modeling solute diffusion in the presence of pore-scale

38
Modeling Solute Diffusion in the Presence of Pore-Scale Heterogeneity * ~ *O Sean W. Fleming (? 2$* Department of Geosciences “me~ 4** 104 Wilkinson Hall, Oregon State University, Corvallis, OR 97331-5506 ~ ,“’ e ,. current address: Waterstone Environmental Hydrology and Engineering Inc. 165038” St., Suite 201E, Boulder, CO 80301 e-mail: [email protected] * Roy Haggerty Department of Geosciences 104 Wilkinson Hal!, Oregon State University, Corval]is, OR 97331-5506 e-mail: [email protected]. edu telephone: (541) 737-1210 * corresponding author Submitted to Journal of Contaminant Hydrology August 10, 1999 key words: djjkrion model, n]dfinzfe, rafe-hmih?dnfas.rIranflcc Culeh, contaminam’ iranporfj dolomile :.....’” . ..... ...... . -. ..,”,- -------- .’ .”-. . ... . .....- . . .. .

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Page 1: Modeling Solute Diffusion in the Presence of Pore-Scale

Modeling Solute Diffusion in the Presence of Pore-Scale Heterogeneity

*

~ *O

Sean W. Fleming (? 2$*

Department of Geosciences “me~

4**104 Wilkinson Hall, Oregon State University, Corvallis, OR 97331-5506 ~ ,“’

e,.

current address:

Waterstone Environmental Hydrology and Engineering Inc.

165038” St., Suite 201E, Boulder, CO 80301

e-mail: [email protected]

* Roy Haggerty

Department of Geosciences

104 Wilkinson Hal!, Oregon State University, Corval]is, OR 97331-5506

e-mail: [email protected]. edu

telephone: (541) 737-1210

* corresponding author

Submitted toJournal of Contaminant Hydrology

August 10, 1999

key words: djjkrion model, n]dfinzfe, rafe-hmih?dnfas.rIranflcc Culeh, contaminam’ iranporfj

dolomile

:.....’” . ...’.. . . . . . . . -. ..,”,- -------- .’ .”-. . . . . . . . . ..- . . .. .

Page 2: Modeling Solute Diffusion in the Presence of Pore-Scale

DISCLAIMER

This repoti was prepared as an account of work sponsoredbyanagency of the United States Government. Neither theUnited States Government nor any agency thereof, nor anyof their employees, make any warranty, express or implied,or assumes any legal liability or responsibility for theaccuracy, completeness, or usefulness of any information,apparatus, product, or process disclosed, or represents thatits use would not infringe privately owned rights. Referenceherein to any specific commercial product, process, orservice by trade name, trademark, manufacturer, orotherwise does not necessarily constitute or imply itsendorsement, recommendation, or favoring by the UnitedStates Government or any agency thereof. The views andopinions of authors expressed herein do not necessarilystate or reflect those of the United States Government orany agency thereof.

Page 3: Modeling Solute Diffusion in the Presence of Pore-Scale

DISCLAIMER

Portions of this document may be illegiblein electronic image products. images areproduced from the best available originaldocument.

Page 4: Modeling Solute Diffusion in the Presence of Pore-Scale

Fleming & Hsrty, Modeling soluie diffusion in the presence of pore-scale l)ettmgeneity. ~

<

Modeling Solute Diffusion in the Presence of Pore-Scale Heterogeneity

Sean W. Flemingll ~ and Roy Haggertyl~s

ABSTRACT

A range of pore diffusivities, DA is implied by the high degree of pore-scale heterogeneity

obsemed in core samples of the Culebra (dolomite) Member of the Rustler Formation, NM. Earlier

tracer tests in the Culebra at the field-scale have confirmed significant heterogeneity in diffusion rate

coefficients (the combination of DPand matrix block size). In this study, expressions for solute

diffision in the presence of multiple simultaneous matrix diffki~~ities are presented and used to

model data from eight laboratory-scale difflision experiments performed on five Culebra samples.

lognormal distribution of Qois assumed within each of the lab samples. The estimated standard

deviation (ad) of ln(D,J within each sample ranges from () to 1, with most values lying between 0.5

and 1. The variability over all samples leads ro a combined ad in the range of 1.0 to 1.2, which

appears to be consistent with a best-fit statistical distribution of formation factor measurements for

similar Culebra samples. A comparison of our estim~tion results to other rock properties sugysts

that at the lab-scale, the geometric mean of D} increases with bulk porosity and the quantity of

macroscopic fefitures such as vugs and fractures. However, ad appears to be determined by

variability within such macroscc)pic features and/w- by micmpore-scale heterogeneity. In addition,

comparison of these experiments to those at larger spatial scales suggests that increasing sample

volume resu]~ ill Xl illcre~se ill ~d,

1Department of Geosciences, 104 Wilkinson Hall, Oregon State University, Conullis, OR 97330-55062 Now at: Waterstone Environmental Hydrolo~ and En&neering, Inc., 165[}3Sth St., Suite 201E,Boulder, CO 80301s Corresponding autho~ e-maii: ha~ertr(i?jjgeo. orst.edu,telephone: (541) 737-1210

A

Page 5: Modeling Solute Diffusion in the Presence of Pore-Scale

1. INTRODUCTION

3

Mass transfer refers to the movement of a constituent from one phase or region to another

along a concen~tion gradient (e.g., WeLj el A, 1984). In the context of solutes in geologic materials,

this involves movement of solute from pores dominated by advection (advecuve porosity) into dead-

end pores dominated by diffusion (diffusive porosity) or onto sorption sites on the surface of grains.

This phenomenon has two well-known and significant implications for solute transport in

groundwater. First the rate of advective transport away from the source decreases through time as

@e solute spends less time in advective porosity and more time in diffusive porosity containing

stagnant water (e.g., Roi)ent et aL, 1986;Qtakoa’o~ arzdKahcct)i, 1993). This phenomenon partly

determines how far and how fast a solute will be transported, and is particukdy important to

evaluation of the environmental risk involved in geolo~-c disposal of nuclmr waste. Secondly,

remediation of a contaminated aquifer by pump-and-treat, soil vapor extraction, and bioremediation

techniques is slowed if mass tram fer from diffusive to advective porosity is rate-limited (Jfeid7erg et

aL, 1987; Bnaseaz and Rae, 1989; Gob< and O.x~, f 991; Gierke et a~, 1992;ArmslnJrg ezuL, 1994; Fry and

I~tok, 1994; Harvey et aL, 1994; Rak-ieott andA4iLir, 1994; Hager~ utzdGordck, 1995). Diffusion in

geologic media also has implications for petroleum migration (e.g., Mann, 7994), evaluation of

residual oil saturation in hydrocarbon resemoir studies (e.g., TonzicJet at., ?973; Dem.r arzdCarhJe,

?98G), determination of @Ar/3qAr cooling histories in geochronology studies (bwra el al., 1989;..

Lvera et aL, 7993), and evaluation of the relationship between fluid and melt inclusions and magma

chemistry (Qin et aL, 1992).

A simplifying assumption made in most treatments of nonequiiibrium mm transfer in

geologic media is that a single rate of sorpricm or diffision is present. The implication of this

assumption is that rock is homogeneous, or can be treated as effectively hc)rnogeneous at the spatial

scale of interest. However, most rock is not homogeneous at the spatial scales at which mms transfer

processes operate. In the context of lab-scale diffision, this heterogeneity may result from variability

Page 6: Modeling Solute Diffusion in the Presence of Pore-Scale

Fleming & Haggmty, M~dclulg SOIUICd, ffmion i IIIC prcsrnce of p@re-sc#le hetemgrnt-i~, %

4

in the volume, size, and geometry of macroporosity or microporosity in aquifer particles and

aggre~tes of particles (Rao el u!., 1980; Pignfzlefb,1990; [P’oofief al., 1990; Bui/andROberls,1991; i%znon

ezd, ?992; ELmzon and RoLerff, 1994) and the external and internal geometry of small lenses of

impermeable material, and the proportion of this material (SJarke~ord, 1991). .4s these factors

control rates of matrix diffision, and as they are heterogeneous at the pore scale, difhsion should

also be heterogmeous at the pore scale. That is, in a given volume of rock multiple rates of

diffhsion occur simultaneously, and “multirate” mass transfer may therefore be needed to adequately

describe solute transport (e.g., Vik?erm-azx,1981; PeditandMU&, 1994; Haggeg andGoRLck, 199~.

The effects of multirate mass transfer have been meamred in lab-scale soil column experiments (e.g.,

BaJ and Robent, 1991; Grah~h! and Kkineidarn,1995; PeditatzdMilLr, 1995; Culveret aL, ?997; W’ertbet

aL, 1997; Hagerzj and GoreLck, 1998; Riigneret aL, 1999) and more recend y in integrated and

comprehensive field-scale studies of the transport properties of the Culek dolomite at the Waste

Isolation Pilot Plan t (WIPP) site (Meig.rwzdBeudteim,irznwicu<Hagtr~ et J, in review;MrKenna el al, in

mien].

The WIPP is a proposed rcpositoq fcjr defense-generated transumnics located about 2(I miles

northeast of Carlsbad, New hfexico (F@lre 1). The Culebra Member of the Rustler Formation, a

Permian evaporitic dolomite, is considered to be the most transmissive laterally continuous

hydrogeologic unit in the WIPP area and the most likely pathway of radionuclide transport from the

repository in the event of human intrusion (Hoi, 1997, A4eig~and BeaAz-m, in reie+. Due to a.

complex history of deposition, diagenesis, and frachlring (see JYol, 1997 for a re~’iew), the Cule&a

dolomite is characterized by a high degree of lithologic and structural heterogeneity (F@tre 2).

Detailed analysis of core has clearly revealed multiple scales of fracturing, along with spatially variable

amounts of vugg porosity and gypsum -fd~ingof \w<gsand fractures; pocn-ly cemented, silt-size

dolomite interbeds are also common (HoJ, 1997). The presence of multirate diffitsive mass transfer

in the Culebra, at both lab- and field-scdes, has been inferred from this observed heterogeneity (Hoti,

Page 7: Modeling Solute Diffusion in the Presence of Pore-Scale

Fleming & HWAWY. Modeling solute diflision iI1 the pmsmce OfpOK-SC21Cl,ettrob~:,city, <

5

195’7),and its effects at the field-scale have been confirmed by suites of tracer tests at two locations

(Mez& and Beanbeim,in rwiez~;Hagerp et a[., in revieq McKenna et a[., in wieu~.

Our objectives in this paper are (1) to formulate a mathematical mode] of diffusion in a rock

with variable diffhsivity (2) to solve the resulting mathematical equations; and (3) to estimate

dkrnbutions of dii%.tsivities from a suite of laboratory diffusion experiments performed upon the

Culebra dolomite.

2. DIFFU!30 N EXPERIMENTS A.ND DATA

Data obtained from static diffusion experiments conducted by Sandia National Laboratories

(Tidw-t4ez d, in$mw) were analyzed in this study. The x-ray imaging technique used in these

experiments is described in Tidwfl and Gh.cr (1994), and detxils of rhe sample selection, experimental

set up, and results are given in Cbnlr&in-Fmzr et al. (1997) and Tidvt# et al. (inp-e.w); a brief oven’iew is

given here. Five small (approximately 6 cm by 4 cm by 2.5 cm thick) rectangular blocks of Culebra

core were selected to represent a range of Culebm porosity types (see Figure 2 and Table 1). Because

of limitations on sample availability, samples with significant interpxticle porosity (silty dolomite,

which is not uncommon in the Culebra) could not be represented among the samples. The samples

were atmched to a constant-concentration tracer resenmir at one end and sealed along their other

edges to form no-flux boundaries. Constant concentration was maintained within l% of a target.

concentration by slow circulation in the tracer resen~oir. The tracer consisted of potassium iodide

(W), dissolved in a sodium chloride &laCl) solution simulating nmurally-occurring Culebra pore

fluids @rine). Each block was i]iitiaily saturated with brine. Tmcer was then allowed to diffuse from

the reservoir into the sample (k-diffision). .At the end of the in-diffusion experiment, x head

gradient was established across the block and tracer wm forced across it until the Kl concentration

within the pore space was equal to that in the reservoir (i.e., until the sample was complete] y flushed

with the I-Clsolution). The reservoirfluid was then replaced with pure NJICI solution, and the tracer

Page 8: Modeling Solute Diffusion in the Presence of Pore-Scale

Fleming & H=q, MO&-Ii,Ig SOILIICdiffusion in tile prrsrIIce of pore-scale llemrowncity. .

6

within the block was permitted to diftlse hck out into the reservc)ir (out-diffusion). Slow

circulation of fluids through the reservoir was again performed to maintain concentrations within 10/o

of the target concentration.

X-ray images of each block were taken at intervals during the in- and out-diffkion

experiments (Tiduz# et al, inpw$. As the presence of the iodide ion alters the amount of x-ray -

energy transmitted through the sample, these images provide maps of porosity and of normalized K.1

concentration in the rock through time. The im~ges were then further processed to provide the

normalized mass uptake and recovery data used in our modeling (F@re 3).

Three important difficulties were encountered during the course of the experiments. Firs~

tracer concentration in the reservoir was accidental y varied during the earl kst phases of the in-

difksion study, resulting in a time-varying boundary condition. Second, sufficient dissolution of

pore-filling ~’psum in sample RC6-G occurred during the course of the experiment that its porosity

was significantly increased; this block was omitted from the out-difft]sion experiment. Lesser

gypsum dissolution also took place in sample 1333-FI. In both cases, this probably occurred while the

sample was being saturated with KI tracer in preparation for the out-diffusion phase (V. Tidwd,

pmsorzafmnmwzicalioz f5’98). Third, it proved impossible to fill]y saturate sample RC4-D with tracer,

so it was also omitted from the out-diffusion phase.

In addition to examining each data set separately, we combined the data from individual

samples to form bulk in- and out-difiision data sets. The bulk data are what would be obtained*

experimentally if all the samples were joined together in parallel along a singje resen’oir, and

normalized mass difksed in or out wm measured for all block at once using a singje x-ray irrnge.

This was done for the purpose of obtaini!lg x rough approximation to”(iiffusicm in a larger, mc]re

heterogeneous volume of Culebra. It is important to re-emphasize, however, that the samples

examined do not represent the full lithologic ~’ari~bilityu’ithin the Culebra. The bulk mms ratio

curve we obtained is the arithmetic mean of the individual mass ratio curves, weighted by the sizes of

the samples. Use of the bulk diffision data sets is intended to simulate a larger-scale scenario in

Page 9: Modeling Solute Diffusion in the Presence of Pore-Scale

Fleming & H~ny, Mode]iIlg SOIUICdiffi,sio,, i,, I]le prcsm,cc oflxm..scalc l,c~crown.ity 7<

which an extended reservoir of solute (e.g., m advective flow pathway) encounters a variety of nmtrix

types, as represented by the different blocks of varying porosity scales and types Figure 2 and Table

1) used in the diffision experiments.

3. MATHEMATICAL AND CO DE DEVELOPMENT

Here we present expressions describing one-dimensional diffkion into or out of a rock matrix

in the presence. of both uniformity and heterogeneity in DP Consider a sample of Culebra dolomite

of bulk porosity, 6, bounded at one end by a reservoir of solute (potassium iodide in our case) with a

time-varying concentration, bounded at the other end by a no-flux boundaq, and having an arbitrary

but uniform initial solute concentration. Conventional, single-rate diffkion (i.e., a single diffkivity)

of ISl tracer into or out of the pore space of the sample is described by the diffusion equatioix

(Eqn. la)

where C is the concentration of solute within the pore space ~4/Ls, or dimensionless if normalized],

and DPis the pore diffisivity ~~/Tl, which is some fraction of the aqueous diffusivity of the solute in

water, D% ~-/Tl. The boundary and initial conditions are.

C(x=z,l)=c, (f) fEq?I. Ilq

3C(X=0,1)=0ax

C(x,l=o) = co

(Eq?l. Id

(Eq?L Id)

Page 10: Modeling Solute Diffusion in the Presence of Pore-Scale

Fleming & H~rty, N40dcling solute diffusion i,l Ihe prcscncc o(pore-scak lIeIrrcgc-neity. . 8

where Co is the initial concentmtion in the sample ~/Ls]. A simple expression for DP is (e.g., Bear,

1972’):

where ~, the tortuosity [-], is defined as F/# (e.g., Be.a~/972); /is the straight-line distance from one

end of the pore to the other ~] and 4 is the actual length along the winding pore ~]; and P/.4~ <1.

DP maybe reduced if sorption occurs within the pore, or if restrictivity is significant (i.e., if the pore

radks is similar to the ionic or molecular radius of the solute, e.g., futterjieti e[uf., 1973). For a

complete review of the theory of dift%sion in rock, see OJkron and A~eref~tiek(199>~.

Taking the Laplace transforms of E9ns. I.a-c simplifies the diffusion equation to a second-

order nonhomogeneous ordinwy differential equation:

(32? p ~.-co—.—t%2 DP DP

where ~ is the Lapl:}ce tmnsform of concentr~tion within the pore space ‘~~d} is the Laplace

parameter. The boundag conditions m-enovx .

W(x = o)=o

ax

and:

C(p,x=1) = c, (p)

(Egn. 3a)

(Eqn.3b)

(Eqn.3.c)

Page 11: Modeling Solute Diffusion in the Presence of Pore-Scale

Flcrnillg.9 Hs~. ~~~delillg SOIUICd!l-kion in IIW pre.tvm- ofpcm-scak lICICrCIWtIViIy.

Solving Eqn. 3.a subject to Eqns. 3.11and c by the method of undetermined coefficients gives:

[1——C(p,x) = c] (P)-:

9

(Egn. 4)

The Oh spatial moment of the concentration profile gives a measure of the solute mass, h4(~, within

the slab at time, &

M(f) = e A Jc(x,l)dx (Eqn.5)

r-o

where A is the cross-sectional mea of rock exposed to the solute resemoir, and which is required if

C(X;tJ is given conventional (three-dimensional) units of mass/unit volume. Taking advantage of the

fact that the Laplace transform is a linear operator, substituting Eqn. 4 into Eqn. 5, integrating and

recognizing the definition of the hyperbolic tmgent gives the following expression for diffisive mass

uptake or release in the presence of uniform DPsubject to the boundmy and initial conditions

encountered in the static dlffision experiments: .

fw(r, Dp) = (oA)L-’Il=lanh(’m)+(Eqn. 6)

where the symbol L-J indicates the inverse Lapkce tram form. Eqn. 6 and the inverse Laplace

transform of Eqn. 4 are generally useful solutions to the diffusion equaticm, m they can

Page 12: Modeling Solute Diffusion in the Presence of Pore-Scale

Fleming & Hqyq. hfodelin~ solute d[ffusio,] III the presence of pwc-sc.alc lIctcrogt-\Iciq. 1()

accommodate any initial concentmtion and a constant or time-vmying boundary ccmcentmtion. For

notational convenience larer in the cleriv~tion, we define i14’(f,DP)thus] y:

A4’((,Dp)=M(f, Dp)/e (Eqn. 7)

Now consider a model of pore-scaJe heterogeneity k u’hich porosity in the rock matrix

consists of many l-D, non-intersecting pores. The pore diffusivity is constant along the lengdl of

each pore but may be different between neighboring pores. Changes in pore dift%sivity are due, at a

rninikn~ to differing tortuosity and cross-sectional area of the pores. Although the pores do in fact

intersecq the assumption of many l-D, non-intersecting pores allows us to retain the simplicity of 1-

D diffkion while incorporating the significant effects-of variable diffusivity. Approaches similar to

this have previously been successfully used to accor-mnodnte the effects of wuiable diffusi~~ityupon

So]ute transport (e.g., &fHi@um etd, ~997; &“.ger/y d (%dl”k, 1998; l]d#yly et u~, ik rwiev).

The total mass diffised into the pcxe space at a gi~’en time is the sum of the contributions to

diffusive mass uptake or release of the different values of DP present in the rock. For the case of a

continuous distribution of 111,total maw uptake or rele~se for the sample is described by the

following expression (Ffemi~g,f998):

M(f) = e ]fc(DJM’(LD,)dD,a

(Eqn. 8)

where the integration limits, a and 12represent the minimum and maximum possible values of DPand

may be taken in general to be () and m, andJ@P) is a densiy function (DFj which describes the

relative frequencies of different values of D? in terms of the prcqmrtion c}fthe total pc)rosiry in which

those values of DPare operative:

[1- f3Dfc(Dp)=-& —, 0’ (Eqn. 9)

Page 13: Modeling Solute Diffusion in the Presence of Pore-Scale

Fleming & HWWIV. ~~OdKIIIWSOIUICdiffusicm in the prc-smlce of p~re-scale I)ctcrogelwity 11

where 9r#3 is the ratio of the porosity constituted by pores with a particular pore diffusivity, DA to

the total porosity of the sample. It is important to note that the use of a DF does not imply that DP

is stochastic. Rather, the fi_mctionJ@P) is simply a means of weighting the contribution, A4’(LDP),to

total mass uptake or release, M(z), made by a particular pore diffusivity, Dp, on the basis of tke

relative (volumetric) prevalence of pores with that value of DP The tidl derivation is given in FLvning

(199/7),but note that Eqn. 8 is very similar in form to an expression presented in the chemical

engineering literature over a quarter of a century ago which quantified diffhsive mass uptake in the

presence of a continuous distribution of ~grainsizes (IWherz and L-JIghLrz,1977).

The functionJ@P) maybe any continuous distribution. A number of general considerations

suggest that a lognormal distribution may be appropriate (Hu~ger~ u)lJ Gonvkk, f~98). Discrete

distributions and alternative continuous DFs have also been used, such as gynma and piece-wise

linear distributions (see Ho.!lwheckel u1., 1999). However, fommtion factor datz from the Culebra

dolomite support the assumption of a lognormal DF (Figure 4), and previous analyses of tracer tests

performed in the Culebra obtained excellent results using a lognormal distribution (Haggero et al, in

fevieu<McKenna et A., in rw&+).

We normalize A4(f)bv the mfisimum total solute mass present in the rock, A4T. In the crise of

diffision into the rock, this is the mass at I = m. Fcx difftlsicm out of the rock, this is the mass at r =

O. This maximum total mass is given by:

iW~=@AIC~ (Eqn. 10)

where the 1is the length of the rock sl;lb as mezsured away from the resenwir and C= is the initial

sample concentration out-diffusion (Co)and the late-time sample concentration for in-diffusion

(C(GCOJI. If normalized conce~ltrxtions are used, C~ = 1.

Page 14: Modeling Solute Diffusion in the Presence of Pore-Scale

Making the appropriate substitutions forjf-@P) and A4’(i,DP)into Eqn. 8 and normalizing by

Eqn. 10 yields:

c, (p) -~

\m’ ‘anh(’w)+dDp

J

(Egn. 11)

where ~ and ad are the mean and standard deviation, respectively, of h@P).

A FORTIL4N77 code was written to so]ve Eqn. 11 for both forward simulation and

parameter estimation. The purpose of the code was to obtain estimates of the values of ~ and

ad from the diffk.ion data previously discussed. Note that a distribution of diffisivities interpreted

from data under the assumption of nonintersecting pores in a parallel arrangement, aligned

approximately nomud to the surface of the sample, should be considered a lumped distribution

representing what may be diffusion in parallel and series in a more complex geometty (Ha~.ger~yad

Gunzkk, f$%’). Several subroutines from the IMSL (h~ternational Mathematics and Statistics

Libraries) Version 3.0 package u’ere used. These subroutines use the de. Hoog algorithm to

numerically evaluate the inverse Laplace mmsform (deHoog e[ al., 19S2),Gauss -Krrn~rod rules to

perform numerical integration, and a modified h\-ell}lerg-h4arqtlardt algorithm (Mtwqwd, 1963) and

a fmite-di fference Jacobian to solve the non] inear least-squares c)ptimization problem. The lower and

upper limits of integmtion were set to the 1 x 10-7and (1 - 1xl O-q percentile values of D*

respectively, for a gi~’en f.ldand ~.+ For kge ~,dues of the Lap]ace parameter, p, the ccmlp]ex vahe of

the hyperbolic tangent in Eqn. 11 was set to [1,0] to overcome numerical difficulties (Ffimit.y, 19%’).

Capability to use Eqns. 6 and 10 to estimate a conventional , singje-rate diffkivity from the

normalized mass data was also incorporated into the code.

...... ..- . . .. . . ... .. ....... . .....---- . . ...... ..... . . . :. --, .--.’ . . .

Page 15: Modeling Solute Diffusion in the Presence of Pore-Scale

Log-space root mean square error @4SE) wm used m a measure of fit, as log-transformed

data shows a greater sensitivity to the late-time, h’ mass ratios at which multirate effects are b~eatest

(e.g., IWJven and Loughh, 1971; fi~ggertyutldGoruftk, 1998). Similar concerns led us to convert the

in-diffusion mass ratio curves, which are large-valued at late times, to:

(Eqn. 12)

which is small-valued at late times. This approach u’as also used by lUdwetZutzdLwghilz(1971).

When the data is then log-transformed, small relative changes in the raw late-time mass ratio data

give rise to significaptl y larger relative changes in the converted and transfomled values.

An approximation of parameter estimation statistics are calculated using the Jacobian, or

sensitivig, matrix. This is a )1by ?Itmatrix, where His the number of pm-arneters to be estimated (1

for a single-rate model, 2 for multirate) and t)t is the number of data points in the mass ratio cumes.

The entries of the Jacobian, JX consist of the deti\~i~ti\~eof the calculated mass ratio at the i:btime,

Mi/MT, with RSPt2Ct to thejb pmXmeter,A (e.g., ~mpnwl ud ~“OJ& 19$7; J%Jwejv et u~.,7996):

{/)h4iA4T

Jv =zp j

(Eqn.13)

The covariance rrultrix is a rZby n matrix estinmted by tding the inverse of the square of the Jzcobian.

and multiplying each entry by the variance of the random error in the observed data (e.g., KtzopzLzn

and VOJJ,1987). As we have no direct measure of the error in the data, we follow the common

approach [e.g., Bani, 1974, p. 178] of using the mean square error between the data and the calculated

cumes as a surro~te for the replicate vmiance. The square roots of the entries along the diagonal of

the covariance m~trix give, in turn, the standard cie~~iations(08(X,confidence intel~’ids) of nomdy-

distributed error about the best-fit values cjf the estinmted parameters. C)ur cc)de returned estimates

Page 16: Modeling Solute Diffusion in the Presence of Pore-Scale

Fleming & Hawq, Nfocleling SOIUIrdiffltsic,n III the presence ofpore-scale IIeterogrm.,ty, 14

of the arithmetic value of M but of the narurd ]o~rithrns of DP and ~d, so in arithmetic space the

confidence internals are symmetric about M but asymmetric about Dp and ~d.

4. RESULTS

Suites of forward simulations demonstrating the effects of variation in M and ad, and

comparing single-rate diffusion to multirate diffusion, are given in F@re 5. Plots of the static

diffusion data and of curves calculated using best-fit single-rate and mulrirate models are given for

two examples in Figure 6. Table 2 summarizes the results for all experiments, giving the best-fit

value of Dp for each sample and for kl k diffusion obtained using a single-rate model, as well as the

corresponding best-fit multimte parameters. Larger ~ values indicate faster diffusion, on average, for

a given block length and larger ad values indicate the presence of a wider range of DP (i.e., more

significant multirate effects). RMSE values m-ealso given , as are estinY.ltes of 95’?/o confidence

intervals for Dp M, and ad.

While the quality of the fits of the calculated curves to the data is generally good, these

matches are inferior to those obrained from analysis of ficlc{-scale CLdcbra tmcer tests using a

multirate mass tram fer model (Htigy-y c! d. it~revicu.~.MdGmw et al, itl mien.) and to those obtxined

from other laboratory data where multirate mass transfer was investiwlted (e.g., lP’erfAet u1.,1997;

Haggerty and Gort&k, 1998). This is attributed to a combination of the quality of our data and model

assumptions that may not be fully did. The scztter app:lrent in Fi<gures3 and 6 may result from

some combination of fzilure to maintain a conscult-concen traticm boundary condition, gypsum

dissolution, and a Izck of precision in the s-ray imaging technique, which is still under develc)pment.

Our assumption of constant diffusit~ity along the pore, though also assumed in other studies of this

type, is likely a poor assumption for a small sample of the CLdcbra dc)lomite, which is high]y

heterogeneous at all spatial scales. The assumptions of purely one-dimensional diffusicm and of a

lognorrnal distribution of diffusivity are potenti;d]y in error, particularly in samples thzt may be

Page 17: Modeling Solute Diffusion in the Presence of Pore-Scale

dominated by a small number of porosity types (for example, fractures and intrmgranuk porosity).

The model used in this paper is best applied when the m’emging volume is large relative to the scale

of heterosneity; this condition is probably not met within some of the individual samples we

examined.

Since D% increases somewhat with concentration (see Cff.mkr,1997), variation in tracer

concentration within the samples with time might have led to changes in DPover the course of the

experiment. However, Cm-h (1976) showed that concentration-dependence of D% has a negligible

effect on concentration profiles and breakthrough curves in systems simik to the static dt ffision

experiments. As the mass ratio curves used in OLMana$sis are integrated concentration curves,

concenwation-dependent Dw should not be a significant source of error. Moreover, we were

permitted to test. whether this was an important effect by noting that the average tracer concentration

within a given sample was significantly higher during the out-diffusion phase than during in-

diffision. If concentration-dependence of D%was present and Imd a significant effect Lipon the

mass curves, then the out-diffusion experiments would ‘giveconsistently larger diffusi~’ities than

tihose obtained with the same sample from the in-diffbsicm experiments. This was not observed

~able 2).

Comparison of D,q of the M tracer to the best-fit distribution of pore diffusivities (for the

multirate model) and the best-fit Dp (for the single-rate model) might provide a means of confirming

the reasonableness of the parameter estimates, because Dp can never exceed D~$ J-+owever, three,

considerations show that such comparisons are bc)th prohlemztic and unnecessary. First, alrhough

DP and Mare well-constrained, the confidence intends about the best-fit values are nonetheless

sufficiently wide (largely due to data scatter) to accommodate any reasonable value of DW for this

system. Second, judging the entire distribution against D“. presumes that the tails of the distribution

should be reliable. However, the lognorrnal distribution is only an approximation to the true

distribution of diffusivities in the rock. Moreover, the sensitivity of any experiment to diffi]sion rates

in the tails of the distributions is lower than thxt to rates of diffusion closer to the mean (Hug<c~ e~

Page 18: Modeling Solute Diffusion in the Presence of Pore-Scale

Fleming & Has+gerty. hfocieliIIg solute dilhioII in the prrsc.i]ce of pore-scale I,ctrrc>gewiry, 1()

A., it~nvz”w).Third, D% is unknown for these experiments, which ccmsisted of a quatemav diffusion

system containing 1%+, Cl-, K+, and 1-ions. Some other species might also hxve been present, such

as calcium and SU1fate ions produced by ,g~psurn dissolution. The complexities of mul ticomponenr

diffusion are discussed in detail in Cm-LT (19Y7) and F.lemitg (1W8); essentially, Dw must be

determined experimentally, which has not been done for this diffusion system.

5. DISCUSS ONI

~.1 Sinrrie-Rare versus Multimte Mode]s

The 9570 confidence ranges in ad for P133-H, RC1-.A, and RC4-D do not include O Table 2).

It is also ciear from the RAKELi~ and RA{SEsRvalues that the mul tir.lte model prrx’ides a quanrifmbly

superior fit. .Multirate diffusion, therefore, occurs in these smnplcs. In contrxst, consen>ative

consideration of the in-diffusion and out-diffhsirm results mken together su<<qeststhar mul tirate

diffision was not detected in samples RC2-B and RC6-G.

Multiple simultaneous diffisivities are significant at the lab-scale in spite of the relatively small

estimated values of ad and the fact that two of the five samples can nc)t be prcn~en to shc)w mu]timte

effects from our modeling of this data. There are three reasons for this. First, the amumed

. distribution is lognormal, so a relatively small ~d represents significtilt ~“arixbilityin DP A cr,lvalue of

0.5, for example, indicates almost ml order of magnitude difference between the 0.02.5 and 0.975

qua.ntile diffkivities. This difference increases to a filctc)r of 50 for a O(Iof 1.

Second, while the ~’isibleeffects of variable diffhsi~’ity upon the mass mtio cun~es generally do

not appear to be large for small Values of o~ (Fi<gure()), single-rate and mu] tirate cunrcs diverge at

later times ~igure 5; see ako pu!lhrm ut~dbgiuftl, ~971; Hug;t+ u}zd~od’”k. ~~~/i’). This k

consistent with the finding by Cw/n@kZ md RAv-f.r (199 S) that even small ~’ariahilitv in di ffusivity,

may have significant implications for long-telrn solute transport.

Page 19: Modeling Solute Diffusion in the Presence of Pore-Scale

Third, we consemmively rejected the hypothesis that a range of diffusivity is present in a given

sample if we could not prove that it was. ~f the 95% confidence range in estimated ad included or

very nearly included O, and if the RMSE vaiues did not show that the multirate model provided a

significantly better fit than the single-rate model, it was concluded that multirate diffusion um not

present. However, these tests do not indicate that a single-rate model is preferred, either.- Any ad

range which included O also included infiniv, the inversion statistics in such a case indicate that it is

impossible to determine from the available data whether multi rate effects are present in that sample.

This is due to a high degree of insensitivity of RMSE, over the dynamic range of the data, for a given

value of ~ (which is rexonab}y well-estimated in all cases), and in the presence of scatter in the data,

to the vaiue of ad . ~f a sin$e-r~ie model was ckdy superior, the rnultirate inversion would return a

value of cd near Owith narrow confidence bounds. Data collection to later times (i.e., over a greater

dynamic range) might facilitate far more reli:lble estimates C)fad (Figure 5).

Work by TidwY Cld. (zkp-m) detected vmi:dility in diffi]si~~ityin samples RC2-B and RC6-G

(for example, RC2-B contains a fmcmre), whereas our mode]ing did not. Tidvvl efd (it~pnx.j

anaiyzed concentrations along parallel transects into the samples, wherein we analyzed the rn:lss in

the whole sample through time. This whole-sample mas measurement is influenced by mulrirate

diffusion in approximately the same manner as a tracer test aicmg a fracture through the rock would

be influenced, insofar m a tracer test mmples all of the diff~lsi~~itiessimultmeously. In addition, both#

whole-sample mass measurements and solute tracer tests are most strongly influenced by small

amounts of rock with Iou’er-than-m’erage di ftisivities (e.g., Cmmi//gLvzmd Rdzti.r, 1998), whereas

the fracture con~lined in RC2-B hzs a higher-than avera<gedi ffusivity. The results obtained using

whole-sample mass measurements are thus more amenable tc) ccm~parison with previous, field-scaie

results. It is also important to recall tklr our results do not preclude the presence of multi-ate effects

in these two samples, m explained previcmsly.

The bulk diffusion data clearly shc)u’ multirate effects, as expected (see Table 2). In addition,

some of the key characteristics of the bulk diffusion cm be assembled frcxn ciiffhsion in the

Page 20: Modeling Solute Diffusion in the Presence of Pore-Scale

individual samples. Using in-diffusion as an example, the geometric mean of the estimated DPvalues

for the individual blocks (2.27 x 10-6mz/hr) is very simik to the estimated geometric mean of the

lognormal distribution for the bulk data (2.26x 10-6 mz/hr). In addition, the minimum estimated

value of DP for an individual block (RC4-D, 9.57 x 10-7mz/hr) corresponds roughly to the 20*

percentile in the lognormal CDF of diffusivities (9.96 x 10-7mz/hr). Slmik-ly, the maximum

estimated value of DP for an individual block (B33-H, 4.78 x 10-Gm~/hr) corresponds roughly to the

80dIpercentile in the lognonnal CDF of diffusivities (5.16 x 10-6m~/hr). Of course, neither the five

single-rate DPvalues nor the five lognormal distributions from the individual slabs combine

additively, in a rigorous sense, to form z new lognormal distribution corresponding to the hulk

experiment. However, it is clear that the estimated Iognormal distribution estimated solely from the .

bulk diffhsion data provides a reasonable representation of the range of pore diffbsivities known to

exist within the individual slabs. A~in we note that the bulk di ffusion data do not represent the full

Iithologic variability within the Ctdebra, and therefore our results should not be taken to represent

the full variability of diffusivity within the Culebra.

5.2 Diffhsiviw and Formation Factor

As diffusivity is inversely proportional to formation factor, the distribution of one should be

similar to that of the other. Unfortunately, calculation of absc)lute D4 values from formation factor.

data may be unreliable and it is therefore difficult to directly convert a CDF of formaticm fhctors to a

CDF of DP However, the standard deviarion of the best-fit lognmmal distribution of formtion

factors determined from all 21 Culebra samples (see figure 4 and caption} shcdd be similar to ad

estimated from the bulk static diffusion experiments. CTfor the fommion f~ctors was found to be

approximately 0.7, which is similm to the values found for bulk diffilsion data. This reasonably close

correspondence serves as supporting evidence for our interpretation of the diffusion experiments,

and raises the possibility that formation filctnrs - which are much easier and cheaper to obtain than

Page 21: Modeling Solute Diffusion in the Presence of Pore-Scale

laboratory diffusion data - mi<ghtprovide an indirect but reasonably reliable means of estimating

pore-scale heterogeneity.

5.3 Otie r Imolicat ions:

It is usefi.d to compare diffusion parameters with conventional descriptions of geologic media.

Our ability to determine firm correlations is currently limited by the small number of samples and the

krge confidence bounds on ~& Nonetheless, it appears that ~ increases with bulk porosity and the

relative presence of certain microscopically visible features (fracturin~ vugginess, and gypsum-

fillina, whereas ~a does not appear to correlate with these parameters or the number of different

types of features present in a given sample (Ffemhg. 7998). Greater interconnectedness of the pore

space due to increased porosity and increased presence of kmgwporosity features likely leads to faster

average rates of diffusion relative to dead-end pores in which solqte becomes trapped (e.g., DyL!!r(i~e/z

and Cmg, 1989). Gypsum occurs in the Culebra within vugs and fracmres (Ho1, 1997),and may

sirnpl y be an indicator of interconnected fracture and vwg porosity. The apparent lack of correlation

between ad and macroscopiczdly visible features su<ggeststhzt ad may be controlled by variability in

pore geometry within these features and/or by micropore-scale (intergmnular or intercrystal]ine)

porosity variability.

Another motivation for laboratory-scale studies was to evaluate whether spatial scaling

da&XIShipS might eXkt. (h?2pafk)ll Of best-fit ~d Values from eXperilnellts at dlree spatial scales

(individual samples, bulk diffusion, and the results of previous field-scde tracer tests) suggests that ad

increases with sampling ~’olume (Ffcni~{<.199X). In our work on sample volumes in the range of 60

to 70 cmJ, the estimzted value of ~d is Oto 1. The bulk diffusion darz lun’e 2 combined sample

volume of 3.3 x 10? cmJ and have an estimated u~ of 1 to 1.2. S@e-well injection-withal raud tests

conducted at the same location as the samples were t.ken from [Me&.ratzdBea//ieti,itznwieu]had

Page 22: Modeling Solute Diffusion in the Presence of Pore-Scale

sample volumes of 2 x 10? m3 to 3 x 10~m3. l-f~ggc~ ‘eiu~.[~~zrw~cu.jestimated ~d on diffisicm rate

coefficients in these tests in the range of 2.5 to 7. Two-well tracer tests conducted at the same site

[kL-Kemzaet d., h retie~] on slightly larger sample volumes had estimated G, values of 5.5 [McKetzme~

al, in reu>u~,although a single-rare model also provided a good representation of the data. We note

that the estimates of ad at the field-scale also incorpomte the effects of ~m-iability in block-size in

addition to variability in Dp

The basic physical reasons for increasing o~ with sample volume are fairly clear. In general,

geologic materials are heterogeneous in most respects, and a greater range in the property of interest

is commonly found if a larger region is considered. As cd is a measure of heterogeneity in Dp withk

the volume of rock sampled, it may increxe as that sampling volume increases and a wider range of

DP is thus encountered. However, at least three conditions preclude determiwltion of a quantitative

relationship between spatial scale and mass transfer at this rime: (1) the small number of sampling

volumes for which Culebra n-nss transfer data are available (2) the samples used in the laboratory

diffusion experiments do not ftdly reflect the range of lithologies in the (ldebra; (3) the uncertainty

in block-size ~’ariabilit-yat the field-scale, the effects of which cannot currently he scpamted from

variability in DP

6, CO NCLUSIONS

..

An expression for solute diffkion in the presence of multiple simul ta.neous matrix

diffisivities, Dp was developed. This was then used to model data from eight labomtcmy-scale

diffusion experiments performed on five core samples (approximately 5 cm by 4 cm by 2.5 cm) of

the Culebra Member of the Rustler Fomxltiolr, a heterogeneous, fracrured, e~-aporitic dolomite. A

]ogyormal distribution of DOwas ;lssumed.

Our main conclusion are: (1) The estimated scmdard de~~iation (o,]) of ln(DJ) within each

Culebra dolomite sample ranges from O to 1. Nlost values lie herween 0.5 wxi 1, implying at least half

Page 23: Modeling Solute Diffusion in the Presence of Pore-Scale

an order of magnitude variation in DPwithin each small sample; and (2) The ~wiability over ail

samples leads to a combined Crdin the range of 1.0 to 1.2, which appears to be consistent with both

diffision results from the individual samples and a best-fit statistical distribution of formation factor

measurements for similar Culebra samples. The high observed degree of variability in mass transfer

rates within even such small volumes as these is of considerable significance to groundwater

remediation and geologic waste disposal issues.

Inferences with respect to geologic controls upon multirate mass transfer parameters should

be regarded as tentative at this time due to limited daw availzl)ility. Nonetheless, important

prelirninaq conclusions in this regard, which should serve as a focus for finure investigations, include

the following (3) Comparison of our estimation results to other rock properties suggests tha~ at the

lab-scale, the geometric mean of DPincreases with bulk porosity and the prevalence of macroscopic

porosity features such as fractures and vugs. This is attributed to increases in the interconnectedness

of the pore space; and (4) Comparison of our results with experiments at larger spatial scales suggests

that increasing sample volume resdts in an increase in ad. The VdUe of cd does not appear to be

correlated to bulk porosity or the prevalence of macroscopic porosity features, but may be

determined by variability within such macroscopic features and/or by micropore-scale heterogeneity.

ACKNOWLEDGEMENTS

We wish to thnk V. Tidwell, L. C. Meigs, R. M. HoIt, S. A. h4cKenna, A. R. Lzppin, and C. F.

Harvey for their comments and su=estions. We also appreciate the logistical support of M. J.

Kelley. This work was funded by Sandia Cmpcmition, a Lockheed Martin company, fc)r the United

States Department of Energy under Ccmtract DE-.AC04-94,%L85[100.

Page 24: Modeling Solute Diffusion in the Presence of Pore-Scale

Fleming & H~vrIY. F.fwlcling SCIILIIeciIlhIs&:I III tlIe prLwIIce oflmrr-scalr lICWmLTn&Iy ‘)7. -.

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Wood, W. W., Kmemer, T. F., and Heron P. P., J r. 1990. Intragmnuk- difthion: .4n impormntmechanism influencing solute transport in cl;lstic ;Iquifers? Science. 247(49.50), 1569-1.572.

Page 28: Modeling Solute Diffusion in the Presence of Pore-Scale

TABLE CAPTIONS

Table k Brief descriptions of Culebm dolomite samples used in the s~ltic diffision experiments,including bulk porosity (adapted from Ctkz>/iun-Fnwre[ al., 1997 and Tidwtl e[ uL,i~zpess).

Table 2 Results for single-rate md multirate pmarneter estimations. D? is the best-fit pore

diffusivity estimated using a conventional single-rate model. Values of M and ad are best-fitparameters of the lognomul distribution of pore diffusivity used in the multimte inversion. The value

M maybe compared to ln(DP). C@ity of the fits to the dam we described by the log-space rootmean square errors for both single-rote (SR) and multirate (MR) inversions. Out-diffisionexperiments were not conducted for samples RC4-D and RC6-G.

I ‘“’“’””-’“’””’””’’”’”””””:~....... .,-.

Page 29: Modeling Solute Diffusion in the Presence of Pore-Scale

Fkvnmg & Haggerty, Modeling .olutr difkiou in ilw presm)ce of pore-scale Iwtcrobm]wiry.

FIGURE CAP TIONS

Figure 1: Location map.

Figure 2: Scales and types of Culebra matrix porosity (from Hoi, 1997).

Figure 3: Mass uptake and recovery data. Figure 3.2: in-diffusion. Vertical axis gives the value of 1-

M@/M(l=m). Figure 3.b: out-diffusion. Vertical axis gives Al(~/M(t=O). Out-diffbsion experimentswere not conducted for sarnpies RC4-D and RC6-G.

Figure 4: Empirical and best-fit CDFS of formation factor. D~ta is for Culebra samples analyzed byTerraTek (HoL, 1997). Samples were taken from the H-19 hydropad, primarily borehole H-19 b4 (RBuuba”m,~cnona~mmmI{)uca~btz,1997); samples used in static difksion experiments were taken fromtbe same location. Best-fit lognorrnal CDF was determined by manual calibmtion and has ageomernc mean of 4.5 (corresponding to a formation factor of 90) and a standard devimion of 0.7.Earlier work at other locations at the \WPP site by Ke&yand SaAier (7990) also suggests thatformation factors in the Culebra dolomite are lognormall~7 distributed. Formation factors arecommonly taken to be inversely proportional to diffusivity (e.g.,Bear, 1972; Ke@ atzdSaw$zier,1990),so reasonably good quality of the fit su~sts that use of a lognormal distribution to approximate thetrue distribution of DP in the Culebra is appropriate. Calculations of DP from formation factors tendto be unreliable, due to the dependence of fommion factor measurements on the properties of theions present in tAe pore fluid and uncertainty in the precise form of the relationship bemveenformation factor and DP (see Kelly atzd.fawkierj 1990 for discussion). However, the standard

deviation of the lognormal distribution of fommtion C.lctors should be a good approximation to ~d inthe distribution of Ilk

Figure 5: Sensitivity analysis. Forward simulations were perfomled for the case of in-diffision.

Verdc~ a..is on both plots gives the value of 1-A4(r)/M(/=m). Figure 5.2: model responses for three

values of W; holding c$rJconstant at 1. Units of pd are hrl. Figure 5.LI:model responses for three

values of ad, holding ~ constant at –13; note that ~d=() corresponds to a conventional single-rate

model. The effects of variation in ad are far more prcmcmnccd at late times and for small values of

the mass ratio, relative to the effects c)fva:iation in pd.

Figure 6: Mass ratio datz md model responses. Best-fit curves were calculated using both aconventional single diffusivity (single-rate model) and a Iognormal distribution of diffusivities(multirate model). Figure 6.x in-diffusion fc)i~an~ple RC1-A. Vertical axis gives the value of 1-

M#)/M(t=@. Figure 6.b: out-diffision for bulk data. Vertical axis gives the value of A4(j)/A4@=O).

Page 30: Modeling Solute Diffusion in the Presence of Pore-Scale

Sample Q L Description

(cm)B33-H 0.15 5.5 .4bundant open \-ugsdirectly interconnected and/or

interconnected by fractures; some qpsurn-filling of rugs. h4ajorporosiw tvpes = interc~stalline. vu,~ . and fractures.

RC1-A 0.13 4.9 Relativelyuniform; single faint lasnin~ minor micro~-ugsand<micro fmctures. hl~jor porositv t-vpes = intercwstdline.

RC2-B 0.09 6.6 Distinct fracture spanning half the length of the s.arnple. Majorporosi~ tvpes = Intercqstdline and fractures.

RC4-D 0.09 5.8 Faint laminations; minor vuggy porosity sc~ttered throubfiou~minor microfmctures. hfajor porosiw tvpes = intercm>stalline.

RC6-G 0.12 6.2 Abundant large (0.025 to 2.0 cm) vugs; abundant fractures;

considerable gypsum-filling of fractures and vugs. h4ajor porositytvpes = intercmstdline, fmctures. and vugs.

Table 1

.

.

Page 31: Modeling Solute Diffusion in the Presence of Pore-Scale

Test DP [mZ/hr] J&d* 2G ad RMSESR ~SE&m

inpp) i 20 h(~d) k ~~

range range range

B33-H in 4.78E-06 .1 ~.() * o.~~~ 0.598 0.730 0.510-1~~ y I)J30 -0.514k 0.0610

3.80E-06, 6.02E-06” -11.8, -12.2 0.563,0.636B33-H out ~.64&06 -11.7 * 3.14 0.946 5.78 3.01

-12.821.15 -0.055522.128.74E-07, 8.72E-06 -8.56, -14.8 0.11+7.88

RC1-A in 1.Wq)(j -13.5 k 0.3-$4 0.938 Q34j 0.169

-13.6 k0.196 -0.0-/29 k 0.8921.00E-06, 1.51E-06 -13.2, -13.8 0.393.2.34

RC1-A out 4.96E-07 -14.5 &0.276 0.560 i3~18 0.163-14.5 ~0.178 -0.580 k 1.73

4.2U3-07, 6.03E-07 -14.2, -14.8 0.0997,3.16RC2-B in 1.49E-06 -13.4 k 0.334 0.666 0.161 0.157

-13.4 do.195 -0.407 i2.081.~jE-06, 1.ME46 -13.1.-13.7 0.0832.5.33

RC2-B out 1.30E-06 -13.5 * 0.240 0.00590 o.~7j 0774

-13.6 Y0.161 -5.13 Y 222E+&1.06E-06, 1.46E-06 -13.3, -13.7 0.()(), m

RC4-D in 9.75E-07 -13.9 k0.622 0.988 ()~ql 0.739

-73.8 ? 0.340 -0.0121 h2.067.23E-07, 1.43E-06 -13.3 .-14.5 Q.126,7.75

RC6-G in 3.66E-06 -12.5 * 0.496 0.0369 0.516 0.517-12,j k 0~7-f -3.30 Y 472

2.83E-06, 4.90E-06 -12.0, -13.0 0, m

Bulk in 2.15E-06 -13.0 f 0.194 0.976 0.?53 0.152-13.1zf O.198 -0.0243 k 0.0178

1.6fiE-06, 2.49E-06 -128, -13.2 0.959,0.994Bulk out 1.15E-06 -13.2 * 0..5.52 1.~[) 1.[)2 0.49.5

-13.7 f0.496 O.18.?&0.6526.84E-07, 1.84E-06 -12.6, -13.8 0.6?5 ~ 30- , -..

-,

Table 2

. . . .. .. . ., . .. .

L

Page 32: Modeling Solute Diffusion in the Presence of Pore-Scale

#

Newt.4exico

/Albuquerque

i+

WIPP

Carisbad ~ )r..

-..\

u

. Locations of SWiwTracer Tests

WIPP SheBoundary

r

,,,:7si’Ov-, ..*.. .s

● H-19

I H-no

o 1 2 miI

1 I

o 2 km

-SW”<

Figure 1

. .... . . -,, .,, . .. ... . . . . . .,—..— . . ., -. ... .

Page 33: Modeling Solute Diffusion in the Presence of Pore-Scale

Fleming & H~rty. Modeiing solute d, ffusion in dIe im.sel}ce of pore-scale Iwterogclwity

1.5m

1.0

0.5

0.0

1.5 \

Porosity Types:

fracturesVugsintercrystallineinterparticleintraparticle

Figure ‘2

10.3 m

0.2

0.1

0.0

0.3

I60 mm

40

20

0

60

I50 pm

25

0

50

31

.

TRI-6!15.5i4.0

Page 34: Modeling Solute Diffusion in the Presence of Pore-Scale

.

1

Mass Ratio

[-1

0.1

Figure S.a

E

1

0

‘e

‘s

0

0

. 333-I-I● RC1-Aa RC2-B. RC4-D. RC6G

.0

.’●

0.

.

.

G

o

c’

10 100

time [hr]

1000

Mass Ratio

H

1:

0.1 -

E

0

0

0..

0●

.

_---l0 B33-I-1 o 0● RC1-.4 ..0 RC?-B o

60.00

0.01 I

10 100 1000

time fllr]

32

. .. . .. . .

Page 35: Modeling Solute Diffusion in the Presence of Pore-Scale

1

CDF [-]

c

..

...

.

.

10 100 1000

formotion fnctor [-]

Figure 4

33

Page 36: Modeling Solute Diffusion in the Presence of Pore-Scale

Fleming & Haggc~, AfOdcling solute diffusiot, in tile prcsmtce of pore-scale hctc.ro~,,rily. ..

Mass Ratio

[-1

o. I

i

1~1

\\

\

\

\

\

0.1

Mass Ratio

[-1

— - Jld=-lz

— pd. -13

. . . . . yd=-l~

10

\

100 1000

—- Gd= o

Csd= 1

. . . . . Gd= ~

\

\

\

\0.01

10 100 1000

time Plr]

Figure 5.b

34

..

.

. ... .. .. .. . ... . .. .. . .. . .--, .. .. .. . . . . .. . .. .. . .

Page 37: Modeling Solute Diffusion in the Presence of Pore-Scale

FIeming & H~rty, Modehg soluIe diffusiO!l in the prcw,cc of pore.scak lwterogcnci(y. ..

1.0

0.9

0.8

0.7

0.6

Mass Ratio 0.5

[-10.4

0.3

0.2

0 ●.

\

\

\

L-Jmullira[e

— - single-rate. Olxcrved

1 10 100 1000,.

time [hr]

Figure G.a

Page 38: Modeling Solute Diffusion in the Presence of Pore-Scale

1

Mass Ratio

[-1

0.1

-.. .●

— multira[e

‘- single-rate

● ob served

, i10 100 1000

time (hrl

36

Fig=re ~.b