloroethane trichlorofluoromethane diethyl ether acetone 1,1-dichloroethene methylene chloride carbon disulfide methyl t-butyl ether (MTBE) trans-1 ,2-dichloroethene 1,1-dichloroethane 2-butanone (MEK) 2,2-dichloropropane cis-1 ,2-dichloroethene chloroform bromochloromethane tetrahydrofuran (THF) 1,1, 1-trichloroethane 1,1-dichloropropene carbon tetrachloride 1 ,2-dichloroethane benzene trichloroethene 1 ,2-dichloropropane bromodichloromethane dibromomethane 4-methyl-2-pentanone (MIBK) cis-1 ,3-dichloropropene toluene trans-1 ,3-dichloropropene 2-hexanone
SURROGATE STANDARDS
dibromofluoromethane
toluene-DB
4-bromofluorobenzene
10338-12 B-128-1-Dup 5/9/06 5/15/06 Water 5 LMM
Concentration
ug/L u u
50 u
180 u u
58 260
u u u
14 2800
110 u
800 u u
53 u u u u u
36 u u u
290 u
70 u u
Recovery
(%)
109
105 98
Quantitation Limit
ug/L 10 1,1 ,2-trichloroethane 10 1 ,3-dichloropropane 10 tetrachloroethene 10 dibromochloromethane 10 1 ,2-dibromoethane 10 chlorobenzene 50 1,1, 1 ,2-tetrachloroethane 50 ethyl benzene
5 m&p-xylenes 30 a-xylene 10 styrene 10 bromoform 10 isopropylbenzene 10 1,1 ,2,2-tetrachloroethane 50 1 ,2,3-trichloropropane 10 n-propylbenzene 10 bromo benzene 10 1 ,3,5-trimethylbenzene 10 2-chlorotoluene 50 4-chlorotoluene 10 tert-butylbenzene 10 1 ,2,4-trimethylbenzene 10 sec-butyl benzene 10 1 ,3-dichlorobenzet:e 10 4-isopropyltoluene 10 1 A-dichlorobenzene 10 1 ,2-dichlorobenzene 10 n-butylbenzene 10 1 ,2-dibromo-3-chloropropane 50 1 ,2,4-trichlorobenzene 10 hexachlorobutadiene 10 naphthalene 10 1 ,2,3-trichlorobenzene 50
Acceptance Limits
(%) 78-114
88-110
86-115
Concentration Quantitation Limit
ug/L ug/L u 10 u 10 u 10 u 10 u 10 u 10 u 10
400 10 290 10 120 10
u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 10 u 30 u 10
U = Below quantitation limit
RL Resource Laboratories, LLC
Lab Number: Sample Designation: Date Sampled: Date Analyzed: Matrix: Instrument Dilution Factor: Analyst:
VOLATILE ORGANICS SW846 Method 5030B/8260B
dichlorodifluoromethane chloromethane vinyl chloride bromo methane chloroethane trichlorofluoromethane diethyl ether acetone 1,1-dichloroethene methylene chloride carbon disulfide methyl t-butyl ether (MTBE) trans-1 ,2-dichloroethene 1,1-dichloroethane 2-butanone (MEK) 2,2-dichloropropane cis-1 ,2-dichloroethene chloroform bromochloromethane tetrahydrofuran (THF) 1,1, 1-trichloroethane 1,1-dichloropropene carbon tetrachloride 1 ,2-dichloroethane benzene trichloroethane 1 ,2-dichloropropane bromodichloromethane dibromomethane 4-methyl-2-pentanone (MIBK) cis-1 ,3-dichloropropene toluene trans-1 ,3-dichloropropene 2-hexanone
SURROGATE STANDARDS
dibromofluoromethane
toluene-D8
4-bromofluorobenzene
10338-13 Trip Blank 5/9/06 5/12/06 Water 1 LMM
Concentration ug/L
u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u
Recovery
(%)
107
101 100
Concentration Quantitation Limit
ug/L ug/L u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 2 u 5 u 2
Quantitation Limit
ug/L 2 2 2 2 2 2
10 10
1 5 2 2 2 2
10 2 2 2 2
10 2 2 2 2 2 2 2 2 2
10 2 2 2
10
Acceptance Limits
(%)
78-114
88-110
86-115
1,1 ,2-trichloroethane 1 ,3-dichloropropane tetrachloroethane dibromochloromethane 1 ,2-dibromoethane chlorobenzene 1,1, 1 ,2-tetrachloroethane ethyl benzene m&p-xylenes a-xylene styrene bromoform isopropyl benzene 1,1 ,2,2-tetrachloroethane 1 ,2,3-trichloropropane n-propylbenzene bromobenzene 1 ,3,5-trimethylbenzene 2-chlorotoluene 4-chlorotoluene tert-butylbenzene 1 ,2,4-trimethylbenzene sec-butyl benzene 1 ,3-dichlorobenzene 4-isopropyltoluene 1 A-dichlorobenzene 1 ,2-dichlorobenzene n-butylbenzene 1 ,2-dibromo-3-chloropropane 1 ,2,4-trichlorobenzene hexachlorobutadiene naphthalene 1 ,2,3-trichlorobenzene
U = Below quantitation limit
RL Resource Laboratories, LLC
Lab Number:
Sample Designation:
Date Sampled:
Date Extracted:
Date Analyzed:
Matrix:
Dilution Factor:
Analyst:
DIMETHYLFORMAMIDE
10338-01
B-5D-I
5/9/06
5/22/06
5/24/06
Water
1
AJD
Method Reference: EPA SW 846, 3rd Edition. Method 8270, modified.
dimethylformamide
SURROGATE STANDARDS
pyridine
U = Below quantitation limit
Concentration
ug/L
u
Recovery
(%) 57
Quantitation Limit
ug/L
50
Acceptance Limits
(%) 40-125
RL Resource Laboratories, LLC
Lab Number:
Sample Designation:
Date Sampled:
Date Extracted:
Date Analyzed:
Matrix:
Dilution Factor:
Analyst:
DIMETHYLFORMAMIDE
10338-02
B-6A-D
5/9/06
5/22/06
5/24/06
Water
1
AJD
Method Reference: EPA SW 846, 3rd Edition. Method 8270, modified.
dimethylformamide
SURROGATE STANDARDS
pyridine
U = Below quantitation limit
Concentration
ug/L
890
Recovery
(%) 72
Quantitation Limit
ug/L
50
Acceptance Limits
(%) 40-125
RL Resource Laboratories, LLC
Lab Number: Sample Designation:
Date Sampled: Date Extracted:
Date Analyzed:
Matrix:
Dilution Factor:
Analyst:
DIMETHYLFORMAMIDE
10338-03
B-8A-D
5/9/06 5/22/06
5/24/06
Water
1 AJD
Method Reference: EPA SW 846, 3rd Edition. Method 8270, modified.
dimethylformamide
SURROGATE STANDARDS
pyridine
U = Below quantitation limit
Concentration
ug/L
480
Recovery
(%) 60
Quantitation Limit
ug/L
50
Acceptance Limits
(%) 40-125
RL Resource Laboratories, LLC
Lab Number:
Sample Designation:
Date Sampled:
Date Extracted:
Date Analyzed:
Matrix:
Dilution Factor:
Analyst:
DIMETHYLFORMAMIDE
10338-04
B-9A-I
5/9/06
5/22/06
5/24/06
Water
1
AJD
Method Reference: EPA SW 846, 3rd Edition. Method 8270, modified.
d i methylfo rma 111 ide
SURROGATE STANDARDS
pyridine
U = Below quantitation limit
Concentration
ug/L
u
Recovery
(%) 62
Quantitation Limit
ug/L
50
Acceptance Limits
(%) 40-125
RL Resource Laboratories, LLC
Lab Number:
Sample Designation:
Date Sampled: Date Extracted:
Date Analyzed:
Matrix:
Dilution Factor:
Analyst:
DIMETHYLFORMAMIDE
10338-05
B-128-1
5/9/06 5/22/06
5/24/06
Water
1 AJD
Method Reference: EPA SW 846, 3rd Edition. Method 8270, modified.
dimethylformamide
SURROGATE STANDARDS
pyridine
U = Below quantitation limit
Concentration ug/L
1600
Recovery
(%) 72
Quantitation Limit ug/L
50
Acceptance Limits
(%) 40-125
RL Resource Laboratories, LLC
Lab Number: Sample Designation:
Date Sampled: Date Extracted:
Date Analyzed:
Matrix:
Dilution Factor:
Analyst:
DIMETHYLFORMAMIDE
10338-06
NBW-L 5/9/06
5/22/06
5/24/06 Water
1 AJD
Method Reference: EPA SW 846, 3rd Edition. Method 8270, modified.
dimethylformamide
SURROGATE STANDARDS
pyridine
U = Below quantitation limit
Concentration
ug/L
u
Recovery (%) 59
Quantitation Limit ug/L
50
Acceptance Limits (%)
40-125
RL Resource Laboratories, LLC
Lab Number:
Sample Designation:
Date Sampled:
Date Extracted:
Date Analyzed:
Matrix:
Dilution Factor:
Analyst:
DIMETHYLFORMAMIDE
10338-07
NBW-U
5/9/06
5/22/06
5/24/06
Water
1
AJD
Method Reference: EPA SW 846, 3rd Edition. Method 8270, modified.
dimethylformamide
SURROGATE STANDARDS
pyridine
U = Below quantitation limit
Concentration
ug/L
u
Recovery
(%) 75
Quantitation Limit
ug/L
50
Acceptance Limits
(%) 40-125
RL Resource Laboratories, LLC
Lab Number:
Sample Designation:
Date Sampled: Date Extracted:
Date Analyzed: Matrix:
Dilution Factor:
Analyst:
DIMETHYLFORMAMIDE
10338-08 ODW-L
5/9/06 5/22/06
5/25/06 Water
1 AJD
Method Reference: EPA SW 846, 3rd Edition. Method 8270, modified.
dimethylformamide
SURROGATE STANDARDS
pyridine
U = Below quantitation limit
Concentration ug/L
u
Recovery
(%) 69
Quantitation Limit
ug/L
50
Acceptance Limits (%)
40-125
RL Resource Laboratories, LLC
Lab Number:
Sample Designation:
Date Sampled:
Date Extracted:
Date Analyzed:
Matrix:
Dilution Factor:
Analyst:
DIMETHYLFORMAMIDE
10338-09
ODW-U
5/9/06
5/22/06
5/24/06
Water
1
AJD
Method Reference: EPA SW 846, 3rd Edition. Method 8270, modified.
dimethylformamide
SURROGATE STANDARDS
pyridine
U = Below quantitation limit
Concentration
ug/L
u
Recovery
(%) 67
Quantitation Limit
ug/L
50
Acceptance Limits
(%) 40-125
RL Resource Laboratories, LLC
Lab Number:
Sample Designation:
Date Sampled:
Date Extracted:
Date Analyzed:
Matrix:
Dilution Factor:
Analyst:
DIMETHYLFORMAMIDE
10338-10
P-20
5/9/06
5/22/06
5/24/06
Water
1
AJD
Method Reference: EPA SW 846, 3rd Edition. Method 8270, modified.
dimethylformamide
SURROGATE STANDARDS
pyridine
U = Below quantitation limit
Concentration
ug/L
u
Recovery
(%) 60
Quantitation Limit
ug/L
50
Acceptance Limits
(%) 40-125
RL Resource Laboratories, LLC
Lab Number:
Sample Designation:
Date Sampled:
Date Extracted:
Date Analyzed:
Matrix:
Dilution Factor:
Analyst:
DIMETHYLFORMAMIDE
10338-11
QB-4
5/9/06
5/22/06
5/24/06
Water
1
AJD
Method Reference: EPA SW 846, 3rd Edition. Method 8270, modified.
dimethylformamide
SURROGATE STANDARDS
pyridine
U = Below quantitation limit
Concentration
ug/L
u
Recovery
(%) 68
Quantitation Limit
ug/L
50
Acceptance Limits
(%) 40-125
RL Resource Laboratories, LLC
Lab Number:
Sample Designation:
Date Sampled:
Date Extracted:
Date Analyzed:
Matrix:
Dilution Factor:
Analyst:
DIMETHYLFORMAMIDE
10338-12
8-128-1-Dup
5/9/06
5/22/06
5/24/06
Water
1
AJD
Method Reference: EPA SW 846, 3rd Edition. Method 8270, modified.
dimethylformamide
SURROGATE STANDARDS
pyridine
U = Below quantitation limit
Concentration
ug/L
1700
Recovery
(%) 75
Quantitation Limit
ug/L
50
Acceptance Limits
(%) 40-125
RL Resource Laboratories, LLC
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