summary report river falls, wi, 54022 507 highland drive

Street Address:Office:

Contract Pharmacal CorpHauppauge, NY135 Adams Avenue

Hauppauge, New York, 11788City, State, Zip:

Phone:

Customer

Summary Report

Report No.:514644

507 Highland Drive

Phone: (715) 426-0246Fax: (715) 426-0251

River Falls, WI, 54022

www.eurofinsus.com/biodiagnostics

05/15/201907/19/201907/19/2019

Date Completed:Date Received:

Date Reported:

ULEVA-Flex Capsules

5446A

R12712

119078374BDI Sample Number:Sample Description:

Serving Size:SKU#: Product#:Lot:

Batch#:

UPC#:

PassSample Summary:

Test Requested Results Criteria Pass/Fail Comments

10 mg/capsule10.58 mg/capsuleCannabinoids (SC0G7) SUSRF01-HPLC

Pass

<1x10^5 CFU/g<10 CFU/gAerobic Plate Count (UMPRE) SUSGA02-Interco

Pass

All <Action LimitsAll <Action Limits Action Limits available upon requestHeavy Metals (Big4-ICP-QQQ) SUSBO02-Interco

Pass

ABSENTNot Detected per 25gListeria (UM7TC) SUSGA02-Interco

Pass

All <Action LimitsAll <Action Limits Action Limits available upon requestResidual Pesticides (PEST_HEMP) COVA-Interco

Pass

All <Action LimitsAll <Action Limits Action Limits available upon requestResidual Solvents (Acids Only) (USPR_ACD_S) COVA-Interco

Pass

All <Action LimitsAll <Action Limits Action Limits available upon requestResidual Solvents (Non Volatile) (USPR_DIN_S) COVA-Interco

Pass

ABSENTNot Detected per 25gSalmonella (UMN6C) SUSGA02-Interco

Pass

<1x10^4 CFU/g<10 CFU/gYeast and mold (UMN2K) SUSGA02-Interco

Pass

ABSENT<10 CFU/gE. Coli (UM73J) SUSGA02-Interco Pass

10 mg/capsule11.18 mg/capsuleCannabinoids Second Analysis (SC0G7) SUSRF01-HPLC

Pass

Report Comment: Subsequent original reports to the summary report are independently paginated as received from the testing laboratory.Pass/Fail criteria are defined by the CVS Health Transparency program with specification limits based on FDA guidelines for dietary supplements products.

1 of 1 -

Eurofins BioDiagnostics, Inc.EBDI.13231 Rev.01292019Summary Report

Emily StressmanAssistant Sales and Project Manager

Eurofins BioDiagnostics, Inc. warrants that it uses due care when performing tests for its customers. However, testing results are only reflective of the sample submitted by the customer. Eurofins BioDiagnostics, Inc. does not warrant the sample is representative of the lot from which the sample is drawn. Except for the testing services provided, Eurofins BioDiagnostics, Inc. makes no warranties or guarantees of any kind, expressed or implied, with respect to the services rendered.

Thank you for your business !

CERTIFICATE OF ANALYSIS

BioDiagnostics, Inc. Attn: QC Dept.507 Highland DriveRiver Falls, WI 54022

05/21/201905/16/2019

QR0000282AR-19-QR-009720-01

Report Date:Entry Date:

PO Number: Hemp INTERCO

Client Code:Batch Code: EUUSGA2-00028715

Eurofins Microbiology Laboratories (Garden Grove)

11390 Knott Ave Garden Grove, CA 92841, US

www.eurofinsus.comTel:+1 714 892 0208

Eurofins Sample Code: 111-2019-05160034Client Sample Code: 119078374Analysis Date: 5/16/2019

Sample Description: Flex CapsulesCondition Upon Receipt: Acceptable

Test ResultUMPRE - Aerobic Plate Count - AOAC 966.23

Method Reference: AOAC 966.23Aerobic Plate Count < 10 cfu/g*

UMN2K - Yeast - BAM Chapter 18

Method Reference: FDA BAM Chapter 18Yeast < 10 cfu/g*Moulds < 10 cfu/g*

UM73J - Total Coliforms - AOAC 991.14

Method Reference: AOAC 991.14Coliforms < 10 cfu/g*Escherichia coli < 10 cfu/g*

UMN6C - Salmonella spp. - AOAC 2004.03

Method Reference: AOAC 2004.03Salmonella Not Detected per 25 g

UM7TC - Listeria spp. - AOAC 2004.06

Method Reference: AOAC 2004.06Listeria Species Not Detected per 25 g

*The test result is covered by our current A2LA accreditation.

Page 1 of 2 Analytical report: AR-19-QR-009720-01

CERTIFICATE OF ANALYSIS

BioDiagnostics, Inc. Attn: QC Dept.507 Highland DriveRiver Falls, WI 54022

05/21/201905/16/2019

QR0000282AR-19-QR-009720-01

Report Date:Entry Date:

PO Number: Hemp INTERCO

Client Code:Batch Code: EUUSGA2-00028715

Eurofins Microbiology Laboratories (Garden Grove)

11390 Knott Ave Garden Grove, CA 92841, US

www.eurofinsus.comTel:+1 714 892 0208

Viridiana CastroMicrobiology Supervisor

Respectfully Submitted,Eurofins Scientific, Inc.

All work done in accordance with the Eurofins General Terms and Conditions of Sale.

Full text at: www.eurofinsus.com/Terms_and_Conditions.pdf

Results shown in this report relate solely to the item submitted for analysis.All results are reported on an "As Received" basis unless otherwise stated.Reports shall not be reproduced except in full without written permission of Eurofins Scientific, Inc.Measurement of Uncertainity may be obtained upon request. Retained samples are discarded 30 days after receipt; certain exceptions apply.

Testing Cert #3329.05

Page 2 of 2 Analytical report: AR-19-QR-009720-01

Certificate of Analysis

2502845-0Report Number:

Report Date: 21-May-2019

Report Status: Final

Eurofins BioDiagnostics, Inc.

Sample Name: Flex Capsules Eurofins Sample: 8458539

Project ID EUROFINS-20190516-0456

PO Number CVD

Sample Serving Size

Description 119078374

Receipt Date 16-May-2019

Receipt Condition Ambient temperature

16-May-2019Login Date

16-May-2019Date Started

Number Composited 10

Online Order 20

Analysis Result

Elements by ICP Mass Spectrometry

<10.0 ppbArsenic

<5.00 ppbCadmium

20.4 ppbLead

<5.00 ppbMercury

Method References Testing Location

Food Integrity Innovation-MadisonElements by ICP Mass Spectrometry (ICP_MS_S)

Official Methods of Analysis, Method 2011.19 and 993.14, AOAC INTERNATIONAL, (Modified).

Pequette, L.H., Szabo, A., Thompson, J.J., "Simultaneous Determination of Chromium, Selenium, and Molybdenum in

Nutritional Products by Inductively Coupled Plasma/Mass Spectrometry: Single-Laboratory Validation," Journal of AOAC

International, 94(4): 1240 - 1252 (2011).

Testing Location(s) Released on Behalf of Eurofins by

Edward Ladwig - DirectorFood Integrity Innovation-Madison

Eurofins Food Chemistry Testing US, Inc.

3301 Kinsman Blvd

Madison WI 53704

800-675-8375

2918.01

These results apply only to the items tested. This certificate of analysis shall not be reproduced, except in its entirety, without the

written approval of Eurofins.

Page 1 of 121-May-2019 5:12 pmPrinted:








PO Number CVD

Sample Serving Size







Online Order 20

Analysis LimitLOQ Result Pass/Fail

Residual Solvents - Class 2 Mix C, Class 3 DMSO (Nonvolatile Solvents)

<50.0 ppm50 ppm Pass50 ppm2-Methoxyethanol

<160 ppm160 ppm Pass160 ppm2-Ethoxyethanol

<880 ppm880 ppm Pass880 ppmN,N-Dimethylformamide

<1090 ppm1090 ppm Pass1090 ppmN,N-Dimethylacetamide

<250 ppm250 ppm Pass250 ppmDimethyl Sulfoxide

<620 ppm620 ppm Pass620 ppmEthylene Glycol

<530 ppm530 ppm Pass530 ppmN-Methylpyrrolidone

<220 ppm220 ppm Pass220 ppmFormamide

<160 ppm160 ppm Pass160 ppmSulfolane


Food Integrity Innovation-MadisonResidual Solvents - Class 2 Mix C, Class 3 DMSO (Nonvolatile Solvents) (

USPR_DI_S)

United States Pharmacopeia, 39th Rev. - National Formulary 34th Ed., Method <467>, USP Convention, Inc., Rockville, MD (

2016). (Modified).




3301 Kinsman Blvd

Madison WI 53704

800-675-8375



Page 1 of 120-May-2019 9:41 amPrinted:








PO Number CVD

Sample Serving Size







Online Order 20

Analysis Result

Residual Solvents - Class 3, Acids Only

446 ppmAcetic AcidAcetic Acid

<200 ppmFormic AcidFormic Acid


Food Integrity Innovation-MadisonResidual Solvents - Class 3, Acids Only (USPR_ACD_S)

[1] United States Pharmacopeia, 39th Rev. - National Formulary 34th Ed., Method <467>, USP Convention, Inc., Rockville, MD

(2015). (Modified)

[2] Zhou, D., Hou, Q., Liu, W., Ren, X., "Rapid determination of formic and acetic acids in biomass hydrosylate by headspace

gas chromatography," Journal of Industrial and Engineering Chemistry, 47:281-287 (2017).




3301 Kinsman Blvd

Madison WI 53704

800-675-8375











PO Number CVD

Sample Serving Size







Online Order 20

Analysis Result

Multi-Residue Analysis for hemp products - 60+ compounds

Spices - Botanicals - and other

Specialty Samples

Matrix Type - To Determine Limit of Quantification (LOQ)

<0.05 mg/kgAbamectin

<0.05 mg/kgAldicarb

<0.05 mg/kgAldicarb sulfone (Aldoxycarb)

<0.05 mg/kgAldicarb sulfoxide

<0.05 mg/kgAzoxystrobin

<0.05 mg/kgBifenazate

<0.05 mg/kgBifenthrin

<0.05 mg/kgCarbaryl

<0.05 mg/kgCarbofuran

<0.05 mg/kgCarbofuran-3-hydroxy-

<0.05 mg/kgChlorantraniliprole

<0.05 mg/kgChlordane, cis-

<0.05 mg/kgChlordane, trans-

<0.05 mg/kgChlorfenapyr

<0.05 mg/kgChlorpyrifos

<0.05 mg/kgCoumaphos

<0.05 mg/kgCyfluthrin

<0.05 mg/kgCypermethrin

<0.05 mg/kgCyproconazole (2 diastereoisomers)

<0.05 mg/kgCyprodinil

<0.05 mg/kgDichlorvos

<0.05 mg/kgDiclobutrazol

<0.05 mg/kgDipropetryn

<0.05 mg/kgDisulfoton

<0.05 mg/kgEndosulfan I (alpha-isomer)

<0.05 mg/kgEndosulfan II (beta-isomer)

<0.05 mg/kgEndosulfan sulfate

<0.05 mg/kgEpoxiconazole

<0.05 mg/kgEthiofencarb

<0.05 mg/kgEtofenprox

<0.05 mg/kgEtoxazole









PO Number CVD

Sample Serving Size







Online Order 20

Analysis Result

Multi-Residue Analysis for hemp products - 60+ compounds

<0.05 mg/kgFenoxycarb

<0.05 mg/kgFenpropathrin

<0.05 mg/kgFenvalerate/Esfenvalerate (sum of isomers)

<0.05 mg/kgFipronil

<0.05 mg/kgFipronil desulfinyl

<0.05 mg/kgFipronil sulfone

<0.05 mg/kgImazalil

<0.05 mg/kgImidacloprid

<0.05 mg/kgMalathion

<0.05 mg/kgMethiocarb

<0.05 mg/kgMethiocarb sulfone

<0.05 mg/kgMethiocarb sulfoxide

<0.05 mg/kgMethomyl

<0.05 mg/kgMetolachlor

<0.05 mg/kgMevinphos (E- and Z-isomers)

<0.05 mg/kgMyclobutanil

<0.05 mg/kgNaled (Dibrom)

<0.05 mg/kgPaclobutrazol

<0.05 mg/kgPermethrin (sum of isomers)

<0.05 mg/kgPropoxur

<0.50 mg/kgPyrethrum (total)

<0.05 mg/kgSpinetoram (spinosyns J and L)

<0.05 mg/kgSpinosad (spinosyns A and D)

<0.05 mg/kgSpirodiclofen

<0.05 mg/kgSpiromesifen

<0.05 mg/kgSpiromesifen enol

<0.05 mg/kgSpirotetramat

<0.05 mg/kgSpiroxamine (2 diastereoisomers)

<0.05 mg/kgTebuconazole

<0.05 mg/kgThiabendazole

<0.05 mg/kgThiabendazole-5-hydroxy-

<0.05 mg/kgThiacloprid

<0.05 mg/kgTrifloxystrobin








Food Integ. Innovation-GreenfieldMulti-Residue Analysis for hemp products - 60+ compounds (PEST_HEMP)

Official Methods of Analysis, AOAC Official Method 2007.01, Pesticide Residues in Foods by Acetonitrile Extraction and

Partitioning with Magnesium Sulfate, AOAC INTERNATIONAL (modified).

CEN Standard Method EN 15662: Food of plant origin - Determination of pesticide residues using GC-MS and/or LC-MS/

MS following acetonitrile extraction/partitioning and clean-up by dispersive SPE - QuEChERS method.

List of the tested pesticides and their limits of quantification (LOQs) are available upon request.


Karelyn Koehn - ManagerFood Integ. Innovation-Greenfield


671 S. Meridian Road

Greenfield IN 46140

800-675-8375

2918.06




507 Highland Drive


Phone: (715) 426-0246

Fax: (715) 426-0251


Customer Name: Contract Pharmacal Corp Date Reported: 07/10/2019

Office: Hauppauge, NY Date Completed: 05/22/2019

Street Address: 135 Adams Avenue Date Received: 05/15/2019

City, State, Zip: Hauppauge, NY 11788 Testing Method: HPLC

Phone:

Cannabinoid Name ID Weight %Conc.

mg/g

Conc.

mg/mL

Sample No: 119078374-Rep 1 Cannabichromenic Acid CBCA ND ND

Crop: Hemp, Industrial Cannabicyclol CBL 0.005 0.05

Variety: ULEVA-Flex Capsules Cannabidiol CBD 1.261 12.61

Lot: R12712 Cannabidiolic Acid CBDA ND ND

Seed Size: Cannabidivarin CBDV 0.018 0.18

Customer Tracking#: Cannabidivarinic Acid CBDVA ND ND

Seeds Per Pound: Cannabigerol CBG 0.006 0.06

Batch: 5446A Cannabigerolic Acid CBGA ND ND

LIMS: Cannabichromene CBC 0.031 0.31

IL: Cannabinol CBN <LOQ <LOQ

Cannabinolic Acid CBNA ND ND

Comments: Δ9-Tetrahydrocannabinol Δ9-THC 0.014 0.14

Δ8-Tetrahydrocannabinol Δ8-THC ND ND

Tetrahydrocannabinolic Acid A THCA-A ND ND

Tetrahydrocannabivarin THCV ND ND

Tetrahydrocannabivarinic Acid THCVA ND ND

Total Cannabinoids 1.335 13.35

Total THC* 0.014 0.14


American Oil Chemists' Society (AOCS)

Sample Information

LOQ= 50ppm or 0.005 wt%

Eurofins BioDiagnostics, Inc. warrants that it uses due care when performing tests for its customers. However, testing results are only reflective of the sample submitted by the customer.

Eurofins BioDiagnostics, Inc. does not warrant the sample is representative of the seed lot from which the sample is drawn. Except for the testing services provided, Eurofins BioDiagnostics,

Inc. makes no warranties or guarantees of any kind, expressed or implied, with respect to the services rendered.

Joseph Zalusky

Approved Chemist, Gas Chromatography

*Total THC is calculated as the sum of Δ9-THC + Δ8-THC + (THCA-A * 0.877) + THCV + (THCV-A * 0.877).

Cannabinoid Analysis ReportPage 1 of 1 Eurofins BioDiagnostics, Inc.

507 Highland Drive


Phone: (715) 426-0246

Fax: (715) 426-0251


Customer Name: Contract Pharmacal Corp Date Reported: 07/10/2019

Office: Hauppauge, NY Date Completed: 06/28/2019

Street Address: 135 Adams Avenue Date Received: 05/15/2019

City, State, Zip: Hauppauge, NY 11788 Testing Method: HPLC

Phone:

Cannabinoid Name ID Weight %Conc.

mg/g

Conc.

mg/mL

Sample No: 119078374-Rep 2 Cannabichromenic Acid CBCA ND ND

Crop: Hemp, Industrial Cannabicyclol CBL 0.006 0.06

Variety: ULEVA-Flex Capsules Cannabidiol CBD 1.333 13.33

Lot: R12712 Cannabidiolic Acid CBDA ND ND

Seed Size: Cannabidivarin CBDV 0.018 0.18

Customer Tracking#: Cannabidivarinic Acid CBDVA ND ND

Seeds Per Pound: Cannabigerol CBG 0.007 0.07

Batch: 5446A Cannabigerolic Acid CBGA ND ND

LIMS: Cannabichromene CBC 0.033 0.33

IL: Cannabinol CBN <LOQ <LOQ

Cannabinolic Acid CBNA ND ND

Comments: Δ9-Tetrahydrocannabinol Δ9-THC 0.012 0.12

Δ8-Tetrahydrocannabinol Δ8-THC ND ND

Tetrahydrocannabinolic Acid A THCA-A ND ND

Tetrahydrocannabivarin THCV ND ND

Tetrahydrocannabivarinic Acid THCVA ND ND

Total Cannabinoids 1.409 14.09

Total THC* 0.012 0.12


American Oil Chemists' Society (AOCS)

Sample Information

ATR-Add Cannabinoid 2nd Analysis per LB. (6/28/19)MD;

LOQ= 50ppm or 0.005 wt %

Eurofins BioDiagnostics, Inc. warrants that it uses due care when performing tests for its customers. However, testing results are only reflective of the sample submitted by the customer.

Eurofins BioDiagnostics, Inc. does not warrant the sample is representative of the seed lot from which the sample is drawn. Except for the testing services provided, Eurofins BioDiagnostics,

Inc. makes no warranties or guarantees of any kind, expressed or implied, with respect to the services rendered.

Joseph Zalusky

Approved Chemist, Gas Chromatography

*Total THC is calculated as the sum of Δ9-THC + Δ8-THC + (THCA-A * 0.877) + THCV + (THCV-A * 0.877).

Cannabinoid Analysis ReportPage 1 of 1 Eurofins BioDiagnostics, Inc.

summary report river falls, wi, 54022 507 highland drive

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