optical emission spectrometer –spark emission · simultaneous thermal analysis –tga + dsc •...

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Optical Emission Spectrometer – Spark emission determination of all in the metal industry required elements including traces of carbon, nitrogen, sulfur and phosphorus for the relevant matrices (base metals), like Fe, Ni, Al, Cu, Mg und Ti Simultaneous Thermal Analysis – TGA + DSC up to 1550 C NETZSCH Jupiter F3 argon, argon/ hydrogen, nitrogen, air DSC analysis possibilities: Melting/crystallization behavior Solidsolid transitions Oxidative stability Purity Determination Specific heat γ‐TiAl Specific heat TG analysis possibilities: Mass changes Temperature stability Oxidation/reduction behavior Decomposition Corrosion studies Compositional analysis balance system iron T Curie α→γ γ→δ melting Dilatometer temperature 10 l Linseis L75 MoSi 2 + 35% ZrO 2 400 600 800 1000 1200 l Oxi temperature [°C] l Temp 4 6 8 l [%] sample rod 0 500 1000 1500 0 200 time [s] 0 2 up to 1500°C atmosphere: inert, reducing, oxidizing sample rod

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Page 1: Optical Emission Spectrometer –Spark emission · Simultaneous Thermal Analysis –TGA + DSC • up to 1550 C NETZSCH Jupiter F3 ... 3/16/2016 1:52:18 PM

Optical Emission Spectrometer – Spark emission

• determination of all in the metal industry required elements

• including traces of carbon, nitrogen, sulfur and phosphorus

• for the relevant matrices (base metals), like Fe, Ni, Al, Cu, Mg und Ti

Simultaneous Thermal Analysis – TGA + DSC

• up to 1550 C

NETZSCH Jupiter F3 

• argon, argon/ hydrogen, nitrogen, air

DSC analysis possibilities:• Melting/crystallization behavior• Solid‐solid transitions• Oxidative stability• Purity Determination• Specific heat

γ‐TiAl

• Specific heatTG analysis possibilities:• Mass changes• Temperature stability• Oxidation/reduction behavior• Decomposition• Corrosion studies• Compositional analysis

balance system

iron

TCurie

α→γ γ→δ

melting

Dilatometer 

 temperature

10 l 

Linseis L75 MoSi2 + 35% ZrO2

400

600

800

1000

1200

lOxi

temperature [°C]

lTemp

4

6

8

l [%]

samplerod

0 500 1000 1500

0

200

time [s]

0

2• up to 1500°C• atmosphere: inert, reducing, oxidizing

samplerod