hwbdocuments.env.nm.gov semiconductors/2003-06-… · 11/06/2003 · sangre de cristo sciences,...

Sangre De Cristo Sciences, LLC

June 11, 2003

Mr. Joe Mauser Philips Semiconductors, Inc. 9201 Pan American Highway NE Albuquerque, NM 87113

9012 Washington NE • Albuquerque NM 87113-2704 (505) 822-8061 • Fax (505) 822-8063

~ENTERED

Re: April 2003 Annual Groundwater Monitoring Results

Philips Semiconductors Albuquerque Facility

Dear Joe,

The following information outlines the events as they took place by Sa11gre De Cri.i;to Sciences, LDC. On April 22 & 23, 2003 representatives from Sangre De Cristo Sciences, LLC (SDC"l, LLl) performed the annual monitoring of 13 groundwater wells on Philips Semiconductors site and on off site NCLF city wells. Five wells at the Philips site, MW-1, MW-2, MW-4, MW-5 & MW-6, and eight wells at the former Nazareth Colorado Landfill (NCLF-2, 3, 4, 5, 6, 7, 8 & 9) were measured for groundwater levels, purged and sampled pursuant to the protocol as listed in the statement of work provided by Philips

Semiconductors.

Mr. Joe Mauser of Philips Semiconductors provided access and direction for the sampling event, while Mr. Scott Pratt and Mr. Elvin Chavez of SJ>Ct:.;, /,LC conducted the groundwater monitoring in accordance with the scope of work. All wells were sampled with a new stainless steel Grundfos Rediflo 2 pump, reel and PTFE tubing. Wells were sampled in order of cleanest or least contaminated to dirtiest or those with higher concentrations of contaminants. Field notes are included as Attachment I.

Methods

The groundwater levels were checked in a1113 monitor wells, measured from the top of each well casing and total well depths were used to calculate the required 3 well volumes for purging. Measurements for the previous event, January 2003, and the current April are illustrated in Table 1. Water levels were slightly lower than those taken in January possibly due to limited precipitation and drought conditions.

Throughout the sampling event and purging of all 13 wells, SDlS, LLC personnel monitored water quality parameters (pH, conductivity and temperature) and recorded all results in field activity logbooks provided by Philip Semiconductors.

The thirteen wells were purged and sampled using a new Grundfos Rediflo 2 stainless steel pump, reel and tubing, which has been dedicated to this project only. Three well

casing volumes were purged and water quality parameters allowed to stabilize prior to collecting groundwater samples for analysis. NCLF-9 was purged dry on April 22, 2003, allowed to recharge overnight, and a sample was collected on April 23, 2003.

All samples were collected in appropriate containers provided by .\ssaigai Analytical I ,<1hornlories, Inc. (,\c\U) of Albuquerque, NM. Samples were labeled, filled and stored in a cooler, on ice and delivered to AA LI with the required chain of custody.

Laboratory Analysis

The groundwater samples were analyzed for Volatile Organic Compounds by USEP A 524.1 and 504.1, Semi volatile Organic Compounds including PAH by USEPA 8270, Pesticides by USEPA 8081A, PCB by USEPA 8082 and Total Metals by USEPA 6010 (ICP-AES) and USEPA 6020 (ICP-MS). All laboratory analytical results, chain of custody forms and QNQC reports are supplied as Attachment 2.

Data Quality Assessment

has reviewed the analytical reports for compliance with data quality objectives, holding times, method requirements, surrogate recoveries, MS & MSD recoveries and their associated RPD. All parameters were performed in strict accordance within holding times and USEP A method requirements and were found to meet all criteria. Trace concentrations of Volatile Organic Compounds (VOC), Semi volatile Organic Compounds (SVOC) and metals were detected in some of the samples, but were below Maximum Contaminant Levels (MCL) as listed in the tables provided by Philips Semiconductors. Trace levels of phthalates were detected but below standards. Phthalates can be attributed to the DI water and decontamination solution being stored in Poly containers. However, these trace amounts do not affect the acceptability or usability of the data set.

Laboratory Results and QA/QC Report

The analytes detected during the April 2003 annual groundwater-monitoring event are listed in Table 2 along with MCL's. The VOC's of concern detected were Tetrachloroethylene, (PCE), Freon 12, and trichloroethene in wells MW-1, MW-2, MW-4, MW-5, MW-6, NCLF-2, 3, 4, 6, 7, 8 & 9. In addition, no pesticides, PCB, PAH or BAP were detected in any of the groundwater samples, and the only metals detected were trace levels, some at the detection limit, of chromium, copper, barium, lead, selenium, and zinc. Trace metals detected appear to be well below their respective MCL. The attached QNQC report shows all associated QC including method blanks, Laboratory Control Sample (LCS & LCSD), Matrix Spikes (MS & MSD) and all supporting statistical data.

, appreciates the opportunity to work for you and Philips Semiconductors and looks forward to continued business with you. If you should have any questions or comments regarding this report or event, please feel free to contact me at (505) 259-9795.

,ctfu. lly ;ubmitted,

~(Ii~ Elvin J. Chavez

President

Philips Semiconductors Environment Department

Analytical Report

For

April 2003 Annual Monitoring Event

Prepared By:

Sangre De Cristo Sciences, LLC

Figure 1- Site Map

Philips Semiconductors 2002 Groundwater Monitoring - Scope of Work

12. Figures 12.1 Site Map

A 5

MW-7

North .__.___.___. _ _.___ I

Pasadena Ave. ~~~~~~·1r

NCLF-6 Albuquerque ~-----~ ...... +i--!-__ ,,_,.... __ .._-+--1--

Sumitomo Sitix

Silicone Inc.

Acres

__ NCLF_-===5

• =====-~-"oi~~~--o~~"·r1~1 =-I=/ ----

& MW-6

· ·f<19le Rock Ave.

L ~CLf-7 ! ... Oaklard Ave. · ·

61 PHILIPS

ve.

Tables 1 & 2

April 2003 Groundwater Depths and Detected Analytes

Table 1. Depth to Groundwater in Philips Semiconductor Monitor

Wells for January 2003 and April 2003 events

Monitor Well # January 2003 April 2003 Difference in Levels Levels Elevation

MW-1 NIA 212.1

MW-2 NIA 199.45

MW-4 NIA 227.6

MW-5 217.9 218.1 -0.20

MW-6 238.93 239.1 -0.17

NCLF-2 NIA 201.6

NCLF-3 NIA 207.2

NCLF-4 NIA 246.3

NCLF-5 NIA 166.5

NCLF-6 NIA 173.5

NCLF-7 212.15 212.2 -0.05

NCLF-8 208.12 208.2 -0.08

NCLF-9 266.07 266.05 0.02

MW

1

Tetrachloroethylene 3.7

(PCE),ppb

Trichloroethene, <0.1

ppb

Frecm-12, ppb <0.1

Bromofonn, ppb 0.54

Bromodichloromethane <l

ppb

Chrornimn (rng'L) 0.04

Barimn ( rng'L) 0.545

V anadimn (rng'L) 0.009

Lead (rng'L) 0.022

Nickel (rng'L) 0.025

Selenimn (miefl) <0.001

Zinc ( rng'L) 0.167

+

Table 2. Detected Analytes in Philips

Semiconductor Monitor Wells for April 2003 MW MW MW MW NCLF NCLF NCLF NCLF

2 4 5 6 2 3 4 5

2.1 2.4 <0.1 0.34 5.3 3.1 2.0 0.14

<0.1 <0.1 <0.1 <0.1 <0.1 <0.1 0.18 0.12

<0.1 0.86 <0.1 <0.1 <0.1 0.22 0.63 <0.1

2.8 0.31 <] <I 0.25 0.13

0.39 <I <l <l

0.02 <0.01 <0.01 <0.01 <0.01 0.02 <0.01 <0.01

0.290 0.172 0.148 0.090 0.087 0.121 0.031 0.171

0,01 0.002 0.001 <0.001 0.002 0.001 <0.001 0.002

0.048 0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001

0.013 0.007 0.003 0.001 0.002 0.022 0.010 0.001

0.001 0.001 <0.001 <0.001 0.001 0.003 0.010 0.002

0.257 0.021 0.009 0.003 0.024 0.014 <0.005 <0.005

Red items Denote Analytes over MCL

NCLF NCLF NCLF NCLF MCL•

6 7 8 9

1.8 1.4 2.2 0.68 5.0 ug/L (ppb)

<0.1 <0.1 <0.1 <0.1 lOOug/I (ppb)

<0.1 <0.l <0.1 0.40 1000 ug/1

0.14 0.18 <l <I

<l <]

<0.01 <0.01 <0.01 0.08 0.05 mg/L

0.084 0.143 0.118 0.177 1.0 mg/L

0.003 0.003 <0.001 0.004 0.020 mg/L

<0.001 <0.001 <0.001 0.004 0.015 mg/L

0.002 0.002 0.010 0.055 1.0 mg/L

<0.001 0.001 <0.001 0.003 0.05 mg.IL

0.016 <0.005 <0.005 0.107 5.0 mg/L

Attachment 1 - April 2003 Field Activity Notes

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Attachment 2 - April 2003 Laboratory Report -QA/QC Report

Client:

Project:

Order:

Sample:

ASSAIGAI ANALYTICAL LABORATORIES, INC. 4301 Masthead NE • Albuquerque, New Mexico 87109 • (505) 345-8964 • FAX (505) 345-7259

3332 Wedgewood, E-5 • El Paso, Texas 79925 • (915) 593-6000 • FAX (915) 593-7820 127 Eastgate Drive, 212-C • Los Alamos, New Mexico 87544 • (505) (>62=2558 ___________ _

PHILIPS SEMICONDUCTORS attn: JOE MAUSER 9201 PAN AMERICAN FRWY NE ALBUQUERQUE NM 87113

PHILIPS SEMICONDUCTORS

APRIL 03 SAMPLE EVENT

0304502 PHl16 Receipt:

Assaigai Analytical Laboratories, Inc.

Certificate of Analysis

04-24-03

1 Explanation of codes

B ' analyte detected in Method Blank

E result is estimated

H analyzed out of hold time

N---" __ te_~tatively identified compound s '

I subcontracted ! - - ------ -- -- -------- - ------------1

1-9 ! see footnote , -- - ___________________ I

STANDARD

~_dr__ aigai Analytical Laboratories, Inc.

-----

MW-#5 Collected: 04-23-03 15:00:00 By: SP

·Matrix: GW

.QC Group

'0304502-01 A X03206

X03206

X03206

X03206

•X03206

, X03206

X03206

X03206

X03206

__ X03206

-·X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

,,X03206

'X03206

X03206

X03206

X03206

X03206

Run Sequence

XG.2003.817.6

XG.2003.817.6

XG.2003.817.6

XG.2003.817.6

XG.2003.817.6

XG.2003.817.6

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XG.2003.817.6

XG.2003.817.6

XG.2003.817.6

XG.2003.817.6

XG.2003.817.6

XG.2003.817.6

--- - ----· --··--

Dilution Detection Prep Run

CAS# Analyte Result Units Factor Limit Code Date Date

EPA 524.2 rev 4 Purgeable VOCs by GC/MS By: JAA 75-34-3 ! 1, 1 Dichloroetha~e ___ - - NIJ- -- -1-~-9 IL

1

. o~i

75:3s=4r-----i-:1-oicil10r-0ethene-----,-- N6----;--ugTL. ________ 0.1

_i~~5-6=I _____ 1,_1__,_1_2~-~loroeth_~n_E! ___ -~ _:_~-[)~--~__LJ2_1 ~ _ L 0.1

630-20-6 1, 1, 1,2 Tetrachloroethane__J__ _f'J_[)_ j ug I L j _ _ _____ _D_:_1 __

79-_o?~~-~- _ ~0~Trich~o~~ltl~flE!_~ND _ _j_~QLL ; 79-34-5 : 1, 1,2,2 Tetrachloroethan~--- _ ND 1

1

ug IL L __ 1 __ _

563-58-6 I 1, 1-Dichloropropene ND ug I L I 1 0.1 n 106-93-4 I 1,2 Dibromoethane (EDB) I ND ! ug IL - i- - := __ 0 ___ 1 ___ _J_ ______ _

95-50-1 1,2 Dichlorobenzene i ND I ug I L 0.1 107-06-2 i 1,2 Dichloroethane (EDC)-- - --ND--! -ug IL --- I o. i ------

--- 1

05-07-03 05-07-03

05-07-03 05-07-03

05-07-03 05-07-03

05-07-03 05-07-03

05-07-03 05-07-03

05-07-03 05-07-03

05-07-03 05-07-03

05-07-03 05-07-03

05-07-03 05-07-03

05-07-03 05-07-03 Y8-87-=5_! _____ i~2 Dichloropropane N~-,-~-g-/ L -~ ----0.1 - ---;:;-:;--t---------------- --+------ ---- - -- - ------- --96-18-4 · 1,2,3 Trichloropropane I ND ug IL 0.1

05-07-03 05-07-03

05-07-03 05-07-03 87-61-6 1,2,3-Trichlorobenzene 1 ND - --ugJL___ -1-- ' 0.5 - ------

-----1 ---- -------------i----------------t- --~---

~250~~~~~- _ ;,-:.-:~~;ii~:~~~I~:~::~: -f--~f----~+----+~-~----~i-=-~~=~ 59461--~;~1 ~~~~~~~~~o!a~---~ ~N~D ~! -~ugg~;/ ~L- tf ~1 J __ ~o-_~1 1-108-67-8 1,3,5-Trimethylbenzene

142-28-9 1,3-Dichloropropane ND I ug IL _ 1 _ ---- 0.2_ - -~ 106-46-7 1,4 Dichlorobenzene ! ND I ug I L I 1 0.1 I ' ~- --- - --------- ------------ ------------ f J --,--- - -----;-- -----1 99-87-6 1,4-lsopropyltoluene · ND ug IL 0.1 -

2,2-Dichloropropane ~-__ NE_- !-ug~/ L - ________ ~~2- ~ -. -- -

__ _3_-:_C_tilorc:t~~~e j N[)_ _ug/_~---- 0.1

594-20-7

95-49-8

05-07-03 05-07-03

05-07-03 05-07-03

05-07-03 05-07-03

05-07-03 05-07-03

05-07-03 05-07-03

05-07-03 05-07-03

05-07-03 05-07-03

05-07-03 05-07-03

05-07-03 05-07-03

05-07-03 05-07-03

05-07-03 05-07-03

106-43-4 4-Chlorotoluene ND ug IL 0.1 05-07-03 05-07-03

REPRODUCTION(J:\15\ft!#§ WOJ:r ~mHAN PJ.!tJ..(P.f:Ql1@@:~ IJB!lOO-ITIEN CONSENT OF AAL Report Date THIS REPORT MAY NOT BE USED IN ANY MANNER BY THE CLIENT OR ANY OTHER THIRD PARTY TO CLAIM

PRODUCT ENDORSEMENT BY THE NATIONAL VOLUNTARY LABORATORY ACCREDITATION PROGRAM.

STANDARD'.



Client:

Project:


APRIL 03 SAMPLE EVENT Order: 0304502 PHl16 Receipt: 04-24-03

Sample: MW- #5

Matrix: GW

QC Group

0304502-01A X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

0304502-01 8 X03200

X03200

0304502-01 c X03165

X03165

Page 2 of 27

Run Sequence

XG.2003.817.6

XG.2003.817.6

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XG.2003.817.6

XG.2003.817.6

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XG.2003.817.6

XG.2003.817.6

XG.2003.817.6

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XG.2003.817.6

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XG.2003.817.6

XG.2003.817.6

XG.2003.817.6

XG.2003. 727.14

XG.2003.727.14

XG.2003. 703.12

XG.2003. 703.12

--------------Collected: 04-23-03 15:00:00 By: SP

-···---·----~·-----

Dilution Detection

CAS# Analyte Result Units Factor Limit Code

EPA 524.2 rev 4 Purgeable VOCs by GCIMS By: JAA ------~----------·-~--------------------~

71-43-2 Benzene ND I ug IL ! 1 0.1 ___ i=. ----~. 108-86-1 Bromobenzene ND I ug IL 1 1 0.1 J__

Bromochloromethane ! NNDD __ .: __LJu_\l_g 11

LL L__1__1

--+;' ____ 0o:._

11_

75-27-4

---,S--2-5--2-----4---- Bromoform - ND- ~- -u~- ~ ~ --1~--- __ L~r-o~ 1 __ -_-_-_- :

74-83-9 Bromomethane ND ! ug IL I 1 1

0.6 1

Bromodichloromethane I 1

-150-6~-~9-~-~'.-,1-1 -___ C_a_~_bho-1 :-r-~eb-t:_:_~-:-l~-:-de-- - - T ~~ !--~~~-~----~-~- ~ ~- --t---· -·-

~25~~:~~1 ! Chlor~~::~::~;ne;hane ~~ -T ~~ ~ ~ I ~ . r·--%. ~ I

67-66-3

74-87-3

156-59-2

c~:::~::.:,. I ~~ + ::;~ 1-: I ~:--c -· -,~:·~::::~:~:?o::,·· I ~LJ :n 1 ~ _, J~ -=-10061-01-5

74-95-3

100-41-4 Ethylbenzene ! ND I ug I L 0.1 1

I

75-71-8 Freon 12 --- --r~ND I ug IL r--1-- - 0.1 t - -1 87-68-3 ____ H_e_x_a_c-hl-orobutadiene I ND --ugTL T--1--i--0.1--t---- i

~::-~:-::-+--- ::i~~~~~~b:~~~~: ~~ ~F$R=- ~-- -r~~~=: 91-20-3 Naphthalene J ND ug IL 1 1

104-51-8 n-Butylbenzene ND ug IL 1 0.1 ·---1~

i 103-65-1 n-Propylbenzene ND ug IL f-----------------------+--~---+-----~--

!-- 95-47-6 a-Xylene ND --+--ug_l_L_ 1

108-38- p/m-Xylenes ND ug IL r---3/106-42

0.1

0.1

0.2

Prep Run

Date Date

05-07-03 05-07-03' >.,,.

05-07-03 05-07 -03

05-07-03 05-07-03·-··

05-07 -03 05-07 -03/

05-07 -03 05-07 -03 ,•

05-07-03 05-07-03·.

05-07 -03 05-07 -03"' "'" 05-07 -03 05-07 -03 !'"·'

05-07 -03 05-07 -03'•"

05-07 -03 05-07 -03'"

05-07-03

05-07-03

05-07-03

05-07-03

"'<l,O-y

05-07-03 .. 05-07-03'-•'>'·

o5-o7 -ot'· · '~ti'"

05-07-03.~

05-07-03 05-07-03''

05-07-03 05-07-0Z.

05-07 -03 05-07-03,'

05-07 -03 05-07-03' •

o5-07-03 05-07-o{ ~,;,

05-07-03 05-07 -03,. .

05-07 -03 05-07 -03~'"' ,..... 05-07-03 05-07-02,,,_ •

05-07 -03 05-07 -03'.·

05-07-03 05-07-03"'' ,.. 05-07 -03 05-07 -o: .....

,. 135-98-8 sec-Butylbenzene ND ug IL r-- 0.1 05-07-03 05-07-0::.,.,,

1_0_0_-4=2=-5============s=t-y-re_n_e ____ ___. __ -___ -_ -No--j _u~/ L j __ 1 _~_-_L~=oJ--~- o5-07-03 05-07-o:>r

/ 156-60-5 t-1,2 Dichloroethene _____ ND ---+___ll2_!~- i 1 . 0.1 . j 05-07-03 05-07-03;·

:~-~-8:--~-1~:--:4--6

-+-1 ---t~-~-~rt-r~-~-~-~-1

:o-~:-;-h~-;-:e-~:-• - 0~~9 _: :::~ ~ =~~-i ~ .. ::::;:: ::::;~~ - -'

C< I

I '1 ----o.3 -- ----: 05-07-03 05-07-0S., •. 1--

--I -·t "-~ 108-88-3 I Toluene ND ug IL 1 I I lt ' .• :~;~: ::::;:~

. --

I 79-01-6 Trichloroethene ND ug IL 1

75-69-4 Trichlorofluoromethane ND i ug IL 1

I

----·-75-01-4 Vinyl chloride ' ND ug IL 1

EPA 504 ED8/D8CP by GCIECD By: ALG

i------·---+---1_,2-Dibromo-3-chloropropan_e ____ N_D __ -r ug IL _

1

1 !----OO .. -Oo2255-~,' __ _

1,2-Dibromoethane, EDB ___ N_D_ _ I _tJQ_l_L_____ _ _ _----t-___ -_--1 SW846 35108/82708 SVOCs by GC/MS By: JM/KAR

1 _1_92_~-~8-~-~-1-_-_~-_-_-_-_-_-_-_-_-_-_1;_~-~4--~-~-:~-~-~-~;-~_:_~_:_:_e_n_:-_-_e-_-_-_-_=======~---~---------_-_r_--_~_:_~-~ _L __ ~-=-== --T--:

05-05-03 05-05-0:"*' 'Ii;: • .,,,'

05-05-03 05-05-03,

04-28-03 04-29-0~·

04-28-03 04-29-0:>" \, ...

Coyote 2001: Reports 1. 0. 011109162500 Report Date 61412003 12:03:51 PM ' .-·!' ·,



Client:

Project:



Sample: MW- #5 Matrix: GW

QC Group

0304502-01 c X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

Run Sequence

XG.2003.703.12

XG.2003.703.12

XG.2003. 703.12

XG.2003.703.12

XG.2003. 703.12

XG.2003.703.12

XG.2003.703.12

XG.2003.703.12

XG.2003. 703.12

XG.2003.703.12

XG.2003.703.12

XG.2003.703.12

XG.2003.703.12

XG.2003.703.12

XG.2003.703.12

XG.2003.703.12

XG.2003.703.12

XG.2003.703.12

XG.2003.703.12

XG.2003. 703.12

XG.2003.703.12

XG.2003.703.12

XG.2003.703.12

XG.2003.703.12

XG.2003.703.12

XG.2003.703.12

XG.2003. 703.12

XG.2003. 703.12

XG.2003. 703.12

XG.2003.703.12

XG.2003.703.12

XG.2003.703.12

XG.2003. 703.12

XG.2003. 703.12

XG.2003. 703.12

XG.2003.703.12

XG.2003.703.12

XG.2003.703.12

XG.2003.703.12

XG.2003.703.12

XG.2003. 703.12

XG.2003. 703.12

Collected: 04-23-03 15:00:00 By: SP

Dilution Detection


SW846 351 OB/82708 SVOCs by GC/MS

541-73-1 I 1-,3-Dichlorobenzene

106-46=71- --1,4-Dichlorobenzene

90-12-0 1-Methylnaphthalene

By: JM/KAR

-- ····--·--

ND --~- -- - ---

58-90-2 2,3,4,6-Tetrachlorophenol ND ··-----+--

ND

ND -

95-95-4 2,4,5-Trichlorophenol

88-06-2 2,4,6-Trichlorophenol -t_-ND

~~~::~:: -- ~ .. :~~ii:~~~~~~:~~l-----i _____ N-0-~-. _:_1~2_8-:_~---+----2_,4_-_D_._initrophenol -~- ____ t-JD '

121-14-2

606-20-2

91-58-7

101-55-3

7005-72-3

100-01-6 ;

100-02-7

2,4-Dinitrotoluene ND

ND -·

Benzo(a)pyrene , ND

Benzo(b & k)tlUor:anthe-;;e-i ____ ND -

ug IL

ug IL

ug IL

ug IL

ug IL

ug IL

ug IL

ug IL

ug IL --- - 1

10

5

1 ! -No____ 1

-J-=ND_~---_j ----'---- 25 -----

' 191-24-2 Benzo(g,h,i)perylene

64-85-0 Benzoic acid -----

! ND i ug IL f 5 ND __ =r---ug/ L -L~-=1--t~ -----+------

bis(2-Chloroethoxy)methane ND ug I L ' 1 ' 1

100-51-6 Benzyl alcohol

111-44-4 bis (2-Chloroethyl) ether -------·-·-

111-91-1

108-60-1

117-81-7

bis(2-Chloroisopropyl)ether ND ug IL r-- 1---t-- -1-----+----~ bis(2-Ethylhexyl)phthalat-e---i---7.2 -u_g__l!:_=_[_ 1_r 5 B

Prep

Date

STANDARD

Run

Date

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

Page 3 of 27 Coyote 2001: Reports 1.0.011109162500 Report Date 61412003 12:04:52 PM

STANOARC



Client:

Project:




QC Group

0304502-01 c X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

0304502-01 D X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

Page 4 of 27

Run Sequence

XG.2003. 703.12

XG.2003. 703.12

XG.2003. 703.12

XG.2003. 703.12

XG.2003.703.12

XG.2003.703.12

XG.2003.703.12

XG.2003.703.12

XG.2003. 703.12

XG.2003. 703.12

XG.2003. 703.12

XG.2003. 703.12

XG.2003. 703.12

XG.2003. 703.12

XG.2003. 703.12

XG.2003. 703.12

XG.2003. 703.12

XG.2003. 703.12

XG.2003. 703.12

XG.2003. 703.12

XG.2003.703.12

XG.2003.703.12

XG.2003. 703.12

XG.2003.703.12

XG.2003.703.12

XG.2003.703.12

XG.2003.785.29

XG.2003. 785.29

XG.2003. 785.29

XG.2003. 785.29

XG.2003. 785.29

XG.2003. 785.29

XG.2003. 785.29

XG.2003.785.29

XG.2003.785.29

XG.2003. 785.29

XG.2003.785.29

XG.2003. 785.29

XG.2003.785.29

XG.2003.785.29

XG.2003.785.29

Collected: 04-23-03 15:00:00 By: SP

Dilution Detection


SW846 3510Bl8270B SVOCs by GCIMS By: JM/KAR

85-68-7 Butylbenzylphthalate ND ug I L ·--+------'----'--------'-----

218-01 -9 Chrysene ND ug IL 1 1 --~-------f-·

53-70-3 Dibenz(a,h)anthracene ND ug I L ----,-

132-64-9 Dibenzofuran ND ug IL l----+-----------·------,------t-----

84-66-2 Diethylphthalate ND ug I L ---+--1 I 1-----y-

131-11-3 Dimethylphthalate ND ug IL

84-74-2 di-n-Butylphthalate ND ug I L

117-84-0 di-n-Octylphthalate ND ug IL 206~4-4--0--1----F-l_u_or_a_n-th_e_n_e ___ ___, __ ~~£15-=- ug I L j_ --1 --1

86737

118-74-1

87-68-3

'---____ F_lu_o_r_e~.~---------________f\J__~ _ i -·- u_g I L . 1

Hexachlorobenzene '__ ND __ -t_ IJ_!:J_f_L __ j Hexachlorobuta<:!_!:~ ___ : ___ __llJ_[)__ __ i_LI_g_~':__ L

Hexachlorocyclopentadiene ND _1_u_1i_~ _J Hexachloroethane __ ND__ _J_ -~_g_l_L __ 1

10 ---10

10

5

Prep Run

Date Date

04-28-03 04-29-0~

04-28-03 04-29-03

04-28-03 04-29-0::.

04-28-03 04-29-0?

04-28-03 04-29-03

04-28-03 04-29-00

04-28-03 04-29-0?

04-28-03 04-29-03

04-28-03 04-29-00

04-28-03 04-29-0:'

04-28-03 04-29-03

04-28-03 04-29-0::i

04-28-03 04-29-07

04-28-03 04-29-03

04-28-03 04-29-0::.

77-47-4

67-72-1

193-39-5

78-59-1

91-20-3

98-95-3

lnden~~:·:~!~~~:yrene · _ ----~N-0DD ru;g ~/ ~L-~ Naphthalene

I 04-28-03 04-29-0'.

-- -: 04-28-03 04-29-03 ------1 Nitrobenzene ND ---i-ug-fl- -+-----------+-----

----------i------t

62-75-9 n-Nitroso-dimethyl-amine ND ug I L 10 -----------+--------r----- ----------

621-64-7 n-Nitroso-di-n-propylamine ND ug IL I 1 · 1 ----t---------------t--------,-----+-------------------

86-30-6 n-Nitrosodiphenylamine ND ug I L 1 1

-:::!~::-- ___ P_e_;-~a-e~-ha-1~-~-~~-:-ne_:_o_l __ ···---T- ~~ __ -: ~~t _ ~=------1~ _l_j :~::~~:~ Phenol --J------N_!J ___ i--~-g_/ ~-~ _ ~---+--- _ 10 --·---1

~----P_y_re_n_e ____ -+-I __ N_D _ _J_ug l_L-___1 ___ 1 - l--1 ~ _1_1_0_-8_6-_1~-· Pyridine I ND _J ug IL I 1 L_10 J___ _____ _I

SW846 3510B/8081A Pesticides by GC/ECD By: ALG ~---~--------~---------~----- --------· ---------·

a-BHC ND I ug I L 1 0.1 !

a-Chlordane 1

ND I ug I L 1 ---o.1 ---+1-_-__ -__ . _ _,~

_3_0_9--00--2---t-------~;_;_ ______ ; __ ~=#~~--=t--~~ ~--~ _ 1. _:_~-t . __ 5_7 __ -_74_-_9---f _____ C_h_l_o __ rd_a_n_e_, t()_tal ________ L _ _1'1~--- ~L~--- -~-------~·1 __ f

d-BHC ; ND ' ug I L I 1 ' 0.1 ---------j------------------------+ - --------------1-------- -~ - I 60-57-1 Dieldrin . ND ug IL 1 0.1 --------+------Endosulfanl -------+---No----- --~iiT"L- '.- -- ----- o~1- -- +- -- ---------- +.------------------ ---+------------ ---- --- --1------

-------· ________ Endosulfan II ~ ___ .!'!_'? ___ , ~g_I ~ , _ 1_ _(l._~----i------Endosulfan Sulfate I ND f ug I L : 1 0.1 J_ '

~:::--:-__ -•• ~---_-_-::::-E_E_n_: ___ :-~-~-i~-~-~-~-~-~-~-t:_n_:_:-~----------------------+·+_------~r l~t1~=r rrri

04-28-03 04-29-03

04-28-03 04-29-0'.

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-0'.

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-0:

04-28-03 04-29-o:_,

04-30-03 05-09-03

04-30-03 05-09-0:

04-30-03 05-09-0:."

04-30-03 05-09-03

04-30-03 05-09-0:

04-30-03 05-09-0~

04-30-03 05-09-03

04-30-03 05-09-0:

04-30-03 05-09-0?

04-30-03 05-09-03

04-30-03 05-09-0:

04-30-03 05-09-0?

04-30-03 05-09-03

04-30-03 05-09-0:

04-30-03 05-09-0:'

Coyote 2001: Reports 1.0.011109162500 Report Date 61412003 12:05:41 PM



Client:

Project:



-Sample: MW- #5 Matrix: GW

QC Group

0304502-01 D X03194

X03194

X03194

X03194

X03194

X03194

X03194

0304502-01 D X03189

X03189

X03189

X03189

X03189

X03189

X03189

0304502-01 E M03548

M03548

M03548

M03548

0304502-01 E M03550

M03550

M03550

M03550

M03550

M03550

M03550

M03550

M03550

M03550

M03550

M03550

Run Sequence

XG.2003.785.29

XG.2003.785.29

XG.2003.785.29

XG.2003.785.29

XG.2003.785.29

XG.2003. 785.29

XG.2003.785.29

XG.2003.750.19

XG.2003.750.19

XG.2003.750.19

XG.2003.750.19

XG.2003.750.19

XG.2003. 750.19

XG.2003.750.19

MT.2003.521.19

MT.2003.511.42

MT.2003.511.42

MT.2003.521.19

MT.2003.551.36

MT.2003.577.13

MT.2003.551.36

MT.2003.551.36

MT.2003.551.36

MT.2003.551.36

MT.2003.551.36

MT.2003.551.36

MT.2003.551.36

MT.2003.551.36

MT.2003.551.36

MT.2003.551.36

Collected: 04-23-03 15:00:00 By: SP

Dilution Detection


SW846 3510B/8081A Pesticides by GC/ECD By: ALG -- - ------ T --- ---- - ---

76-44-8 Heptachlor ND i ug I L 1 0.1 ! I

,,,,._57_3 , Heptoohl" Epo,,de ND I ----,;g, L - _,__:_;_o_1 _:J 72-43-5 1 Methoxychlor ND i ug I L 1 I 0.1 1

6088-51-3 p,p-DDD , ND I ug IL J 1 0.1 1 --~-------- ---- --- -------~ ----- __ i____ --- ----1

-- - - --- p,p-DDE r _ _'.-JD ___ l~i_l-__1-=-~1_ ___ ==9_ 1 j J 1 8~~~~:~~2 Tox:~~~~~total j z~ ---+*- -- ~-I - ~}-_L_ __ ~ SW846 35108/8082 PCBs by GC/ECD By: ALG

~~~::~: I ~::~:: :~~: -+= ~~ ; :n T -tt~t--= 53469-21-9 r- --- Arocl0r1242_________ ND ug IL 1 1-- 6~5- -I - 1

1-2612-29-6 1--- --Aroclor1248 - --Nff ___ T_U9/-C 1 r- o.5 - 1

:~~:::::::·1-------~~~~~~~- ----"- __ -~-~-=----L~-ci ;_~--~~~-~=~~-- ~:~ SW846 3005A/6010A ICP By: JRE

7440-41-1 =-:------BerYliiUm ____ ~---No--l mgl_L:-J= --- -~---()~~~==-==

I ;:::~ --0

;~-- J _;~-~:ttt_:~ __ -i--:-:.! SW846 3005A6020 ICP-MS By: HMR

I 7 440-36-0 :

7440-38-2 :

Antimony _J___ ND mg I L

Arsenic 0.003--T mg/i_

0.001

0.001 I

744o-39:3j _____ B_a-ri-um___ 0.148 r-mg/L ___ ----- - -o:OoT--

~::~::~--- Ca~e:~m --~~ 1 :: ; ~ __ 1 __ 1_~:~~-11----+----

-7_4_4--0---0-2--0-+------N-ic-k-el ____ - ___ ----__ -__ -_-___ , _____ 0.00~- - mg IL _____ 1 _J.=_ o:0o1-7782-49-2

7440-22-4

Selenium ND _rri~J_L __ L __ ~ _ j 0.001

Silver ND mg IL 11 ' 0.001 Thallium ND mg IL 1 0.001 ,

-----·-· --- ___ _J_____ -------- _ _J__ - -- --: 7440-28-0

7440-31-5 . Tin ND mg IL 1 0.001 1

7-44-o-62~ Vanadium 0.001 I mgJL -1 - - -0 -001- -+---

7440-66--6~1 -----Z-in_c___ - -O~Oo-g 1 -mg IL - - 1 -- 0.005 - - 1

I ---------- j --

SW846 7470 Mercury by CVAA By: JRE

STANDARD

Prep

Date

04-30-03

04-30-03

04-30-03

04-30-03

04-30-03

04-30-03

04-30-03

04-30-03

04-30-03

04-30-03

04-30-03

04-30-03

04-30-03

04-30-03

04-30-03

04-30-03

04-30-03

04-30-03

04-30-03

04-30-03

04-30-03

04-30-03

04-30-03

04-30-03

04-30-03

04-30-03

04-30-03

04-30-03

04-30-03

04-30-03

Run

Date

05-09-03

05-09-03

05-09-03

05-09-03

05-09-03

05-09-03

05-09-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-01-03

05-01-03

05-01-03

05-01-03

05-05-03

05-13-03

05-05-03

05-05-03

05-05-03

05-05-03

05-05-03

05-05-03

05-05-03

05-05-03

05-05-03

05-05-03

0304502-01 E M03559 MT.2003.522.27 1 Y439-97-6 I Mercury ND mg/L , 0.0002 1 05-01-03 05-01-03

Page 5 of 27 Coyote 2001: Reports 1. 0. 011109162500 Report Date 61412003 12:06:25 PM

Client:

Project:





Order: 0304502 PHl16 Receipt: 04-24-03

Sample: MW- #6 Collected: 04-23-03 16:20:00 By: SP

Matrix: GW

Dilution Detection

STAN DAR[

Prep Run

QC Group Run Sequence CAS# Analyte Result Units Factor Limit Code Date Date

0304502-02A XD3206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

XD3206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

XD3206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

XD3206

X03206

X03206

X03206

X03206

X03206

X03206

XD3206

X03206

Page 6 of 27

XG.2003.817.7

XG.2003.817.7

XG.2003.817.7

XG.2003.817.7

XG.2003.817.7

XG.2003.817.7

XG.2003.817.7

XG.2003.817.7

XG.2003.817.7

XG.2003.817.7

XG.2003.817.7

XG.2003.817.7

XG.2003.817.7

XG.2003.817.7

XG.2003.817.7

XG.2003.817.7

XG.2003.817.7

XG.2003.817.7

XG.2003.817.7

XG.2003.817.7

XG.2003.817.7

XG.2003.817.7

XG.2003.817.7

XG.2003.817.7

XG.2003.817.7

XG.2003.817.7

XG.2003.817.7

XG.2003.817.7

XG.2003.817.7

XG.2003.817.7

XG.2003.817.7

XG.2003.817.7

XG.2003.817.7

XG.2003.817.7

XG.2003.817.7

XG.2003.817.7

XG.2003.817.7

XG.2003.817. 7

XG.2003.817.7

XG.2003.817.7

XG.2003.817.7

XG.2003.817.7

XG.2003.817.7

EPA 524.2 rev 4 Purgeable VOCs by GC/MS By: JAA 1 75_34-::3i-- 1, 1 Dichloroethane I ND : ug I L j [ 0.1

75~354-i-----1.10icli-loroetl1ene --+---N-D----u-9-,-L- f~- ---~ -_--0-.-1-~-------·-I

05-07 -03 05-07 -O:

05-07 -03 05-07 -03

05-07 -03 05-07 -Os

05-07 -03 05-07-0:

05-07 -03 05-07-03

05-07 -03 05-07 -03

05-07-03 05-07-0:

05-07 -03 05-07 -03

05-07-03 05-07-03'

05-07 -03 05-07 -O: 05-07 -03 05-07-03

05-07-03 05-07-03"

05-07 -03 05-07 -o: 05-07 -03 05-07 -0~

05-07 -03 05-07 -03

05-07 -03 05-07 -O: 05-07 -03 05-07 -03

05-07 -03 05-07 -03

05-07-03 05-07-0'.

05-07-03 05-07-02

05-07 -03 05-07 -03

05-07 -03 05-07 -0~

05-07 -03 05-07 -02

05-07 -03 05-07 -03

05-07 -03 05-07 -0~

05-07 -03 05-07 -0:>

05-07 -03 05-07 -03

05-07 -03 05-07 -0~

05-07 -03 05-07 -0?

05-07 -03 05-07 -03

05-07-03 05-07-0~

05-07-03 05-07-0?

05-07 -03 05-07 -03

05-07-03 05-07-0~

05-07-03 05-07-0?

05-07-03 05-07 -03

05-07 -03 05-07 -00

05-07-03 05-07-0~

05-07 -03 05-07 -03

05-07 -03 05-07 -0'.,

05-07-03 05-07-0~

05-07 -03 05-07 -03

05-07-03 05-07-0~

71-55-6 1, 1, 1 Trichloroethane l_ __ _r-J~---- ~· --ugf L I ___ u _ ___ o: 1

6_3_0~~ 1, 1, 1,2 Tetrachloroethane ---1-

ND ug IL 1 0.1 : ·-·-- ____ _.J._ -----+-- ---- --

79-DD-5 I 1, 1,2 Trichloroethane ND i ug IL 1 0.1

I -79_34~-- 1, 1,2,2 Tetrachloroethane ND _fU9iL. 1 0.1

I - ---~------· -u-91c-r- ------,-- ... - . -- ----<

563-58-6 1, 1-Dichloropropene ND I 1 0.1 --------- ----+---· t----- ·-

106-93-4 1 ,2 Dibromoethane (EDS) i ND ug IL I 1 0.1 I i

·-····---95-50-1 1,2 Dichlorobenzene ND ug IL 1 0.1

I ---- - - --- ··-- -107-06-2 1,2 Dichloroethane (EDC) I ND ug IL 1 0.1

I

----i ! 78-87-5 1,2 Dichloropropane ND ug IL 1 0.1 !

- --- ------96-18-4 1,2,3 Trichloropropane ND ug IL 1 0.1 i ------· ~- ·- -- --1-87-61-6 1,2,3-Trichlorobenzene ND ug IL 1 0.5

----- -· ----I 0.5 !

r

120-82-1 1,2,4-Trichlorobenzene ND ug IL 1 -·--- ------------· ---

95-63-6 1,2,4-Trimethylbenzene ND ! ug IL 1 I 0.1 I

I ----- - - ·- ----- - ----- -----

1,2-Dibromo-3-chloropropane t ND ug I L ,_ _

0

0 .. 2

1

-j~ __ -, 5~1:!3-1 _' 1,3 Dichlorobenzene ~-.!'!.[) __ L_u_g/ L [_ ____ ------! 108-67-8 1,3,5-Trimethylbenzene ND ug IL 1 0.1 1 1

142-28-9 1,3-Dichloropropane --ND- - -ug it:: · i -T--oT-- ; ----i i00-46-7 ______ 1,4 Dichlorobenzene . -- - --- -ND- --- - ---;;9; L---r--1--H~i- i.

1

----j 99-87-6 1,4-lsopropyltoluene ND ug IL r----i r· 0~1--- '

. --· -----.. I - - ·i .... -----------· ------------~~--- ~~ ~ ~ I i1 I . ~}~: ____ _j

4-Chlorotoluene ND ug IL I 1 ---- o~ 1- - . : -------+--------------------+----~·- -------- - -· -·-----· ~' ---..j

Benzene ND ug IL I 1 0.1 !

______ B_ro_m_o_?_~~~-~--~-e_-_-_------N-D---j---u-g_/_L __ j-=[-~]- 0.1 UH_L_ J Bromochloromethane ND I ug I L i 1 0.1 1

-~~7-4-t__=.-s~omoci}chloromeii1~-~~- ~-__ t _-__ N-_D--~-=:-u9-,-L--:=-i ~ · '-- - 0.1 1

96-12-8

594-20-7

106-43-4

2-Chlorotoluene

2,2-Dichloropropane

95-49-8

71-43-2

108-86-1

Bromoform i ND ug I L 1 --~--------------+ ~~--- T-

75-25-2 0.1 ----+------

74-83-9 Bromomethane _, ND ug I L 1 0.6

56-23-5 Carbon tetrachloride ND ug IL 0.1

-1--~--8--~--~-!_-_-+----C-hl-o-ro_b_e_n-ze_n_e---~r-_-_N_~--~--ug_~~-- c-- _ ~ _ J___~._1_---+_-~ 124-48-1 Chlorodibromomethane ND ug/L 1 __ J --~·1-----+-----j

_--:~:~~:: I ===~;~~------r=~~ --=--~~+---r--- ~ 000 ... 111 J ______ _ 74-87-3 _ Chloromethane ___ __j_ ND ug IL 1 1 I 156-59-2 cis-1,2 dichloroethene · ND ug IL 1 0.1 --+---

10061-01-5 cis-1,3dichloropropene ND ug/L ' 1 01 74-95-3 Dibromomethane ----ND ______ --ug~i--1- . o: 1

---+------------~--~----:-·-----~- -- ---------1----- --t--- -100-41-4 Ethylbenzene ND ' ug IL 1 1 ~ 0.1 ·

75-71-8 Freon 12 1

- __f-.J_[)__~:-ug/L-1~_-1--'-----~~ '

87-68-3 Hexachlorobutadiene ___ 1 ___ ND ____ u~_t_L._ __ i- 1 0.1

·9a-0~----1sol)ropYibenzene____ ND _u~!L __ L __ 1 _____ 0.1 ___ L __ _


STANDARD



Client:

Project:



Sample: MW- #6

Matrix: GW

QC Group

0304502-02A X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

0304502-028 X03200

X03200

0304502-02C X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

Page 7 of 27

Run Sequence

XG.2003.817.7

XG.2003.817.7

XG.2003.817.7

XG.2003.817.7

XG.2003.817.7

XG.2003.817.7

XG.2003.817.7

XG.2003.817.7

XG.2003.817.7

XG.2003.817.7

XG.2003.817.7

XG.2003.817.7

XG.2003.817.7

XG.2003.817.7

XG.2003.817.7

XG.2003.817.7

XG.2003.727.15

XG.2003.727.15

XG.2003.703.14

XG.2003.703.14

XG.2003.703.14

XG.2003. 703.14

XG.2003. 703.14

XG.2003.703.14

XG.2003.703.14

XG.2003.703.14

XG.2003.703.14

XG.2003.703.14

XG.2003.703.14

XG.2003.703.14

XG.2003.703.14

XG.2003.703.14

XG.2003.703.14

XG.2003. 703.14

XG.2003.703.14

XG.2003.703.14

XG.2003. 703.14

XG.2003. 703.14

XG.2003. 703.14

Collected: 04-23-03 16:20:00 By: SP



EPA 524.2 rev 4 Purgeable VOCs by GC/MS By: JAA 75-09=2-~-- Methylene chloride ,--- No--r ug IL 1' - 1 I o.5 -----, 05-07-03 05-07-03

.. -------------------------·------ ·-------1----- -------------!-- ---------- ,-------------------c--

91-20-3 · Naphthalene ~--ND i ug IL------~---- 05-07-03 05-07-03

104-51-8 n-Butylbenzene ' ND ug IL 0.1 05-07-03 05-07-03

103-65-1 ! n-Propylbenzene ND ug IL 0.1 05-07-03 05-07-03 --- -------i------------·---

95-47-6 I o-Xylene ND ug IL 0.1 05-07-03 05-07-03

3j~~~~:; I_----= P~~=-----r·--No_T_ug / L-------=----=-=-- -~.2 o5-o7-o3 o5-07-03

~~~::~:: sec-B;t~::~:zene ~~ ~~; ~ --- ~--F--~-~- __ -J-- ~::~~:~: ~::~~:~: 156-60-5 t-1,2 Dichloroethene __ NNDD = uugg 1

1

LL-1

11

I 0.1 05-07-03 05-07-03

: 10061-02-6 t-1,3 Dichloropropene 0.1 05-07-03 05-07-03

98-06-6 tert-Butylbenzene -- - - -NC> -ug-/L - ~~ =--:- 0.1 __ ---~ 05-07-03 05-07-03

127-18-4 Tetrachloroethylene I 0.34 ug IL i_1__ 1- 0.1 I 05-07-03 05-07-03

108-88-3 Toluene I ND ug IL 1 0.3 I 05-07-03 05-07-03

79-01~6 ______ - Trichloroethene _L ---ND +·u9TC-- 1 I 0.1 I 05-07-03 05-07-03

~::~~~ -------~r'.~h~i~~~;;;;~~~n~- -_~J_ ~r __ l~]~-~=-~~-- ~: ~ -~-~=-----] ~::~~:~: ~::~~:~: EPA 504 EDB/DBCP by GC/ECD

--=- _J __ 1,~~~~;;;!;;l:~:~~~~ne_ SW846 351 OB/82708 SVOCs by GC/MS

ND - ----------j---

ND

ug IL

ug IL

130-02-2_ 1,2,4-Trichlorobenzene ND -T--ugfl ( _ 95-50-1 1,2-Dichlorobenzene ND ! ug I L I 1 1

541-73-1 1,3-Dichlorobenzene -- ND-- _ '.-_ -~:-~~--J ____ -11- - ~ =_- 1

1 _

By: ALG

By: JM/KAR

106-46-7 1,4-Dichlorobenzene _____ -- ---ND-- + _

90-12-0 +-' 1-Methylnaphthalene ND ~~;LL j__ 11

~- -~- __ _ 58=9o-=2- , - 2,3,4,6-Tetrachlorophenol ND

-+

95-95-4 I 2,4,5-Trichlorophenol ND uugg ',LL r, - 1 _55 __ _j_ ___ -

88-06-2 2,4,6-Trichlorophenol 1

_ ND 1 ___ _

120-83-2 2,4-Dichlorophenol I ND ug IL 1 1 5 105-67=9-- ---2,4-Dimethylphenol ND ug I L t--1-

--l~~~2-:-------*~~~---- ----~~- ~~; ~ 1--~ -i- --~o-:i'-~:_~ 606-20-2 : 2,6-Dinitrotoluene ND ug I L --:-- _ 1 ____ 1 5 i -------------------·------·-- ' --+---- --- - .. ·-- __ ,

::::~:: : 2-~~~~~~r:~::~~ne - -~- ~~ -~~~t--~---~-+-~---+- -- -1

::::::~ 2-~~::;~:~~::~~ne -i--~~-- ---r _ ~~ ; ~ +---T- ~- =r=~=t==: 88-74-4 -----·----- --~=!'l_i!r:_~~~ri_~ _....L ___ _t-IE___ __ t_ll9 IL _c __ 1_~_ 5 -t==-~ 88-75-5 2-Nitrophenol ND : ug I L 1 5 --t-- ___ )

_91=9-4=2___ --3~~;;;~~~~~--------~;=-._L ~~ ~-~--- _ __ _ ~ \o _ :J ______ j

05-05-03 05-05-03

05-05-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03


STANDARl Assaigai Analytical Laboratories, Inc.


Client:

Project:




QC Group

0304502-02C X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

Page 8 of 27

Run Sequence

XG.2003. 703.14

XG.2003. 703.14

XG.2003.703.14

XG.2003.703.14

XG.2003. 703.14

XG.2003.703.14

XG.2003. 703.14

XG.2003. 703.14

XG.2003. 703.14

XG.2003. 703.14

XG.2003. 703.14

XG.2003. 703.14

XG.2003. 703.14

XG.2003.703.14

XG.2003. 703.14

XG.2003. 703.14

XG.2003. 703.14

XG.2003.703.14

XG.2003. 703.14

XG.2003.703.14

XG.2003.703.14

XG.2003.703.14

XG.2003.703.14

XG.2003.703.14

XG.2003.703.14

XG.2003.703.14

XG.2003.703.14

XG.2003.703.14

XG.2003.703.14

XG.2003.703.14

XG.2003.703.14

XG.2003. 703.14

XG.2003.703.14

XG.2003.703.14

XG.2003. 703.14

XG.2003.703.14

XG.2003.703.14

XG.2003. 703.14

XG.2003.703.14

XG.2003.703.14

XG.2003.703.14

XG.2003.703.14

Collected: 04-23-03 16:20:00 By: SP

Dilution Detection


SW846 35108/82708 SVOCs by GC/MS By: JM/KAR

Prep Run

Date Date

99-09-2 3-Nitroaniline i -ND--____ u_i_!_l-__ T_ 1__ 5 ~-~L __ J 04-28-03 04-29-o:.

534-52-1 4,6-Dinitro-2-methylphenol ND , ug IL 1 1 O 04-28-03 04-29-03 -·--------+-------------------.;_ __________ i _____ ,____ --·---!---------"

__ 1_0_1_-_55_-_3-+-__ 4_-Bromophenyl-phenylether , ND ----~__LJg_l~ __ c _______ -~ 59-50-7 4-Chloro-3-methylphenol-- T ND ' ug I L i 5

04-28-03 04-29-03

04-28-03 04-29-o:'

106-47-8 4-Chloroaniline ND ug IL 5 ' 04-28-03 04-29-03 ---------r-------------t--------+-------,----------

~()0~72-3 ---~<?hlorophenyl-phenylether ND ug I L 1 04-28-03 04-29-03·

100-01-6 4-Nitroaniline ND ug IL 1 --1--·--~---+---, 04-28-03 04-29-o:. --------1--------------------r-----,------- -+-----·

100-02-7 4-Nitrophenol ND ug I L ' 1 I 1 O 04-28-03 04-29-03 -------+--------------------+-----+----+----83-32-9 Acenaphthene _________ _!:JE____ ug IL I- 04-28-03 04-29-03'

208-96-8 Acenaphthylene ND ug I L 1

04-28-03 04-29-0'. ------+-------------+-------+------+------+-------

62-53-3 Aniline ND ug IL ; [ ___ 1 O ____ '-···

120-12-7 Az~:~~::~~ ,-2 _____ j__=~~- -+-~~; ~ ~L-=~ ~~r+- -~ -=j Diphenylhydrazine

55_:-55=3-- _____ B_e_n~z_o_(_a~) -a~nt-h-ra_c_e_n_e---+----N-D ___ j_u_g_/_L ___ l- 1 -[_-__ -____ --+-

1

__ ....,··1

04-28-03 04-29-03

04-28-03 04-29-03'

04-28-03 04-29-0'.

04-28-03 04-29-0~

04-28-03 04-29-0~ _5_o_-3_2_-8_+-____ B_e_n_zo(a)pyrene __ ND I ug I L ___ 1 ___ J _ . _ -1-----i

Benzo(b & k)fluoranthene ND I ug IL _____ 1 __ ' i 04-28-03 04-29-03

Benzo(g,h,i)perylene ND 1 ug I L 1 ' 04-28-03 04-29-0'.> 191-24-2

64-85-0 Benzoic acid ND ug I L 25 ------- --·------------+-------+-----+----+-----+-----1

100-51-6 Benzyl alcohol ND ug I L 5 111-44-4 bis (2-Chloroethyl) ether ND 1 ug I L

04-28-03 04-29-o;

04-28-03 04-29-03

04-28-03 04-29-0'.J

--~-~~-1-:--:-_0_1 __ :-~:-:1:::bb_i-~_s-(~~;_~-C-hh-1~0-:_;_;~~o-P:_~;~;~;:~~f---;~-=~--~-~Jt_ ! =- -----+-------ii 04-28-03 04-29-0: : 04-28-03 04-29-03

117-81-7 : bis(2-Ethylhex~_.9.P_~!~-~~~t~--+ __ N_D _ ___ ug_I_~_

85-68-7 Butylbenzylphthalate I ND ug I L --

218-01-9 Chrysene i ND ug IL ,

5

1

04-28-03 04-29-0'1

04-28-03 04-29-o:

04-28-03 04-29-03 ·---- . -·---- -------- 1- !

· ...:3-70-3 __;_ ____ E1benz(a,h)anthracene I ND u~--L- 1------------+----' 04-28-03 04-29-0'.J

' u~~~It H D~t~~~~:~:~a~e =t~~-~~i~-t-t_~ ~ --~-=-~+_ i ~::~::~~ ~::~::~~ -~1-1_1!_1 Dimethylphthalate ND , ug IL J- __ 1 __ L __ 1 _ ___,. ___ __, 04-28-03 04-29-0Ci

84-74-2 r di-n-Butylphthalate ND : ug IL 1 I 1 04-28-03 04-29-0:

117-84-0 I di-n-Octylphthalate ND---- i--~gTL 1---- ! -- -1 04-28-03 04-29-0:}

-'i,:';° . _ Fl~::::~:oe 1

~~ ~ _1_!_1 =t= ~::~::~~ ~::~::~~ _1_1_fl!~ _ _ _ Hexachlorobenzene J ND '. -~u~g- ;

1_ ~L-- f, -+

1_ ~=t_-=~_-11

1

o0_=Ht·---~~- 04-28-03 04-29-03

87-68-3 Hexachlorobutadie~~------- _ ND

1

. --~---------1--·--·--l' 04-28-03 04-29-03 04-28-03 04-29-0: 77-47-4 I Hexachlorocyclopentadiene ND "9 IL 1 10 1 57:72:·1""-.,. Hexachloroethane

--- ·- -----193-39-5 I lndeno(1,2,3-cd)pyrene

I 78-59-1 lsophorone ·- --------91-20-3 Naphthalene --------98-95-3 Nitrobenzene 62-75-9 n-Nitroso-dimethyl-amine

----- ND _____ _ll(l_i_l:__ _ 1 _ _ ____ 5 _ _ _ _ J

ND I ug IL , 1 1 ND ' ug/ L ~1-~--1--1 -- ---

------···~-------+----------; __ -- ------ - - - --- -- __ ,

ND I ug IL i 1 1 I

i r ND ug IL 1 I 1 ~

ND ug IL I 1 10 I

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-0:

04-28-03 04-29-0~

04-28-03 04-29-03

04-28-03 04-29-0'.




Client:

Project:


AP~L03SAMPLEEVENT



QC Group

0304502-02C X03165

X03165

X03165

X03165

X03165

X03165

X03165

0304502-02D X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

0304502-02D X03189

X03189

X03189

X03189

X03189

X03189

. X03189

0304502-02E M03548

M03548

Run Sequence

XG.2003.703.14

XG.2003.703.14

XG.2003. 703.14

XG.2003.703.14

XG.2003.703.14

XG.2003.703.14

XG.2003.703.14

XG.2003. 785.30

XG.2003.785.30

XG.2003.785.30

XG.2003. 785.30

XG.2003.785.30

XG.2003.785.30

XG.2003.785.30

XG.2003.785.30

XG.2003.785.30

XG.2003. 785.30

XG.2003. 785.30

XG.2003.785.30

XG.2003. 785.30

XG.2003.785.30

XG.2003.785.30

XG.2003. 785.30

XG.2003. 785.30

XG.2003. 785.30

XG.2003. 785.30

XG.2003.785.30

XG.2003.785.30

XG.2003.785.30

XG.2003.750.20

XG.2003.750.20

XG.2003.750.20

XG.2003.750.20

XG.2003.750.20

XG.2003.750.20

XG.2003.750.20

MT.2003.521.22

MT.2003.511 .43

Collected: 04-23-03 16:20:00 By: SP

Dilution Detection


SW846 35108182708 SVOCs by GC/MS By: JM/KAR

621-64-7

86-30-6 - -- ________ j_ ___ _

87-86-5

85-01-8

n-Nitroso-di-n-propylamine

n-Nitrosodiphenylamine ;-=-No-==+--ug ,-c= =--~-t-- _1

ND j ug /~ 1 ---+--------1__ __J ___ i Pentachlorophenol ND I ug I L ~ __ u __ 1 O i ___ j

108-95-2

129-00-0

110-86-1

--------=-e:-~~"-~-en:_------+--~-~- J;~ --:--.--ft r-_____ P_yr_id_ine ___ -- -~- ND I ug I L 1 I 10 u _ _J_ ____ _

SW846 35108/8081A Pesticides by GC/ECD

a-BHC

By: ALG

a-Chlordane ND ug I L- -- 1- 0.1 -~i-- -~ ND ug IL -f-1 r 0 1

309-00-2

57-74-9

Aldrin . ---·---·-·----"------------

b-BHC

Chlordane, total

d-BHC

ND - _ug_i_ ~L I __- -1- --= D.1 _ --:- -- I

~~ -~~ ~~ - -~ --+-----~} -J_ --ND-- -rug-fl- -- (- - 0.1

ND i ug I L : 0.1 -------------'-- ------ _J

60-57-1 Dieldrin

----~ ~~=~:~1~=~1'i ;---*~---- 1 -~~~t i ~} ------ ndosulfan Sulfate

1_ ~D . ~=u9/L-r- ~1 ____ _

72- Endrin j N~ '. ug I L [ 1 __ _ 0 _1 _

. -=--- -----~-~-~-=~-~_in_A~:~ee§_~--e~H --~-~%--G~-L I- ~--- ~ - ~:~ -~----58-89-9 g-i~:;d~ne ____ J_ _ ND ~/ _L __ 1_ __ -~-()_ 1_ _ __

76-44-8 I

1024-57-3 I 72-43-5 I

6088-51-3 ________ £.fJ-DDD _______ l_ __ ND __ +-~~i _J__ 1 ___ 0.1 _1

_ -1 p,p-DDE ND ~ 1· ---~-- --- 0.1 I- -= ]

[ 0~~~~:~;-- --u u ·:ro-;!~~~!1oia1 +- ~~ -H-!U--~~*= --==~=~--~:~--=----SW846 35108/8082 PC8s by GC/ECD

--~--N-D--~-u_g_/_L T-1 - :

ND ug/L 1--1-r 12674-11-21 Aroclor 1016

11104-28-2 I Aroclor 1221

11141-16-5 I Aroclor 1232 ND ug IL ! 1 1

53459:21.9 j Aroclor 1242 12672-2-9--6----t-! ----A-ro-c-lo_r_1_2_4_8 _____ ,_ ___ NE___l_ ug IL _______ --_-_:= 11097-69-1 i Aroclor1254 1 ND ug/L 11096-82-5 I Aroclor 1260 r .. -i\fr) ---, -ug/L

SW846 3005A/6010A ICP

Beryllium ND mg IL

Chromium ND mg IL

0.5

0.5

0.5

0.5

0.5

0.5

0.5

By: ALG

----+----

STANDARD

Prep Run

Date Date

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-30-03 05-09-03

04-30-03 05-09-03

04-30-03 05-09-03

04-30-03 05-09-03

04-30-03 05-09-03

04-30-03 05-09-03

04-30-03 05-09-03

04-30-03 05-09-03

04-30-03 05-09-03

04-30-03 05-09-03

04-30-03 05-09-03

04-30-03 05-09-03

04-30-03 05-09-03

04-30-03 05-09-03

04-30-03 05-09-03

04-30-03 05-09-03

04-30-03 05-09-03

04-30-03 05-09-03

04-30-03 05-09-03

04-30-03 05-09-03

04-30-03 05-09-03

04-30-03 05-09-03

04-30-03 05-07 -03

04-30-03 05-07 -03

04-30-03 05-07 -03

04-30-03 05-07 -03

04-30-03 05-07 -03

04-30-03 05-07 -03

04-30-03 05-07 -03

04-30-03 05-01-03

04-30-03 05-01-03




Client:

Project:



Sample: MW- #6

Matrix: GW

QC Group

0304502-02E M03548

M03548

0304502-02E M03550

M03550

M03550

M03550

M03550

MD3550

M03550

M03550

M03550

M03550

M03550

M03550

Run Sequence

MT.2003.511.43

MT.2003.521.22

MT.2003.551.39

MT.2003.577.14

MT.2003.551.39

MT.2003.551.39

MT.2003.551.39

MT.2003.551.39

MT.2003.551.39

MT.2003.551.39

MT.2003.551.39

MT.2003.551.39

MT.2003.551.39

MT.2003.551.39

Collected: 04-23-03 16:20:00 By: SP

Dilution Detection


SW846 3005A/601 OA ICP By: JRE

i ~-:-:~-;-~;-_~~1-__ -_ ----~-:-:-:e-1~-------+l-__ -_-_ -~--~--------------~----:-_ -~----~~ _--L- 1 ~~-~~~~ -~~ SW846 3005A6020 ICP-MS

~~40-_36_-o _______ Anlimony---------~J~~=~~~£5-=:-~~:~~/~ 744°=~~-- Arsenic I 0.003 1 mg IL L 7440-39-3 Barium ---0.090---r mg--/L I

7440-43-9 Cadmium ND ___ mg J__L _ j 7439-92-1 Lead ND mg IL

By: ---~()1---

------t 0.001

0.001

0.001

HMR

i

i

. ·-·-----~----+--~ 1 0.001

----------+--------- ------+-----~--_____,_--------+------··- --1

7440-02-0 Nickel 0.001 mg IL ------+------------+------+-------------+--

7782-49-2 Selenium ND mg I L

0.001

0.001 I

-----j

Prep Run

Date Date

04-30-03 05-01-0:

04-30-03 05-01-03

04-30-03 05-05-03

04-30-03 05-13-0~

04-30-03 05-05-0:}

04-30-03 05-05-0~

04-30-03 05-05-0:

04-30-03 05-05-D:i

04-30-03 05-05-03

7440-22-4 Silver ND mg IL

7440-28-0 Thallium ND mg IL

0.001

0.001

D4-3D-D3 o5-o5-o: _

I 04-30-03 05-05-03

7440-31-5 Tin ND mg IL

7440-62-2 Vanadium I ____ o:~~----- __ m~ I _L _ 1 _

7440-66-6 Zinc ND mg IL ----~----------------- ---'-------- -------

SW846 7470 Mercury by CVAA

0.001 ---!--------·---- __ ,

0.001 · -1- --oil-o5-r---

By: JRE

04-30-03 05-05-03

04-30-03 05-05-0:

04-30-03 05-05-0:1

0304502-02E M03559 MT.2003.522.28 [ 74-39:97-6 I Me_r_cu_ry ___________ N_D mg i"L I 1 1 O 0002-~--------! 05-01-03 05-01-03

-+----- J_ _______ _j __ · _____ _j__ ___ ____J

Sample:

Matrix:

MW-#4

GW

QC Group

0304502-0JA X03206

X03206

X03206

X03206

XD3206

X03206

X03206

X03206

XD3206

X03206

X03206

X03206

XD3206

X03206

X03206

X03206

XD3206

Page 10 of 27

Run Sequence

XG.2003.814.21

XG.2003.814.21

XG.2003.814.21

XG.2003.814.21

XG.2003.814.21

XG.2003.814.21

XG.2003.814.21

XG.2003.814.21

XG.2003.814.21

XG.2003.814.21

XG.2003.814.21

XG.2003.814.21

XG.2003.814.21

XG.2003.814.21

XG.2003.814.21

XG.2003.814.21

XG.2003.814.21

---------- ------- ------ - - ·- . -- - -·-- ------- -- ---------------- -----------------Collected: 04-23-03 17:40:00 By: SP

Dilution Detection


EPA 524.2 rev 4 Purgeable VOCs by GC/MS By: JAA

Prep Run

Date Date

_75-34-3 _______ H _____ 1, 1 Dichloroethane ! ---- _N_D __ T_u_g_/L ~1=~-= 0.1 ---__ -__ -~ D5-D7-D3 o5-D7-o~

~5_~_:~4 ____ 1, 1 Dichloroethene ND ! ug IL ! 1 ! 0.1 1 05-07-03 05-07-0~

05-07 -03 05-07 -0~

05-07-03 05-07-0?

71-55-6 1, 1, 1 Trichloroethane ND ' ug IL ' 1 0.1 05-07-03 05-07-03

-63o-=-io:5 1, 1, 1,2 Tetrachloroethane ND t ·ug/L t_~~-1=t a: 1- -H--~ --- -

79-00-5 1, 1,2 Trichloroethane ND I ug I L ' I 0.1

79-34-5

563-58-6

106-93-4

1, 1,2,2 Tetrachloroethane _i__ _ _!'J~---f~_l:_ _____ 2_ 0. 1 05-07-03 05-07 -03

1, 1-Dichloropropene : ND ug I L 1 0. 1 05-07 -03 05-07-0~.

1,2 Dibromoethane (EDB) ND ug I L 1 0. 1 05-07 -03 05-07-0? ---------+-------------------+------+-------+------------··-·-+···-----·-··-

95-50-1 1,2 Dichlorobenzene ND ug IL 0.1 05-07-03 05-07-03 ------t--------~---

107-06-2 1,2 Dichloroethane (EDC) ND ug IL 0.1 __[______ 05-07-03 05-07-0~

78-87-5 1,2 Dichloropropane ND ug IL 1 0.1 ... -·- -----+-------+

96-18-4 1,2,3 Trichloropropane ND ug IL 1 0.1

05-07-03 05-07 -Di

05-07 -03 05-07 -03 ---+-------------+--------1-----+----+-

0.5 1---i 05-07-03 05-07-0~ - -----r-~ 87 -61 -6 1,2,3-Trichlorobenzene ND ug IL 1

ND , ug IL -1-- ---.-·t--- ·--- -

95-63-6 1,2,4-Trimethylbenzene ND ' ug I L

1 120-82-1 1,2,4-Trichlorobenzene

96-12-8 1,2-Dibromo-3-chloropropaneT--ND-- -~ -ug ll 1

- ----·-·- ----------------------541-73-1 1,3 Dichlorobenzene _ ~---- ug IL [

0.5 ' 05-07-03 05-07-0~

05-07-03 05-07-03

05-07 -03 05-07 -0~

05-07 -03 05-07 -0~


STANDARD



Client:

Project:



Sample: MW- #4

Matrix: GW

QC Group

0304502-03A X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

Page 11 of 27

Run Sequence

XG.2003.814.21

XG.2003.814.21

XG.2003.814.21

XG.2003.814.21

XG.2003.814.21

XG.2003.814.21

XG.2003.814.21

XG.2003.814.21

XG.2003.814.21

XG.2003.814.21

XG.2003.814.21

XG.2003.814.21

XG.2003.814.21

XG.2003.814.21

XG.2003.814.21

XG.2003.814.21

XG.2003.814.21

XG.2003.814.21

XG.2003.814.21

XG.2003.814.21

XG.2003.814.21

XG.2003.814.21

XG.2003.814.21

XG.2003.814.21

XG.2003.814.21

XG.2003.814.21

XG.2003.814.21

XG.2003.814.21

XG.2003.814.21

XG.2003.814.21

XG.2003.814.21

XG.2003.814.21

XG.2003.814.21

XG.2003.814.21

XG.2003.814.21

XG.2003.814.21

XG.2003.814.21

XG.2003.814.21

XG.2003.814.21

XG.2003.814.21

XG.2003.814.21

XG.2003.814.21

Collected: 04-23-03 17:40:00 By: SP




_100~~~~~- I 1,3,5-Trime.!_hylbenzen_e __ +--__ ND -~g}_l:_r--1 o.1 ____ -+------

142-28-9 I 1,3-Dic~loropropane ND ___ --~J--~-- _ 0.2 106-46-7 ! 1,4 Dichlorobenzene ND ug I L I 1 0.1

1,4-lsopropyitoi;_;-ene----+---ND - ; ug IL - t----1---t--0:1·---------------- ___ ___J_ ___________ -

- --

99-87-6 ----~I -----

594-20-7 2,2-Dichloropropane ND j ug I L 0.2 --95-_49_a ____ i______ 2-Chlorotoluene -- -- -- --------NO___ r -~Q-/i- ----- +------ 0.1 -- -,---

~,'~; I ~4:";~;~~;~eoe ! H: ::_' H:; ~ t : ~ n- ,-::_ --

108-86-1 I -- --- -- Bromobenzene r N_D ___ ug/ L I 1 0.1 f -- -1

--~-Bromochloromethane I-- ND "ug-/ L--~ -- 1----- 6 1 +--- I

;::::~ Bmm~:~:;:::'h'"e i -=- ,"f ,_ _ *:_ ~ -=_: l ~ -r 74-83-9 Bromomethane ______ f\lD_____ ug IL __ ~ __ 1 _t_ O.~ __ - I

' 15

06

~~93

;~7 Ca~h~:r~e~~:~~~:de ~~ ~~<t j--+-+-t~-1-~ -124-48-"1 Chlorodibromomethane 0.15 ug /I--j--~(~-~-0~1 __ l_~~-~,

i~ .. c:~;;:::::. ~~ ~T-=-!= ti~= 1~~:~~~~~51-- c~~~~1.~2d~~~~~~0p~~;:n6e 1- -- ~~ ---~:--{~~1~-=~-~== H~-=L- '

74-95-3 · Dibromomethane ND ----:--ugf-L 1 -- I - O 1 -+-----~o5~;~~~4 I- Et~~:oenn~~ne ____ -~6 -$~ ~~=r---H4=-

- _ __fl7_:_~8:_:__ Hexachlorobutadiene ND ug IL-- 1 L 0.1 r_ - -98-82-8 lsopropylbenzen~ ___ T~--ND ___lj_g_~_ 0.1 J __ _ 75-09-2 ____ l\tl~t~ylene chloride-----+- __ N_D_ ug IL O ~ _ ~----~ 91-20~ Naphthalene J_ ND ug IL 1 104-51-0 ---- - n~-B-utylbenzene ----- · -- -ND- - ug / L 0.1

103-65-1 n-Propylbenzene ND ug IL 0.1

95-47-6 o-Xylene ND ug IL ---

108-38- p/m-Xylenes 3/1 06-42 ----- ~ - - ----

' 135-98-fl_ - ---- sec-Butyl~:_nzene -- -- I - t-.1_[) __ ~-T ug~ L __ L__1= r-- o1 ~~~-1

100-42-_5 s~~!ene I ND i _ug I L __ t_ 1 ___ _()~---- -- I

156-60-5 t-1,2 Dichloroethene ND ug I L 1 0.1 10061-02-6 I t-1,3 Dichloropropene --~~ug IL - ,-----01--~,---

·-------f------- __ , ___________ _j_

tert-Butylbenzene ND : ug IL ! 1 . 0.1 , 98-06-6

Tetrachloroethylene 2.4 i ugiL- ~--1--;--·o.:i--1--~ Toluene -~--T-ug Tl_ L 1 t· o.3 T -- 1

79-~1-6 Trichloroethene ND--TU91L _____ 1-- t 0.1 r - I

~::~~~-4--+ __ T_r_ic_h_~-i~o;;uc%~~;~han_e ____ ~~ j _~~~r=} __ :_~_-~} ~*+-~-~ _-: 127-18-4

108-88-3

05-07 -03 05-07 -03

05-07-03 05-07-03

05-07-03 05-07-03

05-07-03 05-07-03

05-07-03 05-07-03

05-07 -03 05-07 -03

05-07-03 05-07 -03

05-07 -03 05-07 -03

05-07 -03 05-07 -03

05-07-03 05-07-03

05-07-03 05-07-03

05-07-03 05-07-03

05-07 -03 05-07 -03

05-07-03 05-07-03

05-07 -03 05-07 -03

05-07-03 05-07-03

05-07-03 05-07-03

05-07 -03 05-07 -03

05-07 -03 05-07 -03

05-07-03 05-07-03

05-07-03 05-07-03

05-07-03 05-07-03

05-07 -03 05-07 -03

05-07 -03 05-07 -03

05-07 -03 05-07 -03

05-07 -03 05-07 -03

05-07-03 05-07-03

05-07-03 05-07-03

05-07-03 05-07-03

05-07-03 05-07 -03

05-07 -03 05-07 -03

05-07 -03 05-07 -03

05-07-03 05-07 -03

05-07 -03 05-07 -03

05-07-03 05-07-03

05-07 -03 05-07 -03

05-07 -03 05-07 -03

05-07 -03 05-07 -03

05-07-03 05-07-03

05-07-03 05-07-03

05-07-03 05-07-03

05-07 -03 05-07 -03

Coyote 2001: Reports 1. 0. 011109162500 Report Date 61412003 12:09:57 PM

STANDARD



Client:

Project:



Sample: MW- #4

Matrix: GW

QC Group

0304502-038 X03200

X03200

0304502-03C X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

Page 12 of 27

Run Sequence

XG.2003.727.16

XG.2003.727.16

XG.2003.709.15

XG.2003.709.15

XG.2003.709.15

XG.2003.709.15

XG.2003. 709.15

XG.2003.709.15

XG.2003.709.15

XG.2003.709.15

XG.2003.709.15

XG.2003.709.15

XG.2003.709.15

XG.2003.709.15

XG.2003.709.15

XG.2003. 709.15

XG.2003. 709.15

XG.2003. 709.15

XG.2003. 709.15

XG.2003. 709.15

XG.2003. 709.15

XG.2003. 709.15

XG.2003. 709.15

XG.2003. 709.15

XG.2003. 709.15

XG.2003. 709.15

XG.2003.709.15

XG.2003.709.15

XG.2003.709.15

XG.2003.709.15

XG.2003.709.15

XG.2003.709.15

XG.2003.709.15

XG.2003.709.15

XG.2003.709.15

XG.2003.709.15

XG.2003. 709.15

XG.2003. 709.15

XG.2003.709.15

XG.2003. 709.15

XG.2003.709.15

CAS# Analyte

EPA 504 ED81D8CP by GC/ECD

Collected: 04-23-03 17:40:00 By: SP

Dilution Detection

Result Units Factor Limit Code

By: ALG

Prep

Date

Run

Date

1

---_ ___ _ 1,2-Dibromo-3-chloropropane ND ug I L 1

1,2-Dibromoethane, EDB ND ug I L ~----~--

~--·,---·~:~f}=r~~ 05-05-03 05-05-0:.'

05-05-03 05-05-03

! I

SW846 35108/82708 SVOCs by GC/MS 20-82-1 1,2,4-Trichlorobenzene ND ug IL

. -95-50-1 1,2-Dichlorobenzene ND ug IL

5 41-73-1 1,3-Dichlorobenzene ND ug IL -·-·-

06-46-7 1,4-Dichlorobenzene i ND ug IL .. ___ .. _ --- ··-

I 90-12-0 1-Methylnaphthalene ND _J ug IL ---------58-90-2 2,3,4,6-Tetrachlorophenol i ND ug IL I -- --- ------------95-95-4 2,4,5-Trichloro henol ND I u IL 88~06~2-1--2-,4-.-6--T-r-ic_h_lo-ro~henOT----l---N-D--~· u: I L

120-83-2 I 2,4-Dichlorophenol ND : ug IL f----

i 1

! 1

1 ~--· --·-·

1 , ___ -------

1 --- -----

1 ·I ---- -------

1

By: JM/KAR -----------~--]

1

5

I

----+---· I

--!----------+--

5

5

5

105-67-9 2,4-Dimethylphenol ND I ug IL 1

1--+--~

_5_1_-28-5 _________ 2_,4_-_D_in_it_ro_p_h_e_n_o_I -----~----~~----+ ug l[_ 1---+- 10 121-14-2 2,4-Dinitrotoluene ' ND ug IL 1 ' 5

1

69_01-~~-28--~;-2--+---2--2-~-~-~~-:o-n n __ it:-~-~-:~-:-,:-~-e----1-~, __ --_-----~-~--+--~-:-~-~-+-1: =++--~ ---:---1 ·95-=s7-=-_8_-_--+----2_-C_h_lo_r_op_h_e_n_ol __ ~--=--= ____ _N_D ___ ug l_l____j __ 1 +-=-~- ~-C-J

91-57-6 2-Methylnaphthalene ND ug IL 1

1 1

1 : -9-5----48 ___ 7 ---r----2---M-ethylphenol ND I ug I L ;-- i---: 1--~---j

88-74-4 2-Nitroaniline -ND--j -u9fLI 1--r --5 - -=--- 1

88-75-5 2-Nitrophenol ND - ug IL i--1 -~--5-~-91_-_9_4 __ -1_+-__ 3_,3_-_D_ic_h_lo_ro_b_e_n_z_id_in_e ___ -,----~- _ ~ _ ug_J ~ ~ __ I- _ 10 _l_ -

==9=9-=09=-=2========3=-+-:--~-i:-r~-ha_Y~-~l-~ne_:_o_l _______ +-----~---f-<~; ~-- ___ 1

___ J ~ J

534-52-1 4,6-Dinitro-2-methylphenol ND I ug IL I 1 O

04-28-03 04-29-0~.

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-0~,

04-28-03 04-29-0'.'

04-28-03 04-29-03

04-28-03

04-28-03

04-29-0:,C

04-29-0:'

04-28-03 04-29-03

04-28-03 04-29-0'.>·

04-28-03 04-29-0:'

04-28-03 04-29-03

04-28-03 04-29-0s

04-28-03 04-29-0:'

04-28-03 04-29-03

04-28-03 04-29-0s

04-28-03 04-29-0:

04-28-03 04-29-03

04-28-03 04-29-o:r

04-28-03 04-29-m

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-0:

101-55-3 4-Bromophenyl-phenylether ND I ug IL 1 i 04-28-03 04-29-03 ---------T-·--------

59-50-7 4-Chloro-3-methylphenol ND ug I L 5 04-28-03 04-29-03 ----+------106-47 -8 i 4-Chloroaniline ND ug IL 5

7005-72-3 ' 4-Chlorophenyl-phenylether ND ug I L T--:,·-- -, ------------------+-----------+---------- - ··- __________ ,

04-28-03 04-29-0:

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-0'.

04-28-03 04-29-03

04-28-03 04-29-03

100-01-6 4-Nitroaniline ND ug IL 1

100-02-7 4-Nitrophenol ND ug IL

83-32-9 Acenaphthene ND ug I L -------- -------------~----- - .. ---- -r-

26~I~93~~-- ---~-~~n:~i~~!~~E!--· ··· I- ~~ ug IL -- --t---

5

10

-·------------- ---f-·

10 ug IL 12"0~-1·2:;-+----- ------A-n-th_r_a_c-en_e ________ i ND i -~Q/L--~- - 1----~---1------- .. I------·-

I 04~28~03 04~29-0~

04-28-03 04-29-0:.' --------+-------------4-- --------- __ [ ________ _J_ ___ _j_ ______ ---- - --- _,

Azobenzene&1,2- I ___ ND _I ug/L -'---1 __ f ____ L __ ~_J 04-28-03

Diphenylhydrazi~E'._ ___ ---------------,

04-29-03

56-55-3 Benzo (a) anthracene ND ug IL

1

_ 1, _ ~ 11~ ==1

=I 50-32-8 Benzo(a)pyrene ND ug I L I

---1--B_e_n_zo_(_b_&_k_)f_lu_o_ra __ n_th_e_n_e_--1 ___ N_D __ -_ -c~ -_ -_u=g=-/-L_..,. ____ 1____ . 1 __ J ___ I 191-24-2 Benzo(g,h,i)perylene _ __,. __ N_D __ ~ug IL ___ _2 __ 1 __ 1 _ _j·-___ _ 6_4_-8_5_-o_~ ____ B_e_n_z_oi_c_a_c_id ____ ~ ____ N_D ___ ~u_g_/ L_~_ 1__ L ~ _ •

04-28-03 04-29-03

04-28-03 04-29-0~

04-28-03 04-29-0:

04-28-03 04-29-03

04-28-03 04-29-o:r




Client:

Project:



Sample: MW- #4

Matrix: GW

QC Group

0304502-03C X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

0304502-03D X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

Run Sequence

XG.2003.709.15

XG.2003.709.15

XG.2003.709.15

XG.2003. 709.15

XG.2003.709.15

XG.2003.709.15

XG 2003. 709.15

XG.2003. 709.15

XG.2003.709.15

XG.2003.709.15

XG.2003. 709.15

XG.2003. 709.15

XG.2003. 709.15

XG.2003. 709.15

XG.2003.709.15

XG.2003.709.15

XG.2003.709.15

XG.2003. 709.15

XG.2003. 709.15

XG.2003. 709.15

XG.2003. 709.15

XG.2003. 709.15

XG.2003. 709.15

XG.2003. 709.15

XG.2003.709.15

XG.2003. 709.15

XG.2003.709.15

XG.2003.709.15

XG.2003.709.15

XG.2003.709.15

XG.2003. 709.15

XG.2003.785.31

XG.2003.785.31

XG.2003.785.31

XG.2003.785.31

XG.2003.785.31

XG.2003.785.31

XG.2003.785.31

XG.2003.785.31

XG.2003.785.31

XG.2003.785.31

Collected: 04-23-03 17:40:00 By: SP

Dilution Detection


SW846 351 OB/82708 SVOCs by GC/MS By: JM/KAR

100-51-6 Benzyl alcohol ND

ND

ND

ug IL 5 ------~---- ------- ----

111-44-4

111-91-1

bis (2-Chloroethyl) ether

bis(2-Chloroethoxy)methane ·----------· ---+--

ug IL

! ug IL

108-60-1 bis(2-Chloroisopropyl)ether ND 1 ug IL ---------· ----

117-81-7 bis(2-Ethylhexyl)phthalate 5.4 ug IL ·----+-----------------------c--- --------- ---

_8_5_-6_8_-7_+----- Butylbenzylphthalate ND ___ ll_9 l_l I 1

- j - ·1

1 I 5 -t--B I . -1--1 -+-- ---

~; !- D;b:~[~~~~~oe -J.l · I-~! it I ==l=~= u~ ~ - -

--13-1--11--3------- D._i_m_e-th-y-lp-.~-_th_a_la-te ______ -__ -__ -_--+-+-·=--·N_D __ _,.__u_g _/ _L_ L __ 1 __ ·--- -~ _J~ ____ J

B4-7~-~-L di-n-Butylphthalate · ND ug I L 1

1 1 117-84-0 I di-n-Octylphthalate ND i - ug IL __ 1 ___ - - . 1 - ---

---1-----. ------ -·--206-44-0 Fluoranthene ND ug IL ----------- - ---- --~·--------

86737 -- -----

118-74-1

87-68-3

77-47-4 -----

67-72-1

193-39-5

78-59-1 -----

91-20-3 ---- -- ------98-95-3 ------

62-75-9

621-64-7

86-30-6

Fluorene

Hexachlorobenzene - -----

Hexachlorobutadiene

ND

ND

ND

ug IL 1

-~ _______ :___ 10 ug IL ! 1 1 O ene--r --N-D---1--u_g_/_L _f ____ , __ .. 1 o ·---·-----·

Hexach lorocyclope ntad i

Hexachloroethane --r-ND-- ug IL I 5

ug I~ I lndenc(1,2,3-cd)pyren -----·--·--

e ND

lsophorone ND ug IL r------- --------------·--·- -

ND ug IL I

I ND ug IL I ·--+-··-·----- --· ·- -···---·- f--· -- --·- ---

~~ -- I ND __ - U_tJ_!_L_ L -- _ 10

Naphthalene ----·----

Nitrobenzene 1------------ - ---·-· ·-- ------------

n-Nitroso-dimethyl-ami

;e-+J_ __ ~~ --- ~~ ~ ~ -t-- ~------ ~ n-Nitroso-di-n-propylam --------------

n-Nitrosodiphenylamin

----1--

.87~86~-~~]__ _P_e_n-ta_c_h-lo-r-op_h_e_n_o_I . __ ND ____ u_g_/L T 1-- -- 1-0

85-01-8 Phenanthrene --:-----ND - ug I L · t 1 1 _ ~ __ _

;_;~-:-~~-:-:-+-------_-·--:-J-r!:--~n-:: ~~ - I :n · J ~t= SW846 3510818081A Pesticides by GCIECD

--- ""T .. ----- ------,-------------1------;---

a-BHC i ND I ug I L j 1 1 0.1 --------· ··a::c11i0rdane------r--ND-.-i -ug/L [ 1-- + 0.1

309-00-2 Aldrin I ND --i----ug/L- I . - . 1 - - " ______ b ___ B_H_C --- ,- -- ND ug_fL_~

-------· ... ··- t

Chlo~~~~e~ total ---t-. --~~ __ ---~-~+~ f

---- ---··- ----- --------------+-------57-74-9

60-57-1 Dieldrin I ND ! ug IL

0.1

0.1

0.1

0.1

0.1

By: ALG

Eilci05Uifanl-- --I N_D ____ u_g_t_L_ ,-~--=--~=-~~_1 =~===~= Endosulfan II ----+ ND

! Endosulfan Sulfate 1 ND

ug IL

ug IL

0.1

0.1

STANDARD

Prep Run

Date Date

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-30-03 05-09-03

04-30-03 05-09-03

04-30-03 05-09-03

04-30-03 05-09-03

04-30-03 05-09-03

04-30-03 05-09-03

04-30-03 05-09-03

04-30-03 05-09-03

04-30-03 05-09-03

04-30-03 05-09-03

Page 13 of 27 Coyote 2001: Reports 1. 0. 011109162500 Report Date 61412003 12:11:04 PM

Client:

Project:

Order:





0304502 PHl16 Receipt: 04-24-03

STAN DAR[

·---------- ----·-- ------------------ -------Sample: MW- #4

Matrix: GW

QC Group

0304502-03D X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

0304502-03D X03189

X03189

X03189

X03189

X03189

X03189

X03189

0304502-03E M03548

M03548

M03548

M03548

0304502-03E M03550

M03550

M03550

M03550

M03550

M03550

M03550

M03550

M03550

M03550

M03550

M03550

0304502-03E M03559

Page 14 of 27

Run Sequence

XG.2003.785.31

XG.2003.785.31

XG.2003.785.31

XG.2003.785.31

XG.2003.785.31

XG.2003.785.31

XG.2003.785.31

XG.2003.785.31

XG.2003.785.31

XG.2003.785.31

XG.2003.785.31

XG.2003.785.31

XG.2003. 750.21

XG.2003. 750.21

XG.2003. 750.21

XG.2003. 750.21

XG.2003.750.21

XG.2003.750.21

XG.2003.750.21

MT.2003.521.23

MT.2003.511.46

MT.2003.511.46

MT.2003.521.23

MT.2003.551.40

MT.2003.577.15

MT.2003.551.40

MT.2003.551.40

MT.2003.551.40

MT.2003.551.40

MT.2003.551.40

MT.2003.551.40

MT.2003.551.40

MT.2003.551.40

MT.2003.551.40

MT.2003.551.40

MT.2003.522.29

Collected: 04-23-03 17:40:00 By: SP

Dilution Detection


SW846 3510Bl8081A Pesticides by GC/ECD 72-20-8 Endrin ND I ug IL 1 0.1

------

Endrin Aldehyde ND I ug IL 1 I 0.1 - - ------

' ND I ug IL -------t-------

Endrin Ketone 1 I 0.1 ---·-·-------- ----- ... ----- ·-+- --------- , ..

1 ---

58-89-9 g-BHC ND I ug IL 1 0.1

--------- -------- -

I r--

g-Chlordane ND ug IL 1 I 0.1 ---------- -·-- ·- ---- -- ----- l--- - ----

76-44-8 Heptachlor ND I ug IL 1 j 0.1

He~:~~~:y~~1~~ide-- t~-~~ ~~=--r--~: ~I --·---

1024-57-3 .. ~ ·-+- ~:~ 72-43-5 -- ------

6088-51-3 p,p-DDD ND I ug I L 1 0.1

p,p-DDE ND I

ug IL 1 0.1 50-29-3 p,p-DDT ND I ug IL 1 0.1

8001-35-2 Toxaphene, total ND ! ug IL 1 ! 2.5 I --

SW846 3510Bl8082 PCBs by GCIECD By: ALG

~~r~1~~=-~! -~----

T --- ----·- ----12674-11-2 Aroclor 1016 ND ug IL I 1

----- ---·------·-· - ---- ------t---- __ ,, ___ -1 -- .

11104-28-2 Aroclor 1221 ND : ug IL I 1 i

0.5 I

0.5 1---~ ~t_-_-+----j

0.5

11141-16-5 Aroclor 1232 ND I ug IL I 1 ·----~-

53469-21-9 Aroclor 1242 ND I ug IL I 1 -- +---------

I 12672-29-6 Aroclor 1248 ~~--1

ug IL I 1 I

·- ----- ., --- --11097-69-1 i Aroclor 1254 ug IL ' 1

-.

11096-82-5 i Aroclor 1260 ND I ug IL 1

SW846 3005A/601 OA ICP By: JRE 7440-4_1_-7 ______ B_e_ry_l_liu_m _______ N_D ____ m_g_/ L--! --1---0-.0-0_2_J__' -··--=--7_ 4_4 __ o ___ -_47-3_j Chromium 0.01 mg IL ; 1 O 01 L_ 7440-48-4-T cobalt I ND G_l_'=._~ __ 1 _ _[_-o~oi--=1----~ 7440-5_0_-8~1 --- ·-CO£>~!______ t-JD ___ - L ~g IL ' 1 i 0.01 ! u _ _J

SW846 3005A6020 ICP-MS By: HMR 7440-36-0 i Antimony ! ND , mg IL o.ooi--T-- -744o~3a:2---- Arsenic ----r---o:0o1 ___ r mg IL 1 , 0.001 r---~::~:~::: ! c~::~~m ~-~--~::~-~ . ~-~HF ~~~~-~ H ··· 1----=

·-----L------··-------·---·--·---- ·-··---··-···---------~-- --t--·-·---

7439-92-1 · Lead 0.001 mg IL 1 ____ j _ ?·D_01 _-tl __ -j 7440-02-0 : Nickel 0.007 mg IL 1 0.001 i 7782-49-2 I Selenium 0.001 mg I L 1 0.001

7440-22-4 : Silver ND mg IL 1 0.001 -f------+--------j

7440-28-0 ! Thallium ND mg/L 0.001 -------~

7440-31-5 ' Tin ND mg/L 0.001 !

Vanadium t------"-

0.002 mg/L 0.001 -------··-·---· -·· --

7440-62-2 I

7440-66-6 Zinc 0.021 L lllil_1 ~__J o.09_~ __ L_

SW846 7470 Mercury by CVAA By: JRE --------------

-~--N_D_~1_·-_;;,-g_--,_-~=1 . H1_=i__(l.()9~~J--. ----=] Mercury ----

Prep Run

Date Date

04-30-03 05-09-0: .,,,

04-30-03 05-09-0l

04-30-03 05-09-03'

04-30-03 05-09-0:' ... 04-30-03 05-09-03,

04-30-03 05-09-03'

04-30-03 05-09-0:

04-30-03 05-09-03

04-30-03 05-09-03

04-30-03 05-09-0:

04-30-03 05-09-03

04-30-03 05-09-03

04-30-03 05-07-0:.

04-30-03 05-07-0'.'

04-30-03 05-07-03

04-30-03 05-07-0:

04-30-03 05-07-0?

04-30-03 05-07-03

04-30-03 05-07-0:.

04-30-03 05-01-0'.'

04-30-03 05-01-03

04-30-03 05-01-0::.

04-30-03 05-01-02

04-30-03 05-05-03

04-30-03 05-13-0::.

04-30-03 05-05-02

04-30-03 05-05-03

04-30-03 05-05-0~

04-30-03 05-05-0:'

04-30-03 05-05-03

04-30-03 05-05-0'1

04-30-03

04-30-03

04-30-03

04-30-03

05-05-0~

05-05-03

05-05-00

05-05-0:

05-01-03 05-01-03

Coyote 2001: Reporls 1.0.011109162500 Reporl Date 61412003 12:12:04 PM

Client:

Project:






Sample: FIELD BLANK Collected: 04-23-03 19:05:00 By: SP

Matrix: W

Dilution Detection

QC Group Run Sequence CAS# Analyte Result Units Factor Limit Code

0304502-04A X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

·xo3206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

XG.2003.814.24

XG.2003.814.24

XG.2003.814.24

XG.2003.814.24

XG.2003.814.24

XG.2003.814.24

XG.2003.814.24

XG.2003.814.24

XG.2003.814.24

XG.2003.814.24

XG.2003.814.24

XG.2003.814.24

XG.2003.814.24

XG.2003.814.24

XG.2003.814.24

XG.2003.814.24

XG.2003.814.24

XG.2003.814.24

XG.2003.814.24

XG.2003.814.24

XG.2003.814.24

XG.2003.814.24

XG.2003.814.24

XG.2003.814.24

XG.2003.814.24

XG.2003.814.24

XG.2003.814.24

XG.2003.814.24

XG.2003.814.24

XG.2003.814.24

XG.2003.814.24

XG.2003.814.24

XG.2003.814.24

XG.2003.814.24

XG.2003.814.24

XG.2003.814.24

XG.2003.814.24

XG.2003.814.24

XG.2003.814.24

XG.2003.814.24

XG.2003.814.24

XG.2003.814.24

XG.2003.814.24

EPA 524.2 rev 4 Purgeable VOCs by GCIMS By:

75-34-3 1, 1 Dichloroethane ND ug I L 0.1 ---------

75-35-4 1, 1 Dichloroethene ND ug I L 0.1 ·----+--------------------+------+------+---

71-55-6 1,1,1 Trichloroethane ND ug IL 0.1 ----j---~---

630-20-6 1, 1, 1,2 Tetrachloroethane 1

ND ug I L 0.1 79-00-5 1, 1,2 Trichloroethane--IN-D-- , ug I L

79-34:5· 1, 1,2,2 Tetrachloroethane - I - -ND- - j ug IL

~~::::::-~r--·--1-,2_1_~-i~-~-~:-h-~o-:-;h-~-~-:-~-~e-~B) r ----~~. _j ~~ ~ ~ --------------+-

I 0.1

0.1

95-50-1 1,2 Dichlorobenzene I ND i ug I L 0.1

1oi-06Tt- ___ 1_c~ Di_ch_lo_r_oe_th_a_ne:_J~~C) I~ ~--H~-- --~-: _u~g_I~ ----+---~·1 __ _ 78-87-5 1,2 Dichloropropane ND : ug IL 1 0.1

--- ND ---~~9/L- _____ ! ___ 0.-1- ··-·· ·- ---- ------- - -- --- ·-- -- - -----~------

96-18-4 1,2,3 Trichloropropane -------i-· -

-~~- - - ug_!~- -----'-----~ 87-61-6 : 1,2,3-Trichlorobenzene ---·-·-·-'·--·-·---- ------

120-82-1 1 1,2,4-Trichlorobenzene ND ug IL 0.5 95-63=6- r - - -1~2,4-Trini~nzene--

----------1------------ ---~----

ND ug IL

---~-~----- ~ _ ug IL __ I 96-12-8 ·11

541-73-1

1oa:57:sl

142-28-9 I

106-46-7

99-87-6

594-20-7

95-49-8

106-43-4

71-43-2

108-86-1

56-23-5

74-95-3

100-41-4

1,2-Dibromo-3-chloropropane

1,3 Dichlorobenzene --+ __ ND ! ug I L 1,3,5-Trimethylbenzene ND ug IL

1,3-Dichloropropane ND ug IL

1 ,4 Dichlorobenzene ND ug IL - +--

JAA

--------------r------ ------ -

ND

ND

ug IL

ug IL

L _Uf:l '~-- c __ _

0.1 0.1----i

0.1

STANDARD

Prep

Date

Run

Date

05-07 -03 05-08-03

05-07-03 05-08-03

05-07 -03 05-08-03

05-07 -03 05-08-03

05-07 -03 05-08-03

05-07-03 05-08-03

I 05-07-03 05-08-03

05-07-03 05-08-03

05-07 -03 05-08-03

05-07 -03 05-08-03

05-07-03 05-08-03

05-07 -03 05-08-03

05-07 -03 05-08-03

05-07 -03 05-08-03

05-07-03 05-08-03

05-07 -03 05-08-03

05-07 -03 05-08-03

05-07 -03 05-08-03

05-07-03 05-08-03

05-07-03 05-08-03

05-07-03 05-08-03

05-07-03 05-08-03

05-07 -03 05-08-03

05-07-03 05-08-03

05-07 -03 05-08-03

05-07-03 05-08-03

05-07 -03 05-08-03


STAN DARI



Client:

Project:



Sample: FIELD BLANK Matrix: W

QC Group

0304502-04A

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

0304502-048

X03200

X03200

Run Sequence

XG.2003.814.24

XG.2003.814.24

XG.2003.814.24

XG.2003.814.24

XG.2003.814.24

XG.2003.814.24

XG.2003.814.24

XG.2003.814.24

XG.2003.814.24

XG.2003.814.24

XG.2003.814.24

XG.2003.814.24

XG.2003.814.24

XG.2003.814.24

XG.2003.814.24

XG.2003.814.24

XG.2003.727.17

XG.2003.727.17

Sample: MW- #1

Matrix: GW

QC Group

0304502-05A

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

Page 16 of 27

Run Sequence

XG.2003.814.22

XG.2003.814.22

XG.2003.814.22

XG.2003.814.22

XG.2003.814.22

XG.2003.814.22

XG.2003.814.22

XG.2003.814.22

XG.2003.814.22

XG.2003.814.22

XG.2003.814.22

XG.2003.814.22

XG.2003.814.22

XG.2003.814.22

XG.2003.814.22

Collected: 04-23-03 19:05:00 By: SP



EPA 524.2 rev 4 Purgeable VOCs by GCIMS By: JAA --·· -No- __ i_Lig_IL]--1--r-0~5-- -- - --1 o5-o7-o3 05-08-0· -·---

75-09-2 Methylene chloride

91-20-3 Naphthalene ----~~ ~·

----r __ N_D_ --~'-~- (_ 1 C"}-- ---1 05-07-03 05-08-03

104-51-8 n-Butylbenzene ND ug IL ! I 0.1 05-07-03 05-08-00

ND · ug IL t 1 1 o 1 · 05-07-03 05-08-0'

==-=-=--=-:-_-_-~-~-:~-~---~r H---~r~:;---- --~: ~::~~:~: ~::~::~: -103-65-1 n-Propylbenzene

95-47-6 a-Xylene ----- ·-

108-38- p/m-Xylenes 3/106-42 ~-

135-98-8 sec-Butylbenzene ND ug IL 1----o.1 05-07-03 05-08-03

100-42-5 Styrene 0.1 --

156-60-5 t-1,2 Dichloroethen --1-

I 10061-02-6 t-1,3 Dichloropropen e I ND ' ug IL -- ·------1· - -----------------·----- I-0.1

0.1

0.1

---~

05-07 -03 05-08-0.

05-07-03 05-08-0?

05-07 -03 05-08-03

05-07 -03 05-08-0 98-06-6 ! tert-Butylbenzene ND ug I L I

Tetrachloroethylene ND

Toluene ND 1~:7=:18-4 I 108-88-3

I 79-01-6 ! Trichloroethene ND -~--------

75-69 -4 Trichlorofluoromethane ND

75-01-4 Vinyl chloride ND

-- --ug IL

! ug IL

ug IL

ug IL

ug IL 1

0.1 05-07-03 05-08-03

0. 3 I 05-07 -03 05-08-03 --· 1----- -----1

0. 1 ! 05-07 -03 05-08-0

0. 1 . . . - ! 05-07-03 05-08-0~ f-----t---J ~- __ L__ 05-07-03 05-08-03

EPA 504 EDB/DBCP by GCIECD By: ALG

1------------t---1_,2_-D_ib_ro_m_o_-_3_-c_h_lo_ro_p_r_op_a_n_e _ _,_-_-~~-N_D __ -__,._u_g-_f_L- - --1-- H r 0.025 l -~--1,_2_-D_i_br_o_m_o_et_h_a_ne_,_E_D_B __ ~ ___ ND ______ ug_~_~_J ___ ! ___ j_ 0.025_~ __ ]

Collected: 04-23-03 19:00:00 By: SP

Dilution Detection


EPA 524.2 rev 4 Purgeable VOCs by GCIMS By: JAA

75-34-3 1, 1 Dichloroethane ND ug IL 0.1

05-05-03 05-06-0~.

05-05-03 05-06-0?

Prep Run

Date Date

05-07 -03 05-07 -03

05-07-03 05-07-0,

05-07 -03 05-07 -0:'

05-07-03 05-07-0:i

05-07 -03 05-07 -0:.

05-07 -03 05-07 -o-

05-07 -03 05-07 -03

05-07 -03 05-07 -0<

05-07-03 05-07-0-

05-07 -03 05-07 -03

05-07 -03 05-07 -0"

05-07-03 05-07-0'

05-07-03 05-07-03

05-07 -03 05-07 -0~

05-07 -03 05-07 -0'


STANDARD



Client:

Project:



Sample: MW- #1

Matrix: GW

QC Group

0304502-05A

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

Page 17 of 27

Run Sequence

XG.2003.814.22

XG.2003.814.22

XG.2003.814.22

XG.2003.814.22

XG.2003.814.22

XG.2003.814.22

XG.2003.814.22

XG.2003.814.22

XG.2003.814.22

XG.2003.814.22

XG.2003.814.22

XG.2003.814.22

XG.2003.814.22

XG.2003.814.22

XG.2003.814.22

XG.2003.814.22

XG.2003.814.22

XG.2003.814.22

XG.2003.814.22

XG.2003.814.22

XG.2003.814.22

XG.2003.814.22

XG.2003.814.22

XG.2003.814.22

XG.2003.814.22

XG.2003.814.22

XG.2003.814.22

XG.2003.814.22

XG.2003.814.22

XG.2003.814.22

XG.2003.814.22

XG.2003.814.22

XG.2003.814.22

XG.2003.814.22

XG.2003.814.22

XG.2003.814.22

XG.2003.814.22

XG.2003.814.22

XG.2003.814.22

XG.2003.814.22

XG.2003.814.22

XG.2003.814.22

Collected: 04-23-03 19:00:00 By: SP

--- ------------ -------------,--·-·

CAS# Analyte Result Units

Dilution Detection

Factor Limit

Prep Run

Code Date Date

EPA 524.2 rev 4 Purgeable VOCs by GC/MS

96-12-8 1,2-Dibromo-3-chloropropane--T ND ug I L . ------j--------------- -----+----------

By:

0.2

JAA

541-73-1 1,3 Dichlorobenzene I ND ug IL i 0.1

~oa~i--8- _ 1,3,5-Trimethylbenzene I - ~D -~-=-- ug I L --~ - _1 _ 0.1 -+- _ __ I

_1~-28~9-~1 1,3-Dichloroprop~~~------t-- ND I ug I L _ 1 j _ 0.2 .. 1- j 106-46-7 1,4 Dichlorobenzene ND _ ( _ u9_l_L 1 1 __ ~-~~---+--__

1 594-20-7 2,2-Dichloropropane _ 99-87~ 1,4-lsopropyltoluene _NNDD_ t uugg 1

1

LL -+-1-' _ 11___ _ 0

0.21 ___ _)_______' ___ 1

- ~~~~~--~ 2-Chlorotoluene - --NNDD- -- , ~ugg 1

1

LL = __ 1

1

____ 0

0

.11

J 106-43-4 4-Chlorotoluene I

71-43-2 , Benzene ND ; ug IL 1 0.1 J 1aa=a6-_1 ___ sromobenzene___ N-D--l-Li9Tt.:- 0.1 :

- ---.-------------------+--------·--- ... ----+-' Bromochloromethane • ND i ug I L O 1 75-27-4 I Bromodichloromethane _____ --ND- 1 ug IL 0.1

~~::::+~ Br:::;:~~:ne 0~~4--f-~~~~ -f- ~:~ 1506~~:;~~ Ca~h~:r~e~:~:~:de ~+-=~ -~~--_ ----~-~~ 1~-- ___ ~:~ 124-48-1 Chlorodibromomethane _ J-- --~·_2_9 __ ~_LJg__I~--- ____ l_ ____ ~._1 75-00-3 Chloroethane ND ug I L 0.1

67-66-3

74-87-3

156-59-2

10061-01-5 I

74-95-3

100-41-4

75-09-2

91-20-3

-----100-42-5

--- --·----·· ------ --+-----i Chloroform ND ug I L 0.1

--- -------

Chloromethane ND ug I L 0.1

cis-1,2 dichloroethene

cis-1,3 dichloropropen_E!__~ ___ _

Dibromomethane ---------- -----t--

Ethylbenzene 1 - ------ -j

sec-Butylbenzene

Styrene

ND

ND

ND

ND

ND

ug IL

ug IL

ug IL

ug IL

ug IL

ND ug IL ----

ND T-ug /L

0.1

0.1

0.1

0.1

' 156-60-5 t-1,2 Dichloroethene ND

ND

ug IL

ug IL

0.1

0.1

0.1

0.1

0.1

0.1

0.3

- --r------ ---- --- - --

10061-02-6 t-1,3 Dichloropropene

98-06-6 tert-Butylbenzene ND ug IL ---1 - ---

1 -~· ? ____ ~_':-__ I ND ug IL

127-18-4 ----

Tetrachloroethylene

Toluene 108-88-3

-c~=-~D--+----------

79-01-6 -----

Trichloroethene ug/L 1 1 0.1 ·----------- _____ _L ___ -

05-07-03 05-07-03

05-07-03 05-07-03

05-07-03 05-07-03

05-07-03 05-07-03

05-07-03 05-07-03

05-07 -03 05-07 -03

05-07 -03 05-07 -03

05-07 -03 05-07 -03




Client:

Project:



Sample: MW- #1

Matrix: GW

QC Group

0304502-05A

X03206

X03206

0304502-058 X03200

X03200

0304502-05C

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

Page 18 of 27

Run Sequence

XG.2003.814.22

XG.2003.814.22

XG.2003.727.20

XG.2003.727.20

XG.2003. 703.16

XG.2003.703.16

XG.2003.703.16

XG.2003.703.16

XG.2003.703.16

XG.2003. 703.16

XG.2003. 703.16

XG.2003. 703.16

XG.2003.703.16

XG.2003.703.16

XG.2003.703.16

XG.2003.703.16

XG.2003.703.16

XG.2003. 703.16

XG.2003. 703.16

XG.2003. 703.16

XG.2003. 703.16

XG.2003. 703.16

XG.2003. 703.16

XG.2003. 703.16

XG.2003. 703.16

XG.2003.703.16

XG.2003.703.16

XG.2003.703.16

XG.2003.703.16

XG.2003. 703.16

XG.2003. 703.16

XG.2003. 703.16

XG.2003. 703.16

XG.2003. 703.16

XG.2003. 703.16

XG.2003.703.16

XG.2003.703.16

XG.2003.703.16

XG.2003.703.16

-------· ---------·· Collected: 04-23-03 19:0o.·oo By: SP

Dilution Detection



I

=+ T i 75-69-4 Trichlorofluoromethane ND ug/L 1 I 0.1 ----

ug I L . ---1=T-ci.1 i

75-01-4 I Vinyl chloride ND

EPA 504 ED81D8CP by GCIECD By: ALG

E 1,2-Dibromo-3-chloropropane ND ug IL 0.025

I 1,2-Dibromoethane, EDB ND ug IL I 0.025


!=-~R-1-= --- ·- ...... '. . -- . --+-------1 I 1 1 1 1

-I· .. -------- ---f- - --j

1 ~ ·_J ~ r -- -1 5 --~t~ --j------t---

I I 120-82-1 1,2,4-Trichlorobenzene ND i ug IL

I -

1 95-50-1 1,2-Dichlorobenzene ND ug IL

' 541-73-1 ! 1,3-Dichlorobenzene ND ug IL

1()6:45:± --·- ------------ ------

' 1,4-Dichlorobenzene ND ug IL i I

I ,---·-

90-12-0 1-Methylnaphthalene ND ug IL ------·- ·-58-90-2 2,3,4,6-Tetrachlorophenol ND ug IL

I

95-95-4 2,4,5-Trichlorophenol I ND ug IL -

88-06-2 2,4,6-Trichlorophenol ND ug IL ...

! 120-83-2 2,4-Dichlorophenol ND ug IL

Prep

Date

05-07-03

05-07-03

05-05-03

05-05-03

Run

Date

05-07-0:

05-07-03

05-06-0:!

o5-06-o: "

04-28-03 04-29-0:;1

04-28-03 04-29-03

04-28-03 04-29-0:

04-28-03 04-29-03

04-28-03 04-29-01

04-28-03 04-29-0~

04-28-03 04-29-0:.'

04-28-03 04-29-03

04-28-03 04-29-0:. I

105-67-9 2,4-Dimethylphenol ND : ug IL 1 04-28-03 04-29-0~

i I

--I 04-28-03 04-29-03 I 51-28-5 2,4-Dinitrophenol ND i ug IL

·----I 10

-+-------1------- J-----j

121-14-2 2,4-Dinitrotoluene ND ug IL - .. 1 ---- ------

606-20-2 2,6-Dinitrotoluene I ND ). -~_!_I:_ ·-·

5 -- ----1 1 5 1

----------

91-58-7 2-Chloronaphthalene ND ' ug IL

95-57-8 2-Chlorophenol I --f·----ND I ug IL

1 1 ---1--.--1-

91-57-6 2-Methylnaphthalene I ND r-~9·;-c -- - -- ---------· -------~--- -t------95-48-7 2-Methylphenol ND ug IL -----·- --------· 88-74-4 2-Nitroaniline ND ug IL

1 1 i 1 j---1---~--c--- --

-+--__ _______j_ __ -.----· --

5 . ---------

88-75-5 2-Nitrophenol I ND ug IL

91-94-1 3,3-Dichlorobenzidine --+ ND ug IL

5 10

-+----- ------ - ------+------j

3+4 Methylphenol ND -- ---L

ug IL

99-09-2 I 3-Nitroaniline ND ug IL

534-52-1 I 4,6-Dinitro-2-methylphenol ND I ug IL I -5

-+---~-

10 --- ------

101-55-3 I 4-Bromophenyl-phenylether ND ug IL ------~---+-----------· t--------59-50-7 I 4-Chloro-3-methylphenol ND i ug IL

.... -- -- ------ - --ND T ug/L ___ _

ND 1

1 ug IL 1

106-47-8 4-Chloroaniline

7005-72-3 4-Chlorophenyl-phenylether .. -----i-----,- ...

_ND __ -~_1-_f- 1

ND I ug I L I .. 1 ... ----+----··

83-32-9 Acenaphthene ND 1

ug I L. - i--208-96-8 i A_c_e_n_a_p-ht_h_y-le-ne-----+---N-D ___ --r -U'97L-- - -

4-Nitrophenol

100-01-6 4-Nitroaniline

100-02-7

1622;~%-r-- -----· A;h_n:-~c_n;_n_e _______ --+---~-~---:-~-:-~--~ -i·-------c----1· 0--· ----r------1

---------

Azobenzene&1,2- ___ N_IJ____ I ug IL 1

04-28-03 04-29-0~

04-28-03 04-29-0:.'

04-28-03 04-29-03

04-28-03 04-29-0~

04-28-03 04-29-0:.'

04-28-03 04-29-03

04-28-03 04-29-0~

04-28-03 04-29-0:'

04-28-03 04-29-03

04-28-03 04-29-0~

04-28-03 04-29-0~

04-28-03 04-29-03

04-28-03 04-29-0~

04-28-03 04-29-0~

04-28-03 04-29-03

04-28-03 04-29-0~

04-28-03 04-29-0~

04-28-03 04-29-03

04-28-03 04-29-0s

04-28-03 04-29-0:

04-28-03 04-29-03

04-28-03 04-29-0~

04-28-03 04-29-0'. i Diphenylhydrazine

[ _56-55-3 ___ Benzo (a) anthracene N_D_~[_u_g IL L 2 __ _J~_=J---i--_~] 04-28-03 04-29-0~


STANDARD



Client:

Project:



Sample: MW- #1

Matrix: GW

QC Group

0304502-05C X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

0304502-05D , X03194

X03194

X03194

X03194

X03194

X03194

Page 19 of 27

Run Sequence

XG.2003.703.16

XG.2003.703. 16

XG.2003.703. 16

XG.2003. 703.16

XG,2003, 703. 16

XG.2003.703.16

XG.2003.703. 16

XG.2003.703. 16

XG.2003. 703. 16

XG.2003.703. 16

XG.2003.703. 16

XG.2003.703. 16

XG.2003.703. 16

XG.2003.703. 16

XG.2003,703, 16

XG.2003.703. 16

XG.2003.703. 16

XG.2003.703. 16

XG.2003.703.16

XG.2003.703. 16

XG.2003.703. 16

XG.2003.703, 16

XG.2003.703. 16

XG.2003.703.16

XG.2003.703.16

XG.2003.703. 16

XG.2003. 703.16

XG.2003. 703, 16

XG.2003. 703. 16

XG.2003.703. 16

XG.2003.703. 16

XG.2003.703. 16

XG.2003.703. 16

XG.2003.703. 16

XG.2003.703. 16

XG.2003.785.32

XG.2003.785.32

XG.2003.785.32

XG.2003. 785.32

XG.2003. 785.32

XG.2003. 785.32

Collected: 04-23-03 19:00:00 By: SP

Dilution Detection



8enzo(a)pyrene ___ J __ ND ug IL

I Benzo(b & k)fluoranthene J___!'J_I:)__ ____ ~_ ug !_~ _ 191-24-~ __ l_ Benzo(g,h,i)perylene ---+---N_D __ -+_ug I L -+ _________ _

! "·"c' -i- - Be~o!ooo!d ND I "' I L 1 25 ~0_-5_1-6 ___ B_en_z_y~~hCJ_~_ _ ND --··---·~-u~/ L -----1----!--rn 5 111-44-4 bis (2-Chloroethyl) ether ND · ug I L 111-91-1 bts(2-Chloroethoxy)methane ND 1--ug_/L_ 108-60-_1_ bis(2-Chloroisopropyl)ether , =-t-JE_~~J-ugtl- j

B __ 117-8u bis(2-Ethylhexyl)phthalate _ _,1 __ 10 ug IL L +-+- ---~

~~1 ~B;,~~~;,~:~~. I ~~···I :rn i-+~T-+::- · 132-64=9' -+ Dibenzofuran --ND-- I --ug I L I 1 1 1

84-66-2

131-11-3 '

84-74-2

117-84-0

206-44-0

~~f:~~f:~~~~ ·~~~~~~~~~~~~~~~~~~ l~~~~!~i~~~ l~~~i Fluoranthene ND ug I L I 1 ' 1

_____ f'~~~~~~~ __ r~--No~--u9Ti_-;--=-~=- ~ Hexachlorobenzene --1--_l'J_[)_- ___ __Ll_[l_~_

Hexachlorobutadiene ND ug I L

86737

118-74-1

87-68-3 ----

77~4!_:__4 __ L __ HexachlorocyclopentadiEi_n_~-- ND ug IL

67-72-1 Hexachloroethane ND ug IL - ------------ -- t- ------

193-39-5 lndeno(1,2,3-cd)pyrene ND , ug IL 78-59-1 lsophorone - -- - --· ·r ND ug IL

91_~20~~--l__ Naphthalene ----l _ __f'.J[) _____ j ug IL -----i--

10

10

10

5

1

98-95-3 I Nitrobenzene ___ ND ____ I ug I L 1 ___ +-

6-2_:-_15_~-_9 ___ -+t---__ n-_N_it_ro_s_o-dimethyl-amin~ ______ N__[)_ _ _J __ ~~/~ ___ 1_ I__ 10

621-64-7 n-Nitroso-di-n-propylamine · ND I ug IL . 1 r 1 - --- -- --- ---- I . ·- -- --

10

! ~;~~ _ _":~:~~~~:"" ~~ I :: ; ~ I ~ - - 10

108-95-2 Phenol , ND ug IL -r--1 -- --

129-00-0 --pyrene;--------- 1- ND : ug IL 1 -1 ,

110-86_-_1 ~-----P_y_ri_di_n_e __ - N~TLI91L- I --L=:m SW846 35108/8081A Pesticides by GC/ECD

a-BHC ND ug IL 0.1

1---- -

ALG

I -----;---------

Prep

Date

Run

Date

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-30-03 05-09-03

- - -- - i - 0_:_1 ___ -+-__ ; 04-30-03 05-09-03

0' 1 : 04-30-03 05-09-03

a-Chlordane ND ug I L 309-oo---~---~ .. -__ -----A-ld-n-.n-------+---N[)_ -~r-u9-; L

57-74-9

b-BHC ND ug I L

Chlordane, total

d-BHC

Coyote 2001: Reports

ND ug IL

f ND ug IL _____ ..J ___ -- -------- - --

1. 0, 011109162500

0, 1

0, 1

0, 1

04-30-03 05-09-03

04-30-03 05-09-03

04-30-03 05-09-03

Report Date 61412003 12:14:52 PM



Client:

Project:



Sample: MW- #1

Matrix: GW

QC Group

0304502-05D X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

0304502-05D X03189

X03189

X03189

X03189

X03189

X03189

X03189

0304502-05E M03548

M03548

M03548

M03548

0304502-05E M03550

M03550

M03550

M03550

M03550

M03550

M03550

M03550

M03550

M03550

M03550

Run Sequence

XG.2003.785.32

XG.2003.785.32

XG.2003.785.32

XG.2003.785.32

XG.2003.785.32

XG.2003.785.32

XG.2003.785.32

XG.2003.785.32

XG.2003.785.32

XG.2003.785.32

XG.2003.785.32

XG.2003. 785.32

XG.2003. 785.32

XG.2003.785.32

XG.2003.785.32

XG.2003.785.32

XG.2003. 750.22

XG.2003. 750.22

XG.2003. 750.22

XG.2003. 750.22

XG.2003. 750.22

XG.2003. 750.22

XG.2003. 750.22

MT.2003.521.24

MT.2003.511.47

MT.2003.511.47

MT.2003.521.24

MT.2003.551.41

MT.2003.587.61

MT.2003.551.23

MT.2003.551.41

MT.2003.551.41

MT.2003.551.23

MT.2003.551.41

MT.2003.551.41

MT.2003.551.41

MT.2003.551.41

MT.2003.566.14

Collected: 04-23-03 19:00:00 By: SP

Dilution Detection


SW846 35108/8081A Pesticides by GC/ECD By: ALG

Dieldrin ND -I ug IL : 0.1 ------- ------- --- - --

Endosulfan I ND ug I L ' 1 0.1

Endosulfan II __ ___,_ ___ ND____ -UQ/L-~----1-~-0-.1---+--_,

ND

0.1

0.1 -----+----· __ E_n_do_s_u_lf_an_S_u_lfa_t_e __ ~------+-u_g_l_L_~! _____ , __ _

72-20-8 I Endrin L.-_._N_D_--+~g / L - l-----~--~· __ o._1_-t--_ ___, I ND ug IL 1 Endrin Aldehyde

I Endrin Ketone ND ug I L i 1 1--58--8-9--9-+------g--B-H_C _____ .,._ __ N_D ___ +~-u-g-/ L]_···-_--_-_1_--~-- 0.1

I g-Chlordane ==--===-J_~=- ND -- _u~J_--~----~,~~~0~._1 ______ :--_-~ 76-44-8 Heptachlor ! ND

1 ug I L : 1

0.1

0.1

1024-57-3 Heptachlor Epoxide 1--ND----r-u-9/L-~- 1 0.1

72-43-5 Methoxychlor ·-.. ·-1' ND ___ -rug-/ L __ c ___ 1 ---- 0 1~ 4 i 608~-:~--~---~-_::.:::.:::.::_--_ .. -_-_-_·-_-p_,_p-=D=-D_i_)·· _____ ... _.-i-I -~ ~! ug/_t-_l_ 1 o-f ~- -==----·-·-·- __ P_._p-_D_D_E ___ ---+---~-f--_ljg!!:__~-- 1 ~ 1_ ----~

50-29-3 p,p-DDT ND ug IL 1 0.1 -~

8_(l~2:_35_-2~ ___ T_o_xa_p_h_e_n_e_, t_o_ta_l ___ ~ __ N_D __ ~_u_g_l_L~ _ _1 __ J_ __ 2.5 _ __ _ _:

SW846 35108/8082 PCBs by GC/ECD 12674-11-2 Aroclor 1016 ND I ug IL 1

11104-28-2 Aroclor 1221 ND I ug IL 1 ------~---------T-- --------- --·- --------

11141-16-5 Aroclor 1232 ND i ug IL 1 ---- ---

53469-21-9 Aroclor 1242 ND I ug IL 1 .

12672-29-6 Aroclor 1248 ND ug IL 1 -- ------------+-- ---------r------

11097-69-1 Aroclor 1254 ND ug IL __ 1 ----- ----

11096-82-5 Aroclor 1260 ND ug IL 1 ------------- -------------- - .. -- ------ _____ ,, ____ - ___ ,, _____ ..

SW846 3005A/601 OA ICP ------------------·-----~----·-

! ..... -- ----

I 7440-41-7 Beryllium ND mg/L 1 0.002

7440-47-3 Chromium 0.04 ! mg IL 1 0.01 I ---------!---------+------- --------·----~

i 7440-48-4 Cobalt ND I mg/L 1 0.01 ----·-·--

I I 7440-50-8 Copper 0.02 mg/L 1 0.01 .... __j

SW846 3005A6020 ICP-MS By: HMR

. ~---:=:-~-:-:-::-~~----... ~-~----_-_-_A-=.A_n_:-~--:-=-~-=-i~-=-y-=--=--=--=--=--=--=--=-·_-+j~_--_-_-=--_()_--N-~-~--5--_-_-_:-,.:_:-::.-~---,-,-~----~l=. -_-_ ~-.. -~1·-~-:·-~-~-~ ~~-· --_ 1 7440-39-3 Barium i 0.545 · ~!_l:_ i-- 1 O · 0.001 '

7440-43-9 Cadmium ND mg IL : 1 0.001 .

--~_4-4:~~-:-~-~~~~----·_,_·+-------~-===~--=-~-_=N_L=ie_c=:~-:~-1·~---_-_-_-=.·_·_·_··-+c __ ~_:_~~-~--_ ... __ -+: ____ ·~-~--~'-,~~-~t))~_--·_,--H~{_f_~----~ -~-::-~-::-:-::--i-------s--~~:~m ~~ :~ ~ ~ +-~--~ t~~~--- ---1

------·----j------+-----+--- --- . ·- ··-··--- ------~

7440-28-0 Thallium ND mg IL : 0.001

7440-31-5 Tin ·-·--·---+-----------

7440-62-2 Vanadium

--··1 -ND .. - - -·-mg-iL . -;_-__ · ---~~-_-o_.0:.::0:.::1:.:::.::::.:::.:::.:::.::~ I 0.009 . mg IL I 0.001

--~-----------~

STAN DAR£

Prep Run

Date Date

04-30-03 05-09-0"

04-30-03 05-09-03

04-30-03 05-09-0s

04-30-03 05-09-0~

04-30-03 05-09-03

04-30-03 05-09-0~

04-30-03 05-09-0'

04-30-03 05-09-0~

04-30-03 05-09-03

04-30-03 05-09-0:

04-30-03 05-09-03

04-30-03 05-09-03

04-30-03 05-09-0.

04-30-03 05-09-03

04-30-03 05-09-0~

04-30-03 05-09-0.

04-30-03 05-07-03

04-30-03 05-07-03

04-30-03 05-07-0:

04-30-03 05-07 -0?

04-30-03 05-07-03

04-30-03 05-07 -O: 04-30-03 05-07 -0?

04-30-03 05-01-03

04-30-03 05-01-0,

04-30-03 05-01-07

04-30-03 05-01-03

04-30-03 05-05-0"

04-30-03 05-14-0"

04-30-03 05-05-03

04-30-03 05-05-0"

04-30-03 05-05-0'

04-30-03 05-05-03

04-30-03 05-05-0,

04-30-03 05-05-0~

04-30-03 05-05-03

04-30-03 05-05-0,

04-30-03 05-08-0'


Client:

Project:






Sample: MW- #1

Matrix: GW

QC Group

0304502-05E M03550

Run Sequence

MT.2003.551.41

Collected: 04-23-03 19:00:00 By: SP

Dilution Detection


By: HMR

0.167 mg IL L_


Prep

Date

STANDARD

Run

Date

04-30-03 05-05-03

0304502-05E M03559 MT.2003.522.30 I 7439~~~6i-~~--------MerCU':)' ______ =:_:__l___B6 -_L mg IL --~1__:___~ 0_:()_002- - 05-01-03 05-01-03

Sample: MW- #2

Matrix: GW

QC Group

0304502-0GA X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

Page 21 of 27

Run Sequence

XG.2003.814.23

XG.2003.814.23

XG.2003.814.23

XG.2003.814.23

XG.2003.814.23

XG.2003.814.23

XG.2003.814.23

XG.2003.814.23

XG.2003.814.23

XG.2003.814.23

XG.2003.814.23

XG.2003.814.23

XG.2003.814.23

XG.2003.814.23

XG.2003.814.23

XG.2003.814.23

XG.2003.814.23

XG.2003.814.23

XG.2003.814.23

XG.2003.814.23

XG.2003.814.23

XG.2003.814.23

XG.2003.814.23

XG.2003.814.23

XG.2003.814.23

XG.2003.814.23

XG.2003.814.23

XG.2003.814.23

XG.2003.814.23

XG.2003.814.23

XG.2003.814.23

XG.2003.814.23

CAS#

75-34-3 ----75-35-4

71-55-6 --~

630-20-6

79-00-5

79-34-5 ----~---··-

563-58-6

106-93-4

95-50-1 --- --

107-06-2

78-87-5 -------

96-18-4 ------

87-61-6 -------

120-82-1

95-63-6 -----~

96-12-8 ---------

-------------------------·-------· Collected: 04-23-03 20:10:00 By: SP


Analyte Result Units Factor Limit Code Date Date

-----·---1,1 Dichloroethane 05-07-03 05-08-03

----- -·· - - - ---~ ·--

1, 1 Dichloroethene 05-07-03 05-08-03

1, 1, 1 Trichloroethane I 05-07-03 05-08-03

1, 1, 1,2 Tetrachloroethane ! 05-07-03 05-08-03

1, 1,2 Trichloroethane-~~-·--1- 05-07-03 05-08-03

1, 1,2,2 Tetrachloroethane i 05-07-03 05-08-03 ~--·

1, 1-Dichloropropene 05-07-03 05-08-03

1,2 Dibromoethane (EDS) 05-07-03 05-08-03

1 ,2 Dichlorobenzene 05-07-03 05-08-03 -- -- ---------------------------

1,2 Dichloroethane (EDC) '

05-07-03 05-08-03

1,2 Dichloropropane 05-07-03 05-08-03 -- -- -- --

1,2,3 Trichloropropane 05-07-03 05-08-03 -----

1,2,3-Trichlorobenzene 05-07-03 05-08-03 -----

05-07-03 05-08-03 1,2,4-Trichlorobenzene !

~ --1,2,4-Trimethylbenzene I 05-07-03 05-08-03

-----"'--1,2-Dibromo-3-chloropropane I 05-07-03 05-08-03

------ --· ----·------05-07-03 05-08-03

05-07-03 05-08-03

05-07-03 05-08-03

05-07-03 05-08-03

05-07-03 05-08-03

05-07-03 05-08-03

05-07-03 05-08-03

05-07-03 05-08-03

05-07-03 05-08-03

05-07-03 05-08-03

05-07-03 05-08-03

05-07-03 05-08-03

05-07-03 05-08-03

05-07-03 05-08-03

05-07-03 05-08-03

05-07-03 05-08-03


STANDARr



Client:

Project:



Sample: MW- #2

Matrix: GW

QC Group

0304502-0GA X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

0304502-068 X03200

X03200

0304502-0GC X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

Page 22 of 27

Run Sequence

XG.2003.814.23

XG.2003.814.23

XG.2003.814.23

XG.2003.814.23

XG.2003.814.23

XG.2003.814.23

XG.2003.814.23

XG.2003.814.23

XG.2003.814.23

XG.2003.814.23

XG.2003.814.23

XG.2003.814.23

XG.2003.814.23

XG.2003.814.23

XG.2003.814.23

XG.2003.814.23

XG.2003.814.23

XG.2003.814.23

XG.2003.814.23

XG.2003.814.23

XG.2003.814.23

XG.2003.814.23

XG. 2003. 814. 23

XG.2003.814.23

XG.2003.814.23

XG.2003.814.23

XG.2003.814.23

XG.2003.727.21

XG.2003.727.21

XG.2003. 703.17

XG.2003. 703.17

XG.2003. 703.17

XG.2003. 703.17

XG.2003. 703.17

XG.2003. 703.17

XG.2003.703.17

XG.2003.703.17

XG.2003.703.17

XG.2003.703.17

Collected: 04-23-03 20:10:00 By: SP

Dilution Detection


EPA 524.2 rev 4 Purgeable VOCs by GCIMS By: JAA --1

Chlorodibromomethane 1.3 ug IL : 1 0.1 -----+--------------+- ---+-----+ ------+-----+---75-00-3 Chloroethane ND ug IL 1

1

1 i ___ 0:1

67-6_ .. 6 __ -3_+-_____ C_h_lo_r_of_o_rm _______ -+-__ N_D ___ L--~g IL 1 I 0.1 74-87-3 Chloromethane i ND ug IL I 1 I 0.1 1

-156-59-2 ----ci-s--1-,2-d-ic-h-lo_ro_e_t_he_n_e---+-,1--N--D 1 ug IL 1-T 0.1 -t--~, .. -----t-----· --~

10061-01-5 cis-1,3dichloropropene _____ N_D _____ l ug/L 1 , 0.1 _J_ ___ _

124-48-1

74-95-3 Dibromomethane ND ug IL 0.1 ---- --------t---- -----1-------+------ ---- ------

100-41-4 Ethylbenzene ND ug IL 0.1 ________ _

75-71-8 Freon 12 ND ug IL 0.1 ___ __,_ __ -j

87-68-3 Hexachlorobutadiene ND ug IL 0.1 ------+--------------+------f----------+------+------+----

__ 9_8_-8_2_-8_+-____ l_so_p_r_o~p~yl_b_e_nz_e_n_e ___ +-__ N_D __ --+-_u~g_l_L_+------+---- 0.1 __ ~i __ -j __ 7 __ 5-_0_9_-_2-+ ___ M_e __ th_y_le_n_e_c_h_lo_r_id_e ____ + __ N_D __ -+-_u_g_l_L_+ 0.5 I

91-20-3 Naphthalene ND ug IL 1 I 104-51-8 n-Butylbenzene ND ----~~=~g---~-L _ _, ____ -+---~-:~-+-= 103-65-1 n-Propylbenzene l _ --~-+--ll!l-~ '.__ _ _ ____ 1 _____

1

Prep Run

Date Date

05-07-03 05-08-0~

05-07-03 05-08-03

05-07-03 05-08-0C»

05-07 -03 05-08-0~

05-07-03 05-08-03

05-07-03 05-08-03

05-07 -03 05-08-0:

05-07 -03 05-08-03

05-07 -03 05-08-03

05-07 -03 05-08-0:

05-07 -03 05-08-03

05-07 -03 05-08-03

05-07-03 05-08-0:

05-07 -03 05-08-03.

05-07-03 05-08-03

05-07 -03 05-08-0: __ 9_5_-4_7_-6____ o-Xyle!:l!__ ______ L __ N_[)__ i ~~'~-·---~- 0.1 i

1 3j~~~~:; ____ p_l_m __ -X_y __ lenes --1_ _ _t-JE_ l __ ug _J__l-_ _ ___ 1 0.2 J i 05-07-03 05-08-03

' ,,,_,,_, 1- '""""""'""". rn _"(: "ND- -==,,_IL-;~ '--~-0_.1____ _ ___ : 05-07-03 05-08-0~ 1~~42-5 Styrene ____ ND -t-lJ!lLL --4---~-~· __ o_._1 __ +----· 05-07-03 05-08-03

. 156-60-5 t-1,2 Dichloroethene ND +--~~-L-~- -~ 1 0.1 _ -1. 05-07-03 05-08-0:_

: 10061-02-6 I t-1,3 Dichloropropene ND 1 ug IL 1 0.1 ___ 05-07-03 05-08-03

98-06-6 tert-Butylbenzene ND 1 ug IL 0.1 I 05-07-03 05-08-03

127-18-4 Tetrachloroethylene 2.1 ug IL 0.1 05-07-03 05-08-o:

108-88-3 Toluene ND ug IL 0.3 --t---------------t-----·-·---+-----r------+-----------+-----~

79-01-6 Trichloroethene ND ug IL 0.1 ----+------+

75-69-4 Trichlorofluoromethane ND ug I L 0.1 ----~---------------t-------+----r

75-0_1-4_--+-____ Vinyl chloride ND __ _j -----~-g_I L_ 0.1

EPA 504 ED8/D8CP by GC/ECD By: ALG

l---~-1-,~-~~---i~-~~-~-o:_-_!-_e~-~-~-~:-~-~-~-~-n_e ___ ~-~=~#o-------1 ~+--~--1--~~~}=±~~:-_::--:' SW846 35108/82708 SVOCs by GC/MS By: JM/KAR

120-82-1 1,2,4-Trichlorobenzene ) ND ug IL 1 1

95-50-1 1,2-Dichlorobenzene i ND ug IL 1 1 -----t------------------+----·-- --------+------+---~

541-73-1 1,3-Dichlorobenzene ' ND ug I L 1 1 ---------+----------------------1----+----+-----+----j 106-46-7 1,4-Dichlorobenzene 1 ND ug I L 1 1

·--- ------· 90-12-0 1-Methylnaphthalene : ND ug IL 1 1

-------- ---------------------t-----r------------ -t-- ------

2,3,4,6-Tetrachlorophenol ND ug IL 1 5

9S~95-4 2,4,5-Trichlorophe_n~I- _ ·- _!'l_[) __ -_-J _u_g_T_CJ_-_T~_[_~_- __ -~'--__ --_______ , _8_8_-_06_-_2--+ ____ 2_,_4,6-Trichlorophenol ___ __l'J_[)___ j -~-~/ L J 1

1

5 I 120-83-2 2,4-Dichlorophenol ND I ug IL I 1 5

[ 105_:_67-9 ___ 2_.4_:-_Di~e_thylphenol ____ _!'J_[)_ _ _-=- ug I L=l 1 ___ '~-==1

58-90-2

05-07-03 05-08-03

05-07 -03 05-08-03

05-07 -03 05-08-0~

05-07-03 05-08-0?

05-05-03 05-06-03

05-05-03 05-06-0~

04-28-03 04-29-02

04-28-03 04-29-03

04-28-03 04-29-0~

04-28-03 04-29-0?

04-28-03 04-29-03

04-28-03 04-29-0~

04-28-03 04-29-0c

04-28-03 04-29-03

04-28-03 04-29-0~

04-28-03 04-29-0?




Client:

Project:



------------- -·

Sample: MW- #2 Collected: 04-23-03 20:10:00 By: SP

Matrix: GW

QC Group

0304502-0SC X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

Run Sequence

XG.2003. 703.17

XG.2003. 703.17

XG.2003.703.17

XG.2003. 703.17

XG.2003.703.17

XG.2003.703.17

XG.2003.703.17

XG.2003.703.17

XG.2003. 703.17

XG.2003. 703.17

XG.2003.703.17

XG.2003. 703.17

XG.2003.703.17

XG.2003.703.17

XG.2003.703.17

XG.2003.703.17

XG.2003.703.17

XG.2003.703.17

XG.2003. 703.17

XG.2003. 703.17

XG.2003. 703.17

XG.2003. 703.17

XG.2003.703.17

XG.2003. 703.17

XG.2003.703.17

XG.2003. 703.17

XG.2003. 703.17

XG.2003.703.17

XG.2003.703.17

XG.2003.703.17

XG.2003.703.17

XG.2003. 703.17

XG.2003. 703.17

XG.2003. 703.17

XG.2003. 703.17

XG.2003.703.17

XG.2003.703.17

XG.2003.703.17

Dilution Detection


SW846 35108182708 SVOCs by GC/MS By: JM/KAR ' -51Ts~5

121-14-2

2,4-Dinitrophenol ---- -N-D--f-~gTL -2,4-Dinitrotoluen_e __ ___J_ ______ ~fD- 1 ug IL

10

5 - -----------· +--------·-- ·------------_, _______ _

606-20-2 2,6-Dinitrotoluene ND ug IL 5 --·--t----···---- -- --- -- - ---- - --------------·

---~~-:~_-~_::_+ 2-~~~~~~r:~!~F-e~-----l -- ~%--~-~~~ ~·. - -. 1 ·- -- - - -~-91-57-6 · 2-Methylnaphthalene ND ug IL 1 1 I

-~------------·----~-·----+---------· ---- --- +-- - -

--;-~-;;-~_ 't~=:;:~i' I -~~ :H [~-1 .. ~: ~j- ~--~:::: ';::::~::;:· i ~~ -: ~ t- ~ ~--1:0 ~ +--=-~

534-52-1 , 4,6-Dinitro-2-methylphenol , ND 1

ug I L 1 1 O

1oi-=-s5~3·t 4-Bromophenyl-phenylit~er ~ _ ND·-==I~97L- ---- -- 1 ------59-50-7 4-Chloro-3-methylphenol ND ug I L 5 --- ------------------- - -------

----j 106-47-8 ! 4-Chloroaniline ND ug IL i 1 5

7005-72-3T-4~hlorophenYJ.i)henylether--.----ND ug IL i 1

100-01-6 4-Nitroaniline . i ND--.-~gTL [-- 5

--- _J 100-02-7 4-Nitrophenol -·1- -·r;Ji:)----+--~-/L j_ __ 1 10

83-32-9 Acenaphthene _ ND _c_.LJ2.L~. j 1 _ ... . 1 _

, _2_°.8=9~=~-- ___ Acenaphthylene j ·---N-~-----"-~j__1 ___ _1 __ _,_ __ -j 62-53-3 Aniline .. ..... _ ND ug I L L __ 1______ 1 O

1_20-12-7_j_ Anthracene __ NE_ __ t ug IL

. ____ Azobenzene&1,2- _f>J_!)___L_Lj2_1~

56-55-3

50-32-8

Diphenylhydr~zine __ _

Benzo (a) anthracene ND ug I L- c==1-=-=-~-- =1- -=r==:....:

Benz~~~~o~~;l~~r:~:hene 1 ~~ · i . ~~~ ~ +--+--·---+ ___ _)_ ____ ; ---~94_~~-25~~~-- _ Ben~:~~:;~~:~lene -1 ··· ~~:~+-~J~~~---2\=~-~~-~-~

100-51-6 ' Benzyl alcohol ND ug IL 1 5

~ ~ ~ ::4

-1 :_: __ b_i_:-~;--~-2-~c-lo-~~-:1~:~:)1~:~~:~e 1

• __ --~~ ~~ ~ ~ t-~-~ -t--l~- -108-60-1 bis(2-Chloroisopropyl)ether ·-;~~ l ug I L t.·· }- ; ..

_ 1_1_7-_8~::7. bis(2-Ethylhexyl)phtha~cite_ . L ug IL . 5 B

~u_tylbenzylphthalate_-+ ND ug I L 1-- ---·---· 85-68-7

218-01-9

53-70-3 ..

132-64-9

Chrysene , ND ug I L

Dibenz(a,h)anthracene ND ug I L 1 ------------- ------

Dibenzofuran ND ug IL 1 XG.2003.703.17 84-66-2 Diethylphthalate

Dimethylphthalate

ND ug IL XG.2003.703.17 131-11-3

-- - ---- ·---

XG.2003.703.17 84-74-2 ! di-n-Butylphthalate xG.2003.703.17 , i-11~04:·a·T di-n-Octylphthalate

ND ug IL ----- +--------- -- -·

.. ___ N_D ___ ~i _u~-~-61 1 ug IL

--1--!

Prep

Date

STANDARD

Run

Date

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03




Client:

Project:



--·-Sample: MW- #2

Matrix: GW

QC Group

0304502-0SC

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

0304502-0SD

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03t94

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

Run Sequence

XG.2003.703.17

XG.2003. 703.17

XG.2003.703.17

XG.2003.703.17

XG.2003. 703.17

XG.2003. 703.17

XG.2003. 703.17

XG.2003.703.17

XG.2003. 703.17

XG.2003.703.17

XG.2003.703.17

XG.2003.703.17

XG.2003.703.17

XG.2003.703.17

XG.2003.703.17

XG.2003.703.17

XG.2003.703.17

XG.2003.703.17

XG.2003. 785.33

XG.2003. 785.33

XG.2003.785.33

XG.2003.785.33

XG.2003.785.33

XG.2003.785 33

XG.2003.785.33

XG.2003.785.33

XG.2003.785.33

XG.2003.785.33

XG.2003.785.33

XG.2003.785.33

XG.2003.785.33

XG.2003.785 33

XG.2003.785.33

XG.2003.785.33

XG.2003.785.33

XG.2003.785.33

XG.2003. 785.33

XG.2003. 785.33

XG.2003. 785.33

XG.2003.785.33

Collected: 04-23-03 20:10:00 By: SP

Dilution Detection


SW846 351 OB/82708 SVOCs by GC/MS By: JM/KAR

[ 206-44-0 Fluoranthene --=J- __ N_D __ --+-_u_g_l_L_

86737 Fluorene ND ug I L

118-74-1 Hexachlorobenzene . ______ J.. ____ N_D __ -+--_u_g_l_L _ l_ 1

_·_· -~-;-~=6

_7-8

~=3

=:i===H=e=x=~=:=~a=-1~_:_1 ~-~-~-~o_u;_:_~_::_~_~e_ne____ --.-.. -. __ -;-;-__ -.--+ -~t + __ ----~----_-fJ-_--~ -~~---_-·_··_-·_---_·---_,-67-72-1 Hexachloroethane ND ug IL ! 1 · 5 -----+------------------- ---------+-1----------l--- ------ --r---- __________ __,

193-39-5 lndeno(1,2,3-cd)pyrene ND ug I L : 1 1 ------+---------------+-----·(____':'._ _____ , _______ ---------+-· --78-59-1 lsophorone ND ug I L 1 1

I··-----+---------------+------- ·--+----------

__ 9_1-_2_0-_3--f _____ N_a_p_ht_h_a_le_n_e ______ __j _______ N_D ____ -+-_u_g_l_L ___ 1_ ___ _ ·-+---·~

98-95-3 Nitrobenzene i ND ug I L 1 ! ----+---------------+--------·-- ------~---~----- ---·---+---~

62-75-9 n-Nitroso-dimethyl-amine ND ug I L ! 1 10 --------+--------------+-------t----- ----1 621-64-7 n-Nitroso-di-n-propylamine I ND ug IL 1 1 I

----l--------------+-----------·---+-----+-----+--86-30-6 n-Nitrosodiphenylamine ND ug I L 1 1 + 1.

1

-- 87-86-5 : Pentachlorophenol ------+-----N-D---+--u_g_/_L_-+-- 1 -- __ 1_0_ . -- 1

85-01-8 I Phenanthrene ND ug IL 1 1-- 1- ---L---1 ' ------+--------------- - - -- - -~- ----------- - -- - ' ------------+-----__j

I=~:::::: I ~::~ _J-- -~~-- ::;~-+-'------"- ',' r--1 _1~~~-----P_yridine ,--No---+UQ/L --~~-=- --=--: SW846 3510B/8081A Pesticides by GC/ECD By: ALG

---+1

1

____ a--~-~-~-~d-~_n_e __ --_-_--_-_-_-----~-~-------1-T-!-·_· ~-~--~-~ =r==~-----i---~T"=F==-~ 309-00-2 :~:~ -.,.- ~~ ~~; ~ ~-H -~-F-~-~f- f rnml _57_-_74_=9_-·_-+-1-_-_···_-··_·--_-_c_-h_lo_rd_a_ne_,_to_t_al ___ J_ ND I ug/L. r·- ·1---i=~I--;--- · 1

60:57:1--+--- --------- ~~e--~-=r-~------+--~-~--1---~-9-; ~ -t--~-t--%+- i---~ . ug - - _l____:_ __ +- ---

------------~~~_su_lf_an_I ----+

1

• __ NN_DD __ _;_ __ _1Ju_g9 _____ !1. __ LL---~-- _1

1____ 0

0 .. 11

_______ _

---i-~ ---~ndo~~-lfan II . +

72-20-8 I Endos~~:~i:ulfate r_-_____ ~~---~D-__ --- - ~u~g ;/~LL _I u1___ ~0:_~1 - ' -------r-----E-ndririAiciehYcie I · 58-89-9

! Endrin Ketone ~ ND · ug IL O 1

___ g-_B_H_C _____ --++-···_--_--_-N_I::)____ ug I L o: 1

-~g_-C_h_l_or_d_a_ne ____ +l--N~ ug I L 0.1

76-44-8 Heptachlor 1

ND ug I L 0.1 -------+-------------+-- --1----+-------i 1024-57-3 Heptachlor Epoxide ND ug I L 0.1 -----+------------~---

72-43-5 Methoxychlor

6088-51-3 p,p-DDD

50-29-3

8001-35-2

p,p-DDE

p,p-DDT

Toxaphene, total

ND ug IL

---r---N_D ___ 4 ug __ l_L ___ , ____ _ ----+- ___ N_D _____ u_g __ _ I ___ L·----i-----

1 ND ug IL

____ J ___ N_D _ _ ug IL

0.1

0.1

0.1

0.1

Prep

Date

STAN DAR!

Run

Date

04-28-03 04-29-0"

04-28-03 04-29-03

04-28-03 04-29-0:>

04-28-03 04-29-0~

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-o:'

04-28-03 04-29-0~

04-28-03 04-29-03'

04-28-03 04-29-0:

04-28-03 04-29-03-

04-28-03 04-29-03

04-28-03 04-29-0:

04-28-03 04-29-0::<

04-28-03 04-29-03

04-28-03 04-29-0:

04-28-03 04-29-0::<

04-28-03 04-29-03

04-30-03 05-09-0:

04-30-03 05-09-0::<

04-30-03 05-09-03

04-30-03 05-09-0:

04-30-03 05-09-02

04-30-03 05-09-03

04-30-03 05-09-0:

04-30-03 05-09-0?

04-30-03 05-09-03

04-30-03 05-09-0:

04-30-03 05-09-0~

04-30-03 05-09-03

04-30-03 05-09-0~

04-30-03 05-09-0?

04-30-03 05-09-03

04-30-03 05-09-0<.

04-30-03 05-09-0'.'

04-30-03 05-09-03

04-30-03 05-09-0~

04-30-03 05-09-0:

04-30-03 05-09-03

04-30-03 05-09-0~


STANDARD



Client:

Project:



Sample: MW- #2

Matrix: GW

QC Group

0304502-0SD X03189

X03189

X03189

X03189

X03189

X03189

X03189

0304502-0SE M03548

M03548

M03548

M03548

0304502-0SE M03550

M03550

M03550

M03550

M03550

M03550

M03550

M03550

M03550

M03550

M03550

M03550

Run Sequence

XG.2003.750.23

XG.2003.750.23

XG.2003.750.23

XG.2003.750.23

XG.2003.750.23

XG.2003.750.23

XG.2003.750.23

MT.2003.521.25

MT.2003.511.48

MT.2003.511.48

MT.2003.521.25

MT.2003.566.15

MT.2003.551.42

MT.2003.551.24

MT.2003.551.42

MT.2003.551.42

MT.2003.551.24

MT.2003.551.42

MT.2003.551.42

MT.2003.551.42

MT.2003.551.42

MT.2003.566.15

MT.2003.551.24

Collected: 04-23-03 20:10:00 By: SP

Dilution Detection


SW846 35108/8082 PCBs by GC/ECD By: ALG

12674-11-2 I

11104-28-2:

11141-16-5 1

53469-21-9 I

12672-29:61

I 11-097-69-1 I

1 -11 096-82-5 r-

Aroclor 1016

Aroclor 1221

Aroclor 1232

Aroclor 1242

Aroclor 1248

--r- ------ -- -. -- --- ---- -I ND ug IL 1

------;----N~--u-g /L: ______ T __

ND

ND

ND

ug IL

ug IL

ug IL ·-- - - -. %:~:~-~ ~-:-~-- -------~~ --=J--~~it- ~~=-= ~ --- j-

0.5

0.5

0.5

0.5

0.5

0.5

0.5

SW846 3005A/601 OA ICP By: JRE 7440-41-7 Beryllium ----r- ND mg I L i--1-f-o:ooz-T •. - - .

7440-47-3

I 7440-48-4

i 7440-50-8

Chromium 0.02 mg IL + 1 I ()~01--r- -- ' ______ c_o_b_a-1t-------+--N-D---+--m-g-,-L-+---- 1--+=~~()I=====-=

_______ c_o_p_p_e_r ____ ~ ___ o_._1_0_ ~~_L__1 ___ J_ °:01 __ ~I ___ J

By: HMR

Prep

Date

Run

Date

04-30-03 05-07-03

04-30-03 05-07-03

04-30-03 05-07-03

04-30-03 05-07 -03

04-30-03 05-07 -03

04-30-03 05-07 -03

04-30-03 05-07 -03

04-30-03 05-01-03

04-30-03 05-01-03

04-30-03 05-01-03

04-30-03 05-01-03

+ ND : ,:;:;-9, L 1 1 o 001 , 04-30-03 05-08-03

- f --0-:-022=~ rll_g IL I 1 -- 0 001 -- ----- 04-30-03 05-05-03

7440-39-3 Barium ___J___~~-- mg IL -t _1_()_ ____ 0_0_()1__ 04-30-03 05-05-03

7440-43-9 Cadmium 0.001 mg IL 1 0.001 04-30-03 05-05-03 -------------j-------------- --- - - ~ - --

74_3_9_-9_2-_1~ _____ L_e_a_d ______ f---_o_.o __ 4_8_~_m_g_l_L_L __ 1 ___ 0_()_0_1_ _ , 04-30-03 05-05-03

_7_4_40_-0_2_-o ______ N_i_ck_e_l ____ ---j-__ o_._01_3 ___ m_g_l_L_l 10 0.001 · I 04-30-03 05-05-03

7782-49-2 ! Selenium 0.001 1 mg IL t 1 0.001 . • 04-30-03 05-05-03

7440-22-4 i Silver -- ND I mg IL 1 ' 0.001 . ---1 04-30-03 05-05-03 -----~--------·---------------------·------- ---------------+----1

~::~::~:~ Th~lil~um 0~~3 :~ ~ ~ t_ __ 1--~- ~-~~~ ---i 1 ~:::~:~: ~::~::~: 7440-62-2 Vanadium 0.01 O mg IL 1 1 0.001 04-30-03 05-08-03 ---------1------- -·--·------·---- -- ·------- -----7440-66-6 Zinc 0.257 mg IL 10 0.005 04-30-03 05-05-03

SW846 7470 Mercury by CVAA By: JRE 0304502-0SE M03559 MT.2003.522.31 I 7439-97-6 Mercury

I ND mg/L 0.0002 05-01-03 05-01-03

Sample: TRIP BLANK Matrix: W

QC Group

0304502-07 A X03206

X03206

X03206

X03206

X03206

X03206

X03206

Page 25 of 27

Run Sequence

XG.2003.817.4

XG.2003.817.4

XG.2003.817.4

XG.2003.817.4

XG.2003.817.4

XG.2003.817.4

XG.2003.817.4

---- ----- --

Collected: 04-23-03 20:15:00 By: SP




-7-5~3-4:3- ___ 1,1 Dich~roeth~~-- __ j _N~-- _l_ug/L_T_1__ 0.1 _ I _____ j ~::~~:~: ~::~~:~: 7'_5~~5~- 1, 1 Dichloroethene 1 ND j ug I L 1 1 0.1 f 71-55-6 1, 1, 1 Trichloroethane -1 --ND____ 1 --ug IL i 1 O 1 I

630-20-6 1, 1, 1,2 Tetrachloroetha~ _f'JD-=~-= ug 7];-_ !-=- ~--~ CJ_.1 _ j

563-58-6 1, 1-Dichloropropene ND ug I L 1 0.1

05-07-03 05-07-03

05-07-03 05-07-03

05-07-03 05-07-03 _J 05-07-03 05-07-03

05-07 -03 05-07 -03 ;::::~ 1, ,',;:: ;:~::~::::~:"" ~-1 ~:: ~%-_::_ ~~:~ l 1' ---~ =-=- ~=-~~--=-=

----- - - -~---


STANDARC



Client:

Project:



Sample:

Matrix:

TRIP BLANK

w - ------------~------ ----

QC Group

0304502-07 A X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

Page 26 of 27

Run Sequence

XG.2003.817.4

XG.2003.817.4

XG.2003.817.4

XG.2003.817.4

XG.2003.8174

XG.2003.817.4

XG.2003.817.4

XG.2003.817.4

XG.2003.817.4

XG.2003.817.4

XG.2003.817.4

XG.2003.817.4

XG.2003.817.4

XG.2003.817.4

XG.2003.817.4

XG.2003.817.4

XG.2003.817.4

XG.2003.817.4

XG.2003.817.4

XG.2003.817.4

XG.2003.817.4

XG.2003.817.4

XG.2003.817.4

XG.2003.817.4

XG.2003.817.4

XG.2003.817.4

XG.2003.817.4

XG.2003.817.4

XG.2003.817.4

XG.2003.817.4

XG.2003.817.4

XG.2003.817.4

XG.2003.817.4

XG.2003.817.4

XG.2003.817.4

XG.2003.817.4

XG.2003.817.4

XG.2003.817.4

XG.2003.817.4

XG.2003.817.4

XG.2003.817.4

XG.2003.817.4

Collected: 04-23-03 20:15:00 By: SP

Dilution Detection



Prep

Date

Run

Date

I ND . --T ug IL : 0.1 I 05-07-03 05-07-o:

95-50-1.~ ___ 1,_2_D_ichlorobenzene ND --i--~g/L___ ·--~~ --+-----~ 05-07-03 05-07-03

106-93-4 1,2 Dibromoethane (EDB)

' ~7~~:7~;-t 1,21 ~-~--cD_h:_~-~~_:_r~_;_r:_:_~_En __ ~~-c~_)-:_-:_-:-__-+r----- ~-~-- - -~~ ~l_L_ -~-~- J==-~- ~::~~:~: ~::~~:~~ 96:_~_8-_4 __ 1--__ 1_,2_,_3_T_richloropropane i ND ug IL j 1 ' O~ 1 i 05-07-03 05-07-03

05-07 -03 05-07 -0~ 87-61-6 1,2,3-Trichlorobenzene i ND ug IL : 1 0.5 [

1,2,4-Trichlorobenze-ne-- ---+ ND ·--u9-IL.j- _ 1 ·-1 _ o.5 !- , o5-07-03 o5-07-o:

~)5---63---6---+--1-,2-.-4--Trimethylbenzene 1 ND-- -- -- ug /L - 1- · ---o~i--~! ------ 05-07-03 05-07-03.

---~-----

120-82-1

---------'------1-------'----'---- -------·---· -- -·- ··-·t·----·--96-12-8 1,2-Dibromo-3-chloropropane ND ug IL 1 0.2 05-07-03 05-07-0:,-

----+-----------'--''----+-----+---=---1------·- ------·----------~

541-7_3_-1_1--__ 1_,3_D_ic_h_lo_ro_b_e_n_z_e_n_e ___ +--1! __ N_D __ ~ ___ u_g~/_L __ " ___ 1_--+ __ 0._1_-+--- 05-07 -03 05-07-0:

108-67-8 1,3,5-Trimethylbenzene ND ug IL 1 0.1 05-07-03 05-07-03 ---~r---------

142-28-9 1,3-Dichloropropane 1 ND I ug IL 1 0.2 05-07-03 05-07-03

106-46-7 1,4 Dichlorobenzene ND + ug IL 1 0.1 1 05-07-03 05-07-o:

•---l~/;.=;-~-7===~~-----~-=-:~-=-:_D_ls-:_i~=~=~:--'-~-o.:.._y_P_-lt_;_o_1_~-:--~--:----_-_-_-:_-_-_-_-_~-=~-=-~--=~-t~-~~-~-~- -- - ~ --~} _L__l ~::~~:~: ~::~~:~: 95:49-8 2-Chlorotolu-e-ne ______ N_D ___ lu_g_TL. -- 1 --- 0.1 i _J 05-07-03 o5-07-o:

--1-0-6--4--3--4--+-----4-Chlorotoluene - ND- ----I ugfL_ I_ 1 0.1 l ! 05-07-03 05-07-03

1--17o-~-4---8=36---~1=========.~-B~-r_o=_~=-e-_;_b_z_e_e_n_n_:-e~n~e-_-___ --l-;---~-~--- m--- ~;;lJ~--- --~~-~-r-~-~==-j ~::~~:~: ~::~~:~~ Bromochloromethane ND ug IL 1 0.1 i 1 05-07-03 05-07-03

[ 75-27-4 Bromodichloromethane ND ug IL 1 0.1 I 05-07-03 05-07-03 l------+------------

75-25-2 Bromoform ND ug I L 1 0.1 1 05-07-03 05-07-0: i ------+------ --------·-·-1----1 74-83-9 Bromomethane

1

. ND ug IL 1 0.6 I 05-07-03 05-07-0~ I 56-23-5 c·-a-rb_o_n-te-tr_a_c_h_lo-ri-de---1----N-D-- ----u9/L- 1 0.1 I 05-07-03 05-07-03

: ---~=~=:-=:-~-:-:~-~--: ___ C_h_l_o_c_r:-~-~b-r~-:m_e_:z-;-:-t~_a_n_e-----i1 ----:-_~~----- ~~~~-t--1 __ f---- ~:~ ~ ~::~~:~: ~::~~:~~ I 75-00_-3 _ __j_ ____ C_h_lo_r_oeth~__ri_e ___ -----:- ND r ug IL - ~=~ __ l 0.1 I ---1 05-07-03 05-07-03

: _6__7_:('~~3 __ [ Chloroform ND ! ug IL L H +H 0.1 __ ___ _J 05-07-03 05-07-0~ , 74-87-3 l Chloromethane

1 ND ug IL 1 0.1 I 05-07-03 05-07-0?

;-156-59-2 1----- cis-1,2 dichloroethene ~-ND- --ug-/ i:_- -i 1 . 0.1 -1 05-07-03 05-07-03

l 10061-01-5 I cis-1.-3-d--ic-h-lo_r_o_pr_o_p_e-ne----+----N-D---+---u-g_/_L __ , -1·--r---0~1 ! 05-07-03 05-07-0~ : 74-95-3 i Dibromomethane ND ug IL 1 -T- 0.1 -~--1 05-07-03 05-07-0? I -----------+-------+------+-- - - - j-1_1_00_-~ Ethylbenzene ND __ u~~-J ---~-- 0.1 _ ~1 ____ 05-07-03 05-07-03

I 75-71-8 Freon 12 ND ug IL 1 0.1 I 05-07-03 05-07-0~

87-68-3 _J--__ H_e_x_a_ch_l_o_ro_b_u_ta_d_ie_n_e __ -+ __ N_D ____ '---u-~!_':_ __ ~------- . ___ 0.1 -·--·---r------

- _:_~82_~----l----ls_o_p_ro_p_y_lb_e_n_ze_n_e ___ -+--__ N_D _____ --~~_!_I:: _ 1__ _1 __ -l 0.1 --+----

75-09-_2--+ ___ M_e_t_h_y_le_n_e_c_h_lo_ri_d_e _____ J-----~~----l --~gL':__ ~- _ ~ --1- 0.5

9_1-=._20-3 ~---- Naphthalene ND I ug I L ' 1 i i 104-51-8

103-65-1

n-Butylbenzene ND ug I L 1 1 I 0.1 : -·~-,--

0.1 n-Propylbenzene ---1------ ND___ u9TL. - ' l --· -------+-------------+------+------+------l-----~--

05-07 -03 05-07 -0?

05-07-03 05-07-03

05-07 -03 05-07 -0~

05-07 -03 05-07 -0(

05-07 -03 05-07 -03

05-07 -03 05-07 -0~

95-47-6 , o-Xylene 0.14 ug IL 1 0.1 . 05-07-03 05-07-o; 1 oa:3a:.-·--;----p-/m--X-'-y-le_n_e_s------+--0-.3-0 _ __J_u--=g=-/-L--'----__ 1 __ J ____ o:i--. -_-_;--__ · __ --__ --___ -_I,, 05-07-03 05-07-03

3{!CJ6~~ ~

Coyote 2001: Reports 1.0.011109162500 Report Date 61412003 12:19:45 PM -

STANDARD



Client:

Project:



Sample: TRIP BLANK Matrix: W

QC Group

0304502-07A X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

0304502-078 X03200

X03200

Run Sequence

XG.2003.817.4

XG.2003.817.4

XG.2003.817.4

XG.2003.817.4

XG.2003.817.4

XG.2003.817.4

XG.2003.817.4

XG.2003.817.4

XG.2003.817.4

XG.2003.817.4

XG.2003.727.22

XG.2003.727.22

Collected: 04-23-03 20:15:00 By: SP



EPA 524.2 rev 4 Purgeable VOCs by GC/MS By: JAA 05-07-03 05-07-03

05-07-03 05-07-03

05-07-03 05-07-03

05-07-03 05-07-03

05-07-03 05-07-03

05-07-03 05-07-03

05-07-03 05-07-03

05-07-03 05-07-03

05-07-03 05-07-03

05-07-03 05-07-03

135-98-8 I sec~Butylbenzene [ - -ND-- , ug I L . 0.1 100-42-5 ! Styrene ·r;:fr:i ___ i_ ugTL 1 - :--0-:-1---r-----1

156-60-5 t-1,2 Dichloroethene ND-----j -ug I L - . 1 - r----0~1----r-·-- I 10061-02-6 t~1-,3 Dichloropropene _:._. --~D - -1 ~g/ L _l' 1 t~~1~=-=i=---j

98-06-6 ___ tert-Butylbenzen~ _ ___ · l1 -. ~-ND __ _ __I.IQ~--. __ 1_ __ ~ 0.1 1

'

! 127-18-4 Te_t~achloroethylene ---· . ---~ND ug IL I 1 ___________ 0._1 __ --+------ _,

1 108~88-3 ___ Toluene ___ _ ---~D ug IL ! 0.3

79-01-6 Trichloroethene ____ ~ ___ N_D __ ±· ____ u_ ~I L 0.1 75-69-4 Trichlorofluoromethane • ND ug I L

1

0.1

75-01-4 Vinyl chloride ---:_-~= ~-~_fl.__[ 0.1

EPA 504 EDB/DBCP by GC/ECD ALG

: =====-+ 1,~~~~~~;;1:~~~=--t- ND

ND

ug IL --~----

ug IL

By:

0.025 - -

0.025

i 05-05-03 05-06-03

-1 05-05-03 05-06-03

Unless otherwise noted, all samples were received in acceptable condition and all sampling was performed by client or client representative. Sample result of ND indicates Not Detected, ie result is less than the sample specific Detection Limit. Sample specific Detection Limit is determined by multiplying the sample Dilution Factor by the listed Reporting Detection Limit. All results relate only to the items tested. Any miscellaneous workorder information or foonotes will appear below.


STANDARD


Quality Control Summary

Client:

Project:


APRIL 03 SAMPLE EVENT Explanation of codes

.. ,-~-~-~---------------

[)_j Not applicable due to sample dilution

L Not applicable due to MDL proximity Order: 0304502 PHl16

Type: LCS: Lab Control Spike Matrix: WATER

Run Sequence

M03559 MT.2003.522.16

X03200 XG.2003.727.9

XG.2003.727.9

X03206 XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

· XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

Page 1 of 25

Dilution Detection Run

CAS# Analyte Result Units Range Factor Limit Code Date

EPA 245.1 Mercury by CVAA

7439-9~~ ! ~=--H Mercury -------

EPA 504 EDBIDBCP by GCIECD X03200-002

-- •• __ -• T. 1,~~~~~~::!~~~~~:~~~~e r- ~~-19_09_4 ___ -_-___ -__ -_+L-~--:-:-:~-c:-~:~~t--~~ ~ ~:~~I --- -__ -___ -__ -~;-_ El EPA 524.2 rev 4 Purgeable VOCs by GCIMS X03206-013

7-5--34--3-- - 1, 1 rnohlomelh.oe 81 % Reoove,,. 70 - 130 1 -r-NA i 1 .

1

__ 7_5-354_-_-- ~ 1, 1 Dichloroethene 80____________ i %_o_R_e_co_v_e_ry-+-_7_0_-____ 1_3 __ o 1 . --- -- NA ! ,

I ~:;·_56_-_! 1 :-::-~~:::::::~~· ~;- 1J:::::~ ;7:0···-~- :1:3:0:~ ~ J1~+-~NiA~t~ 79-34-5 1, 1,2,2 Tetrachloroethane 100 . % Recovery

S63-58-6 : 1, 1-Dichloropropene ·9a·- , % Recoveryt° 76- - ·130 ·- ----NA-~· ___ , -•-•-••-••••• ---~• -- 0000-•<••< ••-·-+-------+-- ••• H : •-----·---••••--+------j

106-93-4 1,2 Dibromoethane (EDB) 105 ' % Recovery I 70 - 130 ~ 1 NA

95-50-1 1,2 Dichlorobenzene _ _____ 99 '.01~Re~~v_e~~--?~-::_130 ~r-~--=~-NA"-107-06-2 ,2 Dichloroethane (EDC) ___ L_ __ 97 ___ % Rec_o_~-~~~- __ 70 _- 130 1 · NA 78-87-5 1,2 Dichloropropane i 95 · % Recovery 70 - 130 1 NA

-96-1i4-- 1,2,3 Trichloropropane 97 -% Recovery 70 - 130 --1-- NA

87-61-6 1,2,3-Trichlorobenzene 105 % Recovery 70 - 130 NA --------·--------------+-- -~--- ---+---j

120-82-1 1,2,4-Trichlorobenzene ______ , ____ 1 __ 0_5 ___ -+-_% __ R_e_c_o_v_e_ry __ --~0-~ 130 NA

95-63-6 1,2,4-Trimethylbenzene 98 % Recovery 70 - 130 1 NA

:!6-12-8 _I· 1,2·.0ibromo-3-chloropropa_n_e _____ +-r----9-2-----+-0/~Rec~~~-ry 1--~----~_i___1 ---r- NA

541-73-1 _ (_ 1,3 Dichlorob_e_n __ z_e_n_e ___ ,_i' ____ 8 __ 5__ _ _ _ _%Recovery I 70 - 130 1 ___ l _____ NA _______ ··--------108-67-8 i '1,3,5-Trimethylbenzene ! 105 °/a Recovery I 70- 130 : 1 NA

-------~----- ---- -· --- - ------------------'--- f--------.

05-05-03

05-05-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

142-28-9 I 1,3-Dichloropropane ~8 . _ . _ _ _ __,_% ___ R_e_c_ov_e_ry_,~' _7_0 __ -__ 1_3_9 ! .. NA I 05-07 -03

106-46-7 1,4 Dichlorobenzene 98 ---------- ----- --· -·--

99-87-6 1,4-lsopropyltoluene 101

% Recovery 1

% Recovery

70 - 130

- 130 70 H __ N_~~=- ~ 05-07-03

. NA 05-07 -03 ·-- --

594-20-7 2,2-Dichloropropane 88 , % Recovery ----~-----------+ - ------- ·----··

2-Chlorotoluene 97 i % Recovery ----- ---·

···-·---·-

70 - 130

70

______ ,_ ___ __,_ __ -j

1 ; NA ----- -------+-----··----

05-07-03

05-07-03 95-49-8

106-43-4

71-43-2

108-86-1

4-Chlorotoluene

Benzene

99 % Recov!_f'J_ 94 % Recovery

70 ----

70 ~ ::: --·=l~j--'=~ I 05-07-03

--1 05-07 -03

100 70 ...,

Bromobenzene - 130 i 1 ; NA 1

! % Recovery,

97 % Recovery j 70 0 !~-::-::--~--- - :::::~~~;:~~;~~e--~---:~; ~ :::::~ I ~~ ~ ;:~lm~ r-: 1 ~

74-83-9 - - ---8-ro-momelhane I 87 ; % Recovery --70 ·.:--· 130 1 · - 1 ;-- NA ---r---- 1

56-23-5

108-90-7

124-48-1 ----·

75-00-3

Carbon tetrachloride ---+1---95 p;;Recoveryi-70:-130 , 1-·--- NA 1----! Chlorobenzene I 96 rn--1o1o Recove~-- -io _- 130 - NA----r----1

Chlorodibromomethane _ 107 i 0/oRecovery J _fo ___ fao NA -~:--j Chloroethane i 86 Tei/; Rec0very !-7o·.:--1 :30 1 NA

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

67-66-3 - i Chloroform -go- J 0/o Recovery 70 - 136 T 1 · NA I 05-07-03

74-87-3 t Chloromethane --· ··----- --------156-59-2 cis-1 2 dichloroethene

10061_:0_~-~ -_ ----cis-1.~ dichloropropene

...,.+---------------:~---_-[~ :::~1T;:~J-F-J~-~~--106 % Recovery 70 - 130 1 NA

----- ~---- -----~-~

05-07-03

05-07-03

05-07-03


STANDARC



Client:

Project:



D Not applicable due to sample dilution 1

Order: 0304502 PHl16 L Not applicable due to MDL proximity


Run Sequence

X03206 XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

X03206 XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

Page 2 of 25



EPA 524.2 rev 4 Purgeable voes by GC/MS X03206-013

~ ~ m o;:~:::;;,:· i n ---i: .... -J~:~tiliii~-::-r--~r :~;::; -:~_.:::~-I ";:::,~;;:.~::~;· I -~~------~~~~:~:~~ 1 ~~ : __ ~-~~ _' - ~ - --t-~ ~::~~:~~

75-09-2 Methylene chloride I 82 1 % Recovery 70 - 130 _1__ L _NA 05-07-03

91-20-3 , Naphthalene 107 % Recovery 70 - 130 1 ! NA ! 05-07-0'.>

;;:: • ,"::;;~;:::. : r: _ ~ :::::~ ;: : : :: m._~:__, nn ~: I nl ::::~: 3j~~~~:; p/m-Xylenes 94 __ % Recovery 70 - 130 _ --~ ___

1

NA 1

05-07-o:

135-98-8

100-42-5 sec-Butylbenzene 95 % Recovery_ ( __ 2_0_-__1_ :30 · 1 NA_ _j __ ~

Styrene 96 % Recovery 1 70 - 130 1 t NA , --156-60~5--;---t--1-,2--D-ic_h_lo_ro_e_t_h_e-ne- 85 ----- 0io Recovery I 70 130 i 1 - NA I ..

10061-02-6(- t-1,3 Dichloropr_o_pe_n_e __ _:-c----~-1-0~2_-_-_-_-_-_-!-%~~CJ_~ery_L_?O: 130~r-~ l__~~NA ~ _-1_

9

2

8

_; __

016_~_~4_[--_~-----T_~_et_~~-~-~-~-;-:-:_~-h_z_Y_e_le_n_~~e~~~~---...,.+_--=-- --~-07_0 ! ~ ~::::~[ ~ Ji:i ~ -1 ~~ .U t---= 108-88_-3____ _T_o_lu_e_n_e ________ j 93 _!'o~e9_o_v~2'-+---~----1_3_0_L __ _1_ __ J__ NA __ J _____ _

__ 79_-_o~-~- _ _ __ T_r_ic_h_lo_r_oe_t_h __ e_ne ___ ~-----~~- % Recovery ! 70-=._~~ _ . __ 1 1

NA _ _L _ __J 75-69-4 Trichlorofluoromethane ~-----9_8 ___ --+-_% ~~~_c>~_rrL_?9 - 130:1:1 ___ 1 __ __J_ NA I I

, _75_-0_1-4_~_ Vinyl chloride _____ 7_6 ___ ~_% Re~~~ry_L __ ?~ ~-_1_ 30 _ _ __ 1___ -~I __ N_A __ ~--~

EPA 524.2 rev 4 Purgeable VOCs by GC/MS X03206-025

05-07-0:

05-07-03

05-07-0C>

05-07-0:

05-07-03

05-07-o:,

05-07-0'.

05-07-03

05-07-03

05-07-0:

1, 1 Dichloroethane ! 90 - %-Recovery ! 70 - 130 I 1 I NA i I 05-07-03 ·-----c------------~-----·---7---~-----------r--------:-·------,-i----j!

75-34-3 i

75-3:-4 _____ 1 ,_1_D __ i_c_hl_o_ro_e_th_e_n_e ___ c---------- -~_'._ __ _ _ -+% Recovery I 70 - 130 I 1 1 NA 1 _j 05-07-03

7~5 __ 5_-6 ________ 1_,_1_,_1_T __ r_ic_h_lo_r_oe_t_h_a_ne __ ~'----- 99 % Recovery! 70- 130 ____ 1 ______ N_A __ ~11 _____ ! 05-07-o: 1, 1, 1,2 Tetrachloroethane 105 % Recovery 70 - 130 1 NA i

------ '-------- ----~----+--------+

630-20-6

79-00-5 1, 1,2 Trichloroethane ' 91 ! % Recovery 70 - 130 1 NA

79-34-5 1, 1,2,2 Tetrachloroethane ' -- ---i 17- -- -ro;; Recovery 7o-- 130 - - 1 ' NA I ~~-58-6 1 '1-Dichloropropene i 112 p;., Recover;; 70 - 130 1 r NA-- - ----~~ 106-93-4 1 ,2 Dibromoethane (EDS) 99 ! % Recovery 70 - 130 1 j__N_A ___ ---+ __ _,

95-50-1 1,2 Dichlorobenzene 120 i % Recovery 70 - 130 , 1 NA

107~66-21 1,2 Dichloroethane (EDC) 103 i % Recovery 70 - 130 1 - - --NA--- ---78-87-5 I 1,2 Dichloropropane 102 ! % Recovery 70- 130 1__ _ -~~-r----96-18-4 I 1,2,3Trichloropropane 110 !%Recovery 70-130 1 NA

87-61-6 ! 1,2,3-Trichlorobenzene 113 ____ ] %Recover,; 70- 130_j_ 1 NA

120-82-1 I 1,2,4-Trichlorobenzene 120 : % Recovery 76 ~-13-0-=.[-1 NA

~5-6:3_~~ _ :__ 1,2,4-Trimethylbenzene ------12~----- ---%Recovery _ 70 =- 1 :30 __ i - ___ 1 __ --r:----N-A- ---r-----j

:461--~2;~1 1,2-~i.~~::!~::l:~~~~o:ane ----~~ __ ___ _ -~ ~:~;~:~~- ----~~ :-+}~ _[ -+--= -1-----~~--108-67-8 1 1,3,5-Trimethylbenzene - ----- ----fa4 ___ ---%Recovery -7()~130--t----1-- - --N--A----+-----+

-142-28-9 1,3-Dichloropropane --- -- --- .. -- io7- ------ o/~ Reco-;;e;:y -70 - 130 1 1---N-A-----+--_,

1-06-46-7 +--1,4Dichlorobenzerie--------,-- --·-124------0/o Recovery -70~13o 1- NA ------~----------------------~~--- -------~---- ----- -- ---------- ...

99-87-6 1,4-lsopropyltoluene I 138 ; % Rec()very 70 - 130 1 NA ---~--------------- --- -

05-07-0~

05-07-03

05-07-0~

05-07-0?

05-07-03

05-07-0~

05-07-0~

05-07-03

05-07-0~

05-07-0?

05-07-03

05-07-0~

05-07-0~

05-07-03

05-07-0~

05-07-0~

05-07-03

05-07-0~


STANDARD



Client:

Project:



D 1

Not applicable due to sample dilution Order:

-r--L i Not applicable due to MDL proximity 0304502 PHl16


Run Sequence

X03206 XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

X03206 XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

Page 3 of 25




594-20-7 r 2,2-Dichloroprop~ne _______ !_______ 103 I% Recovery. 70 - 130

95-49-8 2-Chlorotoluene I 125 I 0;.; Recovery ~- 70 - 130

Hi~_43_-4_---:- __ --~~~6!.~rOl~ene--~--129 ___ ----[}'~Rec-ov-e~y~~~~~-1_3_~ -~ 71-43-2 Benzene 106 % Recovery 70 - 130

108-86-1 Bromobenzene 1 118 I % Recovery 70 - 130 Bromochloromethane-----;--------92 ___ -, 0;; Reco\/-ery ,- 70---136

-------- -"! ---- . 75-27-4 Bromodichloromethane 105 : % Recovery 70 - 130

15:25-2 -_:-- sromotorm 107 - i 0/o Recovery-, -~~-13~ 74-83-9 Bromomethane 121 I% Recovery 70 - 130

NA

NA

NA

NA

NA

NA

NA

1 NA

1 NA ---t---

NA

X03206-025

-+----

. 5~-23-5 _ _ ____ Carb~~__!etr~~~o__r~~~--+-----106 ______ : o;o_Re~~~~_ry __ . !O - 130 -- - -----------+---_,

1~~90-7 _ _____ Chlorobenzeri_El__ ----+-----1_(:)<t__ _ _0(o_~El_~~~El_r!'_ 70 - 130 124-48-1 Chlorodibromomethane ! 109 % Recovery 70 - 130

NA ________ __,_ __ _,

75-00-3 Chloroethane :---110 -+

67-66-3 Chloroform i 93

. ,',:';:, ju ,;;~~~:,:·~;;~.,-, u i-.--.------_-181: '10061-01-5 - -ciS-1,3 dichloropropene 1 112 1-7~ Dibromomethane --i------- Sia ____ _ [ 1~~-[ -- --l=tilylbenzene~ I__ -111 ___ _

~--~~~-.:::. ·t· ----H:~::~d~:n~ 143

133

98-82-8 lsopropylbenzene 134

75-09-2 Methylene chloride ----------

82 ' ~-- ·--- ------------

91-20-3 Naphthalene 129 104-51:0 I -1i-=-sli!yit>e-r1zene ------ 131

n-Propylbenzene 103-65-1

95-47-6 ----

125

123

120

o-Xylene

! 108-38-i 31106-42

p/m-Xylenes

NA

% Recovery 70 - 130 NA - - --------- --------- -- - -

% Recovery I 70 - 130 1 NA

- --% Re-cov€lfX 70 - 130 1 _1 ~ ~ d __ _ 'Yo ~e_:_~ve~y- f- !_-° - 130 1 _ -~ __ _J

__ % ~e.c:_~v~~ L ?_~_:_ 130 __ 1 ___ ~_f1J_A _I

o/oRecovery_l_ 70- 130 1 " ___ NA-+---'

~ :::::r ;::~::ti ~} ~-*~--I ~0/o" Recovery -- ?o -~ 136 - ---1 -- ' NA

-·--- -----·----·--·-. --------------- ____ __J ______ ,_

% Recovery 70 - 130 1 NA --------+---_,

,010 Re_.c:.ov~~-_!_0 -_1_3_~--1-----1 NA % Recovery 1 70 - 130 I 1 NA

· ; 010Recovery- 1 ?o-~--130 +----1- NA l ---+-------~

_ '010 _ R~cCJ_\/El_~Y~~ !0 - 130 --~ 1 NA % Recovery 70 - 130 NA

'135-98-8 1

I 100:42:5 · I -

sec-Butylbenzene 125 _______ 0 /o -Reco~e;:-y-1-76- 130 NA ,--------i

t-1,2 D~~~~=~oeethene ,--- __ -_ -1:6

3 ----~-~-~:-;~~J=f~~~~~ :~~ ~ l-=-~ 156-60-5

1 10061-02-6 --·--t--·1·--,-3·-D-·i--ch--l-o--ro-·-p--ro--p-e--n-e-----~------1--0 __ 9___________ % Recovery 70 - 130 1 ---N-A-1--··----------------·- - -t·-------------~ --------- _________ ______; _____ +-----1

98-06-6 _____ t_e_rt_-B_u_t_y_lb_e_nz_e_n_e ___ -j ______ 1 __ 2_9 ______ ic-% Recovery 70 - 130 1 .i NA

~.-~~~-~-:_-[ __ --_-_-____ T __ et-~-c-~-~o-j~--~-~-~--y-le_n_e_---_-_ __,_ ______ ~_~ __ :_-_-__ -_ _j_f: ::~;~:~ ;~ ~ ~ ~~ --~-~--:~~~----1~ 7759--609~_:_4~_ . 1

1 Trichloroethene 102 1 % ~ecovery 70 - 130 __ ---~---t------~ Trichlorofluoromethane 116 % Recovery 70 - 130 1 NA

' !5_:0_-1-_-4_-~-j~-----_---__ -_-_-_v_in_y_l_c_-h_lo_ri_d_e __ ._---_-_-_--_·---~-------_--_· __ 9_8 ____ __'Yo Recovery -7~_::_13_0_ 1 -- --=_flJ_A-_J=_=J

EPA 524.2 rev 4 Purgeable VO£_s _l>}'__~_C!_n/l_S _____ _

!5~~~~--' _____ 1_,_1_D_i_ch_l_o_ro_e_th_a_n_e ___ +-___ 10_1 __ -_--_-_~%Rec0ve-ryI_~ci~-~13o ___ . 75-35-4

71-55-6

630-20-6

1, 1 Dichloroethene 84

1, 1, 1 Trichloroethane 94 ---------------+----

1, 1, 1,2 Tetrachloroethane 94

: % Recovery 70 - 130

-:01-,;-ReCOvery- 70 - 130

i % Recovery 70 - 130 ------~------------------~---------~---~--------------L

X03206-031 - - NA·---T---·-,

-c----N.A.-+----c :--N.A.---i----• ' I , -~= NA-~-_1--=~~

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03


STANDARr Assaigai Analytical Laboratories, Inc.


Client:

Project:



D Not applicable due to sample dilution

L I Not applicable due to MDL proximity Order: 0304502 PHl16


Run Sequence

X03206

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

Page 4 of 25



X03206-031 EPA 524.2 rev 4 Purgeable VOCs by GC_l_M_S ___ _

, - 79-00-5 --T 1, 1,2 Trichloroethane 96 I' % RecoveryT 7o-.=-~ 1

79-34-5 - 1 --- 1, 1,2,2 Tetrachloroethane 97 I % Recovery [H76--_1~~] - 1

--NA-~~

_N_A _ _J__j 563-58-6 1 , 1-Dichloropropene 94 I % Recovery i ·· 7o--13o--~ --1-- NA I I

- ---------------------1,2 Dibromoethane (EDB)

--r --- ----- - --96 ' % Recovery 70 - 130 __ 1 - _( NA I

·---------·T

I 106 % Recovery : 70 - 130 1 1 i NA --------.,--------- ·-----.. __ _, __ - -- -- --------+---------

I 94 % Recovery I 70 - 130 ' 1 : NA

------1------- _ ____j_ __________ _J_ ·------95 % Recovery i 70 - 130 I 1 ' NA

% Recoveryr?o~ 130 i -·---

104 1 NA ---- --~

106 % Recovery 1 70 -~ 1 NA

% Recove-r"YT-?o--=--130 ---------

108 1 NA

106-93-4

____ 9_5-_5_0-_1 _____ 1_,_2_D_ic_h_lo_r_o_b_e_nz_e_n_e __ --+1

i _

107-06-2 1,2 Dichloroethane (EDC)

_79_ 68:81!_8~4~_1 ___ 1_,2_D __ ic_h_lo_ro_p_r_o_p_an_e ___ J--+----------1,2,3 Trichloropropane i

87-61-6 1,2,3-Trichlorobenzene t -+-------------+-----

120-82-1 1 1,2,4-Trichlorobenzene -~---- ---~

I 100 % Recovery! 70 - 130 1 I

NA -- ~--------- -- -·-----

99 j % Recovery 1 70 - 130 I 1 NA

104 o/o Recovef"Yl=_7o :- 130 T 1 NA

108 ' % Recovery 70 - 130 1 1 NA

95-63-6 1,2,4-Trimethylbenzene

96-12-8 1,2-Dibromo-3-chloropropane -<------

541-73-1 1,3 Dichlorobenzene --+--------------·- ·-·------

108-67-8 1,3,5-Trimethylbenzene ------·- --------- -·---~-----

142-28-9 1,3-Dichloropropane 97 : % Recovery 70 - 130 1 NA --~- -·----- ... ----- ------

106-46-7 1,4 Dichlorobenzene 101 : % Recovery 70 - 130 1 NA l----------------+---~----- -·-·----- --·- ---------

99-87-6 1,4-lsopropyltoluene --+---

594-20-7 1 2,2-Dichloropropane -95--49-:S t·-----2---C-h-lo-r-ot_o_lu_e_n_e----+----

106-43-4

71-43-2

108-86-1

75-27-4

75-25-2

4-Chlorotoluene

Benzene

Bromobenzene

Bromochloromethane

Bromodichloromethane

·r

-------Bromoform

·----~--

104 ·%Recovery ---

84 ! % Recovery

105 ; % Recovery

105 : % Recovery

95 I% Recovery --- --

101 I% Recovery

_______ j % Recovery 100

95 -

100 % Recovery

70 - 130 1 NA --~-----------

70 - 130 1 NA -~----- r--- ---

., ________ --

70 - 130 1 NA ----~-

70 - 130 1 NA

70- 130 1 NA - ---- -

70- 130 1 NA ---··--1--

70- 130 1 NA --- - ----- -----

70- 130 1 NA ------- __ T ________

·--~

70 - 130 1 I NA ---------- ..

74-83-9

56-23-5

108-90-7 I

Bromomethane

1 % Recovery

101 1 % Recovery I 70 - 130

90 _ j 07o Re-cove .. ri!76-=-13o ~-1 NA

- ! 124 48 1 - - I

' 5-00-3

Carbon tetrachloride

Chlorobenzene

Chi d'b th oro I romome ane

Chloroethane -- --------

7-66-3 ----··

4-87-3 I

56-59-2 I

061-01-5r·· • 10

7 ............. J 4-95-3 I

00-41-4

7

8

5-71-8

7-68-3 -~---

8-82-8

5-09-2 :

9

7

9 ............. ____ + 1-20-3

04~51-:0--i--------1------

03-65-1 I

9 5-47-6 I ---- _______ ,_ ___ .J -

Chloroform

Chloromethane

cis-1 ,2 dichloroethene

cis-1,3 dichloropropene

Dibromomethane

Ethylbenzene

Freon 12 -

Hexachlorobutadiene

lsopropylbenzene

Methylene chloride

Naphthalene

n-Butylbenzene

n-Propylbenzene

o-Xylene

1 i NA I

__ 101 ___ i % Recovery 1 70 - 130- . --------- ---1

1 I NA I I 96 I o ecovery - I I

------~------r= 105 , % Recovery 70 - 130 ' 1

i % Recovery 130 T _____ 1 ____

92 70 ---- --- _ _,_ -·-- ------ --- ·---

91 , % Recovery 70 - 130 1 ----- --- ----

92 % Recovery 70 - 130 1 -------·-·- ---- -- -- ...

99 : % Recovery 70 - 130 1 -~------ -------- - ---·- --- - - --·-

99 _ ~- 0/o~_e_c;~vEl iy _ 70 - 130 1 I

I --- -----~--- ------

NA

f-=~r~+-----j NA

--j------j

98 i % Recovery 70 - 130 1 I ------· ----- --- -

T01~Recover}i .. -------~-------L

93 70- 130 1

NA --+---.....j

NA ~-

103 i % Recovery 70 - 130 1 NA -- ---------·---- --

---- ro;~-RecaverY" r------- ----~-- ---- ---····--

108 70- 130 1 ----------

NA ----I

85 % Recovery 70- 130 1 ! --------------·- ·- -----· r---·------ ·-·--

113 % Recovery 70- 130 1 I ! NA

NA

101 % Recovery 70 - 130 1 1-

NA

102 % Recovery 70 - 130 r----------

1 i

-----------100 % Recovery I 70 - 130 1 I

NA

NA --·----- -

05-07-0:.,

05-07-0:'

05-07-03

05-07-0:C,

05-07-0:'

05-07-03

05-07-0'.:>

o5-07-o:·

05-07-03

05-07-0'.:>

o5-07-o:·

05-07-03

05-07-0J

o5-07-o;

05-07-03

05-07-0'.>

05-07-0:

05-07-03

05-07-03

05-07-0:

05-07-03

05-07-03

05-07-0:

05-07-03

05-07-03'

05-07-0:

05-07-0:<

05-07-03

05-07-0:

05-07-0:>

05-07-03

05-07-0~

05-07-0~

05-07-03

05-07-0<

05-07-0~

05-07-03

05-07-0~.

05-07-0:'

05-07-03

05-07-0~

05-07-0~

05-07-03

05-07-0~

Coyote 2001: Reports 1.0.011109162500 Report Date 61412003 12:30:22 PM·

STANDARD Assaigai Analytical Laboratories, Inc.


Client:

Project:



D Not applicable due to sample dilution ---- ----------------



Run Sequence

X03206 XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

M03548 MT.2003.521.11

MT.2003.511.35

MT.2003.511.35

MT.2003.521.11

M03550 MT.2003.551.12

MT.2003.551.12

MT.2003.551.12

MT.2003.551.12

MT.2003.551.12

MT.2003.551.12

MT.2003.551.12

MT.2003.551.12

MT.2003.551.12

MT.2003.551.12

MT.2003.551.12

MT.2003.551.12

X03194 XG.2003.785.13

XG.2003.785.13

XG.2003.785.13

XG.2003.785.13

XG.2003.785.13

XG.2003. 785.13

X03189 XG.2003.750.4

X03165 XG.2003.622.2

XG.2003.622.2

Page 5 of 25



EPA 524.2 rev 4 Purgeable VOCs by GC/MS X03206-031 1, 108-38- r-- p/m-Xylenes T----- 100 · % Rec;~ery[- 70:-13()"1--1·---:-N.A. T----J

~~~1::: I ---~~sec-B~~:~:zene --- -I . 1'! m-==~~:::£ ~-=~-r---~ £ -n-n I _~.,60~5_ ;:_ t-1,2 D;ohlo<0elheoe : · · 86---- % Recovery-· ·70-:.-130T---.,.-- NA · ,

1

10061-02-6 l_m _t-1,3 Dichloropropene ' 1_90 t>1;;-Recovery, 70- 130~-- UH ______ i\J_~-j---_-_JI 98-06-6 I tert-Butylbenzene 105 ' % Recovery 70 - 130 1 NA l 12rn4 I Tetroohlo<Oethyleoe _ I ;2 ' % Reco"'Y 70 - 130 I ~-:=- ' - -~09~~~~~3 ~ _ Tric~~~ee~~ene=r--= =--~~~ ~~~=$.: ::~:~:~ ;~~ ~~~ +- --~ __ -j_ ~~ --~ =: ~5-6~"- _ Trichlorofluoromethane I 101 ..... Eo Recovery ; _ _2()_- 1 ~O 1 ~- __ NA __ L--75-01~~-L _____ ":'inyl chloride ' ---~---- __ :_ 01o_~_e_c:o'-'_ElrYJ___2_(}-__ 130 ~--1 NA l ___ ~

M03548-002

NA

NA

NA

-----)-----'

----~--1

SW846 3005A6020 ICP-MS M03550-002

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-01-03

04-30-03

04-30-03

05-01-03

•~ ~:~~~~ - ~- ul gg;i~ -i~]-1 ~~~ jl -=l l~l:l~ 7 439-92-1 Lead 97 % Recovery 85 - 115 , 1 I NA =j 05-05-03 7 440-02-0 - -----NiCi<eT -- 95----- % Recovery

1

a5 ~---1- ----1- NA - - -- - ' o5-o5-o3

7!02-49-2 _ selenium - ------ 1 oo -=-Lyo'R.ecover'Y'as.=-m-,.---1-------~----"-----·-c o5-o5-o3

~40-22-4 __ Silver 96 , o,lo_~~-C()Very ~-~-1---1 ----~-NA _ 05-05-03

7440-28-0 Thallium 95 "jo Recovery _ 85_~_ 12_5_ -1 _ 1 _, __ NA 05-05-03

7440-3{:5-,----------nr; 97 _

1_o/o_~~c~"=.2' -~-~.1_1__.5 +-. _1 __ J_. _r-J_}),_ 05-05-03

7440-62-2 Vanadium 96 __ _"-1<> Recovery ~-~21_5_ l. 1 I. NA --~----~ 05-05-03

~4~~-66-~i ------Zinc-- 100 _ % Recovery I _ii_~ ~-21_5 ' NA -----~' 05-05-03

SW846 3510818081A Pesticides by GCIECD X03194-002

;_~~-:~,r-~--~~--~~-·-i-~_~::" - ~ :== I~:::::~ I:~: r ••. j--1-.·.~.·-•·.~--···.=-_l_,-_-__ -.1 ~8-89-9 •-- _ g-8HC ___ t=_H~4 _ . ·- . i ~~ ~e~~"=.2'l__~6_ ==_1_2_3 -i- _ 76-44-8_________ Heptachlor ! 77 _______ G% R~co_very 1 40 - 131 __ NA __ , __ __j 50-29-3 _____ p,p-D~T__ , ________ 94 , % ~ec;()"=ry_L_:3_8_~ 127 NA j__ ___ _J

05-08-03

05-08-03

05-08-03

05-08-03

05-08-03

05-08-03

SW846 35108/8082 PC8s by GC/ECD X03189-002

[ 11095:92:5r==---Aroc1or 1260 . , .. _____ -~~~--=------% Recol/erY:C6o- 120 NA_-~L_J 05-06-03

SW846 35108/82708 SVOCs by GC/MS 120-82-1 1,2,4-Trichlorobenzene 1 79

106-46-7 _ "----- 1,4-Dichloro_~_e_n_z_e-n_e=====-1~1=======72 p!o _l'{ecovery r

__ ]_% Recovery I

Coyote 2001: Reports 1. 0. 011109162500

39 - 98

36 - 97

X03165-002 , NA , l 04-10-03

---: -NA~=1----~--°j 04-10-03

Report Date 61412003 12:30:32 PM



Client:

Project:



D Not applicable due to sample dilution

L _L Not applicable due to MDL proximity Order: 0304502 PHl16


Run Sequence

X03165 XG.2003.622.2

XG.2003.622.2

XG.2003.622.2

XG.2003.622.2

XG.2003.622.2

XG.2003.622.2

XG.2003.622.2

XG.2003.622.2

XG.2003.622.2

XG.2003.622.2

CAS# Analyte Result

SW846 35108182708 SVOCs by GCIMS

Units Range

Dilution

Factor

2,4-Dinitrotoluene 80 ----i-o/c-o-R--e-co-v--e-ry--,--2-4 ___ 9_6 ____ - ( -------+--------+-------+------+------

2-Chlorophenol 7 4 I % Recovery 27 - 121 1 --------·----- ------------j---------t--------j--------t--------

95-57-8

59-50-7 4-Chloro-3-methylphenol 72 ' % Recovery 23 - 97 1 --- ---

100-02-7 4-Nitrophenol 35 ' % Recovery 1 O - 80 1 ----+---------------------~--------

83-32-9 Acenaphthene 83 i % Recovery 46 - 118 1 -----+--------------+---------+------+------+--- - ----117-84-0 di-n-Octylphthalate

1

145 J."'10 Recovery 26 - 127 --_-62-1__--6-4--7---+L-___ -_n-_:_N_i~-ro-so-di-n-propylamine I 81 j o/c~ReCc>Very~M-116--

87-86-5 I Pentachlorophenol 1 81 I % Recovery 9 - 1_~-~----- -- ---

_1_08_-9_5_-2_t---____ P_h_e_n_o_l ______ _L ____ ----~~------i ~ ::~:~:~~ 12- 89 129-00-~J__ Pyrene i _ 26 - 12~_J __

1

Detection

Limit

Run

Code Date

X03165-002

! NA I !---~--·-· -<-·-----

: NA : ----~----- ----------·--·--

: NA : 1-NA - __ , ---

NA

NA

04-10-0~

04-10-0'

04-10-03

04-10-0"

04-10-0"

04-10-03

04-10-0:.,

04-10-0~

04-10-03

04-10-0::»

Type: LCSD: Lab Control Spike Duplicate Precision Matrix: WATER

Run Sequence

M03559 MT.2003.522.17

X03200 XG.2003.727.10

XG.2003. 727.10

M03548 MT.2003.511.36

MT.2003.511.36

MT.2003.521.12

M03550 MT.2003.551.13

MT.2003.551.13

MT.2003.551.13

MT.2003.551.13

MT.2003.551.13

MT.2003.551.13

MT.2003.551.13

MT.2003.551.13

MT.2003.551.13

MT.2003.551.13

MT.2003.551.13

MT.2003.551.13

X03194 XG.2003.785.14

XG.2003. 785.14

XG.2003. 785.14

Page 6 of 25



EPA 245.1 Mercury by CVAA M03559-003 7439-97-6 Mercury 4 RPD .--=-1\l_A -:--_ I 05-01-0:>

EPA 504 ED81D8CP by GC/ECD X03200-003

I - 1 1,2-Dibromo-3-chloropropane _ ~=-3=_--=~~--=[_-RPD----r-o~o-- J__~ 1---=~=~-~-=- ;___ -~

_____ J ___ 1,2-Dib~o_m_oe_t_ha_n_e_,_E_D_B ______ 1_ L __ ~PE _L_?- 20 __ l 1 NA 1

•

05-05-0:

05-05-03

SW846 3005A/601 OA ICP M03548-003

7440-48-4 Cobalt 8 _____l__ RPD 0 - 20 ~-- - ~- --+---~~-- ---- ~::~~:~~ 7~~o_-4_7_-3 ________ C_h_r_o_m_iu_m ____ -+-____ <_1 __ --r-__ RPD ____ -._·-__ ---0 - 20 -- ,-- --- -~

74_4_0--5-0--8~-----C-o-pp_e_r------+---_-_-_-_-_-7~~~~~~~:~~~R~P~D~~~:~~=o_·-_2_0 J- --!=--1-NA-- -- 05-01-03

SW846 3005A6020 ICP-MS M03550-003 7440-36-o I Antimony ___ <_1 ____________ -: _______ R~P~o~~~_:-~~~o~-~-2-0~=-l: I

7440-38-2T ______ Arsenic----------;- --- 2 RPD 0 - 20 1

NA I 05-05-0:l

NA 05-05-0, l440-39-3 ! --B-a-rium --------.----------1------+---R-P--D----+--0---20___ --j--N-A-----+---t, 05 05 0° 1440-43:-gf- _______ C_a_d_m_i_u_m _________ ,___ ~ ____ R_P_D ____ o-2o-- 1 r NA ~ 05:05:0;

--~-:-_~-~-:~~~~:_~--t~----~~~-~~~~N_L-_i:-_:-:_-1~-----~--------t·[_---____ 2~~~~~~~~~~~=~-:-~-~-~-~---~-~-- -- -~----_r-:--- - ~::~::~~ 7782-49-2 I Selenium < 1

1

1 RPD O - 20 1 j NA ---~-l-·---------------+-- ----+------+------- -c--------,------

7440-22-4 ' Silver j RPD O - 20 1 NA ----~-------------+--------- -~-------'--~

7440-28-0 Thallium RPD 0 - 20 NA i

--:-:--:-:-::-~:-'-+~ 1.-·-------=--·=-~··=--.. =·v-=-a=-~=a-i~_d_n-~=u-_m·=--·=--··=--····=--··.:·+_-~--~-~<~~~1 ~--~,--=-=-~--+--:-: ~L ' -:11~~r-~ SW846 35108/8081A Pesticides by GC/ECD

309-00-2 Aldrin 1--1-4 RPD O - 22 ---+------------- +- ___ J 60-57-1 Dieldrin I 5 RPD ! O - 18

72-20-8 -- ---~~-9!!~- -- ------ L---~----- --~RP~-- ~t y--21

X03194-003

-N~-=T~ ____ N~ -- ~- --- ~

NA 1

05-05-03

05-05-0,

05-05-0:'

05-05-03

05-05-0~

05-05-0:'

05-08-03

05-08-0~

05-08-0~


STANDARD



Client:

Project:



D-[ -NaT8{J{Jlicible-due-taSam;;1edilutiOf1 L ;-fli<Jt-app1icab1e"due to MDL proximity 1 Order: 0304502 PHl16 ---- __ J


Run Sequence

X03194 XG.2003.785.14

XG.2003.785.14

XG.2003.785.14

X03189 XG.2003. 750.5

X03165 XG.2003.622.3

XG.2003.622.3

XG.2003.622.3

XG.2003.622.3

XG.2003.622.3

XG.2003.622.3

XG.2003.622.3

XG.2003.622.3

XG.2003.622.3

XG.2003.622.3

XG.2003.622.3

XG.2003.622.3

CAS#

--- -· 58-89-9

76-44-8

50-29-3


Analyte Result Units Range Factor Limit Code Date


g-BHC ;----5-__ ----------=~_R_P_D_--+-_O_- 15 -r ---1 =~-----_---_-N_A __ p Heptachlor 10 RPO 0 - 20 1 NA

-----p,p--D-DT ]__ _________ _?___ RPO o =-27--=l~ __ 1_- -------w\-- -----1

SW846 3510818082 PC8s by GCIECD X03189-003

05-08-03

05-08-03

05-08-03

[ 11096~82-~I Aroclor 1260 ==--==[=--==-=g-==-------= _ __f{_P~_ L __ 9_-==~--I==-J==--=----NA J 05-06-03

SW846 35108182708 SVOCs by GCIMS X03165-003 120-82-1 1- 1,2,4-Trichlorobenzene ___ T_____ 3 --r --RPD ____ o ~ 28-- - ___ 1______ NA

106-46-7 1

1,4-Dichloroben-zene--,-------1-----t-- RPD _____ o-=-28 -"- 1 -----NA--+---

- _RPD_ __ ~~-=-=E:-)a _ J _ ~A 121-14-2 2,4-Dinitrotoluene < 1

0- 40 I _j_NA __ _

~~[~_HI : --jt-----1

:: L+ f :-1 · 50 ' 1- NA- I i

I RPO ! 0 - 42 ! -r-NA --]---[

t ~_Po_=-+- -~-_:_33:_~-~:- r--~~- L __ _J

95-57-8 2 RPO 2-Chlorophenol -- +---

-Chloro-3-methylphenol '

4 RPO 0------~·-- -- - -·-·--- -- ·- --.------·--- --------

4-Nitrophenol 2 RPO 0-- ·--·

Acenaphthene 4 I RPO 0-I --------- ---------- -- --

di-n-Octylphthalate 90 I RPO 0-I

Nitroso-di-n-propylamine 1 I RPO 0-

Pentachlorophenol 4 I RPO 0-

59-50-7 I

- ---·--------· I·

100-02-7 I --- ---

83-32-9

117~04·:0 t-

4

n-

87-86-5 '

108-95-2 Phenol 2 129-00-0 Pyrene - - ----- .J _ --- 16

--------------·--------·- ·---- ·---- ··- ·-----·-·-·-----------

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

Type: LCSD: Lab Control Spike Duplicate Accuracy Matrix: WATER

Run Sequence

M03559 MT.2003.522.17

X03200 XG.2003.727.10

XG.2003. 727.10

M03548 MT.2003.521.12

MT.2003.511.36

MT.2003.511.36

MT.2003.521.12

M03550 MT.2003.551.13

MT.2003.551.13

MT.2003.551.13

MT.2003.551.13

MT.2003.551.13

MT.2003.551.13

MT.2003.551.13

Page 7 of 25



EPA 245.1 Mercury by CVAA M03559-003 7439-9!~~-J__ _ __ M_e_rc_u_ry _____ -~-~--·-_-_·-_·--- 102 - · -- -o;~Recovef}i1~~ao=-~~o~]---_i_~ __ I-w..-~-~ 05-01-03

X03200-003 EPA 504 ED81D8CP by GCIECD ---I~ 1,2--Dibromo-3-chloropropane ---100 _____ 0/oReCoVery ___ 60-..-140---r- ·- r --N;..-

--~!3_=~~I%i. Rec()11_ery_ 6o ~-140-! - __ _ _ j__NA __ . __ _ --- I ---12-oiiJromoetilane, Eos

SW846 3005A/6010A ICP 7440-41-7

7440-47-3

7440-48-4 .. ------+--

7440-50-8 1 _______ L ___ ·----

_B_e_ry_ll_iu_m ____ --j-] ___ 119 _ti ~ ~~c.Cl.verx ~-o - 120 _ Chromium j 114 % Recovery 80 - 120 1

_c_o_b_a_1t ____ ~ __ 1 o? -1 °10 Recovery ; - 80 -_ 120 --:-- ___ 1_ _c_o_pp_e_r _____ ~ ___ 111 ___ : % Recovery: 80- 120 j 1

M03548-003

SW846 3005A6020 ICP-MS M03550-003

~-::-:-::-:~-3 --~~:::L------+-----1-:0:-5----+:-· ~-:-:-:-::-:-:-·~--+------:-:-:--~~ .... ·~ . +=: . ~-7440-43-9 I Cadmium 95 1· 0;., Reco;;-ery ___ 85-~-1-15 -.- .. 1 . NA- -------~-------------·-- ---+-------- -+----------~--7439-92-1 Lead 95 1 % Recovery 85 - 115 · 1 : NA

7~_40_-0_2_-o_~------~- Nickel 94 ~~o~ery- BS-- 115 1 ~~---f\J~~- :-=-=-~ 7782-49-28 __ e_l_e_ni_u_m ____ ~ ___ 1_0_1 ___ ~ Reco11_~2'_ _ 85_-1_1_5 1 ; NA ' !

05-05-03

05-05-03

05-01-03

04-30-03

04-30-03

05-01-03

05-05-03

05-05-03

05-05-03

05-05-03

05-05-03

05-05-03

05-05-03


STAN DAR[



Client:

Project:



--T

D_ I Not applicable due to sample dilution 1



Run Sequence

M03550 MT.2003.551.13

MT.2003.551.13

MT.2003.551.13

MT.2003.551.13

MT.2003.551.13

X03194 XG.2003.785.14

XG.2003. 785.14

XG.2003. 785.14

XG.2003. 785.14

XG.2003.785.14

XG.2003.785.14

X03189 XG.2003. 750.5

X03165 XG.2003.622.3

XG.2003.622.3

XG.2003.622.3

XG.2003.622.3

XG.2003.622.3

XG.2003.622.3

XG.2003.622.3

XG.2003.622.3

XG.2003.622.3

XG.2003.622.3

XG.2003.622.3

XG.2003.622.3


SW846 3005A6020 ICP-MS

Range

Dilution

Factor

Detection

Limit

Run

Code Date

M03550-003

7440 22 4 ·i---· Silver 95 • % Recovery --85-- 115

77444400:23 81 :~5____ ThTal1

_1nium 94 ,%Recovery 85-115 ,_ _ -~i---N-A----+----__, ------------------~

1 NA I ! 05-05-o:, ·----------1----'

1 NA I 05-05-o:

95 , % Recovery 85 - 115 1 05-05-03

05-05-0::i

05-05-o:

Y440-62-2_[~~------V--a-n_a_d-iu_m ________ -+--------94--------,.-% Recovery 85 - ·1···1···-5·--t---_-_-__ 1-__ ~----~.,.1~~~-N-_A ______ :-_-_-_-___,_,

~4~0-66-6 _L_ _ Zinc 99 I % Recovery 85 - 115 1 !

SW846 35108/8081A Pesticides by GC/ECD 9-00-2

I

0-57-1 i

2-20-8

30

6

7

5 ------·--~--- -

8-89-9

76-44-8 I

-So-29-3 -r--

Aldrin

Dieldrin

Endrin

-BHC 9 Heptachlor

p,p-DDT

74 % Recovery I 40 - 120 I 1 I -103 % Recovery I 52 - 126 ' 1

---% Recovery I I 102 56 - 121 i 1

-----

99 % Recove ! 56 - 123 1 ~---- -1---~2'+--- - -- T 86 I % Recovery I 40 _-~1__ I __ 1_ _

--~------1-0_3 ______ _,'_% RecoveryT3$- 127 I 1 __L___ -- ------'--------- --- - L

SW846 35108/8082 PC8s by GC/ECD

NA

X03194-003

~E -J. -- !'!A __ - '. - - _J , __ NA ___ :

05-08-03

05-08-03

05-08-0:

05-08-03

NA . i 05-08-03 ·-·-- _; ____ ~

NA ' I 05-08-0: -- ----------~------_ .. ___ )

--------! 11096-82-5 I Aroclor 1260 63

X03189-003 ·:··--i\J;..----1-= 05-06-0:.:>

SW846 35108182708 SVOCs by GCIMS 120-82-1 I 1,2,4-Trichlorobenzene 77 ; % Recovery

·- -----106-46-7 1,4-Dichlorobenzene 73 i % Recovery -------- --------121-14-2 2,4-Dinitrotoluene 79 : % Recovery

95-57-8 2-Chlorophenol 75 1 % Recovery --· -~--------------

I% Recovery 59-50-7 4-Chloro-3-methylphenol 76 - ~-----~------

100-02-7 I

4-Nitrophenol 35 , % Recovery

83-32-9 I Acenaphthene 79 I% Recovery

117-84-0 1 _____ ?!~.n-Octylphthalate 55 I% Recovery

621-64-7 L n-Nitros~~di~_n-propylamine 82 '%Recovery

87-86-5 ! Pentachlorophenol 84 i % Recovery -------· I - -108-95-2 i Phenol 37 I% Recovery

129-00-0 I Pyrene 83 I% Recovery ------'------I

X03165-003

39 - 98

36 - 97

24 - 96

27 - 121 -- ------- -- -· ____ ...,...

23 - 97 i -------- -·

10 - 80

--· ---·

1

1

1 -----1

·---------1

1 f, -~~E_--·--NA I '

------~---J ' NA I

--------------- .J....... ....... ------' NA I -- ----- i ---i I NA : :

46 - 118 1

' -·

26 - 127 1 ~-----

_j_~~--l- ~ ~---~-~- --~

41 - 116 I '

1 -~--------

9- 103 I

1 '

i---~~--+--~ 12 - 89 1

26 - 127 L ___ 1_ -------

04-10-03

04-10-0:

04-10-0~

04-10-03

04-10-0~

04-10-0?

04-10-03

04-10-0~

04-10-0?

04-10-03

04-10-0~

04-10-0?

Type: MB: Method Blank Matrix: WATER

Run Sequence CAS# Analyte

M03559 EPA 245.1 Mercury by CVAA ---- ·- - ---·

MT.2003.522.15 I 7 439-97-6 Mercury

X03200 XG.2003.727.8

XG.2003.727.8

Result

ND

X03206 XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

EPA 524.2 rev 4 Purgeable VOCs by GC/MS 75-34-3 I 1, 1 Dichloroethane ND 75-35-4

I 1, 1 Dichloroethene ND --·

! 71-55-6 L 1, 1 , 1 Trichloroethane ND --------·--·

Page 8 of 25 Coyote 2001: Reports

Units Range

mg/L

I ug IL :

! ug IL

i ug IL

1.0.011109162500


Factor

·-i--_J ____

Limit Code Date

M03559-001

~~~:~9_02 _1_~ __ _j 05-01-0~

X03206-012

05-05-03

05-05-0~

05-07-0~

05-07-03

05-07-0~

Report Date 61412003 12:32:41 PM

STANDARD



Client: I

I Explanation of codes

Project:


APRIL 03 SAMPLE EVENT ----· - I

Not applicable due to sample dilution i

Order: 0304502 PHl16 D I

I L Not applicable due to MDL proximity


Run Sequence

X03206 XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

Page 9 of 25



EPA 524.2 rev 4 Purgeable VOCs by GCIMS X03206-012

630-20-6 1,1,1,2Tetrachloroethane I ND ug/~LH~r~=---m___ _ 0.1 - 1_~-=-~ 79_~~----~._!_.~Trichloroethane 1 ND ~-'-'=------ ___ 0.1 __ -I _____ _ 79-34-5 1, 1,2,2 Tetrachloroethane r ND ~ __ LJ_9_1_L _ 0.1 ,

~;;~ c2'.~:;i~~~B) ~~ ~.;nHi=-~,-=~H==-=f1-j

~, 1

:f :]f:f t:~f~i~~;) ~~ - _; ~f H ~ -l ~ ~~ : ~ !l--1= ~ 1~~---1_.2_.~-Trichlorobenzene ____ ND __ +~L--1--- 0.5 :

f g:: , ':i~E~~~~~~~~~~:"· I_· ~~ - ~ ~!: ~ ! ~= ~~-; ~--,~i ; ~ -= 142-28-9 1,3-Dichl~~~~~ne ND--=-=-1.JgT~~~

1__ I ~ -. _ 0.2·1=~

:,~;;;:, ---;~~:,:2~:::~- ~~-- Jt I . ~ --:-i~ 1--~~:;; f ... · -J~~:;~~:~::: -=r-=- ~~ -: :::t- ~-=±-=~ -i=tt 1

- -

-----·---- -·--- ·- -- -f ---- -- ------:---~

1oii:86-1_·--------~rci~ob_:nzene ND ___ L ug IL 1 0.1 ____ +-----

--~romochloromet~ri_e _____ ~ ______ l'JE__ ____ L_..LJ.§ll_'::_______ 0.1 _____ ...

~-5=_~-- ___ Bromodichloromethane ND ug I L ________ ~------ -,----0.1-

75-25-2 Bromoform ND ug I L 1 0.1 ______ _,_ __ _

' ,::;::,;, l-~- :-*-:i ...•. ~;::;' _J-:::- ~ -u~ I . -67 -66-3 I 1 I 0 1 I

74-87-3 -------1·-- ·t-~--, --1 I 156_-5-9~21 · ______ j_ __ _1___ T 0.1- "-- ---~

'1~:;;'1__:~·~::,::::;;;:"• --~~ ____ ~~+~-~ I 1 0.1

_100-41-4 ..... __ . Ethylbenzene J _________ l'JE__ ____ ----~f_l:: __ L 75-71-8 Freon 12 ND ug IL I

87-_6_8~3__ _ Hexachlorobuta~iene ND - ----~i L --i-- ----- 0.1·----i-----j ,- .

98_-82:8 __ L lsopropylbenzene ND ug I L 0.1

75-09-2 I Methylene chloride-· ------r ND ug I L 0.5

~~:~ J ,"::i::::::::. HK • irn ~- •-~ -~=- -~_l_

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03


STANDARL Assaigai Analytical Laboratories, Inc.


Client:

Project:



~ii . Not applicable due to sample diluti°.f)=

L , Not applicable due to MDL proximity Order: 0304502 PHl16


Run Sequence

X03206 XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

X03206 XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

Page 10 of 25

Dilution Detection Run CAS# Analyte Result Units Range Factor Limit Code Date


! 95-47-61 a-Xylene I ND 108-38-

3/106-42 p/m-Xylenes 0.21

X03206-012

_1_---~--~-:; ...... /-----1 L_ .. _

ug IL

ug IL

13_5_-9_8_-8__ sec-Butylbenzene ---------~-~~~=~~------ug_J__~--+-- - ~=r=--, ----~~~ i=~-1

~i~:~:~ __ t-1,2 D~~~~=~oeethene-1· · · ·· . . ~~ _ :: ~ [ :_:_-_ ~ ::. ,~----_- _

1l,- -~ _-___ o~.:-1~---_-_LJI

10~~-1-02~, ____ t-1,3 Dichloropropene _________ ND ug IL __ j___ _ 98-06-6 I tert-Butylbenzene ND ug I L 1-~-;- Tetrachloroethylene -- ----cJ.15 ug I L ' 1 -i ----Q.1- 1 I

-- - ·-·- - -- ___ ______i____ __ J____________j

108-88-3 1 Toluene ND ug IL 1 o 3 ' :

~::~:~ -~ Tric~;~~:~~~:~;:e;~ane ~~ ~~ ~ ~ ---- - 1 1· ~0-:."1~----f' --·-1· -75-01-4 I Vinyl chloride ND ug IL _'_'__'_l


o5-07-o:;

05-07-0:

05-07-0:

05-07-02

05-07-03

05-07-0: ..

05-07-0~

05-07-03

05-07-0:

05-07-03

05-07-03

05-07-0:

1, 1 Dichloroethane ND----~ ug IL ! _____ _l ____ 1 ____ _,l __ o_._1 .. _ __,_I ____ ! 05-07-0~ 1, 1 Dichloroethene ND ____ _[ __ . __ uugg 1

1

LL ···-:

1

• -----+----11

___ L--~1i ____j 05-07-03

75-34-3

75-35-4

71-55-6 1, 1, 1 Trichloroethane ND L 0.1 . i 05-07-0~

630-20-6 ~ ,... 1, 1, 1,2 Tetrachloroethane ND ------~~l~-~~-'_l:_ 1 1 -- ~ :-- -~:_1.::_~i=~==1 05-07-0?

79-00-5 1, 1,2 Trichloroethane ND I ug IL 1 , 0.1 _ --·- __ 05-07-03

79-34-5 1, 1,2,2 Tetrachloroethane I ND -----1-·-~9TL ______ .. ___ 1 ! 0.1 --- 05-07-0~ 563-58-6 1, 1-Dichloropropene I ND ug IL --1--t-! --0-.1---t----f 05-07-0:'

. ---~· ----------------~----------·-------1-----+-----+-------- -·-----1,2 Dibromoethane (EDB) ' ND ug IL 1 0.1 05-07-03 1 ---------··--r------j------j

106-93-4 I

95-50-1 1 _ 1,2 Dichlorobenzene I ND -!--- ug IL 1 0.1 __ 05-07-0~

107-06-2 1,2 Dichloroethane (EDC) ND j ug I L 1 0.1 05-07-0:' -- ·--- --·-- -----------+----+-----+----...j

~~=~~~ I 1,2 Dichloropropane ND , ug IL ______ . ___ 1 0.1 05-07-03

:~::~:: ----Hf--~;;;~;_;~--------------;~-- - t.::.~i~+~--j--=-=-----.--~--~--- ~}--; ____ j ~::~~:~~ 120-82-1 1,2,4-Trichlorobenzene ND _J __ (J_~_.'._I::_ ______ ___j_O~--.:~ 05-07-03

95-63-6 1,2,4-Trimethylbenzene l ____ !..JE_ ____ _j __ .lJ,(J_~l:.- · __ L ' ~:~-- +------ 05-07-0:..

96-12-8 1,2-Dibromo-3-chloropropane ND : ug IL ' 0.2 · 05-07-0~ 541-73-1 1----- 1,3 Dichlorobenzene ND t---ug ,-L 1- 1 --01--+-, ---f 05-07-03

108-67-8 1,3,5-Trimethylbenzene ,-------~ 1----U-ugg 1

1

Ll.--1---=-t-+1

__ ;_.::_--~~~-- _ = 05-07-0:..

142-28-9 1,3-Dichloropropane ND I--~-- 05-07-0~

106-46-7 1,4 Dichlorobenzene ND ug IL 0.1 05-07-03 -----------

1,4-lsopropyltoluene ND ug I L 0.1 05-07-0:.. 99-87-6 ' -------i--- -------~·--

2,2-Dichloropropane ND ug IL 0.2 05-07-0~

95-49-8 2-Chlorotoluene i ND . ug IL 0.1 05-07-03

594-20-7

106-43-4 4-C-h-lo-ro-to-lue_n_e--±--.::_.::_N.::_D.::_ __ -_ .. -_-~-----_-_u_9 .::_1.::_L.::._-~_--_-_-_-_-_-_-_-_-+_-_-~----1----0~·1·-- ·t---1 o5-o7-o::i

-71_-4_3--2-+---- Benzene 1 ND ug IL - !---0."1 ___ j_ ___ ! 05-07-o:

168-86-1--i' Bromobenzene I ND ug IL - ----- - -1 1 , 0.1

7:.::-1 B~:::~~;~~~~:;~~:~;e ~~ j_ :: ; ~ i I _::_1--- _-, ------~-:~-------_.,.+ ____ _, 75-25-2 I Bromoform ___ N_D_____ ! ug IL I -.-. 1---t---0:1 ____ -----7~-8~~= ~t_--_-.::_.::_.::_.::_.::_s.::_r.::_o.::_m.::_o.::_m.::_e.::_t-h_a.::_n.::_e.::_.::..::..::..::..::..::.:.::..::..::..::..::..::.N.::.-D_-_ -_ -_ -_ -_ -_ -f~l===u=g=/=L=-_+_~,_-·_·-----~- ~: 1 D.6·--

05-07-03

05-07-o;,

05-07-0:

05-07-03

05-07-0<>


Client:

Project:


APRIL 03 SAMPLE EVENT Order: 0304502 PHl16

--- - ----------Type: MB: Method Blank

Run Sequence

X03206 XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

X03206 XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

Page 11 of 25

CAS# Analyte



Matrix: WATER

Result Units Range

Coyote 2001: Reports 1.0.011109162500

STANDARD

Explanation of codes

Not applicable due to sample dilution

Not applicable due to MDL proximity !


Factor Limit Code Date

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

Report Date 61412003 12:33:58 PM

STAN DARI Assaigai Analytical Laboratories, Inc.


Client:

Project:



~=_[_lllot applicable _due to sample dilution !

L I, Not applicable due to MDL pr9>!_irT1_ity __ Order: 0304502 PHl16

------ --------Type: MB: Method Blank Matrix: WATER

Run Sequence

X03206

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

Page 12 of 25

!

CAS# Analyte Result Units Range

Dilution

Factor

Detection

Limit

Run

Code Date

EPA 524.2 rev 4 Purgeable VOCs by GC/MS X03206-030 120-82-1

95-63-6 I

96-12-8 I

541-::73-11

108-67-8

142-28-9

06-46-7

9-87-6 9

5

9

10

7

10

94-20-7

7

7

5-49-8

6-43-4

1-43-2

8-86-1

5-27-4

5-25-2

- -74 83 9

I

I

56-23-5 I -~--+

108-90-7 I

124-48-1

75-00-3

67-66-3

74-87-3

05-07-03

~ __ :_;~~~~~:~--·_···_-------__:T -- 1-:: _ r~u~ ::::;~: ug IL _ _ L___2_ _ _ __O_l ____ f ____ _, 05-07-0~ ug IL ____ ___J__ 1 ___l_~~--- i 05-07-0::.

---r -~-:-- -~~'I - ---~1~- =-+ __ ~0:.211_ -- . ~::~;:~~ r i 05-07-0:J

___ j_ ___ -1~~--~T- I I 05-07-o:

_ ------+-- 1 - _ I __ o._2_ - - ---- 05-07-03

I 1 B· 1 05-07-03 ____ ______l___ ~ -~ ---- - ------

1 0.1 05-07-0'. - . ---- - --

1 -+ 0.1 05-07-03

--+-+0:_~1---- I~-- ~::~;:~~ 05-07-03

I 1 - - t---0-. -1 ---+----- 05-07-03

Bromomethane ND ug IL --1 0.6 05-07-o:

Carbon tetrachloride ND ug I L I -,--0-.1----'-----

Chlo""''"""e ND ' ,,1 L +------ -l 0.1 ' - I OS-Orn

1,2,4-Trichlorobenzene

I

ND

1,2,4-Trimethylbenzene ND I

1,2-Dibromo-3-chloropropane ND

1,3 Dichlorobenzene ND

1,3,5-Trimethylbenzene ND

1,3-Dichloropropane ND

1,4 Dichlorobenzene ND ug IL I

- -1,4-lsopropyltoluene ND ug IL

·---- -----2,2-Dichloropropane ND ug IL

-- ·--2-Chlorotoluene ND I ug IL

4-Chlorotoluene ND ug IL Benzene ND ug IL I

I -- --

Bromobenzene ND ug IL ---

Bromochloromethane ND ug IL I

Bromodichloromethane ND I ug IL -Bromoform ND ug IL

--~

c-h1-,0-:-~-~-:~-:-~-·~-~-~·-:.-h-an_e __ --+--t------~-i~ ---=i~t;i ];li~tJ ~rn~: 1~~:~~~~~5 . c~~~~

1

,; d~~ch~:~0

p~~;::e ~~ ~:; ~ --= -+ -+--+--{~---)~-=:] ~::~;:~: -- 74-95=3-.---Dibromomethane ND ug IL I

- ~~~~~:- T° Etir~b0enn~~ne ~~ ~:; ~ -----+-1--87-68-3 Hexachlorobutadiene ND ug IL i 0 1

-~::~::: :;~~~:~~b:~~~~: -r----~-~-----·· -"--- ~:; ~ - ~-- --- --! • ~~- - ----~-:~--+------< -9-1--2-0--3-+----- N hth I ---+----N-D ___ ---i /L --1--1-- ·i--1-----

J;Et~ 1 ~-"":I~!~f }::. ~~ --i ~ulg :,~L- i~--·--·-.-= 1_

1

~=:1==_-~o;_-~2t~ ~ - 1 a·S.:-38-"-T p/m-Xylenes ND _ ~ 3/106-42

0.1 0.1

---------'------0.1

---sec-Butylbenzene ND ug IL !

----Styrene ND ug IL

t-1,2 Dichloroethene ND ug IL -- -- --

t-1,3 Dichloropropene ND I

ug IL tert-Butylbenzene I ND ug IL

---

05-07-0~

05-07-0?

05-07-03

05-07-0~

05-07-0?

05-07-03

05-07-0~

05-07-0?

05-07-03

05-07-0~

05-07-0:'

05-07-0~

05-07-03

05-07-o;.

05-07-0~

05-07-03

05-07-0~

05-07-0:


STANDARD



Client:

Project:



Order: 0304502 PHl16

- ----- -- ·- ·-


Run Sequence

X03206 XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

M03548 MT.2003.521.10

MT.2003.511.34

MT.2003.511.34

MT.2003.521.10

M03550 MT.2003.551.11

MT.2003.551.11

MT.2003.551.11

MT.2003.551.11

MT.2003.551.11

MT.2003.551.11

MT.2003.551.11

MT.2003.551.11

MT.2003.551.11

MT.2003.551.11

MT.2003.551.11

MT.2003.551.11

X03194 XG.2003.785.12

XG.2003. 785.12

XG.2003.785.12

XG.2003.785.12

XG.2003.785.12

XG.2003.785.12

XG.2003.785.12

XG.2003.785.12

XG.2003. 785.12

XG.2003. 785.12

XG.2003. 785.12

XG.2003. 785.12

XG.2003.785.12

XG.2003.785.12

XG.2003.785.12

XG.2003.785.12

XG.2003.785.12

XG.2003.785.12

XG.2003.785.12

XG.2003. 785.12

Page 13 of 25

Dilution

Factor

Detection Run

CAS# Analyte Result Units Range Limit Code Date


I ~~~If-------~ric~~~~;~~~:~;:ee~~ane --------}-~-:__---~---~f--------~-~-~-~----~-------. -_f. -·~~-~-]1 __ •---.-. -.J•_--_-__ -_-_~o-__ : __ -~1 _____ -____ F_, - ~-i 75~0~~- __ Vinyl chloride _ ND __ ug_l_l:_____ __j

SW846 3005A/6010A ICP M03548-001

~~~--~:-i-:~-~~1- -~~~~----~±-_-_-_ ~-~-' -~~----1_ ~-!~_~L' i off ff~= SW846 3005A6020 ICP-MS M03550-001

!~~0-36-0 J~ .--· Antimony ND mg/L --T 0.001 ! - - __ ' ________ ------j --- --- ---·~

;_·-~-~:_f_~_-___ c_:_:_:~m -• ---------~--~------:-:-;-~--t---------------j-----1 ---------+-·----:-::=:=i==~r-_-_=-_-=J 7439-92-1 ~ __ ____ Lead ND mg'-~--- _ -~~()()L _j _____ j 7440-02-ill --- - Nickel ND mg I L 1

1

0.001 i I

77~2:~-2 J_ Selenium r---- -- NNDD I --mm_-.~g--~,~LL~-- '__ ------~- - -~1 -1

Oo._009011 -~~~--···----~, 7440-22-4 _l_ ____ Silve_r:_ _ _ _____ --+--------------r--------------~------- ___ ------~--~ 7~4_0_-2_8-_0 _____ _____ Thallium ! ND . mg I L --~----- __ _ 1 0.001 ____ :

~~-m + ~n 1 i_~ H!:] 1 7440-31-5

7440-62-2

7440-66-6

Tin

Vanadium

Zinc

SW846 3510Bl8081A Pesticides by GCIECD X03194-001

05-07-03

05-07-03

05-07-03

05-01-03

04-30-03

04-30-03

05-01-03

05-05-03

05-05-03

05-05-03

05-05-03

05-05-03

05-05-03

05-05-03

05-05-03

05-05-03

05-05-03

05-05-03

05-05-03

____ -------t~--= a-~~:~d~ne ------------~t----~--~-------~~-~ -~-~---~1

1---_4 ~: ~---~--1 ~::~::~: 309-00-2 I Aldrin ND i ug I L O 1 J 05-08-03

b-BHC ND I ug IL -1---~-, 05-08-03

~7~74-9 r_-_·----· -c-h-,o-~d--~-~-ec-. -to-ta-,----+---~--~-----~---~--~---_-_______ +-L---~g-g-~ -~- --~~:-~= ~ __ . _ ~: ~ __ -I ---, ~::~::~:

60:5?-T ' - Dieldrin ! ND i ug/ L -==~1-==Li ---~ 1 05-08-03 ---------- --Endosulfan I - - -1-----NO--____ ! ug I L 0.1 05-08-03

--- -----------+--------------- --- ---------- ----

Endosulfan II ND ug I L 0.1 05-08-03

-----,-- -""'°'""'" S"lfato ~~ OQ IL . _____ ~ -- 1 -_ 0.-1 :__- "-°'~'

~22~ 1------E~-~~~:-:_'.:_:-~-~-:-~d_: e--__ _____, ________ ~~ ~! '.~ --~ -_ ---·~ -.. I{~ -- lrn~~ 7~ _gH--~-:-:0-a~-~-~o_n~----+----~-~----+-- :H ~ --- -- -f-- ~ t *1- I ::::::::

1024-57-3 -·-

6088-51-3

50-29-3

Heptachlor Epoxide ND 1 ug IL , - i -- :-----o-:1-- : -·-----i 05-08-03

ND --- ~-_r ____ ULJ_Q_g __ 'l __ LL __ ---+_ ~ ------~-- -------0.1---+-;----; 05-08-03 p,p-DDD

p,p-DDE

p,p-DDT

ND L ------0.-1 ___ I -----i 05-08-03

----+----N--D-- ug/L 0.1 t~=-J 05-08-03


STAN DARI Assaigai Analytical Laboratories, Inc.


Client:

Project:


APRIL 03 SAMPLE EVENT Explanation of codes ------- ---------------

0 ! Not applicable due to sample dilution Order: 0304502 PHl16

1 i:.-t Not applicable due to MDL proximity


Dilution Detection Run Run Sequence CAS# Analyte Result Units Range Factor Limit Code Date

X03194 SW846 35108/8081A Pesticides by GC/ECD X03194-001

XG.2003.785.12 I 8001-35-2 T-- Toxaphene, total __L__ __N_D __ --_-_--'_1 ___ ug IL [ ___ u ___ --_l-___ 1 ~=2~5 ~· ____ J 05-08-0'.:>

X03194 XG.2003.785.25

XG.2003. 785.25

XG.2003. 785.25

XG.2003. 785.25

XG.2003.785.25

XG.2003.785.25

XG.2003.785.25

XG.2003. 785.25

XG.2003.785.25

XG.2003.785.25

XG.2003.785.25

XG.2003.785.25

XG.2003.785.25

XG.2003.785.25

XG.2003. 785.25

XG.2003. 785.25

XG.2003. 785.25

XG.2003. 785.25

XG.2003.785.25

XG.2003.785.25

XG.2003.785.25

XG.2003.785.25

X03189 XG.2003.750.3

XG.2003.750.3

XG.2003.750.3

XG.2003. 750.3

XG.2003.750.3

XG.2003. 750.3

XG.2003.750.3

X03189 XG.2003. 750.18

XG.2003. 750.18

XG.2003.750.18

XG.2003.750.18

XG.2003.750.18

XG.2003.750.18

XG.2003.750.18

X03189 XG.2003.798.4

Page 14 of 25

SW846 35108/8081A Pesticides by GC/ECD ---------1 a~HC ND --- ·------------~~--

a-Chlordane ND 309-00-2 ------------------~----=r Aldrin ND

b-BHC ' ND

ND Chlordane total

r~. - - ----

=-~ d-BHC --~ ----· ND

60-57-1 Dieldrin ND ---- --~-

Endosulfan I ND

1 Endosulfan II ND

I Endosulfan Sulfate ND 72-20-8 ! Endrin ND

ug IL _________ ,_ ______ _

ug IL ---t---- --

: ug IL

X03194-014 0.1 , I o5-o9-o: ------------- +- --1 0. 1 05-09-03

- -1 -------+---0 .1 I 05-09-o~

--- ---r---------0. 1 05-09-0:

0. 1 05-09-03 l--~~-~-~--~=--==-- ------

I ug IL 0.1 -------·-

i ug IL --

I ug IL --- ----· ---

----±_ ~~ ~-~- I

! :

I ug IL ---1·-

---+----- - -------------

1 0.1 --------+-----'

1 0.1 -- --------+-----'

1 0.1 -- -- -------+----

1 -~ 0.1

---- t m----~-~~~nA~:~:~:e-------1--- ---~~~ ~:; ~ _____ 1 __ 1 __ O~ 1

58-89-9 _[ -------~-----L ______ ~D ' ug/L _ _ ~~ _) ____ _1_ ~}=-___ _ 76-44-8 g~~::~~~~~~ ~~ - ----uu~gg '--,' L~ ~=j1-~- -'.: _Jo~. ~1 _ ____)__

1024-57-3 Heptachlor Epoxide ND r-----t

'--:--~~-~-~=;=::=--+---_~JJ~~~(., ---=-~~-----+--~-l-~--~--=--------i--_-----.::-_-~.---!t-:---.->-l ~~ TJ

05-09-03

05-09-0:

05-09-03

05-09-03

05-09-0:

05-09-03

05-09-03

05-09-0:

05-09-02

05-09-03

05-09-0:

05-09-02

05-09-03

05-09-0:

05-09-02

05-09-03

05-09-0~

SW846 35108/8082 PC8s by GC/ECD X03189-001

12~74-1~2~------Aroci0r101_6_-:==[=~~~-------=----_lJ_g_!__1:_ __ _

11104-28-2, Aroclor1221 J ND _____ u_gl_L I 0. 5 05-06-0?

~--------

0. 5 05-06-03

11141-16-5 1 Aroclor 1232 I ND ___ _l_l9_1 ~--53469-21-9 · Aroclor 1242 ' ND ug IL

1 ----------

1

0. 5 05-06-0~

0. 5 05-06-0? ---------;-------

12672-29-6 ' Aroclor 1248 ND ug IL ------' -----------r------------i-----

11097-69-1 ; Aroclor 1254 ND ________ __l_l~_~ __ __'. ____ _

110~~~2-5 [_____ A_ro_c_lo_r_1_2_6_0 ____ ~_ ~-~------~-ug_I _L_~----~--

05-06-03

05-06-0~

05-06-0?

SW846 35108/8082 PC8s by GC/ECD X03189-014 : 12674-11-2 I Aroclor 1016 ND ug IL .. l 0.5 05-07-03 • 1i104-28~2 1--- -- ------- ~---- .... --·~-·--- -

Aroclor 1221 ND ug IL 0.5 05-07-0::. , - -·----- -L -r _ ~g'-~-

---------

11141-16-5 I Aroclor 1232 ND 0.5 - 05-07-0:' I

-------=!~~--i 53469-21-9 I Aroclor 1242 ND ug IL 0.5 05-07-03

: 12672-29-6 I Aroclor 1248 ND ug IL I 0.5 05-07-0::. -!-

: 11097 -69-1 Aroclor 1254 ND ug IL 0.5 05-07-0:' I 111096-82-5 I Aroclor 1260 ND ug IL 0.5 05-07-03

SW846 35108/8082 PC8s by GC/ECD X03189-027

I 12~7~-~:-~l ______ ~_ro_c_lo_r _10_1_6 ____ ~1 ____ N_D ___ ~_u_g_l_L_~ -- ---~-1-_T o.5 1 05-15-o::.


STANDARD



Client:

Project:

Order:

Type:



0304502 PHl16

MB: Method Blank

Run Sequence CAS# Analyte

SW846 3510818082 PCBs by GCIECD

Result

Matrix: WATER

Units Range

Explanation of codes -- ----------- -·- -----------

D Not applicable due to sample dilution ' -· - ------------

L Not applicable due to MDL proximity

Dilution

Factor

Detection

Limit

Run

Code Date

X03189-027 X03189 XG.2003.798.4

XG.2003.798.4

XG.2003.798.4

XG.2003. 798.4

XG.2003.798.4

XG.2003.798.4

11104-28-2 ! Aroclor 1221 -------------+------ -- -------

~------L. ~91t:~--r--~-- o.5 05-15-03

05-15-03

05-15-03

05-15-03

05-15-03

05-15-03

X03165 XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

Page 15 of 25

ND ug/L .. _L___ ___ ~ t· __ o __ .5 __ ~-·--··--·-11141-16-5 I Aroclor 1232

~~~--~-::--~-::-:+-.--------···-~-~~~::~ ~ ~~~-·- ----~~ ~.o.97. ~69.~I---_-_-_A_r_oc_l_or_12_5_4 ____ :=======N_D_

[ 11096-~~5_[ ____ Aroclor 1260 ND


. ug IL 0.5 -r-----ugJL - ---;--1- o.5··-·--·------I

-= :: J= I =- -I =-I:_~ ~ :--_--_·--+---.....

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10•03

04-10-03

04-10-03

1.0.011109162500 Report Date 61412003 12:36:23 PM

STANDARC



Client:

Project:


APRIL 03 SAMPLE EVENT Explanation of codes -- .. -·-·------- ---

D Not applicable due to sample dilution Order: 0304502 PHl16 L Not applicable due to MDL proximity


Run Sequence

X03165 XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

X03165 XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

Page 16 of 25

------ -------------


Dilution

Factor

Detection

Limit

Run

Code Date

SW846 35108/82708 SVOCs by GC/MS X03165-001

_1_91_-_24_-2 ____ B_e_nzo(g,h,i)perylene ND L---~~--L _ ! 1 _J 1 ~ Benzo(b & k)fluoranthene ND ug I L 1--- ---,-1- [- i -t

64-85-0 Benzoic acid ND I ug I L I 1 ~ __ ~5 _ _ _

100-51-6 Benzyl alcohol ND ug IL 1 =t 5

111-44-4 L___ bis (2-Chloroethyl) ether ND ug I L : --+---1- __ 11 ----+--_,

111-91-1 ' bis(2-Chloroethoxy)methane ND ug IL j 1 108-60-1 bis(2-Chloroisopropyl)ether i ND ug IL -- ..... - ·-··· 1.. - t --1- - I 117-81-7 I bis(2-Ethylhexyl)phthalate -,-----ND ug IL ~--- --- - --1- -~ 5

85-68-7 I Butylbenzylphthalate I ND ug I L 1 _+_1_ __ _,_ __ _, 218-01-9

53-70-3

. 132-64-9 1---. 8.~:~6-2 _J ..... 131-11-3 I

84-74-2 !

117-84-0 I

206-44-0

86737

Chrysene ND ug I L 1 ; 1 1

Dibenz(a,h)anthracene ND ug I L 1 -· T.===f-=-=:~[ Dibenzofuran ND ' ug I L 1 1 1 !

Diethylphthalate ND ug I L 1- . t' Dimethylphthalate ~-- ND I ug IL i-=1===· · r:_-_ _1_ __ ----~

::~~:~~:~:~~:~::::: ---- ---·----~-~----.... -' _u_g_~+- ~-------1--~--lj ----+- ·i-·---;

Fluorene ND :-ug 7L - .1- - ... . , 1 .... :--T Fluoranthene -•-·--- ND -- ·- - i- ~~TL.·-. - ---~ -, I - - 1 1---1

.. ------------·--------·-·-·----·--- ..... --+-· ..... . -· J_ _____ - .. >-••-i------ .......... i ....... - - -1 --

:· -~~:8~~1 __ ( ____ _;e:xaacch~~~~o:u~:~~ennee ·t·---·--- -·~~------:J==-~~~}-=-~=---~~-.. 1-=i==~-=+~~- -+ .. j I :~~:~ I Hexa~:~:~~ra~~:t~:~:iene ~~ .. -------:~~--~-- --~-=n ~'-- ;---

_193-39-5 lndeno(1,2,3-cd)pyrene ND ug I L 1 1

.-1... .. ___ J

78-59-1 lsophorone ND ug I L 1 I 1 I I 91-20-3 Naphthalene ND ug IL - - -- -i---f±=i=j ::::::: ,_N,,::::::~~1°eml"e ~~ j_:::~+-- I ~ -r-+o-=--1---1 621-64-7 n-Nitroso-di-n-propylamine -N~-D~-------+ uugg 1

1

LL : _[ ___ 11__

1

1 1

1

,

1 86-30-6 1 n-Nitrosodiphenylamine

_j_ ---~---j

87-86-5 ' Pentachlorophenol ND r-----ug IL. 10

85-01-8 I Phenanthrene ND ug I L 1 --+. --~ 108~95-2 r·------Phenoi____ ND ug IL 1 1 10 •

. '.. --1- . ----1 - ·t-.. --1 -""--1·-j -10---- ---== 129-00-0

110-86-1

1· 120-82-1

! 95-50-1

541-73-1

106-46-7

90-12-0

58-90-2

95-95-4

88-06-2

Pyrene

Pyridine

SW846 35108/82708 SVOCs by GC/MS

1,2,4-Trichlorobenzene I

1,2-Dichlorobenzene

1,3-Dichlorobenzene

ND ug IL

ND ug IL

X03165-008

~~-----~-~-;-~-l=:-=---1 f-l_~ __ l ____ j 1,4-Dichlorobenzene

ND -+---ug_(L . ··t'---- ---f 1 1 ---~-~ +- ___ _t-l_c:J_______ ug IL _ _____ I .. _1 _____ ,

~~ ----~~~-I ------- I ~ +'·---5·---·-"--------r--- - ------- ------- ··-- - --- ------ ____ __, __ _,

ug IL 1 5

1-Methylnaphthalene i

2,3,4,6-Tetrachlorophenol . t 2,4,5-Trichlorophenol __ -+! ____ N_D __

2,4,6-Trichlorophenol ND ' 5 ---~---- ---~-----

_L ug IL ---------·-'-----·--·--- ..J

04-10-0~

04-10-02

04-10-03

04-10-0~

04-10-0:>

04-10-03

04-10-0::.

04-10-0:'

04-10-03

04-10-0::,.

04-10-0~

04-10-03

04-10-0s

04-10-0:

04-10-03

04-10-0J

04-10-0:

04-10-03 .

04.10-o:r

04-10-0:

04-10-03

04-10-o:r

04-10-0:

04-10-03

04-10-03

04-10-0:

04-10-0~

04-10-03

04-10-0:

04-10-02

04-10-03

04-10-0:

04-10-03

04-10-03

04-22-0~

04-22-0?

04-22-03

04-22-0~

04-22-0?

04-22-03

04-22-0~

04-22-0?


STANDARD



Client:

Project:



1

D. --1- Not applicable due to sampl'!_C!i_'!'_!i~n ~-Order: 0304502 PHl16 L Not applicable due to MDL proximity :

-- ----------------------·---·- ------

Type: MB: Method Blank Matrix: WATER.

Run Sequence

X03165 XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

Page 17 of 25


Dilution

Factor

Detection

Limit

Run

Code Date


120-83-2 · 1 2,4-Dichlorophenol

-1-~5-6!_~9r-----2~4=oimethylphe_~?!

X03165-008 ·-

ND ug IL 5

51-28-5 I 2,4-Dinitrophenol 1

--.·-·-!---.. --------·-- ------f---

ND ug IL , ND ugfl .. -f-------· - i -- fr>

121-14-2 i 2,4-Dinitrotoluene ----~06-20-2 _ L_ . 2,6-Dinitrotoluene

2-Chloronaphthalene

2-Chlorophenol

ND ug IL : 5 -+-----------1 +-----ND 1 _ _ __j __ 5 __ _

91-58-7 . ND I ug IL 1 1 95-57-8

-:

-----·-----· ND -r_-_ -ug_/_L_____ 1 1

-~_:::_~~ t----_ 2-~~::~~;~~~;~~ne -----~~ l ___ -~+~-- -_:=::::-~~J_'; ~:~ _ ~ - - ---j~~-;:-~--- 1: ~~~::;~:~~~:I ----+-------_~N_~D_,,_,,,,,, . I._-.. ~u~g-~/-~L·----- ' 10

91-94-1 3,3-Dichlorobenzidine - ---~·---------------+---- ---+------------~- -------

3+4 Methylphenol ND ! ug I L

99-09-2 --------t-

534-52-1

____ .J

~i- b

Benzo(g, h, i)perylene i ND ug IL -----

Benzoic acid I

ND ug IL - ---- ·----- -

Benzyl alcohol ND ug IL

is (2-Chloroethyl) ether ND ug IL

111-91-1 i (2-Chloroethoxy)methane ND ug IL

(2-Chloroisopropyl)ether ND -ug/l"----r-------- --------- ...

bis ---------~-----r-

1 !

ug I L · 1 5 -+,---: 108-60-1 bis

117-81-7 bis(2-Ethylhexyl)phthalate ND ·-

-

218-01-9 I Chryse_n_e ____ _,_ __ _:i~~- --- --t J------1-----i ND

I

ND

85-68-7 Butylbenzylphthalate ----+-----

53:?0-3T Dibenz(a,h)anthracene

132-64-9 -·-·-·---... !· ... 84-66-2 I

Dibenzofuran

Diethylphthalate

. --- 1 · --r 1 t-----~

-f==- ~~-~-~ -+---::~ --~ J __ -~1····· -1--:::::~ --+--------- ug l_L _ f- __ ·- __ ----~--- -~-- ---~-----j

I ND r-----ND

ND I

04-22-03

04-22-03

04-22-03

04-22-03

04-22-03

04-22-03

04-22-03

04-22-03

04-22-03

04-22-03

04-22-03

04-22-03

04-22-03

04-22-03

04-22-03

04-22-03

04-22-03

04-22-03

04-22-03

04-22-03

04-22-03

04-22-03

04-22-03

04-22-03

04-22-03

04-22-03

04-22-03

04-22-03

04-22-03

04-22-03

04-22-03

04-22-03

04-22-03

04-22-03

04-22-03

04-22-03

04-22-03

04-22-03

04-22-03

04-22-03

04-22-03

131-11-3 Dimethylphthalate

di-n-Butylphthalate

ND i- ug IL ' 1 1 ug IL

I· .. -- .. -"" j I 04-22-03

----------------r-ND I ug IL __ J --:-1J 04-22-03

----~--

84-74-2 _____ _L_




Client:

Project:



-·--------·--·----------

D [ 'iC!t applicable due to sample dilution Order: 0304502 PHl16 L 1

1 _Not applic;ab~_cJ:ie to MDL proximity

Type: MB: Method Blank Matrix: WATER ----------- -------------

Run Sequence

X03165 XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

X03165 XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

Page 18 of 25

Dilution

Factor

Detection Run


X03165-008 SW846 35108182708 SVOCs by GCIMS

1117-84-0- r··- di-n-Octylphthalate

__ 206~~~~~-1- Fluoranthene

ND L ug I L __ - -~f---~1 l--,· ___ _2___1

__ r_ ', 04-22-03 ND ug I L 04-22-0:

~~-----f- "';~ ;H -=+--- ~ mt;,-t ~ :::::: 86737 Fluorene

t-- -+--10---+---- 04-22-0: _'.______________ -. - -1--

118 74 1 H hi b - - exac oro enzene '1 ug

i ------!-- ·-· ··--- ---

87-68-3 Hexachlorobutadiene '

ND I

ug IL 1 -- -- --·--

77-47-4 Hexachlorocyclopentadiene ND ! ug IL 1 , 10 04-22-03 ---r---5 -- 04-22-03 ---= :~-- 1~1···· : 04-22-0~ ..

-- --- .

67-72-1 Hexachloroethane ND ug IL 1 1---- ---

_____ )__ ·-·------~ 193-39-5 lndeno(1,2,3-cd)pyrene ND ug IL 1

··- ·-~-

- 04-22-03 I 78-59-1 lsophorone ND ug IL 1 ----91-20-3 Naphthalene ND ug IL 1 ·-

' 9~:~:~ __ .J_ ___ ' Nitrobenzene ND ug IL 1 ----

6;~;,+~:t .. n-Nitroso-dimethyl-amine ND ug IL 1

------n-Nitroso-di-n-propylamine ND I ug IL 1

·-· -·· -- --· --- .. ·--·-----n-Nitrosodiphenylamine ND ug IL 1

! -------------- --------·· ·---·

10

1 --~-- .. -- ---------t----~

--~---+------~ 10 I I

-------+--_1 --l- ---10 I

87-86-5 1 Pentachlorophenol I ND -85-~----P-he_n_a_n-th-r-en_e ______ + ND

108-95-2 Phenol --i-- - ND

ug IL

- - -'--~-~_L-___I _____ _ 1 ug IL 1

--------------------------·- . i---------· --------1~~-oo_-o_~ _______ P_yr_e_n_e _________ N_D ___ _,r __ ~g_/~ __ .L -----------+------1 __ 110-86-1 Pyridine _________ N_D ___ ~[ __ u_g_l_L_~I _ 10

SW846 35108/82708 SVOCs by GC/MS X03165-011

04-22-03'

04-22-0(

04-22-0~

04-22-03

04-22-0',

04-22-0?

04-22-0:l

04-22-0~

04-22-0?

04-22-03

1,2,4-Trichlorobenzene ND ug IL j ·1--, 1 04-26-0~ ----------l---------------+---------~--------+------+---- --4-------+---< 120-82-1

95-50-1 1,2-Dichlorobenzene ND ug I L j 04-26-0~ .----+----------------t-·--,.---------+-------t----·-·----~--- -------------j----< 541-73-1 1,3-Dichlorobenzene ND ug IL 1 ' 04-26-03 -----------------+----------------~-------+-' -- ·--

_10_6_-4_6_-7 _____ 1_._4-_D_ic_h_lo_r_o_be_n_z_e_n_e __ ~l ____ N_D ------+---u_g_l _L_~--- __ _ L-----t- _ _______ 04-26-0~ 9~-_1_2_-o __________ 1_-M_e_t_h_yl_n_ap_h_t_ha_l_en_e __ -+-i ----~-~------ __ _1:19LL _ __; ____ +_ _ +------+---__, ~:::::~: 58-90-2 2 3 4 6-Tetrachloropheno

1

ug IL_ __ _ __ ______ _ __ _ _ ______ 5 __ ~ __ __,

__ -_9_5-_-9_5_-4_+-! ____________ 2_._4_,5_-T_r_ic_h_lo_r_op_h_e_n_o_l __ ~ _____ N_D _________ ~I' __ u_g_l_L_-+--------- _____ 1_~-~-- ---+~ 04-26-0~ 88-06-2 i 2,4,6-Trichlorophenol 1· ND ; __ _:i_g_I__!. -+------+---1- _L __ 5 __ +--_----1' 04-26-07 120-83-2 1 2,4-Dichlorophenol ND ug IL 1 5 , 04-26-03

-_-1~0_5-_--6_7-_--9~_:-~~~~~-2-_.4-_--D~i_m ___ e_t-h~y~lp~h~e_n-_o-_l--__-_-_--__--++-------------=--------N~-D~-=~-~~~~~.~~-u-g~_l-_L _____ -++_-_-_-_-=_--_-- -~· ------=~-1-_-_-_--+-.,...----=----- =J 04-26-0~ 51-28-5 2,4-Dinitrophenol ND ug I L 1 1 O 04-26-0~

------- - -----------------+---------;------·-+-·-------_,_---- ---+----121-14-2 2,4-Dinitrotoluene ND ug IL 1 1 5 04-26-03 ------- -----·----------+----------+-------t--·-~------+------ ----+----+ 606-20-2 2,6-Dinitrotoluene ND ug I L 1 5 04-26-o:, 91-58-7 1 2-Chloronaphthalene ND ug /-L·---+-\ ------,r-----1 -- +------c-----1 04-26-0~

---~~--~--i- I

:~~1r- -~~~;;:;;;~:~"' , _ ~~ _j~ t-·--------.L=~ . ____ ,_, __ : ::::::~ 88-74-4 1 2-Nitroaniline I __ N_D___ ug IL i 5 ' ' 04-26-03

88-75-5 2-Nitropheno1 ND , ___ -_-_u_9_-C~-___j_i_~= 1 5 I --~ 04.25.0:,

- 1 - I 1_0 _-1j-- ~ 91-94-1 1 3,3-Dichlorobenzidine ND ___ _ tJ_Q_I _!:: H __ L_ _ _ _ _ 04-26-0:

I 3+4 Methylphenol i ND ug I L 1 1 1 ____j 04-26-03

99-09-2 I 3-Nitroaniline -1---- - ND ug I L ___ -±~-_-_-_____ -11 __ - ~- l__-

150--=; __ _j_j' 04-26-03

534~52-1-=:[-_~:4.6-Dinitro-2-methylphenol I ND ug I ~-_J J__ 04-26-o:


Client:

Project:

Order:

Type:



0304502 PHl16

MB: Method Blank



Matrix: WATER

D

L

STANDARD


Not applicable due to sample dilution


Run Sequence CAS# Analyte Result Units Range Factor Limit Code Date

X03165 XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

Page 19 of 25

SW846 35108182708 SVOCs by GC/MS X03165-011 161:55=3- - 4-Bromophenyl-phenylether '.----- -ND -['- U9-IC---,-- --- - -- 04-26-03

04-26-03

04-26-03

04-26-03

04-26-03

04-26-03

04-26-03

04-26-03

04-26-03

04-26-03

04-26-03

·------------------- --i--------

59-50-7 4-Chloro-3-methylphenol ND , ug I L

! 106-47-8

7005-72-3

100-01-6

100-02-7

83-32-9

208-96-8

62-53-3

--------··-·1

621-64-7 ! ______ ...J .. 86-30-6 '

------

87-86-5

---------

4-Chloroaniline ND ug IL ---------- --------------- ---------:--------~--

4-Chlorophenyl-phenylether ND ug I L

4 N"t T ND IL - 1 roam ine I ug _]_ ______ - -- -

4-Nitrophenol ND ug IL --·- ------

; ug IL Acenaphthene ND 1------- ·-- ·--------

Acenaphthylene ND ug IL ·--------

Aniline ND I ug IL

Anthracene ND I _ ug IL _____ ---- ·----·

Azobenzene&1,2- ND I

ug IL Diphenylhydrazine

-· ----- --· ~ - ---- -Fluorene ND ug IL

---exachlorobenzene ND ug IL

exachlorobutadiene ND I ug IL

chlorocyclopentadiene ND ug IL --------- ----

Hexachloroethane ND ug IL I ------·---- ------------- ------

deno(1,2,3-cd)pyrene i ND ug IL I ! ---------- - - --------

lsophorone I ND ~_u_g!_~ --·--- - --Naphthalene ND ug IL

Coyote 2001: Reporls 1.0.011109162500

5

5

5

10 ---+-------------i----j

1 --------------

1 ---+--- ------------J---j

10 -----+-----+-----j

04-26-03

04-26-03

04-26-03

04-26-03

04-26-03

04-26-03

04-26-03

04-26-03

04-26-03

04-26-03

04-26-03

04-26-03

04-26-03

04-26-03

04-26-03

04-26-03

04-26-03

04-26-03

04-26-03

04-26-03

04-26-03

04-26-03

04-26-03

04-26-03

04-26-03

04-26-03

04-26-03

04-26-03

04-26-03

04-26-03

04-26-03

04-26-03

Reporl Date 61412003 12:38:49 PM

STANDARD



Client:

Project:




DT-f.Jot applicable due to sample dilution

Order: 0304502 PHl16 I -Lr_-Not applicable due to MDL proximity I


Run Sequence

X03165 XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

X03165 XG.2003. 703.11

XG.2003.703.11

XG.2003.703.11

XG.2003. 703.11

XG.2003.703.11

XG.2003.703.11

XG.2003.703.11

XG.2003.703.11

XG.2003. 703.11

XG.2003. 703.11

XG.2003.703.11

XG.2003.703.11

XG.2003.703.11

XG.2003.703.11

XG.2003.703.11

XG.2003.703.11

XG.2003.703.11

XG.2003. 703.11

XG.2003.703.11

XG.2003.703.11

XG.2003. 703.11

XG.2003.703.11

XG.2003.703.11

XG.2003. 703.11

XG.2003.703.11

XG.2003. 703.11

XG.2003.703.11

XG.2003.703.11

XG.2003. 703.11

XG.2003.703.11

XG.2003.703.11

XG.2003.703.11

XG.2003.703.11

XG.2003.703.11

XG.2003.703.11

XG.2003.703.11

XG.2003.703.11

XG.2003. 703.11

Page 20 of 25

---- ______ .. ____________ . ______ __



SW846 35108/82708 SVOCs by GC/MS X03165-013

~25~r 1:~~~~~~~~~:~::~:e ---_ ~~ - - I - ~-~;~-~1-- - -r_--= ~ --~~ -- ~ . R 541-73-1 1,3-Dichlorobenzene ND =t ug IL 1 ----+- 1

\_ ·106-46-7_+-· . 1,4-Dichlorobenzene Ni:>"-- ug IL f-------t-· -1 _ _J ____ 1 _

1-::::~ ,,;,~~·~::::;::::::::., H ~~ - :: :: : ~ • - • - ~ u i ; I 95-95-4 I 2,4,5-Trichlorophenol ND ug IL --+ 1 5 --+

7:~:~: i .· 'f :~f :~:~~:~~:, 1

- ~~- · _JI :n t-~ -1

: -r :-= 1

- -

-51-28-5---1-- 2,4-Dinitrophenol ND___ -ui/L_f ___ - ---1 -=i- 10 - -

121-14~ 2,4-Dinitrotoluene ND _____ lug_/_L_~----- - -- 1- ----5--·-,

'12~1- ::~~Iif~~~~~::_;Jr ~~; ~m-:- -¥-i~HL-=lt 1 _88~74-4 1--··· 2-Nitroaniline .. ND =j_~L_ I _ ___)____ _ 1 ~ _____ 5_ i_ __ j 88-75-5 2-Nitrophenol --+-----Nl:) ____ ; ___ ~L-+= ---f- __ 1__±' _______ 5_ +---~ 91-9~:1_1 _ 3,~~~~~J~---L------~~----t ~~ ;+~-- ___ J_ +---- 1 ----~:--~ 99-o9=2T -----3-Nitroaniline ---'·----ND___ ' ----u-Q1'L-tt-- 1

-- 5--:-1 534-52-1 p,6-Dinitro-2-methylphenol ±=-- _f'JD - _' - -u~IL -- _ __! __ J_~ 1_()__~---1~ 101-55.:_~---4~Bromophenyl-phenylether _ ~- _ ~~~_l_L-_-+ 1 ti .. ___ 1 ___ ~ 59-50-7 , 4-Chloro-3-methylphenol ___ N_D __ --t-------ll~'-'=------ _____ _1 __ ~ __ _?________l ___ ~

106-47-8 I 4-Chloroaniline 1 ND 1 u~~---- 1 ' 5 ,

'!:::::;: .~"'"E~::::~t'"·' ~ . ~~ -u~ . ~-== :-~J ~-,:0~- Fl ::: : A:::~~:::~. 1 ~~ 1 :n . --_-- . Hi- -r--i i

1 "~"-' L Az:o~:::~1.2- I - ~~----I~- ~~; ~-- l=-=. ± ~- - L ~ ~-____ j . Diphenylhydrazine

~::::: . -~--Be~:~~:~:)~~;::ne :----z~ ----r ~~; ~ I - ----~ ~ --J-- ~ r ~ -----· -----·-Benzo(b & k)fluoranthene ND - - ---+--ug I L-1---- -1-- ---1- - :--1- -------

191-24-2 J Benzo(g,h,i)perylene I N~ _ ugfl_~_L_-__ -=r__ __ =1-- -=r ___ 1_±-

04-26-0:'

04-26-03

04-26-0J

04-26-0Z

04-29-03

04-29-03

04-29-0:

04-29-03

04-29-0~

04-29-o:·

04-29-03

04-29-01'

04-29-0:_

04-29-0?

04-29-03

04-29-0.,.,

04-29-0J

04-29-03

04-29-0 •. ,

04-29-0'.'

04-29-0:3

04-29-0,

04-29-0'.' . 04-29-03

04-29-0,

04-29-0C

04-29-03

04-29-0,

04-29-0'

04-29-03

04-29-0,

04-29-0'

04-29-03

04-29-Ch

04-29-C'

04-29-03

04-29-0,

04-29-C

04-29-C,

04-29-0"

04-29-oS

04-29-C

Coyote 2001: Reports 1.0.011109162500 Report Date 61412003 12:39:51 PIV1

STANDARD - Assaigai Analytical Laboratories, Inc. - Quality Control Summary --client:

-Project:



D-Nota,;;;iica.bieCioo-to sample dilution -] _order: 0304502 PHl16 L Not applicable due to MDL proximity

- -- ----------------

- Type: MB: Method Blank Matrix: WATER -~Run Sequence -X03165 • XG.2003. 703.11

XG.2003. 703.11 -_ XG.2003.703.11

- XG.2003. 703.11

XG.2003. 703.11 -- XG.2003. 703.11

- XG.2003.703.11

XG.2003. 703.11 -XG.2003.703.11

- XG.2003. 703.11

XG.2003.703.11 -XG.2003.703.11

- XG.2003.703.11

XG.2003.703.11 -- XG.2003.703.11

- XG.2003.703.11

XG.2003.703.11 -- XG.2003.703.11

- XG.2003.703.11

XG.2003.703.11 -- XG.2003. 703.11

- XG.2003.703.11

XG.2003. 703.11 -- XG.2003. 703.11

- XG.2003.703.11

XG.2003.703.11 -XG.2003. 703.11

- XG.2003.703.11

XG.2003.703.11 -XG.2003. 703.11

- XG.2003.703.11

- XG.2003. 703.11



SW846 35108/82708 SVOCs by GC/MS 64-85-0! ____ senZoiC_a_C:ici _____________ ND--====j== ug-~=~-L-

10-o=-51=6-1-- Benzyl alcohol ND ug IL i ------- J_ --------------- -- -- +-

11_1111_~_49:~ t-- bis (2-Chloroethyl) ether NNDD ______ uu_g9_t_1~L---- ' _ bis(2-Chloroetho~2~~~harl_El__, ____ _

1_08-~_()=-1._L- bis(2-Chloroisopropyl)ether ND _u_g_l_L_-+--

_1_ 17-81-7 _l_ __ b~sS2_::_~!~11hexyl)phthalate 27 ug IL

2815~~081-~9 Butylb;~;;~~:halate ____ :- ~~ i ~~ ~ ~ ___ 1 ____ _

53-70-3 Dibenz(a,h)anthracene ND 1----ff ---------+------------------- --· ·- ---- ---------- ------t--

1 ug IL 1 -- ----------ND 132-64-9 Dibenzofuran ---------------------

84-66-2 Diethylphthalate ND --------- -----------

131-11-3 1

Dimethylphthalate ND 84-74-2 ~i ---di:n=-s-u-ty-lp_h_t_ha-1-at-e---+----N-D-------+--------~ -------[ 117-84-0 1 di-n-Octylphthalate ND -206-44-0 I Fluoranthene - ------- - -- _ --~----L ~=867_3_7 -r_~=------~luorene ND 118-74-1 I Hexachlorobenzene ND ---------· ----------r------------

87-68-3 1 Hexachlorobutadiene ND

77~47-~-i--HeJ<ach~ocycl9p_entad1ene --- C--------------N __ D ______ _ 67-72-1 ± Hexachloroethane ND 193-39-5 lndeno(1,2,3-cd)pyrene ND ---- - - ------ --- - -

:~::~:: ~ ~~~~~~::e- --------~~ --------1---- ----- ----·---· ----- ----- -----------

ug IL

ug IL

ug IL

ug IL

ug IL

ug IL

ug IL

ug IL

98-95-3 I Nitrobenzene ND ____ __ ug I L

62-75-9 I n-Nitroso-dime~_Y~~rl1ine __________ f\11:)_____ ug IL 621-64-7 . n-Nitroso-di-n-propylamine ND --! ___ ---uQ/L_T_

------+-

I ----j-------- ------------·---_El6-30-6 I n-NitrosodiP_henylamine ND I ug I L L ____ 1

-t--- r- =r I 1 -~875--8061 --58 ;__ Pentachlorophenol NNDD __ , _LJ_9 l_L I Phenanthrene : ug I L , 1

j-::-~-:t=- :;::: ! ~~ --~'. ___ :_m __ 1=-__ 1-~

25

5

1

X03165-013

i ---- ----- -------+-----l

5

1 -1--1------L----

i I. i

10

10

5

1

I --------1

, I

-~J~] 10 I 1

i I

_[_

1

10

1

10

-t·----1 I I

- -l--------1

~t--~~ I I

-I ------- ---- J 10 I

____ ____J_ ______ ,

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

~Type: MS: Matrix Spike Matrix: WATER -- Run Sequence

- M03559 - MT.2003.522.19

_xo3200 XG.2003.727.12

- XG.2003.727.12 -• Page 21 of 25

--



Range

Dilution

Factor

Detection

Limit

Run

Code Date

M03559-005 7439-97-6 Mercury --- L 120 - -- -T0/~ Recovery L__a_o_~_ 12o_J= = NA 05-01-03

EPA 504 ED8/D8CP by GC/ECD

H- n__l 1,~~~;~;~;:~~~~ne I 78

82

Coyote 2001: Reports 1.0.011109162500

X03200-005 -=NA~-+--j o5-o5-o3

NA ! I 05-05-03

Report Date 61412003 12:39:59 .PM


QC Surrogate Summary

-STANDARl ---Client:

Project:


APRIL 03 SAMPLE EVENT D

Explanation of codes I

~ Not applicable due to sample dilution r" Not applicable due to MDL proximity

1

Order: 0304502 PHl16 ' L -Sample: 0304502-02C Matrix: WATER -Run Sequence

X03165 XG.2003.703.14

XG.2003. 703.14

XG.2003.703.14

-----------------

Dilution Detection Run -CAS# Analyte Result Units Range Factor

8270

_____ _,l ____ *N_ITROBENZENE-D5 84 % Recovery 35- 114=f=-- T

_____ l~ __ *T_E_·:_~-~-~-~-~--L-~_~_1_4 ___ J __ ~-----~;~;~ ___ ;; _-_t441--_L-_~_3 rn I Limit Code Date -NA

NA

NA

X03165-015 ,,. 04-29-0~~ -04-29-0:· -

04-29-0~

Sample: 0304502-020 Matrix: WATER

Run Sequence

X03194 XG.2003.785.30

XG.2003.785.30

X03189 XG.2003. 750.20

XG.2003. 750.20

CAS# Analyte

8081 (DCB) Decachlorobiphenyl #2

(TCMX) Tetrachloro-m-xylene #2

Result

68

81


Units Range Factor Limit Code Date -X03194-016 % Recovery 50 - 150 I NA i I 05-09-0:J-

% Recovery 50 - 150 ~------~----~----~-

J ___ N~ ___ l==J 05-09-03-

8082

I ----! (D_C_B_)_D_e_c_a_c-hl-o-ro-b-ip_h_e-ny_l_#_2_~---9o ______ fo/o- Recovery

__ --·_--_--_-=1_~(_T_C_M_X_)_T_e_t_r_a_c_hl_o_ro_-m_-xy_le_n_e_#_2~ ____ 93 ________ 0_Yo_R_e~~'-'__ery 50 - 150

50 - 150

X03189-016 ,,-05-07-0, -

05-07-0~-

Sample: 0304502-03A Matrix: WATER -------------------· i-

-~---------------


Run Sequence CAS# Analyte Result Units Range Factor Limit Code Date l~ -524 X03206-032 X03206 XG.2003.814.21

XG.2003.814.21 I

-----" 1,2-Dichlo-ro_b_e_n-ze_n_e--d-4_(_S_S_) ~-- ____ 8_2__ 1 % Recovery 76 - 114 ~ -- --NA- ---,-----, 05-07-o~-

Bromofluorobenzene (SS) 83 ' % Recovery 75 - 125 1 -NP; ! 05-07-03 --~--~-~~~~~ I-

Sample: 0304502-03C Matrix: WATER -Dilution Detection Run

Run Sequence CAS# Analyte Result Units Range Factor Limit Code Date -8270 X03165-016 -X03165

XG.2003.709.15

XG.2003.709. 15

XG.2003.709.15

XG.2003. 709.15

XG.2003.709.15

XG.2003. 709.15

--~~T- *2,4-.-6--T-R_l_B_R_O_M_O_P_H_E_N_O_L_~---7-5----~! _%_R_e-covery.

1 *2 FLUOROBIPHENYL 85 °/c Reco e '

10 - 123 ---------t---------43 116 1

--NA--1---· --NA ____ , __ 04-29-03-

04-29-0c

04-29-0~~

04-29-03~

04-29-0::.

04-29-0:i-

I - 0 v ry . - I ---------- --- --

NA *2-FLUOROPHENOL i 43 __ % ~eco~~ry _ 21 - 100 1 ·---~--- ------ f---·------ ------

*NITROBENZENE-05 I 82 % Recovery 35 - 114 1 I

I

f-·---·

*PHENOL-06 33 _ ~-% Recovery 10 - 94 1 -- ---- ---

I

-- --! *TERPHENYL-014 43 % Recovery 33 - 141 1

____ J ____

·---- --- ·-··----

NA

NA

---------------------Sample: 0304502-030 Matrix: WATER

---------···-----,..., Dilution Detection Run -Run Sequence CAS# Analyte Result Units Range Factor Limit Code Date .-X03194 8081 X03194-017

XG.2003.785.31 I UTCMX) Tetrachloro-m-xylene #2 I 86 _,_0(~ Recovery r---5o---=-~5~- I ·1- -~------: --N-A I _J 05-09-o:--

• ~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~

Page 2 of 8 Coyote 2001: Reports 1.0.011109162500 Report Date 61412003 12:23:20 PM -



Client: Explanation of codes Project:

Order:



0304502 PHl16 D ] ~~~-~ app~c_a__b~-~u~ to__~~"}E_le d~~~-n L !. Not applicable due to MDL proximity


Run Sequence CAS# Analyte Result Units Range

8082 X03189 XG.2003. 750.21 ___ . ---f(TCM_X_)_T_e-tr-ac_h_lo_r_o_-m_--x-yl-e-ne-#_2==1 ___ 100 .. _ [_% Reco~eryL50~150 _J

Sample: 0304502-04A

Run Sequence

X03206 XG.2003.814.24

XG.2003.814.24

CAS#

Sample: 0304502-05A

Run Sequence CAS#

Analyte

Analyte

524

Matrix: WATER

Result Units Range

Matrix: WATER

Result Units Range

X03206 XG.2003.814.22

XG.2003.814.22

___ -_=:_J~ _12~~-'1~C:~~-~_'2~El_ne-d4(SS)- _[ _-- -86 ___ _[0iRec:c1_v_e;rrl 76- 114

______ L Bromofluorobenzene (SS) ___ 8!_ _ _ _ 1 o/o R_ecov~r~r_J-2_5-_ -~ 25

----- - ------ --

Sample: 0304502-05C Matrix: WATER ----------------··-·-------- ---------------

Run Sequence CAS# Analyte Result Units Range



X03189-017 ---r---·-r---- -J--_1 ____ J__ __ t-j_A _ _ __ 05-07-03

Dilution

Factor

Detection

Limit

Run

Code Date

05-08-03

05-08-03



X03206-033 -:--NA o5-o7-o3 I

NA 05-07-03



X03165 XG.2003.703.16

XG.2003.703.16

XG.2003.703.16

XG.2003.703.16

XG.2003.703.16

XG.2003.703.16

8270 X03165-017

• --1- -3.i6,;~~~:i:~~;~~~L :: u h~ ::::~ 42~~1-- ~---~1-201~0 : =-~~----~+N~AA-~ :.~ . -r -- - *2-FLUOROPHENOL 45 % Recovery -----+-*NITROBENZENE-05_______ 82 °/c R 35 114-r----1 NA ' j

_*T_~_:_~-~-~-~_Y_L--~-~_1_4 __ J ==~r -~ ~~ ~~~~-ic,~ ~ -~~i-:: -----!------

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03


Run Sequence

X03194 XG.2003.785.32

X03189 XG.2003. 750.22

Page 3 of 8


8081 r· (DCB) Decachlorobiphenyl #2 54 . % Recovery'J --50 - 150 l ---- --- "------------ --

8082 --= [ (D~-~-~--[)-e_-ca_c_h-lo_r_ob_i_ph_e_n_y_I #-2- 72 % Recovery : 50- 150 I __l___ __ _

Coyote 2001: Reports 1.0.011109162500



X03194-018 ·-

1 ---==------~-A- _L_--=J 05-09-03

X03189-018

NA 05-07-03

Report Date 61412003 12:23:30 PM

STANDARD



Client:

Project:




D+-~iVOta,;;;/icable due to sample dil~tion _:

Order: 0304502 PHl16 L_L Not_applicabl~ due to MDL prox1m1ty ...

Sample: 0304502-06A Matrix: WATER

Run Sequence

X03206 XG.2003.814.23

XG.2003.814.23

·---·-- -·---- --· -- ---~---·------------



524 X03206-034 -=------r 1,2-Dichlorobenzene-d4 (SSo=-__ 8_5 ___ ;%ReCoveru=76_- -1-14_J=-1~ r=--NA_~l ___ j 05-08-07

__ ___ I Bromofluorobenzene (S~----8~---J!~ Recove~L 75 -_ 12~ __ L ·-1 __ J_NA I J 05-08-03

---·------------------------·---·--·------------------- ------ - -- -----

Sample: 0304502-06C Matrix: WATER

Run Sequence

X03165 XG.2003.703.17

XG.2003.703.17

XG.2003.703.17

XG.2003. 703.17

XG.2003.703.17

XG.2003. 703.17




04-29-03

04-29-0:1'

04-29-0:

04-29-03

04-29-03

04-29-0:

----------·--·---·--------·---- ---- ---- ·-------------

Sample: 0304502-060 Matrix: WATER --- ---···-----

Run Sequence

X03194 XG.2003.785.33

X03189 XG.2003. 750.23

CAS# Analyte

8081

~ (TCMX) T~trachloro-m-xylene #2_ I 8082

Result Units Range

_____ . (TCMX) Tetracti1oro-m::xyiene#2[___ . _ 94 -=~=-% Recow;ry [ _ 5D _~15o



X03194-019 -, ·-------NA 05-09-0.

X03189-019

~j=-f\J}\_-] __ ] 05-07-0"

Sample: 0304502-07 A Matrix: WATER

Run Sequence

X03206 XG.2003.817.4

XG.2003.817.4

Sample: LCS

CAS# Analyte

524 ---- --,~-Dichlorobenzene-d4 (SS)

Bromofluorobenzene (SS)


Result Units Range Factor Limit Code Date

X03206-026

r--.· . ~~o ____ ·~::r;:~ ~-;~-+ --~~---~~-r-1 _____ __J ___ ,_ ----··-- - ,_______ l __ , ___ c=_.

05-07-0

05-07-03

Matrix: WATER ·-----·----·------ ·--·------ - -- -----· --- ··----···--··----- - -----·-----·- -----· ----

Run Sequence

X03206 XG.2003.800.4

XG.2003.800.4

X03206 XG.2003.817.3

Page 4 of 8


Dilution

Factor

Detection

Limit

Run

Code Date

524 X03206-013

L--=- -l-·-1-,2--D-ic_h_lo-ro_b_e-nz-e-ne---d4-(S-S-) -I 103 --'-_%_R_e_c_ov_e-'-ry-1---_7_6_-_1_14~_-'~-1= -,

1 NN!--A~__J=l

____ __j_____Bromofluorobenzene (SS) [ ___ 104___ % Recovery 75 - 125 I CI' 524

-- ----,---1)-0iCh.lorobenzene-d4 (SS) X03206-025

__ 12_8_ --~1 _%._R_e_co_v_e.c.ry __ i _76_-1_14~; __ .. -~~Jl.==J

05-07-0~

05-07-0~

05-07-C

Coyote 2001: Reports 1.0.011109162500 Report Date 61412003 12:24:31 Pfvr

STANDARD



Client:

Project:



Dj -Notapp/!Cabie-due to saljl,Jii}ilution _

L , ~<J_~_applicable due to MDL proximity Order: 0304502 PHl16

Sample: LCS

Run Sequence

X03206 XG.2003.817.3

X03206 XG.2003.814.20

XG.2003.814.20

X03194

XG.2003. 785.13

X03189 XG.2003.750.4

X03165

XG.2003.622.2

XG.2003.622.2

XG.2003.622.2

XG.2003.622.2

XG.2003.622.2

XG.2003.622.2

Matrix: WATER


Dilution

Factor

Detection

Limit

Run

Code Date

X03206-025 524 --T-Bromofluorobenzene (SS)

____ l_ ___ - -···- ----122 % Recovery ! -75--125 ____ _ 05-07-03

524 ---~------ - ___ T________________ -

__ ___ _._ 1,2-Dichlorobenzene-~4~~)-+------~-1~ _ ___ _ I % Recovery

-----~~o~ofluorobenzene (SS) [ __ 1_~ _ _____l_o!__o_ Recover~

8081

X03206-031

76 - 114 NA -- _l_

75- 125 NA I - --------- ------~-___________ ___l___ ____ _

X03194-002

05-07-03

05-07-03

------,-(TCMX) Tetrachloro-m-xylene #2 L_ _73 ___ ~1_°1c_o_R_e_co_very • 50- 150 _L_ ______ -~--NA- --]---, 05-08-03

8082 X03189-002

----~~-=:_J~(TCMX) Tetrachloro--m-xylene #2 I 84 , % Recovery j 50 - 150 -~A_-_L_J 05-06-03

8270 X03165-002

·2·~~;~~~:i:~:=:~~L :~ I~ ::~:~:rr=-1~~+~~--l----~=~~---~~ --:-=~~ j *2-FLUOROPHENOL 48 --ti/o Recovery-~- - 21.:-100-i _1___ NA i I

---- *NITROBENZENE-D5 79 ., % Recovery; 35-=-114--J - 1 ~ NA " ----1

---_-__ -__ +-_-__ --_~l"-~_:;-~-~-~--~-;-~~--1-~----{-_--· ___ ~--=-~ ~==:k1~1 !~~ -~~- ~-=

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

Sample: LCSD Matrix: WATER

Run Sequence

X03194 XG.2003. 785.14

X03189 XG.2003.750.5

X03165

XG.2003.622.3

XG.2003.622.3

XG.2003.622.3

XG.2003.622.3

XG.2003.622.3

XG.2003.622.3

Sample: MB

Run Sequence

X03206 XG.2003.800.3

XG.2003.800.3

Page 5 of 8



8081 X03194-003 - - ~(TCMX) TetrachiO~o~~-xylene #2 79 --__ t-J_A __ j _ J 05-08-03

8082 X03189-003

. i -NA----=~=] 05-06-03 - __ T ___ -----

: (TCMX) Tetrachloro-m-xylene #2_ [ - --------------- -- ------ ----

8270 X03165-003

*2,4,6-TRIBROMOPHENOL 91 l0/o-ReCQveryf10::-12:3 __ - - r=~~-

---+- - =~-=~~UOROBIPHENYL i 81 [''lo Recovery! 43- 116 I . NA H-----

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

- ,_ *2-FLUOROPHEN_O_L __ 1-' ____ 4_8_----- _1_0/o ~Elcovery • 21-~-1-oo l_NA_

-----~--+~·· ·~--==_*__N_~T-l_TE_·_::-~-;-~-~-:-L:-~-~-:D-4_5 __ -1---------_ -~:: i ~ ~::::~ -::C-~t-J1~t ··-=

CAS# Analyte Result

524 ---~----·---·-·

__ _;____2...3-Dich loroben;z:emei-d4 __ (S_S_)_+-___ 90 · Bromofluorobenzene (SS) 86

-----~-------·--


·- -- -

Matrix: WATER


Units Range Factor Limit Code Date

X03206-012

--- -=-1-~=:~;~fif-1}~-~~r=~~=---t-~~~~-•---~~·~~-••-J 05-07-03

05-07-03

1.0.011109162500 Report Date 61412003 12:24:41 PM

STANDARC



--------- ----------Client:

Project:




- --"-

Sample: MB

Run Sequence

X03206 XG.2003.817.1

XG.2003.817.1

X03206 XG.2003.814.19

XG.2003.814.19

X03194 XG.2003.785.12

------··--------------

CAS# Analyte

524

, I 1,2-Dichlorobenzene-d4 (SS)

' --=----=--=--L__ Bromofluorobenzene (SS)

524

___ i:__ 1,2-Dichlorobenzene-d4 (SS) Bromofluorobenzene (SS)

-~-- --~-

---------· Matrix: WATER

Dilution Detection

Result Units Range Factor Limit Code

X03206-023 -- ·-

93 % Recovery 76- 114 NA _j - -- + 94 % Recovery 75 - 125 NA __J

X03206-030

:~-- --~~:~:~~ :-~~~{~~:=:= -~---- -1--~~ -_-J I 8081 X03194-001 [ ==------[ (TcMx)Tutl-achloro-m-xylene -#2_[ ____ 76_-_-_--:~--: Of<-oRec-ov_e_r~[ 5o_~_15o- - - -1~-- J ____ t-lE_-=::_L ___ _]

Run

Date

05-07-0::.

05-07-0?

05-07-03°

05-07-0:-.

05-08-0:>

X03194 8081 X03194-014

XG.2003.785.25 I _______ . L (Tc'iv1X) Tetrachloro-m-xylene #2 .. ~I ____ 7_8 ___ ~1 °_V~ Rec-overyi50-15o- ~- ~-__:1-- 1=:~~~-- 05-09-03

X03194 XG.2003.807.8

X03194 XG.2003.807. 7

XG.2003.807.7

X03189 XG.2003.750.3

X03189 XG.2003.750.18

XG.2003.750.18

X03189 XG.2003.798.4

XG.2003.798.4

X03165 XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

X03165 XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

X03165 XG.2003.679.4

Page 6 of 8

8081 X03194-026

I _____ _1 (TCMX) Tetrachloro-m-xylene 72 NA I I 05-19-0J

8081 X03194-028 NA 05-19-0~ 1 -- • ----

1 (DCB) Decachlorobiphenyl 71 % Recovery 50 - 150 ________ l----------------j---~----~-·- -+--------

(TCMX) Tetrachloro-m-xylene 77 ! % Recovery j 50 - 150

8082

---·~(_T_CMX) Tetrachloro-m-xylene #2 I

8082

8082

84

38

86

NA 05-19-03

X03189-001

; % Recovery I 50 - 150 ! ~ NA ! ·i _L ________ 1.. __ --05-06-0'.5

X03189-014

--+-!-~-:-:-:-~:-~-:-~~: -:~-:-~-:-~-j:' ___ -_-__ -=_·l~---=----~~-j--:_=_j 05-07-0:

05-07-03

X03189-027 -~-----·-------~--------------~----~--- ----------

(DCB) Decachlorobiphenyl #2 53 -----+--------------+------

(TC MX) Tetrachloro-m-xylene #2 103

% Recovery I 50 - 150

% Recovery i 50 - 150

NA 05-15-03

NA 05-15-o:

8270 X03165-001 -~-------~--------~·--------------

-· _·2~;~;~~~:i~~=~~;~L :~ ~~~-:-~~~!~! _ :~: -~~-~ l ~~--·---~ ~:::~:~~ -----------+--- ------~------ ------ ----- ------------------ --------- - ---------~

___________ __*3_::.f=LUOROPHENOL 50 % Recovery _j__ 3_1__-_ 100_ 1 NA ! 04-10-0:.

*NIT~~~~~~~~:-D_5 ______ ~ ______ ;;_ _ i ~ ::~:~:0- ~50-_ ~~4 *TERPHENYL-D14 _J_____ 80 _____ .

0(~-~e~o_ve_~t-~-~ 1~1

. 1 -.· NJ\ n r..-__ ~ ,..,,,, __ _:)~ __ J__-~~---t----- ~:::~:~~·

8270 . ·- -·--·-·--- ----- ---------------·------· ..

T *2,4,6-TRIBROMOPHENOL 78 i % Recovery 10 - 123 i

*2-FLUOROBIPHENYL 92 I% Recovery 43 - 116 I ---------~ ..

*2-FLUOROPHENOL 53 : % Recovery 21 - 100 I ---~---,----

*NITROBENZENE-D5 87 ' % Recovery 35 - 114 ·--~-----------_)._

*PHENOL-D6 41 I% Recovery 10 - 94 ---1--- --·--

I% Recovery --· --·-·--

*TERPHENYL-D14 57 33 - 141 . -- ·---~-~ - --- ·-

8270

*2,4,6-TRIBROMOPHENOL __ 9_2_-_-_-_-_------~~0_Vo_-R_-e_c_o_ve_ry~j _1_0_-_123 L

Coyote 2001: Reports 1.0.011109162500

-· ------ -- --

1

1

1

1

1

1 ---

X03165-008 -, NA

--NA

NA ----------·-·--

NA

I NA I NA !

i __J

X03165-011 ; ---NA--==l

04-22-02

04-22-03

04-22-0~

04-22-03

04-22-03

04-22-0~.

04-26-0:'"

Report Date 61412003 12:25:40 PM

STANDARD



Client:

Project:


APRIL 03 SAMPLE EVENT Explanation of codes I

-- ·------------------ I D , _ N_o_t applicable due to sample dilution j

Order: 0304502 PHl16 L Not applicable due to MDL proximity '

Sample: MB

Run Sequence

X03165 XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

X03165 XG.2003.703.11

XG.2003.703.11

XG.2003.703.11

XG.2003.703.11

XG.2003.703.11

XG.2003.703.11

Sample: MS

Run Sequence

X03194 XG.2003. 785.16

XG.2003. 785.16

X03189 XG.2003.750.8

XG.2003.750.8

X03165 XG.2003.622.5

XG.2003.622.5

XG.2003.622.5

XG.2003.622.5

XG.2003.622.5

XG.2003.622.5

Matrix: WATER


Dilution

Factor

Detection

Limit

Run

Code Date

8270 X03165-011

*2-FLUOROBIPHENYL 91 % Recovery I 43 _:-__ ~[ ____ ---+ __ N_A_---+----1 *2-FLUOROPHENOL 46 % RecoverYT21- 100 I NA

' -- - ------~--

,------~-----·-------------·-------· I -·--------'· ---~--------

*NITRosENzENE-D5 83 % Recovery ' 35 - 114 ! NA -------.P-H_E_N_O-L--D-6 _____ , ___ -----35------ 0/oReCOveryr---1-o-=-94-~---- NA

*TERPHENYL-D14 7 4 % Recovery ' 33 - 141 NA ----------~---

8270

_j_ !

-------------

* 2,4,6 -TR I BROM OP HEN O L - l_ *2-FLUOROBIPHENYL I

*2-FLUOROPHENOL

88

83

--fO/o Recovery--16~ 123 r --' % Recovery 43 - 116

45 ' % Recovery 21 - 100 -·----------·------------- -

*NITROBENZENE-D5

*PHENOL-D6

*TERPHENYL-014

~~- ______ "/_o_~~co_ver~j- ~5 - 1_1~

--~~---------;;:_;~:~~tit" -1~i_1 _ --~-- ------

Matrix: WATER

X03165-013

04-26-03

04-26-03

04-26-03

04-26-03

04-26-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03



8081 · --~==[ (DCB) Decachlorobiphenyl #2 I

___ __l_(TCMX) Tetrachloro-m-xylene #2 I

8082

37

80

- % RecoverYl}~~=1 ~ _ r 2

' % Recoveryf 50 - 150 J _____ 2

X03194-005 ---- - ~---~---,

NA I

NA r-· ---

-~-: _____ h;~~~ ~=t~:~~::~~~2~:~:~:!~- -~=~=~--~=~r: -- --+tt~~~~~~¥ _H_

-------~-------~

X03189-006 ---,- ----NA--~----i

-i NA 1 j

8270

: -==:I *2,

. -l ----+ 4,6-TRIBROMOPHENOL 88

2-FLUOROBIPHENYL 80

*2-FLUOROPHENOL 38

*NITROBENZENE-05 80

*PHENOL-06 28

*TERPHENYL-014 74

X03165-005

% Recovery 10 - 123 ' 2 NA --·----

% Recovery 43 - 116 2 NA ----------;-

% Recovery 21 - 100 2 NA -t--------------

I -+.% Recovery 1 35 - 114 2 NA ~ 0/o Recovery'.-1o :94--T- --2 - -- -·--

NA -1------------------- -- '

__ _ ~lo Recovery L_ 33 - 141 2 NA

05-08-03

05-08-03

05-06-03

05-06-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

Sample: MSD Matrix: WATER

Run Sequence

X03194 XG.2003.785.17

X03189 XG.2003.750.9

XG.2003.750.9

Page 7 of 8

CAS# Analyte Result

8081 --~

_____ __L(TCMX) Tetrachlor~~_r:ri_:xylene #2 ! 77


Units Range

------,. --·--- -·~---·--- - - -- - L ' % Recovery 50 - 150

------------ -

. -- tl-· ' % Recovery 50 - 150

~~o/o ~ec~~ry_ - ~6- - -150

1.0.011109162500

Dilution

Factor

2

Detection Run

Limit Code Date

X03194-006

J -~"' _n L ______ I 05-08-03

X03189-007 -- --r------,

2 ; NA , I 05-06-03

2 f -NA T -- j 05-06-03 J -- ------- -- L__ __ . _____ _J

Report Date 61412003 12:25:49 PM

STAN DAR[



Client:

Project:



ol Not applicable due to sample dilution

L--1 Not applicable due to MDL proximity Order: 0304502 PHl16

Sample: MSD

Run Sequence

X03165 XG.2003.622.6

XG.2003.622.6

XG.2003.622.6

XG.2003.622.6

XG.2003.622.6

XG.2003.622.6

Page 8 of 8

Matrix: WATER -~·-·---···------------------------



8270 X03165-006

-===f ~-=---2~-~--;~--~·-~-~---;-~-~-:-l~-~-~-~-:-~-L-~---:-:--~~~-~~-. -:-~-~=~:~~~:~~:~~~~-;~-1 -~ -:-;~ r-y T ": : I -1 ----~--.N-l_T_R._O_B_E_N_Z_E_N_E--D-5---1----8-0----1-°/c-o_R_e-co_v_e-ry--1---35 ___ . __ 1 .. 1_4____ 2 - r_--r..JA ___ ------------.P-H-EN-O-L--D-6----+-----3-0-----+--°/c-o_R_e_c_ov_e_ry-+---1 O~ 94 - 2 · t--NA----·============·_T-_E-_R-_P-_H-_E-_N-_Y-_L--=D=-1-4_-_-_--. +--_-_--__ ---_-·7-6-~==- % Recovery ___ -33--~----!~-_--1-__ --+--__ -.. -.. --2=-~------~l __ N_A_~-~

04-10-0::.

04-10-0:

04-10-03

04-10-o:i

04-10-0:

04-10-03


I •• t _. t _. t • f ••• t • t • t • t • f • t • f ••• t • f ••• t • t • ' • t ••• t • t ••••••• f • t ••••• \ • f f t ••••••• t ••• f ••••••

AssAIGAI Chain of C stody Record ~ I ANALYTICAL ·! (f_\ r::::'1y" .

LABORATORIES, INC, Lab Job No.: !J · '_J- .__) }~?}:. i) /)I'· cji 3 Page ol A;

Client L~ It . . ... < ":.:::::: .. , . ~·. ,_\ , , - ,- . .,- - "' i\ ' ., . .::.. . ,. I ) . \ ' . ' .J _) c V'Ji.. I c_, I J v'\ (.},I . \..x Pro1ect Manager I Contact -l () G Iv b t)" .) ..... •

Address .... , n I\ - F. 1c· ,~....,. -,,..·:•.1 '-/ '.J. :') I t~ ,<\ . i f1 v\/1 f.: V ' (. ,4/V • V W 1 h.feifiphone No. ~ .£ 2 7 0 ,) --/

City I State I Zip {\ : Pi (~ t\J ~V., ~? ·+ \ l ~. Fax No. '< ?. 2. 7£..£Q../J

• _....- I I

Proje~tName/Number fh, \/ cf":!. S" :"l""'yi2 [- \)t:NTSamplers:(slgnature) ~.:J ( ,5.;:.·'~ ,,__6;:,:;: \. ' w

Contract I Purchase Order I Quote. ______________ _

,u.J- ~-5

x \I/ I LT·{'

1'v\ \.)J . ~t- 6 /b~o \) ; ~L.

.. ~'Jjf' ·1

G --...........

LT-\'

Relinquishe~.;.. ( '", Date

Signature _.) ~--~ -~-Printed "S c to\'\ ~-

v~. ,,., \;'-. ·1 ,J

Signature ___________ _

Company ML Time

'2 o So

Printed ____________ _

Company __________ ~

Reason ____________ ~ Reason ___________ _

Method of Shipment _____________ _ Comments: - ....,,,..., '- v --v= J ......_ ,..,, - - ' \f e· '1'::...:::I Shipment No. ________________ _

Special Instructions: _____________ _

~ . . ASSAIGAI PROJECT FILE

)(

Date

Time

P.O. Box 90430 ALBUQUERQUE, NEW MEXICO 87199

(SOS) 34S-8964

3332 WEDGEWOOD EL PASO, TEXAS 7992S

(91S) 593-6000

127 EASTGATE DRIVE, 212·C LOS ALAMOS, NEW MEXICO 87S44

(SOS) 662-2SS8

Received by:

Signature __________ _

Printed ___________ _

Company __________ _

Reason ___________ _

After analysis, samples are to be:

u Disposed of (additional fee)

a Stored (30 days max)

U Stored over 30 days (additional fee)

U Returned to customer

~

ASSAIGAI ANALYTICAL LABORATORIES. INC.

Chain of Custody Record ,=c. ( ., ,. ·1 /<·- ,-"'-' ' . i "-' . ( ' LabJobNo.: U .)1...,,. _,r•_)cSet.;-::Z.3 A1lv.q3

Page 2_ of _-:J::e_..J _

Client ("\, • ! .::::.:,,-- --1 \ /"i. \ ,......._ ': ~ ,._ ' r' r"\ i I - ("""'

·- ·. "\' ·;, ,) c.: ,\./\, , '-·'-' .J <.l ~·· C ' Ov -, Project Manager I Contact -so C::. (\I\ Av...s l v--

Te1ephone No. 'R :l 2 - :f b 3 '-f Address _______________________ _

FaxNo. 'B 2 '2. --~ :::::::::-:=' -:::, ~ \ ~--

City/State/Zip __________________ _

Project Name I Number (\:>, . ·- ¢ :?,. "S ./'\ v .... • p I \..~ [.:. Vt: /\JT Samplers : (signature)

Contract I Purchase Order I Quote ______________ _

--r~

Relinqulss:~ \ )

Signature ~-::c:-;::-'\ ~ __.,,.. '

Printed ::::i ., . .::ii\ 'c'v ~~\ Company vV),,,L :1o5o

Date ~-1·

--i·"? Time

Signature ___________ _

Printed ____________ _

Company ___________ _

Reason ____________ _ Reason ____________ _

Method of Shipment _____________ _ Comments: ______________________________ _

Shipment No. ________________ _


ASSAJGAI PROJECT FILE

x

Date

Time


(505) 345-8964

3332 WEDGEWOOD EL PASO, TEXAS 79925

(915) 593-6000

127 EASTGATE DRIVE, 212·C LOS ALAMOS, NEW MEXICO 87544

(505) 662·2558

Received by:


Printed ___________ _

Company __________ _

Reason ___________ _



a Stored (30 days max)

U Stored over 30 days (additional fee)·

U Returned to customer

·-Client:

•. Project:

·order:

ASSAIGAI ANALYTICAL LABORATORIES, INC. 4301 Masthead NE • Albuquerque, New Mexico 87109 • (505) 345-8964 • FAX (505) 345-7259

3332 Wedgewood, E-5 • El Paso, Texas 79925 • (915) 593-6000 • FAX (915) 593-7820 127 Eastgate Drive 212-C • Los Alamos New Mexico 87544 • (505) 662-2MS--------- -----------

, ' Explanation of codes --- -- -------------"

PHILIPS SEMICONDUCTORS attn: DAVID PAULSON 9201 PAN AMERICAN FRWY NE ALBUQUERQUE NM 87113



0304504 PHl16 Receipt:



04-23-03

B analyte detected in Method Blank

E

H

N

s 1-9

result is estimated

analyzed out of hold time

tentatively identified compound ---- -- ---- ---------------

subcontracted

see footnote - i

STANDARD

---- - ----------------------------

'5ample: NCLF-9 Collected: 04-22-03 13:50:00 By: SP

.Matrix: GW

_QC Group

, 0304504-01A

X03206

X03206

. X03206

X03206

;xo3206

.X03206

'X03206

:xo3206

. .X03206

X03206

.X03206

-X03206

X03206

.X03206

X03206

X03206

)(03206

X03206

X03206

X03206

X03206

X03206

X03206

·X03206

Run Sequence

XG.2003.800.7

XG.2003.800.7

XG.2003.800.7

XG.2003.800.7

XG.2003.800.7

XG.2003.800.7

XG.2003.800.7

XG.2003.800.7

XG.2003.800.7

XG.2003.800.7

XG.2003.800.7

XG.2003.800.7

XG.2003.800.7

XG.2003.800.7

XG.2003.800.7

XG.2003.800.7

XG.2003.800.7

XG.2003.800.7

XG.2003.800.7

XG.2003.800.7

XG.2003.800.7

XG.2003.800. 7

XG.2003.800.7

XG.2003.800.7

• ~Pa 4

ACCREDITED

Dilution Detection



75-34-3

75-35-4

71-55-6

1 , 1 Dichloroethane

1 , 1 Dichloroethene -- ·--- ·--···-- ---- --- ----

1, 1, 1 Trichloroethane

630-20-6 1, 1, 1,2 Tetrachloroethane 79-oO~s--- --t ---- ---1-~ ,2 Trichloroethane-

79-34::5---r-1,1;2,2 l-etract110-roetha-ne

ND . ug IL ND ___ r-ug I L

------------,-----------

ND ug IL

ND

ND

ND

ug IL

ug IL

' ug IL 563-58-6- r . -- 1~1---D-ic-h-lo-roprop-en-e ------- -ND-- --- ug I L

0.1

0.1

0.1

0.1

0.1

0.1

0.1

0.1 106-93-4 ·r 1 ,2 Dibromoethane (EDB) ______ ND _____ u97 Ln " 1 -1;2Dichlo-robenzene___ ND ug IL ,_ __ 1---:- o-:1- --- - -95-50-1

107-06-2 . -

78-87-5

96-18-4

87-61-6

120-82-1 ' --- -

95-63-6

96-12-8

541-73-1

108-67-8

142-28-9

106-46-7 ··- ----·-1··

99-87-6

1,2 Dichloroethane (EDC) I .N. D. -----~g!_L ~1 1 - 0.1

1,2 Dichloropropane: I ~N~D= ug I L 1 0.1 ------··-------i-·------- ---------

1,2,3 Trichloropropane ______ N __ D _____ _+__ll. g- _/_-~------ _ __1_ _+-__ 0.1 1,2,3-Trichlorobenzene ND I ug IL 1 0.5

1,2,4-Trichlorobenzene ND Tug IL · 1- 1 ·· - • 0.5-

1,2,4-Trimethylbenzene I - --ND- . J ·ug IL i- - 1 0.1

1--2-Dibromo-3-chloropropane I --N-D--j--ug I L - ~-- 0.2 ·-+

1,3 Dichlorobenzene ND i ug I L ' 0.1 ---+------ - [····--·-·

1,3,5-Trimethylbenzene · ND i ug IL 0.1

1,3-Dichloropropane --No-' ug/1...- - ' 0.2 ------+----- - - ~---

1 ,4 Dichlorobenzene

1,4-lsopropyltoluene

. ND i ug IL I ~--N-D--lu-g/L-- - -T ---

i1--------~ ----1-5_9_4_-2_0-_7~ ___ 2_,2_-Dichloropropane 1 __ _f'JD ---+-ug_l_L __ J 0.2

! 95-49-8 2-Chlorotoluene ND I ug I L I 0.1

106-43-4 _ -------~-Chlorotoluen_e ___ _:::_=-:=_~ND -·[ -:_u9LL _______ --_l __ 9~1_

i I I

-!--

'

.1

Prep

Date

Run

Date

05-06-03 05-07 -03

05-06-03 05-07 -03

05-06-03 05-07 -03

05-06-03 05-07-03

05-06-03 05-07-03

05-06-03 05-07 -03

05-06-03 05-07 -03

05-06-03 05-07-03

05-06-03 05-07 -03

05-06-03 05-07 -03

05-06-03 05-07-03

05-06-03 05-07-03

05-06-03 05-07 -03

05-06-03 05-07 -03

05-07-03

05-06-03 05-07-03

05-06-03 05-07-03

05-06-03 05-07 -03

05-06-03 05-07-03

05-06-03 05-07-03

05-06-03 05-07-03

05-06-03 05-07 -03

05-06-03 05-07 -03

05-06-03 05-07 -03

REPRODUCTIO~fi:Hl~X@W>R.~tm,Cf!S§THAN Pui?L~~S~~~ITIEN CONSENT OF AAL. Report Date 611 THIS REPORT MAY NOT BE USED IN ANY MANNER BYTHECL!ENTORANYOTHER THIRD PARTY TO CLAIM

PRODUCT ENDORSEMENT BY THE NATIONAL VOLUNTARY LABORATORY ACCREDITATION PROORAM.



Client:

Project:



--

Sample: NCLF-9 Matrix: GW

QC Group

0304504-01 A

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

0304504-01 8

X03200

X03200

0304504-01 c X03165

X03165

Run Sequence

XG.2003.800.7

XG.2003.800.7

XG.2003.800.7

XG.2003.800.7

XG.2003.800.7

XG.2003.800.7

XG.2003.800. 7

XG.2003.800.7

XG.2003.800.7

XG.2003.800.7

XG.2003.800.7

XG.2003.800.7

XG.2003.800.7

XG.2003.800.7

XG.2003.800.7

XG.2003.800.7

XG.2003.800.7

XG.2003.800.7

XG.2003.800.7

XG.2003.800.7

XG.2003.800.7

XG.2003.800.7

XG.2003.800.7

XG.2003.800.7

XG.2003.800.7

XG.2003.800.7

XG.2003.800.7

XG.2003.800.7

XG.2003.800.7

XG.2003.800.7

XG.2003.800.7

XG.2003.800.7

XG.2003.800.7

XG.2003.800.7

XG.2003.800.7

XG.2003.727.23

XG.2003.727.23

XG.2003.703.18

XG.2003.703.18

Collected: 04-22-03 13:50:00 By: SP




Benzene ND ug I L f--1-i 0.1 ------··-·-·--+-------------+-----+-_ _::_ __ +---

71-43-2

108-86-1 Bromobenzene ND ug I L 1 I 0.1 --------+--- ---------+----------1-----+--------J___-_____ --·-- ·-·------.

Bromochloromethane ND ug I L 1 0.1 . -------+---------------- --------~ --- - ---1--------

75-27-4 Bromodichloromethane ND ug IL 1 0.1 1

------+--------------+------+-----+------1--------~ - ---------75-25-2 Bromoform ND ug I L 1 0.1 -·-·---+-----------·--- -·- ---- -- -----74-83-9 Bromomethane ND ug IL 1 0.6

----·--------+----------------+------------+------+----!------.. -·- -- -----

_5_6_-2_3_-5_+---__ c_a_r_b_o_n_tetrachloride ND ug IL

108-90-7 Chlorobenzene ND ug IL -------+---------------+----- ~----~---

124-48-1 Chlorodibromomethane ND ug IL ----+-----

0.1

0.1

0.1

75-00-3 Chloroethane _!'J~-~ ug I L 1 0.1 l _-;5-~-:;-~-9=:~2===·=---~=--~c=-i=s--=C-1=-.:=-10=:-:=i:-c=~-

0

=1e-:=~-:=-:=-~=;-e=-n=-e=--~=--~==-=--=· ==~=~==---·------1-_-:-:--~:---~---:_ ~ :~-~ ' ___ -_-:_Li~~ 10061-01-5 cis-1,3dichloropropene ND ug/L 1 0.1 1

Dibromomethane ND i ug I L 1 0.1 i ----f--·--·-------------+----------+-----+----+------1------j

100-41-4 Ethylbenzene ND i ug IL 1 0.1 i 74-95-3

75-71-8 J _____ F_r_e_on_12 ____ --+ __ 0_.4_0_----+i_u_g_l_L_+--_1_---+-__ o_.1_ 1 --i _!_7-68-=31 Hexachlorobutadiene ND ! ug IL 1 0.1 -r-- I

98-82-8 lsopropylbenzene

1

ND

1

. ug I L _j 1 0.1~: 75-09-2 Methylene chloride _ ND _ ug I L ____ 1 __ ---+-__ o_.5 i

_9_1 ___ 2_0 ___ 3----1----N-a_p_h-th·-a-le_n_e ___ ---+!--N-D--1--I -u--g-/-L 1 1 I

104-51-8 n-Butylbenzene L-- ND i ug IL L 0:1 ----r:---=---1 103-65-1 n-Propylbenzene ND ug IL 1 0.1 : I

95-47-6 o-Xylene +---~- : ug/L 1 :- -0:1 --j---- --_J1

I -108-38- p/m-Xylenes 0.24~-TL ___ l --_e=-0.2-=tJ 3/106-42

f 135-98-8 sec-Butylbenzene --+-----N_D __ --1-_ug"---/ _L----1_ 1 o_._ 1 ____ ·--+---------·-j

! 100-42-5 Styrene ND ug I L 1 0.1

' 156-60-5 t-1,2 Dichloroethene ND ug I L 0.1

05-06-03 05-07-03.

05-06-03

05-06-03

05-06-03

05-06-03

05-06-03

05-07-03 I'

05-07-03 ...... _

05-07-031"'·. -,,,,M,

05-07-03 ,,. .. 05-07 -03''--v·

05-06-03 05-07-03<'··· WV•k

05-06-03 05-07 -03 ,,. .. 05-06-03 05-07-03 ... -w

05-06-03 05-07-03/' •. \t)1{.<l-·

05-06-03 05-07-03 ,.

05-06-03 05-07-03'··,·

05-06-03 05-07-03,w'• ~*'-'

05-06-03 05-07 -03 r

05-06-03 05-07-03'<.

05-06-03 05-07-03"

05-06-03 05-07 -03 r

05-06-03 05-07 -03"·•

05-06-03 05-07-03"' ~.,,

05-06-03 05-07-03

05-06-03 05-07 -03 "<0

05-06-03 05-07-03'

05-06-03 05-07 -03,

05-06-03 05-07-03 ,_

05-06-03 05-07 -03"' "" I'

05-06-03 05-07-03"· .

05-06-03 05-07 -03,,

05-06-03 05-07-03 ..,,_. ·-------j------+-----+------+-----j ' .

10061-02-6 t-1,3 Dichloropropene _N_D __ -+-_u-'g'-/-L--+----+---o_.1_-+ __ ___, 05-06-03 05-07-0::i . .,.,,

98-06-6 tert-Butylbenzene ND ug IL 0.1 , 05-06-03 05-07-03,•-

127-18-4 Tetrachloroethylene 0.68 ug IL 0.1 ,

100-0 __ 0-_3 _______ T_o_lu_e_n_e ____ --+ ___ N_D __ + ug __ l_L_;_i ---+-! __ o_.3_---11-----"1

_7_9_-0_1_-6_+---___ T_ri_c_hl_o_ro_e_th_e_n_e ____ + _____ N_D __ ~_u_g_l_L _____ L_9._1__ _ _j__ __ __,

75-69-4 Trichlorofluoromethane ND ---+'

1

_u_g_l_L_~_ 1 0

0

._1

1

1· ii

75-01-4 Vinyl chloride ND _J_ __ u_.c_g_l_L_L______ _ _


1,2-Dibromo-3-chloropropane ND ug I L

____ L___ __ 1_,_2-_D_i_br_o_m_o_e_th_a_n_e_,_E_D_B __ L___ __ N_D ___ _L__u_:_g/L --~ ___ j_ __ ;~~~: _J ____ J SW846 35108182708 SVOCs by GCIMS By: M/KAR

05-06-03

05-06-03

05-06-03

05-06-03

05-07 -03 ,.,, •. r···-·~'<,

05-07-03..,,,.

05-07-03.#"·.

05-07 -03 "' /•

05-06-03 05-07 -03\.,.

05-05-03 05-06-03r'

120-82-1

95-50-1

1,2,4-Trichlorobenzene

1,2-Dichlorobenzene

ND

ND

ug IL

ug IL

--1---,--1- 04-28-03 04-29-03 ... ,..

_ ! --- _ -~- _ __l____ 04-28-03 04-29-03-u•'

------------------------------------------------------------'~_,_ ·, Page 2 of 44 SQLCoyote: Reporls 1.0.0305281535XX Reporl Date 6118103 2:05:39 PM -



Client:

Project:

.~rder:



0304504 PHl16 Receipt: 04-23-03

Sample: NCLF-9 Collected: 04-22-03 13:50:00 By: SP

,\/latrix: GW

Dilution Detection


0304504-01 c X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

SW846 35108182708 SVOCs by GC/MS By: M/KAR

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

XG.2003.703.18

XG.2003.703.18

XG.2003.703.18

XG.2003. 703.18

XG.2003.703.18

XG.2003.703.18

XG.2003. 703.18

XG.2003. 703.18

XG.2003. 703.18

XG.2003.703.18

XG.2003.703.18

XG.2003. 703.18

XG.2003.703.18

XG.2003. 703.18

XG.2003. 703.18

XG.2003.703.18

XG.2003.703.18

XG.2003. 703.18

XG.2003. 703.18

XG.2003.703.18

XG.2003.703.18

XG.2003.703.18

XG.2003.703.18

XG.2003. 703.18

XG.2003.703.18

XG.2003.703.18

XG.2003. 703.18

XG.2003. 703.18

XG.2003.703.18

XG.2003.703.18

XG.2003.703.18

XG.2003.703.18

XG.2003. 703.18

XG.2003.703.18

XG.2003.703.18

XG.2003.703.18

XG.2003.703.18

XG.2003.703.18

XG.2003.703.18

XG.2003.703.18

XG.2003.703.18

XG.2003.703.18

541-73-1 1,3-Dichlorobenzene ---,---------- --- -- -------

ND ug IL 106-46-7 1,4-Dichlorobenzene ND ug IL 90--12~-1- -- 1~rliietti-yiITTi-P-hii1ale~e ND ug IL 1 ,

---+-------------+--------------------------

58-90-2 2,3,4,6-Tetrachlorophenol ND ug IL • 1 1 5

95-9541--2,4,5-Trichlorophenol ND . ug IL ---1 -t 5

f~riif F ·· ·· .. 2f :i::E~;~~:;[_~·~~" ~::;·~ . -_ ~ ·····r-~:1---.----+----j

51-28_:~~' __ 2,4-Dinitrophenol NE___ _____ u_gl_L __ · 1 f---20 121-14-2 ' 2,4-Dinitrotoluene ND ug IL 1 5

- - --------- - - -

606-20-2 2,6-Dinitrotoluene ND , ug I L 5 -------------

91-58-7 2-Chloronaphthalene ND ug IL

_95-5~_-8_;___ _ _. ~::_C~~~r-~~henol ND i ug IL

91-57-6 2-Methylnaphthalene ND _ j _ ug IL 95-48-7 2-Methylphenol

88-74-4 2-Nitroaniline ug IL ---------------------------t-------j--------

88-75-5 2-Nitrophenol ND ug IL 9-,_-94.-11--- 3:3~oicillOroiJe~~idine ND

------------------ -3+4 Methylphenol ND

-------- --------------- -----------

99-09-2 3-Nitroaniline ND ---+--------------- - -

534-52-1 4,6-Dinitro-2-methylphenol ND 101-55-3 4-Bromophenyl-phenylether ND

-----59-50-7 4-Chloro-3-methylphenol ND

191-24-2

ug IL

ug IL

ug IL I - -I _ ug IL ,

I ug IL ug IL

ug IL

5

5

10

1

5

10

1

64-85-0 Benzoic acid ND ug I L 25

100-51-6 Benzyl alcohol ND ug IL 5 1i1=44-4""t--- bis-(2--=Giiloroethyl) ether 1 ND -- r ug IL 1

111-91-1 bis(2-Chloroethoxy)methane I ND -- -:- ug/i__~ ___ 1__l_ 108-60-1 bis(2-Chloroisopropyl)ether_ -L ND l ___ ug IL 1 [ __

117-81-7 bis(2-Ethylhexyl)phthalat~ __ N_[)_ ____ L ug IL 5

1

- - --~ -----1

------- ----- ~

__ _J_ ______ _

Prep

Date

STANDARD

Run

Date

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

Page 3 of 44 SQLCoyote: Reports 1.0.0305281535XX Report Date 6118103 2:05:55 PM



Client:

Project:



..


QC Group

0304504-01 c X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

Run Sequence

XG.2003. 703.18

XG.2003. 703.18

XG.2003.703.18

XG.2003. 703.18

XG.2003.703.18

XG.2003.703.18

XG.2003.703.18

XG.2003.703.18

XG.2003.703.18

XG.2003.703.18

XG.2003.703.18

XG.2003.703.18

XG.2003.703.18

XG.2003. 703.18

XG.2003.703.18

XG.2003. 703.18

XG.2003. 703.18

XG.2003. 703.18

XG.2003. 703.18

XG.2003. 703.18

XG.2003. 703.18

XG.2003.703.18

XG.2003. 703.18

XG.2003.703.18

XG.2003. 703.18

XG.2003.703.18

·-·----·--------------·--~· ---------------

Collected: 04-22-03 13:50:00 By: SP

Dilution Detection


SW846 35108182708 SVOCs by GCIMS By: M/KAR

_2.8_1~8-~~0--8~-~---+l--___ B __ u_t~y-l_bc_e~-~-~-l~-~:-h_a_la_te __ ~_,_-·_---_-_-~---~----· ---+-r--·--~-~--~--~ f =-.1==~-. : -t -=.I 53-70_-3_.,._ ___ D_i_b_en_z_(_a,_h_)a_n_th_r_ac_e_n_e __ .,._ __ N_D ___ ,__u_g_t_C j~_ · 1-1

- __ ~- ___ i

132-64-9 Dibenzofuran ND ug IL I 1 1 •

84-66-2 Diethylphthalate ND ug I L I

131-11-3 Dimethylphthalate ND ug IL _j 1 84-74--2-+----d-i-n---B-u-ty-lp-h-th_a_la-te---+---N-D I ug IL I 1

117-84-0 di-n-Octylphthalate ND-T-u9/Lj- -1 ···--· -------+----j

206-44-0 Fluoranthene ND ' ug I L ; 1 l- - ·I - - ----+---------------______._._.J__ -------- ------

86737 --+----------- --·-·--···

Fluorene ND ug IL ' - - --------- ---- ~--

118-74-1 Hexachlorobenzene ND ug IL I

87-68-3_c--_ _l:l~-~~~~lorobutadiene . - ND==-=ug ll_:__[--__-77-47-4 Hexachlorocyclopentadiene ND ug IL I 10

i

-1 -1

67-72_-1_-j--___ H_e_xa_c_hl_oroet11_an_El_ -- ND _1 -~~L _ f- 5 j- -I

~98~~39~~5 lnden~~:·:~!~~~:yrene ~~ -~--~~< ~-··· 1- 1 1 t------j 91-20~3--i Naphthalene - - r-.ff:i" -- - ugTC-1 -- ( I 1 1- -J 98-95-3 Nitrobenzene ND ug IL 1- 1-- T- -- f- -t--- I

::1-~5~-~~~-7~-+:i ~--~~-n~~-~~N_i~t-i:~~-o~s:~~~~d~i~~~-~:t=_r:=_~=-1~-a=_l;=_m_i~~n=_ee=_ -~=-+~=--~=--~~=-~=--~=--~=+ -~=-~=-~=-~=-~=--~+"--. : 1 _•:__: I -86-30-6 n-Nitrosodiphenylamine ND ug I L 1 1

1

1

87-86-5 Pentachlorophenol ND .. f._ugTL- --1·---.---fo T ---!

,~f-~-.':_--"-~:-~ -~-1-+---,_ -_ ---.----~-=--h-=-:~:-~-:-;-;;-=--~-;-:~~-le~-n_e __ -=--=--=--=--=--=-~'::_-=_-=_-=_-=_~-=~=~----.. ·,...:-----~i-~-~----..,..1 =~ .. -~~.~.1--. -t.·.--.=-.=.-.-

~-------~-- -~~--- _ L H • m

By: ALG

Prep

Date

STAN DAR[

Run

Date

04-28-03 04-29-0:'"

04-28-03 04-29-03

04-28-03 04-29-0::..

04-28-03 04-29-0:'

04-28-03 04-29-03

04-28-03 04-29-0::..

04-28-03 04-29-0?

04-28-03 04-29-03 ' 04-28-03 04-29-o:r,

04-28-03 04-29-02'

04-28-03 04-29-03

04-28-03 04-29-0J<

04-28-03 04-29-0~'

04-28-03 04-29-03.

04-28-03 04-29-08

04-28-03 04-29-o:.

04-28-03 04-29-03

04-28-03 04-29-0::i

04-28-03 04-29-oc·

04-28-03 04-29-03

04-28-03 04-29-03,

04-28-03 04-29-0:'

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-0;

04-28-03 04-29-0:\

0304504-01 D

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

XG.2003. 785.15

XG.2003. 785.15

XG.2003. 785.15

XG.2003.785.15

XG.2003. 785.15

XG.2003.785.15

XG.2003. 785.15

XG.2003. 785.15

XG.2003. 785.15

XG.2003.785.15

XG.2003. 785.15

XG.2003.785.15

XG.2003. 785.15

XG.2003. 785.15

XG.2003. 785.15

SW846 35108/8081A Pesticides by GC/ECD :---·-~1-----a--B-H-C-----~--N-D--~-u_g_/_L_~---.. - --6.1

:--~ - - 1 04-29-03 05-08-03

Page 4 of 44

a-Chlordane ND ug I L 0.1

I 309-00-2 ! _A_ld_r_in ______ .,__ __ N_D ___ +- ug I L i 0.1 b-BHC ND ug I L 1 1 ~ - 0.1 - ------

57 .. _-7_4 ___ 9 _____ C_h_l_o~-~-~-~e-~-t-ot_a_l ___ r----~-~-=r ~~~ ~ r- ~--=- ~:~ _ -=-~-=

60-57-1 I Dieldrin ·---]--- ND -- ! ug/L J 1----:--01- -1 _J_-_~--~-~-=o-0=-~-l;-:n_n_I\ ___ -+--'~----------~--~ - -:: ;{ i: : ~ :_I_-- 1

Endosulfan Sulfate __ !'l.D_ _ ug I~ I 0~1 I I 72-20-8

1

1 Endrin ND --~_.':: J 1 _ _()~ 1 _ _ J Endrin Aldehyde ND ' ug I L 1 1 0.1 -- --- ---- f --- ~-+---- --~ - --

Endrin Ketone ND ug I L 1 1 0.1 _ ... j

g-BHC ND ug IL 0.1 , 58-89-9 -~-~~~- ------+------+---

.. ·---~-----~~_h_lo_rd_a_n_e ____ f---__ N_D __ ug IL 0.1

04-29-03 05-08-0(

04-29-03 05-08-03

04-29-03 05-08-03'

04-29-03 05-08-0:.

04-29-03 05-08-03

04-29-03 05-08-03'

04-29-03 05-08-0'.

04-29-03 05-08-0?

04-29-03 05-08-03

04-29-03 05-08-0'.

04-29-03 05-08-0~

04-29-03 05-08-03

04-29-03 05-08-0:

04-29-03 05-08-0?

SQLCoyote: Reports 1.0.0305281535)()( Report Date 6118103 2:07:09 PM

Client:

,=>roject:

Order:


APruL03SAMPLEEVENT



0304504 PHl16 Receipt: 04-23-03


11/latrix: GW

Dilution Detection


SW846 3510B/8081A Pesticides by GC/ECD By: ALG

Prep

Date

STANDARD

Run

Date

0304504-01 D

X03194

X03194

X03194

X03194

X03194

X03194

X03194

XG.2003. 785.15

XG.2003.785.15

XG.2003.785.15

XG.2003.785.15

XG.2003.785.15

XG.2003.785.15

XG.2003.785.15

76-44-8

1024-57-3

Heptachlor

Heptachlor Epoxide

ND ug IL

ug IL

- ---o~1 _ T ____ ! o4-29-o3 o5-08-o3

0304504-01 D

X03189

X03189

X03189

X03189

X03189

X03189

X03189

0304504-01 E

M03548

M03548

M03548

M03548

0304504-01 E

M03550

M03550

M03550

M03550

M03550

M03550

1\1103550

M03550

M03550

M03550

M03550

M03550

0304504-01 E

M03559

Page 5 of 44

XG.2003.750.6

XG.2003.750.6

XG.2003.750.6

XG.2003. 750.6

XG.2003.750 6

XG.2003.750.6

XG.2003.750.6

MT.2003.521.26

MT.2003.511.49

MT.2003.511.49

MT.2003.521.26

MT.2003.566.16

MT.2003.577.18

MT.2003.551.45

MT.2003.551.45

MT.2003.551.45

MT.2003.551.25

MT.2003.551.45

MT.2003.551.45

MT.2003.551.45

MT.2003.551.45

MT.2003.566.16

MT.2003.551.45

MT.2003.522.32

- -----

ND 0.1

72-43-5 Methoxychlor ND ug I L O 1

6088-51-3 ---p~p~Doo-------i--- ND -ug/L--+-- 1 0.1 -1 : ---c--------p~p-DDE--~--j\.fr). ug IL . . 1 .. +·---0·-:1·-- _._1·----=--J

8~~~~:~~2 ---- Tox:~~~~~tota1 -· --~- -~~ -1~-~ci ~-~ -r=i-=- -_ ~:~ -L--~~-i SW846 35108/8082 PCBs by GC/ECD By: ALG 12674-11-2 ! Aroclor 101-6 ---------ND r ugJLT- 1 i --o~s--T .. 1

111_04_=-2_8_-2~--- Aroclor 1~21 · ND_ __ J_ii~hm-+- ___ 1 +-o~--~--1 ~:::~~~~::_: ~;:~::; ~~!~ - . ~~ - ::; ~ I =- ~ I -~_J

' 12672-29-6 Aroclor 1248 I ND ug IL 1 0.5 F I ~~~:-:-::-2-9-:5-1--+---·-_--_·-------~-;-:-~-::-;-~~:~--~~-===t3~- --=t --~;~:- ~ _+~--~---[~--SW846 3005A/601 OA ICP By: JRE

I ~::~::~:~_; ----~_:_:o_Y m-l-liu_i-u:-... -.-.. _____ ! ___ oN~s- -

7440-48-4 I Cobalt - -:----ND- -i :ci ~ ~ +~~---~§b0o012 -----l

mg IL 0.01

74~0-50-8 c::-- Copper ND mg/L 0.01

SW846 3005A6020 ICP-MS By: HMR --0.001 -· I

~::~~f~~ 1-==-_-__ -_-A--~-::t~y- =~=~-----~-~ 7 44-c):'3-9-_3-l-

mg/L ND

o __ .o __ o_3 ___ .,.. _111g / L i 0.001

0.177 mg IL I 0.001 Barium

7440-43-9 Cadmium ---~=--~-°-~~+mg/I ---- _____ g o_o1 0.004 I mg I L 1 0.001

--~----------------

L 7 439-92-1 Lead -r--------- -~

7440-02-o Nickel 0.055 mg IL 10 0.001 ---- --------+---·

7782-49-2 Selenium 0.003 mg I L --------silVer____ ND___ 1- mg~~--____ _

Thallium ND I mg I L

I 7440-22-4

7440-28-0

Tin --ND ~-mg/ L 1 --

~::~~~:: ___ ~~--~~~u~-----' ---~-~~~ J-:; ~ ~ +=-~= l~ 7440-31-5


0.001 --

0.001

0.001

0.001

0.001

0.005

By:

]_ O.oo_o2 __ m_g_/_L_ -, --

' j_ --ND 7439-97-6 t Mercury

JRE

04-29-03 05-08-03

04-29-03 05-08-03

04-29-03 05-08-03

04-29-03 05-08-03

04-29-03 05-08-03

04-29-03 05-08-03

04-29-03 05-06-03

04-29-03 05-06-03

04-29-03 05-06-03

04-29-03 05-06-03

04-29-03 05-06-03

04-29-03 05-06-03

04-29-03 05-06-03

04-30-03 05-01-03

04-30-03 05-01-03

04-30-03 05-01-03

04-30-03 05-01-03

04-30-03 05-08-03

04-30-03 05-13-03

04-30-03 05-05-03

04-30-03 05-05-03

04-30-03 05-05-03

04-30-03 05-05-03

04-30-03 05-05-03

04-30-03 05-05-03

04-30-03 05-05-03

04-30-03 05-05-03

04-30-03 05-08-03

04-30-03 05-05-03

05-01-03 05-01-03

SQLCoyote: Reports 1.0.0305281535XX Report Date 6118103 2:07:28 PM

STANDARD



Client:

Project:



- --- ·---- ----Sample:

Matrix:

NCLF-5

GW

QC Group

0304504-02A X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

Page 6 of 44

Run Sequence

XG.2003.800.8

XG.2003.800.8

XG.2003.800.8

XG.2003.800.8

XG.2003.800.8

XG.2003.800.8

XG.2003.800.8

XG.2003.800.8

XG.2003.800.8

XG.2003.800.8

XG.2003.800.8

XG.2003.800.8

XG.2003.800.8

XG.2003.800.8

XG.2003.800.8

XG.2003.800.8

XG.2003.800.8

XG.2003.800.8

XG.2003.800.8

XG.2003.800.8

XG.2003.800.8

XG.2003.800.8

XG.2003.800.8

XG.2003.800.8

XG.2003.800.8

XG.2003.800.8

XG.2003.800.8

XG.2003.800.8

XG.2003.800.8

XG.2003.800.8

XG.2003.800.8

XG.2003.800.8

XG.2003.800.8

XG.2003.800.8

XG.2003.800.8

XG.2003.800.8

XG.2003.800.8

XG.2003.800.8

XG.2003.800.8

XG.2003.800.8

XG.2003.800.8

XG.2003.800.8

XG.2003.800.8

Collected: 04-22-03 15:30:00 By: SP



EPA 524.2 rev 4 Purgeable VOCs by GCIMS By: JAA 75-3~L 1, 1 Dichloroethane _ ND · l _ ug I L_TJ: ~ . 0.1_ - I __ -~ 05-06-03 05-07-03.

-75-~-- 1, 1 Dichloroethene _ ~ ND I~ L i _ ._1 __ -~' __ 0:1 --f Hj 05-06-03 05-07-03"·

71-55-6 i 1,1,1 Trichloroethane :---f---N~--=:) ug /~ __ 1_±-~- . · -j 05-06-03 05-07-03

':::: , : .:·.~ ~~:::~:~:~:"· . ~~ +~: : ~ t : . . · {: _ E' ~ -~ ~::~::~: ~::~; :~: - ;,::, 1 ';~;2D~::::::~~=oe ' . ~~ ..• . i . :: ; ~ , LI -~ : -= .•. · 1 :::,::: ::;;;:

106-93-4 1,2 Dibromoethane SEDB) I - ND~.- ug /.L-1 _}. .: --.. 0.1 .... -·-.f~~. ___,~ 05-06-03 05-07-03'

_9_!i:~°=-1_ 1,2 Dichlorobenzene ~--;-~~ __ ~- t__~1 . ___ 05-06-03 05-07-02~ 107-06-2 1,2 Dichloroethane (EDC) : . ND f ug IL : 1 . r 0.1 ' . . 05-06-03 05-07-03,

78-87-5 1,2 Dichloropropane --C ND ----=-+ ug I L--~~ ~ 1:-:__~ _0_:_1_ ~ +~~~~ 05-06-03 05-07-03

:~::~:~±= ~ .. ~ .. ~-~~:~~::~:~::::--~·· ---~~----;- ~~ ~-t----+- +--j --~}--+---1 ~::~::~: ~::~;:~~ ~:::.: ! ::;::~~~~~'~':::~: -1 - ~~ -~:;~ r--: f-rr=ri ::=: ::;;;: 96-12-8 1,2-DlbrOnio-3-chloropropar;e-·--ND--~-UgfL-+--1-=r-0.2- , ---

1 05-06-03 05-07-03

54H>1 1,3 D;ci1lombe"'eOe-1· ND I "'IL~, -- 1 -- - o~-- ~ -, 05-06-03 05-07-03

108-67-8 1 1,3,5-Trimethylbenzene •. -~ . ug?tt 1 -.··· -0.~ ~.-

1

. --~~-1 05-06-03 05-07-0:C

142-28-9 1,3-Dichloropropane .. ND i ug ~-- 1 - l--- 0.2_ . _ _ 05-06-03 05-07-03·

:;o; · : :~~:::;,:::: --t-:~ I ::;-~ j : ~: r---.-~ ~::~::~: ~::~;:~~-=~~t:.: I · 2,~--~~~~;~:i~::ne .• ~~- ~~ -~~- ' ~~·~ -~ l-~~~ F---~~F-= ~ ---~_] ~::~::~~ ~::~;:~:

I ';,;:; ~ __ 4-~~==r ~~-=W-~~~~ .1-- ~ -.. r- ~: i--.j ~::~::~: ~::~;:~: j1oa.:S6-1_ Bromobenzene --~ --~l--ug I L--~-1-~~ __ O~-y--_i 05-06-03 05-07-03

Bromochloromethane · ND I ug IL 1 I 0.1 1 05-06-03 05-07-0$

! i~~i-+--- Bromodichloromethane ~D ___ ,_ -~_§_~-f ___ 1___ 0.1 05-06-03 05-07 -0:'

05-06-03 05-07-03

05-06-03 05-07-0J

05-06-03 05-07 -O~-"

05-06-03 05-07 -03

05-06-03 05-07-0J

75-00-3 Chloroethane ND i ug IL 0.1 05-06-03 05-07-0C ---- -- ---- ---- -- ___ [ --- ---- -~ ---+---- - --~--

67-66-3 Chloroform .l ND 1

ug IL 1

1 0.1 05-06-03 05-07-03

· 74-~7-3_. -Ch!Oro~ ---__ L ND_=--Lig_~~l-~1 f-=~.:.1 -__ r_- 1 05-06-03 o5-o7-o~

I ~i~;', [ ,::·; \2 ~:~:~;:;:,: · :~ I :: ;s_ 1--- ' H- I _: ::::: :~:;;; · 74-95-3 • Dibromomethane ND 1 ~- _1 ---ii-i ·-=j 05-06-03 05-07-0J

i -100-414!· Ethylbenzene -~-- --u~!__'::__L_1_~ O~~-.=I___ • 05-06-03 05-07-0~ [ =75-7~ Freon 12 ND ··t'. ug IL , 1 0.1 05-06-03 05-07-03 I 87-68-3 Hexachlorobutadiene ND ug IL ;--- 1 0.1 05-06-03 05-07-03

98-82-8 lsopropylbenzene ND ug./ L L_ 1 r· 0.1 05-06-03 05-07-0:




Client:

?roject:



-- ----- -~~------·.


QC Group

0304504-02A X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

0304504-028 X03200

X03200

0304504-02C X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

Page 7 of 44

Run Sequence

XG.2003.800.8

XG.2003.800.8

XG.2003.800.8

XG.2003.800.8

XG.2003.800.8

XG.2003.800.8

XG.2003.800.8

XG.2003.800.8

XG.2003.800.8

XG.2003.800.8

XG.2003.800.8

XG.2003.800.8

XG.2003.800.8

XG.2003.800.8

XG.2003.800.8

XG.2003.800.8

XG.2003.727.24

XG.2003.727.24

XG.2003.703.19

XG.2003.703.19

XG.2003.703.19

XG.2003.703.19

XG.2003.703.19

XG.2003. 703.19

XG.2003. 703.19

XG.2003. 703.19

XG.2003.703.19

XG.2003. 703.19

XG.2003.703.19

XG.2003.703.19

XG.2003.703.19

XG.2003.703.19

XG.2003. 703.19

XG.2003.703.19

XG.2003.703.19

XG.2003.703.19

XG.2003.703.19

XG.2003.703.19

XG.2003. 703.19

------------ ----~---·- ----- -----------------

Collected: 04-22-03 15:30:00 By: SP



EPA 524.2 rev 4 Purgeable VOCs by GCIMS By: JAA 75-09-2

91-20-3

104-51-8

103-65-1

95-47-6

108-38-3/106-42

M~;:::::~:·---------+1- ~r---:rn 1: ~ ,--- :\--1~ -1 n-Propylbenzene ND ug_ TC -- _ 1 _! __ D.1 ____ - ------ - i

o-Xyle __ n_e ______ ~ __ ---ND____ _ug 1~_r=1--T __ o.1-_ _ ~ _______ PlrT1~Xylenes __ _!\JD___ ug IL _1 __ _1_L 0.2 l_ __ :

~ ~~~:~~! sec-B;1~::~:zene ~~ I ~: ~ ~T=- ~--r-3 ~ J :-: -156-60-5 1 t-1,2 Dichloroethene ND ! ug IL I 1 t 0.1

10061-02-6 ! _t-1,3 Dichloropropene N~--~~J_u_g ll_l __ 1 -1-~ 0._1_ -

98-06-6 i tert-Butylbenzene ____ _ ND 1 ug I L l _ 1 I-- 0_1 ____ J __ 127-18-4 Tetrachloroethylene2t 0.14 ug IL ' 1 ' O 1 11

1

108-88-3 Toluene - ND ug I L -+ 1 I 0.3 - --i,

79-01-6 _______ Trichloroethene _ _(): 12 _ i__u~ l_l____ 1 _ O 1 __ '

75-69-4 Trichlorofluoromethan~ _ _ __ N_D __ ~L ___ 1 I CJ_ 1___ __ 75-01-~----- __ ~inylchlonde ____ ND ug_IL_ _____ 1 __ L 0.1 _L__~

EPA 504 EDB/D8CP by GC/ECD By: ALG

[ _ -==[·--1-,2-Dibromo-3-chloropr~j)ane--. 1,2-Dibromoethane, EDB

-- ---- ---- ---

----------·

0.025 ND , ug IL ---- -------1-----

ND _L lJ_[J_~ L_ _ 0.025


05-06-03 05-07 -03

05-06-03 05-07 -03

05-06-03 05-07 -03

05-06-03 05-07 -03

05-06-03 05-07 -03

05-06-03 05-07-03

05-06-03 05-07 -03

05-06-03 05-07 -03

05-06-03 05-07 -03

05-06-03 05-07 -03

05-06-03 05-07 -03

05-06-03 05-07 -03

05-06-03 05-07 -03

05-06-03 05-07 -03

05-06-03 05-07 -03

05-06-03 05-07 -03

05-05-03 05-06-03

05-05-03 05-06-03

04-28-03 04-29-03 I 120-82-1

95-50-1

1,2,4-Trichlorobenzene -NNDD-,1

--uugg 11

-LL j--- 11

- ~ ___ _ 1 ,2-Dichlorobenzene I 04-28-03 04-29-03

i 541-73-1 1 _1,3-Dichl~robenzene 1· N __ D ___ 1

_ u~_l_l-_ _1~:__~ 1 • l 04-28-03 04-29-03

[ 1cJ6-4e.:7 1,4-Dichlorobenzene L ND ug IL j_ __ 1 [ __ i_ __ ~t-==-- -j 04-28-03 04-29-03

__ 9 __ 0-__ 1 __ 2-__ 0~ ___ 1-__ M __ e __ t_hylnaphthalene - ·1- ND I ug '-~ J__ 1 I 1 -+-_______j 04-28-03 04-29-03

58-90-2 2,3,4,6-Tetrachlorophenol 11

ND 1

ug IL : 1 1

5 i ! 04-28-03 04-29-03

95-95-4 1 2,4,5-Trichlorophenol ____ -~-°--' ~_l ____ 1 _ [ 5 I 04-28-03 04-29-03

88-06-2 2,4,6-Trichlorophenol ND ) __ u_gl_L-_J ___ 1 __ j_ 5 ~j--=-= 04-28-03 04-29-03

120-83-2 2,4-Dichlorophenol ND ' ug IL ~--- 1 I ___ ~-----+------ 04-28-03 04-29-03

105-67-9 1 2,4-Dimethylphenol ------+-- ND ' ug I L i----- 1 _]_ __ ~----+- ___ 04-28-03 04-29-03

51-28-5 j 2,4-Dinitrophenol NNDD uugg 1

1

LL I 11

_ ----1---~5~- --t-- _ , 04-28-03 04-29-03 121-14 2 [' 2,4-Dinitrotoluene 04-28-03 04-29-03

_6:1~~2:;2- ---- 2-~~~~:~~::~:~:~~e ~~ -~:-~~-+----~~---~ ---+=-: ~::~::~: ~::~::~: --+-------------------- ---- - - --- __ T _______ -- J I

95-57-8 2-Chlorophenol ND l ug IL i 1 : 1 · ' 04-28-03 04-29-03

~:~~ -'-~;~::~~:~:t-- --~~=~=i _j_~-rj ::::: :::::: 88-75-5 2-Nitrophenol ND ' ug I L 5 I 04-28-03 04-29-03

91-94-1 3,3-Dichlorobenzidine -ND----t--ug IL 1 () ---- - 04-28-03 04-29-03 - ___________ )_ --- -- ----

3+4 Methylphenol ND ! ug IL 04-28-03 04-29-03




Client:

Project:



Sample: NCLF-5

Matrix: GW

QC Group

0304504-02C X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

Page 8 of 44

Run Sequence

XG.2003. 703.19

XG.2003.703.19

XG.2003. 703.19

XG.2003. 703.19

XG.2003. 703.19

XG.2003.703.19

XG.2003.703.19

XG.2003.703.19

XG.2003.703.19

XG.2003.703.19

XG.2003.703.19

XG.2003.703.19

XG.2003.703.19

XG.2003.703.19

XG.2003.703.19

XG.2003.703.19

XG.2003.703.19

XG.2003. 703.19

XG.2003. 703.19

XG.2003. 703.19

XG.2003. 703.19

XG.2003.703.19

XG.2003.703.19

XG.2003.703.19

XG.2003.703.19

XG.2003.703.19

XG.2003.703.19

XG.2003. 703.19

XG.2003. 703.19

XG.2003. 703.19

XG.2003. 703.19

XG.2003.703.19

XG.2003.703.19

XG.2003.703.19

XG.2003.703.19

XG.2003. 703.19

XG.2003. 703.19

XG.2003.703.19

XG.2003.703.19

XG.2003.703.19

XG.2003. 703.19

XG.2003. 703.19

----- ----·---Collected: 04-22-03 15:30:00 By: SP

------------- - ---------

Dilution Detection



99-09-2 3-Nitroaniline ND I ug I L 1 5 I ' __ 5_3_4--5--2---1 -+---4-,6---D-in-it-ro---2--m-et_h_y_lp_h_e-no_l_-+-__ N_D ___ T_ ug IL-- ---1 --1-----10 --- -----

_1_0_1-_5_5-_3--+ __ 4_-B_r_o_m_o_p_h_e_n_yl_-p_h_e_n_y_le_th_e_r_-+-__ N_D __ +-11 _u_g_f_L_·,_·-_--:-1--=:1--____ 1 _____ -+ __ __,

59-50-7 4-Chloro-3-methylphenol ND i ug IL 1 5

106-47-8 4-Chloroaniline ND ' ug IL 1 5

7005-72-3 4-Chlorophenyl-phenylether I ND I ug I L -----1---+---1--+-------t 1··0--0--0-1--6---1----4---N-it-ro_a_n-il-in_e ___ ___,,- -·-·--N-D---+-1 -ug_/ _L~i---1--·--· - 5-

1 00-02-7 4-Nitrophenol ND -- t ·-u-g·-,-L-_.-_ --~--1---+--1 0------+------ -1

83-32-9 Acenaphthene ND I ug I L : 1 1 --------1--- --------------1.----·--------t-· ----~----- ----- - -----

208-96-8 Acenaphthylene ND I ug I L 1 1 -62~5·-3·--3--1------- Aniline ' . ND--r ug IL -- -1- + 10

120-12-7 Az~:~~:~:~~.2- - ~~~-=r;_~-~ rn-~- n ~-d ~ ·--- Diphenylhydrazine , · - -- _L_ --- - - ~---

------1-------------~--------~-----------

56-55-3 Benzo (a) anthracene ND ug I L 1 1 -------!--------------+-----------+----+-----·- ----·--- -

50-32-8 Benzo(a)pyrene ND ug I L ! 1 I 1

___ ]._ -·

------+-_-_ -B-e--nz_o_(_b_&_k_)_fl-uo_r_a_n_th·-e-ne---1----~-~----J: ~ ~-i: i ~ ~ : n =-~

~~~:, ~--··:::~~,=~~,, ~~ ----+-----~-~--~-~--+-t--__ L~-::----2t_~~ !------·-·

111-44-4 , bis (2-Chloroethyl) ether ND ug IL 1 ' 1

11_1_!_1_:_1_~2-Chloroethoxy)m_e_th_a_n_e_+--__ N_D___ I ug IL 1¥

1 108-60-1 bis(2-Chloroisopropyl)ether ND ~ ugfl - 1 1 ----- -- - - --- --r--------~

117-81-7 bis(2-Ethylhexyl)phthalate 5.6 i ug ~-- ,_____1_ 5 B

-~5:!3_~~7 Butylbenzy_lp_h_th_a_la_te _____ N_D_. _____ ~- ug IL 1 1 --+! _________ , Chrysene ND ug I L ! 1 1

----~---------------+,-----+---------+-------+-----1------t

53-70-3 Dibenz(a,h)anthracene ND ug IL 1 1 1 :

218-01-9

Prep

Date

Run

Date

04-28-03 04-29-02

04-28-03 04-29-03

04-28-03 04-29-0~

04-28-03 04-29-03

04-28-03 04-29-03'

04-28-03 04-29-o:.

04-28-03 04-29-02-

04-28-03 04-29-0:3'

04-28-03 04-29-0:..

04-28-03 04-29-0:> . 04-28-03 04-29-03

04-28-03 04-29-o:,

04-28-03 04-29-02

04-28-03 04-29-0~

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-0:

04-28-03 04-29-03

04-28-03 04-29-03"

04-28-03 04-29-0<.

04-28-03 04-29-0:'\

04-28-03 04-29-03

04-28-03 04-29-0:

04-28-03 04-29-0~

04-28-03 04-29-03'

04-28-03 04-29-0<.

132-64-9 Dibenzofuran ND ug I L ! 1 , 1 1 ! 04-28-03 04-29-0~

i _--2-~-=~=:;~--~·---~f----·---:-~-~~-,~-·~-{-f-'~-f-;.f ~ ~~ -:it~t1 -:J j ~jj'.~~ ~~~~~ 86737 Fluorene ND · ug I L : 1 _1 _ ___j___j 04-28-03 04-29-0?

1_8~-~~-7_8-~-~-1--~--:eexxa:ch~~~~bbu~:~~ennee_ --T ~~ ~;;~ -" 1 I . ~~ . _j_ ---l ~::~::~: ~::~::~: 77-47-4 1 Hexachlorocyclopent~_cl_i~~~-- 1 ND I ug IL 1 O _, ____ ! 04-28-03 04-29-07

67-72-1 Hexachloroethane ND ug IL 5 I 04-28-03 04-29-03

-193-3~--- lndeno~,3-cd)pyrene ND·-t-ug-TL-· _1__ ___ ::+-__:=_ 04-28-03 04-29-o:-

78-59-1 __ lsophorone I ND I ug I L _ _ _____ _, ____ 1 I 04-28-03 04-29-0:'

::::::: ' z,:~:~:::~: _ -__ I_ 3~ --! :lli_r- 1 • 1 :::::::: ::::::::

62-75-9 n-Nitroso-dimethyl-amine l ___ NI) __ L _u_gt_L ___ L 1 __ L_1_C} _ __j_ _____ J 04-28-03 04-29-07"

SQLCoyote: Reports 1.0.0305281535XX Report Date 6118103 2:11:23 PM··



Client:

i'roject:



Sample: NCLF-5

Matrix: GW

QC Group

0304504-02C

X03165

X03165

X03165

X03165

X03165

X03165

X03165

0304504-02D

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

0304504-02D

X03189

X03189

X03189

X03189

X03189

X03189

X03189

0304504-02E

M03548

M03548

Run Sequence

XG.2003.703.19

XG.2003.703.19

XG.2003.703.19

XG.2003.703.19

XG.2003.703.19

XG.2003.703.19

XG.2003.703.19

XG.2003.785.18

XG.2003. 785.18

XG.2003. 785.18

XG.2003. 785.18

XG.2003. 785.18

XG.2003. 785.18

XG.2003.785.18

XG.2003.785.18

XG.2003.785.18

XG.2003. 785.18

XG.2003. 785.18

XG.2003. 785.18

XG.2003.785.18

XG.2003.785.18

XG.2003.785.18

XG.2003. 785.18

XG.2003.785.18

XG.2003.785.18

XG.2003.785.18

XG.2003.785.18

XG.2003. 785.18

XG.2003.785.18

XG.2003.750.7

XG.2003.750.7

XG.2003.750.7

XG.2003.750.7

XG.2003.750.7

XG.2003.750.7

XG.2003.750.7

MT.2003.521.27

MT.2003.511.50

CAS# Analyte

SW846 35108/82708 SVOCs by GCIMS

621-64-7

86-30-6

Collected: 04-22-03 15:30:00 By: SP

Dilution Detection


n-n~~~~r:~:~~~::~:i:l::i:e u ru -~~--~ -~~~~ -=- -~ - ~-- -~ -87~86~5- --- ---rentaGillOrOPhenOI ____ 1- -- --ND- ug I L .. 1 I - 16 -----+-----~

85-01-8 Phenanthrene ------t--ND _____ -/L _____ 1 ___ I 108-95-2 ------Phenol-- ____ _J --ND- ~~/L 1- + 10

--+---------------- -

129-00-0 Pyrene . ND ug IL

110-86-1 ___ I _____ P_y_rid-in_e____ - - _i ___ ND - - - -ug/-i_


ul- ----:~;~~~~~n:· u --T -- -~~-- ug IL

ug IL

ug IL 309-00-2 Aldrin ND

b-BHC ND ug IL ! -5-7--7-4--9---l----C-hl-o-rd_a_n_e_, t-o-ta-1-----+---N-D ____ u_g_/_L ______ ------

d-BHC -- -- -- ---------------

60-57-1 Dieldrin

ND

ND

ug IL

ug IL

10

0.1

0.1

0.1

0.1

0.1

0.1

0.1

By: ALG

--+----------·---------------+-------~------------+-------+--------+--------

Endosulfan I ND , ug I L

--- --En-cia5U1Tail11=:-----=1=~E _ __i-u9_.t~_ Endosulfan Sulfate -----~- _ _f'JE_ _ __ lJ_9_~ L

72-20-8 Endrin i ND ug I L ---+----E-nd-r-in-A-ld-e-hy_d_e _____ T ____ ND_____ ug I L -

-----1-------------------- -Endrin Ketone ! ND ug I L

58-89-9 g-BHC - -r -- ND ug I L

0.1

0.1

0.1

0.1 ----- ------ -1

"·~~it:~f:"· ~~ -i ~m ~J 1--n~~=--76-44-8

1024-57-3

72-43-5

6088-51-3 p.p-DDD ---ND--~-ug/i.:-- - 0.1 -------1

p,p-DDE ND ug I L 0.1 I

50-29-3 -+------p.-p-_D_D_T --r--No-- -ug/L 0.1

8001-35-2 Toxaphene, total - - ___ f ___ N_D ________ -ugTL 2.5 -~---------------__J_- ------ --- - --------

SW846 35108/8082 PC8s by GC/ECD By: ALG

[ 12674:11·:2·· -- --Aroclor 1016- -- T ND ug IL 1_..j_ 0.5

! 11104-28-2 Aroclor1221 -~---~1--ND - __ ug~':__ 1 0.5

11141-16-5 Aroclor 1232 I ND ug IL - · 1·--[-- 0 5 :

; ;;ii~~~~~ . -. -il!;i, .. --r=-. ~-i-l> ~~-t ~~J-_ SW846 3005A/601 OA ICP

7440-41-7 Beryllium ______ T __ ND ___ m9/C 7 440-4-7--3-+------C-h_ro_m_i_u_m ______ J-_ !'J_[) ___ ~ rT19-'~-·--_ - -

By:

0.002

0.01

JRE

Prep

Date

STANDARD

Run

Date

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-29-03 05-08-03

04-29-03 05-08-03

04-29-03 05-08-03

04-29-03 05-08-03

04-29-03 05-08-03

04-29-03 05-08-03

04-29-03 05-08-03

04-29-03 05-08-03

04-29-03 05-08-03

04-29-03 05-08-03

04-29-03 05-08-03

04-29-03 05-08-03

04-29-03 05-08-03

04-29-03 05-08-03

04-29-03 05-08-03

04-29-03 05-08-03

04-29-03 05-08-03

04-29-03 05-08-03

04-29-03 05-08-03

04-29-03 05-08-03

04-29-03 05-08-03

04-29-03 05-08-03

04-29-03 05-06-03

04-29-03 05-06-03

04-29-03 05-06-03

04-29-03 05-06-03

04-29-03 05-06-03

04-29-03 05-06-03

04-29-03 05-06-03

04-30-03 05-01-03

04-30-03 05-01-03


Client:

Project:







Matrix: GW

Dilution Detection

STAN DARE'

Prep Run


0304504-02E

M03548

M03548

0304504-02E

M03550

M03550

M03550

M03550

M03550

M03550

M03550

M03550

M03550

M03550

M03550

M03550

MT.2003.511.50

MT.2003.521.27

MT.2003.566.17

MT.2003.577.19

MT.2003.551.46

MT.2003.551.46

MT.2003.551.46

MT.2003.566.17

MT.2003.551.46

MT.2003.551.46

MT.2003.551.46

MT.2003.551.46

MT.2003.566.17

MT.2003.551.46

SW846 3005Al6010A ICP

I .. 7440-48-4 I

7440-50-8 . -~--

SW846 3005A6020 ICP-MS By: HMR · 7440::3-6--0-------A-n-t-im_o_n_y _____ j___ ND mg I L 1 I 0.001 1 ·:

------+-----------------t------+----+ - -- -~------L__J 7440-38-2 Arsenic 0.002 mg IL 1 I 0.001 -~

~440-_3 __ 9-_3---+-----·--B __ ar_iu_m _____

1. _____ o __ ._1 __ 71_---t_m_g_l _L_-c---1- _ L _ 0~09~ __ --~

7440-43-9 _,__ _____ c_ad_m_i_um ND ___ mg IL 1 1 1 0.001 r=-- j 7439-92-1 Lead i ND mg IL ~ 1 0.001 , 7440-02-0 ---N-ic_k_e_l _____ t 0.002 ___ mg IL - - 1 0.001- ----j ---------+------- ------~• ------- · ··-· r - -1 778_~-4_9_-2_,__ _____ s __ el~~-iu_m ______ ~i ____ o_.002 ···---_mg IL _l _ _1_ __ ~_1_ __ l ______ J 7440-22-4 I Silver i ND mg IL I 1 0.001 I I

744-_o-_2_8_-_o-+1 ___ -::_-·-_T=h=a=l=liu=m=========--j-+--------N~--- mg IL I 1 J_ _ _():._~1__ __ i ____ J I Tin ND mg I L 1 0.001 I

-----------+--· --------------+-------7440-31-5

7440-62-2 Vanadium 0.002 mg IL 1 0.001 I

I 7440-66-6 Zinc ---N-D--+--m-g_/_L-+-1- -· - o:cios-- I --------'-------------+--------'-------~-~---~---~--~


04-30-03 05-01-0:.'

04-30-03 05-01-03

04-30-03 05-08-0:;-

04-30-03 05-13-0:.''

04-30-03 05-05-03

04-30-03 05-05-03•

04-30-03 05-05-0?

04-30-03 05-08-03.

04-30-03 05-05-03··

04-30-03 05-05-0:.'

04-30-03 05-05-03

04-30-03 05-05-03

04-30-03 05-08-0:'

04-30-03 05-05-03

0304504-02E

M03559 MT.2003.522.33 [ _ 7439-~ _____ M_er_c_u~ry _____ -+--__ N_D_ J: mg I L ~I ____ 0.0~~2 I ____ J 05-01-03 05-01-0:>


QC Group

0304504-03A

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

Page 10 of 44

Run Sequence

XG.2003.800.9

XG.2003.800.9

XG.2003.800.9

XG.2003.800.9

XG.2003.800.9

XG.2003.800.9

XG.2003.800.9

XG.2003.800.9

XG.2003.800.9

XG.2003.800.9

XG.2003.800.9

XG.2003.800.9

XG.2003.800.9

XG.2003.800.9

XG.2003.800.9

XG.2003.800.9

XG.2003.800.9

Collected: 04-22-03 16:45:00 By: SP

Dilution Detection



71-55-6 1, 1, 1 Trichloroethane i ND ug IL I 1 0.1 I 630-20-6 1, 1, 1,2 Tetrachloroethane , ND ug I L_J_ 1 0.1 1 I

79~0_0 __ -5_+---__ 1,_1_,2 Trichloroethane ND uugg 1

1 LL ,·, 11

~- __ 00_~_ 11 __

1,! _______ j,

79-34-5 1, 1,2,2 Tetrachloroethane ND I

--56-3--58-6 1, 1-Dichloropropene ND --1 -ug I L , 1 I 0.1 , ;

~:':,'~ , ~~~~:,:~::::~~~- ~~ i-:~:r ++=-~c, ... 107-06-2 1,2Dichloroethane(EDC)·-·1·--ND ug/i_ __ , 1 . 0.1 1

----------··---------1---- -----•·- --- j ____ --- - -----r-~---~

_ "78_!_7~~--~---1_,2_D_ic_hloropropane i ND .. _ j ug I L 1 I 0.1 ~-'

1,2,3 Trichloropropane ND · ug IL--·+·- _1 __ -1--~---~---j 96-18-4

87-61-6

120-82-1

95-63-6

96-12-8 -

' 541-73-1

1,2,3-Trichlorobenzene ND uugg 1

1

LL L 11

.. . ... ·-o~.--s~-- --~I __ -· -----~:·:· 1,2,4-Trichlorobenzene ND

1,2,4-Trimethylbenzene


1,3 Dichlorobenzene

ND

ND

ND

ug IL

ug IL

ug IL

0.1

1 I 0.2 -- --.-1·----- r- ----o .. :·1------

Prep Run

Date Date

05-06-03 05-07-0<

05-06-03 05-07 -03.

05-06-03 05-07-03

05-06-03 05-07-0<

05-06-03 05-07-03

05-06-03 05-07 -03

05-06-03 05-07 -O(

05-06-03 05-07 -03.

05-06-03 05-07-03°0

05-06-03 05-07 -Oc 05-06-03 05-07-03

05-06-03 05-07-03

05-06-03 05-07-0:'.

05-06-03 05-07-03

05-06-03 05-07-03.

05-06-03 05-07-0<,.

05-06-03 05-07 -0:.'

SQLCoyote: Reports 1.0.0305281535XX Report Date 6118103 2:12:50 PM.

Client:

?roject:







Matrix: GW

Dilution Detection

STANDARD

Prep Run


0304504-03A

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

;(03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

'/(03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

Page 11 of 44

XG.2003.800.9

XG.2003.800.9

XG.2003.800.9

XG.2003.800.9

XG.2003.800.9

XG.2003.800.9

XG.2003.800.9

XG.2003.800.9

XG.2003.800.9

XG.2003.800.9

XG.2003.800.9

XG.2003.800.9

XG.2003.800.9

XG.2003.800.9

XG.2003.800.9

XG.2003.800.9

XG.2003.800.9

XG.2003.800.9

XG.2003.800.9

XG.2003.800.9

XG.2003.800.9

XG.2003.800.9

XG.2003.800.9

XG.2003.800.9

XG.2003.800.9

XG.2003.800.9

XG.2003.800.9

XG.2003.800.9

XG.2003.800.9

XG.2003.800.9

XG.2003.800.9

XG.2003.800.9

XG.2003.800.9

XG.2003.800.9

XG.2003.800.9

XG.2003.800.9

XG.2003.800.9

XG.2003.800.9

XG.2003.800.9

XG.2003.800.9

XG.2003.800.9

XG.2003.800.9


0.1 - -~~:::::: 1 ·~::=~~~~1:~~~e- ] _ ~~- -=l ~: ~ ~ -=i--

~:;_; ~::-~::~~;,~;::;: : ~±-::;~ f ~.~ 594-20-7 2,2-Dichloropropane ND ___ j _ _lJ9_~_L-_ +- _ 1 _ 0.2

0.2

95-49-8 2-Chlorotoluene ND · ug I L I 1 , 0.1

106-43-4 I 4-Chlorotoluene ~~-==+-t-ug /L-=[: __ i.=- l 0.1

71-4~-2 _L Benzene N~--· . _ug_l~J __ 1_-l 0.1

108-86-1 Bromobenzene ND 1 ug IL ! 1 i 0.1 ------ -+------~--- - '

75-27-4

75-25-2

I 74-83-9

56-23-5

108-90-7

124-48-1

Bromochloromethane ND · ug IL ' 1 ! 0.1

Bromodichloromethane ND ug IL ~ -

' 0.1

Bromoform 0.18 i ug/L -~-------------"- --- -----4------- ~--1-

Bromomethane

Carbon tetrachloride

Chlorobenzene

Chlorodibromomethane

. ND , ug IL -- . . I· ·-· ---- ------------ -- -

-+=-B~-=~ ~~~~ -ND ug IL , 0.1

By: JAA

-i

::--::--:-:---+··_·-··---====c_c-hc=::-1-:_o-::=:=::=~-m-:-n-ee==-==~-------·+------_ ------~-.~---- :: ; ~ 'r~'-:_ ~ ~~~' --156-59-2 cis-1,2 dichloroethene _____ N __ D __ --+-_u_g_l_L _____ 1 _o_._~----

10061-01-5 cis-1,3 dichloropropene ND ug IL 1 0.1 1

-1-704-6~-45 __ 1_--_~4-::_~_--_--_-·_·--_--_D_i~-;-~Y-~-:e-:-:-:h-:_en_e _____ -+~------·-~-·~ - ~-~ci-~--~-+=-~----------:-. --~: ~ +---J ----------~----- 1···----'--- -- -j -- ------

75-71-8 Freon 12 ND ug/L , 1 0.1 ' --07 ___ 50---3~----H-e_x_a_c_h_lo_r_obutaciiene---------N--D----+---u-g- / L 0.1 I

' 97

85

--00

29

--02

lsopropylbenzene 1 ND uugg 1

1

LL ______ 1

1

___ _ 0

0

..

5

1 ~1 --~ Methylene chloride - ND 1

91-20-3 Naphthalene - l jD ug IL 104-51-8 n-Butylbenzene ND -- r- ug IL -- -1-- 0.1

103-65-1 - -----n-Propylbenzene N-D--~-ug I L1 - ____ , _____ o--.-1·---

95-47-6 - --o-X:yle-ne - - -- --No-IUgTi_ 1 -- -- - ---- - ,----

108-38- p/m-Xylenes __ N~-~1_u~~----_1 __ 3/106-42

~~~::::: --·- sec-B~t~;~~:zene ---- I ~~- -----~~ ~ ~ --+------------------1- - l-------------1--------;

156-60-5 t-1,2 Dichloroethene I ND I ug I L . 1 -------·--·-·-- ···········----··--·---------r--------·- -- : ----

10061-02-6 t-1,3 Dichloropropene ~ N[)_ ___ J -~g IL i _1 __ 0.1

~9::~:~ I T::~:r:::~~~' -- ~~ -m tm:: ~~~1~- ... -~~ 79-01-6 j Trichloroethene NN·---~D--------1--~u_g9_ 1

1

LL__ 1 0

0 .. 11

75-69.4-T Trichlorofluoromethane - -----·-------·-·---- ---· ---+-------+---- t· .. -----~· ----· ·-

75:~~~-- _________ -'-'~~chlor~ ND ' ug I L _! _ _1__l_ ___ o~

05-06-03 05-07 -03

05-06-03 05-07 -03

05-06-03 05-07 -03

05-06-03 05-07-03

05-06-03 05-07 -03

05-06-03 05-07 -03

05-06-03 05-07 -03

05-06-03 05-07 -03

05-06-03 05-07 -03

05-06-03 05-07-03

05-06-03 05-07-03

05-06-03 05-07-03

05-06-03 05-07 -03

05-06-03 05-07 -03

05-06-03 05-07 -03

05-06-03 05-07 -03

05-06-03 05-07-03

05-06-03 05-07-03

05-06-03 05-07 -03

05-06-03 05-07-03

05-06-03 05-07 -03

05-06-03 05-07 -03

05-06-03 05-07 -03

05-06-03 05-07-03

05-06-03 05-07-03

05-06-03 05-07-03

05-06-03 05-07-03

05-06-03 05-07 -03

05-06-03 05-07-03

05-06-03 05-07-03

05-06-03 05-07-03

05-06-03 05-07 -03

05-06-03 05-07 -03

05-06-03 05-07 -03

05-06-03 05-07 -03

05-06-03 05-07 -03

05-06-03 05-07 -03

05-06-03 05-07 -03

05-06-03 05-07-03

05-06-03 05-07-03

05-06-03 05-07-03

05-06-03 05-07-03


Client:

Project:






---· ---·----------·----Sample: NCLF-7 Collected: 04-22-03 16:45:00 By: SP

Matrix: GW

STANDARD

--------- --···-------

QC Group

0304504-038 X03200

X03200

0304504-03C X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

Page 12 of 44

Run Sequence

XG.2003.727.25

XG.2003.727.25

XG.2003. 703.20

XG.2003.703.20

XG.2003.703.20

XG.2003.703.20

XG.2003.703.20

XG.2003.703.20

XG.2003. 703.20

XG.2003. 703.20

XG.2003.703.20

XG.2003. 703.20

XG.2003. 703.20

XG.2003.703.20

XG.2003.703.20

XG.2003.703.20

XG.2003. 703.20

XG.2003.703.20

XG.2003.703.20

XG.2003.703.20

XG.2003. 703.20

XG.2003. 703.20

XG.2003. 703.20

XG.2003.703.20

XG.2003.703.20

XG.2003.703.20

XG.2003. 703.20

XG.2003. 703.20

XG.2003.703.20

XG.2003.703.20

XG.2003.703.20

XG.2003. 703.20

XG.2003.703.20

XG.2003.703.20

XG.2003.703.20

XG.2003. 703.20

XG.2003.703.20

XG.2003.703.20

XG.2003.703.20

XG.2003. 703.20

Dilution Detection


EPA 504 ED8/D8CP by GC/ECD . . . . _ .. _ By~ _ ALG

I

___ 1,2-Dibromo-3-chloropropane+~-- ND___ r~gTL -~ .. _1 _ __j__0.025.· =---- 1 1,2-Dibromoethane, EDB __L_~ ~~ __ 1_j_ 0.02~_l__ __ _]

SW846 35108/82708 SVOCs by GC/MS By: M/KAR

- 120.-82-1 1,2,4-T ri<hloroboo,eoe__J ND -- - :. ug I _l-_ I -. 1 J- . - -1. -. _j___] ___ _::_-:_0-1 . 1,2-Dichlorobenzene __ ~_D ___ ~s+L __ 1 _______ 1__ -+--~·

541-73-1 1,3-Dichlorobenzene J _ ___l'JD ug IL 1 1 __L___ _100-'6-7 I _ 1,4-Diohlorobe"eoe _ ' - NO _ -~ "' i j_ I - 1 _ 1-- 1 -__ --_I_~ _ ~:: , 2 ;,::~::::;~::::h:ool -.1 -- ~~ _ •I ~~ ;_~ .' +-. . i _ . ~--- ~ _' - -~-,

95-95-4 2,4,5-Trichlorophenol ND ! ug IL 2=1= 5

- as~06-2 2,4,6-Trichlorophell_Cll___ 1 - ~-- ug /-~~-}+ -~=--

1

120-83-2 2,4-Dichlorophenol ND ug IL · 1 . 5 j_. , -105-67-9 2,4-Dimethylphenol ND ug IL 1 -.-~_ ~:_ 51-28-5 2,4-Dinitrophenol ND '. ug IL H 10 121-14-2 2,4-Dinitrotoluene ND 1 ug IL --1-- ___ 5 ___ 1 ---

6901~~28~;2 2-~~~~:~~t:~~:~:l~~e -1---- ~~ I ~~; ~ -t-~ - ~ ~ - ~ --+ --1 95-57-8 _ 2-Chlorophenol -=-=i __ _r.JD - ~ _ ~ ug IL ~ 1--- ~1 ~r~l

_91-57-6 I 2-Methylnaphthalen_e ____ ___f\l[) ___ . LI!]~J_ 1_L_1 ___ ! ___ j :5-4~~+---- 2-Methylphenol _ -t--- _t-1!>__ }i

1

_ ""--'--' 1

_,__: _,_ __ r---~ __ 88~~4-4

1___ 2-Nitro_aniline ___

1 _ ND ___ ,_u~-q- _ 1 : ___ 5__ -1

:::::: i n '-~~;~::::::~:· =-: ~!--- ' 1ffi- ~- ! - ,:,- - -H c

99.:0~~ 3-Nitroaniline i ND ug / L ' -1--r- 5 --:-- --534-52-1 4,6-Dinitro-2-methylphenol ND ug I L :---1 -r --10----t------1

·----101-55-3 4-Bromophenyl-phenylether ND ug I L ' 1 1

59-50-7 4-Chloro-3-methylphenol ND I ug I L 1 , 5 106-47-8 4-Chloroaniline --+-----ND I ug_/_L--+-1 --15 ------

~::: • 4-Chlo:~::::~thec -; _ -~~ f:fil-'=f-+-l- 1 ~-~ 83-3-2--9~1-- Acenaphthene __ NNDD -i uu

9g

1

1 LL H=+1 --·- ' ··-~1 __ . --------· • -2o8-9~-8-~ Acenaphthylene .

62-5 1 10 • : 120- _ 1 ___ ;___1 ___ ~. ---i

-3-3 Aniline ND ug IL '

12-7

--

---56-5

50-3

5-3

2-8

191-24-2 I

Anthracene

Azobenzene&1,2-Diphenylhydrazine

Benzo (a) anthracene

Benzo(a)pyrene --

Benzo(b & k)fluoranthene ·-·

Benzo(g, h, 1 )perylene --~.

1_-_ c [--j ND ug IL I

ND ug IL I

ND ug IL ~ --

ND ug IL "

ND ug IL I --- -----·-

ND ____ l _LJ(l _l_L

Prep

Date

05-05-03

05-05-03

04-28-03

04-28-03

04-28-03

04-28-03

04-28-03

04-28-03

04-28-03

04-28-03

04-28-03

04-28-03

04-28-03

04-28-03

04-28-03

04-28-03

04-28-03

04-28-03

04-28-03

04-28-03

04-28-03

04-28-03

04-28-03

04-28-03

04-28-03

04-28-03

04-28-03

04-28-03

04-28-03

04-28-03

04-28-03

04-28-03

04-28-03

04-28-03

04-28-03

04-28-03

Run

Date

05-06-03,

05-06-03•

04-29-02·

04-29-03,

04-29-03'

04-29-02,_

04-29-03,

04-29-03"· . 04-29-0Z

04-29-03

04-29-03'

04-29-0<

04-29-03

04-29-03'

04-29-0<

04-29-0~

04-29-03'

04-29-0:>.

04-29-0~

04-29-03'

04-29-0~.

04-29-0~ ..

04-29-03

04-29-0~.

04-29-0?

04-29-03

04-29-00

04-29-0:'

04-29-03

04-29-0::r

04-29-0:"

04-29-03

04-29-0::.

04-29-0'.'

04-29-03_

04-29-03'

04-28-03 04-29-03

04-28-03 04-29-0~.

04-28-03 04-29-0?

04-28-03 04-29-03


Client:

?roject:


AP~L03SAMPLEEVENT




- -


Matrix: GW

Dilution Detection

QC Group

0304504-03C

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

0304504-03D

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

Run Sequence

XG.2003. 703.20

XG.2003. 703.20

XG.2003. 703.20

XG.2003.703.20

XG.2003.703.20

XG.2003.703.20

XG.2003. 703.20

XG.2003.703.20

XG.2003.703.20

XG.2003.703.20

XG.2003.703.20

XG.2003.703.20

XG.2003.703.20

XG.2003.703.20

XG.2003.703.20

XG.2003.703.20

XG.2003. 703.20

XG.2003. 703.20

XG.2003. 703.20

XG.2003.703.20

XG.2003.703.20

XG.2003.703.20

XG.2003.703.20

XG.2003. 703.20

XG.2003. 703.20

XG.2003. 703.20

XG.2003.703.20

XG.2003.703.20

XG.2003.703.20

XG.2003. 703.20

XG.2003. 703.20

XG.2003. 703.20

XG.2003.785.19

XG.2003. 785.19

XG.2003. 785.19

XG.2003.785.19

XG.2003.785.19

XG.2003.785.19

XG.2003.785.19

XG.2003.785.19

XG.2003. 785.19


SW846 35108/82708 SVOCs by GCIMS ---- - ------- 1 ------,---- --- -

Benzoic acid ND 1 ug I L I 1 25

100-51-6--t----B-e-n-zyl alcohol - -ND----rug I L --P. ] 5

64-85-0

111-44-4 --~is (2-Chloroethyl) eth:r ~-ND __ ::::_:I::Ug IL_:: --1~~-- 1

-11-1--9-1--1-+-bis(2-Chloroethoxy)methane ND I ug IL 1 1

108-60-1 bis(2-Chloroisopropyl)ether ND-- - f UQ7L-:-1·--; 1

! 117-81-7 ------

85-68-7

218-01-9

53-70-3

132-64-9

84-66-2

131-11-3

84-74-2

117-84-0

---· Dimethylphthalate

di-n-Butylphthalate

di-n-Octylphthalate

206-44-0 I Fluoranthene -~-------

86737 Fluorene - . -

118-74-1 i Hexachlorobenzene - --· -87-68-3 Hexachlorobutadiene

ug IL

--·--

ND ug IL --------

ND ug IL ·--- -----~---- --------- ---

77-47-4 Hexach lorocyclopentad iene

67-72-1

193-39-5 ----------·--78-59-1

91-20-3

98-95-3

Hexachloroethane

lndeno(1,2,3-cd)pyrene

lsophorone

Naphthalene

Nitrobenzene -t------------

--

62-75-9 n-Nitroso-dimethyl-amine

621-64-7 n-Nitroso-di-n-propylamine --+------

86-30-6 n-Nitrosodiphenylamine

87-86-5 Pentachlorophenol

--- -I __ J

-----------+-85-01-8 Phenanthrene

108-95-2 ' Phenol --------t------129-00-0 1 Pyrene

~ 10-8~1_ _ _1_ _ Pyridine


ND ug IL ---·-- -------

ND ug IL

ND ug IL ··-

----T a-BHC --- --~, - ___ N_D_ - -ug IL

a-Chlordane ND _t_ _ __LJQ_~~ 309-00-2 ; Aldrin ND 1 ug IL

--~D ---4:::ug~TL:

__ ;__ ~~---H~~-t ND ___ r

b-BHC

57'7:~~~9 ' Chlordane, total d-BHC

---------- - -- - - --- ---60-57-1 Dieldrin

-- -------·- ---------+--

' Endosulfan I

I ----- ~=-- Endosulfan II

-, I 0.1

0.1

0.1

0.1

0.1

0.1

By: M/KAR

By: ALG

STANDARD

Prep Run

Date Date

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-29-03 05-08-03

04-29-03 05-08-03

04-29-03 05-08-03

04-29-03 05-08-03

04-29-03 05-08-03

04-29-03 05-08-03

04-29-03 05-08-03

04-29-03 05-08-03

04-29-03 05-08-03

Page 13 of 44 SQLCoyote: Reporls 1.0.0305281535)()( Reporl Date 6118103 2:14:49 PM



Client:

Project:



---------------·-- -----· ---------- ·-----Sample: NCLF-7 Collected: 04-22-03 16:45:00 By: SP

Matrix: GW ---------···-------- --------

QC Group

0304504-03D X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

0304504-03D X03189

X03189

X03189

X03189

X03189

X03189

X03189

0304504-03E M03548

M03548

M03548

M03548

0304504-03E M03550

M03550

M03550

M03550

M03550

M03550

M03550

M03550

M03550

M03550

M03550

M03550

Run Sequence

XG.2003.785.19

XG.2003. 785.19

XG.2003.785.19

XG.2003.785.19

XG.2003.785.19

XG.2003.785.19

XG.2003. 785.19

XG.2003.785.19

XG.2003. 785.19

XG.2003. 785.19

XG.2003.785.19

XG.2003. 785.19

XG.2003.785.19

XG.2003. 750.10

XG.2003. 750.10

XG.2003. 750.10

XG.2003.750.1 O

XG.2003. 750.1 O

XG.2003.750.1 O

XG.2003.750.10

MT.2003.521.28

MT.2003.511.51

MT.2003.511.51

MT.2003.521.28

MT.2003.566.18

MT.2003.577.20

MT.2003.551.47

MT.2003.551.47

MT.2003.551.47

MT.2003.566.18

MT.2003.551.47

MT.2003.551.47

MT.2003.551.47

MT.2003.551.47

MT.2003.566.18

MT.2003.551.47

Dilution Detection


SW846 3510818081A Pesticides by GC/ECD By: ALG I Endosulfan Sulfate 1 ~~ _pm 1-r_~ ~1- - ----

72-20-8 Endrin ----- --

Endrin Aldehyde --------~--

Endrin Ketone ND ug IL 1 0 1 - -- ____ I - - -- ---- ---

58-89-9 g-BHC __ ND I ug IL 1 _____ 0.1_ ---------I ----

I g-Chlordane ND ug I L 1 : 0.1

I - - . -- -------r------ -------

76-44-8 i Heptachlor ND ug IL 1 0.1 ---- ---·-·t-· -

I 1024-57-3 I Heptachlor Epoxide ND ug IL 1 ! 0.1 - - -··-------·--

I i 72-43-5 Methoxychlor ND ug IL 1 I 0.1

------ 1--1 6088-51-3 I p,p-DDD ND ug IL 0.1 ---- --- --------

I p,p-DDE ND ug IL 1 I 0. 1

50-29-3 i p,p-DDT ND ug IL 1 i 0.1 ----- ----------

8001-35-2 I Toxaphene, total ND ug IL 1 I 2.5 ---


112674-11-2 I Aroclor 1016 I ND j ug IL I 1 1 O 5 +- i

i 11104-28-2 i Aroclor 1221 --t ND ! ug I L [ - 1 --1----o:s -- ---1 11141-16-5 i -A-ro-c-lo_r_1_2_32 ___ -~~t-=-~NE0 __ =:

1_ uugg~/~LL~ II - 1

1 --~1, 0

0 .. 55

- _f __ _ } 53469-2-1=91- - Aroclor 1242 -1 ~ ~~:~::::~ I ~~~~:~~ ~ ~:: ~ ~~- -- - -: ~T--~ _-- ~- ~~~ --~ 1109_6 __ -_8_2-_5~ ____ A_r_oc_l_or_1_2_6_0 ___ ~ ___ N_D ug IL [__1_~· _0._5 __ ~Lj

SW846 3005A/6010A ICP By: JRE

7440-41-7 Beryllium I ND mg/L 1 1 0.002 I i ---------

I

! 7440-47-3 Chromium I ND mg/L 1 0.01

---7440-48-4 Cobalt ND mg/L 1 0.01

- ------ , __

7440-50-8 Copper ND mg/L 1 0.01 -- -- --- --- L_ __

__________ I

SW846 3005A6020 ICP-MS By: HMR ------------------------------------7440-36-0 Antimony ND _j___rT1Q_~_L _1 __ H_U():~_1 _ _J___ __ _J

::-:-:--:~:-~-:-~:~~~~~~~~-c-A_B_a_:-s_:_iu-n_i~~:~~~------+ 1' __ ~_:_1~-~--"J __ ~ __ : __ ; __ ~----·--- ~- ·-. i t= 7439-92-1 Lead ND I mg IL 1 0.001 !

-----+--------------f------~i---'-----+---+-------l-----7440-02-0 Nickel 0.002 . mg IL 1 0.001

7782-49-2 Selenium 0.001 I mg IL 1 0.001

7440-22-4 Silver ND 1 mg IL 1 0.001 --------+------------------- -------'------ --- -~--·-·-·-·· ----------------+---7440-28-0 Thallium ND I mg IL 1 0.001 -------1------------------J___·----- ---'=---__J__ ___ ___J _______ --.. -~ --

7440-31-5 I Tin ND ! mg IL +---~-- 0.~01

7440=~~~~1 ____ v_a_n_ad_i_um__________ _Cl_:0Cl_3 _ i~ ~m-gg 1

1

LL ! 1 _ _CJ_.001_--+-- __ 1 7440-66-6 Zinc ND __ ___ _ _ j_ Cl_:9()5 _ _L ___ j SW846 7470 Mercury by CVAA By: JRE

Prep

Date

STANDARD

Run

Date

04-29-03 05-08-03

04-29-03 05-08-03' -

04-29-03 05-08-02

04-29-03 05-08-03_

04-29-03 05-08-03""

04-29-03 05-08-0:'

04-29-03 05-08-03.

04-29-03 05-08-03"

04-29-03 05-08-0{

04-29-03 05-08-03'

04-29-03 05-08-03''·

04-29-03 05-08-0~ .

04-29-03 05-08-02 -

04-29-03 05-06-03

04-29-03 05-06-0:C

04-29-03 05-06-0~

04-29-03 05-06-03

04-29-03 05-06-03

04-29-03 05-06-0<'

04-29-03 05-06-03,

04-30-03 05-01-0:,

04-30-03 05-01-0:>

04-30-03 05-01-03

04-30-03 05-01-0:>.,

04-30-03 05-08-02

04-30-03 05-13-03

04-30-03 05-05-0'.;-

04-30-03 05-05-0:c

04-30-03 05-05-03

04-30-03 05-08-o;-,.

04-30-03 05-05-0::

04-30-03 05-05-03

04-30-03 05-05-03

04-30-03 05-05-0Z

04-30-03 05-08-03

04-30-03 05-05-03

0304504-03E M03559 MT.2003.522.34 7439-97=6T ______ Mercury ___ - _____:]_~--ND-_~ mg IL - 1 - : 0.0002 r---~ 05-01-03 05-01-0:

---- _l__ ________ _J____ --


STANDARD



Client:

Project:



-----


QC Group Run Sequence

Sample:

Matrix:

NCLF-6

GW

QC Group

0304504-04A

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

:X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

Page 15 of 44

Run Sequence

XG.2003.800.10

XG.2003.800.10

XG.2003.800.10

XG.2003.800.1 O

XG.2003.800.10

XG.2003.800.10

XG.2003.800.10

XG.2003.800.10

XG.2003.800.10

XG.2003.800.10

XG.2003.800.10

XG.2003.800.10

XG.2003.800.10

XG.2003.800.10

XG.2003.800.1 O

XG.2003.800.10

XG.2003.800.10

XG.2003.800.10

XG.2003.800.10

XG.2003.800.10

XG.2003.800.10

XG.2003.800.10

XG.2003.800.10

XG.2003.800.10

XG.2003.800.10

XG.2003.800.10

XG.2003.800.1 0

XG.2003.800.10

XG.2003.800.10

XG.2003.800.1 o XG.2003.800.10

XG.2003.800.10

XG.2003.800.1 o

XG.2003.800.10

XG.2003.800.1 0

XG.2003.800.10

XG.2003.800.1 0

------------- --- ..

Collected: 04-22-03 16:45:00 By: SP

Dilution Detection

CAS# Analyte Result Units Factor Limit

Collected: 04-22-03 18:00:00 By: SP

Dilution Detection

CAS# Analyte Result Units Factor Limit

Code

Prep

Date

Run

Date

Prep Run

Code Date Date


-~~fI==-=--~~~~:------~-~- ~=~*=[>_}~-!-=~~ ~:~ -_r_ __ J ~::~::~: ~::~~:~: :~~~;~~-~ 1, 1\1.'~ ~~~~:~o;l:~::~~=ne ~~ ~u~g ;/ ~L I ~1 t, --==·~0:.--~1 ___ 1__ ·-··-Jji ~::~::~: ~::~~:~: 79-00-5 1, 1,2 Trichloroethane ND T 05-06-03 05-07-03

7_~-34-5 1, 1,2,2 Tetrachloroethane ND ug IL

1

__1___ _ 0.1 _:_ ____ j 05-06-03 05-07-03

~~:::::: 1,21

~i~~~:~o:;::~~~~~B) ~~ ~~; ~ ~---- - ~:} -~1 ~::~::~: ~::~~:~: 95-50-1 1,2 Dichlorobenzene ND ug IL - +-- 1-------,----Cl-1 I 05-06-03 05-07-03

~:;;_ 121~~;;;~c1 j- ~~--- ~J ::H=--:-=-~H ::::::: :~~;:: 96-18-4 1,2,3 Trichloropropane · _ ND 1 ug/ L J 1 . 0.1 _L 05-06-03 05-07-03

87-61-6 1,2,3-Trichlorobenzene 1 ND 1-ug~_L-__J 1 ----+-- 0.5 __ L _____ j 05-06-03 05-07-03

_ 120-8~~~--1_,_~.-~~~~~~:_ri_z_~~~ ND _ ___ ~~}L I 1

0.5 [ __ j 05-06-03 05-07-03

;,~;~ , "~i~7~~:::::,. ~~ :: ; ~ _ l1--_~_--_=:1-_ -_-_- ~·~ -- • ~ -I :::::::: ::::; ~: 108-67-8 1,3,5-Trimethylbenzene ND ---c- u9/L , _ 0.1 · - 05-06-03 05-07-03

142-28-9 1,3-Dichloropropane ND ug IL i 1 O 2 - - - 05-06-03 05-07-03

106-46-7 ___ 1_:~~~~~~ri_e j ND f ug I L r---1--- - o: 1 --l-=~~ 05-06-03 05-07-03

;:L __ ~:}~F,~ii,::::: __ -] ------~~- _J :u ! , ~·~--~ _j :::::: :::;~: 106-43-4 4-Chlorotoluene __ J_ __ ~_[)__-i _ _ll_g_i_L __

1 _ __ O 1 _ L __ .J 05-06-03 05-07-03

71-43-2 Benzene I ND I ug IL i 1 0.1 • 1 05-06-03 05-07-03 - - r----;-;----1-----------,------j

108-86-1 Bromobenzene ND 1

ug IL i 1 0.1 , 05-06-03 05-07-03

Bromochloromethane ND ! ug IL--- - 1- - --- -6~1 -- --- 05-06-03 05-07-03 -------j-----------'-------

75-27-4 Bromodichloromethane ND ' ug IL 1 I O 1 05-06-03 05-07-03

---~-:-:~-:-::-+---- ::::::-~ 0~~ :_ :u~g ;/ ~L ' =ct=1 ~0-.:~1- --:,-- -- - ~::~::~: ~::~~:~: 56-23-5 Carbon tetrachloride -e--ND -~- f- - 05-06-03 05-07-03

---·---+-------------+-----___,------------+----108-90-7 Chlorobenzene

124-48-1 Chlorodibromomethane ------+-----·--·-··------------------ -·-

75-00-3 Chloroethane

67-66-3 Chloroform -----+---- --------------74-87-3 Chloromethane

156-59-2 cis-1,2 dichloroethene

SQLCoyote: Reports

I ..

ND ug IL

ND ug IL - ND - T ~1i:

ND

ND

ND

l _ ug IL ug IL

ug IL

1.0.0305281535XX

_ _1_ j_ __ 0:_1_ --- --- 05-06-03 05-07-03 1 . 0.1 ' 05-06-03 05-07-03

1 0.1 __ ;_ __ , 05-06-03 05-07-03

o. 1 I 05-06-03 o5-o7 -03 -- -- - -- _,_ --- - -- --- ----- - -- -1

0.1

0.1

Report Date

05-06-03 05-07 -03

05-06-03 05-07 -03

6118103 2:17:43 PM



Client:

Project:



Sample: NCLF-6

Matrix: GW

QC Group

0304504-04A X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

0304504-048

X03200

X03200

0304504-04C

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

Run Sequence

XG.2003.800.10

XG.2003.800.10

XG.2003.800.10

XG.2003.800.1 O

XG.2003.800.10

XG.2003.800.10

XG.2003.800.10

XG.2003.800.10

XG.2003.800.10

XG.2003.801.1

XG.2003.800.1 0

XG.2003.800.10

XG.2003.800.10

XG.2003.800.1 o

XG.2003.800.10

XG.2003.800.10

XG.2003.800.10

XG.2003.800.1 O

XG.2003.800.1 O

XG.2003.800.10

XG.2003.800.10

XG.2003.800.10

XG.2003.727.26

XG.2003.727.26

XG.2003.703.21

XG.2003.703.21

XG.2003.703.21

XG.2003.703.21

XG.2003.703.21

XG.2003.703.21

XG.2003.703.21

XG.2003.703.21

XG.2003.703.21

XG.2003.703.21

XG.2003.703.21

XG.2003.703.21

XG.2003.703.21

XG.2003.703.21

XG.2003.703.21

Collected: 04-22-03 18:00:00 By: SP

Dilution Detection


EPA 524.2 rev 4 Purgeable VOCs by GCIMS By: JAA : 10061-01-5 cis-1,3 dichloropropene , N_D __ -+-i _u_g_l_L _____ ~_0.1 +=-1

I

I

i

74-95-3

00 41 4 1 - -75-71-8

- ---------87-68-3

98-82-8

75-09-2

91-20-3

104-51-8

103-65-1

i !

---------------Dibromomethane ___ :__ __ ._l'J[)__ j ug IL 0 1 · I

E . ND --r ----~ I ~·~ rn I -~-t~:~

1 I 1 - __ _j - - - - -l -- --1

thylbenzene i ug IL i

Freon 12 ______ J ND i ug IL ! ---

Hexachlorobutadiene I ND ug IL I I

lsopropylbenzene ND ug IL ------

Methylene chloride ND ug IL !

c Naphthalene ND ug IL

---- -------+------------1 I 0.1 I I n-Butylbenzene ND I ug IL

------ --------]·-----------n-Propylbenzene ND ! ug IL !

I '

~---1 -1---a.1 ·--:--1 ug I L 1 1 I 0.1 1 1

__ ~g ~t.-1 _- -1-= }~ o 2_- -~----~ 95-47-6 1 o-Xylene ND

--------C-----

108 -38 - .1

_______ p/m-Xylenes ND 3/106-42 ------~----

135_-9_8_-8--f ____ sec-_Butylbenzene 1 _l'J_D __ _ 1

ug I L

100-4_2-_5-+-____ Styrene ________ + _ __f\J_[)_ ___ ~. ug IL

156-60-5 t-1,2 ~ichloroethene ---J----N9____ , ug I L

1 1°~~2~~~-6 t-1,3 Dichloropropene 1 ND ug IL 98-06-6 tert-Butylbenzene - --1- __ No___ ug I L 0.1

0.1 127-18-4 Tetrachloroethylene I 1 8 -~---~g~~ --· ___ J ___ _

108-88-3 Toluene ND ug IL 0.3

79-01-6

75-69-4

Trichloroethene ND ug I L 0.1

Trichlorofluoromethane ND ug IL 0.1 -- ---------+---'-----+----+------+---

75-01-4 Vinyl chloride ND ug IL 0.1


I 1 ·~~~~~o·b-~-o-:_!_~c-t~-:-~-:-~-;-~-;-n_e_~--~-~=-=~F~~ ~-~--1 _ 1 __ Ju ~:~~: J_____ J SW846 35108/82708 SVOCs by GCIMS By: M/KAR

: {~~~~t~J++-=-= 106 -- -.Ll9TcJ-=1-- L-i-- : -=l 90- : ug I L • 1 1 · !

58- _L_ -~~_l_L _J_ __ 1__ -=£_~==1-==j 95-95-4 2,4,5-Tnchlorophenol ND ' ug IL ! 1 5 • ' ------------------- ----------1--- I --------------~'----._)

-82-1 I 1,2,4-Trichlorobenzene ND i --·---50-1 I 1,2-Dichlorobenzene ND

-73-1 I 1,3-Dichlorobenzene ND '

-46-7 I 1,4-Dichlorobenzene ND ----1-- ----+---

12-0 1-Methylnaphthalene ND ·-·-· -

90-2 2,3,4,6-Tetrachlorophenol ND -··

2,4,6-Trichlorophenol ND ug IL 1 1 t-- 5 ' I

2,4-Dichlorop-henol ==~ ND ug~-:-i~=l-~~~-==-~-j 2,4-Dimethylphenol ND ug I L . 1 I 1

88-06-2

1~1-~1_8-~-~-2---+--- · -::::~ii~i~1;~~~~;:~ -- -- · :~ --~~ _-- ~L--~~+--t=---F--=f ~~-~0--~-f~~-~= 606-20-2 2,6-Dinitrotoluene ND ug I L ! 1 5

i -~~~;--~----+-----_2-~~~~~~r:~::~~ne r- ---~-~ ··- -~-~~+FT~ --r~-~L_~-

Prep

Date

STAN DAR['

Run

Date

05-06-03 05-07 -0:'

05-06-03 05-07-03

05-06-03 05-07-o:..

05-06-03 05-07-03'

05-06-03 05-07-03

05-06-03 05-07 -0.> ...

05-06-03 05-07 -0~

05-06-03 05-07-03

05-06-03 05-07-0<>.

05-06-03 05-07 -0:>-

05-06-03 05-07-03

05-06-03 05-07-0<!·

05-06-03 05-07-0;j.

05-06-03 05-07 -Ot

05-06-03 05-07 -03.

05-06-03 05-07 -O;j

05-06-03 05-07 -0:'

05-06-03 05-07 -03,

05-06-03 05-07 -03

05-06-03 05-07-0:

05-06-03 05-07 -03

05-06-03 05-07 -03'

05-05-03 05-06-0:

05-05-03 05-06-03

04-28-03 04-29-03"

04-28-03 04-29-0:.

04-28-03 04-29-03

04-28-03 04-29-03"

04-28-03 04-29-0~.

04-28-03 04-29-03

04-28-03 04-29-03'

04-28-03 04-29-0~.

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-o:. ..

04-28-03 04-29-0~

04-28-03 04-29-03

04-28-03 04-29-0~

04-28-03 04-29-03

Page 16 of 44 SQLCoyote: Reports 1.0.0305281535)()( Report Date 6118103 2:19:03 PM

STANDARD



Client:

Project:




QC Group

0304504-04C X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

Page 17 of 44

Run Sequence

XG.2003.703.21

XG.2003.703.21

XG.2003.703.21

XG.2003.703.21

XG.2003.703.21

XG.2003.703.21

XG.2003.703.21

XG.2003.703.21

XG.2003.703.21

XG.2003.703.21

XG.2003.703.21

XG.2003.703.21

XG.2003.703.21

XG.2003.703.21

XG.2003.703.21

XG.2003.703.21

XG.2003.703.21

XG.2003.703.21

XG.2003.703.21

XG.2003.703.21

XG.2003.703.21

XG.2003.703.21

XG.2003.703.21

XG.2003.703.21

XG.2003.703.21

XG.2003.703.21

XG.2003.703.21

XG.2003.703.21

XG.2003.703.21

XG.2003.703.21

XG.2003.703.21

XG.2003.703.21

XG.2003.703.21

XG.2003.703.21

XG.2003.703.21

XG.2003. 703.21

XG.2003. 703.21

XG.2003. 703.21

XG.2003.703.21

XG.2003.703.21

XG.2003.703.21

XG.2003. 703.21

Collected: 04-22-03 18:00:00 By: SP

Dilution Detection



91-57-6 2-Methylnaphthalene ----

95-48-7 2-Methylphenol


88-75-5 2-Nitrophenol

91-94-1 3,3-Dichlorobenzidine

3+4 Methylphenol

ND

ND

ND

ND

ND

ND

ug IL

ug IL

ug IL

ug IL

ug IL

ug IL 99-09-2 3-Nitroaniline . ------- -ND -r -ug-i L:

__ 5_3_4--5-2---1--+---4-.-s---D-i-n--ifro-.::2.._metllY1i>heno1 -- ·--- =- ~o~TlJ_§J_,_~ -- 1

5

5

10

1

5 ---~-- -----

1 10

101-55-3 4-Bromophenyl-phenylether ND i ug IL _ L 59-50-7 4-Chloro-3-methylphenol ND ug I L 1 i 5

By: M/KAR ----i--

Prep

Date

Run

Date

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03 7=~~4-Chlo~~~~,::~:::ylothoc +I i! i 1 ~ j i= 1;0 :~::r- :::.:::~::. --~~ _ -----~-~-;-~ 1 :- 1

I 04-28-03 04-29-03

I 04-28-03 04-29-03

62-53-3 Aniline ND ug I L ' ----- - -------120-12-7 Anthracene ND ug IL

-----t----Azoben~ene&1,2- ND ug IL -- -- --·1 Diphenylhydrazine ------- ·

56-55-3 : Benzo (a) anthracene • ND ; ug I L . 1 :-

'°''~ I --- "'"'~.----;-r;ro : ",,-c-11 ---1--r 1 - -- ---1

1:1~24~2---F~-B~~;~~~:.~.~~~:~~~~:ne __ 1 __;~ ~t~f ~~~-J __ -~-=L --_-1

64-85-0 I Benzoic acid _NI) __ L_ ug ~-11 _ 1 __ · __ 25 j1

__

1 100-51-6 I Benzyl alcohol ND i ug IL 1 5 _J_ ---- - -- -

111-44-4 I bis (2-Chloroethyl) ether ND 1 ug I L 1 1 ' -- -- - -- - -- - L --- - - -

- _ _L

111-91-1 bis(2-Chloroethoxy)methane ND ug I L I 1 1 1

108-60-1 bis(2-Chloroisopropyl)ether I ND ug I L

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

117-81-7 bis(2-Ethylhexyl)phthalate i _ __ f\J_[) ___ :- ugiL _j__ __ 1 ___ ,_ 5 I 04-28-03 04-29-03

85-68-7 Butylbenzylphthalate I ND ug I L 1 1 218-01-9 Chrysene ~D -ug-/ L- - 1 -1-- 1

_1_5_332--~-:4--~-9-+------D_ib_e_~z_i~-:-·~-~:;~~~""' ~~ :: ; ~I :j 1--~ -+~ _-- -i -84---66---2--+----D-ie-th_y_lphthaiate- ' ND ug IL 1 -1-- --1

131-11-3 Dimethylphthalate Nol -u9/i. 1 1 - --

- 84_:7_4-_2_-·-+---di-n-B.lJ!YIP~!~~!~te Nl) ___ _J_-_tJ_g Ii= __ 1 _ i _ 1 -r----117-~4~~ -i--- di-n-Octylphthalate __ N~J __ u_gL~ __ [_ 1 _ _i_ ___ _ 20_6.._~4-0 1 ____ F_l_u_or_anthene ND : ug I L '

1~:~::1 . Hexa=~~o0::;:nzene ~~ - j ~~~-~ --f 87-68-3 Hexachlorobutadiene

77-47-4 Hexachlorocyclopentadiene

1

10

10

10

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03




Client:

Project:



Sample: NCLF-6

Matrix: GW

QC Group

0304504-04C X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

0304504-04D X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

0304504-04D X03189

X03189

X03189

X03189

X03189

Page 18 of 44

Run Sequence

XG.2003.703.21

XG.2003.703.21

XG.2003.703.21

XG.2003.703.21

XG.2003.703.21

XG.2003.703.21

XG.2003.703.21

XG.2003.703.21

XG.2003.703.21

XG.2003.703.21

XG.2003.703.21

XG.2003.703.21

XG.2003.703.21

XG.2003.785.20

XG.2003.785.20

XG.2003.785.20

XG.2003.785.20

XG.2003.785.20

XG.2003.785.20

XG.2003.785.20

XG.2003.785.20

XG.2003.785.20

XG.2003.785.20

XG.2003.785.20

XG.2003.785.20

XG.2003.785.20

XG.2003.785.20

XG.2003.785.20

XG.2003.785.20

XG.2003.785.20

XG.2003.785.20

XG.2003.785.20

XG.2003.785.20

XG.2003.785.20

XG.2003.785.20

XG.2003.750.11

XG.2003.750.11

XG.2003.750.11

XG.2003.750.11

XG.2003.750.11

Collected: 04-22-03 18:00:00 By: SP

Dilution Detection


SW846 35108182708 SVOCs by GCIMS By: M/KAR ----------------------------.,---·---- ----·--

67-72-1 Hexachloroethane ND ug IL : 5 _1_9_3--3-9--5- lndeno(1,2,3-cd)pyrene -r--N-D--+---u_g_/_L_1 __ 1 --+-------+------

78-59---1 --+--·-·-1-so_p_h_o-ro-ne-----·----;---- _ N_D_ -·-+-u9/_L_f __ 1 91-20-3

---··-NaJ)hthalerle _____ ---- r- --No- -- , -- ·ug"i L- --1 -·---1·--·--+---·-----

98-95-3

I 62-75-9 Nitrobenzene ---~----- Nl:J.~--~=;=ug/L_-_[- 1

n-Nitroso-dimethyl-amin~ ND , ug I L

__ n-Nitroso-di-n-propylamin~c_=- Nl:J.=~-+ -_ ug '-~ __ 621-64-7

86-30-6 n-Nitrosodiphenylamine ND ug I L ----+---- ----------~----- --------- ----~-- ----87-86-5 Pentachlorophenol ND ug IL ----+--------- ··----- ----·---------- --·--··· -----85-01-8 Phenanthrene ND ug IL

10

1

10

108-95-2 Phenol ND ug/L 10 -----------t-------------j------t-----+------+------t--

129-00-0 Pyrene ND ug IL 1 ----+-----------·------ ·--------- ------

110-86-1 Pyridine ND ug IL -~-------------~----


a-BHC ND I ug IL

10

0.1

By: ALG

Prep

Date

Run

Date

04-28-03 04-29-03'

04-28-03 04-29-03·

04-28-03 04-29-0:> .•

04-28-03 04-29-03-

04-28-03 04-29-03°

04-28-03 04-29-0:>.

04-28-03 04-29-0:''

04-28-03 04-29-03°'

04-28-03 04-29-00.,

04-28-03 04-29-0:''

04-28-03 04-29-03

04-28-03 04-29-0:>.

04-28-03 04-29-0:'

04-29-03 05-08-03

-_-__ --_-_--_----+-____ a_-_C_hlo_r_d_a_n_e ___________ N_D __ -rl __ u_g_l_L_,__ __ -t-__ o._1 _ __J____ 04-29-03 05-08-0:>

309-00-2 Aldrin ND

1

1 ug IL I 0.1 I 04-29-03 05-08-0?

b-BHC ND ug I L 1 I 0 1 04-29-03 05-08-03

57-74-9 Chlordane, total ND ug IL t° 1· o: 1 ----------+---------!--------·--- t--

d-BHC ND I ug I L I 1 0.1 --6-o--57--1-~·-------D-ie-ld-ri_n _______ N_D_ -;---Li

9/L.--r 1 --- - - o.1

-E--n--do_s_u-lf_a_n_I ____ ,,, __ N_D __ -+--_u_g_/_L_+---1·---f-- ·0.1·-----------+----

Endosulfan II ND ug IL 0.1 -----+-----

· ·---------+----E_n d_o_s_u_lf_a n_S_u_lfa_t_e __ -+ __ N_D ____ , -~__!_l-_ __________ o_. _1_ ---+--____,

72-20-8 Endrin ND 1 ug I L 0.1

____ E_n_d_ri_n_A_ld_e_h_y_de ___ -+-___ N_D ___ ~I _ug_l_L---+--------+--~---------Endrin Ketone ND ; ug I L 0.1

i ~i t _:_-0.1 - - i

--- ----6~1- - ---------

58-89_-_9_+--____ g_-c_g~-~-~-dc_an_e ___ -__-__[_~~-0~ -- , __ ~~ ~ ~ -j 1::~~:;~3 Hept::~:;;l;~Xiden n----+-n-n~~-- .'. ~~~t I -_

__ 72_-_43_-_5 --+--------M_e __ th_~xychlor _____ L -ND---~-ug/L -i=. 6088-51-3 p,p-DDD ND , ug IL 0.1 --------- ------------~-----~----+----j------

p,p-DDE 1

ND i ug I L 0.1

04-29-03 05-08-0:>

04-29-03 05-08-07

04-29-03 05-08-03,

04-29-03 05-08-0:>

04-29-03 05-08-0:'

04-29-03 05-08-03

04-29-03 05-08-03

04-29-03 05-08-0Z

04-29-03 05-08-03

04-29-03 05-08-03

04-29-03 05-08-0Z

04-29-03 05-08-03

04-29-03 05-08-03'

04-29-03 05-08-0i

04-29-03 05-08-03.

04-29-03 05-08-03

50-29-3 p,p-DDT ND ug I L 0. 1 04-29-03 05-08-0: - ----- - ----------

, __ 00_0_1_-3_5_-2~ ____ T_o_xa_p_h_e_n_e_, t_o_ta._I ____ L ___ ND __ ~_u_g_l_L_~--~--2_.5_~--- 04-29-03 05-08-03

SW846 35108/8082 PC8s by GC/ECD 12

11

11

53

12

674-11-2

104-28-2

141-16-5

469-21-9

672-29-6 -·-------·- -- ---------

Aroclor 1016

Aroclor 1221

Aroclor 1232

Aroclor 1242

Aroclor 1248 -~~---1--- - --·-·-- ·-·-· .. ----

By: ALG

_l__i-5 --[--·--- I

0.5 I :

--+--- --- ----ND ug IL 1

;--o.5--++- I !0~5 - ---1.

·- -o.5-- ---1

ND ! ug I L -1~~ 1

- --- -----

ND ug IL ! 1 ND - -- ug IL I 1-

- __________ L__ __ _ ND

I ug IL

I 1

04-29-03 05-06-03.

04-29-03 05-06-o:

04-29-03 05-06-0~

04-29-03 05-06-03

04-29-03 05-06-o::.


STANDARD



Client:

Project:




QC Group

0304504-04D X03189

X03189

0304504-04E M03548

M03548

M03548

M03548

0304504-04E M03550

M03550

M03550

M03550

M03550

M03550

M03550

M03550

M03550

M03550

M03550

M03550

0304504-04E M03559

Run Sequence

XG.2003. 750.11

XG.2003.750.11

MT.2003.521.29

MT.2003.511.52

MT.2003.511.52

MT.2003.521.29

MT.2003.566.21

MT.2003.587.62

MT.2003.551.48

MT.2003.551.48

MT.2003.551.48

MT.2003.566.21

MT.2003.551.48

MT.2003.551.48

MT.2003.551.48

MT.2003.551.48

MT.2003.566.21

MT.2003.551.48

MT.2003.522.35


QC Group

0304504-05A

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

Page 19 of 44

Run Sequence

XG.2003.800.13

XG.2003.800.13

XG.2003.800.13

XG.2003.800.13

XG.2003.800.13

XG.2003.800.13

XG.2003.800.13

XG.2003.800.13

XG.2003.800.13

XG.2003.800.13

XG.2003.800.13

XG.2003.800.13

Collected: 04-22-03 18:00:00 By: SP



SW846 3510818082 PCBs by GCIECD

[ 11097-69-1 I Aroclor 1254

;-.,-1~96-82-51 Aroclor 1260

SW846 3005A/601 OA ICP

ND

ND -~----~·

ug IL

ug IL

144o=41-711·--·---· --B-e-ry-11-iu_m__ N? ____ l_rn~l_L-_ 1

7440-47-3 , Chromium ____________ N_D l mg IL 7440-48-4 1 Cobalt ND I mg IL

---------- - ---j--7440-50-8 Copper ND mg IL

By:

0.002

0.01

0.01

0.01

JRE

SW846 3005A6020 ICP-MS By: HMR 744o-=36-oT ___ Antimony - ND ____ mg-/i_ ' 6.001

,..,_,,_, AraO,Tc" - --- j Mo3" -- m, IL 1 ' 0.001 I

I~::~::::: c~~~~m___ -. __ 0;~4 _i~p·· -- C_-{_~~:~~~=r-.---.

I 7439-92-1 I Lead • ND ---- - rn~-~ ___ 1 -~ 0.001 __ ! ---1 ~~~~~~~----- - s~~~i:

1

m _ -----=- -~~~2

_ ~~ ~ t ~=-~~~~-~:~~~--~=---~ 7440-22-4 i Silver NE_____J_ mg IL

1

1 ____ "·- 0.001 744o-:2a-o--1--- Thallium ND I mg IL I · 0.001

7440-3-.,-:-5t ==-------!!~---~-- ND ____ mg IL--~- 0.001 7440-62-2 Vanadium j 0.003 mg IL 0.001 --~---------i 7440-66-6 Zinc I 0.016 I mg IL 0.005


04-29-03 05-06-03

04-29-03 05-06-03

04-30-03 05-01-03

04-30-03 05-01-03

04-30-03 05-01-03

04-30-03 05-01-03

04-30-03 05-08-03

04-30-03 05-14-03

04-30-03 05-05-03

04-30-03 05-05-03

04-30-03 05-05-03

04-30-03 05-08-03

04-30-03 05-05-03

04-30-03 05-05-03

04-30-03 05-05-03

04-30-03 05-05-03

04-30-03 05-08-03

04-30-03 05-05-03

I 7439-97-6 Mercury ND ]_~g i L -[_=T- Lo.000_2_~-!_ ___ 05-01-03 05-01-03

Collected: 04-22-03 19:10:00 By: SP



EPA 524.2 rev 4 Purgeable VOCs by GC/MS ~5-34~3--[ · -· -- i-,1-Dichloroethane --n-- ND ug I L

75-35-4 ! 1, 1 Dichloroethene ND • ug I L 71-55_-6--;- -- 1, 1, 1 Trichloroethane - f .. ;jff- --t- -u9/L- i

630-20-6 1 1. 1. 1.2 Tetra-C:ti1<:>raelh-ane _____ No--ru-g1 L_ ( _

79-00-5 1,1,2 Trichloroeth~ri_e_ __ 1

ND . ug IL_ -1 79-34-5 1, 1,2,2 Tetrachloroethane ND ! ug I L __

563-58-6 1, 1-Dichloropropene ND ug I L

0.1

0.1

0.1

0.1

0.1

0.1

0.1

By:

-------- --- --------+------

106-93-4 1,2 Dibromoethane (EDB) ND ug I L ·----

___ 9_5-_5_0-_1--+ ___ 1_,_2_D_ic_h_lo_robenzene ND J_u_gl __ L_ _____ _ 1,2 Dichloroethane (EDC) ND ; ug I L

1 ~~~ ~~:~~~~~~~~~:~e- --!_ ___ ;~ =l-=~~ ~-t 107-06-2

78-87-5

96-18-4

SQLCoyote: Reports 1.0.0305281535XX

0. 1

0.1

0.1

Report Date

JAA

05-06-03 05-07 -03

- - I 05-06-03 05-07-03 . I

I, 05-06-03 05-07-03

05-06-03 05-07-03

05-06-03 05-07-03

05-06-03 05-07-03

05-06-03 05-07-03

05-06-03 05-07-03

05-06-03 05-07 -03

05-06-03 05-07 -03

05-06-03 05-07 -03

05-06-03 05-07 -03

6118103 2:22:18 PM

STANDARc Assaigai Analytical Laboratories, Inc.


Client:

Project:


APmL03SAMPLEEVENT Order: 0304504 PHl16 Receipt: 04-23-03


Matrix: GW ---------- ------------

QC Group

0304504-05A

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

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Page 20 of 44

Run Sequence

XG.2003.800.13

XG.2003.800.13

XG.2003.800.13

XG.2003.800.13

XG.2003.800.13

XG.2003.800.13

XG.2003.800.13

XG.2003.800.13

XG.2003.800.13

XG.2003.800.13

XG.2003.800.13

XG.2003.800.13

XG.2003.800.13

XG.2003.800.13

XG.2003.800.13

XG.2003.800.13

XG.2003.800.13

XG.2003.800.13

XG.2003.800.13

XG.2003.800.13

XG.2003.800.13

XG.2003.800.13

XG.2003.800.13

XG.2003.800.13

XG.2003.800.13

XG.2003.800.13

XG.2003.800.13

XG.2003.800.13

XG.2003.800.13

XG.2003.800.13

XG.2003.800.13

XG.2003.800.13

XG.2003.800.13

XG.2003.800.13

XG.2003.800.13

XG.2003.800.13

XG.2003.800.13

XG.2003.800.13

XG.2003.800.13

XG.2003.800.13

XG.2003.800.13

XG.2003.800.13



Dilution Detection

Factor Limit Code

By: JAA

Prep

Date

Run

Date

I 87-61-6 1,2,3-Trichlorobenzene r--- ND ____ ugTL--i 1

120-82-1 1,2,4-Trichlorobenzene r·- --~iliO-____ L__u_g_tL1- 1

o.5 . T ----: 05-06-03 o5-o7-o3'

0.5 +- - --- 05-06-03 05-07 -03.

05-06-03 05-07 -0::.. .. 95-63-6 1,2,4-Trimethylbenzene __ +-1 __ N_D __ ~-'-~ __ _l ___ 1 __ ---+ __ o_._1_--+-------•

96-12-8 1,2-Dibromo-3-chloropropane I ND ug I L ' 1 0.2 __j__ _____ j 05-06-03 05-07-0:<c

541-73-1 1,3 Dichlorobenzene : ND ug IL 1 i 0.1 , j 05-06-03 05-07-03

_1~8-67-8 1,3,5-Trimethylbenzene ND ug IL 1 I 0.1 I 05-06-03 05-07-0:>,

142-28-9 I 1,3-Dichloropropane ND ug I L 1 L 0.2 05-06-03 05-07-03'

==1_0-6=-4_-_-6_--7_-_++-

1

/_ -___-___-___-___-___1-___,-4_-_D-___ic-___h-___l-o __ r-___o-___b-e_-n_z-___e-___n-___e-___-___-___-___-~:==--------N-----D--_~_-_-_+-f-----_u-g_-_l-___L-___~:-----~----1-----~-~l----0-._ 1 __ +----j 05-06-03 05-07-o3''

99-87-6 1,4-lsopropyltoluene ND ug IL 1 0.1 05-06-03 05-07-0:l-. • -----------+----------· 594-20-7 2,2-Dichloropropane ND ug IL 1 0.2 05-06-03 05-07-03''

- ----+--------------+--------+----+------+---- ·------95-49-8 2-Chlorotoluene ND ug I L 1 i 0.1

- ---+-----· --- -------+-------- ---- - ---

71-43-2 Benzene ND----+----ug_/ _L_ 1 - l 0.1 --106-43-4 4-Chlorotoluene ND ug IL 1 ,

10.1t

_1_0-8--=--8-6--1__, ____ -______ B_ro_m_o_b_e_n_z_e-ne ___ __,I _____ ~-~N=D=======u-g_-,-·-L:· --=- __ f _ _l ~:-1 -- _ ~-- _ -~ Bromochloromethane I ND ' ug IL 1 0.1

~~75-27-4 Bromodichlorometh_a_n_e __ -+-1 ---~-- ug IL 1 1 ~ _ ~~~:.1- --+- -1 ~ __ :: __ :: __ :_:___, ____ B_r:_~_

0

o_mm_0

_:~_~_:_n_e ____ l1---_~-~---+--~-~-'_, -~-LI ~---_Ji ~1i I 56-23-5 Carbon tetrachloride ND ug I L i 1 0.1

-----------+------------ ----+----------- ------ ----108-90-7 Chlorobenzene ND ug I L 1 ___

1____ 0.1 1 I

124-48-1 Chlorodibromomethane ND ug IL 1 0.1 i - ------+-----------·---f------ J

75-00-3 Chloroethane ND ug I L 1 0.1 I -------- -------+----- ------~-----·- ------

1 67-66-3 Chloroform _ __r.JD ___ L ~g IL ____ 1____ 0.1 _________ _

1 74-87-3 ! Chloromethane ND ' ug IL 1 ' 0.1 --------------+---------- ----------+- ·---------1------------.. ·--- ------- ---<---- -- -

-~56-~_9_-2_1---__ c __ i_s-1,2 dichloroet~e_n_e __ --+-1 ___ ~~ ___ __llg_i_l-_ __ 1 0.1

1 10061-01-5 _ c!s-1,3 dichlorop_ro __ P __ e_n_e_~1- __ N __ D ______ ~_ug_I_ L_ 1 0.1

74-95-3 Dibromomethane ND ' ug IL 1 0.1

100-41-4 Ethylbenzene ___ ~_ ND ug IL ___ ,__(l_:-1__ -1

75-71-8 Freon 12 ND ug IL 1 0.1 . 87-68-3--+---H-e_x __ a_c_h_lo-ro_b_u_ta_d_i_e-ne-------+---N-D- ug_/ L -1-- ----__ ~1 _____ I ---1

98-82-8 ; lsopropylbenzene ND ug IL 1 i 1~·1s I

;_---~~~~-e~:~eh~~a~:~o:ide-----+------~~-~--+-- ~~ ~ ~ ___ --~--] o;s _ _ -__1_04_-5[E;n-Butylbenzene ND -ug I~- l- 1 - -- --~:!- -~-- _ _ ~5~:~~1 1 n-Pr:~:~~=~=ene ~~ ~~ ~+ · _ -~--L--~~~--~ +~~-~---~

108-38- p/m-Xylenes ND U!:J_l __ L 1 , 0.2 T _____ _J 3/106-42

135-98-8

100-42-5

156-60-5

sec-Butylbenz_~~~-------r-:- ~~~ _ - -u97L --r Styrene ND ---~9/L!--

t-1,2 Dichloroethene ND ug IL _l __ _

0.1

0.1

0.1

>4,

05-06-03 05-07-03

05-06-03 05-07-0~-

05-06-03 05-07-0~ ~I

05-06-03 05-07 -03

05-06-03 05-07-03--

05-06-03 05-07 -0?'

05-06-03 05-07 -03

05-06-03 05-07-03·

05-06-03 05-07 -0?'

05-06-03 05-07 -03

05-06-03 05-07-03

05-06-03 05-07 -02

05-06-03 05-07-03

05-06-03 05-07-03

05-06-03 05-07-02

05-06-03 05-07-03

05-06-03 05-07-03

05-06-03 05-07-02

05-06-03 05-07 -03

05-06-03 05-07 -03

05-06-03 05-07-0::

05-06-03 05-07-03

05-06-03 05-07-03

o5-06-03 05-07-o:

05-06-03 05-07-03

05-06-03 05-07 -03

05-06-03 05-07 -O::

05-06-03 05-07-0::.

05-06-03 05-07 -03

05-06-03 05-07-03

05-06-03 05-07-0::. 10061-02-6 t-1,3 Dichloropropene ------+-----

98-06-6 tert-Butylbenzene

I _j_ ND ----j ug I L

~--N_D __ ~ ___ ':!_§ ~---.L---~ 0.1 ---1 --~; 05-06-03 05-07-0~ __ J____ __J

-~-----~----




Client:

Project:




QC Group

0304504-05A

X03206

X03206

X03206

X03206

X03206

0304504-058 X03200

X03200

0304504-05C

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

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Page 21 of 44

Run Sequence

XG.2003.800.13

XG.2003.800.13

XG.2003.800.13

XG.2003.800.13

XG.2003.800.13

XG.2003.727.27

XG.2003.727.27

XG.2003.703.22

XG.2003. 703.22

XG.2003.703.22

XG.2003. 703.22

XG.2003.703.22

XG.2003.703.22

XG.2003. 703.22

XG.2003.703.22

XG.2003. 703.22

XG.2003. 703.22

XG.2003.703.22

XG.2003. 703.22

XG.2003. 703.22

XG.2003. 703.22

XG.2003. 703.22

XG.2003. 703.22

XG.2003. 703.22

XG.2003.703.22

XG.2003.703.22

XG.2003.703.22

XG.2003.703.22

XG.2003.703.22

XG.2003.703.22

XG.2003.703.22

XG.2003.703.22

XG.2003. 703.22

XG.2003. 703.22

XG.2003. 703.22

XG.2003. 703.22

XG.2003. 703.22

XG.2003.703.22

XG.2003.703.22

XG.2003.703.22

Collected: 04-22-03 19:10:00 By: SP

Dilution Detection



Prep

Date

Run

Date

~~~~~~1_-~_·_-_-._·_----·~T-_~--ic~e-~_t_v-~-o_~-;-n_:-:_~-~-~-i,-0_~-~-~-t-~-~-~~n_;-~-~-.-e-,--,----_-_··~-----_-_-_ _:-._-::_-::_-::_~-::_L-::_-::_-::_-::__~~-=-.. _-__ -;-_--;-=_-.--~----r~=:~-~ 1~1 05-06-03 05-07 -03

05-06-03 05-07-03

05-06-03 05-07 -03

05-06-03 05-07 -03

05-06-03 05-07 -03


• _-==i--~t~~~:;~;~~~:~~~~:-_r--~!---~---- --SW846 35108/82708 SVOCs by GC/MS

--~-

120-82-1 1,2,4-Trichlorobenzene ND I ug IL ; 1

~--}-:~-~-}-t----j-I-:,-~-~-],~!~;~~~~;--_-~_'._=_-_f [iff H j H

1 58-90-2 2,3,4,6-Tetrachlorophen_o_I -+---ND __ ug I~ J~_1_ _ : 5

1 ~5~5-4__ 2,4,5-Trichlorophenol ND ! ug IL I 1 5 88-06-2 2,4,6-Trichlorophenol ND ug IL 5

120-83-2 2,4-Dichlorophenol ND ug IL

105-67-9 2,4-Dimethylphenol ND I ugfl l

152\-~18~~2 i ::::~ii~i~t;::a~~;:~ ~-- ~~ --;--~:~~-i -606-20-2 2,6-Dinitrotoluene ------ND- J=ug~L=T=------- 5

91-58-7 2-Chloronaphthalene ND i ug IL 'i .

5

:~::~:: 2-~~~h~~:~~t~:~~ne ~~----T ~~~~-T--~f=j__ ~ 9-5-4a:7]___ 2-Methylphenol --1--- ND I ug IL r ·- ----

1

5

10

~~~~:i-- -----~~~::;:~~~;I__ I ~~----~~ ~ ~ 91-94-1 3,3-Dichlorobenzidine I N~--------~(l__l_~---

99:09=2-- - -- ·- . - ~~:-~i:r~:~;;01

_ _ 1--H~~-~L~~~-~----~~--+_ 5

534-52-1 4,6-Dinitro-2-methylphenol j ___ _t-J_[)_ _L __ tJg~_l:_ _, 1 1 O

5

101-55-3 4-Bromophenyl-phenylether '1 ND ·1

ug IL .

59-50-7 4-Chloro-3-methylphenol - ~-=-~_IJ ___ l-~(Jf L i 5

10-6-47-8 ______ 4-C::~~O!D!_ll_i~~-----_t-JD i ug IL 5

7005-72-3 4-Chlorophenyl-phenylether ND ug I L

1

1._ _ ______ 1_

100-01-6 ! 4-Nitroaniline ND ug IL 1 5

By: ALG 05-05-03 05-06-03

- --- --------:

By: M/KAR

- ----"------

! -t---

! 05-05-03 05-06-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

I 04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

100-02-7 I 4-Nitrophenol ND ug IL I -1--~10--83-32-9 ~-----Acenaphthene -N-6----, -u9/Ll-1----I -----+-----

200-96-0 Acenaphthylene I ND r ugTL.--'---1--1 1

I 04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

62-53-3 Aniline H--L---~~-'- ug IL . --~~-=--_;___-~_- 10 120-12-7 Anthracene . ND ug IL 1 ------~-----------·-----·-· ----- -----------~----

SQLCoyote: Reports 1. 0. 0305281535XX Report Date 6118103 2:27:45 PM

STAN DAR['



Client:

Project:



--------·-------Sample: NCLF-8

Matrix: GW

QC Group

0304504-05C

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

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X03165

X03165

X03165

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X03165

X03165

X03165

X03165

X03165

X03165

X03165

0304504-05D

X03194

X03194

X03194

Page 22 of 44

Run Sequence

XG.2003. 703.22

XG.2003. 703.22

XG.2003. 703.22

XG.2003.703.22

XG.2003.703.22

XG.2003.703.22

XG.2003.703.22

XG.2003. 703.22

XG.2003. 703.22

XG.2003.703.22

XG.2003. 703.22

XG.2003.703.22

XG.2003.703.22

XG.2003.703.22

XG.2003.703.22

XG.2003. 703.22

XG.2003. 703.22

XG.2003. 703.22

XG.2003. 703.22

XG.2003. 703.22

XG.2003.703.22

XG.2003.703.22

XG.2003. 703.22

XG.2003. 703.22

XG.2003. 703.22

XG.2003.703.22

XG.2003.703.22

XG.2003.703.22

XG.2003.703.22

XG.2003.703.22

XG.2003. 703.22

XG.2003. 703.22

XG.2003.703.22

XG.2003.703.22

XG.2003.703.22

XG.2003. 703.22

XG.2003.703.22

XG.2003.785.34

XG.2003.785.34

XG.2003. 785.34

---·----- -- - ------------·----Collected: 04-22-03 19:10:00 By: SP

---·------------ -·----- ----

Dilution Detection


SW846 351 OB/82708 SVOCs by GC/MS By: M/KAR

I -=----50-32-8


-r~-·] l_ ____ . __ _

Benzo(b & k)fluoranthene ND ; ug I L 1 1 1 I ,

__ B_e-~z_e~_~_:_~a_a_)n_P~_h;_:n_c;_n_e ___ _,_ ___ ~-~-· _f ~f i -f : T-~ -1-9-1--24 ___ 2 _ _,.. ___ B_e_n_z_o_(g-.-h-,i)_p_e_ry_le_n_e----+--N-D- i ug IL 1 · -1 - 1 ----r--- -

·--------+-------------~ ---+--64-85-0 Benzoic acid ND ug I L 25 -----+----- ---- ·-·--- _______ j_ ____ .

100-51-6

111-44-4

111-91-1

108-60-1 !

Benzyl alcohol ND ug I L ' 5 ---!- --- ----- _,_ _____ __,___ ____ _

bis (2-Chloroethyl) ether ND _ ug I L ---+ bis(2-Chloroethoxy)methane ND ug I L

----+---bis ( 2 -Ch Io r o is op ro p y I) ether ND ug IL

---------+-------------+--- ·--j----+-117-81-7

85-68-7

218-01-9

53-70-3

132-64-9

84-66-2

131-11-3

84-74-2

bis(2-Ethylhexyl)phthalate ND

Butylbenzylphthalate ND

Chrysene ND

Dibenz(a,h)anthracene ND

Dibenzofuran ND

Diethylphthalate ND

Dimethylphthalate ND

di-n-Butylphthalate ND 117-84-CJ1 ___ d_i-n-Octylphthalate ____ J+-- ND

ug IL

ug IL

ug IL

ug IL

ug IL

ug IL

ug IL

ug IL

ug IL

5

1 1 i

-1 1_ --r~ 1 ---' __ 1 __ - - . _ _J

-- ~- ~ - ~ -- -

1 1 ~

Prep

Date

Run

Date

04-28-03 04-29-03, \.,

04-28-03 04-29-0:.>

04-28-03 04-29-03 '

04-28-03 04-29-03'

04-28-03 04-29-o::;;

04-28-03 04-29-03, ..

04-28-03 04-29-03~·

04-28-03 04-29-0~ ..

04-28-03 04-29-03,

04-28-03 04-29-03'"

04-28-03 04-29-0Z'"

04-28-03 04-29-03,

04-28-03 04-29-03''

04-28-03 04-29-02

04-28-03 04-29-03.

04-28-03 04-29-03

04-28-03 04-29-02

04-28-03 04-29-03.

04-28-03 04-29-03"

04-28-03 04-29-02 206-44-~+1

--- Fluoranthene ___ · · .. _N_D __ _

-:~~+::-----::::~~~ . -~+ ::;~ : __ ~'~ ! 04-28-03 04-29-03.

"·".:~.::~~;~~;:'"• . ·- ~~ - 1 ::-; ~--1 :1 .• -- -~1~ 1-~1-' lndeno(1,2,3-cd)pyrene ND 1_u_g_/_L_l--------

lsophorone ND ug I L 1 1 i

77-47-4

67-72-1 i I 193-39-5 i

78-59-1

91-20-3 Naphthalene , ND ug IL 1 1 1

98-95-3 . Nitrobenzene ~- ug IL . i= 1 __ '. __ 1_

04-28-03 04-29-03

04-28-03 04-29-02

04-28-03 04-29-03

04-28-03 04-29-03"

04-28-03 04-29-0Z .

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-0:i.

04-28-03 04-29-02 62-75-9 I n-Nitroso-dimethyl-amin~--+~ ug I ~--f- 1 10 , _6_21_-6_4_-_7~i __ n_-_N_itroso-di-n-propylamine · I ~- 1 u!;l_/~i_ ___ 1 _ 1 -----+----- 04-28-03 04-29-03 ··

·1' - :~::~:: n-~:~t::~i~~=~~:n::ne i ~~---~~~t , ____ ~ I _ 110 - ~::~::~: ~::~::~~ 85-01-_8--+ ____ P_h_e_na_n_t_h_re_ne

1 ND ug_jL , 1 1 ____ L_____; 04-28-03 04-29-03

"'':'~' Phoool + -ND "' IL 1 . 1Cl._ l_J 04-28-03 04-29-0~

i-~-~-~:~~:~ ::~:~n: t ~~ ~~ ~ ~ r--110· - t _] ~::~::~: ~::~::~:


1----·-+-1 ____ a-_B_HC__ 1 ND ug-/L-,----0.-1 t~-__J

I . 309-00-2 ' a-c;:~~~ane _____ -+1-_-__ -__ -_~~ --~ -~~ ~ ~ I . -- -~~=--c=j 04-30-03 05-09-03 .

04-30-03 05-09-0:.>

04-30-03 05-09-03

SQLCoyote: Reports 1.0.0305281535XX Report Date 6118103 2:28:35 PM ·



Client:

Project:



Sample: NCLF-8

Matrix: GW

QC Group

0304504-05D X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

0304504-05D X03189

X03189

X03189

X03189

X03189

X03189

X03189

0304504-05E

M03548

M03548

M03548

M03548

0304504-05E M03550

M03550

M03550

M03550

M03550

M03550

M03550

M03550

Page 23 of 44

Run Sequence

XG.2003.785.34

XG.2003. 785.34

XG.2003.785.34

XG.2003. 785.34

XG.2003. 785.34

XG.2003. 785.34

XG.2003. 785.34

XG.2003.785.34

XG.2003.785.34

XG.2003.785.34

XG.2003.785.34

XG.2003.785.34

XG.2003.785.34

XG.2003.785.34

XG.2003. 785.34

XG.2003. 785.34

XG.2003.785.34

XG.2003.785.34

XG.2003. 785.34

XG.2003.750.24

XG.2003.750.24

XG.2003. 750.24

XG.2003.750.24

XG.2003.750.24

XG.2003.750.24

XG.2003.750.24

MT.2003. 521. 30

MT.2003.511.53

MT.2003.511.53

MT.2003.521.30

MT.2003.566.22

MT.2003.577.24

MT.2003.551.49

MT.2003.551.49

MT.2003.551.49

MT.2003.551.29

MT.2003.551.49

MT.2003.551.49

i I

Collected: 04-22-03 19:10:00 By: SP



SW846 3510Bl8081A Pesticides by GCIECD By: ALG ------------------------ -------- --- ---------- ------ --- ·- ---,--- - ---- -,

57-74-9 '

-------· - --

--------

-

72-20-8

58-89-9

76-44-8

1024-57-3

72-43-5 ·-·-· -----

6088 51 3 -

50-29-3 i 8061~35="2-T

b-BHC

Chlordane, total

d-BHC

Dieldrin

Endosulfan I

Endosulfan II

Endosulfan Sulfate

Endrin

Endrin Aldehyde

ND , ug IL 1 0.1 I 04-30-03 05-09-03

__ f'J_l=J__~_y-~~-J 1 . 0.1 _,_____ - 04-30-03 05-09-03

.. _ _ NN_ o0

--+- uugg 1

1

LL _1[ __ 11

_ '·, 00

.. 11

_ -~- _ _ _' 04-30-03 05-09-03 04-30-03 05-09-03

~ -=~~ ~ t :~1; T. 6.1 f ~~= ~:::~:~: ~::~::~: --~----N"D ___ .,..u91L+ 1 - o.1

-- ---- 04-30-03 o5-o9-o3

ND ug IL t-1-~--1- ~~~--~ =-~ 04-30-03 05-09-03 -·

-·--·------N_D __ i__LJ_Q_I_~ 1 I 0.1 t I 04-30-03 05-09-03

ND : ug I L 1 , 0.1 04-30-03 05-09-03 - - -ND-- ----;- ug ~--1 -- - :- 0.1 --1 04-30-03 05-09-03

--NNp

0 __ ~_ 11_ uugg 1

1

LL T1

~1--=- j O 1 -r-~~ 04-30-03 05-09-03 1 0 1 ' ' 04-30-03 05-09-03

~~ - _:::~ ~ l_ ~ -t-:~ J i :::::::: :::::;:

Endrin Ketone

g-BHC

g-Chlordane

Heptachlor _,, _______ Heptachlor Epoxide

Methoxychlor

p,p ODD ND ug I L I 1 O 1 04-30-03 05-09-03

~:~:~~~ ·--· -- -~~- --~~-~ t -r--~~~ ~=-~+- ._.-~.~I -.--_--.-_·_! ::::: ::::~:: -

._1=_o_xa~~.~.~~,_~t<l_l_ _ ___i_ ___ N_l=J__ [ -~g/ cj---1 ___ i_-_-2.~ _ 04-30-03 05-09-03


12674-11-2 Aroclor 1016 - -·---+---------

11104-28-2 Aroclor 1221

ND

ND --

ug IL

ug IL

11141-16-5 Aroclor 1232 ND ug IL 53469-21-9 Aroclor 1242 I ND -~-- ugTL _____ _

0.5

0.5

0.5

0.5 ---------------+ --- I ---

' 12672-29-6 I Aroclor 12-:_s____ I ND ~u~L-

j 11097-69-1 ! Aroclor 1254 i ND ~-ug IL 1 0.5

0.5

04-30-03 05-07-03

04-30-03 05-07-03

04-30-03 05-07-03

04-30-03 05-07-03

04-30-03 05-07 -03

04-30-03 05-07 -03

04-30-03 05-07 -03 1 11-096-82-5' -- -----.Arociar-1-26_0_. :~=-~-::_o-::_-_L-Li9 TC_ -· ··1---~--o.5

SW846 3005Al6010A ICP By: JRE 74_4_0--4-1--7-,----------8erYil.i_u_m-----~--N-D--~-m-g/L l - f--~-0.-002--:---__J

~::~::::: c~::~~m -----~-----·-~-·~-·-_-_--+-_:_:_~ ~-=~- }----_ ~:~~ -T- -]

7 440-50-8 Copp~-- _______ ~ _ --~-[)_ _ mg_l_L_t_1 ___ 0.01 l __ __J

04-30-03 05-01-03

04-30-03 05-01-03

04-30-03 05-01-03

04-30-03 05-01-03

04-30-03 05-08-03

04-30-03 05-13-03

04-30-03 05-05-03

04-30-03 05-05-03

04-30-03 05-05-03

04-30-03 05-05-03

04-30-03 05-05-03

04-30-03 05-05-03


STAN DAR[ Assaigai Analytical Laboratories, Inc.


Client

Project:



Sample: NCLF-8

Matrix: GW

QC Group

0304504-05E M03550

M03550

M03550

M03550

0304504-05E

M03559

- --

Run Sequence

MT.2003.551.49

MT.2003.551.49

MT. 2003. 566. 22

MT.2003.551.49

MT.2003.522.36

Sample: NCLF-4

Matrix: GW

QC Group

0304504-0SA X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

Page 24 of 44

Run Sequence

XG.2003.817.5

XG.2003.817.5

XG.2003.817.5

XG.2003.817.5

XG.2003.817.5

XG.2003.817.5

XG.2003.817.5

XG.2003.817.5

XG.2003.817.5

XG.2003.817.5

XG.2003.817.5

XG.2003.817.5

XG.2003.817.5

XG.2003.817.5

XG.2003.817.5

XG.2003.817.5

XG.2003.817.5

XG.2003.817.5

XG.2003.817.5

XG.2003.817.5

XG.2003.817.5

XG.2003.817.5

XG.2003.817.5

XG.2003.817.5

XG.2003.817.5

XG.2003.817.5

XG.2003.817.5

XG.2003.817.5

XG.2003 817.5

Collected: 04-22-03 19:10:00 By: SP




0.001

0.001

By: HMR

0.005

By: JRE

04-30-03 05-05-03-1,,,

04-30-03 05-05-03 ;-·

04-30-03 05-08-0~

04-30-03 05-05-0:F-

-------1 7439-97-6 Mercury -~--N_D_~: _m_g_l_L j ____ 1 ____ [ 0.00_02_~1 -~] 05-01-03 05-01-03"

Collected: 04-23-03 10:05:00 By: SP

Dilution Detection



-~::~::: ~:~ ~:~~:~~~::~:~: --- ~~ f ~~~~F~-~~=i~- --r~-~. 71-55-6 1, 1, 1 Trichloroethane - --~--1 OQ/ L _;_ }~ 0 1_ f

630-20-6 1, 1, 1,2 Tetrachloroethane ND u~_J__~ _ _L___1 ___ -~ 1 _ _ __ _

_ _7~~~:~-- 1, 1,2 Trichloroethane , ___ ND ug I L 1 0.1 79-34-5 1, 1,2,2 Tetrachloroethane ' ND ug I L 1 0.1 __ J_ __ _

563-58-6 1, 1-Dichloropropene ND ug I L 1 0.1 --[ 106-93-4 1,2 Dibromoethane (EDB) ND ug I L 0.1

i - --- -- -

[ __ :_5-5~~ 1,2 Dichlorobenzene ND ug I L 0.1 ---------1

! 107-06-2 1,2 Dichloroethane (EDC) ND i ug IL 0.1

II 78-~7=sl1 1,2 Dichloropropane ~----~g f L 0.1 96-18-4 1,2,3 Trichloropropane ND ug IL ' 1 0.1 87-61-6 1,2,3-Trichlorobenzene-r~- u9/L--1 - --i 0.5

120-82-1 1,2,4-Trichlorobenzene l ND ' ug IL O 5 f 95-63-6 1,2,4-Trimethylbenzene ND l uQ/~-1--;-----o~i - . - -I

---+-- - - _____ _j_ _______ I _____ .J 96-12-8 1 2-Dibromo-3-chloropropane ND 1-ug-TL-- 1 O 2

Prep

Date

Run

Date

05-07-03 05-07 -0""

05-07 -03 05-07-02

05-07 -03 05-07 -03 ,&

05-07-03 05-07-03'-'

05-07 -03 05-07 -02''

05-07-03 05-07 -03 ' 05-07 -03 05-07-03•·

05-07 -03 05-07 -O<

05-07-03 05-07-03.

05-07 -03 05-07-03'•

05-07-03 05-07 -0~

05-07-03 05-07-03

05-07 -03 05-07 -03

05-07-03 05-07-0::"

05-07 -03 05-07-03.

05-07 -03 05-07-03' ---------t---------------·-------------

541-73-1 1,3Dichlorobenzene 1 ND ug/L ! 1 o. 1 05-07 -03 o5-07-oc· -----------+---- ---+-----+------------------- ---··

108-67-8 1,3,5-Trimethylbenzene ND ug IL 1 1 0.1 05-07-03 05-07-03. ---------------------t------·---t--------t-----142-28-9

106-46-7 1,3_~Dichloropropane -+----N_D __ -+-_u_g_l_L_+-- -~ _ 1 __ -~2__________ 05-07-03 05-07-03"

1,4 Dichlorobenzene ND ug IL 1 0.1 05-07-03 05-07-0:. _:_-9~-~7-_-5-----,-i ___ 1_,4 ___ 1s_o_p-ro_p_y_lto-l-ue_n_e---+--N-D---+,-u_g_/_L_+---1--1- 0.1 05-07-03 05-07-03

__ 59_4_-2_0_-7----tl ___ 2_,_2_-D_i_ch_lo_r_o_p_ro_p_a_ne ___ --+ __ N_D ____ ' _ _LJ_g!_L ___ 1 __ __ 0.2 __ L____ 05-07-03 05-07-03'

95-49-8 l 2-Chlorotoluene ND ug IL 1

1 0.1 05-07-03 05-07-0~. -----+--------------------------------------- ----- - --- -106-43-4 4-Chlorotoluene ND , ug IL 1 1 0.1 05-07-03 05-07-0::< ---------""----------------------+----- ·- -- ----------71-43-2 Benzene ND , ug IL 1 0.1 I- -

1

05-07-03 05-07-03' -----+------ ----------------·- -- ------------- ----+--------i----~

108-86-1 Bromobenzene ND i ug IL 1 0.1 ! 05-07-03 05-07-0~ .. --------- -----------

Bromochloromethane ND u IL 1 ' 0.1 I 05-07-03 05-07-0~

75-27-4 Bromodichloromethane -------------- --

75-25-2 Bromoform ---- -·· -----·~--------

SQLCoyote: Reports 1.0.0305281535)()( Report Date

05-07-03 05-07-03'

05-07 -03 05-07-0~

6118103 2:30:00 PM

STANDARD



Client:

Project:




QC Group

0304504-06A

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

.X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

0304504-068

X03200

X03200

0304504-06C

X03165

X03165

X03165

X03165

X03165

X03165

X03165

Page 25 of 44

Run Sequence

XG.2003.817.5

XG.2003.817.5

XG.2003.817.5

XG.2003.817.5

XG.2003.817.5

XG.2003.817.5

XG.2003.817.5

XG.2003.817.5

XG.2003.817.5

XG.2003.817.5

XG.2003.817.5

XG.2003.817.5

XG.2003.817.5

XG.2003.817.5

XG.2003.817.5

XG.2003.817.5

XG.2003.817.5

XG.2003.817.5

XG.2003.817.5

XG.2003.817.5

XG.2003.817.5

XG.2003.817.5

XG.2003.817.5

XG.2003.817.5

XG.2003.817.5

XG.2003.817.5

XG.2003.817.5

XG.2003.817.5

XG.2003.817.5

XG.2003.817.5

XG.2003.727.28

XG.2003.727.28

XG.2003.703.23

XG.2003.703.23

XG.2003.703.23

XG.2003.703.23

XG.2003.703.23

XG.2003.703.23

XG.2003.703.23

Collected: 04-23-03 10:05:00 By: SP

Dilution Detection


EPA 524.2 rev 4 Purgeable VOCs by GC/MS By: JAA 1 7~_-83-9 Bromomethane ~--ND ug IL [-1--T-- 0 6 -

56-23-5 Carbon tetrachloride~- N~i--~~-! L __ l_ _~ _ _l __ ~~_1__ 108-90-7 Chlorobenzene ND ug IL± 1 1 O 1

124-48-1 Chlorodibromomethane ND- ___ u_g!_L ___ _1 _____ ~r-~ -75-00-3 Chloroethane ND ug I L 1 1 0.1

67-66-3 Chloroform --~ 1--ug/L 1 0.1 ---·----·-------- ---------

74-87-3 Chloromethane ND 1 ug IL 1 0.1 156-59-2 -----cis-1,2 dichloroethene I ND , _u_g_/_L __________ ,_ _____ o ___ .1 ___ _

ci·-~::;;:~?P"' -----+1-----~-~--.-__ +1

_-__ -~_:_; _~ _1 1:=J~: 10061-01-5

74-95-3

• 100-41-4 I I 75-11-8

87-68-3 I 98-82-8

--------75-09-2

91-20-3

104-51-8

Freon 12 0.63 ug IL 0.1 --+-------------+------------+------- --- -

Hexachlorobutadiene I ND ug/L 0.1 ----+-----+-------+-----

N_D_-------j_u_g / L 0.1 , ,

ND _u_g_/ L__ ---1--=c()=5==-~ _: ND ug I L 1 _J ___ 1___ ~- __ _, ND ug I L 1 ! 0.1 I

- -- -------;--- ---+--

lsopropylbenzene _____ __J_ __ Melhyleoe ohl,,lde ==* _

Naphthalene ·-·-- -----

n-Butylbenzene

Prep Run

Date Date

05-07-03 05-07-03

05-07 -03 05-07 -03

05-07 -03 05-07 -03

05-07 -03 05-07 -03

05-07 -03 05-07 -03

05-07 -03 05-07 -03

05-07 -03 05-07 -03

05-07-03 05-07-03

05-07 -03 05-07 -03

05-07-03 05-07 -03

05-07 -03 05-07-03

05-07 -03 05-07-03

05-07-03 05-07-03

05-07 -03 05-07 -03

05-07 -03 05-07 -03

05-07 -03 05-07 -03

05-07-03 05-07-03

103-65-1 n-Propylbenzene r---ND ug I L 0.1 __ L ' 05-07-03 05-07-03

ND ug IL -- --- ---- r---95-47-6 o-Xylene

-- --- -ug IL 108-38- p/m-Xylenes __________ _J__ - --

3/106-42 -- -- -- ----------ND

-- ------T 135-98-8 sec-Butylbenzene I ---------·---- - - -

ND ug IL

100-42-5 Styrene I -------------· i .. ---

ND ug IL

156-60-5 t-1,2 Dichloroethene I i ND ug IL

10061-02-6 t-1,3 Dichloropropene ' ND ug IL

- 98-06-6 --r-- tert-Butylbenzene ND ug I L __________ _j_ --------- --···-- -----t------------------+-----------+---127-18-4 Tetrachloroethylene 2.0 ug IL

-----f------------------------·-----·--108-88-3 Toluene ND ug IL

0.1

0.2

0.1

0.1

0.1

0.1

0.1

0.1

0.3

79-01-6 Trichloroethene 0.18 ug I L 1 i 0.1 75-69-4 -T-r-ic-h-lo-ro-fl-uo_r_o_m_e-th_a_n_e ____ c---_ND - ug t L · --1----r- o~i

-----+---------------·-----~------ --------------- . ---1- ----- 75-01~ Vinyl chloride _ [ ~~----- ug IL ____ ___ 1 0.1

1 05-07 -03 05-07-03 -I

05-07 -03 05-07-03

05-07 -03 05-07 -03

05-07 -03 05-07-03

05-07 -03 05-07 -03

05-07 -03 05-07 -03

05-07-03 05-07-03

05-07 -03 05-07-03

05-07-03 05-07-03

05-07-03 05-07-03

05-07-03 05-07-03

05-07 -03 05-07 -03


i ~--------~--t-- 1 ·~~~~~~~::!~~~~~:~~~§~-~---~-~--___ ---t-f _-_~;-~-~-= r~~~~----_T_! u_~:~~~-=f=-_-__ -1 SW846 35108/82708 SVOCs by GC/MS

120-82-1 1,2,4-Trichlorobenzene ND -----------+------95-50-1 1,2-Dichlorobenzene ND ·-· ------+---------------+--------

541-73-1 1,3-Dichlorobenzene ND

106-46-7 1,4-Dichlorobenzene ND

90-12-0 1-Methylnaphthalene ND

58-90-2 2,3,4,6-Tetrachlorophenol --------~·- --~-----------

95-95~!__ 2,4,5-Trichlorophenol

ND

ND

By: M/KAR

ug I L-J=:1 ___ _ ug IL 1 1 I

-- - u~/ L_=:=-___ 1 j_ - -- -----,------ -ug IL ; 1 '

---ug IL

ug IL

ug IL

5

5

05-05-03 05-06-03

05-05-03 05-06-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03




Client:

Project:



Sample: NCLF-4

Matrix: GW

QC Group

0304504-0GC

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

Page 26 of 44

Run Sequence

XG.2003. 703.23

XG.2003. 703.23

XG.2003. 703.23

XG.2003. 703.23

XG.2003. 703.23

XG.2003.703.23

XG.2003.703.23

XG.2003.703.23

XG.2003.703.23

XG.2003. 703.23

XG.2003. 703.23

XG.2003. 703.23

XG.2003.703.23

XG.2003.703.23

XG.2003. 703.23

XG.2003.703.23

XG.2003. 703.23

XG.2003.703.23

XG.2003.703.23

XG.2003.703.23

XG.2003.703.23

XG.2003.703.23

XG.2003.703.23

XG.2003.703.23

XG.2003. 703.23

XG.2003.703.23

XG.2003.703.23

XG.2003.703.23

XG.2003.703.23

XG.2003. 703.23

XG.2003. 703.23

XG.2003.703.23

XG.2003. 703.23

XG.2003. 703.23

XG.2003.703.23

XG.2003.703.23

XG.2003. 703.23

XG.2003. 703.23

XG.2003. 703.23

XG.2003. 703.23

XG.2003. 703.23

XG.2003.703.23

Collected: 04-23-03 10:05:00 By: SP

----- -- ---------- ----

Dilution Detection



88-06-2 2,4,6-Trichlorophenol ND ug I L 5

120-83-2 2,4-Dichlorophenol ND ug IL 5 ---+-------------+--------+----+----i----

__ 1 o_5_-6_7_-9_f--__ 2_4-_D_im_e_th_y_lp_h_e_n_o_I ___ ,,__ __ N_D __ -+-_u_g_l_L __ -+----- ____ 1 ____ 1 ____ +----

51-28-5 2,4-Dinitrophenol ND ug IL 1 1 O -- -- +------·---

121-_1~- _____ -~-·4_-_D_in_it_ro_tolue~~- _ __ t-j_IJ__ _ _IJ9 I L 1

1 5 606-20-2 i 2,6-Dinitrotoluene ND ug I L 1 5 -------+----------------- --+---------- ---------------

91-58-7

Prep Run

Date Date

04-28-03 04-29-03'

04-28-03 04-29-03""

04-28-03 04-29-o:...

04-28-03 04-29-03-•

04-28-03 04-29-03 .•

04-28-03 04-29-0~ ..

04-28-03 04-29-03-' 2-Chloronaphthalene

1

. ND ug I L 1 1 ,_ -9--5--5-7---8-~---2--C-h_l_o-ro_p_h_e-no-l------+---N-D _________ ug_/_L_ i- 1 r 1 ' 04-28-03 04-29-03'·

::~-~--------+----_-_--2~-M~2_:--M_:_:_e-~-!-1~_o_;_a-~-h-~-:-~-n-:_0_1_e_1-n~e~------_--+-, ----~--~----------·+-· ----::-·· -'.-~. J r=-r~~ ~ -_----~ ::::: ::::::~ ----+--------------+-----+-----+---------f------+

88-75-5 2-Nitrophenol I ND ug I L 1 5

91-94-1 3,3-Dichlorobenzidine i ND ug IL ! 1 10 -----+--------------+------+----+-----·---~------+---~

3+4 Methylphenol i ND ug I L ! 1 1 -·--·-----t--------------r---------t------+-----t----------- ----i--------------99-09-2 3-Nitroaniline i ND ug I L I 1 5

534-52-1 4,6-Dinitro-2-methylphenol ! ND ug IL 1 10 I

i 101-55-3 I 4-Bromophenyl-phenylether ND : ug IL , 1 1

59-50-7 1 4-Chloro-3-methylphenol ND Tu9' L~_:I=:__ - __ s ___ ~"·_--__ --__,-106-47-8 4-Chloroaniline ND i ug IL 1 5 ,

---------f-------------------- -- ----- --1- -- - ,_ -i - -, ___ 7o_o_5-_7 __ 2-_3--+-_4-Chlorophenyl-phenylether ND ' uugg 1

1

LL 1

1

I

5

1 _f_ _ 100-01-6 4-Nitroaniline ND 100-02-7 ·4_-N-it-ro_p_h_e-no-I-------+--l--N-D---+---u-g_/_L--+--1~1o- - -- -----+-----------·------j-------+------- _____ I - ---- --- -

8_3~3_2 __ -_9_+--____ A_c_e_n_a_p_ht_h_e_n_e ___ --+-I __ N_D ___ + __ ug_/ _L ___ l ___ 1__~ __ _1___ _ 208-96-8 Acenaphthylene , ND ug I L 1 : 1

62-53-3 Aniline ND ug I L 1 1 10 -12-0--12-7 ~-----·---A-n-th_r_a-ce_n_e------+----N-D---+---u_g_/_L_+--1----i----- 1--

----+-------------+------+------+-----t---- ------· ------ -----

Azobenzene&1,2- [ ___ N __ D ___ -i--__ u_g_l_L_~ __ 1 _____ L __ 1 _____ _

111-44-4

111-91-1

Diphenylhydrazine

bis(2-Chloroethoxy)methane

108-60-1 ' bis(2-Chloroisopropyl)ether

117-81-7 1 bis(2-Ethylhexyl)phthalate

85-68-7 1 Butylbenzylphthalate

218-01-9 ! Chrysene

53-70-3 i --·. ------L-

132-64-9 i

84-66-2

Dibenz(a,h)anthracene

Dibenzofuran

Diethylphthalate

ND

ND

ND

ND

ND

ND

ug IL

ug IL

ug IL

ug IL

ug IL

ND . ug IL 1 ND-- ----c I L 1 ___ f--__ IJ~ ---- ------L

5

04-28-03 04-29-0:'..

04-28-03 04-29-0C' ., 04-28-03 04-29-03

04-28-03 04-29-0S

04-28-03 04-29-0:.>

04-28-03 04-29-03

04-28-03 04-29-0:>.

04-28-03 04-29-0:"·

04-28-03 04-29-03

04-28-03 04-29-0:>

04-28-03 04-29-02·

04-28-03 04-29-03

04-28-03 04-29-0::.

04-28-03 04-29-0?.

04-28-03 04-29-03

04-28-03 04-29-0:1·

04-28-03 04-29-03'

04-28-03 04-29-0:..

04-28-03 04-29-0:>

04-28-03 04-29-03

04-28-03 04-29-0::..

04-28-03 04-29-0:>

04-28-03 04-29-03

04-28-03 04-29-0C,

04-28-03 04-29-0:>

04-28-03 04-29-03

04-28-03 04-29-0:'.

04-28-03 04-29-0:'

04-28-03 04-29-03

04-28-03 04-29-0'.l

04-28-03 04-29-0~


STANDARD



Client:

Project:



---------···--- ----------- -------Sample: NCLF-4 Matrix: GW

QC Group

0304504-0SC

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

0304504-0SD

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

Page 27 of 44

Run Sequence

XG.2003.703.23

XG.2003. 703.23

XG.2003. 703.23

XG.2003.703.23

XG.2003.703.23

XG.2003.703.23

XG.2003.703.23

XG.2003. 703.23

XG.2003. 703.23

XG.2003.703.23

XG.2003.703.23

XG.2003.703.23

XG.2003. 703.23

XG.2003.703.23

XG.2003.703.23

XG.2003.703.23

XG.2003.703.23

XG.2003. 703.23

XG.2003.703.23

XG.2003. 703.23

XG.2003. 703.23

XG.2003.785.48

XG.2003.785.48

XG.2003.785.48

XG.2003.785.48

XG.2003. 785.48

XG.2003.785.48

XG.2003.785.48

XG.2003.785.48

XG.2003.785.48

XG.2003. 785.48

XG.2003.785.48

XG.2003.785.48

XG.2003.785.48

XG 2003.785.48

XG.2003.785.48

XG.2003.785.48

XG.2003.785.48

XG.2003.785.48

XG.2003. 785.48

XG.2003.785.48

Collected: 04-23-03 10:05:00 By: SP

Dilution Detection


SW846 35108182708 SVOCs by GC/MS By: M/KAR -·--·

ND -~-- ;_;g/Lr--1- r 1

-1----r~ I ~ ~ . ·-

! --1-----1-~.---~

: ~ml• ~:~J=-1 fr10_-1--

16

:;~32

;~5 lnd~~:~~.~~;~c~~;y~ne- --.----~~ --~-- ~~ ~ ~ ..... IL' __ -_ -__ i_

1

_-__ --_ '..' __ -_-_-_·_- -·.··--~- --__ -_ -_-_-__ - ----

78~59--1-+--------1-s-·-o-phoro;;e--_____ ND I ug / i 1 1

131-11-3 Dimethylphthalate

84-74-2 di-n-Butylphthalate ND ~ug IL_ --------------- ·--117-84-0 di-n-Octylphthalate ' ND ug IL

·-- -----206-44-0 Fluoranthene ND ug IL

---------.- ----86737 Fluorene ND ug IL

---118-74-1 Hexachlorobenzene ND ug IL ·-- i-----87-68-3 Hexachlorobutadiene ND · ug IL

-----77-47-4 Hexachlorocyclopentadiene ! ND I ug IL

--

Prep

Date

Run

Date

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

~~~.=:_ -· ---- - Naphthalene _1 -~E=-=-j-uiiL

Nitrobenzene · ND ' ug I L 98-95-3 ----r-------------------------

6_2_-7_5~.:__ n-Nitroso-dimethyl-amine L ND ___ ug_~'=.__ _ 10

-~.I 04-28-03 04-29-03

l 04-28-03 04-29-03

-1 04-28-03 04-29-03

n-Nitroso-di-n-propylamine I ND ug I L . !

-:-~:-:~-::-f- n-~:~t:~~i~~:~~:n::ne i ~-~---~-~-~-~-t-=f ___ -- = 1 , ~- -~--j 1805~~91~~2 1

Phe;~:~:ene 1

~-~---+--~-~-~-~-t. _=i---=--:~~-r.----·-----. -·· ---+----· --P-y-re_n_e ________ N_D __ +--_ug_/ L_ t-___ 1-_-_.----1- -----T---

-~~~:~~~~+--·----P-yr-id-in_e _______ _L_ __ N_D__ ug I L [ 1 10 ___ J

621-64-7


,,~, l ,.;=:::- · I b-BHC t-

ND , __ ug I L -----·--

- ~D ___ _u§~ . L

ND ug IL L_ ND ug IL

0.1

0.1 --~--- -----------r------

57-74-9 ! Chlordane, total ND ug I L 1 0.1

6-0--5-7--1-+-----~-~-~-:-~-~-~·-~_:_,-_--_- .·--~-~--+-. -~rn ~+=ii-~ j · .1 _ --1

Endosulfan Sulfate ND ! ug I L 1 ! 0.1 ·---·--·---------L-. ·- -·----,------ --- -- -1 I

72-20-8 : Endrin ND I ug I L 1 0.1 , -------··ti ------ ------------------!- - -- . - I - ~-- -1----

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-30-03 05-1 0-03

04-30-03 05-10-03

04-30-03 05-10-03

04-30-03 05-10-03

04-30-03 05-1 0-03

04-30-03 05-1 0-03

04-30-03 05-10-03

04-30-03 05-1 0-03

04-30-03 05-10-03

04-30-03 05-10-03

04-30-03 05-10-03

04-30-03 05-10-03 Endrin Aldehyde 0.2 _ --+ ug I L ' 1 0.1

EndrinKetone i --~-- ! _u9_/L 1 0.1 1 04-30-03 05-1 0-03 j

58-89-9 g-BHC ND ug IL 0.1 ----

g-Chlordane 1 ND ug I L , 0.1

76-44-8 ____ H_e __ ~-t_a_c_~lc:_r_ ___ =_:t-----N~-=- ug IL ~----_1-~J- 0.1 --I ___ J

1~~[ Heptachlor Epoxide ~- N_D __ ~ ug/_L , 1 [_ 0.1 J _ ·-··

6::~~:~~~-c-----M-:-~-~--~-~-~-h-l_o_r ____ ~=-=-=-=-~=-~=-=---1+-, ·----~--:-:-t I ~-t: ~ 1 i --------

04-30-03 05-1 0-03

04-30-03 05-1 0-03

04-30-03 05-10-03

04-30-03 05-1 0-03

04-30-03 05-1 0-03

04-30-03 05-1 0-03

04-30-03 05-10-03




Client:

Project:



Sample: NCLF-4

Matrix: GW

QC Group

0304504-06D

X03194

X03194

0304504-06D

X03189

X03189

X03189

X03189

X03189

X03189

X03189

0304504-06E M03548

M03548

M03548

M03548

0304504-06E

M03550

M03550

M03550

M03550

M03550

M03550

M03550

M03550

M03550

M03550

M03550

M03550

Run Sequence

XG.2003. 785.48

XG.2003. 785.48

XG.2003.750.33

XG.2003.750.33

XG.2003. 750.33

XG.2003.750.33

XG.2003.750.33

XG.2003. 750.33

XG.2003. 750.33

MT.2003.521.31

MT.2003.511.54

MT.2003.511.54

MT.2003.521.31

MT.2003.566.23

MT.2003.587.63

MT.2003.551.50

MT.2003.551.50

MT.2003.551.50

MT.2003.551.30

MT.2003.551.50

MT.2003.551.50

MT.2003.551.50

MT.2003.551.50

MT.2003.566.23

MT.2003.551.50

Collected: 04-23-03 10:05:00 By: SP

Dilution Detection



[ __ 50-29-3 p,p-DDT NNDD I uugg 11 LL - -li~.-._: __ - ___ 1

1 ___ --_--_-=~Lr--_

20 ..

51 ~=- 1t,'-_=-_·•.-.·-_.·_-;f• i 8~~1_:_~ ___ Toxaphe~tota_l __ ~-----~-

SW846 3510818082 PCBs by GCIECD By: ALG 12674-11-2 Aroclor 1016 11104-28-2 Aroclor 1221 11141-16-5 Aroclor 1232

1--------j------------+I--- ~~ ~--=~~~~+-~-~:-___ -~-:- r .. !

ND ug I L 1 0.5 1

53469-21-9 Aroclor 1242 I ug IL 1 0.5 I -----+--------------+-------+------ ----+------+- -------

ND 12672-29-6 Aroclor 1248 ND j ug IL__ _ __ 1 0.5

--------------r-----~-~

i 11097-69-1 Aroclor 1254 i 11096-82-5 Aroclor 1260

ND ug IL 1 0.5 ND I ug IL 1 ,--- -Cl~S--

-· -- -·--------J_ ___________ c______ -·- --· --------

------+------------·-

SW846 3005A/6010A ICP By: JRE

' r I ;:~r:~?~---~hc~fo~b~af ul-t~ -~<~--~---~N~---D~=~T-~~IL:--__ ____ + ------i- _ _ mg IL 1 1

7 440-50-8 Copper _L ND mg I L _j_ ___ 1_ ~-

SW846 3005A6020 ICP-MS By: HMR 7440-36-0 Antimony ND mg/L 1 0.001

--------- -----------7440-38-2 Arsenic 0.004 mg/L 1 0.001

--~·

7440-39-3 Barium 0.031 mg/L 1 0.001 -------- -·

7440-43-9 Cadmium ND mg/L 1 0.001 --

7439-92-1 Lead ND mg/L 1 0.001 i I I

, ____ I 7440-02-0 Nickel

' 0.010 mg/L I 10 0.001

-- -------·-7782-49-2 Selenium 0.010 mg/L i 1 0.001 ----- -- -7440-22-4 Silver ND mg/L 1 0.001

I 7440-28-0 ----- ---- ---~--

Thallium ND mg/L 1 I 0.001

17440-31-5 i ----------

Tin ND mg/L 1 I 0.001 I

I 7440-62-2 Vanadium ND ~--mg IL 1 ! 0.001 7440-66-6 Zinc ND mg/L 1 i 0.005

--·-------


STANDARr

Prep

Date

Run

Date

04-30-03 05-10-03'

"·· 04-30-03 05-10-03

l

04-30-03 05-07-0:..

04-30-03 05-07-0::C·

04-30-03 05-07-03-.'

04-30-03 05-07-0<. •.

04-30-03 05-07-0;'!

' 04-30-03 05-07-03 ' 04-30-03 05-07-0<>-

04-30-03 05-01-0:.'

04-30-03 05-01-03

04-30-03 05-01-00

04-30-03 05-01-0?"

04-30-03 05-08-03

04-30-03 05-14-0~

04-30-03 05-05-07

04-30-03 05-05-03

04-30-03 05-05-03-

04-30-03 05-05-07

04-30-03 05-05-03_

04-30-03 05-05-0:-S

04-30-03 05-05-0<.

04-30-03 05-05-03

04-30-03 05-08-03'

04-30-03 05-05-0: ..

0304504-06E

M03559 MT.2003.522.39 [_ 7439-97-6 [ Mercury ND. ____ ] _mg-TL-[ [----·-----, -~· --~_o_.o_oo~-- __ ______J 05-01-03 05-01-03

Sample: NCLF-2

Matrix: GW

QC Group

0304504-07 A X03206

X03206

X03206

Page 28 of 44

Run Sequence

XG.2003.800.11

XG.2003.800.11

XG.2003.800.11

Collected: 04-23-03 13:20:00 By: SP

Dilution Detection



75-34-3 I 75-35-4

- 71~_5:6=t=

SQLCoyote: Reports 1. 0. 0305281535)()( Report Date

Prep Run

Date Date

05-06-03 05-07-03

05-06-03 05-07 -o:., 05-06-03 05-07-0::<

6118103 2:33:05 PM

STANDARD



Client:

Project:



-- --- --------.. ···-·--·--·-------·


QC Group Run Sequence GAS#

Receipt: 04-23-03

---- - - - --- -------·-

Collected: 04-23-03 13:20:00 By: SP

Dilution Detection

Analyte Result Units Factor Limit Code

Prep

Date

Run

Date

0304504-07 A X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

EPA 524.2 rev 4 Purgeable VOCs by GC/MS By:

Page 29 of 44

XG.2003.800.11

XG.2003.800.11

XG.2003.800.11

XG.2003.800.11

XG.2003.800.11

XG.2003.800.11

XG.2003.800.11

XG.2003.800.11

XG.2003.800.11

XG.2003.800.11

XG.2003.800.11

XG.2003.800.11

XG.2003.800.11

XG.2003.800.11

XG.2003.800.11

XG.2003.800.11

XG.2003.800.11

XG.2003.800.11

XG.2003.800.11

XG.2003.800.11

XG.2003.800.11

XG.2003.800.11

XG.2003.800.11

XG.2003.800.11

XG.2003.800.11

XG.2003.800.11

XG.2003.800.11

XG.2003.800.11

XG.2003.800.11

XG.2003.800.11

XG.2003.800.11

XG.2003.800.11

XG.2003.800.11

XG.2003.800.11

XG.2003.800.11

XG.2003.800.11

XG.2003.800.11

XG.2003.800.11

XG.2003.800.11

XG.2003.800.11

XG.2003.800.11

XG.2003.800.11

XG.2003.800.11

1, 1, 1,2 Tetrachloroethane ··r ND ug I L I

79-00-5 1, 1,2 Trichloroethane ----r--N-D---+--u_g_/_L_-+-----······-·· _, 630-20-6 I

---~------ -------79-34-5 1, 1,2,2 Tetrachloroethane ND ug IL

--r--------·--------~-----j---- .. 563-58-6 1, 1-Dichloropropene ND ug I L

·-------- --106-93-4 1,2 Dibromoethane (EDB) i

I ND ug IL ----------- ---------r-------- - --··

95-50-1 1,2 Dichlorobenzene ! ND ug IL - - ---- -- _, ____

---~

107-06-2 1,2 Dichloroethane (EDC) I ND ug IL -- ------ t ND - ---Li911.: 78-87-5 1,2 Dichloropropane

- --·· - -- - - ----------------

96-18-4 1,2,3 Trichloropropane ND ug IL -- -------- ·- - ---------

87-61-6 1,2,3-Trichlorobenzene ND ug IL - . - _ _. ___ ·-- -·----- ---- ---- -

120-82-1 1,2,4-Trichlorobenzene ND ._ .. _ll~~ ---- -----95-63-6 1,2,4-Trimethylbenzene ND ug IL 96-12-8 1 ,2-Dibromo-3-chloropropane ND ug IL

-- -------541-73-1 1,3 Dichlorobenzene ND ug IL

---·- ---108-67-8 1,3,5-Trimethylbenzene ND ug IL 142-28-9 1,3-Dichloropropane ND ug IL

---.-- --· 106-46-7 1 1,4 Dichlorobenzene ! ND ug IL

99-87_-6_+--__ 1_,4_-_ls_o_p_ropyltoluene ---~~-----N~---~--ugh 594-20-7 2,2-Dichloropropane 1 ND ug I L

1

1

J_· 1~-· I __ 1 ____ 0~~- . _, ____ !

1 0.2 i

_ -.. -~.-.. -.--L~:_L-1 ~ 1 ___ ~ ___ 0:1 l.-~ ..

0.1

0.2 i - --,--- ..

0.1 I 95-49-8 2-Chlorotoluene ----1-----ND -ug/L--1-- -------------->

106-43-4 4-Chlorotoluene ND ug IL

ug IL 71-43-2 Benzene -----, ----N-D 1-08-86-1 i Bromobenzene ND ug I L

Bromochloromethane ND ug I L 75-27-4 I Bromodichloromethane ND ug IL

~-------+----

75-25-2 Brom ofo rm ND ug I L 74-83-9 Bromomethane ND ug IL

Carbon tetrachloride ND

0.1

0.1 .. -------

0.1

0.1 -------------- ----- ·- -- -----~

. ____ 0.:_1 ____ L 0.1 - · 1

0.6

_:~_?_-_1 __ _

05-06-03 05-07-03

05-06-03 05-07 -03

05-06-03 05-07 -03

05-06-03 05-07 -03

05-06-03 05-07 -03

05-06-03 05-07-03

05-06-03 05-07-03

05-06-03 05-07-03

05-06-03 05-07-03

05-06-03 05-07-03

05-06-03 05-07 -03

05-06-03 05-07 -03

05-06-03 05-07 -03

05-06-03 05-07 -03

05-06-03 05-07 -03

05-06-03 05-07-03

05-06-03 05-07-03

05-06-03 05-07-03

05-06-03 05-07-03

05-06-03 05-07-03

05-06-03 05-07 -03

05-06-03 05-07 -03

05-06-03 05-07-03

05-06-03 05-07 -03

05-06-03 05-07-03

05-06-03 05-07-03

05-06-03 05-07-03

05-06-03 05-07-03 56-23-5

108-90-7 Chlorobenzene ND 0.1 I 05-06-03 o5-o7 -03

124-48-1 Chlorodibromomethane ND ug I L 1 . +------ 05-06-03 05-07-03 0.1 ----

75-00-3

67-66-3

74-87-3

----+-- ----- ·--

Chloroethane ND ug I L 1 , 0.1 ------------··---·-------+-----------•- ·- -- -- ----------t--

Chloroform ND _lJ~__l_L-_ _____ 1 __ , 0.1

Chloromethane ND ug IL 0.1 __j 1-56--5 -----~----Q 1 ----- I

--~--·.:.--·---"--- -·-··- ·I ---·---·- e··-·- - - ·------·---· ----- ·-- I

---------

9-2 cis-1,2 dichloroethene ND ug IL ·-------

10061- 0.1 01-5 cis-1,3 dichloropropene ND ug IL 74-9 5-3

1-4 100-4

75-7 1-8

I Dibromomethane I Ethyl benzene

Freon 12

- ----------------+--·-ND ug IL

---··------

I ND ug IL -

I ND ug IL 87-6 1 0~1- - :

:::::-:-:--'---M_lse_o~-h:-:-~:,;:::: .. +-~-~-~! ~~; ~. ! :-~=-t~~-.·~.-J -=1

-----8-3

I Hexachlorobutadiene ND ug IL ---------·--

104-51-8 _ri~_ut_yl~:fl.~:n: ___ ---==~~-~- --ugTL 0.1 !

05-06-03 05-07 -03

05-06-03 05-07-03

05-06-03 05-07-03

05-06-03 05-07 -03

05-06-03 05-07-03

05-06-03 05-07 -03

05-06-03 05-07 -03

05-06-03 05-07 -03

05-06-03 05-07 -03

05-06-03 05-07-03

05-06-03 05-07 -03

05-06-03 05-07-03

05-06-03 05-07-03


STAN DAR['



Client:

Project:



---- -------------- ----

Sample: NCLF-2

Matrix: GW

QC Group

0304504-07 A

X03206

X03206

X03206

Run Sequence

XG_2003.800_ 11

XG_2003.800_ 11

XG_2003_800_ 11

CAS# Analyte

--------- - --------------- - -------------·-------

Collected: 04-23-03 13:20:00 By: SP

---- ------------------

Dilution Detection


Prep Run

Date Date


103-65-1

95-47-6

108-38-3/106-42

n-Propylbenzene ND ug IL 1 : o.1--T---1------0--X-y-le_n_e-----+---__ ND ug I L 1 ____ c _ -~-1 _ _ _

p/m-Xylenes ND ug IL 1 I 0_2 ---+----- ----------~

--- - ---·-- --

05-06-03 05-07-02"

05-06-03 05-07 .03'' -

05-06-03 05-07-o;,_

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

XG.2003.800.11 ! 135-98-8 sec-Butylbenzene ND ug IL 1 0.1 -~------ o5-06-03 05-07-o::._

05-06-03 05-07-0:>

0304504-078

X03200

X03200

0304504-07C

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

Page 30 of 44

XG.2003.800.11

XG.2003.800.11

XG.2003.800.11

XG.2003.800_11

XG.2003.800.11

XG.2003.800.11

XG.2003.800.11

XG.2003.800.11

XG.2003.800.11

XG.2003.727_29

XG.2003.727.29

XG.2003. 703.24

XG2003.703.24

XG.2003.703.24

XG.2003_70324

XG.2003-703.24

XG.2003. 70324

XG2003. 703.24

XG.2003. 703.24

XG.2003.703.24

XG_2003_70324

XG_2003.70324

XG.2003.70324

XG.2003.70324

XG.2003-70324

XG.2003_70324

XG.2003.70324

XG.2003. 703.24

XG2003.703.24

XG.2003.703.24

XG.2003_70324

XG.2003_70324

XG.2003.70324

XG.2003.70324

XG.2003. 703.24

- ------+---100-42-5

156-60-5

10061-02-6

98-06-6

127-18-4 ------+--

108-88-3

79-01-6

75-69-4

75-01-4

-

Styrene

t-1,2 Dichloroethene

t-1,3 Dichloropropene

tert-Butylbenzene

Tetrachloroethylene

Toluene

Trichloroethene

Trichlorofluoromethane

Vinyl chloride


--·-----I ND ug IL

-----------t ND

' ug IL

I ND i ug IL

I

ND ug IL

5.3 ! ug IL

ND i ug IL

I ND ug IL ------

I ND ug IL

I ND ug IL - ---- --- -----

--1 o_ 1

I ---- -1 o_ 1 '

1 0.1 - ---- -

1 0.1 ---··· --·------

1 o_ 1 ----

1 0_3 I -----··---

i 1 0.1 i \ 1 0.1 : I --

0.1 1 I I 1 _j ___ - - _ _______L____ __ J

By: ALG

__ J ! ~-------: 1,2-Dibromo-3-::chloropropane T--=- N~---' 1,2-Dibromoethane, EDB ND _________ J __ _____________ :

--

ug IL -1 0.025

0.025 ug IL - ----- ---- _L__ -


192~0--:8o_2_-1_1---+1 ___ 1_.2_._4_-T_r_ic_h_lo-ro_b_e_n_ze_n_e--+-------ND ___ l _uugg-,/ -LL- --t--=-=11=======-

1- _-----~---------=

1,2-Dichlorobenzene ND 1 -----f-------~---·-- -

541-73-1 1,3-Dichlorobenzene ND ' ug IL 1 1 - --·-------+------------+: -------+----- --------+----1-------

106-46-7 1,4-Dichlorobenzene ND ug I L i 1 __ 1 1

90-12-0 1-Methylnaphthalene ND ug IL ; 1 1 ' -----+----------------t----N-D---t-------+--1----+,--- -- -~---

--05-06-03 05-07 -03 --

05-06-03 05-07 .o:,_,

05-06-03 05-07 -0:"'

05-06-03 05-07 -03 "-

05-06-03 05-07 -OJ-

05-06-03 05-07-0:."

05-06-03 05-07-03

05-06-03 05-07-03-

05-05-03 05-06-02

05-05-03 05-06-03

04-28-03 04-29-03

04-28-03 04-29-0:.'

04-28-03 04-29-03

04-28-03 04-29-03--

04-28-03 04-29-0:'

04-28-03 04-29-03 5985--9905-_42 2, 3,4, 6-Tetrach lorophen_o __ I _-+-------- ___ uu_g

9

_t1 _LL---+--------j _

55 i

2,4,5-Trichlorophenol ND 1 _ ___j' 04-28-03 04-29-0'.:l ---------------+---- ----+-------- --------t------- ------

88-06-2 i 2,4,6-Trichlorophenol ND ! ug IL 1 5 : 120-B-3--2---+l---2-,4--D-i-c-hl_o_ro_p_h_en_o_l ______ ---+ __ N_D ___ T __ ug IL 1 -5 --- -----

105-67-9 2,4-Dimethylphenol ND ! ug IL I 1 1

__ 51_-28-5 ~-----2_.4_-D_in_it_ro_p_h_en_o_l ____ -___ ~~-ug-/L --~· - 1 --[=- ___ 1g_ ----~=--j 121-14-2 2,4-Dinitrotoluene ND ug IL _____ 1

1

... I 5

5

, ~

6_0_6_-2_0_-2---+ ___ 2_,6_-_D_in_it_ro_t_ol_u_en_e ___ ~_ ND _ _1:19/ L i f-- _ ·-------j 91-58-7 2-Chloronaphthalene ND ug IL 1 1

---------+----------- -·----+--------- ----+-----

'~"~ 2-Chlornpheool ND :: ; ~ L' • 1

--=l=j_:_i--~-:-~---~+-:f--_-_--~=·2~-=-~=-; __ M-'"-~-~-j~-::-~-~-~-~-::-n_e _________ -++-!-----=_ -~---~-------~: :n L~~1J~1i0-=!-_. . ·~·· 91-94-1 3,3-Dichlorobenzidine ND I ug IL

__ 3_+_4Methylphenol ______ ND_- jug~~---- 1-- __ 99-09-2 3-Nitroanilin~ ___ _J_ ND - f- ug IL [ _ 534-52-1 4,6-Dinitro-2-methylphenol ! ND ug I L I

-- ----+---- --f- - -----~ ------L- - -

_1_0_1-5_5_-3 ~- 4-Bromophenyl-phenylether I ND Lu~!_~ _L _

04-28-03 04-29-0:

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-0:

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-o:

04-28-03 04-29-03

04-28-03 04-29-0:5

04-28-03 04-29-0:

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-0:

04-28-03 04-29-03

04-28-03 04-29-03'

04-28-03 04-29-o:

04-28-03 04-29-0~


Client:

Project:

Order:

Sample:

Matrix:

QC Group





0304504 PHl16 Receipt: 04-23-03

NCLF-2

GW

Run Sequence

Collected: 04-23-03 13:20:00 By: SP

------- --- ·-------··

Dilution Detection


STANDARD

Prep Run

Date Date

0304504-07C

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165


X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

Page 31 of 44

XG.2003. 703.24

XG.2003.703.24

XG.2003. 703.24

XG.2003.703.24

XG.2003.703.24

XG.2003.703.24

XG.2003.703.24

XG.2003.703.24

XG.2003.703.24

XG.2003. 703.24

XG.2003.703.24

XG.2003. 703.24

XG.2003.703.24

XG.2003.703.24

XG.2003. 703.24

XG.2003. 703.24

XG.2003. 703.24

XG.2003.703.24

XG.2003. 703.24

XG.2003. 703.24

XG.2003. 703.24

XG.2003.703.24

XG.2003.703.24

XG.2003.703.24

XG.2003.703.24

XG.2003. 703.24

XG.2003. 703.24

XG.2003.703.24

XG.2003.703.24

XG.2003.703.24

XG.2003.703.24

XG.2003.703.24

XG.2003.703.24

XG.2003.703.24

XG.2003.703.24

XG.2003.703.24

XG.2003. 703.24

XG.2003. 703.24

XG.2003.703.24

XG.2003. 703.24

XG.2003.703.24

XG.2003. 703.24

------~------ - ---· ----,------ ----

59-50-7 4-Chloro-3-methylphenol ND ug IL

106-47-8 4-Chloroaniline ND -- ---- - --- -- ---------------

700::~2-3 , 4~_hlo~oyhenyl-phenylether ~ __l\J_[)_ _ [ ug I L _ 1

::;~t :~::~::~:, -- --1 -- ~~--~~~~~ ~- ' 83-32-9 Acenaphthene ND ug I L 1 t --- - - ------1

5

5

5

10

1

2~:~6~_!!_,_ Acenaphthylene _ND ug I L ~ __ 1 ___ _

62-53-3 i _P._12!i~e_________ ND ugl_ L --1---1____ 10

120-12-7 [ __ Anthracene Nf? _ _J_ug_f_I:-__ f _ 1 ___ J_

-----i Azobenzene&1,2- __ !'J_i:J_ __ . ug I _l:_ __ l_ ~ i...

I Diphenylhydrazine _____ _

56-55-3 _B_~nzo (a) anthracene __ _+_ ___ N_I:)__ _u_g __ l_L ___ _,_______ 1

50-32-8 Benzo(a}pyrene I ND ug I L 1

_1_9_1-_24_-2_+--_·--·~~::;~(~.~:)::;~::oe --1 -~~ ·-- *- 1

I

1

64-85-0 Benzoic acid ND ug I L ~ ---'-- _ 25

100-51-6 Benzyl alcohol ND ug IL 1 5 __ ,, ______ _

111-44-4 bis (2-Chloroethyl) ether · ND ug I L _ 111-91-1 bis(2-Chloroethoxy)methane t=_ND : ~iL---+------i 108-60-1 bis(2-Chloroisopropyl)ether I ND ! ug IL

m-81-7 _bis(2-Ethy1ilexy1)phtha1~t€l_J_i? ___ J~u9TL __ 85-6~--7--~~b.El_~Y_!p_httialate___ I -~_!? __ --~ ug IL

218-01-9 Chrysen_e N ~ ___ _)_ _1:19_1 L 53-70-3 Dibenz(a,h)anthracene ND I ug I L

- -f- --··- ----- ··r-132-64-9 ! Dibenzofuran ND ug IL

84--~=2-j- ___ HDie_thylphthalate _H l\j!>__ ug I L

131-11-3 I Dimethylphthalate ND ug IL ·--;-------

84-74-2 di-n-Butylphthalate ND ' ug IL

: 117-84-0 di-n-Octylphthalate 1 ND ug I L 1 '

2~:;:~o Fl~~~:~1~~----·.~ -:;;~ l ;- 1--118-74-=-1- Hexachlorobenzene I ND I - ugfLL-- 1 - -10-87~68-3 Hexachlorobutadiene--t··--ND ____ I ug / L ___ -_-1--~ __ 1~

:~~~~~~ Hexa~:~;~~~~?eti~~=i~ne j-- _ ~~- _ ~<~ ~ ~ . ~ ---+-- 1~ 193-39-5 lndeno(1,2-~3~Cd)pyreile-- ! --- ND- ---,----ug/L- - 1 ~}-__

1_

78-59-1 lsophorone ND ug IL 1 --·---·----------- -----

91-20-3 Naphthalene ND ug IL 98-95-3

62-75-9

Nitrobenzene ND ug IL n-Nitres-o-~dimethyl-amine ____[_:::: ~~=~=yg ii ---+.-_________ _,

621-64-7 n-Nitroso-di-_n~propylamine _J __ !'J_D __ ~ L 1

10

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

i 04-28-03 04-29-03

86-30-_6_~-~~j!~sodiphenylamin~ _ J_ __ N_D__

1

ug _l_':__f.-__ 1 _

87-86-5 Pentachlorophenol ____ ND __ _tJg_t:_L l 1 __ _ 10 .--· .=j

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03




Client:

Project:


APruL03SAMPLEEVENT Order: 0304504 PHl16 Receipt: 04-23-03

Sample: NCLF-2

Matrix: GW

QC Group

0304504-07C X03165

X03165

X03165

X03165

Run Sequence

XG.2003. 703.24

XG.2003. 703.24

XG.2003. 703.24

XG.2003.703.24

--·----- -----------

Collected: 04-23-03 13:20:00 By: SP

Dilution Detection



----1 ND

-1 :tu- I

1 =---1 --------ND I 10 ;------·~ --

i ND

I

1 I ' '----- __ J I ND ug IL I 10 I

--- _J_ ______________

I 85-01-8 Phenanthrene l---------t------------i 108-95-2 Phenol

----------f--

129-00-0 Pyrene --~----+----

110-86-1 Pyridine ------------


Prep Run

Date Date

04-28-03 04-29-03-

04-28-03 04-29-03'·

04-28-03 04-29-0C.,,

04-28-03 04-29-0:.>·

0304504-07D X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

XG.2003.785.26 a-BHC l __ N_D __ ug IL --r-- ---------

0.1 04-29-03 05-09-03'

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

0304504-07D X03189

X03189

X03189

X03189

X03189

X03189

X03189

0304504-07E M03548

M03548

M03548

M03548

Page 32 of 44

XG.2003.785.26

XG.2003.785.26

XG.2003.785.26

XG.2003. 785.26

XG.2003. 785.26

XG.2003.785.26

XG.2003.785.26

XG.2003.785.26

XG.2003.785.26

XG.2003.785.26

XG.2003. 785.26

XG.2003. 785.26

XG.2003. 785.26

XG.2003.785.26

XG.2003.785.26

XG.2003.785.26

XG.2003. 785.26

XG.2003.785.26

XG.2003.785.26

XG.2003.785.26

XG.2003. 785.26

XG.2003. 750.15

XG.2003. 750.15

XG.2003. 750.15

XG.2003.750.15

XG.2003.750.15

XG.2003. 750.15

XG.2003. 750.15

MT.2003.521.34

MT.2003.511.55

MT.2003.511.55

MT.2003.521.34

-----+---- --+-----f---------------a-Chlordane ND 04-29-03 05-09-0~.

309-00-2 Aldrin ND 04-29-03 05-09-0:.>

b-BHC ND 04-29-03 05-09-03 -----+--- ------+ 57-74-9 ! Chlordane, total ND 04-29-03 05-09-0::.-----------+---------------- -----

04-29-03 05-09-0:.>

04-29-03 05-09-03

d-BHC

I

ND ug IL 1 0.1 ---· -----60-57-1 Dieldrin ND I ug IL 1 0.1

I --- ----- --04-29-03 05-09-0:">·

04-29-03 05-09-0?

Endosulfan I ND I ug IL I 1 0.1 ----- -- _____ .,..

. -----1

... _______

Endosulfan II ND ug IL 1 0.1 ---·-- ----·-

04-29-03 05-09-03

04-29-03 05-09-0:i

Endosulfan Sulfate ND ug IL I

1 I 0.1 - - - -! - ---

72-20-8 Endrin ND ug IL 1 0.1 -- " ---------~---

i Endrin Aldehyde ND ug IL 1 : 0.1 04-29-03 05-09-0?

Endrin Ketone ND ug IL 1 0.1 04-29-03 05-09-03

58-89-9 g-BHC ND ug IL 1 0.1 04-29-03 05-09-03·

04-29-03 05-09-0:.' [ ---

g-Chlordane ND i ug IL 1 0.1 - --~--

76-44-8 04-29-03 05-09-03

04-29-03 05-09-03-

04-29-03 05-09-0Z

04-29-03 05-09-03

04-29-03 o5-09-0s

04-29-03 05-09-0Z

04-29-03 05-09-03

Heptachlor ND ug IL : 1 0.1 ---- - ---- --- ---

1024-57-3 Heptachlor Epoxide ND ug IL 1 I 0.1 --- _____ , ----

I

6

:-,:-:--_:-,_:-

3

_4_, ___ --_-----M-~-I~-~-i-''_'~~-----------~1 ---~ ~f c tt ~i- +-1 8001-35-2 Toxaphene, total __ ~~---1 ug I _l-___ l n1 ___ L 2.5 ! n_J

SW846 35108/8082 PC8s by GC/ECD

ND

ND 1

12674-11-2 I Aroclor 1016 ----+-

, 11104-28-2 1 Aroclor 1221 '----- - ----- ----+----

ND

ND

ND

2.1141:2u_ -5 A~oclor 1232 53469-21-9 Aroclor 1242 ----------- --12672-29-6 Aroclor 1248 --------- -

11097-69-1 : Aroclor 1254 ND 1 12~=~-~~:5 I Aroclor 1260 ND

SW846 3005A/6010A ICP 7440-41-7 I Beryllium ND

-----·----7440-47-3 Chromium ND ----'----- -- --· 7440-48-4 i Cobalt ND

·---7440-50-8 I Copper ND

---- -----

By: ALG

r :: ;~ r~~----;-u :: r= 04-29-03 05-07-03""'

04-29-03 05-07-0<

; ug/L i 1=s.5 1 04-29-03 05-07-03 r-u9-1t.:_:_1 ___ -- o.5 -r- - -i 04-29-03 05-07-03" r :::~ . : 6: i - 04-29-03 05-07-0:

.... L "'IL ~ L _ _o:5 :!j 04-29-03 05-07-03

04-29-03 05-07-03'

By: JRE ----

mg/L i 1 TM02 I ~ 04.30.03 05-01-0<

+--=o:?1--~r~~-~~ 04-30-03 05-01-03

~-~~Cl_~-+- ~ 04-30-03 05-01-03

I mg/L 1

T -- . "'" ~ -

mg/L 1 ----------------

mg/L I 1 0.01 - j 04-30-03 05-01-0~




Client:

Project:




QC Group

0304504-07E

M03550

M03550

M03550

M03550

M03550

M03550

M03550

M03550

M03550

M03550

M03550

M03550

Run Sequence

MT.2003.566.24

MT.2003.587.64

MT.2003.551.51

MT.2003.551.51

MT.2003.551.51

MT.2003.566.24

MT.2003.551.51

MT.2003.551.51

MT.2003.551.51

MT.2003.551.51

MT.2003.566.24

MT.2003.551.51

CAS# Analyte


Collected: 04-23-03 13:20:00 By: SP

Dilution Detection


By: JRE

Prep Run

Date Date

04-30-03 05-08-03

04-30-03 05-14-03

04-30-03 05-05-03

04-30-03 05-05-03

04-30-03 05-05-03

04-30-03 05-08-03

04-30-03 05-05-03

04-30-03 05-05-03

04-30-03 05-05-03

04-30-03 05-05-03

04-30-03 05-08-03

04-30-03 05-05-03

0304504-07E

M03559 MT.2003.522.40 j 7439-9~------ Me_r_cur~' ND f-rT19-T1._-r -1-r-0~0002---=-~~=] 05-01-03 05-01-03

Sample: EQUIP. BLANK Matrix: GW

QC Group

0304504-0SA

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

Page 33 of 44

Run Sequence

XG.2003.800.5

XG.2003.800.5

XG.2003.800.5

XG.2003.800.5

XG.2003.800.5

XG.2003.800.5

XG.2003.800.5

XG.2003.800.5

XG.2003.800.5

XG.2003.800.5

XG.2003.800.5

XG.2003.800.5

XG.2003.800.5

XG.2003.800.5

XG.2003.800.5

XG.2003.800.5

XG.2003.800.5

XG.2003.800.5

XG.2003.800.5

XG.2003.800.5

XG.2003.800.5

------------ --- - - --- ---- ------

Collected: 04-23-03 13:40:00 By: SP



EPA 524.2 rev 4 Purgeable voes by GC/MS By: JAA

75-35-4 ~: ~ ~:~~::~:::~:~: -+-~%---- ~~ ~ ~ r---~-------1 -------~-:~ - ~~-- -: ~::~::~~ ~::~~:~~ 71-55-6 1,1,1 Trichloroethane ND _LilJ_f L _ _J _ 1 ___ .) __ 0.1 ---f1 --=--

11

1

05-06-03 05-07-03

630-20-6 1,1,1,2 Tetrachloroethane -·-- __ NN?D._ __ ___ uugg 1

1

LL [1·, 1

1 j' 0

0 .. 11

---+-I ____ 1

05-06-03 05-07-03 79-00-5 1, 1,2 Trichloroethane 1 05-06-03 05-07-03

·75_34~3-T I

__ 7_9_-_34_-5_+-__ 1_, __ 1_ .~_,_2_T_e_t~~-~_h_lo_ro:!~a-~~---- ___ __!J_~---i--- ug IL _ _'.__2 __ t_ 0.1 _J 05-06-03 05-07-03 563-58-6 1, 1-Dichloropropene ND i ug I L 1 L 0.1 ! 05-06-03 05-07-03

1~6-.:_~~ 1,2 Dibromoethane (EDB) ND 1 ug IL 1 ~ 0.1 --I--- 05-06-03 05-07-03

__ 9_5_-5_o_-1_+--__ 1_,2_D_ic_h_lo_ro_b __ e __ n_z_ene ______ ND ug IL _;__--~- _D_: 1 -+ 05-06-03 05-07-03

107-06-2 1,2 Dichloroethane (EDC) ND ug IL ~ 1 0.1 05-06-03 05-07-03 -- ----+ - ____ ,

78-87-5 1,2 Dichloropropane ND ug IL I 1 1

0.1 · 05-06-03 05-07-03

-9-6--18 ____ 4--+---1·.-2-,3--T--r-ic--h-1oropropane- __ --_-_L ________ ND_____ "'n t 1 [-Of - --~ os.-05-03 os-01-03

__ 8_7_~6_1_-6_+-__ 1_,_2_,3_-T_r_ic __ hlorobe~ze~: ____ ~D ---:

1

---U-ugg 1

1

LL II -1

1

-- - -_oo~.55 - ~ ~, 05-06-03 05-07-03

1 120-82-1 1,2,4-Trichlorobenzene --+ ND __ , 05-06-03 05-07-03

_9_5-_6_3-_6_f---__ 1 _,2_,4_-_T_ri_methylben~:_n_:___ _ ___ --~D __ ~_L'~_J_1 __ +-_ 9._1 05-06-03 05-07-03

96-12-8 1,2-Dibromo-3-chloropropane ND 1 ug IL 1 1 1

0.2 05-06-03 05-07-03 541-_-73 ___ 1 _t~, ---1-3 Dichlorobenzene · · ND___ ug I L--1---1 --1- - 0.1 05-06-03 05-07-03

108-67~~ 1,3,5-Trimethylbenzene ND · ug ,-j_ · r 1 ' 0.1 o5-06-03 o5-o7-o3

. ~~~iJ- ~:~:=~:.:~:~: --~r-Jr; u_ ~=~li- -=-1 :~~:: :~:::: --~


Client:

Project:






Sample: EQUIP. BLANK Collected: 04-23-03 13:40:00 By: SP

Matrix: GW

STANDARr

------------- -----

QC Group

0304504-0SA

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

0304504-088

X03200

X03200

Page 34 of 44

Run Sequence

XG.2003.800.5

XG.2003.800.5

XG.2003.800.5

XG.2003.800.5

XG.2003.800.5

XG.2003.800.5

XG.2003.800.5

XG.2003.800.5

XG.2003.800.5

XG.2003.800.5

XG.2003.800.5

XG.2003.800.5

XG.2003.800.5

XG.2003.800.5

XG.2003.800.5

XG.2003.800.5

XG.2003.800.5

XG.2003.800.5

XG.2003.800.5

XG.2003.800.5

XG.2003.800.5

XG.2003.800.5

XG.2003.800.5

XG.2003.800.5

XG.2003.800.5

XG.2003.800.5

XG.2003.800.5

XG.2003.800.5

XG.2003.800.5

XG.2003.800.5

XG.2003.800.5

XG.2003.800.5

XG.2003.800.5

XG.2003.800.5

XG.2003.800.5

XG.2003.800.5

XG.2003.800.5

XG.2003.800.5

XG.2003.727.32

XG.2003.727.32

Dilution Detection



594-20-7 ! 2,2-Dichloropropane ------+---

95-49-8 2-Chlorotoluene ND ug IL 0.1 ------+------ --1------~-

106-43-4 4-Chlorotoluene ---- -------~-------------+--71-43-2

108-86-1

Benzene

ND I ug IL ND --1 -ug IL

0.1

0.1

0.1 Bromobenzene ND ug I L 1 -----l-------+---=---+------1------1------j

Bromochloromethane ND ug I L --~ 1 0.1 -------,------j--------j

_7_5_-2_7-_4----1-__ B_ro_m_o_d_ic_h_lo_ro_m_e_t_ha_n_e __ --1--, __ N_D __ -+-_u__c_g_l_L_+-11 __ 1 __ --1-__ o_.1 __ -+----1

75-25-2 Bromoform : ND ug I L 1 1 1 0.1 - -------+-----------------:- --+------+-------:-----------+-- ------

i __ 7_4-_8_3-_9_-+ _____ B_r_om_o_m_e_th_a_n_e ___ -+-__ N_D ______ u~__I:__ , 1 , O~ 56-23-5 Carbon tetrachloride ND ug I L 1 0.1

l----+-------------+---------1--------'------- --··----------+-----!

Chlorobenzene i ND ug I L i 1 0.1 108-90-7 -----+-------------1-------+---=--+----+------f------j 124-48-1 Chlorodibromomethane I ND ug IL I 1 0.1

-----------l-------------i- ------+----+----+-------1-----1 Chloroethane ND ug I L I 1 0.1 75-00-3

--·-·-··----+--------------·--+.-----t-----+---+-----+,-----j

I 67-66-3 Chloroform I ND ug IL 1 0.1 I

i 7 4-87-3 Chlorometha_n_e ____ -+i--N-D---+--u-'g-/_L_.;...1 __ 1_-+---0-.1--+-i ---1

156-59-2 cis-1,2 dichloroethene ! ND ug IL 1 0.1 I ! 1_0_0_61--0-1--5·-+---_=c=is=-1=·=3=d=ic=h=lo=ro=p=r_o-p=e=n=e=========N=D=----~--~~.'._ __ 1_f-----__ o_._1 ___ -Ti __ --+

74-95-3 Dibromomethane ND ug I L 1 0.1 1

----------'-------'----'---------+- -- -- ----- ---------------4-------

1 ~o5~;41-~~-4-+---·--:_-~-:_-:_-E:t_~-:__~-:-:n=n=~~=n=e===-:_-:_-:_-=_-~-~--~-~------+-~~;-~ _ 1 ~: ~ -~t- __ _ 87-68-3 Hexachlorobutadiene ND ug IL 0.1 ----+---

98 -82 -8 lsopropylbenzene ND ug I L 1 ---+-------'---c _____ _

0.1 ----+---___,

75-09-2 Methylene chloride ND ug I L 1 0.5

91-20-3 Naphthalene ND ! ug IL -----~-----·-+-----------

104-51-8

-103-65-=1---r

95-47-6 t

n-Butylbenzene

n-Propylbenzene

a-Xylene

ND t ug IL 0.1 ----N"o- ---1J91c-r-- 0.1---+----

--'--------l--

ND ug IL 0.1

108-38-3/106-42

p/m-Xylenes ND ug I 1=_J____ __?_:2_~_

------

f-----1-35--9-8--8-~I ----sec--B--u-ty-lb_e_n_z_e-ne ____ l ___ N_D ______ u_g_/_L ___ 1 _________ 0_.1 ___ ~_+ ___ _ _________ ,__ ____________ ___. _________ --- ----- -··-----

100-42-5 i Styrene ND , ug IL 1 0.1 ----+------

156-60-5 I t-1,2 Dichloroethene I ND ug IL 1 0.1

I 10061-02-6 I t-1,3 Dichloropropene I ND ug IL 1 .L. o~1 ------+---------------+-· -------·-.. ·--·-------'------------'------

98-06-6 tert-Butylbenzene ND ; ug IL 1 0.1 -----+---------------l------'-----'------ -·-· --------- l-~-------------- --

127-18-4 Tetrachloroethylene ND I ug IL 1 0.1 108-88-3 Toluene ND i ug IL 1 -- - -5~3---- -----79-01-6 Trichloroethene ND I ug IL 1 0.1

___ 7_5-_6_9-_4---+ __ T_r_ic_h_lo_r_of_lu_o_ro_m_e_t_h_an_e __ -+-__ N_D ___ ~ ug IL 1 0.1 ,_ __ _

_7_5-_01_-4_~ ____ V_in_y_l _ch_l_o_rid_e ___ ~ __ N_D __ ~, -_u_-_-g __ l_L __ -~1 ____ 1_-_·. -_ ~-_9-'~--~--~

EPA 504 EDB/DBCP by GC/ECD By: ALG -------~-------

-------·+---1_,2_-_D_i_ b_ro_m_o_-_3_-c_h_l o_ro_p_r_o p_a_n_e_+--_ ND__ " _ ___IJ_g_~':_ _l _ ·--ao~5a __ I 1,2-Dibromoethane, EDB ND - ug I L - i 025 :

_----l-_________________ ~----~---~-- - -

Prep Run

Date Date

05-07-0:.:> ,, 05-06-03 05-07 -03

05-06-03 05-07 -O:'Y.

05-06-03 05-07 -0? ..

05-06-03 05-07 -03

05-06-03 05-07 -O::i"'

05-06-03 05-07-0?" '··

05-06-03 05-07 -03,

05-06-03 05-07-03-.

05-06-03 05-07-0:''

05-06-03 05-07-03_

05-06-03 05-07 -03

05-06-03 05-07-0Z

05-06-03 05-07-03.

05-06-03 05-07 -03

05-06-03 05-07 -OZ

05-06-03 05-07-03

05-06-03 05-07 -03

05-06-03 05-07-0::

05-06-03 05-07 -03

05-06-03 05-07 -03

o5-06-o3 05-07-0c

05-06-03 05-07-03

05-06-03 05-07 -03'

05-06-03 05-07 -De

05-06-03 05-07 -03

05-06-03 05-07 -03

05-06-03 05-07 -Oc

05-06-03 05-07-0:.

05-06-03 05-07 -0~

05-06-03 05-07-03

05-06-03 05-07 -O:.

05-06-03 05-07 -0:.'·

05-06-03 05-07-03

05-06-03 05-07 -o:.

05-06-03 05-07-0?

05-06-03 05-07 -03

05-06-03 05-07 -00

05-05-03 05-06-0?

05-05-03 05-06-03


Client:

Project:

Order:

Sample:





0304504 PHl16 Receipt: 04-23-03

EQUIP. BLANK Collected: 04-23-03 13:40:00 By: SP

Matrix: GW

QC Group Run Sequence

Dilution Detection


SW846 351 OBl8270B SVOCs by GCIMS By: M/KAR 1 f - f --T - ----- ---- ..

120-82-1 1,2,4-Trichlorobenzene ND I ug IL

95-50-1 1,2-Dichlorobenzene ND ug IL ------ ·--·

541-73-1 1,3-Dichlorobenzene ND ug IL --- ---·--

106-46-7 1,4-Dichlorobenzene ND ug IL ------ --- ----

90-12-0 1-Methylnaphthalene ND ug IL _____ ,, _______ ------

58-90-2 I 2,3,4,6-Tetrachlorophenol ND ug IL -----·------ ----------

. -~5-95-4 1----l~-:..5-Trichlorophenol i 88~06-_2_L 2,4,6-Trichlorophenol ND

120-83-2 I 2,4-Dichlorophenol ND 1 ug IL I 1 ! 5 '

105:57-9 1 2.4=DimethYlphenol ___ ND , ug/L l- -1 - 1 +- --51-28-5 I 2,4-Dinitrophenol- -------ND_____ ug IL l 10 r 121-14-2 2~4-Dinitrotoluene----~ ND - -Li9TC -1-- - 5 I

- l ---606-20-2 2,6-Dinitrotoluene ND ug I L 5 !

:9511::5778:768 2-~~~~~:r:~::~~ne-==:=-----~--~-·-_::_:::_-uuu-g~-/;_LLL--+: - - _ _;___1 -i·~~ .. 2-Methylnaphthalene ND

95-48-7 1 2-Methylphenol --~--ND . __ _lJ~_l_L_,_--_--_--_-,~--1_ -~-+---j 88-~~:4 _ _, ____ 2_-_N_it_ro_a_n_il_in_e_ ND ug IL I 5 88-75-5 : 2-Nitrophenol ND ug IL -- --,- 5 91-94-1 --------r----

99-"~ 534-52-1

101-55-3

59-50-7

106-47-8

7005-72-3

----- ---- ---3,3-Dichlorobenzidine ND ug I L 10 --- -- _________ ____, __ _

3+4 Methy~E_h~~o_l_ ______ N_c:J_ ug I L ~ 3-Nitroaniline ND 1 ug I L _ ____, __ 5 _j

4,6-Dinitro-2-methylphenol ND ug I L 1 O ___ [

4-Bromophenyl-phenylether ND ug I L _ j l _ -1 4-Chloro-3-methylphenol ND ug I L 1 5 I ,

---j--- --- --+-----4-Chloroaniline _f'ID r-u~1J:::_=:-___ 1 __ - 5

4-Chlorophenyl-phenylether ND ug I L I 1 . .L

I I

Prep

Date

STANDARD

Run

Date

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

0304504-0BC

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

XG.2003.703.25

XG.2003.703.25

XG.2003.703.25

XG.2003.703.25

XG.2003.703.25

XG.2003. 703.25

XG.2003. 703.25

XG.2003. 703.25

XG.2003. 703.25

XG.2003. 703.25

XG.2003.703.25

XG.2003.703.25

XG.2003.703.25

XG.2003. 703.25

XG.2003.703.25

XG.2003. 703.25

XG.2003.703.25

XG.2003.703.25

XG.2003. 703.25

XG.2003. 703.25

XG.2003. 703.25

XG.2003. 703.25

XG.2003.703.25

XG.2003.703.25

XG.2003.703.25

XG.2003.703.25

XG.2003.703.25

XG.2003.703.25

XG.2003.703.25

XG.2003. 703.25

XG.2003. 703.25

XG.2003.703.25

XG.2003.703.25

XG .2003. 703 .25


4-Nitrophenol

ND ug IL 5 i 04-28-03 04-29-03

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

Page 35 of 44

XG.2003. 703.25

XG.2003.703.25

XG.2003.703.25

XG.2003.703.25

XG.2003.703.25

XG.2003.703.25

XG.2003.703.25

XG.2003. 703.25

100-02-7 J 83-32-9 I

208-96-8

62-53-3 ----

120-12-7 i

.L ND ug IL

Acenaphthene , ND ug IL --- --- -~---------- - - - -

Ac_:~_Cl~~-~h_!'l~n_e ___ ______j_ _ _t-1~ _ _ ug IL

Aniline ND ---1-----

Anthracene ND -------------·- -----------~--------- ~------------

56-55-3

so-32::S-T


ND

Benzo (a) anthracene ND - -·- -r-u9fi_--,~~ 1 _

10

Benzo(a)pyrene _ --1- ND : ug I L . t ... 1 1

__ _

-1::_9::_1-::_24::_--2_-:_-~~~-~-~-~-~-~-~=~··-_.~-~f-i~~-:-r~-~e-t~-:n_e _ ___,i ____ ~~- _]_-~~~~~~+ ~ ,_-H - 1 ~=L : 64-85-0 Benzoic acid ND I ug I L • 1 I 25 l'

::::::·: .;:(~-~~:~~:~~:::~:"" -~ ~-~-----at~-: ~-----L ~ ~~!----··---=

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03


STAN DAR['



Client:

Project:



------------- -------- -Sample: EQUIP. BLANK Collected: 04-23-03 13.-40:00 By: SP

Matrix: GW

QC Group

0304504-08C

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

0304504-08D

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

Page 36 of 44

Run Sequence

XG.2003.703.25

XG.2003. 703.25

XG.2003. 703.25

XG.2003.703.25

XG.2003.703.25

XG.2003.703.25

XG.2003.703.25

XG.2003.703.25

XG.2003. 703.25

XG.2003. 703.25

XG.2003. 703.25

XG.2003.703.25

XG.2003.703.25

XG.2003.703.25

XG.2003.703.25

XG.2003.703.25

XG.2003_703.25

XG.2003.703.25

XG.2003.703.25

XG.2003.703.25

XG.2003. 703.25

XG.2003.703.25

XG.2003. 703.25

XG.2003.703.25

XG.2003.703.25

XG.2003.703.25

XG.2003.703.25

Dilution Detection



~.~ :: ; ~ ~ :i-=:__:_ I B j :-_-__ 2_~-=_58_-_:--8-_1-___ 79=:=====B=u=t_y __ l_~-e-h_n_~=:=l~=~=:h=a=la=t_e __ ----_--:_-+-_-_-__ -~-~----i1 _uu\gg 111~LL_~_t· 11

1 t1

______ 1

1

1 ___ ~11 ___ ~~

1

1

I 53-70-3 Dibenz(a,h)anthracene ND

132-64-9 ----D-ib_e_n_z-of-u-ra-n-=--=--=--=----_-_-+1_::__==-__ N __ D __ _J___ug_l _L __ ~_ 1 __ j___ 1 _=r=_:~ _ -~~6:_2 __ -+ ____ D_ie_t_hy_lp_h_t_ha_l_at_e ________ _,__ __ N_D _____ l -~g IL 1 1 1 __ 1 .. __ 1 ---~ 131-11-3 Dimethylphthalate ND ug IL ' 1 1 _1 _ 84-74-2 I di-n-Butylphthalate ND -+---ug_/_L----+--1---,-·-- 1 -+----____,

! __ 1~_?_=B4-D1----d-i-n---O-c-ty-lp-h-th_a_la_t_e=-====:-=--=--=--=-N-_D ___ =_---===u=g=/=L=::_::__::__1 ___ =-=--~· --_ ~- ~ ~:--=~-

I 108-60-1 bis(2-Chloroisopropyl)ether

117-81-7 bis(2-Ethylhexyl)phthalate

206-44-0 Fluoranthene ND ug I L 1 1 -----t------l

86737 Fluorene ND ug I L 1 1 118-74-1 Hexachlorobenzene ND ug I L 1 10 -------+--------------+-------+----+--- -- --~-------+------+ _0 __ 7-_68_-_3--+ ___ H_e_x_a_ch_lo_robutadiene ____ N_D __ ~1 _ug!_~ 1 1-~- _ _ __ _ 77-47-4 Hexachlorocyclopentadiene ND I ug I L 1 1 O ---+----------------+-·---

, ____ 6_7_-7_2 __ -_1_+---___ H_e_xa_c_h_lo_r_oe_t_ha_n_e ___ +----___ ND ug '-~- ___ 1 ___ ~_ _ _ __ 193-39-5 lndeno(1,2,3-cd)pyrene ! ND , ug I L 1 1 -----+----- ------+--- --- ----+---------r -- ----~+ - --~~~~~-----ls_o_phorone ___ ND j ug IL , 1 1 -~ _ ~·-----9~=:0-3 ~-- Naphthalene : ___ ND __ ;___ui~~=J __

1 __ 1 ____ _

_-:~1-:_:-;======n_-N_it_ro_: __ i:_r-~-~-~-:z_t~-~-l~_am_in~ 1 -~~-~1 ;~~t J __ ~+--L--11

()_ 1

__ -=J 621-64-7 ! n-Nitroso-di-n-propylamine ND , ug IL 1 : 1 86-30-6 I n-Nitrosodiphenylam-in--e----+------N-D____ I ug IL 1 --'--1~---=- --

1 __ 87-86-5f---l __ P_e_n_ta_c_h_lo_r_op_h_e_n_o_I __ 1---N_D __ +'-_u_g_l_L---+ __ 1 __ _ _ -~~--+-----j , ___ 85-01_-8_+j _____ P_h_e_n_a_nt_h_re_n_e ____ -+-__ N_D ____ u_g_l_L_

108-95-2 Phenol ND ug I L 10

129-00-0 Pyrene ND i ug IL

Prep Run

Date Date

04-28-03 04-29-03

04-28-03 04-29-03'

04-28-03 04-29-0<

04-28-03 04-29-03«

04-28-03 04-29-03"

04-28-03 04-29-0:.

04-28-03 04-29-03.

04-28-03 04-29-03'

04-28-03 04-29-0::..

04-28-03 04-29-03·

04-28-03 04-29-03.

04-28-03 04-29-0::.'

04-28-03 04-29-0:>

04-28-03 04-29-03'

04-28-03 04-29-o::,.

04-28-03 04-29-0~.

04-28-03 04-29-03.

04-28-03 04-29-0:>

04-28-03 04-29-0:>

04-28-03 04-29-03.

04-28-03 04-29-0<>.

04-28-03 04-29-0:'

04-28-03 04-29-03

04-28-03 04-29-0:).

04-28-03 04-29-0:>.

04-28-03 04-29-03

04-28-03 04-29-0::.

XG.2003.703.25 I_ 110-86-1 - __ _J 04-28-03 04-29-0:> Pyridine ND ug IL 1

----~ --~- ---~-

10

XG.2003.929.22

XG.2003.929.22

XG.2003.929.22

XG.2003.929.22

XG.2003.929.22

XG.2003.929.22

XG.2003.929.22

XG.2003.929.22

XG.2003.929.22

XG.2003.929.22

XG.2003.929.22

XG.2003.929.22

XG.2003.929.22

SW846 3510818081A Pesticides by GC/ECD By: ALG 1--- a-BHC -----,--No-- T ug IL 1 2 O 1 i 04-29-03

1-=-----===:i-===-=----=--a--C-h-lo_r_d-an-e ND mg IL , - 2--+---0~--~---_-___ -_1-___ -__ -____j---1 04-29-03 06-03-03

: 309-00-2 ' Aldrin -----+----N-D- -~u~LL 2 0.1 04-29-03 06-03-0c i--------~----------------1------- t------+------- ----------

--------·----+-! _______ b_-_B_H_C______ ND I u_g!_~-- __ 2_--+-1 __ o_._1_--+----- 04-29-03 06-03-03 57-74-9 Chlordane, total ND f ug IL 2 0.1 04-29-03 06-03-03

--------+-------------+---------+----+------ --------+--___, __ ------+ _____ d_-B_H_C _______ +--__ N_D __ _L ug IL 2 0._1 __ -+-_ __ 04-29-03 06-03-0c

-~o_-_5 __ 7_-1_+--____ D_i_el_d_rin ______ 1+--__ N_D __ Lu_g_l_L_+-_2_--+-__ o_.1_--+----- 04-29-03 06-03-03

~=-~----_-+-i----_-_-_-_-_-_-_~-=_~-d_d_:_s_s_~-=_1~-fa_a_~_-_1\-=_-=_-=_-=_-=_-~----+~:~--------~--~---+--~-~-~-~--'-, ---~{~~-~J-H~:-~ i ~::~::~~ ~::~~:~: Endosulfan Sulfate ! ND ug I L 2 , o_ 1 04-29-03 06-03-03

Endri-n---------+--N--D __ -~g /L 1 - 2 j __ _<J:} - , 04-29-03 06-03-03

---~=-===___,_1-______ E_n_d_rin-Aldehy_de ____ -+-

1

1 __ N_D__ ug I L 2 , 0.1 ----+----- ·-: 04-29-03 06-03-0:

Endrin Ketone ND , ____ ug I L 2 0.1 I 04-29-03 06-03-03

06-03-03

72-20-8

--------------------

SQLCoyote: Reports 1_0_0305281535XX Report Date 6118103 2:40:51 PM



Client:

Project:



Sample: EQUIP. BLANK Collected: 04-23-03 13:40:00 By: SP

Matrix: GW ---------------·-----·

QC Group

0304504-08D

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

0304504-08D

X03189

X03189

X03189

X03189

X03189

X03189

X03189

0304504-08E M03548

M03548

M03548

M03548

0304504-08E

M03550

M03550

M03550

M03550

M03550

M03550

M03550

M03550

M03550

M03550

M03550

M03550

Run Sequence

XG.2003.929.22

XG.2003.929.22

XG.2003.929.22

XG.2003.929.22

XG.2003.929.22

XG.2003.929.22

XG.2003.929.22

XG.2003.929.22

XG.2003.929.22

XG.2003. 750.16

XG.2003. 750.16

XG.2003. 750.16

XG.2003. 750.16

XG.2003. 750.16

XG.2003.750.16

XG.2003. 750.16

MT.2003.534.10

MT.2003.511.58

MT.2003.511.58

MT.2003.521.35

MT.2003.566.25

MT.2003.577.27

MT.2003.551.52

MT.2003.551.52

MT.2003.551.52

MT.2003.566.25

MT.2003.551.52

MT.2003.551.52

MT.2003.551.52

MT.2003.551.52

MT.2003.566.25

MT.2003.551.52

CAS# Analyte Result

SW846 3510B/8081A Pesticides by GC/ECD

58-89-9 I g-BHC .. -------+------------ ______________ .. i g-Chlordane

-76-44~-- ---HeptachiOr-- -

1024-57-3 Heptachlor Epoxide

ND

ND

ND ·- -- -+------ ----- ------

ND

Dilution Detection

Units Factor Limit Code

By: ALG ug IL __ 2 _____ 0 -1- __ ;_ __ ~

~-~-~~-- ;_ ~-=~~~=±==---= ug IL 2 ' 0.1 : '

--------t------------~------ --- --------------

6::~~:~~3 Me:~P~~~~~~ ___ -~ __ _;_ ___ I _~~;-~ -t-- =~-= _ ~~~ p,p-DDE I ND f ug I L I 2 0.1

8:~~:~~~~~~-~~~=~=T~~t:i--- ----_J- - ~~--- -- ~: ~~ +-- -~- T~}~

SW846 3005A/601 OA ICP By: JRE

;~~ --= ~~~-i-:-~-';"_:: ___ --HU~. _ ;L_jl;t: ~~I ~~J~ 7440-50-8 Copper ND mg IL 1 J__ ?.01 I j

SW846 3005A6020 ICP-MS By: HMR

7440-~6-o --"Ar1'tim0i1Y-- - --; - No i mg ;-L __ f-- 1-- --·-1- 0.001--_;_ __ ~~=

7440-38-2 Arsenic ND mg IL 1

1 I 0.001 7440-3-9--3-t------B-a-r-iu_m ______

1 __ ~--mg IL -,---1---,-6~001 __ _

i ~::~::~:~ Ca~e:~um ~~+~~+'c-1

--+---~:~~-'---- _ ~;:~:~::~ : s~~~i:1m ----+--~-~- ---~ci;~-1---~-----~:~~-~==--=---=1 7440-22-4 Silver I ND mg IL ,--1---r--o.oo:J--! -- -7440-28-0 Thallium I ND mg IL -t------1-J--o 00-1 _J_____

7440-31-5 - ---T'ill- --- --- -- i --ND- - mg IL 1 i o.001--;----

7440-62--2---- Vanadium ___ _j_ ND mg/L - i o._001

7440-66-6 Zinc ____ _j_ __ N~-- mg IL l 0.005 ---~-------•


Prep

Date

STANDARD

Run

Date

04-29-03 06-03-03

04-29-03 06-03-03

04-29-03 06-03-03

04-29-03 06-03-03

04-29-03 06-03-03

04-29-03 06-03-03

04-29-03 06-03-03

04-29-03 06-03-03

04-29-03 06-03-03

04-29-03 05-07 -03

04-29-03 05-07-03

04-29-03 05-07 -03

04-29-03 05-07 -03

04-29-03 05-07 -03

04-29-03 05-07-03

04-29-03 05-07-03

04-30-03 05-03-03

04-30-03 05-01-03

04-30-03 05-01-03

04-30-03 05-01-03

04-30-03 05-08-03

04-30-03 05-13-03

04-30-03 05-05-03

04-30-03 05-05-03

04-30-03 05-05-03

04-30-03 05-08-03

04-30-03 05-05-03

04-30-03 05-05-03

04-30-03 05-05-03

04-30-03 05-05-03

04-30-03 05-08-03

04-30-03 05-05-03

0304504-08E

M03559 MT.2003.522.41 [ 7439-97-6 [ Mercury ....... _T __ . 1

_L_~-~- ___ .1 ____ ~_9_! __ ~ ___ l _ ! = ~.0002 ·T=] 05-01-03 05-01-03

Page 37 of 44 SQLCoyote: Reports 1.0.0305281535)()( Report Date 6118103 2:41:27 PM

STAN DAR['



Client:

Project:



Sample: TRIP BLANK Matrix: GW

QC Group

0304504-0SA X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

Page 38 of 44

Run Sequence

XG.2003.800.6

XG.2003.800.6

XG.2003.800.6

XG.2003.800.6

XG.2003.800.6

XG.2003.800.6

XG.2003.800.6

XG.2003.800.6

XG.2003.800.6

XG.2003.800.6

XG.2003.800.6

XG.2003.800.6

XG.2003.800.6

XG.2003.800.6

XG.2003.800.6

XG.2003.800.6

XG.2003.800.6

XG.2003.800.6

XG.2003.800.6

XG.2003.800.6

XG.2003.800.6

XG.2003.800.6

XG.2003.800.6

XG.2003.800.6

XG.2003.800.6

XG.2003.800.6

XG.2003.800.6

XG.2003.800.6

XG.2003.800.6

XG.2003.800.6

XG.2003.800.6

XG.2003.800.6

XG.2003.800.6

XG.2003.800.6

XG.2003.800.6

XG.2003.800.6

XG.2003.800.6

XG.2003.800.6

XG.2003.800.6

XG.2003.800.6

XG.2003.800.6

XG.2003.800.6

XG.2003.800.6

Collected: 04-23-03 13:50:00 By: SP




--~:-:-::-:-:---+---~-:-~ -~-:~-~-::-~-:-::-~-:-~-:----+---~-~--·-'--~-ci-~-~-- -~~~~r- ~~--~- _--i __ ·1 ~::~::~: 05-07-03

05-07-03"· ' -7--1--5-5--6___, ___ 1,1,1 Trichloroethane ND ug IL - ·1 ·· r·_()_._1_· ----+·-_·-_-_·-··...,·· 05-06-03 05-07-0:., ..

05-06-03 05-07-03· 630-20-6 1, 1, 1,2 Tetrachloroethane ND ug I L 1 I 0.1

_79-00-5 1, 1,2 Trichloroethane _______ l. _______ N_D ___ -1--::_-=._u-g"--_/-::_L-::_-::_~_--_1_-_._j_ri-_--_-_0_~_1 __ -- ------ 05-06-03 05-07-03'·

1, 1,2,2 Tetrachloroethane i ND ug IL 1 : 0.1 05-06-03 05-07-0:.. 79-34-5

563-58-6 1, 1-Dichloropropene ----1 ND ug I L 1 0.1 05-06-03 05-07-03

I 05-06-03 05-07-03''' ·-------l----------·------+-------l---'------1-----·

_1:-5~-:-:-~4-f----1_,2_1 __ ~_ib_~-~cm_h_~-~:-hb-:-~-:-~-~-~_B_) --+-1 --~-~----- _ ~ci+~-- _ -+-i-%.+ -------

---·------1--------------f------l-----+-----l----------+---j 107-06-2 0.1

0.1

1,2 Dichloroethane (EDC) ND ug I L ---~--------------+----··----- __ _:: __ +----~----1-------1

78-87-5 1,2 Dichloropropane i ND ug IL -----+----- - ----- -r----· _ .. ·----- -- --

_9_6-_1_8_-_4_r- ____ 1_,_2,_3_T_r_ic_h_lo_r_op_r_o_p_an_e __ ~1-___ N_~-- ~_l:_j_ 1 , 0.1 l 18;;~~~~1 ~ :~:!~~~:~~::~:::~::~: ~--- -~~-----L--~: ~ ~ i ---~ - L- ~:~ ~ ===1 _9_5-_63_-_6--+ __ 1_,2_,_4_-T_r_im_e_th_y_lb_e_n_z_e_ne __ ~! ____ N_D______ ug IL I 1 I 0.1 I

96-12-8 1,2-Dibromo-3-chloropropane : ND ug IL i 1 0.2 I j

541-73-1 1,3 Dichlorobenzene _____ ND I ug IL , 1 __ _ _ 9~~------i----~ 108-67-8 1,3,5-Trimethylbenzene 1 ND ug IL i 1 __ o·~--+---1

1_1_4_2-_2_8-_9__, ____ 1_,3_-_D_ic_h_lo_ro_p_r_op_ane ND ug IL j -~- • 0:2 J ---~

106-46-7 1,4 Dichlorobenzene i ND ug I L 1 1 : 0.1 I :

::;';;', ~:~~::~:.~:::: - : ~~ :: ; ~ • : ~~ T -95-49-8 2-Chlorotoluene I ND ug I L

1 1 0.1 I

-i-06 ___ 4_3-.4-+---- 4-Chlorotoluene i ND ug I L 1 1 1 0.1 --+------ ! -----1-----------------+-------l-- -+--------+---~1-----------j

_7_1-_43-2 ____ Benzene 1 ND ug IL I 1 ~-----~1- __ ~- I

108-86-1 Bromobenzene ND ug I L 1 1 : 0.1 ---------+----·- . -· --~- ----~ _________ ____, ______ +-------"

Bromochloromethane i ND ug I L : 1 0.1

Bromo:;:~:~:~;thane __ I ___ -~~--t~~ -+-+---%.~- r----

Bromomethane --- .. --" -- ND l ug IL 1 I 0.6 ---- --·--·----+-·-· ---·------ -----1----------f----------- ------

75-27-4

75-25-2 ----·-·----74-83-9

56-23-5 Carbon tetrachloride ND ug I L 1 ~ 0.1 -1-08--9-0--7-1------C-hlorobenzene ND ug IL ---1----t-- 0.-f --~----

--r-----

_1~~~~~~-- ___ C_h_lo_r_o_d_ib_ro_m_om_e_th_a_n_e __ -1---__ N_D _____ ~~i_~-- -----~--- _____ o __ · __ 1_ ---+---

75-00-3 Chloroethane ND ug IL 1 0.1 ---------------+------l-----+-----1---

Chloroform ND ug I L 1 0.1 ---------------1------------------+-------'---'---_j__ ___ __j_ _____ -+-__ _,

67-66-3

74-87-3 i Chloromethane ND ug IL 1 0.1 ----------'------------ ---------- -- ----··--·-------- ~-------- --- --- -- ------

__ 1_5_6-_5 __ 9-_2--+; ___ ci:::~.2-~!9hl~?_e_th_e_n_e ___ -+----N~ __ _J __ lj~L~--- __ 1 -_-_1_- --~~~ 1~~6-~~----cis-1,3dichloropropene ND ~_ll9-~_ 1 [ ------+-----1

_7_4_-9:!_i__ ______ D_ibr _o_m_o_m_~_th_an_e_____ ----~~----_[ _ ~-~'~ ____ 1 _ __j_ ___ o_._ 1 ____ ~ ___ _

10~:41-4 ! Ethylbenzene N_I)__ 1

__ u~~~ 1 0.1 -------+----1-----

--:~-:-::-:-:--+! ___ H_e_x_a_c_~-~:-~o-nb_~-:-ad_i_e-ne-----'----~-~-----~~-~-- ---~ --+---~-}----t-- ----------+----'-----'----

98-82-8 lsopropylbenzene ND ug IL ___ 1 _ -~O~!_L_ __ _

05-06-03 05-07 -0:> ..

05-06-03 05-07 -03·

05-06-03 05-07-03' ,,. 05-06-03 05-07-0::i. ..

05-06-03 05-07 -0'.'

05-06-03 05-07 .03'

05-06-03 05-07-0s,.

05-06-03 05-07-0:.>'

05-06-03 05-07-03,

05-06-03 05-07 -Os

05-06-03 05-07-0:>

05-06-03 05-07 -03

05-06-03 05-07-03,

05-06-03 05-07-02'

05-06-03 05-07 -03

05-06-03 05-07 -03

05-06-03 05-07 -07 ., 05-06-03 05-07-03.

05-06-03 05-07-03

05-06-03 05-07-07

05-06-03 05-07-03.

05-06-03 05-07 -03'

05-06-03 05-07-0:'

05-06-03 05-07 -0~

05-06-03 05-07-0:3'

05-06-03 05-07 -0~

05-06-03 05-07-0~

05-06-03 05-07-03

05-06-03 05-07-0:

05-06-03 05-07-03

05-06-03 05-07-03'

05-06-03 05-07-0:.

05-06-03 05-07-03

05-06-03 05-07 -03

05-06-03 05-07-0:.


STANDARD



Client:

Project:



Sample: TRIP BLANK Matrix: GW

QC Group

0304504-09A

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

0304504-098

X03200

X03200

Run Sequence

XG.2003.800.6

XG.2003.800.6

XG.2003.800.6

XG.2003.800.6

XG.2003.800.6

XG.2003.800.6

XG.2003.800.6

XG.2003.800.6

XG.2003.800.6

XG.2003.800.6

XG.2003.800.6

XG.2003.800.6

XG.2003.800.6

XG.2003.800.6

XG.2003.800.6

XG.2003.800.6

XG.2003.727.33

XG.2003.727.33

Sample: NCLF-3

Matrix: GW

QC Group

0304504-1 OA

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

Page 39 of 44

Run Sequence

XG.2003.800.12

XG.2003.800.12

XG.2003.800.12

XG.2003.800.12

XG.2003.800.12

XG.2003.800.12

XG.2003.800.12

XG.2003.800.12

XG.2003.800.12

XG.2003.800.12

XG.2003.800.12

XG.2003.800.12

XG.2003.800.12

XG.2003.800.12

XG.2003.800.12

Collected: 04-23-03 13:50:00 By: SP

Dilution Detection



75-09-2

91-20-3

104-51-8

103-65-1

95-47-6 i 108-38-3/106-42 135-98-8 I

100-42-5

156-60-5

10061-02-6 I

r-- -------- ___ ,, __ -

Methylene chloride ND ug IL 0.5

Naphthalene ND ug IL I ------- _._ ________ - - - -· -- -- ·-------------------------

n-Butylbenzene ND ug IL 0.1 ----- ----------------

n-Propylbenzene ND ug IL ---

o-Xylene ND ug IL ---- ____ _._J_

p/m-Xylenes ND ug IL ----- - ---- - --· ---- -·- --·-----------

1 i O.~

---~[~~:t~_t:_ ----s-ec--s;t~!~:-zen_e_ · -- -~-~~ _ J ~~ ~-~-T--~--1--~-~ ---f=~--~

t-1,2 Dichloroethene ND ! ug IL I ' 0.1 l t-1,3 Dichloropropene ___ f-J_[)_ _

1 ug IL i 0.1 -~ ___ _

98-06-6 , tert-Butylbenzene ND ug I L 1 0.1 , -------t--- ----------------·- -·------ ----c- ------ -1 - !. I - I

:~:::::: Tetrac~~~~:~~ylene ! ~~ -;-~~; ~ ~--~-+---~:-~ ! -1 - -----------·--------- ----+ ----f----- I I --1---- -1

79-01-6

75-69-4

75-01-4

-Tri-c~-~~-~:~~~~-~o-t:_ee-~~-a-ne---+-----N_D __ :--""-'-' i 1 j O

1 t-Vinyl chloride __ --~~- __ j_ __ ~~~-t~- ~-+ -~:-~ --- _. .... 1

EPA 504 EDBIDBCP by GCIECD By: ALG

Prep Run

Date Date

05-06-03 05-07 -03

05-06-03 05-07-03

05-06-03 05-07-03

05-06-03 05-07 -03

05-06-03 05-07 -03

05-06-03 05-07 -03

05-06-03 05-07 -03

05-06-03 05-07 -03

05-06-03 05-07-03

05-06-03 05-07 -03

05-06-03 05-07-03

05-06-03 05-07-03

05-06-03 05-07-03

05-06-03 05-07-03

05-06-03 05-07 -03

05-06-03 05-07 -03

1

---_ ----1,2-0ibromo=-3-chlo-ro-p-ro_p_a_n_e_~--N-D--~-ug t L 1 I 0.025 o5-05-03 o5-06-03

1,2-Dibromoethane, EDB ND ug I L ---1 io.o.25 05-05-03 05-06-03 -------· : __ - . I_ --

Collected: 04-23-03 11:20:00 By: SP




~:~~;::_J--=_ ~: ~ ~:~~::~:::~:~: --+----~-~---+--~-~-;-~_-_+==~=~~I- -~: ~ -f -~ ~::~::~: ~::~;:~: ___ 1_,_!_._1__~c_h_l_o_ro_e_th_a_n_e __ --t-__ N_D ___ t-_u_g_l_':__~ ___ 1 ___ l 0.1 ___ ; -~ 05-06-03 05-07-03

1, 1, 1,2 Tetrachloroethane N_D __ +-~L--~---1 _____ --i 0.1 --'-----! 05-06-03 05-07-03 1, 1,2 Trichloroethane ND ug IL I 1 ' 0.1 1 05-06-03 05-07-03

---------··--- ----------------------- -------- ---- -- - +-------- ---- .j

79-34-5 1, 1,2,2 Tetrachloroethane _ -~~--- j ug IL i 1 0.1 05-06-03 05-07-03

ND --l- ug IL j _ 0 1 05-06-03 05-07-03

ND 1

ug IL I 0.1 __ ~ 05-06-03 05-07-03

1,2 Dichlorobenzene ND j ug IL [ 1 0.1 I 05-06-03 05-07-03

10?-06~2----1,2oicillOroethclne(EoC) ND I ug/L r -1- --- 0.1 ' i 05-06-03 05-07-03

78-87.:S-- 1,2 Dichloropropane -· 1- __ N_D_ -1--ug-/L- r1- 1 o 1 i : 05-06-03 05-07-03

96-18-4 1,2,3 Trichloropropane ND ~L-- -- 1 1 0~1 -t- -! 05-06-03 05-07-03

,';;:~·, : :~:~ ~::::~:::::;: - ~r=-f ~~; t -. : i _ :: __ - I :::::::: :~;::: 95-63-6 1,2,4-Trimethylbenzene ND , ug IL 1__ l _ 0.1 _ _ 05-06-03 05-07-03

----------+----------

563-58-6 : 1 , 1-Dichloropropene --- -------L-- --- - ------~----~--------

106-93-4 1,2 Dibromoethane (EDB)

95-50-1




Client:

Project:



--- ·-----~-·--·------ ------- -------

Collected: 04-23-03 11 :20:00 By: SP Sample: NCLF-3 Matrix: GW

QC Group

0304504-10A X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

X03206

Run Sequence

XG.2003.800.12

XG.2003.800.12

XG.2003.800.12

XG.2003.800.12

XG.2003.800.12

XG.2003.800.12

XG.2003.800.12

XG.2003.800.12

XG.2003.800.12

XG.2003.800.12

XG.2003.800.12

XG.2003.800.12

XG.2003.800.12

XG.2003.800.12

XG.2003.800.12

XG.2003.800.12

XG.2003.800.12

XG.2003.800.12

XG.2003.800.12

XG.2003.800.12

XG.2003.800.12

XG.2003.800.12

XG.2003.800.12

XG.2003.800.12

XG.2003.800.12

XG.2003.800.12

XG.2003.800.12

XG.2003.800.12

XG.2003.800.12

XG.2003.800.12

XG.2003.800.12

XG.2003.800.12

XG.2003.800.12

XG.2003.800.12

XG.2003.800.12

XG.2003.800.12

XG.2003.800.12

XG.2003.800.12

XG.2003.800.12

XG.2003.800.12

XG.2003.800.12

XG.2003.800.12

Dilution Detection



96-12-8 1,2-Dibromo-3-chloropropane I ND 1

ug IL I 1 ~0.-2 ~

~:::~~ 1 .~~-~~~~~~:::~::~e +: N~D~ u~-g~/~~L : ---.1~ --._ti ~00()_.~2'.- l 142-28-9 1,3-Dichloropropane 106-46-7 1,4 Dichlorobenzene . ' -ND- . u-g IL -1 ·- --0.1-T-----=1

::~ ~:~~E:::::: I ~~ -t::~f ~ +-~l i 1 ~1~~~~4 4-C~l:~~~~~ene +=~~ ~~-i- ~=f- ~:}--L~-1 1Q8:85.1 Bromobenzene ND ug I L ± 1-- - O ~ I ~

Bromochloromethane ND ug I L 1----t-· 0.1

75-~f-41-- Bromodichloromethane __ No:=l ug IL - ' - 1 ~h._1 __ --_

75-2~ Bromoform -T ~=- ug/Lt 1 jo.1 1

74-83-9 I Bromomethane I ND ug 1Li 1 I 0.6

15:~:3;~7 -I -- ~~~:~~~~:de-~--L -- ~~- ~-f~~~t --·---~-~~;---~\ EJ 124-~-- Chlorodibromomethane __ · .. __ 0.~'1_ -+- ug~- . _ _2_ ,_ O.~ ---[- _'

:~:~~:~ ,-----c~~e---+- ~~-jj-L ~~-~~ 1 ~--1---~~~---~,----l -- --+---.. -------- ----·----------1------------ --j _74-87-3 L Chloromethane ---·f--~D ~g/L-r __ 1 __ ' -~--1 ____ _

156-5--=~- cis-1,2 dichloroethene ND --~TI- ___ 1_J__~1 : _

1

10061-01-5 cis-1,3 dichloropropene ND I ug IL · 1 \ o._1-+~ 74-95-3 D;bromometh'"e ND I "" L 1 I o,~--+ -1

, _1_0~-41-4 Ii Ethylbenzene ND ~I ug f_!::.__f----1 -~·-1 __ ,

1

1

787

5--67

81--8

3 , Freon 12 0.22uu_g

9

_ 1

1 LL : __ 11 ____ ~00_.11_ __

Hexachlorobutadiene ND

' 135-98-8 sec-Butylbenzene I ND i ug~-- 1 r_H_c>:-1=~1-_---1 . 100-4~ Styrene · ND I u~_ 1 : 0.1 f- j I ,,,_,...-r- t-1,Wohlocoetheoe =+ -ND m- "' '-~ I ::_. I _:o 1 1- - ! , 10061-02-6 1 t-1,3 Dichloropropene __ : ND i ug IL , 1 I 0.1 : _ 1

-,';;'.,';: 1 _ ,.~:~:::;:~.- , ~J~ -=r~ii:~-Er - :~-t-J , 108-88-3 ; Toluene 1 ND : ug IL ! 1 0.3 t' : -~9~1-6 I -----TrichiOrOe!hene - H~-N~___j_ ug /L-J--1 _____ 0:1n_-~- ~=--J

STANDARD

Prep

Date

05-06-03

05-06-03

05-06-03

05-06-03

05-06-03

05-06-03

05-06-03

05-06-03

05-06-03

05-06-03

05-06-03

05-06-03

05-06-03

05-06-03

05-06-03

05-06-03

05-06-03

05-06-03

05-06-03

05-06-03

05-06-03

05-06-03

05-06-03

05-06-03

05-06-03

05-06-03

05-06-03

05-06-03

05-06-03

05-06-03

05-06-03

05-06-03

05-06-03

05-06-03

05-06-03

05-06-03

05-06-03

05-06-03

05-06-03

05-06-03

05-06-03

05-06-03

Run

Date

05-07-03'

"' 05-07-03 ..

05-07-03

'" 05-07-03

05-07-03-

05-07-03

05-07-03

05-07-03-

05-07-03

05-07-03

05-07-03·-

05-07-0:?

05-07-03,

05-07-03

05-07-0:?'

05-07-03

05-07-03

05-07-0:'

05-07-03,

05-07-03'·

05-07-0c

05-07-03

05-07-03'

05-07-0:

05-07-03

05-07-03'

05-07-0~

05-07-03

05-07-03'

05-07-0:

05-07-0:'

05-07-03'

05-07-0~

05-07-0?

05-07-0~

05-07-03

05-07-0.

05-07-0"

05-07-03

05-07-0-

05-07-0'

05-07-03

Page 40 of 44 SQLCoyote: Reports 1.0.0305281535XX Report Date 6118103 2:43:45 PM.



Client:

Project:



----- ------------------------- -------------- ----------- --Sample: NCLF-3 Matrix: GW

QC Group

0304504-1 OA X03206

X03206

0304504-1 OB X03200

X03200

0304504-1 oc X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

Run Sequence

XG.2003.800.12

XG.2003.800.12

XG.2003.727.34

XG.2003.727.34

XG.2003.703.26

XG.2003. 703.26

XG.2003. 703.26

XG.2003. 703.26

XG.2003.703.26

XG.2003. 703.26

XG.2003.703.26

XG.2003. 703.26

XG.2003. 703.26

XG.2003.703.26

XG.2003.703.26

XG.2003.703.26

XG.2003.703.26

XG.2003.703.26

XG.2003.703.26

XG.2003.703.26

XG.2003.703.26

XG.2003.703.26

XG.2003.703.26

XG.2003.703.26

XG.2003.703.26

XG.2003. 703.26

XG.2003. 703.26

XG.2003.703.26

XG.2003.703.26

XG.2003.703.26

XG.2003.703.26

XG.2003. 703.26

XG.2003.703.26

XG.2003. 703.26

XG.2003. 703.26

XG.2003. 703.26

XG.2003. 703.26

XG.2003.703.26

XG.2003.703.26

Collected: 04-23-03 11:20:00 By: SP

Dilution Detection



I .

75-69-4 ·r. - Trichlorofluoromethane r- ··~·· -~!:)-~±- ug I L_T==-1 _-: 0.1 _L-] 75-01-4 1 Vinyl chloride ND -~~!_L [ . 1 __ i _0~1_ = ! =]

EPA 504 EDBIDBCP by GCIECD By: ALG

II -

_____ 1 __ .2-D~:.:.:.o. --3.-chloropropane --~~N-·DD--=ruug9 11

LL ~-~1 -=f. ~ 00

._002255=-+----··.1

_ 1,2~[)ibro111oethane, ED_B_____ L . • .•. J ______ , __ .. __ .L.. __ _


' 120:.-82-'1 .. _l 1,2,4-Trichl_o __ r.o __ b_enzene ND I ""UQ/LT_1_ L f- +- ' : 95-50-1 t- 1 2-Dichlorobenzene ND .- ~ =~'ii.. L --1-l -- f t= __ .J

·54j_73:j'-. ----·1,3-Dichlorobenzene ND t ug I L j __ 1 __ j_ __ 1 . i---==' 106-46-7 i 1,4-Dichlorobenzen~ ___ __j __ __l'J.c:l_ ___ L_u_g IL I 1 1

90-1~-~ _ _2_:-~thylnaphthalene __ t ND _u~ !_!:__ 1 -~ _5~90-2 2,3,4,6-Tetrachlo~op_ll_eln~-- _ _t-J_[) __ __ _ ug IL 5

1, _ ---1

95-95~4 _ -~_.4_.5-Trichlorophenol __ ND u2_t_L:____ 5 .. __ -1 88-0~-~- ____ 2,4,6-Trichlorophenol_ _ N.!:>__

1

ug IL 5 .. _ ... -:! ______ ._·_-_~' 120~8-=~-- 2,4-Dichlorophenol .... J _ -~~ _ ug IL 5

105-67-9 f 2,4-Dimethylphenol ' ND ug IL -·-----,.-------·

51-28-5 2,4-Dinitrophenol ND ug IL 1 O -·- ---- ---- ----------

121-14-2 2,4-Dinitrotoluene ND ug IL ----+---------606 -20 -2 I 2,6-Dinitrotoluene ND ug IL

--- -·--------+-----·t 91-58-7 2-Chloronaphthalene ND ug I L ---~------ ------ ------- -- -- 1----·~--

95-57-8 2-Chlorophenol ND ug I L .. ---.. ·j-------

1 91-_5_7_-6_+---__ 2_-M_e_t_h_y_ln_a_p_hthalene 1

ND 1 ug I L

2;~~:~:~~l~nneol ····--r. ~~ -~~ ~~ ~ ~ ______ _ 95-48-7

88-74-4

88-75-5 2-°NitrOPilS~ ND -- --ug I L -,---1 --

91-94-1 3,3-Dichlorobenzidine ND U91Li-1 --

3+4 Methylphenol ND ug I L 1

5

5

5

10

----+------------ --- ----- ------ ·-·-+----.. -- ... 99-09-2 3-Nitroaniline ND ug I L 5

101-55-3 4-Bromophenyl-phenylether ND ug IL

s34:s2C1 -- -4.6-rno;t,.,-2-methylphMOI t --~ ,-g··-,--L·---t--·---t-- . 10

-- - - - --- _______ .,_._.-...... , 59-50-7 4-Chloro-3-methylphenol ND ug IL

106-47-8

7005-72-3

100-01-6

100-02-7

83-32-9 ----

208-96-8 ..

62-53-3

120-12-7

- - ---

4-Chloroaniline ND ug IL +·----------t---

4-Chlorophenyl-phenylether ND

4-Nitroaniline

4-Nitrophenol

Acenaphthene

Acenaphthylene

Aniline

Anthracene ------ - -------

Azobenzene& 1 ,2-Diphenylhydrazine

ND

ND

ND

ND

ND

ND

ND

ug IL

ug IL

ug IL

ug IL

---+---------------+-------------56-55-3 Benzo (a) anthracene ND ug IL

- ----------5

10

1

10

I j

Prep

Date

STANDARD

Run

Date

05-06-03 05-07-03

05-06-03 05-07 -03

05-05-03 05-06-03

05-05-03 05-06-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-03


STANDARD



Client:

Project:



Sample: NCLF-3

Matrix: GW

QC Group

0304504-1 OC X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

X03165

0304504-10D X03194

X03194

X03194

X03194

X03194

X03194

Page 42 of 44

Run Sequence

XG.2003.703.26

XG.2003.703.26

XG.2003.703.26

XG.2003. 703.26

XG.2003.703.26

XG.2003.703.26

XG.2003.703.26

XG.2003.703.26

XG.2003.703.26

XG.2003.703.26

XG.2003.703.26

XG.2003.703.26

XG.2003.703.26

XG.2003.703.26

XG.2003.703.26

XG.2003.703.26

XG.2003.703.26

XG.2003. 703.26

XG.2003. 703.26

XG.2003. 703.26

XG.2003.703.26

XG.2003.703.26

XG.2003. 703.26

XG.2003.703.26

XG.2003. 703.26

XG.2003.703.26

XG.2003.703.26

XG.2003. 703.26

XG.2003.703.26

XG.2003.703.26

XG.2003.703.26

XG.2003.703.26

XG.2003.703.26

XG.2003. 703.26

XG.2003. 703.26

XG.2003.785.28

XG.2003.785.28

XG.2003.785.28

XG.2003.785.28

XG.2003.785.28

XG.2003. 785.28

Collected: 04-23-03 11 :20:00 By: SP

Dilution Detection



! 50-32-8 I Benzo(a)pyrene ---r- -ND -~ il. -, 1 + 1: r~-, --· --Benzo(b & k)fluoranthene---r·-~------ug/L"l-~-i___~ __ _1~--- ~-~

191-24-2 Benzo(g,h,i)pery1ene=t--=iD _ ~u.- !_

1. __ 1

64-85-0 Benzoic acid ND ug I L 1 2 ----~- -------100-51-6 Benzyl alcohol ND 1 ug IL 1 5 ,

111-44-4 - bis (2-Chloroethyl) ether ----r;JD· ug/L' ---1--, - -1-- 1-- I

1 ···--+--- 1=E=-~------+---------------j-------j-----j------~r--- -- -

108-60-1 bis(2-Chloroisopropyl)ether ND ug IL 1 1 ]·-

117-81-7 bis(2-Ethylhexyl)phthalate 1 60 ug IL 1 5~jB "_ 1

2815~:~-~9 ' Butyl~~~~:~:alate _ -~~ _ ~:; ~±'.·-- --~ ~ ,':,_:: o;be~~:~;:~thra:'""e ~ f :::H-+-f i-- '_J

. --~~~66-2 D1ethylphthalate : ~-rrug ~ __ 1 _ __J____1 -~I __ J 1_31-11-3__ Dimethylphthalat_e ___ l~-- _tJ_~/L 1 _!--.,.---~--+-- I

,;~~~20 I -- :::~:~~::::::;:: ~ - -~~ H ' _::; ~ I _L Lt J 2~~:~0 -1==-~i~~~--=t= ~~-=-L ~:;t-;-=~-J--~+--~~-==J 118-74-1 Hexachlorobenzene -~- ug IL 1 1 _ _(_ __ __1_0:_ + 87-68-3 Hexachlorobutadiene ND ug '+-f=+ I 1 O _ 1 :;~::~ Hexa~~xo::~ra~~~~:~:iene ~~ -~ ~: ;tt=:~------1 ___ 15~ ~ 193-39-5 lndeno(1,2,3-cd)pyrene N_i:>____J_ _ u~ !~ _!_-1 _ 1 _:_____

;~:::: ~:::~;;;. I ---:- i :n ,-~-+ -~ - I

:;:~-, ,"~:~:~~'.~!.::;;, I £ ; ::~. ~-~t=-=1~_0 ____ --.. _~--~·-'·i····_-_.·_-1 86-30-6 n-Nitrosodiphenylamine 1 ND ug I L 1 ---·- -·-·~"

87-86-5 Pentachlorophenol ND ug IL I 1 10 I ·

':~:~: I Phe=~~:t ~~ I :: ; ~ : f ~ IH -· ~ 110-86-1 Pyridine ND I ug IL___ ~- ---~---i

111-91-1 ND ug IL bis(2-Chloroethoxy)methane


Prep

Date

Run

Date

04-28-03 04-29-03F

04-28-03 04-29-03"·

04-28-03 04-29-o::·

04-28-03 04-29-03.

04-28-03 04-29-03'•·.

04-28-03 04-29-0(

04-28-03 04-29-031'

04-28-03 04-29-03"•· .

04-28-03 04-29-o(,

04-28-03 04-29-03.

04-28-03 04-29-03''

04-28-03 04-29-0'.

04-28-03 04-29-03

04-28-03 04-29-03

04-28-03 04-29-0:'.

04-28-03 04-29-0:3

04-28-03 04-29-03

04-28-03 04-29-0:.

04-28-03 04-29-0?

04-28-03 04-29-03.

04-28-03 04-29-0:.

04-28-03 04-29-0?

04-28-03 04-29-03

04-28-03 04-29-0:.

04-28-03 04-29-0?

04-28-03 04-29-03

04-28-03 04-29-0<.

04-28-03 04-29-0?

04-28-03 04-29-03

04-28-03 04-29-0Ci .

04-28-03 04-29-02

04-28-03 04-29-03

04-28-03 04-29-o:,

04-28-03 04-29-0:

04-28-03 04-29-03

I ,,,~ . ·-~~~i"· f- ~_i=~i:i tr 1=H~-1 J ~~rn ~~= Chlo~~;~e~tota1 ___ ·~1_-··_--_:;tJ~:;t r=-~---+ :~ T _: ::::::::

05-09-o:,·

05-09-0'.

05-09-03

05-09-03

05-09-0'.

05-09-03

SQLCoyote: Reports 1. 0. 0305281535XX Report Date 6118103 2:45:05 PM

STANDARD



Client:

Project:




QC Group

0304504-10D X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

X03194

0304504-1 OD X03189

X03189

X03189

X03189

X03189

X03189

X03189

0304504-1 OE

M03548

M03548

M03548

M03548

0304504-10E

M03550

M03550

M03550

M03550

M03550

M03550

M03550

M03550

M03550

M03550

M03550

Page 43 of 44

Run Sequence

XG.2003.785.28

XG.2003.785.28

XG.2003.785.28

XG.2003.785.28

XG.2003.785.28

XG.2003.785.28

XG.2003.785.28

XG.2003. 785.28

XG.2003.785.28

XG.2003.785.28

XG.2003.785.28

XG.2003. 785.28

XG.2003.785.28

XG.2003.785.28

XG.2003.785.28

XG.2003. 785.28

XG.2003. 750.17

XG.2003. 750.17

XG.2003. 750.17

XG.2003. 750.17

XG.2003. 750.17

XG.2003. 750.17

XG.2003. 750.17

MT.2003.521.36

MT.2003.511.59

MT.2003.511.59

MT.2003.521.36

MT.2003.566.26

MT.2003.587.65

MT.2003.551.53

MT.2003.551.53

MT.2003.551.53

MT.2003.551.35

MT.2003.551.53

MT.2003.551.53

MT.2003.551.53

MT.2003.551.53

MT.2003.566.26

- - - - - --------------------------

Collected: 04-23-03 11:20:00 By: SP

Dilution Detection


SW846 3510B/8081A Pesticides by GC/ECD By: ALG 60

-

57

-1

I ---E-n~~:~r~~nl-- .. rn-1--~-~~-=- ~ ~~ ~ ~ f ~: ~ l ul :_ -EndosUifanil----1 -No ___ --ugh -- _ 1 ___ t---0~1::==c::_j

=---~=-=- __ -Endosulta.nSUifate ___ I --_N::o---=- . ug IL I 1 I 0 1 f I 72

-

20

-

8 Endri~~l::hyde ~~ T~~ ~ ~-=t- ~ -~=-~: ~ --== -=~ - - -- -! Endrin Ketone ! ND ug IL t- -1-- - 0.1 '

~:::: gd:~::~ ~~ t-;rn ~--;_ :0-_:1 _-r-.·.: ··~.I 1024-57-3 Heptachlor Epoxide ND

,::::,',+ M:::~~~t -. ~~ : ~~ i ~ I rr r-----. 1 50-29-3 . p,p-DDT !'!~--- _! __ ug_f__l-_ _l 1 0.1

8_001-~5-2 _,_____ Toxaphene, total ND ___ ~_ll_g_f _ _l-__L _ 1 2.5


12674-11-=2"!"'- Aroclor 1016 i--=-t-.J~-~~g-Z::L_}_1 __ - 0.5 - -- 1

:~:::: : - ~::~:J:t--=y ~i_·· -- :: : ~ ~L : -r=u==1' = .•. ~~~:~::::~ _ _;~~~~-~~~~+--~~ _ 1 ~;~t • L-~---,----~i_-_ - --=1

1 11096-82-5 Aroclor 12~~ _ .. 1 __ flj~---- ug IL 1 j 0.5 . _J

SW846 3005A/601 OA ICP By: JRE I 7440:41--7 Beryllium

-

1 0.002 -·-· i·

ND i mg/L

Prep

Date

Run

Date

04-29-03 05-09-03

04-29-03 05-09-03

04-29-03 05-09-03

04-29-03 05-09-03

04-29-03 05-09-03

04-29-03 05-09-03

04-29-03 05-09-03

04-29-03 05-09-03

04-29-03 05-09-03

04-29-03 05-09-03

04-29-03 05-09-03

04-29-03 05-09-03

04-29-03 05-09-03

04-29-03 05-09-03

04-29-03 05-09-03

04-29-03 05-09-03

04-29-03 05-07-03

04-29-03 05-07 -03

04-29-03 05-07 -03

04-29-03 05-07 -03

04-29-03 05-07-03

04-29-03 05-07 -03

04-29-03 05-07 -03

04-30-03 05-01-03

: 7440-47-3 ' Chromium o 02 i mg IL 1 O 01 1

cobalt ~D ---[~in.~~=- 1---r-o~~-=t=--co~£.~-- ----~___t-.l_[)_-~_111_g IL _ 1 o 01 1

I 7440-48-4

I 7 440-_50_-_8 ~-

I 04-30-03 05-01-03

04-30-03 05-01-03

04-30-03 05-01-03

SQLCoyote: Reporls 1.0.0305281535XX Reporl Date

04-30-03 05-08-03

04-30-03 05-14-03

04-30-03 05-05-03

04-30-03 05-05-03

04-30-03 05-05-03

04-30-03 05-05-03

04-30-03 05-05-03

04-30-03 05-05-03

04-30-03 05-05-03

04-30-03 05-05-03

04-30-03 05-08-03

6118103 2:46:48 PM

Client:

Project:

Order:





0304504 PHl16 Receipt: 04-23-03

Sample: NCLF-3 Collected: 04-23-03 11 :20:00 By: SP

Matrix: GW

Dilution Detection

QC Group Run Sequence CAS# Analyte Result Units Factor Limit

0304504-10E SW846 3005A6020 ICP-MS By:

M03550 MT.2003.551.53 I 1440-66-6 I Zinc 0.014 =r_:mg TCJ- -1 · -- 1

---- I 0.005

0304504-10E SW846 7470 Mercury by CVAA By:

STANDARC

Prep Run

Code Date Date

HMR 04-30-03 05-05-0~

JRE

M03559 MT.2003.522.42 I 1439-97 -6 I Mercury ND [mg ;-c-i--1-~ . [__~:OD?~ ·r--=1 05-01-03 05-01-03

Unless otherwise noted, all samples were received in acceptable condition and all sampling was performed by client or client representative. Sample result of ND indicates Not Detected, ie result is less than the sample specific Detection Limit. Sample specific Detection Limit is determined by multiplying the sample Dilution Factor by the listed Reporting Detection Limit. All results relate only to the items tested. Any miscellaneous workorder information or foonotes will appear below.

Page 44 of 44 SQLCoyote: Reports 1.0.0305281535XX Report Date 6118103 2:47:34 PM.



Client:

Project:



Order: 0304504 PHl16 Not applicable due to MDL proximity

-----.·----------- -----


Run Sequence

M03559 MT.2003.522. 16

X03200

XG.2003.727.9

XG.2003.727.9

X03206 XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

Page 1 of 25

Dilution

Factor

Detection Run


EPA 245.1 Mercury by CVAA M03559-002 7439~97~6-T Mercury _______ 9_8 ____ -_-_-_=:Li-~% Recoveryf 80--120=-- =-1-

EPA 504 EDBIDBCP by GCIECD


1,2-Dibromoethane, EDB

X03200-002 104 _______ I_ °lc_o Recovery-,1,--60-~--140 _i-_-__ 1_-_-_- r-NA--i-=J 9_9 ___ ~1_%_o_R_ecovery: _ 6_0 - 140 j_ __ 1 ___ t-=~~--~L-=.J

EPA 524.2 rev 4 Purgeable VOCs by GC/MS X03206-013 ·· ·r-----1 7-5--3_4-~3-__ -_:·· 1, 1 Dichloroeth_a_n_e ___ r_--_-_-_-__ 81 ____ '_% __ o_R_e_c_o_ve_ry ~ 70-130-r 1 . ~A---t---i

NA ! : 75-35-4 I 1, 1 Dichloroethene 80 _ ,,% __ R_e_co_v_ery i

71~ 1, 1, 1 Trichloroethane 91 % Recovery

70 - 130 1 --- ---

7_(l~_~q-~---~ - . J ___ ~_:_ ___ _,; -------+---- ------·-

_1

~0

6° __ --_ _; ::~:~:~ I -;~_> ~~~~- 1 ~~ +-----1 100 , %Recoveryt 70- 130 - __ , ____ NA ___ I "

630-20-6 i 1, 1, 1,2 Tetrachloroethane

79-00-5 -:-----1,1,2 Trichloroethane

79-34-5 1, 1,2,2 Tetrachloroethane

563-58-6 i 1, 1-Dichloropropene - -- ---~----.. C--------- -~- -----

98 1

% Recovery I 70 - 130 NA

05-01-03

05-05-03

05-05-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03 --------------------------+-------- - - 1- - - 1- ----------

1 ~~-_1_.~l:)~~romoethane (EDB) 105 ___ __ -t%o Recovery 70 ~--130_,._ _ __ _.. ,_ NNAA __ +=i ______ 05-07-03

95-50-1 1,2 Dichlorobenzene ~~ ~o Recov~ry __ !_()-_ ~30 L. 05-07-03

107-06-2 1,2 Dichloroethane (EDC) 97 I % Recovery 70 - 130 _l_ 1 NA 05-07-03

78~8~ 1,2 Dichloropropane 95 o/o Recovery I 70:.-130 --1- -~ NA 1---- 05-07-03

96-18-4 -1- 1,2,3 Trichloropropane 97 lo/o Recoveryi-70-- -130 --1-- -~ NA o5-07-o3

"87~61-6- __ 1_._2,3-Trichlorobenzene 105 I 0/o Rec~~~-~t m_:- _130 1 I - N __ A ____________ -j

120-82-1 ___ 1,2,4-Trichlorob~~zene 105 % Recovery! 70- 130 1

1

j'- NNAA __ 11 ______

1 05-07-03

95-63-6 1,2,4-Trimethylbenzene 992

8 °0~0 RReeccoovveeryry 1

1 77o

0 -_

1133

00

______ 1_ -------1--NA --+-- -~ 05-o7-o3

96-12:a-T1":2.Dibr0ma=3.:chloroP"ropane " g 1 o5-o7-o3

541-73-1+ 1,3 Dichlorobenzene ---~====-~~--- . % Recovery i 70- 130 -~--T=-~~--L--~ 05-07-03

108-67-8 1,3,5-Trimethylbenzene 105 '%Recovery 1 70- 130 1 : NA i I 05-07-03 ---- -· "---·--- ---1·----.--------J_------------t------- i---------------1----"

142:2_8:9 1,3-Dichloropropane ___ ~~ _____ J_'% Recovery I _!_q~_ 13_()_ L __ 1 NA _ ,__ _ : 05-07-03

05-07-03

106-46-7 1,4 Dichlorobenzene 98 'o,to__~~~11_ery 70-_130~1 ___ 1 --~---r-- 05-07-03

99-87-6 1,4-lsopropyltoluene 101 : % Recovery 70 - 130 ! NA , 05-07-03

594-20-7 2,2-Dichloropropane 1 88 ·-·: 01~RecovefY"T7o---13o! ___ --~--NA" o5-07-03

95-49-8 2-Chlorotoluene I 97 _

1

% ~~cov~ry -~-~~----------NA 05-07-03 1

106-43-4 1---- -4-Chlorotoluene I 99 °1< Recovery 70 130 1 1 NA 05-07-03 --y-1-..--43-2 -; Benzene r--- -- -- 94-----ro:a Recovery ~-GO 1--1- - ---NA _L __ -- 05-07-03

i0~6- 1 ~=Bro~~~~::::~heane 19°7° -------t;;···-·nl ~;~~~:~:~~ - ~f-~-~~+=~~--- ~; 1 ~::~~:~:

-7~:27~4- ____ BrOrll_~-~~l_oromethane - -- --101 - - %-Recovery I 7() ___ fa_o r---1 --NA I 05-07-03

75-25-2 Bromoform 107 : % Recovery 70 - 130 1

1 NA ____________ J 05-07-03 74~83-9 1 - Bromomethane ;- 87 - ·· -:-,;;o- Recovery ___ io-~-136T NA o5-o7-o3

,'!':~~ r C•~:,:,:~:~~::'· -'H :: rn -_-~::-~::~:--;~~ -~-~~-r 1 -- ~~ --~- -- -~::~~ :~: 124-..--48-1 --cliiorociibromomethane • 107' _____ ' 0/o Recove~---ro---130 1 -----NA- o5-o7-o3

:}~~~:: J-__ ----~~~~~~e :~ . ~ ::-~~-~:~T~~-~~~ 1 =-==~~-~- ~::~~:~: 74-87~3 Chloromethane 87 . % Re~~~.':Y_L_!__0_-_130__ 1 _____ l\j_~-- 05-07-03

156-59-2 cis-1 2 dichloroethene 91 % Recovery! 70- 130 ! NA I 05-07-03

10061:01.=_5 • cis-1.~dichloroprop~ne 106 %Recovery! 70-130 ____ r---NA----~--= 05-07-03

SQLCoyote: Reports 1.0.0305281535)()( Report Date 6119103 9:32:34 AM

STAN DAR['



Client:

Project:


APruL03SAMPLEEVENT Explanation of codes

~J Not applicable due to sample dilution

L _l Not applicable due to MDL proximity Order: 0304504 PHl16 ----------


Run Sequence

X03206 XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

XG.2003.800.4

X03206 XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

Page 2 of 25

-------------------------- -



EPA 524.2 rev 4 Purgeable VOCs by GC/MS 74 95 3 -- -·----oibromomethane 97 --- -.,-o/c-R.ecoveryT_70_13o __ _ - - 0 --

100-41-4 Ethylbenzene 91 % Recovery 70 - 130 1 NA -~--- -- ··-··.

05-07-o(· ...

05-07-oi

05-07-03"

05-07-0(

05-07-03

05-07-03'·

05-07-0:".

05-07-03•·

75-71-8 Freon 12 90 '%Recovery 70 - 130 1 NA ·----·- ·-- ----

87-68-3 I Hexachlorobutadiene 103 % Recovery 70 - 130 1

98-82-8 I lsopropylbenzene 105 '%Recovery 70 - 130 1

75-09-2 I Methylene chloride 82 % Recovery 70 - 130 1 I -- - ----- ---

'\;;<

05-07-03

05-07-0::,,. NA

91-20-3 I Naphthalene 107 ~°(o Recov_:ry 70- 130 1 -1-04-51-8 t-------n-Butylbenzene

---

______L---~--- % Recovery 70- 130 i 1 ----L-· 103-65-1 n-Propylbenzene 98 -~ Recovery _ 70- 130 I 1

----~ ---·-- ·--- i 95-47-6 a-Xylene 97 : % Recovery 70 - 130 1 ------ -- - ---- ------··-·-··-·-·

108-38-3/106-42 135-98-8

100-42-5

156-60-5

I -p/m-Xylenes I 94 ___ ___f\l~_l ___ J 05-07-03 i % Recovery 70 - 130 I 1 .L

--- - - ---- --

sec-Butyl benzene 95 . % Recovery 70 - 130 1 i NA 05-07 -03· ___ T_NP._ -_J_ ~ o5-o7-o3··

1---Nli.-··· 1··j o5-o7-o:>

----------------------------------- -------- ·-----r-

Styrene 96 ·%Recovery 70 - 130 1

t-1,2 Dichloroethene 85 % Recovery 70 - 130 1

10061-02-6 I

98-06-6

127-18-4

108-88-3

79-01-6 1

t-1,3 Dichloropropene --f----------------------- ---· ·------ ---

102 % Recovery ----r- NA , 05-07-0:.> --------------- ~--

70 - 130 1 r-- -----------+---------'

tert-Butylbenzene 100 1 % Recove~_.::__1_~~-- 1 NA ' 05-07-03

-------+--75-69-4 I

is-01:4· t I.

Tetrachloroethylene 97 i % Recovery i 70 - 130 1 NA -------c----- -·--+---- -----

70 - 130 : NA Toluene

Trichloroethene


Vinyl chloride

93 % Recovery i -----------+-------+---------- - - --

98 % Recovery i 70 - 130 _____ __ _ NA_ _ _

98 ____;{o Recovery I 70 - 130 NA -+ 7~ ____ ,_°;'o~e~~veryJ -~0_-_1]0 _____ ----==~-f'.J_A_~--


75~34:~ l ---1,--1-D ___ i_c-hl-o-ro-e-th_a_n_e ___ t~I _-__ -_-_-___ -_-_9_0 __ ~----.-~.-~o-RR;;---eccoovveerryyT-27-o0==_:=11 3300--:-1_. -~-11--==-- NNAA -~1 ___ --1_1

~::::: t- ,\\~-i~-i:-~0-1:-~-:-:~-~-:-~-e----+------:-~----~·, -;o-R-ec_o_v_e-ry-+--7-0----13--0- ---:i-- ~- NA --~----~ 630-20-6 1, 1, 1,2 Tetrachloroethane ·---- 10--5··--------·---~i0-Vo Recovery -70 ::- ·13·()--~-1- ----, - NA--i ------i

-~--- ------------+------------------+-------+-------~-

05-07-0:>

05-07-0:.'

05-07-03

05-07-o:;

05-07-0Z

05-07-03

05-07-0:;

05-07-0Z

05-07-03

79-00-5 I 1, 1,2 Trichloroethane 91 i % Recovery 70 - 130 1 NA i i 05-07-03

79-34-5 1, 1,2,2 Tetrachloroethane 117 ! % Recovery 70 - 130 1 I NA : i 05-07-0Z

563-58-6 1, 1-Dichloropropene _ -~-~~ -=i}~---=-~--~ % Rec~~ery_ -___ -7._0 _____ ·_-1_3._0--+---1---+---N-A---+I--____,

106-93-4 1,2 Dibromoethane (EDB) 99 : % Recovery 70 - 130 1 NA 1 I -------+---------------t-----------.-------t------ -- ··-- - ~----t---..J

19o5;:0i;2·+----1-,2-1 -~-ic-~-\~-~-:-;~-hb_ae_nn-:-~E-nD_e_C_) ____ ---- - ··~-~~---- -----~-=-:-~~~~ ---~t ~-~~ -- ~ ~~ I ~ 1,2 Dichloropropane 102 , % Recovery [ 70 - ~30 1 --t NA ___ 1__ __ _ 78-87-5

96-18-4 ------~'-87-61-6

120-82-1

95-63-6

96-12-8

541-73-1

_1_,~_,3 Trichloropropane ! 11 O ' % Recovery : 70 - 130 ' __ --_--__ 1 ____ -__ --~ ___ _NN_.~A___ i ____ _

1,2,3-Tnchlorobenzene 113 : 0/o Recovery i 70 - 130 _ I 1,2,4-Trichlorobe_~~-n~ _____ J____ --~~o____ . ~ _°(o __ ~e~~vert: __ 7__0 - 130 ~--------- _J_ __ .1'1_~--1,2,4-Trimethylbenzene ·-----·· 1_24 ____ j_% REl9overy :_~-_ECJ__. __ ~--- -f- NN.!'A

1,2-Dibromo-3-chloropropane _ -~09 i % Recovery I 70 - 130_~ _ 1_ _ --+--_,

1,3 Dichlorobenzene 130 % Recovery 70 - 130 1 NA __ -_68_·-=67_--=8======1=·=3 __ -._5-_~!-~-~m-et_h_y_lb_e_n-ze_n_e ______ --_-_-__ -___ 1_3_~------------------t-_0-Vo_R_e_c_o_v_e_ry-t--7-0---13--Cl--\ 1- -1

42-28-9 1,3-Dichloropropane , 107 % Recovery 70 - 130 1--1-- -: NA

NA

06-46~i ___ 1_,_4_D_i-ch_l_o_ro_b_e_n-ze_n_e--~----1-2_4 ____ -t-0-Vo Recovery- -- 70 - 130 ! 1 t- -NA-

99_-8 __ 7_-6_~ __ 1_.4 __ -_ls __ o_p_ro_p_y_lt_o_lu_e_n_e __ ~i _________ 1_3_8 ___ ~1 _%_R_ec_o_v_e_ry_~~ - _130 ) _ _ 1 ___ .l_NA __ !.. ______ _

05-07-03

05-07-03·

05-07-0Z

05-07-03

05-07-03

05-07-o:

05-07-03

05-07-03

05-07-0:

05-07-03

05-07-03

05-07-0:

05-07-03

05-07-03'

05-07-0:

SQLCoyote: Reports 1.0.0305281535XX Report Date 6119103 9:34:01 AM



Client:

Project:


APRIL 03 SAMPLE EVENT D

L

Explanation of codes ~ ------ - -- ----- -- -- . "'- ----- --

Not applicable due to sample dilution Order: 0304504 PHl16 . __ N()t ~[JPlicab/e due to/1.4£?_~(Jf()~~"!~fI J Type: LCS: Lab Control Spike Matrix: WATER

Run Sequence

X03206 XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

XG.2003.817.3

X03206 XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

Page 3 of 25




5~_~2_0-_7_~- 2,2-Dichloropropane 1_0_3 ___ 1 ~0 RReeccoovveerryy11 - 7

7

0

0

-_ 11 3300 -T~_-:-11 _____ 1 NN_AA__ ·-i----~ 95-49-8 i 2-Chlorotoluene 125 "

1(JEl-43-4-I 4-Chlorotoluene 1_2_9 __ --+--i-, -%_0-_R ___ e_c-o~v_-e-ry-rm~=~o_O[_ __ , NA __ [ ____ --•

71-43-2 I Benzene 106 i % Recovery I 70- 130 r' 1 NU_' I - --------1----------------·----- - ---------~--- ---------------, ----------------- - --- ------- ---~-- -- --- - - -··- ---108-86-1 Bromobenzene 118 : % Recovery I 70 - 130 1 : NA

----------+-----------r::- i------:----- ---- ----- ·-- . . ---t---

Bromochloromethane 92 1 % Recovery I 70 - 130 1' 1 NA -------------------------·-·---- -------··---- -··· 1' -·---·- -·· • -·-------··---··--··------------------1--

1 ~~~~~~-~--Bromo:::~~~~~;thane ~~~ __$ ::~~~:~ ;~ ~-~~~ +--+--- ---~~- _____ _ ~;[~-~:: =~==~a~~~~~e~r:~h~:~de ~~~ l, ~o :R:e~c:o-~v:e~ry~ !I ;7~0~=~1-~3~011=t1-~=~~-~--~-~N--~A_==_+ -~

__ ~08-90-7 I ________ Chlorobenzene 1 104 re

;~~:~~1 [ ---~1or~~~~~~~~-~----~~~--- ~ ~:~~~!-(y-f--~~~-}~~ =-T"--1 ~~=t=l 67:66:3 I - - Chloroform 93 % Recovery :--70---130 L- 1 :--f'J_~-t---~ 74-87-3'- Chloromethane 117 % Recovery i 70 - 130 : 1 i NA ------~ -------- -- --- I j __ l ____ j

156-59-2 ___ cis-1,2 dichloroethene -----~~-------"f'o_~~c;_ovef}l__~-~~:_1_3_0 _ _L _ i NA j. 10061-01-5 · Gis-1,3dichloropropene 112 %Recovery! 70- 130 i NA

' 74-95-3 - ---Dibromomettlane___________ g() ----- - 0/oReco\/erY ~ 76 - f3o j NA

! 10~=41-4 -~ _ --~E!_llYJ':_e_ri_~e_ri~ _ -·- __ _ __ _ 111 . ---=-~~-%-~ecove~--=?o---130--[=- - ~----~ NA • :

75-71-8 ~------~_E _______ ~ ______ 143 _________ _;__0!o_~~co_very ___ 7_~_- __ 1~9 +---~---L-NA __ J ___ j

;~ . ";::::;::;::~:· ~:! ~ :::::~ • ~}:: i ·-+ ---!-- -~~ ! ---- ~ 75-09-2 , Methylene chloride 82 ~o Recovery I 70 - 130 _ ~-1 - -1

1

~--91-20-3 _I _ Naphthalene 129 % Recovery 1 70 - 130 1 NA - -- ------+ - ---- ---------···-·---- ··--·--- --!- ----------- ------------4---------·------ ------

104-51-8 I n-Butylbenzene 131 % Recovery 1 70 - 130 i 1 NA ·--------------------,----------1------

103-65-1 n-Propylbenzene 125 % Recovery I 70 - 130 : 95-47-6 ! o-Xylene --- 123 % Recovery l-?o--:_-130---;-- -

- --------!--------------------------~-------------------------------·----------_J__ ____ _

, 108-38- I p/m-Xylenes 120 % Recovery ! 70 - 130 31106-42 I - -------------- -------~----------·-----

NA

NA

NA

j~-~,-:,- -t--:-e-:--:-~:-t:-io-:~-:-ez_t:--:-:-e--~----~-~6-~---• ~ ~::::tt~=~--f =t ~1~~- --~ 98-06-6 130 , NA

t-1,3 Dichloropropene 109 % Recovery 70 -

129 70 -

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03 127-1s=4·i- -- 130 1 -+--N-A----+---1 05-07-03

tert-Butylbenzene % Recovery -- ----··-·--

Tetrachloroethylene 104 % Recovery 70 -

' 1o~=sa-3 ~I 130 -+-----1 --~~- _ o5-o7-o3 Toluene 105 % Recovery 70 ---------

79-01-6 130 NA 05-07-03 I% Recovery Trichloroethene I 102 70 -I ------------- _______ ) ______ _

75-69-4 i T richlorofluoromethane 116 I% Recovery 70 - 130

130 Vinyl chloride 98 --i-o;o Recovery 70 ----------- -- - - ----- - ---- - ----- ----- ------- - - --

_75-=-01-4 l _ EPA 524.2 rev 4 Purgeable VOCs by GC/MS

75-34-3 1, 1 Dichloroethane 101______ 0;;-Rec0v-eryj 70 - 130 ----- -l

1, 1 Dichloroethene 84 % Recovery ! 70 - 130

1, 1, 1 Trichloroethane ~~--- -e-°!o Recoveryl=7:0~_:::~9 1, 1, 1,2 Tetrachloroethane 94 i % Recovery I 70 - 130

75-35-4 !

71-55-6 1--630-20-6 _ t


NA 05-07-03

NA 05-07-03

X03206-031 NA 05-07-03

-- --- -- ---- -- +----~

Report Date

NA 05-07-03

05-07-03

05-07-03

6119103 9:34:26 AM



Client:

Project:



. of Not applicable due to sample dilution r · CT NcifjpPlicable due to MDL proximltY.I Order: 0304504 PHl16


Run Sequence

X03206 XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

Page 4 of 25

--------------------·-·---·-----------------·---- ---------·--------------·-




-;::-::: : --D~: ;;::~:::~:,. -r ·. : ---,-~ ::::~~ :r:~ -1-= ~ l : -1 I ~[~ 1.21 ~i~~~:~0:::~:~~~s)- ;--=-~~==-~ . ·~~: ~~~--t---+=+-i ! -1-.----

95-50-1 1 ,2 Dichlorobenzene 106 % Recovery 70 - 130 1 NA ----- --- : - -------------------,---------------107-06-2 1,2 Dichloroethane (EDC) 94 I % Recovery 70 - 130 1 NA I

· 78.:Sl--5---- 1,2 Dichloropropane ___ 9_5__ % Recovery 70 - 130 - - -1 -~--NA ~r=-_-96-1~4 r _ 1,2,3 Trichloropropane 104 % Recovery 70 - 130 --1--r NA -+---= 87-61-6 +-- 1,2,3-Trichlorobenzene 106 % Recovery I 70- 130 _____ 1__ NA_-+-----i

~!~_-1_·_._ 1,2,4-Trichlorobenzene___,_ ____ 108 1 % Recovery 7~- 130 ___ 1 _____ NA _ i 95-63-6 1,2,4-Trimethylbenzene 100 % Recovery 70 - 130 1 NA

96~1T-Bt-- 1,2-Dibromo-3-chloropropane 99 % Recovery - 7

7

0

0

-_ 1

1

3

3

°0

1_.

1

-- 1

1

I NNAA --- ----

-541~i~a= 1 3 Dichlorobenzene 104 , % Recovery 1

108-6~4 ~,3,5-Trimethylbenzene 108 1 % Recovery 1 70- 130 -,---1-- - NA - -

~~:::::~ I ~::-~ii~~,':;:~~~~:~: --:·~- I ~ ::~:~:~ ~ _ _: ~ ==-~ ~~ =-·l=l 99-87-6 1,4-lsopropyltoluene 104 % Recovery 70-- 130 -···---1- ' -~ ~

':::,': '~~;~:~::,:;:"· ' 1~5 - ~=·~~ .· :=·1: -1 ~~::;>i .. . :::::::::: =i- !~ ~:~::~I jt ;~: r ; ~ r: u~ -·--.. - Bromochloromethane ---;---- ... -~- 1 0/c R -- 70 130--t-- ----- ·-· .,. ---:

.. _ . -··---- ________ . _ _ __ ____( _o _ e~over~ - ___ J_ 1 __ ~-Ill~- __ _,____ 1 75-27-4 Bromodichloromethane 95 1 % Recovery 70 - 130 1 NA 1s-25-2 -:-· _____ sromoform ---·---1()o ____ l 0£Recovery- _?_o--130 _L_:=t-N~.~~----74-83-9 i Bromomethane - ____ 1_C>_f ____ % Recovery . 70- 130 : 1 _____ i____!'l_~-56~2~ - - carbon tetrachloride 90 % Recovery~--7o -13o_i_ - 1 1 NA -~

_,_ ___ --~- --- ----------- -~ 108-90-7 Chlorobenzene 101 % Recovery/ 70- 130 i 1

1 NA

05-07-0Y' \,_.

05-07-03 ..

05-07-03'·-

05-07-03

05-07-03 ..

05-07-03'

05-07-03,

05-07-03.

05-07-03'

05-07-03.

05-07-03,

05-07-03''

05-07-03

05-07-03 ..

05-07-03'

05-07-03.

05-07-03•

05-07-03.

05-07-03.

05-07-03 05-07-03 ..

05-07-03

05-07-03

05-07-03

05-07-03.

05-07-03

05-07-03-

05-07-03.

05-07-03

05-07-03

05-07-03-

05-07-03'

05-07-03

05-07-03

74-95-3 , - Dib_r.o_m_om_et_h_a_ne _________ . __ 9_9 _____ % Recovery 70 - ·130 1 -~-~~_l _____ J 05-07-0:'

1oo4H I Elhylbeo"oe 98 ___ -+--0fc_o _Recovery 70 - 130 1 1

NA i · 05-07-03

75-71-8 Freon 12 . ___ 93 ____ ; ~o RReeccoovveerryY. ;~.- 7700 ~-2133_ 00 ______ 11-?N-~A~--- ~::~~:~: 87-6~-3 __ Hexachlorobutadiene 103 ___ " _J ~8~2-8___ lsopropylbenze __ n_e ___ - -_·-·-++-----10-8 __ '%Recovery : ___ 70 - 130 i 1 _ ( __ NA __ 05-07-03

75-09-2 I Methylene chloride 8~- % Rec_overy j 70 - 130_ !- __ 1__ ~A ___ -·-~ 05-07-03 - 9_1_-2_0-_3_ [~~- Naphthalene 113 % Recovery 70 - 130 ! 1 NA 05-07-02

-----·--------1------- -------·------ - ---- --- --1--------

104-51-8 n-Butylbenzene 101 t' % Recovery 70 - 130 NA 05-07-03

! 103-65-1 n-Propylbenzene 102 % Recovery 70 - 130 1 1--NA___ 05-07-03 +------+----··-· -t·----·----+----1

____ o_-X_yle_n_e_____ _ __ 1_0_0_ _ ---~ Reco~ry 70 - 130 ____ 1_ ! NA 05-07-o:: 95-47-6

SQLCoyote: Reports 1.0.0305281535XX Report Date 6119103 9:35:24 AM·

STANDARD



Client:

Project:



[)j Not applicable due to sample dilution -1 L L _f1Jot applicable due to MDL proximity Order: 0304504 PHl16


Run Sequence

X03206 XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

XG.2003.814.20

M03548 MT.2003.521.11

MT.2003.511.35

MT.2003.511.35

MT.2003.521.11

M03550 MT.2003.551.12

MT.2003.551.12

MT.2003.551.12

MT.2003.551.12

MT.2003.551.12

MT.2003.551.12

MT.2003.551.12

MT.2003.551.12

MT.2003.551.12

MT.2003.551.12

MT.2003.551.12

MT.2003.551.12

X03194 XG.2003.785.13

XG.2003. 785.13

XG.2003. 785.13

XG.2003. 785.13

XG.2003. 785.13

XG.2003. 785.13

X03189 XG.2003. 750.4

X03165 XG.2003.622.2

XG.2003.622.2

Page 5 of 25


EPA 524.2 rev 4 Purgeable VOCs by GCIMS -- ··------~-----~- -~------ --·

Range

Dilution

Factor

Detection Run

Limit Code Date

X03206-031 108-38-

3/106-42 __ ____E/_fl1_-Xyl~n_e~ __ 100 ______ ,_"f'o_"_eC()_Very 70 - 130 NA ! 05-07-03

135-98-8 sec-Butylbenzene ___ - -r- H 99 - 0/o RecolleryT 70 - 130 NA 1 100.42.5 Styrene r---10-o-----p1c,-R-ecovery 70- 130 i- NA

i~" ,~~f ~gJI:~~=~= @ g~~~ ~U~, ~ m~~~-F-=--J -1

~:~~8

:~:3

-~ -- ----;rid{~--:-~-:u-~-:~-;-:e_en_t~-a-n-e---+-----~~--1-~-o.-~.--1~--- ~ :::~~ :n~: --~ -J : ~+= 75~0~~~- L vfnyl chfor-fde 82 ~yo-Reco_very 70 - 130 ~- -1- _ _J_ NA -t --

SW846 3005A/6010A ICP M03548-002

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

120 I 1· ---NA---,-- 05-01-03 111 ' % Recovery : 7440-41-7 i Beryllium ~40-47-3 I C-h-ro-m-iu-m----~-

80-115 ; % Recovery :

7440-48:4 [- HU Cobalt 1

7~4~:50-8 ______ Coppe_r _____ l___

99 _ _ _L0/o_~~c~v~_ry __ 1

104 ' % Recovery i ---~-

80 -80-80 -

~lit~~ 3:__ -=j ::::::: 120 ~---- : ___ f'J~__ __ _j 05-01-03

SW846 3005A6020 ICP-MS M03550-002 744a:36-o __________ Antimo-ri-y·---- ··· ···r- -- -----~--====~-io/o_R-_e-_cavery r_--a~~~--11-5~--=i=~-- NA

~::~:~::r= ----~~----_-_-_--_-_-_ ~a_=_;_-~_-_m_~~----------_ --------·-~--- --·-~--_-_l,r, =-- 104 , % Recovery L ~~_:-_1_1_s_1 ___ _1_ NA -" 98 % Recovery~ 85 - 115 _L 1 _ j_ __ NA _ -L---7440-43-9 ___ £ad_rrli~_rll ·-f -----~~------- "f'o_~e_9~veryJ__~5-=_1_1_!i_+ I NNAA_ -!---·----,

~::~:~~:~ -------~-i:~I- -- -I ~~ ~~:~:~:;~' -~~= ~~~ ~ - 1 NA I - - -1

1

7!_-82--4-9--2 i_ ___ S_e_le_n_i_um ______ ~' ____ 100 , % Recovery 85- 115 !-==NN=AA-=~t=J,

I~~:~~~-::-:-~ T~~~:~ :: i ~ ::~~~:~' :~: H~- ~ - '. -__ NNAA~-= i=-==

440-31-5.. ' Tin 97 ' % Recovery i 85 - 115 -i 440-62-2 j Vanadium 96 ; % Recovery i 85 - 115 NA

440-66=6 J _ _ _ _:_ -_z=in=c===================1_00 ____ ,._o;,_~--R_e_c_ov_e_rr_--_'--_85_-=._f1~ NA '- ____ _J

SW846 3510818082 PCBs by GCIECD X03189-002

05-05-03

05-05-03

05-05-03

05-05-03

05-05-03

05-05-03

05-05-03

05-05-03

05-05-03

05-05-03

05-05-03

05-05-03

05-08-03

05-08-03

05-08-03

05-08-03

05-08-03

05-08-03

1 11096-82~5 I Aroclor 1260 -----~~-----__"!"--Re_9_~v~_ry_L 60- 120I--~ ___ J NA --. --- ] 05-06-03

SW846 351 OB/82708 SVOCs by GC/MS

120-82-1-· [ __ 1_._2.4-Tr~1orc:1J.:l'l.z_e_~: ___ _ 106-46-7 I 1_._~_-_c:>~c_hlo_ro_b_e_nz_e_n_e _____ _

79 72

% Recovery i

% Recovery 39 - 98 36 - 97

04-10-03

04-10-03


STANDARC Assaigai Analytical Laboratories, Inc.


Client:

Project:



! D _ _J Not applicable due to sample dilution

! L i Not applicable due to MDL proximity Order: 0304504 PHl16


Run Sequence

X03165

XG.2003.622.2

XG.2003.622.2

XG.2003.622.2

XG.2003.622.2

XG.2003.622.2

XG.2003.622.2

XG.2003.622.2

XG.2003.622.2

XG.2003.622.2

XG.2003.622.2

CAS#

____________ ,_

121-14-2

95-57-8

-- 59-50-7

100-02-7

83-32-9

117-84-0 --

621-64-7

87-86-5 ----------108-95-2

129-00-0

Analyte

SW846 35108182708 SVOCs by GCIMS

2,4-Dinitrotoluene

2-Chlorophenol t------··--

4-Chloro-3-methylphenol

4-Nitrophenol -----

Acenaphthene ·-·-

di-n-Octylphthalate

n-Nitroso-di-n-propylamine

Pentachlorophenol

Phenol

Pyrene

Result Units

80 '%Recovery

74 % Recovery

72 % Recovery

35 % Recovery

83 % Recovery -·

145 % Recovery ·-·--- .. --

81 .. ! % Recovery

81 '%Recovery -·--

38 , % Recovery -----

98 % Recovery --

Range

24 - 96

27 - 121

23 - 97 ~-

10 - 80

46- 118

26 - 127

41 - 116

9- 103 ---

12 - 89 -·-

26 - 127



X03165-002

1 ' NA I

1 i NA i 1 ' NA

1 I NA

1 --t---

1 NA

1 ' NA .. -·f-·-·-·---

1 J~--1 NA

l ---·-·--·---

1 NA ----+-------~----

1 NA ~

----~

04-10-0<,.

04-10-03 04-10-03 ...

04-10-0<,.,

04-10·0~

04-10-03.

04-10-03'"

04-10-0:!'

04-10-03''

04-10-03


Run Sequence

M03559

MT.2003.522.17

X03200

XG.2003.727.10

XG.2003.727.10

M03548

MT.2003.511.36

MT.2003.511.36

MT.2003.521.12

M03550

MT.2003.551.13

MT.2003.551.13

MT.2003.551.13

MT.2003.551.13

MT.2003.551.13

MT.2003.551.13

MT.2003.551.13

MT.2003.551.13

MT.2003.551.13

MT.2003.551.13

MT.2003.551.13

MT.2003.551.13

X03194

XG.2003. 785.14

XG.2003.785.14

XG.2003.785.14

Page 6 of 25



EPA 245.1 Mercury by CVAA M03559-003 7439-97-6 _ r_ Mercury _______ L ·-- ---------·--

4 NA _._J 05-01-03

EPA 504 ED81D8CP by GCIECD X03200-003

-__ --_-_-----------------Tl - 1,2-Dibromo-3-chloropropane l _____ ··-_-_--_3-_-_-_-=---___ -____ -_R __ -_P __ D__ I ·a-- 20---1-1 -- --- NA j~ . 1,2-Dibromoethane, EDS __ J_ RPO - r o--=---26 --r ---1 I -- NA -=r::= SW846 3005Al6010A ICP M03548-003

7440-47-3 - ------- -----

NA [l Chromium < 1 RPD 0 - 20 1 ---

Cobalt 8 i RPD 0 - 20 1

I

-·--~----

--1-- ~~· -i ___ Copper 7 RPD 0- 20 1

- -- ----+-7440-48-4

7440-50-8

SW846 3005A6020 ICP-MS M03550-003 ---- --7440-36-0 Antimony < 1 RPO 0 - 20 NA

7440-38-2 Arsenic 2 RPD 0- 20 NA ------

7440-39-3 Barium < 1 RPO 0 - 20 NA

7440-43-9 Cadmium 2 RPD 0 - 20 NA ----·------7439-92-1 Lead

I 2 RPD 0 - 20 NA

----- --·--- ... -----------I 7440-02-0 Nickel 1

7782-49-2 Selenium 1 < 1

7440-22-4 Silver ! -------1----~40-~- Thallium !

7440-31-5 Tin 1

Vanadium ! 2 I +--- ---·--Zinc < 1

----t----------1-=:~~~==HH= ;=~--;--i------RPO O - 20 [-- --1° r --NA ----~

RPO 0- 20 ! NA ---+---------+-------

RPO 0- 20 i NA -j---··----. ------j-------j

RPD 0- 20 NA ~;~~::~~L -·--~-------- -------··--------'--~~-- ~------------~-~

SW846 3510818081A Pesticides by GC/ECD

Aldrin

Dieldrin

Endrin

05-05-0:.'"

05-05-03

04-30-03

04-30-0Z

05-01-03.

05-05-03"

05-05-0Z

05-05-03

05-05-03

05-05-0::..

05-05-03

05-05-03

o5-05-0c

05-05-03

05-05-03"

05-05-0::.

05-05-03

05-08-03

05-08-0i ..

05-08-03


STANDARD



Client:

Project:



' D_,_ Not a~ei~~bie~cijfi__to samp!e di'1!_tl0n. I

Order: 0304504 PHl16 L Not ap{Jl_icable due to MDL proximity J


Run Sequence

X03194 XG.2003. 785.14

XG.2003. 785.14

XG.2003. 785.14

X03189 XG.2003. 750.5

X03165 XG.2003.622.3

XG.2003.622.3

XG.2003.622.3

XG.2003.622.3

XG.2003.622.3

XG.2003.622.3

XG.2003.622.3

XG.2003.622.3

XG.2003.622.3

XG.2003.622.3

XG.2003.622.3

XG.2003.622.3

- --- --


SW846 3510B/8081A Pesticides by GC/ECD --------- -- - .

g-BHC 5 RPO 0 - 15 58-89-9 I

76-44-8 T-- Heptachlor 10 RPO ! 0 - 20 - ---1- ' -------------- ------ ·-1

50-29-3 i p,p-OOT ~- __________ RPO _ _l_ __ ~::-~!

SW846 35108/8082 PCBs by GCIECD

l 1~0!)6-8.2~5_1_ Aroclor 1260 ________ _] __ 9 RPO 0 - 33

Dilution

Factor

----------

Detection

Limit Code

X03194-003

NA r·----· · NA

NA

X03189-003

NA ·1 - ··· 1

Run

Date

05-08-03

05-08-03

05-08-03

05-06-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03


Run Sequence

M03559 MT.2003.522.17

X03200 XG.2003.727.10

XG.2003.727.10

M03548 MT.2003.521.12

MT.2003.511.36

MT.2003.511.36

MT.2003.521.12

M03550 MT.2003.551.13

MT.2003.551.13

MT.2003.551.13

MT.2003.551.13

MT.2003.551.13

MT.2003.551.13

MT.2003.551.13

Page 7 of 25



EPA 245.1 Mercury by CVAA M03559-003 7439-97-6-,- ------·-Me-rC:Li-;y-- -------------102 - - ; 010-Re!coveryT so- - 120 NA 05-01-03

EPA 504 EDB/DBCP by GC/ECD

= ---,- 1,2-0ibromo-3-ch~o!~J:lr.opa_rie ]=-_- ~ 1.2-0ibromoethane, EOB

·---- -----

----~- ____ _L_ -

100

98

X03200-003

UT~=~i --i-----j_ ______ l ____ J

SW846 3005A/6010A ICP M03548-003

74-40---41--7-1

- Beryllium ____ =l ______ 1~~--==l?'o Recovery I 80 - 120 _ -=-~~ _-------1- - N~A~ =+1 7~40-47-3 I ______ c11romiur11_ ______ '.._ ___ 114 : % Recovery i 80 - 120 1 _.j 7440-48-41= Cobalt ____ 10~- ... __ %Recovery! 80 --12-0-j---- [ _____ ;

7~.icJ~50-8_1_ ________ gopper 111 % Recov_El_rX~--8~- 120 I ~_f'J"p, ______ J

SW846 3005A6020 ICP-MS M03550-003

~::~:~::~ ------ ----1~~-- ---- ~-: =-:-~-:~-:-~-1~1 -:-:~ ~~: 1----~- ~+-~~ I

~i--l~~=-l=-L------- -----~--c-:-~-if ~ -__ ___,__-_--E · ~ ~~~~~; t m j~= ~---__ -.~;-.~-.•. -_-.... -j.~ Antimony

Arsenic

7782-49-2 Selenium 101 ' % Recovery , 85 - 115_j_ ___ 1 __ NA __ .... •.····-··

05-05-03

05-05-03

05-01-03

04-30-03

04-30-03

05-01-03

05-05-03

05-05-03

05-05-03

05-05-03

05-05-03

05-05-03

05-05-03

SQLCoyote: Reporls 1.0.0305281535XX Reporl Date 6119103 9:37:25 AM



Client:

Project:



D Not applicable due to sample dilution 1 Order: 0304504 PHl16 L Not applicable due to MDL proximity '


Run Sequence

M03550 MT.2003.551.13

MT.2003. 551. 13

MT.2003.551.13

MT.2003.551.13

MT.2003.551.13

X03194 XG.2003.785.14

XG.2003.785.14

XG.2003.785.14

XG.2003. 785.14

XG.2003. 785.14

XG.2003. 785.14

X03189 XG.2003. 750.5

X03165 XG.2003.622.3

XG.2003.622.3

XG.2003.622.3

XG.2003.622.3

XG.2003.622.3

XG.2003.622.3

XG.2003.622.3

XG.2003.622.3

XG.2003.622.3

XG.2003.622.3

XG.2003.622.3

XG.2003.622.3



SW846 3005A6020 ICP-MS M03550-003 7440-2 2-4·r-· Silver 95 ; % Recovery 85 - 115 1

8~-1-- : % Recovery f-------

Thallium 94 85 - 115 1 i -- - -·-·----

1-5 I Tin 95 i % Recovery 85 - 115 1

-~~ ;% Recovery ---- -·-·------- --

Vanadium 94 85 - 115 1 -- ---------------- --r----------

6-6 L Zinc 99 I % RecoveryJ_~~~5 ___ 1

NA ----

7440-2

7440-3

-± ~~ t---

7440-6

SW846 3510818081A Pesticides by GCIECD X03194-003 · a-oe:oaTr Aldrin ------7-4·-----~0-Vo_R_e_c_o_ve-ry~,-4-0---1-20-~1-·---- NA I

60-57-1 ] Dieldrin 103 % Recovery 52 - 126 NA I 72-20-8 ! Endrin 102 % Recovery 56 - 121 NA --·---·----t---------------j·----------t--------j-----~----i-------r-------1

::~:: . H:~~?o~c _;,- ~ }~~~!-~~jtt=-, :---+-----+ SW846 3510818082 PCBs by GCIECD X03189-003

05-05-0~

05-05-03

05-05-03""

05-05-0"

05-05-03

" 05-08-03 •. 05-08-0:',.,

05-08-03 ,. 05-08-03

05-08-0:":k

05-08-0::>

l _ 11_0~~~~=~ [ .. _ _ Aroclor 1260 J 63 --r--·N.A.--[- _J 05-06-03

120-82-1 NA

i 621-64-7

X03165-003

---

04-10-0:h

04-10-0:.>

04-10-03

04-10-03-

04-10-0:.>

04-10-03

04-10-03·

04-10-0?

04-10-03

04-10-03

04-10-0Z

04-10-0~


Run Sequence

M03559 MT.2003.522.15

X03200 XG.2003.727.8

XG.2003.727.8

X03206 XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

Page 8 of 25

- -·-------- ----- -~------- ----------------------------



M03559-001 ------

7439-97-6


Mercury ND --------------·----------------~-----

__ u_; ____ } __ =~r-0.0062 I I 05-01-03

EPA 504 EDB/DBCP by GC/ECD X03200-001

1,2-Dibromo-3-chloropropane I ND ug I L -------~- ----

1,2-Dibromoethane, EDB ND ug I L - - -- ----~------------------------ ------------~ .. --- ----------

---r-~:~~: I I 05-05-03'"

05-05-o:


7~~4~- ~---1_,1_D_i_ch_l_or_o_e_th_a_n_e __ ~ ____ N_D ____ -+-__ ug_/ _L_-+-------'---!~ __ 75-35-4

71-55-6

1, 1 Dichloroethene ND ug I L 1 ----+-----+------~-----·

1, 1, 1 Trichloroethane ND ug I L --~------------~-------~-----~--------·--L

SQLCoyote: Reports 1.0.0305281535XX Report Date

X03206-012 05-07-03

05-07-03'·

05-07-o::'

6119103 9:38:17 AM'

STANDARD



Client:

Project:



D Not applicable due to sample dilution Order: - ------ -----------

' L Not ap_plicable_:Ju_e_t~!!fDL proximity __ , 0304504 PHl16


Run Sequence

X03206

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

Page 9 of 25




63i~ 1, 1, 1,2 Tetrachloroethane __ j___ ND i- _ u~/_L ___ -: ,-~=~~~~~~-=-~-79-00-5 . 1, 1,2 Trichloroethane : ND i ug I L

- --------·-- - - - -·---------·---------·- __ _j _____ _

05-07-03

05-07-03

79:3~:u5 - 1, 1,2,2 Tetrachloroethane -----~E___ ug IL 05-07-03 563-58-6 1,1-Dichloropropene , ND ug IL 0.1 05-07-03

1~6~93-4= --="L2_~~b-m~~~t~~~~~(~~B) -- ;---==~~D . ug IL 0.1 05-07-03

95-5~_1 1,2 Dichlorobenzene _: ______ N_I:)_ ___ ug_/ L 0.1 05-07-03

107-06-2 I 1,2Dichloroethane(EDC) ND ug/L 1 0.1 05-07-03

78-87-5 _j_ _ _ -1~2-oichloropropane ND ------ ug~~---1-------T 1 0.1 o5-07-03

96-18-4 1,2,3 Trichloropropane ND __ ----~-~! ____ _ --+---1_ 0.1 05-07-03 87-61-6 I 1,2,3-Trichlorobenzene ND ug IL i I 1 , -o.·5----------, 05-07-03

-1-20-82-1 r----{2-;-4-Trichlorobenzene ND ug IL 1

- ---f: , _ O 5 05-07-03

;:::e '·''~-::::;~::,. ~~ :;~ : - -~,-:; ::::;~: 541-73-1 1,3 Dichlorobenzene +- __ ND __LJ_g_/ L__ _____ _ _ 1 ---0.1 05-07-03

_108-67-8 _i ___ 1_2,5-T_r~~:_thylbe_nzene -~D ____ J __ ug IL -~--1_ __ o_._1________ 05-07-03

;:;~~~r--J ::~::~;~~'.:::: --~i---1 :n =1~ L '-==:=:~ 1 = :~:::: ~~,-~~::"= : ~~- I ~-r--~+-~-1Jtt- m~~1

I 108:86-1 i Bromobenzene ND _ -----+-~---- _____ -_ --~---~-- . J 0.1 t , 05-07-03

I

-----r- Bromochloromethane ·-+---NE__ j ug / L I~ o.c_r--=.~ 05-07-03

~~~:::: _

1

__ ___B~o-m~~~;:~:~::ne I --~~ ___ !--~:~~ : -~~=1=~ 1 ·: __ ~) i ___ j ~::~~:~: I 74-83-9 Bromomethane -1- _ NE_--- __ j_-ugiL 0.6 ·-· j 05-07-03

~6-23-5 Carbon tetrachloride I ND i ug IL 0.1 05-07-03

I

08-90-7 Chlorobenzene __ ~~- _____ 0.1 JI ____ 1

_. 05-07-03

124-48-1 i Chlorodibromomethane ND 0.1 05-07-03 I t --- ___J

:~!~ !---==~*~~~~~~~-=~~=-~~ --~~~~--,-- 1- ~+---~ ~::~~:~: 74-87-3 , Chloromethane ND ug IL 0.1 05-07-03

-. -· ---------cis-1, 2 dichloroethene ND ug IL 05-07-03

cis-1,3 dichloropropene -T ND ug IL---- 05-07-03

Dibromomethane ND ug I L 05-07-03 ---- -------+--------

100-41-4 Ethylbenzene ND ug I L 1

1 0.1 05-07-03 ----- ---- -- - '

1 0.1 -- - ---- -L- -- - __ _J

05-07-03 75-71-8 Freon 12 ND ug IL ---------+---------

87-68-3 , Hexachlorobutadiene ND ug IL 1 I 0.1 I o5-o7-o3 -------·---- • 0.1 ' : 05-07-03

i -oE~-W 05-07-03

I -021 ____ [__ --1 ~::~~:~:

r-0~1__ j _ =~ 05-07-03

98-82-a-r-- lsopropylbenzene·-· -------- ------ ----- ·-------· 75-09-2 Methylene chloride

ND ug IL

91-20-3

I ND I ---~-----------·

ND ug IL

ug IL

Naphthalene ------------------------~---

n-Butylbenzene ND ug I L -------1- ------------- ··-- ----~ -----------

103-65-1 · n-Propylbenzene __ ___J ____ ND _ ___ 1

ug IL

104-51-8




Client:

Project:



-------- ------------··-----


D_T/V~t applicable due to sample dilution )'

L lt\iot applicable due to MDL proximity Order: 0304504 PHl16


Run Sequence

X03206 XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

XG.2003.800.3

X03206 XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

Page 10 of 25




I -~~ p/:~;~ennees .-1~ ___ l ~~ ~ ~--~---~- -Im--~- ~T· ~+I3 135-98-8 sec-BS~~::~~ze~-- ___ NNDD _---=r-- uugg~//=LL ~ -- +-~~- -11 --=-~tT-0~.·-11

1 j

100-42-5·1-··· ':'..'..'.'"'__ __ -t--1 -156~S0-5+ t-1,2 Dichloroet~--=--ND -=~ -ug_iL I=-==- _ __)._- -1 _ : ~-i___ f 10061-02:6 , - t-1,3 Dichloropropene +--_ __!'ID __ .+_.ug IL __ · __ ___ f--- 1 r ~--- ~-j' 1 98-o6:s· · · tert-Butylbenzene =± ND ug I L • ± 1 1 0.1

~-~:~::~: : ~ Tetrac;~~~:~:ylene - ___ O~~ . ... t ~~~t=r=--~-. ----~==1'-- ~:}- ~- , 79::01--5~1 - Trichloroethene ------r---·-ND·--- 1---uQi_L_i ______ + -1 -- ·--0-.1-- -----1 ~~~~~~=ld n~ch~~r11~~~~~;~han~ J = ~~ _· _+ ~;-~~~ ~J- _-= --_- L--~ t- ~:~- - , _--1


75~34-3---,+· 1, 1 Dichloroethane -~ --- -UQI L -i-=-- r:-- 1 --~- --N.11=1 75-35-4 -- , ---------w-·Dichloroethene -~~----~~g/_L_ --- - I -1-- 1 __ 0 ___ 1

_7-1:=5~-6 1--1~1.1 Trichloroethane-·· ----~ ug IL - - :--11 01_ , --1

: 67.39_~~~ =---i=I_ -+- .. , ~F~~-·_t, -J ! I 79-34-S·t -·--1- -~1- -! -563-58-6 ..... . ·-·1--~

_1;;~90~~4 01 +-----~ H -· ~ _ ==r-~ ~J____HH~· 1

107-06-2 J 1,2 D1chloroethane (EDC) -~1---~~---_ll§l_/L--+-- ___ J __ 1_____ 0.1 +--78~8~~ 1,2 Dichloropropane --~• --~------J ___ __ll2_f_L -+-~'--·. ___ ·--~-- --~1- +----

96-18-4 I 1,2,3Trichloropropane i ND 1 ug/L 1 0.1 I 1

87-61-6 r-- -1,2,3-Trichlorobenzene==t=_ _ ND=~-----~_!_~~~ 120-82-1 ! 1,2,4-Trichlorobenzene I ND ug IL

o5-07-o:{ ~,,

05-07-03,

05-07 .03,,.

05-07 -03". . 05-07-03~.

05-07-03.

05-07-03~

05-07-03.,,.

05-07-03c•

05-07-03'• .. 05-07-03'.

05-07-03i·

'"'' 05-07-03

05-07-03·.

05-07-03•

05-07-03

05-07-03

05-07-03' •·

05-07-03

05-07-03•·

05-07-02•

05-07-03.

05-07-03··

05-07-02

05-07-03.

05-07-03'

05-07-02'

05-07-03.

05-07-03'

05-07-0~~

05-07-03

05-07-03'

05-07-0~

05-07-03

05-07-03

o5-07-o:

05-07-0~

05-07-03

05-07-o:.

05-07-0~·

05-07-03''

05-07-0~

SQLCoyote: Reports 1. 0. 0305281535)()( Report Date 6119103 9:39:39 AM

STANDARD



Client:

Project:



D [ -NoTapplicable due to sample dilution j Order: 0304504 PHl16 -----r_-_-_ -- ----_----------·-·-------------- -·-

L j _ f'.J_?_t applicable due to MDL proximity


Run Sequence

X03206 XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

XG.2003.817.1

X03206 XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

Page 11 of 25



EPA 524.2 rev 4 Purgeable voes by GCIMS X03206-023

;5i:~:3~~: --~==~'.!:~::~------- -~==~=-::;~~- --~ --==1f ::L=J ::::;~: 75-00-3 Chloroethane _____________ ND ug IL r· _____ 1

___ CJ_J__:=__ __ --1 05-07-03

67-66-3 Chloroform ND ug IL 0.1 I 05-07-03

74-87-3 Chloromethane ND ' ug IL 0.1 , 05-07-03

156-59-2 cis-1,2 dichloroethene ~ ug IL 1 O 1 1 05-07-03

10704~~~~~ _ cis-~;~r:~:~:~;::ne --- - --~~~~ ~~ ~ ~ -----+-~- ~: ~ --~ ~::~~:~: ~o5~~41~~4 J Et~::nn~;ne ----~~ -J _~-J == --~ ~~i-=1 :~;::: 87-6~~-L Hexachlorobutadiene ND i ug /~ __ . __ -~- 1 0.1 I

1

05-07-03

98-82-~ _ ~---- lsopropylbenzene ND , ug IL 0.1 , I 05-07-03

75-09-2 Methylene chlorid<: _______ --- ~ -ND J _ ~~!_L ___ j _ _ ~ 0.5 -: _____ 1

05-07-03

19

0~~5°1-~8 ----n-~:;1~~i~~e----- --~----i---$'c-~1----- -t_ --~ ~ o\ --~-= ~::~~:~: ~~~~;~~1_1 ----n-=Proi>Ylb"enzene N_D ___ _ j __ _tJg_l_L__--+-----==t=--2 __ ~- _0:.1 _:_______ o5-o7-o3

1

108-38- ------~~~een;s _____ J~~-=-~ ~~~-~~-~- -~- ~~-;-~_!-~~---=--j___- ~ ; -- ~~ ~-: _ -- ~::~;:~: ~106-42 _ _ _________ ----- T

I ::~~~ _ ,_:::~~;:~::::::. _J~jL~J£ -~L -- : --~· ~ ·--=1 ~::~;:~: 0.1 _J __ ~j 05-07-03

11109o8~01~6~26-6_L t-1,3Dichloropropene I ND ug/L m----m- L 1 0.1 : i 05-07-03

- tert~Butylbenzene , ND ug I L --- - --1 i 127--18-4 ~-----i-eiracl11oroethy1ene , N_D _______ ---ug/L----------1

108-88-3 Toluene ND ug IL 1

----------~ ----· ·--- - ·------- -------------~- --------t---------1---

79-01-6 Trichloroethene


Vinyl chloride

__________ -~[) __ ----- ---~.§l~--L-ND ug IL

ND ug IL ----L __ 1

---------

0.1

0.1

0.3 --

0.1

0.1

0.1


7-5--34--3-~- 1,1 Dichloroethane t- -~[)_ [_ ug IL F-==-~.:::J~~--r~~~~l-----~

~~::::: --@~h~~~::~~:~e I --~~-~-+- ~~~-~ -_ ~- - -- ~ _L--~~t0_~~---~ 630-20~6u- _ __1_._1_.!_._2 T:_trac~l~roeth-ane·-1-- ND u-, ___ u_g / L

1 1 0.1 L ____ ~

;::~~:: .. __ 1-, 1

1

,;.': ;~~~;~%~~::~~=ne __ : .. _ ~~ -~11~=i=--=- ------==~=1

-_ ~-~~ ~~f _ _i-----~ 563-58-61 1, 1-Dichloropropene I _r-1_[) _______ __j_ __ _llg_/_':: _ _j__ ; _o_: 1 -i-----J 106-93:-4-- 1,2 Dibromoethane TE"bB)---;------ ND ! ug IL 1 ----- ~ - 0.1 · I ----- ---------------~---·-·-:·-------- -· -- ------- -------- ----1 95-50-1 1 _ 1,2 Dichlorobenzene I ND ~---- ------~-- -~------°:.~ -i io7-06-2_1 __ 1,zoictlioro-ethane (EDC) ND ug IL 1 0.1 - ·

- - 1- --------------------- - ---~

7~8~- ___ _1·~-D~c~l?r~ropane ND ug IL 1 0.1_--+--96-18-4 ! 1,2,3 Trichloropropane ND ug IL -------,---f-----~--0.1

87::51..6 -J 1,2,3-Trichlorobenzene [__ ND - -T-~~9:!I=- ___________ L_ -----0.5 ___ -----

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03




Client:

Project:


APRIL 03 SAMPLE EVENT Explanation of codes [:

DrNot-a~licabl~ due to sample dilution r' L : Not applicable due to MDL proximity Order: 0304504 PHl16

---------·----- ------------------- ----


Run Sequence

X03206 XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

XG.2003.814. 19

Page 12 of 25



EPA 524.2 rev 4 Purgeable VOCs by GC/MS X03206-030 120-82~- 1,2,4-Trichlorobenzene ND --------ug,t:_- ~----- - 1---~-05-=S

95:5,_, I - 1,2,4-T<lmelhylboowoe ND __ --_+_ i' --~uu=99 11

LL 1- ----=-l- 1

1 _--__ f- 0

0:_2

1 ~--96-12-8 _ 1,2-Dibromo-3-chloropropane N_[) _ _

1

541-73-1 1,3 Dichlorobenzene ND __ ____LJg__/__[_ _ __ _ __ _ 1 L~-- , 108-67-8 1,3,5-Trimethylbenzene ND ug IL 1 0 1 I

-----------142-28-9 1,3-Dichloropropane ND

---106-46-7 1,4 Dichlorobenzene ND ------ =j ;; '.T- - ~ -f -~ ~ -j ~:

. ------+---~g IL _ __ ___ _ 1___ 0~:1_ 99-87-6 1,4-lsopropyltoluene ND ----

--~ ~~-~ _______ J ____ _1_ ____ 1___~·~---L-ug I L 1 1 ' 0.1

1

594-20-7 2,2-Dichloropropane ND --~-- ---r--

95-49-8 2-Chlorotoluene ! ND --~-~ e---- ... -- ----·--------- ---------- --------- -------··

--B--en __ z __ e __ n __ e ________ , -- --ND _____ ~--~-~-;-~- :----- - nmrn___ : --~+---r --Bro~:~~::~:~heane-----+----------------~--~- ---~~---: -~~-~----+-== ~=-=~~- 1-------_ ~: ---~--:· ~------------+--

106-43-4 4-Chlorotoluene ND ---~·-71-43-2

108-86-1 '

_7_5~_27_:::-4 ______ -----~~~--B __ r __ o __ m __ o __ d_ic __ h __ lo_r __ o __ m __ e __ th __ a __ n __ e_ ND --1 ugltL - -- - __j__ __ T_ 75-25-2 Bromoform ND ug I L ----f-- --- --------74-83-9 Bromomethane ND ug IL

0.1

0.1

0.6 ------------t------------c------ ---------j------

56-23-5 Carbon tetrachloride ND ug I L 0.1 -+-----

---+--

108-90-7 Chlorobenzene ND ug IL ' , 0.1 - ____ c__ ________________ ~---------+---------+--------t ---j--------j

124-48-1 Chlorodibromomethane ND ug IL 1 1 0.1

:~~~:~ l----c--c_h_~--~--~~--:--~:--~--~--e-----1-------~--~-------+----~--~-;--~---+ I ,-~: ~ 1

,:,:.--~~--~~--5----;:·;~::::::::,: +-----~----~----t-;ffi-_ ~~= i' =- ~ ~~r ~r--L -74-95-3 --~~r11omethane ==t==No ~gTC- _~--- -~~ -=I _____ i -- _0_._1--~= 100-41-4 Ethylbenzene .l ND ug/L___ _______ 1 I 0.1 __ _

75-71-8 Freon 12 · ND ug IL 1 0.1

0.1 ----~~I---.

05-07-031 ,_ 05-07-03

05-07-03'"

05-07-03'' 'v-

05-07-03,

05-07-03'

05-07-03. ., 05-07-03,.

05-07-03'

05-07-03,_

05-07-03,

05-07-03''

05-07-03.,

05-07-03

05-07-03'

05-07-03.

05-07-03-

05-07-03.

05-07-03.

05-07-03-

05-07-03

05-07-03.

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03

05-07-03-

05-07-03'

05-07-03

05-07-03

05-07-03

0.1 i 05-07-03

----~----------------1---

127-18-4 -1-108-88-3 .

SQLCoyote: Reports 1.0.0305281535)()(

0. 1 05-07-03 - .. --·------

Report Date

0. 1 05-07-03

05-07-03

05-07-03

05-07-03

6119103 9:45:07 AM



Client:

Project:



o 1 --NOt-BPPiiCabte dUe tOSalnp1e ditUtion ___ · Order: 0304504 PHl16

. --------- ----- - --- ------------

L ' Not applicable due to MDL proximity


Run Sequence

X03206 XG.2003.814.19

XG.2003.814.19

XG.2003.814.19

M03548 MT.2003.521.10

MT.2003.511.34

MT.2003.511.34

MT.2003.521.10

M03550

MT.2003.551.11

MT.2003.551.11

MT.2003.551.11

MT.2003.551.11

MT.2003.551.11

MT.2003.551.11

MT.2003.551.11

MT.2003.551.11

MT.2003.551.11


Dilution

Factor

Detection

Limit

Run

Code Date


79-o1:£l Trichloroethene___ ---------ND ug IL -~-- ____ --+· .. _ _ .. _-1-----:----=:~1 __ -f .. ' I 75~69-4 · ___ .l"_r_ichlor~fluoromethane ND _______ 1 . _ LJ_g_l_L_______ 1 ______ ~1_-+-75-01-4 Vinyl chloride ND ug IL 1 0.1 ,

- ----·- --· --- ----- ---- -- ·----- ---------------·-----·-------

SW846 3005A/601 OA ICP

SW846 3005A6020 ICP-MS M03550-001

05-07-03

05-07-03

05-07-03

05-01-03

04-30-03

04-30-03

05-01-03

; 744_0=~6_:_0_·--~~=--Antimony _________ ~=t= -mg/ L- ! _______ -·-_-_o_._oo_1_--r·-----i 05-05-03

~::-~-::-::-:-;-------·--~-:-r~-:m_ic ____ __,. ___ R ~~ ~ ~ j--- - ---- -- 1 ~:~~~ -:------- ~::~::~: 7440-43-9 T-----C-ad_m_i_u_m-----+-----ND I --mg/ L- r-__ -_···· ___ -_--__ -_---____ 1 . . 0.001' -r---~ 05-05-03

~::~~~-~~--~1-~~~-- ~i:::1 _--_---_----_-j-_:~----=--=--=--~--~-=-=-=-=----r-___ ;-~-~-~- ~ 1- --__ :- ~~~~ r _ =j ~::~::~: 7782-49-2 j Selenium ND mg I L 0.001 I ' 05-05-03 7440-22-4 I- --------S-1-·lv_e_r --- ND mg IL 0.001 - i ---1 05-05-03

- ----------Th_a_ll-iu_m______ ND mg IL 0.001 , ------] 05-05-03 7440-28-0

MT.2003.551.11 1 7440-31-5 Tin ND

ND

ND

mg/L

mg/L

o. oo 1 I o5-o5-o3

MT.2003.551.11 7440-62-2 Vanadium

Zinc

- I 0.001 . I 05-05-03

MT.2003.551.11 i 7440-66-6 mg I L ___ _J ____ _ -------------~

0.005 I i 05-05-03

X03194 XG.2003.785.12

XG.2003.785.12

XG.2003. 785.12

XG.2003. 785.12

XG.2003. 785.12

XG.2003.785.12

XG.2003.785.12

XG.2003. 785.12

XG.2003. 785.12

XG.2003. 785.12

XG.2003. 785.12

XG.2003. 785.12

XG.2003. 785.12

XG.2003. 785.12

XG.2003. 785.12

XG.2003. 785.12

XG.2003. 785.12

XG.2003. 785.12

XG.2003. 785.12

XG.2003. 785.12

Page 13 of 25

SW846 3510B/8081A Pesticides by GC/ECD X03194-001 - --------------- a-BHC ND ; ---uQ~ -- --Q.1--i--- -1

I ,:_,_,~_~:r c~,~~~§~~., In -·-·~~ ~1H~- -=~~-=r~;--I

'60-57~ - ~~:~r~ ------L-----~~ - -+- ~~ ~ ~ -+-----+--+--+--~~-: --~ 1

- ---~ -T · ·· Endosulfan I ND I _ ~_i_L __ -t=---J=~--1 _ j o:1 _, ____ 1

--~i En~;::i;:~f~nu:;ate ~~ ~~ ; ~ I- ~ 1

_ ~==__:! , 72-20-8 Endrin ND I ------------ ---

Endrin Aldehyde ND --- -------------Endrin Ketone

58-89-9-- g-~~~~d~ne n ---r=-- -- ~-~ --- ; --~~; ~ ------ -+- -t--~}- ,----i 7644-8-~----~Ptaehlo~- ND ug/L -- -- 1- - I 0.1 ---;-----1

1024-57-3 HeptachlorEpoxide ND -ug/L ___________ 1 ____ 1 _ I - 6.1--+---~

72~43-5 ===--Metti_o~C:-~1~;:·---=~==~-__ t-i_CJ_-=---- --ug/ L.- ·- - ·· 1 1 -- 0~1=-==----6088-51-3 p,p-DDD ---+-- ND ug IL 0.1 _, ____ _

__ p,p-DDE _____ j_____ ND ug IL 0.1

05-08-03

05-08-03

05-08-03

05-08-03

05-08-03

05-08-03

05-08-03

05-08-03

05-08-03

05-08-03

05-08-03

05-08-03

05-08-03

05-08-03

05-08-03

05-08-03

05-08-03

05-08-03

05-08-03

05-08-03




Client:

Project:



- ----------------. -----


Not applicable due to sample dilution i L ·:_ · No!iPJ.ucaiJt_e__~ue to MDL proximity - ;: Order: 0304504 PHl16


Run Sequence

X03194

XG.2003.785.12

XG.2003.785.12

X03194 XG.2003.785.25

XG.2003.785.25

XG.2003.785.25

XG.2003.785.25

XG.2003.785.25

XG.2003.785.25

XG.2003. 785.25

XG.2003. 785.25

XG.2003.785.25

XG.2003.785.25

XG.2003.785.25

XG.2003.785.25

XG.2003.785.25

XG.2003.785.25

XG.2003.785.25

XG.2003.785.25

XG.2003.785.25

XG.2003. 785.25

XG.2003. 785.25

XG.2003.785.25

XG.2003.785.25

XG.2003.785.25

X03194 XG.2003.807.8

X03194 XG.2003.807.7

X03189 XG.2003. 750.3

XG.2003.750.3

XG.2003. 750.3

XG.2003.750.3

XG.2003. 750.3

XG.2003. 750.3

XG.2003. 750.3

X03189 XG.2003.750.18

XG.2003. 750.18

XG.2003. 750.18

Page 14 of 25



SW846 3510Bl8081A Pesticides by GC/ECD X03194-001

5~:29-3 ·. p,p-DDT I ····-_!-l_[)__ 8001-35-2 Toxaphene, total ! ND

----

ug IL

ug IL --+---··_-----:-~- T-· ~.~ I ·=i ____ ti_~. -

SW846 3510Bl8081A Pesticides by GC/ECD X03194-014 -~- ---~----------··-----------~

I a-BHC ND ug I L 1 I 0.1

I

. a-Chlordane ND ug I L 1 0.1

r- 309-00-2 .. :~~~ ~~ ~~ ;-~---+---_·_··_···--+-===~=----·--.-... +L·-··--~:-~--+-----1 I .. -1.---------------+----------1---=---+-----1-------+-----+--·-

;

57-7~-·~9rdane, total ND ! ug l __ L_--+! _______ 1 1 ..... , ___ o_.1 __ +----j

eo-_

57

_-

1

----.1-,··----.-_--~=~=~=~=~~=:-d-~-o_:-;_lu_:_l-[-_:-:=1-1-1===-.. _--:-: -_-__ - ~~ ~1 __ - -r ~ -~~~ -~ = _72

_.20

_0

j _E_nd_o_s_~-~:-~-i~_u_1t_a_te______ -Z~--_j; -:Vi+- __ ~l-~-T ~~ ! i

--_--_-·-r---_ Endrin Aldehyde -- ND · - •----uQ/ L - : f . -1 -:=- 0.1 __ ~~-- j ~-___ E_n_d_ri_n_K __ et_o_n_e __ ···--·-+-----N~------=1---~~ IC --1------=:=-- --~-~ ±--/

5a:99-=91--· g-BHC ND ug I L I 0 1 ' ----1 ~- · · g-Chlordane ND ug I L I ~ -- o: 1 i ----1

76-44-8 I Heptachlor ·-· ND ug IL - 1 1 0.1 i

102~~5-_7_-3--+i ____ Heptachlor Epoxide ND ug IL ---· L __ 1 __ ' t0.1 .. ~ 72-43-5 ~- Methoxychlo_r ____ t-- NNDD ___ ] uugg 1

1 LL --+-----! __

11_ . ___ oo .. ~·11.. ____ ___j__J',' . ~o~~~~~c=- p,p-DDD 1

----· -+------p,p-DD§ ___ ~ ~~ II ~gg; ~ ....... -·-- ·--- ~: ~ -- ·-I • 50-29-3 I _P_, p_-D_D_T ____ j -· 8001-35-2 ! Toxaphene, total 1-- ND - · 1 ug IL 2.5

SW846 3510Bl8081A Pesticides by GCIECD X03194-026

05-08-03~ 05-08-03.

05-09-03'"

05-09-0(

05-09-03 •.

05-09-03 '·

05-09-03 •.

05-09-03·

05-09-03\ ' 05-09-03 •.

05-09-03·

05-09-03 ••

05-09-03 ...

05-09-03

05-09-03

05-09-03 .

05-09-03·

05-09-03

05-09-03·

05-09-03.

05-09-03

05-09-03

05-09-03•

05-09-03

72-43-5 1 Methoxychlor I -==N=D==========-u_g-/ L .~-----~--·-·----·

o.~ _Hr= 05-19-03

SW846 3510B/8081A Pesticides by GCIECD X03194-028 -7-2--4-3--5--i - Methoxychlor I ND

---~-----~

1----o.1··-J ___ =:] 05-19-03 --~---.--+---·

ug IL

SW846 35108/8082 PCBs by GC/ECD X03189-001

'1-2-67-4--1-1--2 · Aroclor 1016 I ND ug IL _l ______ . ____ J_ 0.5 , ]

11104-28-2 ' Aroclor 1221 I ND ug IL 1 0.5 1 I

~~:~::~~~!~ ·-r ~~ : - ~~~F~--~---~--~- f ~! f-J :;:~:::::: ~---· ~~~-;-:~-~-::-:-~----~~.-_- ~~~-~I ==!=+ f ~!~ 53469-21-9 I

SW846 35108/8082 PCBs by GC/ECD

1

12674-11-2 1 Aroclor 1016 ND ug IL

11104-28-2 i Aroclor 1221 ND ug IL ---- - -- ----- ----- ·--------·--· ·-·--·---·---·-- -----··

i 11141-16-5 Aroclor 1232 ND ug IL

X03189-014 ,--- fj I ,, ~::

05-06-03

05-06-03•

05-06-02

05-06-03

05-06-03

05-06-02··

05-06-03.

05-07-03

05-07-02 ...

05-07-03

SQLCoyote: Reports 1.0.0305281535)()( Report Date 6119103 9:50:35 AM···

STANDARD



Client:

?roject:



[)J . A!otapplicabl~_ d'!_e to sample dilution _

L ~t applicable due to MDL proximity I Order: 0304504 PHl16

- -~-- - ----


Run Sequence

X03189 XG.2003. 750.18

XG.2003.750.18

XG.2003.750.18

XG.2003.750.18

X03189

XG.2003.798.4

XG.2003. 798.4

XG.2003.798.4

XG.2003.798.4

XG.2003.798.4

XG.2003. 798.4

XG.2003. 798.4

X03165

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

· XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

Page 15 of 25

CAS# Analyte Result

SW846 35108/8082 PC8s by GC/ECD 53469-21-9 : Aroclor 1242 ----··· -r-----ND ~2_672-29-6 ; ______ Aroclo!~-~~~- _____

1

__ =~~---i-11097-69-1 : Aroclor 1254 1 ND -· ----+------------ i 110~6-82-5 I --~clor_~6_?__ ··-1 ____ ND--

12674-11-2

11104-28-2

11141-16-5

53469-21-9 -------- -- ---

12672-29-6

SW846 35108/8082 PC8s by GC/ECD

Aroclor 1016

Aroclor 1221

Aroclor 1232

Aroclor 1242

Aroclor 1248

ND

ND

ND

ND

ND

Units

ug IL

ug IL

ug IL

ug IL

Range

---·"---·

ug IL I ug IL -+----

_________ .. ___ ,_ ___ __,__ ug IL !

ug IL

ug IL

11097-69-1

11096-82-5 •

Aroclor 1254 ND . ug I L

Aroclor 1_2_6_0 ___ ~_·_· -_·_·· -~~~--_l_=-ug/_L_ =i===== SW846 35108/82708 SVOCs by GC/MS



0.5

0.5

0.5

X03189-014

-- L _________ -

X03189-027

i --- --- -- -----

-~}-t·--- _j

-~=I X03165-001

05-07-03

05-07-03

05-07-03

05-07-03

05-15-03

05-15-03

05-15-03

05-15-03

05-15-03

05-15-03

05-15-03

· ~25~~80~~1-I \~~~~~~~~;~:~::~:e -- ~~ I -~~l -- -------r ~:::- ~:~~~;,~:::~:,:~: -~ ~g ::;~ ... --=-~~------_-j_---_~

T--~~ 04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

-58:90-2 - -- -2,3,4,6-Tetrachlorophenol ND .. _ __j__ ug IL ·--- --------==-==----- -__ _,__ ___ . __ -____ _,~ 95-95-4 ' 2,4,5-Trichlorophenol ND ug IL I

88-0~t' --~6-Trichlo_r:c:ip_~e-~o~ ND ug J ~ 120-83-2 2,4-Dichlorophenol ND ug IL

---·- - -------- -- -- ---~------------ --- ---- -

- ---------: -- -----

10~67-9 f 2,4-Dimethylphenol i ND ug_l_L ____ _

152\-~18~~2 -+- ~ .. :~~ii~i~t;~~~~;:l----~+=------~-~- --~-- ~~ ~~ -' -------

1

69°t~2:~2 -- 2-~~~~:~~~t~~~:,:~e ·-----·-~~=---+=--~~TC-·---_·-------·--'-

SQLCoyote: Reports 1.0.0305281535XX Report Date

5

5

! 04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

6119103 9:51 :25 AM



Client:

Project:



- - --- ---------------


D L Not applicable due to sample dilution " Order: 0304504 PHl16 L Not applicable due to MDL proximity


Run Sequence

X03165 XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

X03165 XG.2003.696.6

Page 16 of 25



SW846 35108182708 SVOCs by GC/MS X03165-001 -----

208-96-8 Acenaphthylene . - !---

ugil..- _T _____ -- - ---1-----i---1- . · :---, ND

--------, 10 I

-- ·1· ... 1---+.-.. _______ J---j 1 ' .

-~---~-_J

62-53-3 Aniline '------·--1 120-12-7 Anthracene

. ---~--Azobenzene& 1,2-------- Diphenylhydrazine

_[ ____ ~-~---· _-·-_-+-t- ~~ ~ ~--+-----~-ND ug IL

----------·------~---~

56-55-3

50-32-8 I

;,1

~~~~~= I ~~ ~ ~ I ~~-~----~=~L-~----i--~- -:~ -1- ------- - --- --- I --- ----- · ·· .:__---i

Benzo (a) anthracene ----+--

Benzo(a)pyrene --- ----

' -~~ ---- r--~~-t_ __ I_=~=---_'._ 1 j---~- -~-= 160:~:1-~6 '-~----------8-~~it~i:l::~~I - ---~~--- _J=--~-~J ___ _c__ __ -=r_~-- l 2

: -----'

191-24-2

Benz o ( b & k)fluoranthene

Benzo(g, h, i)perylene

-1-11--44-4- 1 bis (2-Chloro_e_t-hy-l)_e_t_he_r__ ND ug IL ! 1 I 1 ~ - 1 ----

111::91._1 J_- bis(2-£~1o_r_o_et_h_ox_y_)_m_e_th_a_n_e_~ ___ N_D_ -~--u_g_l_L __ _

_108-60-1 _ ~. bis(2-Chloroisopropyl)ether ND ----1- ug I L 117-81-7 1 bis(2-Ethylhexyl)phthalate ND . ug IL -----·· --t------+-

85-68-7 ! Butylbenzylphthalate ND ug IL --+-------1

218-01-9 I Chrysene ND ug IL -------.. -~---------------+-----------

53-70-3 I Dibenz(a,h)anthracene ND ug IL 1_3_2_-6_4_--9=-+j_-_.-_-_-_-_-_·-_D-:_ib-:_e-:_n-z_o-:_f-u_-r_a-:_n-:_-:_-:_-__--+------N-D _____ ug IL--+---- ·-- _[- _

84-66-2 1 Diethylphthalate ND ug I L I

131-1i.:J---f-- Dimethylphthalate ~- ___ N_D ______ ,__ -- - -- ----~· --------_____ J.._

84-74-2 I

117-84-0 j 1 • 1

- - ---l----1 ' 1

di-n-Butylphthalate I

ND

ND di-n-Octylphthalate

04-10-0~ •.

04-10-03

04.10-o:l""

04-10-0~

04-10-03"

04-10-0:'

04-10-0:1

04-10-03"

04-10-0<

04-10-03,

04-10-03"·

04-10-0:.

04-10-03.

04-10-03'·

04-10-0< ..

04-10-03

04-10-03'

04-10-0:.

04-10-02'

04-10-03"

04.10-0:

04-10-0~

26~-44-~l-- Fluoranthene ND I 04-10-03

---FiUOreile--~---=~------ND __ :=--=--_i __ Ll§l!_L _ _____ __ --~-L-- 04-10-o:c 86737 !

Hexachlorobenzene ND 1

ug IL . : 10 1 04-10-02-

! ~~~~~~: -~~-~-:e~::~~~:~~~~:~:~::~~ene 1 --:-T=~~~!-~~--:------=r -~---+5~=+--.---=~-~- 1 ~::~~:~: 1 67-72-1 Hexachloroethane --1- ND _I ___ ug IL : - - f 04-10-0:>-

193-39-5-+-__ lndeno(1,2,3-cd)pyrene NNDD uugg t1

LL ___ 1 ____ J_. 1

1 I ___ J

1

°044-_ 11 °0-_00 ~-· 78-59~1_1 _____ . ___ lsophorone -

:~-::-~:-:-!- - ~i;::~z-1:-~-:--- . --=~N-~D~--~-----.• ~.1,-___ =--. ~u-~g- ~/r-L - ~---_=-~1~---~-__ -_L-~-~-·1-~0--_---_-_-i ___ -_-_J·_·--.-.. ~-=-_-: ~0:4: ~1 ~o:~o~ 62~75-9_L n-~~o_=.o-dimethyl-amirie __J_ __ _L _ v

62-1-64-7 -~-n-N. itros_~~di-n-propyla. mine__ j-- N.D ug IL ; 1 i 1 I 04-10-0:' 86_-_30-6 I n_-.N_ itrosodiphenylam_.~n_e ND __ ·-·----- ---ug TL.·----. -----1-1--1--1-------- ' 04-10-03

. .. - ug IL I -+ ---1-- .. 1 ·-· 10 -~----j 04-10-0~ 87:8_():5 1 Penta~~~orophenol i-... ND -------r---------+--- _ 1------~----, 85-01-8 ~- --· Phenanthrene 'I ND ug IL 1 ___ -L _ _1_ _________ J 04-10-o:-

108-95-2 Phenol ND i ug IL i 10 : ! 04-10-03 129-00-o ' Pyrene --N-D----+---u-g_/_L---+------- - -+- -- ,---1·----1-----i 04-10-0s .. J I .

I ug I L 1 1 O I 04-10-0< 110-86-1 Pyridine ND

SW846 35108182708 SVOCs by GCIMS X03165-008 120-82-1 I 1,2,4-Trichlorobenzene ND i-ugtl

____________ L__ ______ ----· -~-==-1-~--~-1==-~J 04-22-03.

SQLCoyote: Reports 1.0.0305281535XX Report Date 6119103 9:52:33 AM'·

STANDARD



Client:

?roject:


AP~L03SAMPLEEVENT

----




Run Sequence

X03165 XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

Page 17 of 25

CAS# Analyte

SW846 35108182708 SVOCs by GC/MS 95-50-1

541-73-1

1 · -- 1,2-Dichlorobenzene I

I 106-46-7 i

90-12-0

58-90-2

I

.L ---

1 95-95-4 I --- ····------!----·

88-06-2 I

1,3-Dichlorobenzene --------------------1,4-Dichlorobenzene

1-Methylnaphthalene

2, 3,4,6-Tetrachlorophenol

2,4,5-Trichlorophenol

2,4,6-Trichlorophenol

--·

Result Units Range

-- -· -

ND ug IL

ND

I

ug IL I

I

ND ug IL

ND ug IL

ND ug IL 1- -- --ND ug IL

ND -~ __ u~__!_L __ 4 ND . 120-83-2 ti . 2,4-Dichlorophenol 1 ug IL 1

-1------- L- --- -

10~67-9 _ _ 2,4 D1methylphenol I ND ug IL

1 ~1-=2!l~+- 2,4-Dinitrophenol ± ND ~. __ _tJ_!!_f_L_ I

121-14-2 , 2,4-Dinitrotoluene ND · ug IL !

-

Dilution

Factor

Detection

Limit

Run

Code Date

X03165-008

---~i -·-·r----------_ _1_ ___ --+--

1 - . -·------~------+-----j

1 ----+-----j

5

5 5

-----+----

--~----+--1 !

---- - --- ' - ·10 -+---+------5

04-22-03

04-22-03

04-22-03

04-22-03

04-22-03

04-22-03

04-22-03

04-22-03

04-22-03

04-22-03

04-22-03 _____ l_______________ _ ________ __J__ ___ - ---- -·-

','t::,'i'- ~ = 2~~~;~~::~:::~~. J--=- ~t -:_:r*-. ----:-- . i =±-_:1=] ::::::: ::1:~ I _:-2+:::;~~;::"' - H -:---+-~ 1--~~ t ~ t-~ . ; ~::::

• :~:; ' ,~g~1~;jff:::· ~-- -I ;ii~ I -=~ ~L~~O-=[~] ~~~~~ 99-09-2 ---~=N_i_troanilin~--------------- ND +- -Lig/T r----=-- --- 1 __ L ___ L ___ J ___ j 04-22-03

534-52-1 1 4,6-Dinitro-2-methylphenol ND ug IL ~ · 1 _J 10 t I 04-22-03

101-55-3 4-Bromophenyl-phenylether ND ug IL - ---- _ ~~_-11- - 11_~=-+--- ·5

1-- -j ~ _ -~_', 04-22-03

59-50-7 4-Chloro-3-methylphenol ND _,_ ----u-gTi_ 04-22-03

106-47-8 _ ~ ~=~~~=-~-~'219_r_o_aniline ND ug / L I -i- --=-l--=-5- --~-- -J 04-22-03

' 7005-72-3 1 4-Chlorophenyl-phenylether ND ug I L I ' 1 04-22-03

. ___ __[__ ___ ug ;1:_---r-- -~- j _t5 - -- 1 --- 04-22-03 100-01-6 4-Nitroaniline ND ---------~---

: 100-02-7 f----

83-32-9

4-Nitrophenol ND ug I L · 1 10 1

04-22-03

___ 1 __ l _ _! ___ j__ __ -- 04-22-03

1 i 1 04-22-03

Acenaphthene ND ug IL

208-96-8 ug IL Acenaphthylene ND 62-53-3 Aniline

---10--+----j 04-22-03

-----ND i ug IL

-- ------- -·---·----l - -------------------120-12-7

- ---

Anthracene

Azobenzene& 1,2-Diphenylhydrazine

56-55-3 I Benzo (a) anthracene -------+ 50~32.=_8 -l-- _ ~=-~~?-~~le_Y~:_ne _ 1

• Benzo(b & k)fluoranthene 1

-- ___________ _j_ ____ --- ----·-----------------+ 19~-2~=._2_ j _ Benzo(g,h,i)perylene !

64-85-0 Benzoic acid I

100-51-6 Benzyl alcohol

..

ND

ND

ND

ND

ND -----~--

ND

ND

ND ------ _________ ,___ __ _

111-44-4 bis (2-Chloroethyl) ether ND

---- ------

ug IL

ug IL

ug IL

ug IL -- ----------

ug IL ---------------

ug IL

ug IL

ug IL ----

ug IL ---------

111-91-1 ~- bis~-Chloroethoxy)_m __ e_th_a_n_e ________ --+------+--ND ug IL

108-60-1 bis(2-Chloroisopropyl)ether ND ug IL

117-81-7 bis(2-Ethylhexyl)phthalate ND ug IL


! - - -1

1

1

-r~-=1 f - - -I

1 1 I

1 1 --· --- j-----~ -1 - - 25 I - i

--c---~ --~=~~-1------ ~ -~--~ ~c=-=L.~ --~ --~=~1

I 1 I 1

1 ~---+----

- - 1 5 --~· _____ J

04-22-03

04-22-03

04-22-03

04-22-03

04-22-03

04-22-03

04-22-03

04-22-03

04-22-03

04-22-03

04-22-03

04-22-03

Report Date 6119103 9:55:03 AM



Client:

Project:



D L. Not applicable due to sample dilution '·i ! L ! Not applicable due to MDL proximity Order: 0304504 PHl16


Run Sequence

X03165 XG-2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

X03165 XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

Page 18 of 25



SW846 35108/82708 SVOCs by GC/MS X03165-008

-~~~-~:-1-_~9-~--- ______ B_u_t_y_lbc_eh_n~_Y_~~-~-:-ha_l_at_e ___ I,_, __ · ·---~--~------_··-__ - -=~ ~~ ~ ~-== ---==-~~~~- j-=--=~~~~~_,-- ~ -~-+----- ~::~~:~; 1 53-70-3 [ Dibenz(a,h)anthracene ND ug IL l i32-64-9-r Dibenzofuran j ND ug IL

i 8~-66-~~1 ____ D_ie_th_y_lp_h_th_a_la_t_e ____ l ____ N_D ___ -r-_u_g_/ L---r-----r------~---r---" 131-11-3 ! Dimethylphthalate ND ug IL

·-8--4--7-4--2---cl----d-i-n--Butylphthalate ND ug I L

117-84-0 · di-n-Octylphthalate ND ug IL ---~-t---------------·---+--------+------+---------------------- -~------

206-44-0 i Fluoranthene l ND ug I L 1 --·---------------1---------------t------j----

86737 i Fluorene ND ug I L 1-------_l ' 118-74-1 I Hexachlorobenzene i ND ug IL

--r-------r-----r-------~------ 1-----------87-68-3 t Hexachlorobutadiene t ND ug IL I 10 -·-77--4-7--4--·~-H_e_x_a_c-hl-o-ro-c-yc_l_op_e_n-ta-d-ie_n_e--+----N-D-----+--u-g--/-L-·--~-----~·----r--10---+--_,

--------------~----- - ·--·- !-·--

1

10

67-72-1 Hexachloroethane ND ug IL 5 ----·--·--·-c---·--- -··------

193-39-5 lndeno(1,2,3-cd)pyrene i ND ug IL I

78-59-1 ! lsophorone I ND ug I L 1 91-20-3 1--···---N-a_p_h-th_a_le_n_e _____ --tl----N-D-----j-1--u-g_/_L __ _,._. ______ -------1- 1 1

· -98---95--3- -: · - ----N-it-ro_b_e-nz_e_n_e_ ND f~ug-TL-· -=~~=- __ =--=--=---=-~- ~--62-7_5-_9_·-_.,1 __ n-_Nitroso-dimethyl-ami_n_e ____ .,..11 _____ N_D _____ I_ --ugTL___ 1 o 621-64-7 n-Nitroso-di-n-propylamine I ND ' ug IL

86-30-6 !. _ . __ n_-_N_itr_os_o_d_ip_h_en __ y_la_m_i_ne __ ~ _______ N __ D_ ~ _ug IL_ t_ __ _ 1 ~ =- _L 87_-~~--5 ____ F'_t;lntachlorophenol --·- 1 ______ N_D ___ -+1 __ u_g_l_L___ __ . _ _ _1 __ ~ __ 1_0 _____ __,. __ _,

85-0_1-_8---t---·--Phenanthrene ___ N __ D ___ _,i __ u_g_l_L__ _ __ f 1 , _ 1 108-95-2 : Phenol ND ug I L 1 1 10 129-00-0 r· Pyrene ND ==r--ugll ___

1

-----+---1-;--:i---+----j

-i-10-a6:-1··T--=====P=y=ri=d-i_n=e=====-=----_-+-L=----N-D- -- 1- ug IL 1 1 j 10 -~--SW846 35108/82708 SVOCs by GC/MS X03165-011

----·· ~------------~------~-----------,.------~-~--·----~--~

120-82-1 1,2,4-Trichlorobenzene ND ug IL 1

95-50-1 1,2-Dichlorobenzene ND ' ug IL -----1- -·------------+-----------t-----+---·-----·---r------------------ -------··-t-----t

541-73-1 1,3-Dichlorobenzene ND ug IL ------------+----------+-----+------+-------+-------+--------·

106-46-7 1,4-Dichlorobenzene ND ug IL ---~--- -------------~-------+---------t·-------- --

90-12-0 1 1-Methylnaphthalene ND ug IL 1 58-90-2 1 2,3,4,6-Tetrachlorophenol ___ N_D ___ -- ··-~ · ug IL +-1-

--------------r-----i-------------+- - -----2,4,5-Trichlorophenol ND ug IL f 1

2,4,6-Trichlorophenol ND ug IL ' 1 5 --~-------~-------------------------J- ------- - --- -------------- ~------ ···-

120-83-2 2,4-Dichlorophenol ND i ug IL f ! 1 5 105-67-9 j 2,4-Dimethylphenol ND ___

1

1 ____ u_g_I_~ __ ;.-=- ____ _L ____ 1_u ___ t=_1_-__ --_·-_--_·-

51-28-5 1 2,4-Dinitrophenol -~~---------~!_L __ 1____ 10

i-2i-14-2·-I 2,4-Dinitrotoluene ND ________ L~-~--~! _____ -_·-·_·-·+-;_·-----~-~==-·~=:===-5--_-_-_-r+----_-___ _,_,

u6_D6-20-2 1------~ 6-Dinitrotoluene ND I ug IL --·- -f---·-·-·------·-+---5----t---i 91-58-7 2-Chloronaphthalene ND ug IL 1 1 ····---.!..-----------+------~--~---+--·

95-57-~_. J . ··- 2-Chlorophenol ND ug IL _ .. _ L __ _1_ ___ ~----··--+-----t 91~~7~~j_ ___ 2~f\ll~!hY~~P~!h_~l~_n_ei__ __ _ __ .. _ND ug ! L_ _ _______ 1_ ____ 1_

5 ,-----;·--··--·-

5 88-06-2

"" 04-22-03 . ,.

04-22-0'-.

04-22-03

04-22-03

04-22-0:'..

04-22-03·

04-22-03¥

04-22-0"° 04-22-03'

04-22-03'·

04-22-0'1. ..

04-22-03-" %·,

04-22-03

04-22-03'

04-22-0:.>

04-22-03

04-22-03-

04-22-0:.>"

04-22-03

04-22-03--.h

04-22-0:?•'

04-22-03

04-22-03·

04-22-0?

04-26-03

04-26-03'

04-26-0Z

04-26-03.

04-26-03

04-26-0:

04-26-03

04-26-03'

04-26-0:?

04-26-03.

04-26-03'

04-26-0:'.

04-26-03

04-26-03

04-26-0:..

04-26-03

SQLCoyote: Reports 1.0.0305281535XX Report Date 6119103 9:56:39 AM ·



Client:

.:iroject:



--~------ --·· -- - -I D Not applicable due to sample dilution 1

Order: 0304504 PHl16

-----


Run Sequence

X03165 XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

,XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

· XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

· XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

Page 19 of 25



SW846 35108/82708 SVOCs by GC/MS X03165-011 95-48-i_!_ ------2-rvieiilYIPl1e-r1al ______ ---ND I __ u~~_L: __ ·---~~1- ]=::!-=-- 04-26-03

~~:~:;: j . ·- ----~;-~J~~~~~~~------- ~-~-----+~--~-:--~-~ __ :__ - - -=----r-~ ~ ___ ___;___ -+----- ~::~::~: ::::-::~-ti - ~·~:~:::=:~F- --1--~~ -[ ~:; t i =~~-±: ~ ~ I ::::: 534-52-1

1 _ 4,6-Dinitro-2-methylphenol ~--- _ ~[) -~-- ~g-TL-_ -r~==---- ___ _ _ __ _1_ __ 1 o 04-26-03

101-55-3 ___ j 4-Bromophenyl-phenylether ND ug IL i 1 1 04-26-03

59-50-7 I ... ~::chlciro-~hYIPheno-1 - __ F ___ -- _ND ug I L -r--- -T--- - 04-26-03

106-47-8, 4-Chloroaniline N_D "Li9 /L.---j---=-==r= ___ 1_== _s _ 04-26-03

71o0~~671;3_-~ ____ 4_-C_,h_lo_r_~-~N-hi:-r:-:-l~-~l-~;-;-y_le_th_e_r_-+----- ~~ ___ --~~~~--t-------~. --+ --· '.; -~-1

~::~::~:

1803~~~: __ 1 -----A-4~-~-~-:o_:_h~-~-:n-o~-----+----~--~----- ---ug ~ ~- --+==-~===t--~-===~-~~-- ____ 1 ~:-~:-~:

-2--0-8--9-6--8-'------A-c_e_n_a-ph-t-hy-l-en-e----+-----ND ---~ ~~IL -+--1 · 1--1- ~ 04:26:03

1622;~13;~7 ---A--z-:--b~--~--~-li--i=;-&-~-1--:-_2 ___ -----+-------~-~----jt-----~-:-;-~-----+---=--=- : J-i-~ -1 :::::: Diphenylhydrazine

i 56-55-3

~~~i~;;~. - ~~- L _f [[~-=f _0~1-tJ-f :~~t- b;:;;_~i~~f b;t:~::,. -i - :N~~D ~ ~-Lulg-i/~l-J~--±~~ !-

1

- Lj1~1I --, 04-26-03

04-26-03

04-26-03

04-26-03

04-26-03

04-26-03

04-26-03

04-26-03

04-26-03

04-26-03

1 · 50-32-8

I 191-24-2

108~60-1--1- bis(2-Chloroisopropyl)ether += 1

·----·---------···----------- ·---- ---- ------------------------------ -r I 5 ----,--1 117-8i-=7 - bis(2-Ethylhexyl)phthalate 11 o ug I L

h5:6~_-7_,_ ____ ~IJty_l~e_n_ylpht_ti~~~te _____ , _______ 1~8___ ___ ug IL , ____ 1 ____ ,_ ___ 04-26-03 218-01-9 · Chrysene , ND ug J L I 1 1 04-26-03

--Dii:lenz(a~hianthracene----1--·- ND ----------u9;1._- __ 1

___ 1 ___ 1=~-1--__. __ ~ 04-26-03

E:, , _ ~:;~~;:::~ 1 ~~- :m_ --== -~-1- ~'---_1 :::~: t1;~~~0----- --~~;~;;; __________ ---~:1---+ ~:~~ __ -L ~ ~::~::~: 206-44-0 ----~~_i:_a_n_the_n_e -----+ ND 1 ug IL 1 , 04-26-03

1~~-~73-:-1 --~-------H __ e_x __ a_:_~u_l:_:o_e;_:_n_ze_n_e_=-----__ ++--- ~~ m----+~--~~ --- --1--, - 1

1

0 ~::~::~: ~~~~~tr Hex;~~~;;:~;~o~;~~-~:-~_~e_n_e ____ +-----~--~ 1- ~~+t __ _!__: · -- ! -~ 1--~~---·-_, --~ ~::~::~: 16

;;:~-~ 1----l-nd-~-~-:-~·1-c~-~0-,;-~c-~-~p-:-~:-n-e--+----~--~------_ __J____.!_ ~~-t--+ ----~t--- --~ _ _c_ __ j ~::~::~:

53-70-3




Client:

Project:





Run Sequence

X03165

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

X03165

XG.2003. 703.11

XG.2003. 703.11

XG.2003. 703.11

XG.2003.703.11

XG.2003.703.11

XG.2003. 703.11

XG.2003. 703.11

XG.2003. 703.11

XG.2003. 703.11

XG.2003. 703.11

XG.2003.703.11

XG.2003.703.11

XG.2003.703.11

XG.2003.703.11

XG.2003.703.11

XG.2003.703.11

XG.2003.703.11

XG.2003.703.11

XG.2003. 703.11

XG.2003.703.11

XG.2003.703.11

XG.2003. 703.11

XG.2003. 703.11

XG.2003. 703.11

XG.2003. 703.11

XG.2003.703.11

XG.2003.703.11

XG.2003.703.11

XG.2003.703.11

XG.2003.703.11

XG.2003.703.11

Page 20 of 25



SW846 35108/82708 SVOCs by GC/MS X03165-011

~~~~~:: L-- - -N-':-~-~-~h-oa_r~e-nn_ee ___ __,_ --~~-- -- ...... --1-- -~~ ~ ~ - -------~ --1~ ---~- ~ =t=l 98-95~3-i Nitrobenzene -----·-----N-D----+1---u-g_/_L _ _j_ _____ -_-~_-_-:--_-_-____

11

11

____

1

, -~~--~1-~1·0· ~l- I 62-75-9 ! n-Nitroso-dimethyl-amine ND ___ --+---u9/L-- · 621-64-7 I n-Nitroso-di-n-propylamine -----N6 _____ 1 ug IL

---8-6--30--6·--- 1 n-Nitrosodiphenylamine ND r-··ugt_L __

8_7 ___ 8_6 ___ 5-+---Pentachlorophenol ·-·N6_____ ug IL _1 ___ -I 10 '

f-~--~-:~~ ~-._-l_ ---__ -~-p-"~J,~~-~-en-e-------~~-=-~-----+~---~-~-'l_-_~-=.~-=--=-~+--~-=-=-----_-_--_-_-_-_------=--+··~------~_··_-_-_._j_-_--~+-:t-r l SW846 35108182708 SVOCs by GC/MS

-----120-82._-1--+l--1_,2_,4_-T:ichlorobenzene

95-50-1 1,2-Dichlorobenzene 541-73-1 .. ! 1,3-Dichlorobenzene

106-46-7 I 1,4-Dichlorobenzene ---------+.-----------~

90-~j_. 1-Methylnaphthalene

58-90-2 ! 2,3,4,6-Tetrachlorophenol ------

_95-95-4 J-_- 2,4,5-Trichlorophenol

88:06~~~2,4,6-Trichlorophenol

120-83-2 2,4-Dichlorophenol .. }-----

105-67~9 J.. ... 2,4:Dimethylp~e_n_o_l __ _J_I _

51-28-5 I 2,4-Dinitrophenol 1·

12~~14-2 r=---2,~-Dinitrotoluen-e---1---606-2?~ __ .l.. ____ ~·?-Dinitrotoluene 91-58-7 i 2-Chloronaphthalene 95:57-ST ___ - 2-Chlorophenol

! 91-57-6 I

95-48-7

88-74-4

2-Methylnaphthalene

2-Methylphenol

2-Nitroaniline

X03165-013 ·-

1

1 . -·

1

~ 1

I I - -1

I 5 I c _ _j ____

=r··-··-------l==-ND ug IL - -~--. ---- -- -----------'----

ND ug IL ------ --- ----------- - - -

N~--------~_L._ _ _j ___ -- -ND . ~_L ___ _[ ND ug IL

ND ug IL

' ~~ ~ ~ - --···- - - --+---r-+- : 3-· --- ·----- ----- ----- -------- -----~---·----------

~~ --i ~~+~-==~~-~-~~~--±~-+--+~ ~- .... ------ND ________ L ug/L I l- 1 10 i I ND '. ug I L 1 . 5 -~

-t --!---- - ~ I -1 ND !----ug-T"i: --; _1 _____ • --5-- --------1 ND ~[_- . -"------i-·--: 1 i ND ug I L -- -; 1 -. - 1 --,

-+··----·

ND

ND

ND ug IL i 1 1

ND ug IL

ND ug IL l- ---~----- --~--------j-------1--~------ - _L~---·

ug IL

2-Nitrophenol ND

3,3-Dichlorobenzidine ND

3+4 Methylphenol ND

ug IL

-~~=-1· ug IL

99-09-2 3-Nitroaniline ND ug IL ·-- . - ---------~---- ------- - -

4,6-Dinitro-2-methylphenol ND 534-52-1 ug I L -+--------------+---------+-------··-- ·--···

4-Bromophenyl-phenylether ND 101-55-3 ug/L ------------1----------+- ------------- -----··

5

10

1

5 10

5~_50_-_7 -+---4-Chloro-3-methylphenol ND _ H t,· ug IL i 106-47-8 4-Chloroan_i_lin_e ___ -+-____ ND --+· ug IL + ___ 1 ___ -r-----+---

':~:::: ~-•-Chlo'E~:::::~;'-'e_t_he_r _ _(_ ___ ~-~----_J-'-;-~~ l_-_~f t=+--r----83-32=-91 ··· · __ A_c_e_n_a_p-ht_h_e-ne-----'--- ND ' ug I c-+--- 1 : 1 • i

208-9~~ Acenaphthylene _____ ;_ __ =-~~~==±--ug 11:=r·--m 1 _fH--H 1 m--:--1

04-26-0"" ..

04-26-03

04-26-03'

04-26-0:>.

04-26-03·

04-26-03 ,. 04-26-03.

04-26-03•

04-26-03' , 04-26-0:>.

04-26-0:'-"

04-29-03.

04-29-0Z>·

04-29-02

04-29-03.

04-29-03

04-29-02

04-29-03

04-29-03

04-29-0~

04-29-03

04-29-03

04-29-0::'

04-29-03

04-29-03

04-29-02

04-29-03

04-29-03

04-29-0:'

04-29-03

04-29-03

04-29-0Z

04-29-03

04-29-03

04-29-0~

04-29-03

04-29-03

04-29-0:0

04-29-03

04-29-03

04-29-0~

04-29-03

SQLCoyote: Reporls 1.0.0305281535)()( Reporl Date 6119103 10:49:07 AM



Client:

?reject:



D Not applicable due to sample dilution Order: 0304504 PHl16

- ----~-·- ---------------

L Not applicable due to MDL proximity


Run Sequence

X03165 XG.2003. 703.11

XG.2003.703.11

XG.2003.703.11

XG.2003. 703.11

XG.2003.703.11

XG.2003.703.11

XG.2003. 703.11

XG.2003. 703.11

XG.2003. 703.11

XG.2003.703.11

XG.2003. 703.11

XG.2003. 703.11

XG.2003. 703.11

XG.2003.703.11

XG.2003.703.11

XG.2003.703.11

XG.2003. 703.11

XG.2003. 703.11

XG.2003.703.11

XG.2003.703.11

XG.2003.703.11

XG.2003. 703.11

XG.2003.703.11

XG.2003.703.11

XG.2003. 703.11

XG.2003.703.11

XG.2003.703.11

XG.2003.703.11

XG.2003. 703.11

XG.2003.703.11

XG.2003.703.11

XG.2003.703.11

XG.2003.703.11

XG.2003.703.11

XG.2003.703.11

XG.2003.703.11

XG.2003.703.11

XG.2003. 703.11

XG.2003. 703.11

Page 21 of 25



SW846 35108182708 SVOCs by GCIMS -52.:s3:3-1· 120-12=71

Aniline ND ug I -i..--1-----·--· .

------~~t_h_ra_~:r:i_e________ ·-ND ___ -r= ug IL.:__~-- ___ . 1 Azobenzene&1,2- ____ ND__ I ug IL 1

Diphenylhydrazine 56--5-5--3 --+----8-e-nz_o_(_a_) -a-nt-h-ra_c_e-ne ______ N_D · ·· ----ugTL-_J~=~------+-- ... _!jO.::_~ Benzo(a)pyrene ND ;__ --~~!~_i1 -----+-- _1_

Benzo(b & k)fluoranthene ND ug I L , 1 -·----+--- --- - -·- -- --

191-24-2 Benzo(g,h,i)perylene ND ~~!_L __ l _______ j ___ 1 64-85-0 Benzoic acid ND ug I L 1 •

1 100-51-6 Benzyl alcohol ---t-----· ND ug il-----, --------1--

--------+- ·-·-------~------- . . . .. ·-----!-··-111-44-4 , bis (2-Chloroethyl) ether ND ug IL

111-91-1 bis(2-Chloroethoxy)methane ND ug IL 108-60-1 bis(2-Chloroisopropyl)ether I ND ---- - ~-Tl..

X03165-013

10

' 11?-8WT bis(2-Ethylhexyl)phttialate ____ T ___ ----z?___ ug IL ··-···----· 5 '

85-68-7 - -- -Butylbenzylphthalate ND , ug I L !- -1 1 -- -r ---· --t - 1--- .f --·--·---+---·

::;::, D;be~~::~:;:::~~,. · · ·~"N-~DD_ .. _ I ~_,~u :g' ;/' ,L~_-;-r=~ i +-=-1

=-=-~ !:::;,~~~~: ND 1 "91L =--:-==I-~~ 117-84-0 I di-n-Octylphthalate ND -+- ug/L --- ----1---+-- 1- --

___ ----------L------ ----- --- -- - ------ i --- ---

206-44-0 Fluoranthene ND ---~_J___ 1 ; 1 86737 Fluorene ND ug I L I ! 1

1~8-74-1 ···· ·Hexachlorobenzene i -----~~==-----Ugll-C~-- ______ t~--- _L-=10--:= _ ~~::~:: He::~~~~~~~~:~:~~::~ene -·+ ------~-~-----, ~~ ~ ~ --·--------- -f-- 1 I-~~ -----t-67-72-1 Hexachloroethane 1 ND. -----~,-- ug IL--- --+---~ • ---5--r-·

L1'"'"' t .. --1nden0{1,2,3-cd)pyrene -No-··-----r-u9/L-- 1- ---i- --------78-~~~ _ _ lsophorone ND ug I L +-_ __L ___ _2__ _ -~-+--j

::::~~~-t~- ~i:::::~:~: _NN~DDD---=T-[ uuuggg Ill LLL ... l._1· .. __ _LI - _111 • n-~-1 = 6~75-9 1-_ _ri~Nitroso-dime_~hyl-amine 1 o 62~~4-7 . n-Nitroso-di-n-propylamine ND ·· 1 --ug/l..-1----:=--T ---- --1- - - ---

JJ!t,t-~:2~:~:oe ----~·- "'''-+-==- -~~j1 ~-L~~1;~ II --:

129-ocl-o j'- Pyrene 1

----------·-·-----·--·· _____ l______ --r------' 110-86-1 . Pyridine 1 ! 10 ; ;

--·------ ------- I_---·-----------'

ND ug IL

ND ug IL

ND ug IL -----ND ug IL

------ND ug IL

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

SQLCoyote: Reports 1. 0. 0305281535XX Report Date 6119103 10:49:37 AM



Client:

Project:



DJ Not applicable due to sample dilution i

L I Not applicable due to MDL proximity Order: 0304504 PHl16

Type: MS: Matrix Spike Matrix: WATER -----------~----··-·-----------

Run Sequence

M03559 MT.2003.522.19

X03200 XG.2003.727.12

XG.2003.727.12

M03548 MT.2003.521.14

MT.2003.511.38

MT.2003.511.38

MT.2003.521.14

M03550 MT.2003.551.37

MT.2003. 551. 37

MT.2003.551.17

MT.2003.551.37

MT.2003. 551. 37

MT.2003.551.37

MT.2003.551.17

MT.2003.551.37

MT.2003.551.37

MT.2003.551.37

MT.2003.551.37

MT.2003.551.37

MT.2003.551.37

MT.2003.551.17

MT.2003.551.37

X03194 XG.2003. 785.16

XG.2003. 785.16

XG.2003. 785.16

XG.2003. 785.16

XG.2003.785.16

XG.2003.785.16

X03189

XG.2003. 750.8

X03165

XG.2003.622.5

XG.2003.622.5

XG.2003.622.5

XG.2003.622.5

XG.2003.622.5

XG.2003.622.5

Page 22 of 25



EPA 245.1 Mercury by CVAA M03559-005

~I _%_R_e_c_o_ve_ry~I _BO_-__ 1_20_1~----~_NA_ [_ ___ =:] 05-01-0:.

EPA 504 EDB/DBCP by GCIECD X03200-005

I 1,2-Dibromo-3-chloropropane -Ff---·-_--___ 78_ I % Recovery --6o~-14c5T--1- - -T NA L:=J 1,2-Dibromoethane, EDB J _______ 8_2 ___ -_T~0/o-Recovery 60- 140 -------~-:~~[~N~ C__J

SW846 3005Al601 OA ICP M03548-005

05-05-02

05-05-03'

119 1 % Recovery- - BO - 120 I - -T--NA - 05-01-0"' --- -----Bery 11 i um 7440-41-7

7440-47-3 I ·------+--

Chromium _1_1_5-----+-%-o-R-ecovery 80 - 120 i NA 05-01-0:" ---~---- ----- -----+----+------ ------~

7440-48-4 Cobalt 98 % Recovery 80 - 120 NA 05-01-03,

7440-50-8 I Copper 112 % Recovery 80 - 120 I NA 05-01-0"' ___ _J_ ______________ ~-------~-

SW846 3005A6020 ICP-MS M03550-005

~~~~:::~ I A;:::~i7 19084 ! ~ ::~~~:~ _;: ~~~--+---~---+--~-~-~-·-__,

~40-39-3 -I Barium 99 i % Recovery 70 - 130 __ 1 ~- _ NA

7440-39-3 Barium ' 100 , % Recovery ! 70 - 130 1 NA ----- ----~-- -------j------- -- + ----~----1

7440-43-9 I Cadmium ! 1 NA

7 439-92-1 Lead 1 NA _______________ )___ ;

10 NA , ________ , ____ _ 1 NA

i7B2-49-2 ---1 - Selenium -· -- ---~ 9 1· --~----N-A--+ ·-------1

7440:22-4-:_-i----:---S-il-ver___ - --=-=: 92____ %Recovery 70- 130 .L__:_·-_-_---_1_-_____ ,l __ N_A _ ___, ___ ._

7440-28-0 Thallium 96 % Recovery 70 - 130 i 1 NA ---- ----. ----f---f-------------·--+-·--7440-31-5 Tin 110 %Recovery 70- 130 I 1 NA

7440-62-2 Vanadium r-------- --i-----+---------- ·-· - ·---------------t-----1

88 % Recovery 70 - 130 1 NA r 7440-66-6~------ -·- --- --------+----------f------+--__,

54 I % Rec~very ; 70 - 130 --

Zinc ----

10 NA -----r--· -~--

7440-66-6 Zinc -~ ___ 8_6 ___ J_D,fo ~~covery I 70- 130 1 NA

SW846 35108/8081A Pesticides by GC/ECD X03194-005

-~~5°;~2 1---- ~~~~ir~n t _ ___ __ 170~ _--_-: ~ ::~;y~~1_4_5~_:_--_!~~ ~- <_L -- ~---~~- ·-- +-----__,

72-20-8 I Endrin 99 i Ojo Recovery I 56 - 121 i 2 NA_-+--------J

58-89-9 g-BHC 94 -=I% Recovery i 56 - _ __1_2~_ L_ ___ ~----- __ NA

:~::::: I H:.~~~~~r :! i ~ ::~:~:~. ;~: ~~-~--f-__ =-t-~~~-:~=~~~---+----J X03189-006

05-05-02

05-05-03.

05-05-0~

05-05-02'

05-05-03.

05-05-0J

05-05-0<

05-05-03_

05-05-03·

05-05-02'

05-05-03

05-05-03

05-05-0<

05-05-03

05-05-03

05-08-0:

05-08-03.

05-08-03

05-08-0:.

05-08-03

05-08-03

80 ] % Recov~~_:-_ _1_~_o_J__ 2 NA I H __ ] 05-06-0:

106-46-7 '

121-14-2 I

95-57-8

1,4-Dichlorobenzene

2,4-Dinitrotoluene

2-Chlorophenol ------~---------

59-50-7 4-Chloro-3-methylphenol -------~-~--------------

100-02-7 4-Nitrophenol

81

78

% Recovery 24 - 96

- ··- ' 0io Recovery 27 - 121 -- ------- ----------+------------ ___ _;_ _______ --

X03165-005 1--rw..- 04-1 0-02

NA 04-10-03 - ----- ----+------+----

2

2

NA

NA

74 , % Recovery 1 23 - 97 2 NA

04-10-0:

04-10-0~

04-10-03

04-10-0~ 37 ____ To/oRecovery:-10~ 80 J_2 ____ , _____ N __ A __ ~-------

SQLCoyote: Reports 1. 0. 0305281535XX Report Date 6119103 10:50:22 AM··



Client:

?reject:



- --------------------------- -D ! Not applicable due to sample dilution 1

Order: 0304504 PHl16 L _,--Not applicable due to MDL proximity 1

Type: MS: Matrix Spike Matrix: WATER ---------- ----------------------

Run Sequence

X03165 XG.2003.622.5

XG.2003.622.5

XG.2003.622.5

XG.2003.622.5

XG.2003.622.5

XG.2003.622.5



SW846 35108182708 SVOCs by GCIMS X03165-005

NA i 04-10-03 I ----

1 NA 04-10-03 ---- --

! NA 04-10-03 --------i

NA 04-10-03 ~~t o-~f ~"' ~--- ---i-=~-~t~~~!~~~* ,-~~~ NA 04-10-03

- -- --

NA 04-10-03

108-95-2 I Phenol ' 36 % Recovery 2 r --------------------!- -·-·-- ----------- -- -

I 129-00-~ l _____ -~yrene ----· 1 _____ 8~------~?oReco_very______ 2

Type: MSD: Matrix Spike Duplicate Precision Matrix: WATER

Run Sequence

M03559 MT.2003.522.20

X03200 XG.2003.727.13

XG.2003.727.13

M03548 MT.2003.521.15

MT.2003.511.39

MT.2003.511.39

MT.2003.521.15

M03550 MT.2003.551.38

MT.2003.551.38

MT.2003.551.18

MT.2003.551.38

MT.2003.551.38

MT.2003.551.38

MT.2003.551."l 8

MT.2003.551.38

MT.2003.551.38

MT.2003.551.38

MT.2003.551.38

MT.2003.551.38

MT.2003.551.38

MT.2003.551.18

MT.2003.551.38

X03194 XG.2003.785.17

XG.2003.785.17

XG.2003. 785.17

Page 23 of 25



EPA 245.1 Mercury by CVAA M03559-006

7439~:~-61==~----Me_r~~-ry -------5- RPO 0 - 20 1- NA --,--1 05-01-03 __ L___ -

EPA 504 ED8/D8CP by GC/ECD X03200-006

-=-==--F~1._~·.:=-:!~~~1:~::~-o 0_P;_n_e_~--11 ------~RPO - [ o- 20 1 NA 1 05-05-03 12 1 - RPO _,_j -c)=-;fo - - 1

____[_____ ---- ---·-· -----------------

n HNA ___ r ___ j 05-05-03

SW846 3005A/601 OA ICP M03548-006

~~---+==~ 05-01-03

05-01-03 ~~:~::~:: F==~ - ~hcer~ob:ai~lt: -__ ·_-- ____ <_=-_71_1 _____ -_-_-----·~---· __ --_.-1-!.·· __ -_:_:_-~_-_-_-_:-_-___ o_- 20 ~L-- 1

i ~~;~::~:: t-_~_-_ _ __ Coppe' · 7 ::~ -H 1 ·- ~ -NA----~-~ 05-01-03

j -- ~}). __ J ___ J 05-01-03

SW846 3005A6020 ICP-MS M03550-006 ----~--- ----- --~--

, 7440-36-0 i Antimony 3

i ~~~1~~~ l -- ---~~r~~~ . ------------~ 1

~4o-39=3j-- Barium

___ R_P_O _j_ _ _<J= ~0- _. • NA ----c------j

_R_P_O __ ! __ 0 _- _ 20

RPO 0 - 20 10

NA

NA

: 7440-43-9 I Cadmium , 7439~92-1t --L~-----

--

7 RPO 0 - 20

< 1 RPO 0- 20 -------------- --------- - ----r-

NA

NA

2 RPO 0 - 20 1 NA

7440-02-0 Nickel -----<1-- - · RPO -1-0~ 20 1 O NA -- --+----; -------------• - -----------··- ---- ---------- ( _________________________ -+-------- I

7440-02-0 ' Nickel 2 : RPO I O - 20 • 1 NA

7782--49=2_-l!- ------~elenium < 1 -r RPO rnr-- ·0·- :zo · --H Hi --- HL __ NA____ ..

7440-22-4 Silver 2 -----t--L1_,: .•. -_--.---·--··_-RRRR···:Pp_o~D- -----t---:-.:,:; -~oo __ ~ __ --·-2~~·-~oo· -- - _[·-----_ -~~11 __ -_ -__ -_ ~=-~Nr¥~A- --~----------. ;:rn:}~= ~--~:,:~:: _ --- __ ±=_ <_124_1___ - I 0 - -

7440-66-6 1 Zinc 14 RPO -i--~-~-0 [ 10

i446=56-:-6-l Zinc 1 RPO ' 0 - 20 ' 1 - _ ______l_ ________ . _____ _

NA ---------~

NA

SW846 35108/8081A Pesticides by GC/ECD X03194-006 - 5 ---1 -RPO I 0 - 22 - 2 ---- _N_A_~--

- < 1 -~-- -1 - - H ---=~~-. ~r--=j! -~' ----~--~~-- _l _ _;;)~- i __ ; - _L__

309.00-2 r ---Aldrin

60-57-1 Dieldrin 7-2--2-0--8 j· ' -

------ -----··--------Endrin

05-05-03

05-05-03

05-05-03

05-05-03

05-05-03

05-05-03

05-05-03

05-05-03

05-05-03

05-05-03

05-05-03

05-05-03

05-05-03

05-05-03

05-05-03

05-08-03

05-08-03

05-08-03




Client:

Project:


APmL03SAMPLEEVENT Explanation of codes _____ " ______________ _

D Not applicable due to sample dilution -Order: 0304504 PHl16 L Not applicable due to MDL proximity

-------------------------Type: MSD: Matrix Spike Duplicate Precision Matrix: WATER

Run Sequence

X03194

XG.2003.785.17

XG.2003. 785.17

XG.2003.785.17

X03189

XG.2003. 750.9

X03165

XG.2003.622.6

XG-2003.622.6

XG.2003.622.6

XG.2003.622.6

XG.2003.622.6

XG.2003.622.6

XG.2003.622.6

XG.2003.622.6

XG.2003.622.6

XG.2003.622.6

XG.2003.622.6

XG.2003.622.6




- _-::~::~:~::~~~~-~--_-_HP_~_i_~-c~-~-r-- -~----~-1-------=·----,-~I ----=-:-~-----t--~---:---~-1 t~~ ~ ~~ ~ -1 • SW846 3510818082 PC8s by GCIECD X03189-007

A

05-08-0~,

05-08-03•

05-08-03'

[ 1109~:~~-:5_ l Aroclor 1260 [ < 1 --~-R_P_o_=r ___ o - 33 1 ·--2--[--NA 05-06-0~--

SW846 35108182708 SVOCs by GCIMS X03165-006 12-o--82--1-- 1,2,4-Trichlorobenzene 3 RPO T 0 - 28

~--2

2

2

NA 04-10-0:.>'

1----N_-A--_ _,_f--_-__ -__ -_J 04-10-03' 106-46-7 1,4-0ichlorobenzene 4 ____ ,____R_P_O_ --t 0 - 28

0 - 38 121-14-2 2,4-0initrotoluene 4 ---~[ __ R_P_O__ _ __ _ NA : ! 04-10-0::..

_1_:0:_;~_0:2_:~_7 ~--4--:_c_h 2-1-~-~-o_:--_t-;_:~:~~h~-h-~-n-~-~-h-l_e_n~o~I~~~~~~~---_ --<:=1~--==--==--_ -~t=·--==-· ===:=-~--~~:-~-:-~-:- -~- ~22 ! ~N~Atl. ~ 83-32-9 ; Acenaphthene RPO 0 - 31 117:84-0 -~ ---d-i--n--Octylphthalate 5 RP-O-~l~-0---20---+- 2 NA --+-----1 621-64-7 n-Nitroso-di-n-propylamine 2 RPO I O - 38 2 NA

87-86-5 Pentachlorophenol << 11 I RRPPOO -=Do --~4502 r- '2- - ..=---NN-AA- --108-95-2 , Phenol 129-oo:o- · -- ------Pyrene- - ----- -- -- - --- - < 1 RPO o - 31 2 NA - -----

-· -·---· ___________________ .,________ -- ---------- --- -- -----------

04-10-0:.>'

04-10-03, r

04-10-0:ci.

04-10-0:'" .,

04-10-03

04-10-0'1

04-10-0?

04-10-03 --·

04-10-0s-

Type: MSD: Matrix Spike Duplicate Accuracy Matrix: WATER

Run Sequence

M03559

MT.2003.522.20

X03200

XG.2003.727.13

XG.2003.727.13

M03548

MT.2003.521.15

MT.2003.511.39

MT.2003.511.39

MT.2003.521.15

M03550 MT.2003.551.38

MT.2003.551.38

MT.2003.551.18

MT.2003.551.38

MT.2003.551.38

MT.2003.551.38

MT.2003.551.18

Page 24 of 25



M03559-006 EPA 245.1 Mercury by CVAA 1439:97_5 ·r------

1 Mercury 126 I% Recovery [ 86~--120=1=-~-~-----i- NA_] ____ ] 05-01-03·

EPA 504 ED8/D8CP by GC/ECD X03200-006

I -!

---+--1,_2_-0_i_br_o_m_o_-3_-_c_hl_o_ro_p_ro_p_a_n_e--1 ____ 8_8 ____ --+'_%_o_R_e_co_v_e_ry-+-_6_0- 14~=i==NA I __ l _ J _ _ 1,2-0ibromoethan_e_, _E0_8 __ ~ ___ 9_3___ % Recovery 60 - 14~~[-~ _ _L_ NA_~. -~]

7440-41-7

7440-47-3

7440-48-4

7440-50-8

7440-36-0 -----

7440-38-2

7440-39-3

SW846 3005A/6010A ICP

Beryllium

Chromium

Cobalt

Copper

SW846 3005A6020 ICP-MS M03550-006

Antimony ____ ,__ ___ 95 I% Recovery_ __ 7_0_~-130:=-j_-_~-~~-=I=--N_A_--_-+--_ ____,

Arsenic -~-----10_3 _______ ! % Recovery 70 - 130 1 ' NA

- ------ --- Barium I 98 ! % Recovery 70 - 130---+ __ 1 o_ NA Bariu_m _____ +--- 93 1 % Recovery 70 - 130 NA

05-05-0~

05-05-03

05-01-03'

05-01-0'._

05-01-03.

05-01-01"

05-05-0:

05-05-03

05-05-03"

05-05-0: 7440-39-3 I

7440-43-9 Cadmium I 91 % Recovery 70 - 130 NA I 05-05-0~ ------~- --------------7439-92-1

7440-02-0

----- .. ---,-·-.------ -

Lead 96 ' % Recovery ; 70 - 130 Nickel _"""'93___ --,, % Recovery[7o~-13o , 10 -----------·--~'-----~ - ------~--·---- _.:._____i______ __ ------~-~-

05-05-03

05-05-0~

SQLCoyote: Reports 1.0.0305281535)()( Report Date 6119103 10:51:44 AM

STANDARD



Client:

,=>roject:




- ___ ,, - ------------------··-·------ ·----- ------·----------------------- - -

Type: MSD: Matrix Spike Duplicate Accuracy Matrix: WATER

Run Sequence

M03550 MT.2003.551.38

MT.2003.551.38

MT.2003.551.38

1\llT.2003.551.38

MT.2003.551.38

MT.2003.551.38

.lllT.2003.551.18

MT.2003.551.38

X03194 XG.2003.785.17

XG.2003.785.17

XG.2003. 785.17

XG.2003. 785.17

XG.2003. 785.17

XG.2003. 785.17

X03189 XG.2003.750.9

X03165

XG.2003.622.6

XG.2003.622.6

XG.2003.622.6

XG.2003.622.6

XG.2003.622.6

XG.2003.622.6

XG.2003.622.6

XG.2003.622.6

XG.2003.622.6

XG.2003.622.6

XG.2003.622.6

XG.2003.622.6

Page 25 of 25


Dilution

Factor

Detection

Limit

Run

Code Date

SW846 3005A6020 ICP-MS -- -----i---

! 7 440-02-0 '

I 7782-49-2

7440-22-4

7440-28-0 I

Nickel --- - - - 80~----=_L!o-ReCoWYf?o--~iio

Selenium ____ 9_4 __ ___l_!o Recovery ! 70 - 130

Silver 90 i % Recovery ! 70 - 130 Thallium - -- --96- --- T01;Recovery i 10 - 130

I 7440-31-5 !

7440:62-=-n-7 44c):65:::[3_1_

_ -----~----------- 96 -- _";o~~c~v~rr_j 70- 130 Vanadium 86 · % Recovery i 70 - 130 '

7440-66-6 I Zinc 63 . o/o Recoveryf?o - 130 -----zinc- 84----~o/o- Rec~~ery 1-10 - 130

SW846 3510818081A Pesticides by GCIECD ------~-- --------~-----~--

309-00-2 Aldrin 68 , % Recovery 40 - 120 ;

M03550-006 -~--NA----r~l

- ----- - --1- -- 1

1 NA I I

1 NA . I ----t-----~

NA -- - - ------------

NA

1 NA

10 NA

NA

X03194-006 - --

2 NA

60-57-1

72-20-8

Dieldrin 103 1 % Recovery 52 - 126 2 NA

I 58-89-9 !

76-44-8

50-29-3

Endrin

g-BHC

Heptachlor

p,p-DDT

--19°8°- --- ~~:~;~~~~~:- ::-<~ ~~--1 · ~~r--B}--· +------j

82 '%Recovery 40 - 131 · 2 1 NA

--~--------------~-

~2 ___ ~o Recovery 38 - 127 2 NA __ _J __ _

SW846 3510818082 PCBs by GCIECD X03189-007

11096-82-5 81 % Recovery 60 - 120 I Aroclor 1260 '

2 NA ---- ----------------------------

SW846 35108182708 SVOCs by GCIMS 1 - 1~-2~

2-·o~=-_-:_-481

-

426-=-:~'ul __ -_._ · 1-~2~4:-fricil10r0be-nzene-- --1-----77-----c%-R:ecO'very 39 _ 98

1,4-Dichlorobenzene ~-- ____ ii=--~o-Recovery • H--~-6--97 H ____ 2 _ - ----- -

2

.: ____ ---"

05-05-03

05-05-03

05-05-03

05-05-03

05-05-03

05-05-03

05-05-03

05-05-03

05-08-03

05-08-03

05-08-03

05-08-03

05-08-03

05-08-03

05-06-03

04-10-03

04-10-03

04-10-03 2,4-Dinitrotoluene -~----- 78 ____ j__!o R_ei_covery_.__ __ 24 - 96 2

~5-57-8 I 2-Chlorophenol ' 77 i % Recovery• 27 - 121 , 2 59-50-?T 4-Chloro-3-methylphenol f--· 70-----to/o Recovery r---23 --_9_7~ _2 ___ _ 100-02:7 -r- - u~f'.Jjtrophe_ri_~ ! 38 : % Recovery , 10 - 80 - 2

NA 04-10-03 NA --~1 -~: 04-10-03

-+-----_J NA 04-10-03

- -' 2 NA 04-10-03 83-32-9 1 Acenaphthene 78 . - : % Recovery 46 - 118

------ -----.,------, 2 NA 04-10-03

2 NA 04-10-03

2 NA I 04-10-03 _j

111-84-_o__ di-n-Octylphthalate ~~----67 : ___ ~_'%F~~_c:overy ._ 26 ~--1_3! _1 ! 62-1-64-7 -----;i=-Nitroso-di-n-propYfarnine - -r 80 1 % Recovery • 41 - 116

~7-86-5_ ; H __ _P___ei_ntachlorophenol 83 _ HJ~_Recov_t3ryJ_ __ ~H- 103

108-95-2 i Phenol 36 : % Recovery ! 12 - 89 2 NA 04-10-03 -------------- __ , -- -t------------

129-00-0 I Pyrene 83 __ __j__~°_ Re_c:ovE'lr~J_-~6 - 127 2 NA 04-10-03


STANDARD



Client:

Project:



···----. ··-·-·-------------


D-l Not applicable due to s~mple dilutionj Order: 0304504 PHl16 L Not applicable due to MDL proximity

- -


Run Sequence

X03206 XG.2003.800.7

XG.2003.800.7

-------


524

Range

Dilution

Factor

Detection

Limit

Run

Code Date

X03206-016

_______ -___ -_-II ___ -1-,2---Dichlorobenzene-d4 (SS)------95---~ - _%"'eco_veryj ~6~_-1_14-T ----- --- - - ---NA ---+-----'

_ Bromofluorobenzene (SS) _____ ~-- _ _ --· % R_e9overy L_~~----~5 I NA

05-07-03

05-07-03

Sample: 0304504-01 c Matrix: WATER

Run Sequence

X03165 XG.2003.703.18

XG.2003.703.18

XG.2003. 703.18

XG.2003.703.18

XG.2003.703.18

XG.2003.703.18



8270 X03165-019

--_-_---- _-*2,4~6-TRIBROMOPHENOL- -----100 ____ 0/c,R:ecovery '16- 123-~ ---1 NA --1 ------~--- "2-FLUOROBIPHENYL 90 i °(o_~ecovery --43_ -116--=--=-~-~~--~==-=~J\~~~

*2-FLUOROPHENOL 52 • % Recovery 21 - 100 1 NA

-----~1--·_~IT~~~~~~~~:-05 ~~ ~ ::~~~:~~ ~50-_ ::1---1- ·--·-~--- ~-~]-=-_-__ *T_E_R_PH_E_N_Y_L_-D_1_4 __ ~-----~~---- % Recovery I_ 3_3 - 141 I _ }NA

+---~ i i

I i

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

Sample: 0304504-01 D Matrix: WATER

Run Sequence

X03194 XG.2003. 785.15

CAS# Analyte

8081 -- ----(TCMX) Tetrachloro-~-xylene #2 1 ·

8082

Result

---81



X03194-004

NA · l - . - -- __ _c________J

05-08-03

X03189-004 X03189 XG.2003.750.6

-------. ----·--·-·--- ---·-·------ ---------------~--- -· ..... --------- -,--------_____ U!_C_MX)_Tetrachloro-m-xyl~~~!!~l _______ ~3 ____ '_o/_"_~_ec~vef!' __ ~o-~_1_5_Cl _ _1_ _____ 1_ NA 05-06-03

-- --------- ---- _._,,. ________________ -- ------

Sample: 0304504-02A

Run Sequence

X03206 XG.2003.800.8

XG.2003.800.8

CAS# Analyte

524

_____ - ____ .l-_-1~--D-ic-hlarobenzene-d4 (SS) Bromofluorobenzene (SS)

Sample: 0304504-02C

Run Sequence

X03165 XG.2003.703.19

XG.2003. 703.19

XG.2003. 703.19

XG.2003.703.19

CAS# Analyte

8270 _ -~-·2,4,6-TRIBROMOPHENOL ___ I

-----r *2-FLUOROBIPHENYL

" *2-FLUOROPHENOL i

*N ITROBENZENE-D5

Result

94

99

Result

88

89

40

86

Page 1 of 10 SQLCoyote: Reports

Matrix: WATER



X03206-017 % ~-ecovery I 76 - 114_1_ --- -- -- N_A- _--=] 05-07-03

______ ,_% Reco~ry __ 75 - 1_2_5_~-- _ ______ NA 05-07-03

Matrix: WATER

Units Range

Dilution

Factor

Detection

Limit

Run

Code Date

X03165-020

~~::::~ :~: ~~:r-+--F~~r1 ----····- -------- ---+-_____ _____j____..__ __ •••••••

.. 1-o/o Recovery 21 - 100 1 ; NA +-

l"foRecover_L __ 35 - 114 _ 1 r-.J_A __ L __ J

04-29-03

04-29-03

04-29-03

04-29-03

1.0.0305281535XX Report Date 6119103 9:22:10 AM



Client: Explanation of codes (

Project:


AP~L03SAMPLEEVENT D Not applicable due to sample dilution 'r Order: 0304504 PHl16 L Not applicable due to MDL proximity


Run Sequence

X03165 XG.2003. 703.19

XG.2003. 703.19

CAS#

8270

I __



X03165-020 *PHENOL-D6 30 % Recovery 10 ~-9·4-E-1 : NA ' I

*TER_P_H_E_N_Y_L_-_D_14 ___ ~-====8=1 ========°/c=o=R=e-co_v_e_ry-+-_-__ -~_-3-~--.-~-4-_1-. ·- ___ --~- -~-T--NA--+-..=J 04-29-o:(

04-29-03

·----------------·------------------------- - -·


Run Sequence

X03194 XG.2003.785.18

X03189 XG.2003.750.7

XG.2003.750.7


8081 ---- --- -- ----·------1-------------·------------ -----

1 (TCMX) T:!~chlo~o-m-xylene #2 86 • % ~=~v:r~-~-~-~__1_5~_ :_ ----- -

8082 (DCB) Decachlorobiphenyl #2

---=--=----~~(!_~~~ Tetrachloro-m-xylene #2 I

- ----- -- - -- --------

Dilution

Factor

Detection

Limit

Run

Code Date

X03194-007

-~~~--NA ---J ] 05-00-03

X03189-005 -~--,---: 05-06-03

J ___ -·-- ;_ --·-·-·-· I NA I : 05-06-03 •. - L_ ______ L__ _____ I


Run Sequence

X03206 XG.2003.800.9

XG.2003.800.9



524 X03206-018

I

. -~-1,2-Dichlorobenzene-d4 (SS) i---- - -76_11_4_1 --1 •.. - NA ---;-----i

______ i - Bromofluorobenzene (SS)·---+----96-------t-----t-==7=5=-~-·13_5 r-=J---~ °[ -~_N-A __ i~_j 05-07-03

05-07-0:"


Run Sequence

X03165 XG.2003. 703.20

XG.2003. 703.20

XG.2003. 703.20

XG.2003.703.20

XG.2003.703.20

XG.2003. 703.20


8270 *2,4,6-TRIBROMOPHENOL r· -- . -·-·35··------ j-ofo-Recovery 10-- 123

*2-FLUOROBIPHENYL 85 I % Recovery I 43 - 116 *2-FLUOROPHENOL --~1-----To;; Recovery! 2.1 - 1·00

---- ----- -- - .___ . . . . I --

82 ! % Recovery l 35 - 114 ------1--------- -

, *PHENOL-06 28 , % Recove~ 10 - 94 - ------r-----.TER_P_H_E_N_Y_L--014- -_-_-___ -- --77 ___ --1 % Reco_,_;_e_rrr__~i~~!41-

*N ITROBENZENE-05



X03165-021 NA 04-29-02

NA 04-29-03

NA 04-29-03' ----

1 04-29-02" NA NA

____ J ___ ,

04-29-03. ------ -----~----------;

' NA .l 04-29-03 ____ l ___ -·--

----- --- ··--- ----------------

Sample: 0304504-030

Run Sequence

X03194 XG.2003. 785.19

X03189 XG.2003.750.10

Page 2 of 10

CAS# Analyte

8081 _ j_~TCM~) Tetrachloro-m-xylene #2 I

8082

Result

80

SQLCoyote: Reports

Matrix: WATER



'%Recovery I 50 - 150 :

X03189-008 NA

L ___ _ ___ L __ ~__J 05-06-0:0

1.0.0305281535XX Report Date 6119103 9:24:56 AM ..



Client:

Project:



Sample: 0304504-030

Run Sequence

X03189 XG.2003.750.10

-

CAS#

Sample: 0304504-04A

Run Sequence CAS#

Analyte

8082

. (TCMX) Tetrachloro-m-xylene #2

Analyte

524 X03206 XG.2003.800.10

XG.2003.800.10

i --------

1 -

- ---------- - .. -·-

Sample: 0304504-04C

Run Sequence

X03165 XG.2003.703.21

XG.2003.703.21

XG.2003.703.21

XG.2003.703.21

XG.2003.703.21

XG.2003.703.21

CAS#

Sample: 0304504-040

Run Sequence

X03194

XG.2003.785.20

X03189 XG.2003.750.11

XG.2003.750.11

---

CAS#

I I -

Sample: 0304504-05A

Run Sequence CAS#

8081

Analyte

*PHENOL-06

*TERPHENYL-014

Analyte

i (TCMX) Tetrachloro-m-xylene #2 i

8082

(DCB) Decachlorobiphenyl #2

(TCMX) Tetrachloro-m-xylene #2

Analyte

Matrix: WATER

Result Units Range


D~ot applicable due to sample dilution- -

c_ i Not applicable -due to }v1DL proxirr1_ifI_ •



X03189-008 --- -- ----------- -- - --- -

89 % Recovery 50 - 150 ' NA 05-06-03

Result

Result

Result

Matrix:

Matrix:

WATER

Units

WATER

Units

Range

76 - 114

75 - 125

Range



Dilution

Factor

X03206-019 NA-B' ------_ . - I NA ' _______ J

05-07-03

05-07-03

Detection

Limit

Run

Code Date

X03165-022

~ ::~:~:~ !-- :~ :-~}}_j_--~--~-- ------- -· NA , i % Recovery 21 - 100 . 1

--------t- --- .. .. -+-----%Recovery 35 - 114 ' 1

. ==~;-=~----11.1 ~----- __ j

I NA '

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

% Recovery 10 - 94 t -----

-~o Recovery 33 - 141

~A---1---- I

n -1 --_§_ -1 _1

Matrix: WATER



X03194-009 -

74 ---o;;ReC:overy. ~o-~1~o_J-~= 1 ~==--~~~==T~=- J 05-08-03

X03189-009 --- ------5-5-----o;~--Recoveryf 50 ~1-so-r __ 1_ - -1. -_--NA £------_ 1_

ai___ % Recovei --_yo--_1~50 =~-i _-__ 1 l N!- -- =~-- I 05-06-03

05-06-03

---- ------···-- ----------Matrix: WATER

Result Units Range

Dilution

Factor

Detection

Limit

Run

Code Date

X03206

XG.2003.800.13

XG.2003.800.13

524 X03206-022

Page 3 of 10

-----r ---101 ______ Ofo-_ R __ e __ co_v_ery- 1_76 -_f_1_4 T-_-- -- - ,------- -·1 ____ -----1-- 1,2-Dichlorobenzene-d4 (SS)____

98 _

010 R_eco~~rY__7_5 __ 1

25 11

~: _ NNAA ____ i,-_-_-_-_-__ -_-_I! ____ J__ __ E:l_romofluorCJ_ti.:_n_z:~=-·~~S) -~-- "

05-07-03

05-07-03


STANDARf Assaigai Analytical Laboratories, Inc.


Client:

Project:



- -------------------

Explanation of codes --------- - --.------·----- ------'<,.

D N_()f__~fJE_~~b!e due to sample dilution -' Order: 0304504 PHl16 L Not applicable due to MDL proximity '

--- ------- -- --Sample: 0304504-05C Matrix: WATER

Run Sequence

X03165

XG.2003. 703.22

XG.2003.703.22

XG.2003.703.22

XG.2003.703.22

XG.2003.703.22

XG.2003.703.22

CAS# Analyte Result

8270

! . __ __:-=-·:··-~2.4~6-TRIBROMOPHENOL ~ 84

I *2-FLUOROBIPHENYL L 89 ____ ,, ____

-- ,- .

. ------· i -

*2-FLUOROPHENOL

*NITROBENZENE-D5

*PHENOL-D6

*TERPHENYL-D14 _______ __J_____ _______ _

I 50

84 ------ -- ----

36

78 -------

---------



X03165-023

% Recovery] __ 1 0 ---.,-·-

123

% Recovery i 43 - 116

% Recovery' 21 - 100 - - -·----·-

T-= +- ~~· -~--04-29-o:;,

04-29-02

04-29-03

04-29-0s

04-29-02

04-29-03 1 NA Ii ...••

- 1 i ---NA - ----1---

NA - J - ------

% Recovery 35 - 114 +-----

% Recovery 10 - 94 I

% Recovery 33- 141


Run Sequence

X03194

XG.2003.785.34

X03189 XG.2003.750.24

XG.2003.750.24

---- ·--



8081 X03194-020

(TCMX) Tetrachloro-m-xylene #2 r---------- -

86 ___ · %~ec;o~_i:_tl 50 - 15a_r_ -1- · -T-NA----;~ o5-o9-o3

8082 X03189-020 ---------------- -

(DCB) Decachlorobiphenyl #2 -- -------~--- - ---o,10--R.8Covery l 50 - 150

50 - 150

NA ' 05-07 -Os

(TCMX) Tetrachloro-m-xylene #2 1

--- - -------- - ------+----- -----~ -

9~---- __ ;_"lo~~overy NA -~ - 05-07-0:' ----- -- ___ _]_ ____ _


Run Sequence

X03206

XG.2003.817.5

XG.2003.817.5

CAS# Analyte Result

524

___ - ----~-Dichlorobenzene-d4 __ (SS_)_,_/ ___ 1_0_0_

l_ ___ B_ro_m_o_flll_c:'"_()_b_e_nz_e_n_e_(_S_S_) _ J___ _ 96



X03206-027

·-:-%Recovery I 76 - 114 r-. 1-- --, NA I I ·-°ic-o_R_e_co_v_e_ry_,_/_7_5 ___ 1_2_5 - ----- --= ~- __ J ____ J 05-07-0?

05-07-03

--- ----------------- ---

Sample: 0304504-06C

Run Sequence

X03165

XG.2003. 703.23

XG.2003. 703.23

XG.2003. 703.23

XG.2003. 703.23

XG.2003. 703.23

XG.2003. 703.23

CAS# Analyte

8270 - 1--*2~4,6-TRIBROMOPHENOL j

I

-*2-FLUOROBIPHENYL II

*2-FLUOROPHENOL

__ *_N_IT_R_O_BE_N_Z_E_N_E_-0_5_-_---+r-__ -_-

! *PHENOL-06 t - t

I

' *TERPHENYL-D14

-~---------- .

Matrix: WATER



X03165-024 ------------~---

_8 __ 6 ______ -+_%_R_e_c_o_v_e_ry_ ~~To~-~-?~ -T-------___ N_A_--1-----91 % Recovery 43 - 116 NA

-~------------C----C-·--. -----------+----- --------- -----50 % Recovery 21 - 100 ~

85 % Recovery _,_1 __ 3_5_-_~_1-1_-4_-_-~---_ -_ -_ -_-_----1--HA--~-~-------+---_, 36 --~i_°lc_o _R_ecovery: ~O - -~4 ___

1 __ ---+--__,

_ -~':___ _____ : 0_Yo_Reco_vEl_rY . 33 - 141

1 J NA

04-29-03 ..

04-29-03.

04-29-0<.

04-29-03

04-29-03

04-29·0'-

Page 4 of 10 SQLCoyote: Reports 1.0.0305281535XX Report Date 6119103 9:26:36 AM •

Client:

Project:

Order:



0304504 PHl16

Sample: 0304504-060



Matrix: WATER ------------------------

Run Sequence CAS# Analyte Result Units

8081

STANDARD


D r -NoTapplicable due to sample dilution I -+ _____ -j

L · Not applicable due to MDL proximity j


Range Factor Limit Code Date

X03194-021 X03194 XG.2003.785.48

XG.2003.785.48

--- (DCB)Decachlorobiphenyl #2--T ____ 6_7 ___ _ -----------~------ - --T

%~ecovery_t-~~ - 150 NA

NA

05-10-03

05-10-03

X03189 XG.2003.750.33

XG.2003.750.33

----+----

(TC M X) Tetrachloro-m-xylene #2 I 85

8082 - ---- ---- - -· ------,-------------

(DCB) Decachlorobiphenyl #2 i 61

I ___________ , (TCMX) Tetrachloro-m-xylene #2 ! 60

% _Rec~~'!'_, _ 50 - 150

· % Recovery 50 - 150

% Recovery 50 - 150


Run Sequence

X03206 XG.2003.800.11

XG.2003.800.11

CAS#

524

Analyte Result Units Range

-------


Run Sequence

X03165 XG.2003. 703.24

XG.2003.703.24

XG.2003. 703.24

XG.2003. 703.24

XG.2003.703.24

XG.2003.703.24

- -


8270 ~~4,6~TRIBROMOPHENOL _____ _ 89

! *2-FLUOROBIPHENYL 87 : % Recovery 43 - 116

_______ !- *2-FLUOROPHENOL - ------~--T0/o Recovery 21 - 100

---L----~~ITROBENZENE-05 85 --r0/o _~ecovery _35 - 114

*PHENOL-06 I 36 1

<yo Re~°\.'~l!'_f _ 1 o - 94 --- - ;TERPHENYL-D1·4-----~----i2 ·%Recovery 1 33 - 141

--


Run Sequence

X03194 XG.2003. 785.26

XG.2003. 785.26

X03189 XG.2003.750.15

XG.2003.750.15

Page 5 of 10

CAS# Analyte Result

8081

-- --------+· -(DCB) Decaciliorobiphenyl #2 !

- (TCMX) Teirachloro-m-xylene #2 I 51

75

SQLCoyote: Reports

Units

· % Recovery 1

. %Recovery i

1.0.0305281535XX

Range

50 - 150

50 - 150

X03189-021

. -NA -~I NA 1

05-07-03

05-07-03 ----------- _l



Dilution

Factor

X03206-020 05-07-03

05-07-03

Detection Run

Limit Code Date

X03165-025

; =--NA-[-=-= NA _i_ 1

-----~- --- . -- ----1 NA -- I NA

NA

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03



X03194-011 r - NA -----r- -- ·1 +-----~--- -, NA i --~--------·-· J

NA

NA

X03189-011

05-09-03

05-09-03

05-07-03

05-07-03

Report Date 6119103 9:26:56 AM

STAN DARE' Assaigai Analytical Laboratories, Inc.


Client:

Project:



-------------- -------


D -I -Not applicable-due to sample dilution

1...-i--Not applicable due to MDL proximity Order: 0304504 PHl16

Sample: 0304504-0BA Matrix: WATER

Run Sequence

X03206 XG.2003.800.5

XG.2003.800.5

CAS# Analyte

524

1,2-0ichlorobenzene-d4 (SS)


Result Units Range



05-07-0<

05-07-03-

-- ----------~--·----------------

Sample: 0304504-0BC Matrix: WATER

Run Sequence

X03165 XG.2003.703.25

XG.2003.703.25

XG.2003.703.25

XG.2003. 703.25

XG.2003.703.25

XG.2003.703.25



8270 X03165-026 ------~------------------------- --·----------

---+---·_2_,4_, 6_-T_R_l B_R_O_M_O_P_H_EN_O_L_l ____ 14 % Recovery 10- 123 ' 1 _NA - !, '

*2-FLUOROBIPHENYL 86 % Recovery 43 - 116 1 NA

-,--·--1 04-29-03• '\4,.·

04-29-03 -----------------r---------t-----+-----t------~-----+---t

*2-FLUOROPHENOL 10 % Recovery 21 - 100 1 NA 04-29-0~----------~------------+---------+------+-------+---- -··-------+-----+---_.j

*NITROBENZENE-05 84 i % Recovery 35 - 114 1 NA 04-29-03' -----+-------------!----··-- ------+------t----··---~------ "'

*PHENOL-06 18 I % Recovery 1

10 - 94 : 1 NA 04-29-03 · -----+------------------·--------+-----ti-- j-----+------j ____________ *_T_E_R_P_H_E_N_Y_L-_0_14 _______ _j ____________ 80 ___ ~0_Yo_R_e_c_o_ve_ry-+-__ 33 - 141_L_L__ NA ___ __J 04-29-0s


Run Sequence

X03194 XG.2003.929.22

CAS#

I

Analyte

8081

(TCMX) Tetrachloro-m-xylene #2 !



X03194-012

81 '

-~--1 % Recovery I --------------~-----

50 - 150 --- ---2-- __ N_A __ I ~ 06-03-os,

X03189 XG.2003.750.16

Sample: 0304504-09A

Run Sequence

X03206 XG.2003.800.6

XG.2003.800.6

CAS#

Sample: 0304504-10A

Run Sequence CAS#

8082 X03189-012 ~-(TCMX) Tetrachloro-m-xylene #2 r--- 86 1, % Recovery I 50 - 150-T~-----1-----[---NA~ o5-07-o<

-----------------Matrix: WATER



Matrix: WATER



524 X03206-021 X03206 XG.2003.800.12

XG.2003.800.12 -- ----- -~ ·;~-~~;;~~r~::_zne_z:_:_-=-~-~-~-~-) ~ ___ :: =~ ~-tj~;~~ _;:-~ }}f=f +-=-~1-~---+-1-~ 05-07-03

05-07-03

Page 6 of 10 SQLCoyote: Reports 1_0_ 0305281535XX Report Date 6119103 9:28:07 AM'

STANDARD



Client:

Project:



D Not applicable due to sample dilution Order: - --~--- -~-----------

L Not applicable due to MDL proximity 0304504 PHl16


Run Sequence

X03165 XG.2003.703.26

XG.2003.703.26

XG.2003.703.26

XG.2003.703.26

XG.2003.703.26

XG.2003.703.26

------ -------

CAS# Analyte

8270

*2,4,6-TRIBROMOPHENOL

*2-FLUOROBIPHENYL

*2-FLUOROPHENOL -- --~-------------

-- ! ___ *Nl!~<?BENZENE-05 T *PHENOL-06

-t- *TERPHENYL-014

Result

------

Units Range

Dilution

Factor

Detection

Limit

Run

Code Date

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03

04-29-03


Run Sequence

X03194 XG.2003.785.28

X03189 XG.2003.750.17

Sample: LCS

Run Sequence

X03206

XG.2003.800.4

XG.2003.800.4

X03206 XG.2003.817.3

XG.2003.817.3

X03206 XG.2003.814.20

XG.2003.814.20

X03194 XG.2003.785.13

X03189 XG.2003. 750.4

X03165

XG.2003.622.2

XG.2003.622.2

XG.2003.622.2

XG.2003.622.2

XG.2003.622.2

XG.2003.622.2

Page 7 of 10



8081 X03194-013

i (TCMX) Tetrachloro-m-xylene #2 I 84 ------~--- ~---

_ % R:c;overy l ~9--_~o_T=--=~=-::T==~A -~r---=:] o5-09-03

8082 X03189-013

--=-JJi'cM~!~!_r;:i_chloro-m-xylene #2 ]_ __ ------~~-==~ _ _:__ 1- 0/o-Re-c~very [ _ 50---i-so 1_ -- J_ - -t-.1~---- J 05-07-03

--------------- --- -

Matrix: WATER



524 X03206-013

----~-~:--~f~~~~0B~~=~:-+---+=~--r ~; =-, -J - - - I 1,2-Dichlorobenzene-d4 (SS) 103

---=-l~_ci_rri~f~~orobenze-ne (SS--) --r-L-__ ---104

05-07-03

05-07-03

524 X03206-025

1,2--0ichlorobenzene-d4 (SS)

__ ::_:-I Bromof~~robenzene (SS)

128

122 _____ pxR:ecaverY-f-75:_:-~1~

1 ---T---T----~1:'=1=-_J 05-07-03

% Recovery 1

75 - 125 j 1 · NA 1 05-07-03

524 -u~-- r 1,2-0ichlorobenzene-d4 (SS)


8081

X03206-031 - -----~--l 115 1 % Recovery __ 7_6---1141-- 1 -- -J --NA --l--J

1 ·---1-1-2----+I- -- - --j-------+-----f----

- __ 1°10 Recovery 75 --~ _ 1 _ ---~~- __ ~-----

X03194-002

[ ~-==-J(TCMX) Tetrachloro-m-~~le_n_e_#_2~[ ____ 7 __ 3 ___ [°/o~e_c;ov_e_ry~[_5_0_- ~=~ __ _J--- NA

8082 X03189-002

05-07-03

05-07-03

05-08-03

-~_==1:(TC!Jl~)_ Tetrachloro-m-xylene #2 NA 05-06-03

8270

*2,4,6-TRIBROMO_P_H_E_N_O_L_-t--___ 84 _iJ>_Recovery _10-_ 123 *2-FLUOROBIPHENYL 84 i % Recovery 43 - 116

---j----------------

*2-FLUOROPHENOL 48 % Recovery 21 - 100

_ -L---.:!'J_'.TR<?BENZENE-05 *PHENOL-06

79 _ _ __ j_"/o Recovery

--=-- -~----+~ ~-!~~~;;J-*TERPHENYL-014 - --------1

- --- J

SQLCoyote: Reporls 1.0.0305281535)()(

X03165-002

! NA ! l . -NA - I ) ____________ - ·<---~-

NA J-_J ~~+--

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

Reporl Date 6119103 9:29:10 AM

Client:

Project:

Order:



0304504 PHl16



STAN DAR['

··------------ ----------


· -C>l-/Voi applicable due to sample dilution -.! [ Cl Not applicable_ci~'!_tO_ MDL E_'3_Xim_ity__"._

Sample: LCSD Matrix: WATER

Run Sequence

X03194 XG.2003.785.14

X03189 XG.2003. 750.5

X03165 XG.2003.622.3

XG.2003.622.3

XG.2003.622.3

XG.2003.622.3

XG.2003.622.3

XG.2003.622.3

-·

Sample: MB

Run Sequence

X03206 XG.2003.800.3

XG.2003.800.3

X03206 XG.2003.817.1

XG.2003.817.1

X03206 XG.2003.814.19

XG.2003.814.19

X03194 XG.2003.785.12

X03194 XG.2003. 785.25

X03194 XG.2003.807.8

X03194 XG.2003.807.7

XG.2003.807.7

X03189 XG.2003.750.3

X03189

XG.2003.750.18

XG.2003.750.18

Page 8 of 10



8081

=-~ l rr_c_~~_)_!et~~cll_l~~m-xylen~ 8082

79

X03189-003

NA I _J ----- ---- ----~-

% Recovery- -50- 150~--1 ---- - ---- __l__ ______ -- -- - - '----- --- --

(TCMX) Tetrachloro-m-xylene #2 j __ _ 84

8270 X03165-003 ---T-*2,4,6-TRIBROMOPHENOL I 91 ·: 0/~Recoveryr-10-=- 1231____ 1 NA

.. --L *2-FLUOROBIPHENYL r-==. ==~·c ·---%Recoveryl -43_-~-1·1~ H =I~=~ ~ NA __ --+---·-

..... ___ + _ *2-FLUOROPHENOL ______ i 48 : % Recovery • 21 ~- 100 __ L __ _1_ ___ ( NA *NITROBENZENE-D5 82 I % Recovery 35 - 114 · 1 ! NA

*PHENOL-D6 -·35··--- % Recovery i 10 - 94 -- ----T-- t NA : - - -:

- - - ~-- ___ _:!_ERPHENYL-D14 62 % Rerov~l 33 - 141 _l ___ rn1 .... t~=NA~=± i

05-06-0::.

04-10-03·

04-10-03

04-10-0:'>,

04-10-03

04-10-03

04-10-03 •.

--------------·- ---·--- ------------- ··-- -· ----- ---·--·-----'

Matrix: WATER



524 X03206-012

05-07-03

05-07-02 : ~-:f;~~:t~ F ~E--~~;~-- ---------~~ --f ---1

----------

·• 1

··· 1,2-Dichlorobenzene-d4 (SS) 90 ----------·--· -

! Bromofluorobenzene (SS) 86

524 X 03206-023

____ +-__ NA·--=~------- o5-o7-o3

j NA i 05-07-03•

=r--1.2-DiC:t1iOr:ober1Ze_n_e.:ci4 (ss)· L __l__ Bromofluorobenzene (S~l__ __ j

-~ -----------------------,------- --1-

93 : % Recovery I 76 - 114±· .. 94 · % Recovery 75 - 125

524 X03206-030 ·- - ----1--1 ,-2--D-i-ch_l_o_r_o_b_en_z_e_n_e--d-4_(_S_S_) _____ 8_1 ___ =~-~~c~~~ ]~~ 76 ~- _1_ 1 __ 4_ -+----- NA 05-07-02

Bromofluorobenzene (SS) 84 1 % Recovery ! 75 - 125 05-07-03

8081 X03194-001

___ -_· -(_T=C=M=X~)_T_-e_l_ra_c_ii-_1o_ro_~--m __ ~ic_-Y_1e_-n_e_#_2_--·_,-._--_--_··· ___ 76 ___ _J_ % ~~covery 5_o=~~-L~--~=-T=BE----~-~ 05-08-03•

8081 X03194-014

78 .. - NA==-- --, 05-09-02

8081

! (TCMX) Tetrachloro-m-xylene L ___ _ 72 ; % Recovery I __ 5~ - 150_]~-----X03194-026

-~--~=-] 05-19-03.

8081

(DCB) Decachlorobiphenyl

.. 1

(TCMX) Tetrachloro-m-xylene

8082

71 ! % Recovery: 50 - 150 , 77-----+1-%-R-ecovery : . 50 - 150

X03194-028 1 ~I _N_A_---r ____ l ! __ =L_~~ --~

X03189-001

1----}JTCMX) Tetrachloro-m-xylene_#_2~1 ____ 8_4_ _L"lo__R_e_co_v_e~~5o-~--1~0 I~~ 1. --~-_f'J~ _L=====I

8082

(DCB) Decachlorob1phenyl #2 1 38

----" <.f~~X) Tetrachloro-m-xylene #21 ____ 86 __

05-19-03'

05-19-0::

05-06-03

05-07-03

05-07-0~

SQLCoyote: Reporls 1.0.0305281535XX Reporl Date 6119103 9:30:12 AM···

STANDARD



Client:

Project:


APruL03SAMPLEEVENT D

L

Explanation of codes --- --- -----------------

Not applicable due to sample dilution Order:

- -- --------------------

Not applicable due to MDL proximity 0304504 PHl16

Sample: MB

Run Sequence

X03189 XG.2003. 798.4

XG.2003.798.4

X03165 XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

XG.2003.622.1

X03165 XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

XG.2003.696.6

X03165 XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

XG.2003.679.4

X03165 XG.2003. 703.11

XG.2003. 703.11

XG.2003. 703.11

XG.2003. 703.11

XG.2003. 703.11

XG.2003. 703.11

Sample: MS

Run Sequence

X03194 XG.2003.785.16

XG.2003.785.16

X03189 XG.2003.750.8

XG.2003.750.8

Page 9 of 10

Matrix: WATER



8082

--=- +~~~~~ -~:~:~~:::~:::~:~:!2 J

X03189-027

53 __ __i!o Recovery I 5-o=-150T1- - : NA--B 103 ; % Recovery ! --~~ ~ _ 150_] _i_=-:.T _ N~- ~- --

8270 X03165-001 - - -------- ---- -- ------ ------ ----- r -*2,4,6-TRIBROMOPHENOL 83 % Recovery+ 10 - 123 NA

*2-FLUOROBIPHENYL ______ -=SI:- Tio Recov~I)'-'-- - 43 - 116 -+-------- NA *2-FLUOROPHENOL 50 % Recovery 21 - 100 NA

-------------+-- -- - ----+:- - ·-·-----+--··--------~

*NITROBENZENE-05 79 1 % Recovery 35 - 114 NA ------+----------- ----------- -L

*PHENOL-06 37 1 % Recovery 1 O - 94 NA ·- -------- --~--- . - - -·---- -- - -·-·---·-- ___ _,

*TERPHENYL-D14

8270 -------------------

*2,4,6-TRIBROMOPHENOL -------------------------+-

' -----i-----

-----+____ j_ _J_

8270

*2-FLUOROBIPHENYL

*2-FLUOROPHENOL

*NITROBENZENE-05

*PHENOL-06

*TERPHENYL-014

I r *2,4,6-TRIBROMOPHENOL ! - -----

*2-FLUOROBIPHENYL

80 : % Recovery NA

X03165-008

78 i % Recovery 10 - 123 NA -- 92 ____ j _% Recovery 43- 116 NA

53 --fo/o Recovery 21 - 1 00

__ _:_a-r:~_:_l07o_Recove_ryj 35 - 1_14 ______ _

NA __ [

NA

41 : % Recovery I 10 - 94 --- --+-- _____ t ___ _

57 % Recovery I 33 - 141

NA

NA

X03165-011

91 % Recovery -43 - 116 - - - 1 ----- NA 92 - - -o/o Recovery--1 o --12311 - -,---NA -

*2-FLUOROPHENOL --46 --i % Recovery j 21 - 100-- --1- N-A-------~---_,

... *f'Jl!~OB~~-~f'J-~~5 __ _, ____ 82_____ j % ~9o_v_~r+~-=-~ - - 1 , ___ NA-~---~

--------!-------------

_l *TE·-:-~-~-~-~-y_L--~-~-1-4----+----~~---- ---1 ~::~:~:~I ;3o_- 19441 t --~--=-_L_ _~;H---~====

8270 X03165-013

05-15-03

05-15-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-10-03

04-22-03

04-22-03

04-22-03

04-22-03

04-22-03

04-22-03

04-26-03

04-26-03

04-26-03

04-26-03

04-26-03

04-26-03

·2:4~6-=fRi"El_R_O_M_O_P_H_E_N_O_L _____ 8_8___ -r% Recovery --~~ --1_23 -r-. -·__ ------N-;;..--------~ 04-29-03

-----~----.-2-_F_L_U_O_R_O_B_l_P_H_E_N_Y_L __ +---- 83 I% Recovery 43 - 116 : NA --1 04-29-03 ------------------+---------f-----+-----~--------f----j

*2-FLUOROPHENOL 45 ! % Recovery 21 - 100 I NA I _ j 04-29-03

------==--.-N-l_T_R_O_B_E_N_Z_E_N_E ___ D_5--+------- 83 mJ_oio_~-e~ove_ry r 3§~=i_1_4 NA __ j ____ j 04-29-03

_ ·f;;-~E_H_~B~-~~14 !-- ~--~=~;-~-_--~~;_:_:~~~~~-j 313°-- 1

9441 ~~ j ______ : ~::~::~~ - j

... I

Matrix:

CAS# Analyte Result

8081

- -------- ---- -

WATER

Units Range

Dilution

Factor

--- --- ---(DC-B)DeC8ChlorobfJ)h-9nY1#2--!---37 ________ - I o/o Recovery 50 - 1-50

---(l"C::_lll1Xl_Tetrach1o!_:>~ri:i_-xy1e_ne #21 _______ so_ _____ ! 0;Fi~~eryl5o-1-56

- -

2

2

8082 ----- -- (DCB) Decachlorobiphenyl #2- T

- - -==:iTCMX) Tetrachloro-m-xylene #2 I

7 4 - --- --1% Recover~T-so - 150 2 85 -- - --1 o/:-Recovery -so-:: ·:iso 2

I - --- ------------

Detection

Limit

Run

Code Date

X03194-005

NA

NA

05-08-03

05-08-03

X03189-006 - -NA _f ___ i 05-06-03

-·===-NA:~-:_]_____ 05-06-03


STANDARD



---- -"----- ---·-------Client:

Project:


APmL03SAMPLEEVENT Explanation of codes

D Not applicable due to sample dilution i

L_ rNo_! f1PP1icable du_e to MDL proximity_: Order: 0304504 PHl16

--·---·--··--------- ----·-------·--··--·--··----

Sample: MS

Run Sequence CAS#

Matrix:

Analyte Result

WATER ---------··--- -------------- -

Units Range

Dilution

Factor

Detection

Limit

Run

Code Date

8270 X03165-005 X03165 XG.2003.622.5

XG.2003.622.5

XG.2003.622.5

X G. 2003. 622. 5

XG.2003.622.5

XG.2003.622.5

iu I ·2~;~~~~:i:~:::~LOL t----:~ . . ! ~ :::::~ i :: : ::! j- : + ~~ _ -. : _ ~;~~~~~~:~~~~ :---- ::--4::::;.~ ~::::~-~~-- r- ~f-1~ -._

04-10-03''

04-10-03

04-10-03'

04-10-03.

·-- - · *PHENOL-06 ---r---~-- - I %Reoo"~ I 1o · 941-2-·- - NA .

--1 *TERPHENYL-014 : 74 · ·. % Recovery, 33 - 14T . · --2-- ··-l· --~ __________ J ___________ ---------- ---------~------- ------·------ ---------------

,, 04-10-03.

04-10-03··

--- ---- -------··-- ------------·--·-----Sample: MSD

Run Sequence

X03194 XG.2003. 785.17

X03189 XG.2003.750.9

XG.2003.750.9

X03165 XG.2003.622.6

XG.2003.622.6

XG.2003.622.6

XG.2003.622.6

XG.2003.622.6

XG.2003.622.6

Page 10 of 10

I

Matrix: WATER



8081 X03194-006

_ ~_(TCMX)_Tet~chloro-m-xylene #2 I __ . 77 ~-- L~ Reco~ery' 50 -- 15~-}__~ - - [ ____ NA--=~ 05-08-03'

8082 X03189-007

--- -i=:;:(DCB) Decachlorobipheny~i___- 71- _ I 0/o Recov_ery-[ 5_0- -15~ ___3 __ --,--- ~~. -1- I

- J (TCMX) Tetrachloro-m-xyle~------7_8__ ~Recovery~-- 1~- _2__ NA~--

8270 X03165-006

·2,4,6-TR1sR0MoPHENOL go 1 % Recovery 1-1 o - 123 I --2~-NA+- ~ -+--- *2-FLUOROBIPHENYL __!l<l___ % Recov~~' _2__ f NA _ i *2-FLUOROPHENOL 40 : % Recovery. 21 - 100 ____ 2 __ ---~-+----

-- l ·::·-~-O-~B-~_£_t __ ~~-~-~-~_:_5

_~/ __ -· __ ~~ J;:::~ ~ .. •~ : i ~~1==--

05-06-03,.

05-06-03

04-10-03.

04-10-03.

04-10-03

04-10-03

04-10-0:;.

04-10-03

SQLCoyote: Reports 1.0.0305281535)()( Report Date 6119103 9:31:24 AM· ..

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(505) 662-2558

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ASSAIGAI ANALYTICAL LABORATORIES, INC.

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ASSAIGAI PROJECT FILE


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127 EASTGATE DRIVE, 212·C LOS ALAMOS, NEW MEXICO 87544

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Special Instructions:--------------




u Stored over 30 days (additional fee)


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