preparation of polymer samples for microspectroscopy€¦ · preparation of polymer samples for...
TRANSCRIPT
![Page 1: Preparation of Polymer Samples for Microspectroscopy€¦ · Preparation of Polymer Samples for Microspectroscopy Kristen Wiley Senior Cleanroom Microscopists, McCrone Associates](https://reader033.vdocuments.net/reader033/viewer/2022053008/5f0c52ab7e708231d434d41b/html5/thumbnails/1.jpg)
Preparation of Polymer Samples for MicrospectroscopyPreparation of Polymer Samples for MicrospectroscopyKristen WileySenior Cleanroom Microscopists, McCrone AssociatesAugust 27, 2015
![Page 2: Preparation of Polymer Samples for Microspectroscopy€¦ · Preparation of Polymer Samples for Microspectroscopy Kristen Wiley Senior Cleanroom Microscopists, McCrone Associates](https://reader033.vdocuments.net/reader033/viewer/2022053008/5f0c52ab7e708231d434d41b/html5/thumbnails/2.jpg)
Thank You for Joining Us.The Webinar Will Begin Shortly.
The premier microscopy resource, combining the talents and skills of its staff in the areas of materials analysis,
instrument sales, and education.
The McCrone GroupThe McCrone Group
![Page 3: Preparation of Polymer Samples for Microspectroscopy€¦ · Preparation of Polymer Samples for Microspectroscopy Kristen Wiley Senior Cleanroom Microscopists, McCrone Associates](https://reader033.vdocuments.net/reader033/viewer/2022053008/5f0c52ab7e708231d434d41b/html5/thumbnails/3.jpg)
EDUCATION & TRAINING
Hooke College of Applied SciencesHooke College of Applied Sciences
Light Microscopy Microspectroscopy
Electron Microscopy Sample Preparation
Scheduled Courses and Custom Training
![Page 4: Preparation of Polymer Samples for Microspectroscopy€¦ · Preparation of Polymer Samples for Microspectroscopy Kristen Wiley Senior Cleanroom Microscopists, McCrone Associates](https://reader033.vdocuments.net/reader033/viewer/2022053008/5f0c52ab7e708231d434d41b/html5/thumbnails/4.jpg)
INSTRUMENT SALES
McCrone Microscopes & AccessoriesMcCrone Microscopes & Accessories
Linkam Thermal Stages Laboratory Supplies
JEOL NeoScope Benchtop SEM Digital Imaging Systems
Nikon Microscopes and Measuring Equipment
Trusted Advisors to Scientists Worldwide
![Page 5: Preparation of Polymer Samples for Microspectroscopy€¦ · Preparation of Polymer Samples for Microspectroscopy Kristen Wiley Senior Cleanroom Microscopists, McCrone Associates](https://reader033.vdocuments.net/reader033/viewer/2022053008/5f0c52ab7e708231d434d41b/html5/thumbnails/5.jpg)
Our team solves your most complex particle identification problems
Experienced Industry Professionals
MATERIALS ANALYSIS
McCrone AssociatesMcCrone Associates
![Page 6: Preparation of Polymer Samples for Microspectroscopy€¦ · Preparation of Polymer Samples for Microspectroscopy Kristen Wiley Senior Cleanroom Microscopists, McCrone Associates](https://reader033.vdocuments.net/reader033/viewer/2022053008/5f0c52ab7e708231d434d41b/html5/thumbnails/6.jpg)
ISO 14644 Class 5 Cleanroom
![Page 7: Preparation of Polymer Samples for Microspectroscopy€¦ · Preparation of Polymer Samples for Microspectroscopy Kristen Wiley Senior Cleanroom Microscopists, McCrone Associates](https://reader033.vdocuments.net/reader033/viewer/2022053008/5f0c52ab7e708231d434d41b/html5/thumbnails/7.jpg)
Polymers Polymers Different Forms
Wikipedia.com
![Page 8: Preparation of Polymer Samples for Microspectroscopy€¦ · Preparation of Polymer Samples for Microspectroscopy Kristen Wiley Senior Cleanroom Microscopists, McCrone Associates](https://reader033.vdocuments.net/reader033/viewer/2022053008/5f0c52ab7e708231d434d41b/html5/thumbnails/8.jpg)
Preparing Polymer Samples for FTIRPreparing Polymer Samples for FTIR
Rubber Stoppers Plastic Shavings
![Page 9: Preparation of Polymer Samples for Microspectroscopy€¦ · Preparation of Polymer Samples for Microspectroscopy Kristen Wiley Senior Cleanroom Microscopists, McCrone Associates](https://reader033.vdocuments.net/reader033/viewer/2022053008/5f0c52ab7e708231d434d41b/html5/thumbnails/9.jpg)
MethodsMethods
Selection of the appropriate sampling method is critical to achieving good results!
![Page 10: Preparation of Polymer Samples for Microspectroscopy€¦ · Preparation of Polymer Samples for Microspectroscopy Kristen Wiley Senior Cleanroom Microscopists, McCrone Associates](https://reader033.vdocuments.net/reader033/viewer/2022053008/5f0c52ab7e708231d434d41b/html5/thumbnails/10.jpg)
• Are made from a large cover glass Micro Cover GlassesMicro Cover Glasses
![Page 11: Preparation of Polymer Samples for Microspectroscopy€¦ · Preparation of Polymer Samples for Microspectroscopy Kristen Wiley Senior Cleanroom Microscopists, McCrone Associates](https://reader033.vdocuments.net/reader033/viewer/2022053008/5f0c52ab7e708231d434d41b/html5/thumbnails/11.jpg)
Micro Cover GlassesMicro Cover Glasses
![Page 12: Preparation of Polymer Samples for Microspectroscopy€¦ · Preparation of Polymer Samples for Microspectroscopy Kristen Wiley Senior Cleanroom Microscopists, McCrone Associates](https://reader033.vdocuments.net/reader033/viewer/2022053008/5f0c52ab7e708231d434d41b/html5/thumbnails/12.jpg)
• Are made from a glass slideGlass WedgeGlass Wedge
![Page 13: Preparation of Polymer Samples for Microspectroscopy€¦ · Preparation of Polymer Samples for Microspectroscopy Kristen Wiley Senior Cleanroom Microscopists, McCrone Associates](https://reader033.vdocuments.net/reader033/viewer/2022053008/5f0c52ab7e708231d434d41b/html5/thumbnails/13.jpg)
Glass WedgeGlass Wedge
1mm
![Page 14: Preparation of Polymer Samples for Microspectroscopy€¦ · Preparation of Polymer Samples for Microspectroscopy Kristen Wiley Senior Cleanroom Microscopists, McCrone Associates](https://reader033.vdocuments.net/reader033/viewer/2022053008/5f0c52ab7e708231d434d41b/html5/thumbnails/14.jpg)
Micro ToolsMicro ToolsSmall particles require small tools
• Tungsten needle
• Carbide scribe
• Curved forceps
• KBr holder
![Page 15: Preparation of Polymer Samples for Microspectroscopy€¦ · Preparation of Polymer Samples for Microspectroscopy Kristen Wiley Senior Cleanroom Microscopists, McCrone Associates](https://reader033.vdocuments.net/reader033/viewer/2022053008/5f0c52ab7e708231d434d41b/html5/thumbnails/15.jpg)
Micro KBr CrystalsMicro KBr Crystals• Purchased as 1” x 1” x 4mm crystal
![Page 16: Preparation of Polymer Samples for Microspectroscopy€¦ · Preparation of Polymer Samples for Microspectroscopy Kristen Wiley Senior Cleanroom Microscopists, McCrone Associates](https://reader033.vdocuments.net/reader033/viewer/2022053008/5f0c52ab7e708231d434d41b/html5/thumbnails/16.jpg)
![Page 17: Preparation of Polymer Samples for Microspectroscopy€¦ · Preparation of Polymer Samples for Microspectroscopy Kristen Wiley Senior Cleanroom Microscopists, McCrone Associates](https://reader033.vdocuments.net/reader033/viewer/2022053008/5f0c52ab7e708231d434d41b/html5/thumbnails/17.jpg)
![Page 18: Preparation of Polymer Samples for Microspectroscopy€¦ · Preparation of Polymer Samples for Microspectroscopy Kristen Wiley Senior Cleanroom Microscopists, McCrone Associates](https://reader033.vdocuments.net/reader033/viewer/2022053008/5f0c52ab7e708231d434d41b/html5/thumbnails/18.jpg)
Results??? To Be Continued:Results??? To Be Continued:
![Page 19: Preparation of Polymer Samples for Microspectroscopy€¦ · Preparation of Polymer Samples for Microspectroscopy Kristen Wiley Senior Cleanroom Microscopists, McCrone Associates](https://reader033.vdocuments.net/reader033/viewer/2022053008/5f0c52ab7e708231d434d41b/html5/thumbnails/19.jpg)
Are There Any Questions??Are There Any Questions??
![Page 20: Preparation of Polymer Samples for Microspectroscopy€¦ · Preparation of Polymer Samples for Microspectroscopy Kristen Wiley Senior Cleanroom Microscopists, McCrone Associates](https://reader033.vdocuments.net/reader033/viewer/2022053008/5f0c52ab7e708231d434d41b/html5/thumbnails/20.jpg)
Kristen Wiley and Heidi TaleskySenior Cleanroom Microscopists
[email protected] • [email protected] •(630) 887‐7100
Thank you for joining us.