technical program of the 41th north american thermal … · 2016. 6. 29. · yoshida (tokyo...

Technical Program of the 41th

NORTH AMERICAN

THERMAL ANALYSIS SOCIETY CONFERENCE

August 4-7, 2013

Holiday Inn University Plaza Bowling Green, Kentucky

Program at a Glance Sunday, August 4, 2013

15:00–21:00 Registration

17:00–21:00 Opening Reception, General/Student Poster Sessions, Exhibition (Events Center/Exhibits)

Ballroom C/D

Monday, August 5, 2013

8:00–8:05 Greetings

8:05–8:50 Plenary Lecture (NATAS Award for Outstanding Achievement): Thermal Analysis of Fibrous Proteins by Prof. Peggy Cebe (Tufts

University) Ballroom C/D

8:50–9:00 Travel Break

Room MTG Room #5 Salon B MTG Room #2 MTG Room #1

9:00–12:00 Energetics

Coffee Break 10:40–11:00

Advances in Instrumentation and

Methods


Polymers, Nanocomposites, and Glasses: Thermal and Rheological Behavior


Honorary Symposium Prof. Dr. Ozawa/Dr. Flynn

Kinetic Phenomena in Practical Process


12:00–13:10 Lunch

Ballroom C/D 13:10–13:20 Travel Break

13:20–16:20 Energetics

Coffee Break 15:00-15:20

Biomaterials and Bio-inspired Materials


Polymers, Nancomposites, and Glasses: Thermal and Rheological Behavior


Honorary Symposium Professor Dr. Ozawa/Dr. Flynn Kinetic Phenomena in

Practical Process


Tuesday, August 6, 2013


8:05–8:50

Plenary Lecture: Crude oil, Tobacco, Polymers, Coffee and Soot: Analysis of complex materials by Thermal Analysis - Photoionisation Mass Spectrometry by Prof. Ralf Zimmermann (Joint Mass Spectrometry Centre, University of Rostock and Helmholtz Zenthrum Munchen,

Germany) Ballroom C/D



9:00–12:20

Development of Oxygen Carrier for Chemical Looping Combustion


Polymer and Organic Materials Degradation


Honorary Symposium Professor Wunderlich Thermodynamics, Liquid Crystal, Crystallization


Honorary Symposium Professor Dr. Ozawa/Dr. Flynn Kinetic Phenomena in

Practical Process


12:20–13:30 Lunch Break


13:40–18:00 Thermophysical Properties

of Materials


Polymer and Organic Materials Degradation




Simultaneous and Combined Techniques


18:00–18:30 Business Meeting

19:00–19:30 Reception – WKU Center for Research & Development

19:30–21:30 Banquet – WKU Center for Research & Development

Wednesday, August 7, 2013


8:05–8:45 Plenary Lecture: Dispersion and Transportation of Radioactive Nuclear in Environments -Fukushima and Tokyo by Prof. Hirohisa

Yoshida (Tokyo Metropolitan University, Japan) Ballroom C/D


9:00–12:00 Environmental Technology

and Green Chemistry Coffee Break 10:20–10:40

Standardization and Databases


General



Food Pharmaceutical


Inorganic Materials

End of Conference

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Table of Contents Program at a Glance ......................................................................................................... inside front cover Table of Contents .........................................................................................................................................2 President’s Message .....................................................................................................................................3 2013 NATAS Session Organizers ...............................................................................................................4 2013 NATAS Conference Exhibitors ..........................................................................................................5 2013 NATAS Award Winners .....................................................................................................................6 Previous Award Winners .............................................................................................................................7 2013 NATAS Conference Sponsors ............................................................................................................8 2013 NATAS Officers & Councilors ..........................................................................................................9 2013 NATAS Committee Chairs ...............................................................................................................10 2013 NATAS Conference Committee .......................................................................................................11 NATAS Regional Sections ........................................................................................................................12 NATAS-Mettler Outstanding Achievement Award Lecture .....................................................................13 41st NATAS Meeting Technical Program ..................................................................................................17 Author Index .............................................................................................................................................40 Map of Meeting Rooms ................................................................................................... outside back cover

© North American Thermal Analysis Society. All rights reserved. Individual authors may reproduce their contribution for personal or company use. Additional copies of NATAS 2011 conference abstracts and papers can be obtained by contacting: NATAS c/o Thermal Analysis Laboratory, Western Kentucky University, The Center for Research and Development, 2413 Nashville Road, Bowling Green, KY 42101. Phone: 270-745-2220, Fax: 270-745-2221, Email: [email protected].

Printed by X-CD Technologies, Toronto, Ontario, Canada, www.x-cd.com Cover photo credit: Coldwell Banker (www.coldwellbankerbg.com)

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4

2013 NATAS Session Organizers Advances in Instrumentation and Methods (AIM)

Dr. Takahisa Tsugoshi (AIST, Japan)

Biomaterials/ Bio-Inspired Materials (Bio) Prof. Peggy Cebe (Tufts University) Prof. Xiao Hu (Rowan University)

Dr. Ozawa/Dr. Flynn in Memoriam: Kinetic Phenomena in Practical Process (Kin)

Prof. Sergey Vyazovskin (University of Alabama-Birmingham) Prof. Nobuyoshi Koga (Hiroshima University, Japan)

Energetics (Nrg) Dr. Atsumi Miyake (Yokohama National University) Mr. Wim de Klerk (TNO-Defense, Security and Safety)

Environmental Technology and Green Chemistry (Env)

Prof. Yuko Nishimoto (Kanagawa University, Japan)

Food and Pharmaceutical (FnP) Prof. Etsuo Yonemochi (Hoshi University)

General (Gen) Dr. Madhavi Vadlamudi (Exxon Mobil Research and Engineering)

General Poster (GP) Prof. Chi-Min Shu (National Yunlin University, Taiwan)

Inorganic Materials (IoM) Prof. Li-Xian Sun (Dalian Institute)

Polymer and Organic Materials Degradation (Deg)

Prof. Bob Howell (University of Central Michigan) Prof. Dr. Crisan Popescu (DWI at the RWTH University of Aachen)

Polymers, Nanocomposites, and Glasses: Thermal and Rheological Behavior (PNG)

Prof. Sindee Simon (Texas Tech University) Dr. Yung Koh (Texas Tech University)

Prof. Bernhard Wunderlich in Memoriam: Thermodynamics, Liquid Crystal, Crystallization (BW)

Prof. Christopher Li (Drexel University) Prof. Stephen Cheng (University of Akron)

Simultaneous and Combined Techniques (SCT)

Prof. Andrew McGhie (University of Pennsylvania) Prof. Ralf Zimmermann (University of Rostock and Helmholtz Zentrum München) Dr. Tadashi Arii (Rigaku Corporation)

Standardization and Data Bases (Std) Dr. Haruka Abe (AIST Japan)

Student Poster (SP)

Thermophysical Properties of Materials (TPM)

Dr. Satoshi Endo (ULVAC-RIKO, Inc.) Prof. Junko Morikawa (Tokyo Institute of Technology)

Workshop on the Development of Oxygen Carrier for Chemical Looping Combustion using Thermal Analysis (Oxy)

Dr. Song Sit (Cenovus) Prof. Yan Cao (Western Kentucky University)

5

2013 NATAS Conference Exhibitors

Airgas, Inc. 3000 Industrial Drive Bowling Green, KY 42101-4068 270-842-9486 [email protected] www.airgas.com

AKTS AG TECHNOArk 1 3960 Siders SWITZERLAND +4 1 (0) 848 800 221 [email protected] www.akts.com

DSC Consumables, Inc. 1201 10th Street NW Austin, MN 507-438-9807 [email protected] www.dscconsumables.com

Extrel CMS, LLC 575 Epsilon Drive Pittsburgh, PA 412-963-7530 [email protected] www.extrel.com

Instrument Specialists, Inc. 133 East Main Street, P.O. Box 280 Twin Lakes, WI 53181-0280 262-877-3600 [email protected] www.instrument-specialists.com

J&C Consultation and Technology 6 Barter Crescent Forest Hill, Vic 3131 +61 3 9878 7297 [email protected] www.caotechnology.com.au

Linseis Inc. 109 North Gold Drive Robbinsville, NJ 08691 609-223-2070 [email protected] www.linseis.com

Mettler-Toledo Inc. 1900 Polaris Parkway Columbus, OH 43240 800-638-8537 www.mt.com

RT Instruments, Inc. Fred Klein 1240 Churchill Downs Ave. Woodland, CA 95776 Phone: (530) 666-6700 [email protected] www.rtinstruments.com

Systag System Technik AG Bahnhofstrasse 76, CH-8803 Rüschlikon, Switzerland +41 (0)44 704 54 54 [email protected] www.systag.ch

TA Instruments 159 Lukens Drive New Castle, DE 19734 302-427-4000 [email protected] www.tainstruments.com

ULVAC-RIKO, Inc. 401 Griffin Brook Drive Methuen, MA 01844 USA 978-686-7550 www.ulvac-riko.co.jp

6

2013 NATAS Award Winners

NATAS-Mettler Award for Outstanding Achievement (sponsored by Mettler-Toledo)

Prof. Peggy Cebe Tufts University

NATAS Fellow

Dr. Michael Kessler Iowa State University

NATAS Outstanding Service Award

Dr. Bob Howell Central Michigan University

NATAS Student Award

(sponsored by TA Instruments, Western Kentucky University Len Thomas Student Travel Fund, and NATAS)

Ran Tao, Texas Tech University Lonchun Zhong, North China Electric Power University

Shang-Hao Liu, Yunlin University of Science and Technology Prithwish Chatterjee, Arizona State University

NATAS Student Travel Award

(sponsored by TA Instruments, Western Kentucky University Len Thomas Student Travel Fund, and NATAS)

Hamed Janani, Florida A & M University Yun-Ting Tsai, Yunlin University of Science and Technology

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Previous Award Winners

NATAS-Mettler Award for Outstanding Achievement

NATAS Fellows NATAS Outstanding Service Award

2012 B. Howell 2011 A. McGhie 2010 J. Menczel 2009 R. G. Alamo 2008 W.-P. Pan 2007 E. L. Charsley 2006 C. E. Schick 2005 D. J. W. Grant 2004 S. Vyazovkin 2003 G. Delia Gatta 2002 V. Mathot 2001 G. McKenna 2000 M. Reading 1999 S. Cheng 1998 A. Riga 1997 Y. Kanna 1996 M. E. Brown 1995 J. C. Seferis 1994 S. St. John Warne 1993 Y. Godovsky 1992 H. Starkweather 1991 J. F. Johnson 1990 V. Balek 1989 R. B. Prime 1988 J. Rouquerol 1987 H. Bair 1986 H. G. Wiedemann 1985 E. A. Turi 1984 L. Mandelkern 1983 R. S. Porter 1982 J. Chiu 1981 T. Ozawa 1980 J. H. Flynn 1979 D. Dollimore 1978 J. K. Gilham 1977 H. Kambe 1976 P. K. Gallagher 1975 F. E. Karasz 1974 J. Sestak 1973 E. M. Barrall, III 1972 F. and J. Paulik 1971 B. Wunderlich 1970 W. W. Wendlandt 1969 R. L. Stone 1968 R. MacKenzie

2012 R. Ozao 2011 C.-M. Shu 2010 D. J. Burlett 2009 None 2008 E. L. Charsley

P. Cebe 2007 M. Reading 2006 S. Vyazovkin 2005 C. E. Schick

L. C. Thomas 2004 M. Keating

C. M. Neag 2003 M. Brown

S. L. Simon 2002 B. Howell

J. Menczel 2001 D. Jones

L. Judovits 2000 None 1999 K. Lavanga 1998 H. Friedman 1997 W.-P. Pan 1996 I. Goldfarb

L. Whiting 1995 R. Seyler

J. Oxley 1994 l. Harrison

P. Ronco 1993 S. Cheng 1992 A. Riga 1991 M. Jaffe 1990 R. Chartoff

J. Seferis R. Blaine

1988/9 C.M. Earnest Y. Khanna A. R. McGhie A. K. Sircar H. Starkweather

1987 S. St. J. Warne R. Weiss H. Wiedemann

1986 D. Dollimore F. Karasz W. Prest, Jr.

1985 P. Gill J. Gillham R. MacKenzie L. Mandelkern R. B. Prime

1984 H. Bair B. Barrall, II J. Elder R. Johnson R. Porter

1983 J. Johnson G. Langer H. McAdie C. Murphy W. Wendlandt

1982 D. Brazier R. Ferrillo J. Maurer E. Pearce B. Wunderlich

1981 J.Chiu J. Flynn P. Gallagher P. Garn E. Turi

2012 S. Simon 2011 M. Varma-Nair 2010 K. F. Schoch, Jr. 2009 R. G. Blaine D. E. G. Jones 2008 T. S. Ramotowksi 2007 M. J. Rich 2006 W. Hammetter 2005 L. Judovits 2004 W. P. Pan 2003 D. Burlett 2002 B. Wunderlich 2001 C. M. Earnest 2000 C. M. Neag 1999 S. Dyszel 1998 S. Mikhail 1997 M. Keating 1996 J. Enns 1995 A. Riga 1994 L. Boyter 1993 B. Bachman 1992 A. McGhie 1991 R. Hutchinson 1990 M. Steiner 1989 B. Fabricant 1988 C. B. Murphy 1987 R. C. Johnson 1986 H. McAdie 1985 P. Gallagher 1984 J. J. Mauer 1983 R. G. Ferrillo 1982 J. Chiu 1981 E. Turi

8

2013 NATAS Conference Sponsors

The following sponsors are gratefully acknowledged for their financial support of the 2013 NATAS Conference.

Cenovus Energy Welcome Reception

Institute for Combustion Science & Environmental Technology, Western

Kentucky University Student Awards

Mettler-Toledo, Inc.

Casino Night Entertainment, Outstanding Achievement Award

Ohio Valley Thermal Analysis Society Student Sponsorship Awards

TA Instruments

Monday’s Spotlight Lunch & Student Awards

9

2013 NATAS Officers & Councilors

President

JOSEPH MENCZEL 412 Stampede Rd.

Fort Worth, TX 76131 Phone: 817-847-8450 [email protected]

Vice President

(President-Elect) BRIAN GRADY

University of Oklahoma 100 E. Boyd St.

Norman, OK 73019 Phone: 405-325-4369

[email protected]

Secretary

PRASHANTH BADRINARAYANAN Dupont Experimental Station

200 Powder Mill Rd. Wilmington, DE 19803 Phone: 302-695-3100

[email protected]

Treasurer

TOM RAMOTOWSKI NUWC Division Newport,

Road 1512, B-1170 1176 Howell St., Code 2131

Newport, RI 02841-1708 Phone: 401-832-5111

[email protected]

Executive Councilor

ERIC SCHOCH Northrop Grumman

1745A W. Nursery Rd. MS Z-18

Linthicum, MD 21090 Phone: 410-765-1362

[email protected]

Education Councilor

QUENTIN LINEBERRY ICSET

2413 Nashville Rd., STE C2 Bowling Green, KY 4201

Phone: 270-780-2532 [email protected]

Meetings Councilor

BOB HOWELL Applications in Polymer

Science, DW 263 Central Michigan University Mount Pleasant, MI 48858


Publications Councilor

QUEENIE KWOK NRCan Canadian

Explosives Research Laboratory

Bells Corners Complex 1 Haanel Dr.

Ottawa, Ontario Canada K1A 1M1


Staff Management

TERRILL MARTIN Western Kentucky University

Center for Research & Development 2413 Nashville Rd.

Bowling Green, KY 42101 Phone: 270-745-2530

[email protected]

10

2013 NATAS Committee Chairs

Academic Liaison

MICHAEL KESSLER Iowa State University

Department of Materials Science and Engineering Ames, IA 50011


Awards

WEI-PING PAN Western Kentucky University

ICSET Department of Chemistry


[email protected]

Education

BOB HOWELL Central Michigan University

Applications in Polymer Science DW 263

Mt. Pleasant, MI 48859 Phone: 989-774-3582

[email protected]

ICTAC Representative WEI-PING PAN

Western Kentucky University ICSET

Department of Chemistry Bowling Green, KY 42101


Local Sections SUBHASH C. MOJUMDAR

University of Guelph Department of Chemistry

50 Stone Rd. E Guelph, ON, N1G 2W1

Canada Phone: 519-896-1929

[email protected]

Membership MARICELA AMARILLAS

Raytheon Company 1151 East Hermans Road

MS TU/807/G5 Tucson, AZ 85756


NATAS Notes Editor TINA M. ADAMS

The Lubrizol Corporation 29400 Lakeland Blvd. Wickliffe, OH 44092 Phone: 440-347-8509

[email protected]

Photographer/Historian ALAN RIGA TechCon Inc.

6325 Aldenham Drive Cleveland, OH 44143-3331


Publicity/Marketing BOB FIDLER

Netzsch Instruments N.A. LLC 37 North Avenue

Burlington, MA 01803 Phone: 704-948-9534

[email protected]

Vendor Relations BOB FIDLER

Netzsch Instruments N.A. LLC 37 North Avenue

Burlington, MA 01803 Phone: 704-948-9534 Fax: 704-948-9535

[email protected]

Volunteers TINA M. ADAMS

The Lubrizol Corporation 29400 Lakeland Boulevard

Wickliffe, OH 44092 Phone: 440-347-8509 Fax: 440-347-4713

[email protected]

Website / Database Western Kentucky University

2413 Nashville Road, C-2 Bowling Green, KY 42101

Phone: 270-901-3490 Fax: 270-745-2221

[email protected]

Long Range Planning Vacant

11

2013 NATAS Conference Committee

Conference Chair WEI-PING PAN



[email protected]

Conference Vice Chair TERRILL MARTIN

Western Kentucky University Center for Research & Development


[email protected]

Technical Program Chair RIKO OZAO

SONY Institute of Higher Education Atsugi, Kanagawa, 243-8501

Phone: +81-46-250-8936 [email protected]

Technical Program Vice Chair CHI-MIN SHU

National Yunlin University of Science and Technology Douliou, Yunlin, Taiwan 64002, ROC

Phone: 886-5-534-2601 [email protected]

Conference Proceedings Chair DIANA S. SMIRNOVA

ExxonMobil Research & Engineering Company

1545 Route 22 East Annandale, NJ 08801 Phone: 908-730-2093

[email protected]

Short Course Chair WEI-PING PAN



[email protected]

Conference Exhibition Chair (Exhibits) WEI-PING PAN



[email protected]

Poster Committee GeneralPoster(GP)

Chair:Prof.CHI‐MINSHU(Chair)NationalYunlinUniversity,TaiwanDr.QUENTINLINEBERRY(Judge)WesternKentuckyUniversity

Prof.YANCAO(Judge)WesternKentuckyUniversity

StudentPoster(SP)Prof.ATSUMIMIYAKE(Judge)

YokohamaNationalUniversity,JapanMs.QUEENIEKWOK(Judge)

CanadianExplosivesResearchLab,CanadaProf.PEGGYCEBE(Judge)

TuftsUniversity

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NATAS Regional Sections

Bay Area Thermal Analysis Society Alex Tregub

Intel Corporation 2880 Northwestern Parkway

Santa Clara, CA 95052 (408) 653-9408

[email protected]

Canadian Thermal Analysis Society Subhash C. Mojumdar University of Guelph

Department of Chemistry 50 Stone Rd. E

Guelph, ON, N1G 2W1 Canada

(519) 896-1929 [email protected]

www.ctas.org

Texas & Southwest Thermal Analysis & Rheology Forum (NaTex)

Sindee L. Simon Texas Tech University

Department of Chemical Engineering Lubbock, TX 79409

(806) 742-1763 [email protected]

www.depts.ttu.edu/che/natex/home.php

Thermal Analysis Forum of the Delaware Valley Steve Sauerbrunn

University of Deleware Center for Composite Materials

Newark, DE 19716 (302) 831-6692

CELL (302) 545-5895 [email protected]

13

NATAS-Mettler Outstanding Achievement Award Lecture


Thermal Analysis of Fibrous Proteins

Peggy Cebe

Tufts University Medford, MA 02155

[email protected]

ABSTRACT I am deeply honored to be selected as the recipient of the 2013 NATAS Award for Outstanding Achievement, sponsored by Mettler-Toledo. In this lecture, I will describe how thermal analysis can be applied to investigate the structural transitions in fibrous proteins, especially those derived from silk. These materials are biocompatible and biodegradable making them useful for biomedical applications such as drug delivery vehicles and implantable devices. The first study involves fibroin, the protein extracted from the cocoon of the domesticated B. mori silkworm. The silk molecule adopts a variety of secondary structural conformations including non-crystalline helices, random coils, and turns, and crystalline beta pleated sheets. Silk presents several challenges to the thermal analyst, viz., it readily absorbs water, forms very small and imperfect crystals, and degrades prior to melting. Heat capacity analysis of the glass transition was undertaken to quantify the non-crystalline structures and clarify the role of bound water. To overcome thermal degradation, fast scanning chip calorimetry was used to show the melting behavior of fibroin, demonstrating for the first time the close thermal analogy between these bio-macromolecules and synthetic polymers. The second study involves spider silk-like di-block copolymers specially synthesized to contain hydrophilic and hydrophobic blocks. Differential scanning calorimetry and real time infrared spectroscopy, along with modeling of the solid state heat capacity, were techniques used to study the thermal transitions among the secondary structures in these novel materials.

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Plenary Lecture

Tuesday, August 6, 2013

Crude Oil, Tobacco, Polymers, Coffee and Soot: Thermal Analysis of Complex Materials and Thermal Processes Using Photo-Ionization Mass Spectrometry

Ralf Zimmermann1, Sebastian Wohlfahrt2, Michael Fischer2, Robert Geissler2, Georg Matuschek2,

Thorsten Streibel3, Mohammad Reza Saraji-Bozorgzad4, Thomas Denner5, Andreas Walte4

1JMSC (Helmholtz Zentrum München/CMA and University of Rostock)

Germany ([email protected]) 2 Helmholtz Zentrum München, 3University of Rostock, 4Photon GmbH, 5Netzsch

ABTRACT

Mass Spectrometry with soft Photo-Ionisation (PIMS) [1] enables the direct detection of traces of intact molecules from complex organic vapours as well as in pyrolysis or combustion off-gases. This renders PIMS as a perfect tool for Evolved Gas Analysis (EGA) for determining molecular organic signatures of desorption, pyrolysis and combustion processes in Thermal Analysis (TA) and applied combustion research.

Conventional EGA mass spectrometry using electron ionisation (EI) gives solely restricted information - mainly on the most abundant small molecules such as CO, CO2 or CH4. More complex organic molecules usually are not detectable due to the molecular fragmentation associated with EI. Thermal analysis coupled fragmentation-less (i.e. soft) PIMS (using Single Photon Ionisation, SPI or Resonance-Enhanced Multiphoton Ionisation, REMPI) recently was successfully applied for analysis of the evolved pattern of intact organic molecules [2].

In the lecture initially a briefly explanation of the principles of the used photo-ionisation mass spectrometry approaches is given.

In the following, the different experimental constellations for coupling of thermal analysis and thermal processes to PIMS are presented and discussed.

The photo-ionisation methods are used in conjunction with different mass spectrometer systems (time-of-flight MS (TOFMS), ion-trap MS with MS/MS (ITMS), quadrupol MS (QMS), high resolution/exact mass TOFMS (HR-TOFMS)), various sample inlet systems (capillary-coupling, skimmer-coupling, direct- and micro-probe-sampling) and different thermal analysis devices (thermogravimetry (TG), differential scanning calorimetry (DSC), thermal desorption (TG), pyrolyser (Py)).

The main part of the lecture discusses various applications of the time-resolved on-line detection of the molecular organic signature of thermal processes by Thermal Analysis-Photo-Ionisation Mass Spectrometry (TG-PIMS). This includes analyses of the evolving organic compounds from the thermal decomposition of polymers, coffee beans during simulated coffee-roasting processes, crude oils during

15

simulated distillation processes and pyrolysis of bio mass by TG-PIMS devices. A thermal desorption/pyrolysis approach (TG/Py-PIMS) is used e.g. for detection of traces of harmful substances (drugs, explosives) and analysis of the chemical composition of ambient aerosols and soot.

Direct monitoring of combustion and pyrolysis processes finally can be used for industrial process monitoring purposes. The comparison of TG-PIMS laboratory results and pilot-plant process studies finally suggest the applicability of the laboratory instruments for simulation of industrial processes. In summary the potential of thermal analysis hyphenated to soft photo-ionisation mass spectrometry for industrial applications as well as applied and fundamental research is demonstrated.

References [1] L. Hanley, R.Zimmermann, Anal. Chem. 81 (2009) 4147-4182 [2] M.R.Saraji-Bozorgzad et al., Anal. Chem. 80 (2008) 3393-3403, R. Geissler et al., Anal. Chem. 81 (2009) 6038-6048,M.R.Saraji-Bozorgzad et al., J. Therm Anal. Calorim. 105 (2011) 691-697.

16

Plenary Lecture

Wednesday, August 7, 2013

Distribution and Transportation of Radioactive Nuclear in Environments –Fukushima and Tokyo

Hirohisa Yoshida Tokyo Metropolitan University

Japan [email protected]

ABTRACT

Huge amount of radioactive nuclear polluted the environment in East Japan, including Tokyo by the accident of Fukushima Nuclear Power Plant on March 12, 2011. We have investigated the distribution of radioactive nuclear in environment, such as the depth concentration profile of soil and the cross sectional profile of plants, and the change of radioactive nuclear concentration in the environment in Fukushima and Tokyo from May 2011 to May 2013.

The presentation included the following contents: - The distribution of radioactive nuclear in soil and plants in Fukushima. - The distribution of radioactive nuclear in Tokyo. - The transportation mechanism of radioactive nuclear in the environment in Fukushima. - Project of riving community in Fukushima.

*Full paper available on Proceedings CD

17

41st NATAS Meeting Technical Program

Sunday, August 4, 2013

Opening Reception, General/Student Poster Session, Exhibition Events Center/Exhibits, Ballroom C/D

Chair: Prof. Chi-Min Shu, National Yunlin University, Taiwan 17:00 to 21:00

* GP-1 Thermal Decomposition of RDX/AP by TG-DSC-MS-FTIR Q. Jiao, Y. Zhu, H. Huang, H. Ren (Beijing Institute of Technology)

GP-2 Synthesis, Structure, and Thermal Properties of Metal-Organic Frameworks Built with s Block Metal Ions and Carboxylates B. Yan, R. Vakiti, Y. Cao, W. Pan, C. Webb (Western Kentucky University)

* GP-3 Material Characterization of Heat Shrinkable Film – A Comparability Study Z. Sevinc, C. Strobel (Baxter)

* GP-4 Moisture Effect on Melt Rheology of Copolyester – Thermoplastic Polyester Elastomer (TPE) Blend Z. Sevinc (Baxter)

GP-5 Multifunctional Silk-Zein Protein Alloy Biomaterials X. Hu (Rowan University)

GP-6 Thermoanalysis as a Tool in Characterization of Waste from the Steel Industry H. Mothe Filho, P. Castro (Departamento de Geociências/UFRRJ)

GP-7 Comparative Thermal Stability of Gelatin Based Gel Containing Chitosan, Montmorillonite, and Laponite Nanoparticles J. Prado, S. Vyazovkin (University of Alabama Birmingham)

* GP-8 The Use of Three-Dimensionally Ordered Macroporous (3DOM) LaFeO3 Perovskites as Oxygen Carriers in Chemical-Looping Reforming of Methane F. He (Guangzhou Institute of Energy Conversion, Chinese Academy of Sciences)

GP-9 Determination of Thermal Degradation Behavior of Oligo/Poly(Ethyl-2-Cyanoacrylate) Using DSC/TGA S. Guns, W. de Klerk, G. Groeneveld, A. van der Heijden, M. de Puit (TNO)

GP-10 Physico-Geometric Kinetic Analysis of Thermal Decomposition of Solids in an Undergraduate Thermal Analysis Laboratory N. Koga, Y. Goshi, M. Yoshikawa, T. Tatsuoka (Hiroshima University)

* GP-11 Thermal Instability of Organic Carbonates with Charged Cathode Materials in Lithium-Ion Battery J. Hsu, Y. Duh, C. Kao, W. Ou (Chia-Nan University of Pharmacy & Science)

GP-12 Temperature Modulated Differential Scanning Calorimetry as a Tool for Characterizing Waxes T. Adams (The Lubrizol Corporation)


18

GP-13 Cure Kinetics of Glycidyl Azide Polymer With Electron Acceptors Molecules by Means of DSC Analysis C. Dubois, E. Comtois, R. Pontes (Ecole Polytechnique Montreal)

GP-14 Kinetic Analysis of Coal Pyrolysis G. Labojko, A. Plis (Institute for Chemical Processing of Coal)

GP-15 Fast Scanning Calorimetry of Polyethylene E. Zhuravlev, M. Vadlamudi, A. Wurm, M. varma-nair, C. Schick (University of Rostock)

* GP-16 Evaluation of Thermal Hazard For Commercial 14500 Lithium-Ion Batteries T. Hsieh, Y. Sun, Y. Duh, C. Kao (National United University)

* GP-17 Thermal Behavior of Lithium-Ion Battery Electrolytes with Differential Scanning Calorimeter Y. Sun, T. Hsieh, J. Hsu, Y. Duh, C. Kao (National United University)

GP-18 Coupling of Thermogravimetry to a New Time of Flight Mass Spectrometer with a Photon Ionization Source M. Saraji-Bozorgzad, M. Fischer, T. Gröger, A. Walte, M. Bente-von Frowein, T. Denner, R. Zimmermann (Photonion GmbH)

* GP-19 Proposal of a Method for Optimizing Fitting Parameters in Thermal Analysis J. Lopez-Beceiro, M. Rios Fachal, J. TarrÃo-Saavedra, S. Naya, R. Artiaga (University of A Coruna, Spain)

* GP-20 Limited Oxygen Index and Flame Retardancy of Functionalized Novolacs / Epoxy Composites on Glass Fiber Cloth H. Wu, W. Yang, C. Hsieh (Taiwan Union Technology Corporation)

GP-21 Thermal Hazard Assessment of Reactive Systems L. Yang (Intertek)

GP-22 Thermal Analyses of Esterified Lignin from Sugarcane F. Silva, V. Calado, N. Pereira Jr. (Universidade Federal do Rio de Janeiro)

GP-23 Developing and Testing a Model for Loading Salts from Solutions into Nanopores R. Farasat, S. Vyazovkin (U Alabama at Birmingham)

GP-24 Calorimetry and Thermokinetics Studies on Al-LiBH4 Composite for Hydrogen Generation F. Xu, F. Xu, L. Sun, H. Liu (Guilin University of Electronic Technology)

GP-25 A Novel Microencapsulated Phase Change Materials Based on Highly Thermal Conductive Shell for Thermal Regulation H. Zhang, F. Xu, L. Sun (Guilin University of Electronic Technology)

GP-26 Water State in Methyl Cellulose Thermo Reversible Hydrogels Containing Salt and Polyethylene Glycol Y . Nishimoto (Kanagawa Univ.)

GP-27 Thermal Behavior of Vacuum Grease Measured by Vacuum Thermobalance S. Endo, M. Yoshiizumi, N. Oikawa, K. Shimada, N. Gonohe (Ulvac-Riko, Inc.)


19

GP-28 Study on Thermal Decomposition of Polymers by Simultaneous Measurement of TG-DTA and Miniature Ion Trap Mass Spectrometry equipped with Skimmer-type Interface T. Arii, L. Celiz (Rigaku Corporation)

GP-29 Practical Determination of Heat Capacity of Pharmaceutical Crystals/Glasses Using Modulated-Temperature Differential Scanning Calorimetrys E. Yonemochi, T. Harada, K. Kawakami, Y. Yoshihashi, K. Terada (Hoshi University)

GP-30 Development of Far Infrared Ray Based Drying Unit Using Woodceramics Y. Okachi, K. Ogawa, T. Jyunichiro, T. Okabe (Iwate University)

Student Poster Session Events Center/Exhibits, Ballroom C/D

18:00 to 21:00

* SP-1 Pyrolysis Characteristics and Kinetics of Fresh Biomass With Different Initial Moisture M. Zhang, F. Min (Anhui University of Science and Technology)

SP-2 Functionalization and Modification of Naphthaquinone Analogs as HER2 Inhibitors D. Lella, C. Stevens, B. Yan (Western Kentucky University)

* SP-3 Estimation of Thermal Hazard and Thermokinetic Paramerters for Tert-Butyl Peroxy-2-Ethyl Hexanoate by Theoretical Kinetic Model and Mass Spectrometry Technology Y. Tsai, M. You, F. Tsai, C. Shu (Graduate School of Engineering Science and Technology Doctoral Program)

SP-4 Thermal Stability Analysis on Inhibited Butadiene Monomer by Calorimetric Approaches S. Shen, T. Wang, Y. Tsai, C. Shu (Department of Applied Geoinformatics, Chia Nan University of Pharmacy and Science)

SP-5 Thermal Hazard Assessment of Propylene Oxide Reaction Using DSC and VSP2 S. Weng, S. Liu, H. Hou, Y. Yu, Y. Lin, C. Shu (National Yunlin University of Science and Technology)

SP-6 Complex Evaluation of Non-Isothermal and Isothermal Kinetic Analysis Methods for 2,2'-Azobis (Isobutyronitrile) Y. Yu, S. Liu, H. Hou, Y. Lin, S. Weng, C. Shu (National Yunlin University of Science and Technology)

SP-7 Thermogravimetric Analysis of Non-Biodegradable X-Ray Contrast Media Over TiO2 S. Annarapu, M. Nee (Western Kentucky University)


20

SP-8 Thermokinetic Parameters of Cumene Hydroperoxide by DSC G. Shiue, J. Chen, M. Lee, C. Huang, C. Shu Hsiuping University of Science and Technology)

SP-9 Thermal Hazard Analysis and Thermal Stability Parameters Evaluation for Lauroyl Peroxide Mixed With H2O and Dry Fire-Extinguishing Chemicals by Novel Calorimetric Technology T. Hsieh, Y. Tsai, R. Chang, C. Shu (Chienkuo Technology University)

SP-10 Expression, Purification and Identification of Fibroblast Growth Factor-1 G. Ison, R. Paripelli (Western Kentucky University)

SP-11 Thermal Decomposition Characteristics Evaluation of Tert-Butyl Peroxy-3,5,5-Trimethylhexanoate (TBPMH) by DSC and TAM III Y. Chang, Y. Tsai, C. Shu (National Yunlin University of Science and Technology)

* SP-12 Reactive Hazards Assessments on the Symmetrical Organic Peroxides via Calorimetric Techniques Y. Duh, S. Wu, C. Kao (National United University)

* SP-13 Thermal Behavior of Cashew Gum By Simultaneous TG/DTG/DSC-FTIR C. Mothe, J. Freitas (Federal University of Rio de Janeiro)

* SP-14 Thermal Evaluation of Base Bleed Propellants C. Mothe, P. Paula, M. Mothe (Federal University of Rio de Janeiro)

SP-15 Heat Storage Capacity Analysis of a Novel Molten-Salt Filled with Nanoparticles for Concentration Solar Plants D. Wu, Z. Liu, Y. Nian, Z. Han (North China Electric Power University)

SP-16 Study of Mercury Adsorption by Selected Chinese Coal Fly Ashes L. Zhong, Y. Teng, Z. Liu, Z. Sui, K. Zhang, W. Pan (North China Electric Power University)

* SP-17 The Glass Transition and Rheology of a Polystyrene Nanocomposite R. Tao, S. Simon (Texas Tech University)

* SP-18 Controlled Morphology of Thin Film Silicon Integrated With Environmentally Responsive Hydrogels P. Chatterjee, Y. Pan, E. Stevens, T. Ma, H. Jiang, L. Dai (Arizona State University)

SP-19 Structural Phase Transition and Electrical Conductivity of Ba2-xLaxFe2O5+d T. Okiba, E. Niwa, F. Fujishiro, T. Hashimoto (Nihon University)

SP-20 Thermal Properties of Salts Y. Salazar, J. Grebowicz (University of Houston, Downtown)

SP-21 Selecting Polymer Candidates for Surgically Implanted Materials by Advanced Derivative Analysis of DSC W. Eng, S. kozawz, A. Walker, J. McNulty, M. Song, A. Riga (Case Western Reserve University)


21

SP-22 Selection of Medical Plastics by Thermogravimetric Analysis (TGA) and Enhanced Derivative Analysis W. Eng, S. kozawz, M. Song, A. Riga, p. kota, t. black, D. Park, M. Tedesco (Case Western Reserve University)

SP-23 Synthesis of TiO2 Based on Hydrothermal Methods Using Elevated Pressures and Microwave Conditions C. Lu (Institute for Combustion Science & Environmental Technology)

SP-24 The Synthesis and Characterization of Graphene Oxides Based on a Modified Approach Y. Lin

SP-25 Miscibility and Molecular Mobility of Amorphous Solid Dispersions of Nifedipine and PVP X. Yuan (University of Kentucky)

SP-26 Ionic Conductivity in Non-Ionic Materials U. Avala (Western Kentucky University)

SP-27 Comparative Studies on Fire-rated and Standard Gypsum Wallboard H. Javangula (Western Kentucky University)

SP-28 Adsorptive Removal of Heavy Metals from Water Using Water Bamboo Husk Particles H. Asberry (Western Kentucky University)

SP-29 Sorption of Bisphenol-A, 2 Naphthol, and Doxepin onto a 1-Hexadecylamine-Cu(II)-Amine Functionalized Indium Tin Oxide Electrode J. Biechele-Speziale (Western Kentucky University)

SP-30 The thermal Analysis and properties of Ionic Liquids V. Kolanka, Y. Cao, C. Webb, W. Pan (Western Kentucky University)

* SP-31 Thermal Characterization of Cosmetics Developed From Keratin Hydrolyzed From Feathers' Poultry T. Gutierrez, M. Mothe, C. Mothe (UFRJ)

SP-32 The Effect of Particle Size and Metal Contents on Arsenic Distribution in Coal-fired Fly Ash C. Song, L. Zhong, D. Xu, C. Jiang, Z. Sun, Y. Teng, H. Xu, L. An (North China Electric Power University)


22

Monday, August 5, 2013 Morning Sessions

Plenary Session

Ballroom C/D Wei-Ping Pan, Western Kentucky University (Conference Chair)

Riko Ozao, SONY Institute of Higher Education (Technical Program Chair)

8:00 - 8:05 8:05 - 8:50

Greetings NATAS-Mettler Award for Outstanding Achievement Lecture Thermal Analysis of Fibrous Proteins Prof. Peggy Cebe (Tufts University)

Pln-1

Energetics Meeting Room #5

Dr. Atsumi Miyake, Yokohama National University Mr. Wim de Klerk, TNO-Defense, Security and Safety

Organizers 9:00 – 9:40 Recent Accidental Explosions in The Process Industries in Japan

A. Miyake (Yokohama National University) Nrg-1

9:40 – 10:00 * Effects of Micro-/Nano-Aluminum on Thermal Decomposition of Hexogen/Ammonium Perchlorate Y. Zhu, Q. Jiao, H. Huang, H. Ren (Beijing Institute of Technology)

Nrg-2

10:00 – 10:20 Oxygen Scavenging Enhances Exothermic Behavior of Aluminum Fueled Thermites O. Mulamba (Texas Tech University)

Nrg-3

10:20 – 10:40 Thermal and Hazard Characterization of Triacetone Triperoxide Q. Kwok, C. Badeen, H. Feng, R. Turcotte, S. Singh (Canadian Explosives Research Laboratory)

Nrg-4

10:40 – 11:00 BREAK 11:00 – 11:20 Influence of Temperature in The Nitration of Sulfamates

Y. Sugie, A. Miyake (Japan Carlit Co., Ltd.) Nrg-5

11:20 – 11:40 Improved Stability of Double Base Propellants M. Lesley , J. Melin, J. Sims (ATK Aerospace Systems)

Nrg-6

11:40 – 12:00 * Thermal Instability of Organic Esters and Ethers with Deposited Lithium in Lithium-Ion Battery J. Hsu, Y. Li, Y. Duh, C. Kao (Chia-Nan University of Pharmacy & Science)

Nrg-7


23

Advances in Instrumentation and Methods Salon B

Organizer: Dr. Takahisa Tsugoshi, AIST, Japan 9:00 – 9:40 * Simultaneous Measurement of Thermogravimetry-Differential Thermal

Analysis and Miniature Ion Trap Mass Spectrometry equipped with Skimmer-type Interface, TG-DTA-ITMS T. Arii, L. Celiz (Rigaku Corporation)

AIM-1

9:40 – 10:00 Highly Resolved Online Organic-Chemical Speciation of Evolved Gases from Thermal Analysis Devices Using Single Photon Ionization Mass Spectrometry M. Saraji-Bozorgzad , T. Gröger, M. Fischer, A. Walte, E. Post, T. Denner, R. Zimmermann (Photonion GmbH)

AIM-2

Determination of the Specific Heat Capacity at High Temperatures M. Zemo, E. Hempel, J. Schawe (Mettler Toledo)

AIM-3

10:00 – 10:20 Applications of Differential Scanning Calorimetry High-Pressure Crucibles for Process Safety Assessments R. Kwasny (Fauske & Associates, LLC)

AIM-4

10:20 – 10:40

10:40 – 11:00 BREAK 11:00 – 11:20 Progress of Thermal Conductivity Measurement System

S. Endo (Ulvac-Riko, Inc.) AIM-5

11:20 – 11:40 Measurement of Contact Angles using Enthalpy of Immersion Data B. Grady, Y. Liu, R. Jentoft (University of Oklahoma)

AIM-6

11:40 – 12:00 * Novel Validation on Pressure as a Determination of Onset Point for Exothermic Decomposition of DTBP Y. Duh, W. Wang, C. Kao (National United University)

AIM-7

Polymers, Nanocomposites, and Glasses: Thermal and Rheological Behavior Meeting Room #2

Prof. Sindee Simon, Texas Tech University Dr. Yung Koh, Texas Tech University

Organizers 9:00 – 9:20 The Tg-Confinement Effect in Polymers: Measurement by DSC and Its

Fundamental Underlying Origin J. Torkelson, C. Evans, H. Deng (Northwestern University)

PNG-1

9:20 – 9:40 The Glass Transition, Bulk and Shear Rheology of a Polystyrene Nanocomposite R. Tao, S. Simon (Texas Tech University)

PNG-2

9:40 – 10:00 The Glass Transition of Nanoconfined Polycyanurate: Intrinsic Size and Surface Effects E. Lopez, S. Simon (Texas Tech University)

PNG-3


24

10:00 – 10:20 Effect of Carbon Nanotubes on Thermal Behavior of Poly(L-lactide) and Poly(D-lactide) Electrospun Fibers Y. Zhu, B. Mao, P. Cebe (Tufts University)

PNG-4

10:20 – 10:40 Influence of Processing Conditions on Polymer Crystallization Measured by Fast Scanning DSC J. Schawe (Mettler-Toledo AG)

PNG-5

10:40 – 11:00 BREAK 11:00 – 11:20 Glass Transition and Structural Recovery of Single Polystyrene Ultrathin

Films Y. Koh, S. Gao, S. Simon (Texas Tech University)

PNG-6

Dr. Ozawa/Dr. Flynn in Memoriam: Kinetic Phenomena in Practical Process Prof. Sergey Vyazovskin, University of Alabama-Birmingham

Prof. Nobuyoshi Koga, Hiroshima University, Japan Organizers

9:00 – 9:40 Kinetics and Elementary Mechanisms in Solid-Gas Reactions

M. Pijolat (Ecole des Mines de Saint-Etienne) Kin-1

9:40 – 10:00 Thermodynamic and Kinetic Analysis of Chemical Reaction between CO2 and Ba1-xSrxCeO3 – Evaluation as New CO2 Absorbent Material T. Hashimoto, E. Niwa, R. Sato, R. Yoshizawa, F. Fujishiro (CHS, NIhon University)

Kin-2

10:00 – 10:20 A Multiscale Approach for the Kinetic Modeling of CaO Carbonation L. Favergeon, L. Rouchon, M. Pijolat (Ecole des Mines)

Kin-3

10:20 – 10:40 Adapting Thermal Analysis Methods to Characterize Anion Exchange Reactions in Nanodimensional Layered Metal Hydroxides J. Hossenlopp, C. Machingauta (Marquette University)

Kin-4

10:40 – 11:00 BREAK 11:00 – 11:20 Kinetic Modeling of De- and Rehydration of Solids for

Thermochemical Energy Storage M. Molenda, M. Linder, A. Wörner (German Aerospace Center (DLR))

Kin-5

11:20 – 11:40 * Understanding Cold-Cap Reactions of Nuclear Waste Feeds through Evolved Gas Analysis (EGA) J. Chun, C. Rodriguez, M. Schweiger, P. Hrma (Pacific Northwest National Laboratory)

Kin-6

11:40 – 12:00 Kinetics and Mechanism of Thermal Transformations of Sodium Dicyanamide in Nanopores and Bulk B. Yancey, S. Vyazovkin (U Alabama at Birmingham)

Kin-7


25

____________________________________________________________________________________

Monday Luncheon Ballroom C/D 12:00 to 13:10

Sponsored by TA Instruments ____________________________________________________________________________________


Afternoon Sessions

Energetics Meeting Room #5

Dr. Atsumi Miyake, Yokohama National University Mr. Wim de Klerk, TNO-Defense, Security and Safety

Organizers 13:20 – 13:40 Can We See the Light: Thermal vs. Impact Sensitivity?

J. Oxley, J. Smith, M. Porter, R. Rettinger (University of Rhode Island) Nrg-8

13:40 – 14:00 A Study of Chemical Compatibility Using Heat Flow Calorimeter: 2,4,6-Trinitrotoluene with Contact Materials E. Turpeinen, M. Sairiala (Finnish Defence Forces Technical Research Center)

Nrg-9

14:00 – 14:20 Thermal Decomposition of High Performance Oxidizer Ammonium Dinitramide under Pressurized Condition H. Matsunaga, H. Habu, A. Miyake (Yokohama National University)

Nrg-10

14:20 – 14:40 Reactive Characteristics of Triazolone and Metal Nitrate Mixtures S. Yoshino, K. Sakamoto (Nihon University)

Nrg-11

14:40 – 15:00 Pressure Effect on the Thermal Decompostion of Ammonium Nitrate: A Kinetic Investigation A. Vargeese, K. Muralidharan (Department of Chemistry)

Nrg-12

15:00 – 15:20 BREAK 15:20 – 15:40 Prediction of Thermal Aging of Materials by Modified Kinetic

Analysis Based on Limited Amount of Experimental Data Points B. Roduit, M. Hartmann, P. Folly, A. Sarbach (AKTS Inc.)

Nrg-13

Biomaterials and Bio-Inspired Materials

Salon B Prof. Peggy Cebe, Tufts University Prof. Xiao Hu, Rowan University

Organizers 13:20 – 14:00 Assessing the Competiveness of Bio-Derived Polymers

M. Jaffe (New Jersey Institute of Technology) Bio-1


26

14:00 – 14:20 Energy Transduction and Elasticity Model of Resilin Biomaterials X. Hu (Rowan University)

Bio-2

14:20 – 14:40 * TMDSC in Distinguishing Between the Hydrophobic and Hydrophilic Forces Driving the Self Assembly of Lipid Nanotubes J. Matisons, T. Barclay (Gelest Inc)

Bio-3

14:40 – 15:00 Poly(Lactic Acid) Blend Fibers P. Cebe, K. Li (Tufts University)

Bio-4

15:00 – 15:20 BREAK 15:20 – 15:40 Understanding the Thermal Decomposition of Double Base Propellants

through Molecular Modeling J. Melin, J. Sims, M. Lesley (ASRC Federal Space and Defense)

Bio-5

15:40 – 16:00 Thermodynamic Analysis of a Photosynthetic Microbial Fuel Cell C. Xiang, Y. Zou, L. Sun, F. Xu (Guilin University of Electronic Technology)

Bio-6

16:00 – 16:20 Cashew Gum: Functional Properties on SHR Rats Cardiovascular System and Thermal Analysis C. Mothe (Federal University of Rio de Janeiro)

Bio-7

Polymers, Nanocomposites, and Glasses: Thermal and Rheological Behavior Meeting Room #2

Prof. Sindee Simon, Texas Tech University Dr. Yung Koh, Texas Tech University

Organizers

13:20 – 13:40 Thermal Processing of Polymer-Metal Composites Using Microwave Radiation A. Wurm, R. Nicula, S. Vaucher, C. Schick (University of Rostock)

PNG-7

13:40 – 14:00 Enthalpy Recovery of Polystyrene: Does a Long-term Aging Plateau Exist? Y. Koh, S. Simon (Texas Tech University)

PNG-8

14:00 – 14:20 Heat Capacity Studies of Dynamic Systems S. Aubuchon, K. Mohomed, J. Browne

PNG-9

14:20 – 14:40 * Thermal Properties of Nanomodified Asphalts Binders M. Mothe, C. Mothe, M. Pinto, L. Leite (Federal University of Rio de Janeiro)

PNG-10

14:40 – 15:00 * Estimation of Critical Cooling Rate for Binary Metallic Glasses using TTT Diagram S. Prajapati, A. Patel, A. Pratap (The M.S.University of Baroda, Vadodara)

PNG-11


27

Dr. Ozawa/Dr. Flynn in Memoriam: Kinetic Phenomena in Practical Process Meeting Room #1

Prof. Sergey Vyazovskin, University of Alabama-Birmingham Prof. Nobuyoshi Koga, Hiroshima University, Japan

Organizers 13:20 – 14:00 * Isothermal and Non-Isothermal Radical Polymerization Kinetics Using

DSC and Detailed Mechanistic or Isoconversional Methods D. Achilias (Aristotle University of Thessaloniki)

Kin-8

14:00 – 14:20 * Comparative DSC Kinetics of The Reaction of DGEBA with Aromatic Diamines. IV. Iso-Conversional Kinetic Analysis V. Zvetkov, V. Calado, S. Djoumaliisky (Institute of Mechanics, Bulgarian Academy of Sciences)

Kin-9

14:20 – 14:40 High Temperature Solid-Solid Transition in Ammonium Chloride Confined to Nanopores R. Farasat, B. Yancey, S. Vyazovkin (U Alabama at Birmingham)

Kin-10

14:40 – 15:00 Reconciling the Ozawa and Kissinger Methods of Nonisothermal Kinetic Analysis R. Lyon, N. Safronava (Federal Aviation Administration)

Kin-11

15:00 – 15:20 BREAK 15:20 – 15:40 Simple Test for Detecting Influence of Sample Aging on its Thermal

Behavior. Peculiarities of Autocatalytic Reactions B. Roduit, M. Hartmann, P. Folly, A. Sarbach (AKTS Inc.)

Kin-12

15:40 – 16:00 Kinetics of Cumene Oxidation V. Krongauz, J. O'Connell, M. Ling (Baxter Healtcare Corporation)

Kin-13

16:00 – 16:20 Kinetic Analysis of Coal And its Char Oxycombustion using Isoconversional Methods G. Labojko, A. Plis, P. Babinski (Institute for Chemical Processing of Coal)

Kin-14


28

Tuesday, August 6, 2013 Morning Sessions

Plenary Session



8:00 – 8:05 8:05 – 8:50

Greetings Crude oil, Tobacco, Polymers, Coffee and Soot: Analysis of complex materials by Thermal Analysis - Photoionisation Mass Spectrometry Prof. Ralf Zimmermann (University of Rostock and Helmholtz Zenthrum Munchen)

Pln-2

Workshop on the Development of Oxygen Carrier for Chemical Looping Combustion using Thermal Analysis Meeting Room #5

Dr. Song Sit, Cenovus Prof. Yan Cao, Western Kentucky University

Organizers

9:00 – 9:20 * TGA Measurement of Reactivity of Candidate Oxygen Carrier Materials A. Chambers (Alberta Innovates-Technology Futures)

Oxy-1

9:20 – 9:40 * Characteristics of Biomass Chemical Looping Gasification Using Iron Ore as an Oxygen Carrier Z. Huang, F. He, Y. Feng, K. Zhao, A. Zheng, S. Chang, H. Li (Guangzhou Institute of Energy Conversion, Chinese Academy of Sciences)

Oxy-2

9:40 – 10:00 * Lanthanum-Promoted Copper-Based Oxygen Carriers for Chemical Looping Combustion Process S. Sit, Y. Cao, H. Zhao, W. Pan (Cenovus FCCL Ltd, Canada)

Oxy-3

10:00 – 10:20 Study on Characteristics of Cu-Based Oxygen Carrier with Coal Char for Chemical Looping Combustion H. Zhao, Y. Cao, W. Pan (Institute for Combustion Science & Environmental Technology, Western Kentucky University)

Oxy-4

10:20 – 10:40 Sewage Sludge Ash as an Low Cost Oxygen Carrier for Effective Chemical Looping Combustion G. Labojko, E. Ksepko, M. Sciazko (Institute for Chemical Processing of Coal)

Oxy-5

10:40 – 11:00 BREAK


29

11:00 – 11:20 Kinetic Study of Copper-Based Oxygen Carrier for Chemical Looping with Oxygen Uncoupling Y. Ku, H. Wu, S. Shiu, P. Chiu (National Taiwan University of Science and Technology)

Oxy-6

11:20 – 11:40 Transient Temperature Variations in a CLC Packed Bed of Large Particles X. Guo, Y. Sun, R. Li, F. Yang (University of Shanghai for Science and Technology)

Oxy-7

11:40 – 12:00 Asphalt (Bitumen)-Fuelled Chemical Looping Combustion Based on Copper-Based Oxygen Carriers Y. Cao (Institute for Combustion Science & Environmental Technology)

Oxy-8

Polymer and Organic Materials Degradation Salon B

Prof. Bob Howell, University of Central Michigan Prof. Dr. Crisan Popescu, DWI at the RWTH University of Aachen

Organizers

9:00 – 9:40 Gas Phase Combustion of Flame Retardant Polymers in the Microscale Combustion Calorimeter R. Lyon, R. Walters, S. Crowley (Federal Aviation Administration)

Deg-1

9:40 – 10:00 * Thermal Degradation of Trimethylolpropane/Adipic Acid Hyperbranched Poly(ester)s T. Zhang, B. Howell, P. Smith (Michigan Molecular Institute)

Deg-2

10:00 – 10:20 * Flame Retardant Potential of Phosphorus Esters B. Howell (Central Michigan University)

Deg-3

10:20 – 10:40 Phosphorus Esters Derived from Isosorbide/Undecylenic Acid Y. Daniel, B. Howell (Central Michigan University)

Deg-4

10:40 – 11:00 BREAK 11:00 – 11:20 * A Model- Free Method for Evaluating Theoretical Error of Kissinger

Equation Y. Cheng (Nanjing University of Science and Technology)

Deg-5

11:20 – 11:40 * Monomer Distribution and Depletion in Vinylidene Chloride Copolymerization D. Beyer, P. Smith, B. Howell, J. Kosman, C. Thieme (The Dow Chemical Company)

Deg-6

11:40 – 12:00 Conversion of Vinylidene Copolymers to Highly Absorptive Carbon L. Zhang, B. Howell (Central Michigan University)

Deg-7

12:00 – 12:20 Functionalized Tartaric Acid Esters W. Sun, B. Howell (Central Michigan University)

Deg-8


30

Prof. Bernhard Wunderlich in Memoriam: Thermodynamics, Liquid Crystal, Crystallization Meeting Room #2

Prof. Christopher Li, Drexel University Prof. Stephen Cheng, University of Akron

Organizers 9:00 – 9:20 Giant Molecules Based on “Nano-Atoms”: A New Platform for

Engineering Structures at Nanometer Feature Sizes S. Cheng (University of Akron)

BW-1

9:20 – 9:40 * Thermal Analysis of Oriented Polymeric Systems J. Menczel

BW-2

9:40 – 10:00 Professor Bernhard Wunderlich – Thermal Analysis Pioneer M. Jaffe (New Jersey Institute of Technology)

BW-3

10:00 – 10:20 * Melt Miscibility and Isothermal Crystallization Kinetics of Blends of Homogeneous Isotactic Propylene-1-Hexene Copolymers H. Janani, R. Alamo (FAMU-FSU College of Engineering)

BW-4

10:20 – 10:40 Relationship Between the Rigid Amorphous Phase and Mesophase in Electrospun Fibers P. Cebe, Q. Ma, M. Pyda, B. Mao (Tufts University)

BW-5

10:40 – 11:00 BREAK 11:00 – 11:20 Nucleation and Crystallization of Polymer/Inorganic Nanocomposites

A. Wurm, E. Zhuravlev, D. Pospiech, C. Schick (University of Rostock) BW-6

11:20 – 11:40 * Heat Capacity of Poly(3-Hydroxybutyrate) M. Pyda, A. Czerniecka, A. Czerniecka (Rzeszow University of Technology)

BW-7

11:40 – 12:00 Strain-Induced Polymer Crystallization: A Molecular Approach Y. Nie, H. Gao, W. Hu

BW-8

Dr. Ozawa/Dr. Flynn in Memoriam: Kinetic Phenomena in Practical Process Meeting Room #1

Prof. Sergey Vyazovskin, University of Alabama-Birmingham Prof. Nobuyoshi Koga, Hiroshima University, Japan

Organizers

9:00 – 9:20 ICTAC Kinetics Committee Recommendations for Collecting Thermal Analysis Data for Kinetic Computations S. Vyazovkin (Chem Dept, U Alabama-Birmingham)

Kin-15

9:20 – 10:00 TG Measurements for Kinetic Analysis of Thermal Decomposition of Solids N. Koga, M. Yoshikawa (Hiroshima University)

Kin-16


31

10:00 – 10:20 A Kinetic Model for Isothermal and Non-isothermal Reactions to form Thermosetting Polymers J. López Beceiro, S. Fontenot, C. Gracia-FernÃ¡ndez, R. Artiaga, R. Chartoff (University of A Coruña)

Kin-17

10:20 – 10:40 Gelation Kinetics of PAM/PEI System: DSC Investigation K. El-karsani, G. Al-Muntasheri, A. Sultan, I. Hussein (King Fahd University of Petroleum & Minerals)

Kin-18

10:40 – 11:00 BREAK 11:00 – 11:20 Study of Kinetics of Crystallization of Metallic Glass 2826A using

Iso-conversional and Model Fitting Methods A. Pratap, T. Rao, H. Shevde, K. Lad (The Maharaja Sayajirao University of Baroda)

Kin-19

Tuesday, August 6, 2013 Afternoon Sessions

Thermophysical Properties of Materials

Meeting Room #5 Dr. Satoshi Endo (ULVAC-RIKO, Inc.)

Prof. Junko Morikawa (Tokyo Institute of Technology) Organizers

13:40 – 14:00 * Dynamic Mechanical Analysis (DMA) to Help Characterize Vespel SP-

211 Polyimide Material for Use as a 750 °F Valve Seal for the Ares I Upper State J-2X Engine D. Wingard (NASA/MSFC)

TPM-1

14:00 – 14:20 * Thermal Conductivity of Thick Film Tungsten Metallization used in High-Alumina Ceramic Microelectronic Packages M. Eblen (Kyocera America, Inc.)

TPM-2

14:20 – 14:40 Measuring the Thermal Conductivity of Non-Aqueous Heat Transfer Fluids Utilizing the C-Therm TCi Analyzer A. Harris (C-Therm Technologies Ltd.)

TPM-3

14:40 – 15:00 * Thermal Study of HNIW and Mixtures Containing Aluminum Powder M. Xiang, Q. Jiao, Y. Zhu, J. Yu, l. chen (School of Mechatronical Engineering, Beijing Institute of Technology)

TPM-4

15:00 – 15:20 * Thermal Decompositions of Dialkyl Peroxides Studied by DSC J. Hsu, Y. Duh, C. Kao, J. Yo, L. Wen-Lian (Chia-Nan University of Pharmacy & Science)

TPM-5

15:20 – 15:40 Comparative Studies on Fire-rated and Standard Gypsum Wallboard H. Javangula, Q. Lineberry (Western Kentucky University)

TPM-6

15:40 – 16:00 BREAK


32

16:00 – 16:40 Temperature Wave Analysis for the Precise Measurement of Thermal

Diffusivity and Thermal Conductivity J. Morikawa, T. Hashimoto (Tokyo Institute of Technology)

TPM-7

16:40 – 17:00 High-Resolution Adiabatic Scanning Calorimetry of Phase Transitions in Some Calorimetric Reference Materials J. Thoen, J. Leys, P. Losada-Pérez, C. Glorieux (Laboratorium voor Akoestiek en Thermische Fysica, Departement Natuurkunde en Sterrenkunde, KU Leuven)

TPM-8

17:00 – 17:20 Ionic Conductivity in Non-Ionic Materials U. Avala, A. Riga, Q. Lineberry (Western Kentucky University)

TPM-9

17:20 – 17:40 Thermal Decompostion of Pyridinol and 3-Azido Triazole M. Hood, S. Dharavath (Drexel University)

TPM-10

17:40 – 18:00 * Thermal Properties Measuring of Biomass Wet Porous Media Based TPS Method and Thermal Conductivity Model W. Zhu, H. Lin, Y. Cao, B. Li (ZhengZhou Tobacco Research Institute of CNTC)

TPM-11

Polymer and Organic Materials Degradation Salon B

Prof. Bob Howell, University of Central Michigan Prof. Dr. Crisan Popescu, DWI at the RWTH University of Aachen

Organizers 13:40 – 14:00 Micro-Tubes of Keratin

C. Popescu (DWI at the RWTH Aachen University) Deg-9

14:00 – 14:20 Platinum(IV)-functionalized Acrylate Monomers P. Chhetri (Central Michigan University)

Deg-10

14:20 – 14:40 Phosphorus Derivatives of 1,1-Di(4-aminophenyl)-1-dopylethane X. Han, B. Howell (Central Michigan University)

Deg-11

14:40 – 15:00 Thermal Decomposition of a Chitosan Phosphoramide M. Al-Omari, B. Howell (Central Michigan University)

Deg-12

15:00 – 15:20 Phosphorus-Nitrogen Compounds from a Triepoxide S. Lazar, B. Howell (Central Michigan University)

Deg-13

15:20 – 15:40 Properties of Phosphonate Esters K. Mikek, B. Howell (Central Michigan University)

Deg-14

15:40 – 16:00 BREAK 16:00 – 16:40 Properties of Multiply-substituted Phenolic Phosphorous Esters

M. Fisher, B. Howell (Central Michigan University) Deg-15


33



Organizers

13:40 – 14:00 Integration of Ultrafast Scanning Calorimetry with Micro Raman Spectroscopic Investigation D. Zhou, G. Xue, X. Wang (Nanjing University)

BW-9

14:00 – 14:20 Determining Multiple Component Tgs in Miscible Blends and Immiscible Blends Down to the Limit of Infinite Dilution J. Torkelson, C. Evans (Northwestern University)

BW-10

14:20 – 14:40 Temperature Dependence of the Gibbs Free Energy Change During Polymer Crystallization J. Schawe (Mettler-Toledo AG)

BW-11

14:40 – 15:00 Crystallization Behavior and Phase Structure with Long Chain Branch (LCB) Architecture: Model LCB Polyethylenes M. Vadlamudi, R. Alamo (ExxonMobil Research and Engineering Company)

BW-12

15:00 – 15:20 * The Application of Thermal Analysis in Nuclear Waste Management J. Grebowicz (University of Houston-Downtown (UHD))

BW-13

15:20 – 15:40 Controlling Ion Transport in Solid Polymer Electrolytes C. Li (Drexel University)

BW-14

15:40 – 16:00 BREAK 16:00 – 16:20 Wild Silk Based Biomaterials X. HU, J. Buchicchio,

E. Zulker, S. Mazzi, B. Anderson (Rowan University) BW-15

16:20 – 16:40 Thermal Analysis and Structure Characterization of Liquid Crystalline Epoxy Resins Cured in a Magnetic Field Y. Li, M. Kessler (Iowa State University)

BW-16

16:40 – 17:00 Investigation of Incompatible Reaction for Epoxy Resin by Calorimetric Technology and Theoretical Kinetic Model J. Tong, Y. Tsai, C. Shu (National Yunlin University of Science and Technology)

BW-17

17:00 – 17:20 Existence of Time Lag in Crystalline to Smectic A (K- SmA) Phase Transition of 4-Decyl-4-Biphenylcarbonitrile D. Sharma (UML)

BW-18

17:20 – 17:40 * Crystallization Kinetics of Ti20Zr20Cu60 Metallic Glass by Iso-conversional Methods using Modulated Differential Scanning Calorimetry S. Kasyap, A. Patel, A. Pratap (The M.S.University of Baroda, Vadodara)

BW-19


34

Simultaneous and Combined Techniques Meeting Room #1

Prof. Andrew McGhie, University of Pennsylvania Prof. Ralf Zimmermann, University of Rostock and Helmholtz Zentrum München

Dr. Tadashi Arii, Rigaku Corporation Organizers

13:40 – 14:00 Software-assisted Evaluation using TG/PI-QMS with Skimmer

Interface for Polymer Products T. Tsugoshi, Y. Mishima (NMIJ/AIST)

SCT-1

14:00 – 14:20 Thermal Analysis/Evolved Gas Analysis using Single Photon Ionization - Mass Spectrometry for the Investigation of Coffee M. Fischer, S. Wohlfahrt, M. Saraji-Bozorgzad, G. Matuschek, T. Denner, R. Zimmermann (Helmholtz Zentrum Munich)

SCT-2

14:20 – 14:40 Temperature Modulated Differential Scanning Calorimetry in Characterization of Ethylene Vinyl Acetate Copolymer T. Adams (The Lubrizol Corporation)

SCT-3

14:40 – 15:00 Evolved Gas Analysis of Polyphenylene Oxide J. Browne, S. Aubuchon, K. Mohomed (TA Instruments)

SCT-4

15:00 – 15:20 Applications of Evolved Gas Analysis by FT-IR, MS and GC-MS Coupled with TGA and Simultaneous TGA/DSC Thermal Analyzers P. Shapiro, I. Beta (NETZSCH Instruments North America, LLC)

SCT-5

15:20 – 15:40 * Dielectric Thermal Analysis and Differential Scanning Calorimetry Studies Led to a Unified Polaron Theory of Ionic Conduction of Organic and Inorganic Crystalline Materials A. Riga, K. Alexander, D. Mantheni, M. Maheswaram, I. dos Santos (Case Western Reserve University)

SCT-6

15:40 – 16:00 BREAK 16:00 – 16:20 Evolved Gas Analysis (EGA) in TG and DSC With Single Photon

Ionization Mass Spectrometry (SPI-MS): Molecular Organic Signatures from Pyrolysis of Soft and Hard Wood, Coal, Crude Oil and ABS Polymer M. Saraji-Bozorgzad, T. Streibel, A. Walte, R. Geissler, E. Kaisersberger, T. Denner, R. Zimmermann (Photonion GmbH)

SCT-7

16:20 – 16:40 * Thermal Characterization of Poly-L-Lactide by Dielectric Analysis and Modulated DSC J. Lopez-Beceiro, C. Gracia-Fernandez, S. Gomez-Barreiro, A. Älvarez-García, B. Älvarez-García, S. Zaragoza-Fernández, R. Artiaga (University of A Coruna, Spain)

SCT-8

16:40 – 17:00 * Thermal Evaluation of Heavy Oils by Simultaneous TG/DTG/FTIR M. Mothe, C. Mothe, C. Carvalho (Federal University of Rio de Janeiro)

SCT-9


35

17:00 – 17:20 Preparation and Characterization of Activated Carbon from Bitumen H. Zhao, Y. Cao, W. Pan (Institute for Combustion Science & Environmental Technology, Western Kentucky University)

SCT-10

17:20 – 17:40 * The Application of Combined Methods of Thermal Analysis for the Characterization of Rocks Containing Hydrocarbon Z. Jaco, J. Grebowicz (University of Houston - Downtown)

SCT-11

17:40 – 18:00 Enhanced Derivative Analysis Uncovers New Thermal Analytical Data of TGA (Second Derivative) Decomposition and DSC (First and Second Derivative) Melting Processes of Chemicals, Drugs and Polymers A. Riga, W. Eng, J. Kirsh, S. kozawz, M. Song (Case Western Reserve University)

SCT-12

NATAS Business Meeting Knight’s Hall 18:00 to 18:30

Reception and Banquet

WKU Center for Research & Development 19:00 to 21:30


36

Wednesday, August 7, 2013 Morning Sessions

Plenary Session



8:00 – 8:05 8:05 – 8:50

Greetings Dispersion and Transportation of Radioactive Nuclear in Environments -Fukushima and Tokyo Prof. Hirohisa Yoshida (Tokyo Metropolitan University)

Pln-3

Environmental Technology and Green Chemistry Meeting Room #5

Organizer: Prof. Yuko Nishimoto, Kanagawa University, Japan 9:00 – 9:20 Harmful-Reagent-Free Separation and Concentration System of Boron

with Freeze and Melt Process of Environmental Water Y. Nishimoto (Kanagawa Univ.)

Env-1

9:20 – 9:40 Photocatalytic Aerobic Oxidations by Ruthenium Porphyrins Using Visible Light and Molecular Oxygen R. Zhang (Western Kentucky University)

Env-2

9:40 – 10:00 Tetracycline Capped Gold Nanoparticles: Biofriendly Synthesis and Its Potent Antimicrobial Activity Y. Kherde, A. McDade (Western Kentucky University)

Env-3

10:00 – 10:20 Eco-Friendly Synthesis of Antimicrobial Gold Nanoparticles and Its Antimicrobial Activity M. Shah (Western Kentucky University)

Env-4

10:20 – 10:40 BREAK 10:40 – 11:00 Effect Of Modified Fly Ash With Hydrogen Bromide On The

Adsorption Efficiency Of Elemental Mercury W. Orndorff, N. Song, Y. Teng, Y. Zhang, Z. Liu, Y. Cao, W. Pan (Western Kentucky University)

Env-5

11:00 – 11:20 Thermal Investigation of Stepwise Reactions During Co-Gasification Of Coal And Biomass W. Orndorff, Q. Liu, X. Geng, Y. Zhang, Y. Cao, W. Pan (Western Kentucky University)

Env-6

11:20 – 11:40 * Current DEA Measurements of Polar Ionic Conduction and the DSC Neel Temperature Establishes the Longevity Of Nickel Oxide Crystals A. Riga (Case Western Reserve University)

Env-7


37

Standardization and Databases Salon B

Organizer: Dr. Haruka Abe, AIST Japan

9:00 – 9:40 Development of Experimental Data Validation Methods and Property Prediction Models in Thermodynamics C. Muzny (N.I.S.T.)

Std-1

9:40 – 10:00 The progress in ISO/TC61/SC5 for “Determination of thermal conductivity and thermal diffusivity of plastics” from 2000 to 2013 J. Morikawa, H. Lobo, L. Hälldahl, B. Hay, M. Rides, K. Koennecke, P. Le Parlouër, S. Eldin (Tokyo Institute of Technology)

Std-2

10:00 – 10:20 Uncertainty in Measurement of Specific Heat Capacity by Differential Scanning Calorimetry H. Abe, H. Kato, N. Yamada

Std-3

10:20 – 10:40 BREAK 10:40 – 11:00 * Environmental Consciousness in Japan after the Great East Japan

Earthquake and Application to Thermal Analysis - Analysis using Eco-MCPS, a Web-database for Ecomaterials and Products R. Ozao, T. Utsumi, T. Ishii, Y. Shinohara, H. Kakisawa (SONY Institute of Higher Education)

Std-4



Organizers 9:00 – 9:20 Thermal Decomposition of Dicumyl Peroxide Decomposition by DSC

and VSP2 J. Chen, G. Shiue, M. Lee, C. Huang, C. Shu (Hsiuping University of Science and Technology)

BW-20

9:20 – 9:40 Isothermal Kinetics Evaluation of Cumene Hydroperoxide Mixed with Phenol for Autocatalytic Reaction via TAM III Test C. Huang, S. Liu, C. Shu (National Yunlin University of Science and Technology)

BW-21

9:40 – 10:00 Thermal Hazard Analysis and Thermal Stability Parameters Evaluation for Lauroyl Peroxide Mixed with H2O and Dry Fire-Extinguishing Chemicals by Novel Calorimetric Technology A. Li, C. Shu (National Yunlin University of Science and Technology)

BW-22

10:00 – 10:20 Evaluation of Incompatible Hazard for TBPO Mixed with Inorganic Acid or Base by Thermal Analysis Technology Y. Chang, C. Shu, Y. Tsai (National Yunlin University of Science and Technology)

BW-23


38

10:20 – 10:40 BREAK 10:40 – 11:00 Research into The Thermal Hazard Decomposition of 1,1-Bis(Tert-

Butylperoxy)Cyclohexane with Mineral Acid Contaminants K. Hsueh, R. Chang, C. Shu (Chung Hwa University of Medical Technology)

BW-24

11:00 – 11:20 Study on Thermal Hazards for Isoprene Mixed with Aluminum Oxide M. You, S. Weng, M. Liao, C. Jhu, Y. Tsai, C. Shu (Chienkuo Technology University)

BW-25

11:20 – 11:40 * Thermal Stability Analysis of Dicumyl Peroxide by Advance Kinetics-Based Simulation Approach N. Zang, X. Qian, C. Shu (State Key Laboratory of Explosion Science & Technology)

BW-26

11:40 – 12:00 Investigation of Thermal Instability of Phenol Process in the Presence of Reactants and Incompatibilities Y. Lin, S. Liu, H. Hou, S. Weng, Y. Yu, C. Shu (National Yunlin University of Science and Technology)

BW-27

Food and Pharmaceutical Meeting Room #1

Organizer: Prof. Etsuo Yonemochi, Hoshi University 9:00 – 9:20 Factors Affecting the Physical Stability of Amorphous Pharmaceutical

Formulations E. Yonemochi, Y. Yoshihashi, K. Terada (Hoshi University)

FnP-1

9:20 – 9:40 In Vivo Study of Kanamycin Encapsulated Gold Nanoparticles D. Pender, R. Dakshinamurthy (Western Kentucky University)

FnP-2

9:40 – 10:00 Synthesis, Characterization of Harnessed “Green” Gold Nanoparticles and Its Applications in Health and Environment R. Dakshinamurthy (Department of Chemistry, Western Kentucky University)

FnP-3

10:00 – 10:20 Molecular Level Interaction of Human Fibroblast Growth Factor-1 (hFGF-1) with Anti-Diabetic Drug R. Paripelli (Western Kentucky University)

FnP-4

10:20 – 10:40 BREAK 10:40 – 11:00 The Clopidogrel Bisulphate Polymorphy Characterization by

Modulated Differential Scanning Calorimetry K. Wang (Zhejiang University)

FnP-5


39

General Salon B

Organizer: Dr. Madhavi Vadlamudi, Exxon Mobil Research and Engineering

11:00 – 11:20 * Existence of Time Lag in Crystalline to Smectic A (K- SmA) Phase Transition of 4-Decyl-4-Biphenylcarbonitrile (10CB) Liquid Crystal D. Sharma (UML)

Gen-1

11:20 – 11:40 Liquid Crystals: From Dynamic Photonics to Solar Energy Q. Li (Kent State University)

Gen-2

11:40 – 12:00 * Environmentally Friendly Surfactant Additives for Nucleate Pool Boiling Enhancement B. Dikici, E. Edidiong (Embry Riddle Aronautical University)

Gen-3

Inorganic Materials Meeting Room #1

Organizer: Prof. Li-Xian Sun Dalian Institute 10:40 – 11:00 * Thermal Analytical Investigation of Fossiliferous Concretion of

Santana Formation H. Mothe Filho, C. Mothe (Departamento de Geociências/UFRRJ)

IoM-1

11:00 – 11:20 * Thermal Instability of Organic Carbonates with Discharged Cathode Materials in Lithium-Ion Battery J. Hsu, Y. Duh, C. Kao, W. Ou (Chia-Nan University of Pharmacy & Science)

IoM-2

11:20 – 11:40 Structural Phase Transition Behavior of Pr2NiO4+d and Nd2NiO4+d E. Niwa, K. Wakai, T. Hori, T. Nakamura, K. Yashiro, J. Mizusaki, T. Hashimoto (Nihon University)

IoM-3

11:40 – 12:00 Thermodynamic and Catalytic Study on Hydrogen Storage /Phase Change Materials L. Sun, F. Xu, H. Zhou, H. Chu, H. Zhang, Y. Zou, C. xiang, S. Qiu (Gunin University of Electronic Technology)

IoM-4

40

Author Index

Abe, H., Std-3 Achilias, D., Kin-8 Adams, T., GP-12, SCT-3 Alamo, R., BW-4., BW-12 Alexander, K., SCT-6 Al-Muntasheri, G., Kin-18 Al-Omari, M., Deg-12 Älvarez-García, A., SCT-8 Älvarez-García, B., SCT-8 An, L., SP-32 Anderson, B., BW-15 Annarapu, S., SP-7 Arii, T., GP-28, AIM-1 Artiaga, R., Kin-17, GP-19, SCT-8 Asberry, H., SP-28 Aubuchon, S., PNG-9, SCT-4 Avala, U., SP-26, TPM-9 Babinski, P., Kin-14 Badeen, C., Nrg-4 Barclay, T., Bio-3 Bente-Von Frowein, M., GP-18 Beta, I., SCT-5 Beyer, D., Deg-6 Biechele-Speziale, J., SP-29 Black, T., SP-22 Browne, J., SCT-4, PNG-9 Buchicchio, J., BW-15 Calado, V., GP-22, Kin-9 Cao, Y., Oxy-3, Oxy-8, SP-30, Oxy-4, SCT-10,

GP-2, TPM-11, Env-6, Env-5 Carvalho, C., SCT-9 Castro, P., GP-6 Cebe, P., Bio-4, BW-5, PNG-4, Pln-1 Celiz, L., GP-28., AIM-1 Chambers, A., Oxy-1 Chang, Y., SP-11, BW-23 Chang, R., BW-24, SP-9 Chang, S., Oxy-2 Chartoff, R., Kin-17 Chatterjee, P., SP-18 Chen, J., BW-20, SP-8 Chen, L., TPM-4 Cheng, Y., Deg-5 Cheng, S., BW-1 Chhetri, P., Deg-10 Chiu, P., Oxy-6

Chu, H., IoM-4 Chun, J., Kin-6 Comtois, E., GP-13 Crowley, S., Deg-1 Czerniecka, A., BW-7 Dai, L., SP-18 Dakshinamurthy, R., FnP-3, FnP-2 Daniel, Y., Deg-4 De Klerk, W., GP-9 De Puit, M., GP-9 Deng, H., PNG-1 Denner, T., SCT-2, GP-18, AIM-2, SCT-7 Dharavath, S., TPM-10 Dikici, B., Gen-3 Djoumaliisky, S., Kin-9 Dos Santos, I., SCT-6 Dubois, C., GP-13 Duh, Y., SP-12, AIM-7, GP-11, TPM-5, IoM-2,

GP-16, Nrg-7, GP-17 Eblen, M., TPM-2 Edidiong, E., Gen-3 Eldin, S., Std-2 El-Karsani, K., Kin-18 Endo, S., GP-27, AIM-5 Eng, W., SP-21, SP-22, SCT-12 Evans, C., PNG-1, BW-10 Farasat, R., GP-23, Kin-10 Favergeon, L., Kin-3 Feng, H., Nrg-4 Feng, Y., Oxy-2 Fischer, M., SCT-2, GP-18, AIM-2 Fisher, M., Deg-15 Folly, P., Nrg-13, Kin-12 Fontenot, S., Kin-17 Freitas, J., SP-13 Fujishiro, F., SP-19, Kin-2 Gomez-Barreiro, S., SCT-8 Gao, S., PNG-6 Gao, H., BW-8 Geissler, R., SCT-7 Geng, X., Env-6 Glorieux, C., TPM-8 Gonohe, N., GP-27 Goshi, Y., GP-10 Gracia-Fernandez, C., SCT-8, Kin-17 Grady, B., AIM-6

41

Grebowicz, J., BW-13, SP-20, SCT-11 Groeneveld, G., GP-9 Gröger, T., AIM-2, GP-18 Guns, S., GP-9 Guo, X., Oxy-7 Gutierrez, T., SP-31 Habu, H., Nrg-10 Hälldahl, L., Std-2 Han, X., Deg-11 Han, Z., SP-15 Harada, T., GP-29 Harris, A., TPM-3 Hartmann, M., Nrg-13, Kin-12 Hashimoto, T., Kin-2, SP-19, IoM-3 Hashimoto, T., TPM-7 Hay, B., Std-2 He, F., GP-8., Oxy-2 Hempel, E., AIM-3 Hood, M., TPM-10 Hori, T., IoM-3 Hossenlopp, J., Kin-4 Hou, H., SP-5., SP-6., BW-27 Howell, B, Deg-3, Deg-2, Deg-4, Deg-7, Deg-8,

Deg-10, Deg-11, Deg-12, Deg-13, Deg-14, Deg-15, Deg-6

Hrma, P., Kin-6 Hsieh, C., GP-20 Hsieh, T., GP-16, GP-17 Hsieh, T., SP-9 Hsu, J., GP-11, Nrg-7, TPM-5, IoM-2, GP-17 Hsueh, K., BW-24 Hu, X., GP-5, Bio-2, BW-15 Hu, W., BW-8 Huang, C., BW-21, SP-8, BW-20 Huang, Z., Oxy-2 Huang, H., GP-1, Nrg-2 Hussein, I., Kin-18 Ishii, T., Std-4 Ison, G., SP-10 Jaco, Z., SCT-11 Jaffe, M., Bio-1, BW-3 Janani, H., BW-4 Javangula, H., SP-27, TPM-6 Jentoft, R., AIM-6 Jhu, C., BW-25 Jiang, C., SP-32

Jiang, H., SP-18 Jiao, Q., GP-1, Nrg-2, TPM-4 Jyunichiro, T., GP-30 Kaisersberger, E., SCT-7 Kakisawa, H., Std-4 Kao, C., GP-11, SP-12, AIM-7, TPM-5, IoM-2,

GP-16, Nrg-7, GP-17 Kasyap, S., BW-19 Kato, H., Std-3 Kawakami, K., GP-29 Kessler, M., BW-16 Kherde, Y., Env-3 Kirsh, J., SCT-12 Koennecke, K., Std-2 Koga, N., GP-10, Kin-16 Koh, Y., PNG-6, PNG-8 Kolanka, V., SP-30 Kosman, J., Deg-6 Kota, P., SP-22 Kozawz, S., SP-21, SP-22, SCT-12 Krongauz, V., Kin-13 Ksepko, E., Oxy-5 Ku, Y., Oxy-6 Kwasny, R., AIM-4 Kwok, Q., Nrg-4 Labojko, G., GP-14, Kin-14, Oxy-5 Lad, K., Kin-19 Lazar, S., Deg-13 Le ParlouËR, P., Std-2 Lee, M., SP-8, BW-20 Leite, L., PNG-10 Lella, D., SP-2 Lesley, M., Bio-5, Nrg-6 Lesley , M., Nrg-6 Leys, J., TPM-8 Li, A., BW-22 Li, B., TPM-11 Li, C., BW-14 Li, H., Oxy-2 Li, K., Bio-4 Li, Q., Gen-2 Li, R., Oxy-7 Li, Y., Nrg-7 Li, Y., BW-16 Liao, M., BW-25 Lin, Y., SP-24

42

Lin, Y., BW-27, SP-6, SP-5 Lin, H., TPM-11 Linder, M., Kin-5 Lineberry, Q., TPM-6, TPM-9 Ling, M., Kin-13 Liu, H., GP-24 Liu, Q., Env-6 Liu, S., SP-5, SP-6, BW-21, BW-27 Liu, Y., AIM-6 Liu, Z., SP-15, SP-16, Env-5 Lobo, H., Std-2 Lopez, E., PNG-3 López Beceiro, J., Kin-17, GP-19, SCT-8 Losada-Pérez, P., TPM-8 Lu, C., SP-23 Lyon, R., Kin-11, Deg-1 Ma, Q., BW-5 Ma, T., SP-18 Machingauta, C., Kin-4 Maheswaram, M., SCT-6 Mantheni, D., SCT-6 Mao, B., PNG-4, BW-5 Matisons, J., Bio-3 Matsunaga, H., Nrg-10 Matuschek, G., SCT-2 Mazzi, S., BW-15 Mcdade, A., Env-3 Mcnulty, J., SP-21 Melin, J., Bio-5, Nrg-6 Menczel, J., BW-2 Mikek, K., Deg-14 Min, F., SP-1 Mishima, Y., SCT-1 Miyake, A., Nrg-5, Nrg-10, Nrg-1 Mizusaki, J., IoM-3 Mohomed, K., PNG-9, SCT-4 Molenda, M., Kin-5 Morikawa, J., TPM-7, Std-2 Mothe, C., SP-13, SP-14, Bio-7, PNG-10, SCT-

9, IoM-1, SP-31 Mothe, M., PNG-10, SCT-9, SP-31, SP-14 Mothe Filho, H., GP-6, IoM-1 Mulamba , O., Nrg-3 Muralidharan, K., Nrg-12 Muzny, C., Std-1 Nakamura, T., IoM-3

Naya, S., GP-19 Nee, M., SP-7 Nian, Y., SP-15 Nicula, R., PNG-7 Nie, Y., BW-8 Nishimoto, Y., GP-26, Env-1 Niwa, E., IoM-3, SP-19, Kin-2 O'connell, J., Kin-13 Ogawa, K., GP-30 Oikawa, N., GP-27 Okabe, T., GP-30 Okachi, Y., GP-30 Okiba, T., SP-19 Orndorff, W., Env-6, Env-5 Ou, W., GP-11, IoM-2 Oxley, J., Nrg-8 Ozao, R., Std-4 Pan, W., Oxy-4, SCT-10, GP-2, SP-30, Oxy-3,

SP-16, Env-6, Env-5 Pan, Y., SP-18 Paripelli, R., FnP-4, SP-10 Park, D., SP-22 Patel, A., PNG-11, BW-19 Paula, P., SP-14 Pender, D., FnP-2 Pereira Jr., N., GP-22 Pijolat, M., Kin-1, Kin-3 Pinto, M., PNG-10 Plis, A., GP-14, Kin-14 Pontes, R., GP-13 Popescu, C., Deg-9 Porter, M., Nrg-8 Pospiech, D., BW-6 Post, E., AIM-2 Prado, J., GP-7 Prajapati, S., PNG-11 Pratap, A., Kin-19, PNG-11, BW-19 Pyda, M., BW-7, BW-5 Qian, X., BW-26 Qiu, S., IoM-4 Rao, T., Kin-19 Ren, H., GP-1, Nrg-2 Rettinger, R., Nrg-8 Rides, M., Std-2 Riga, A., SCT-6, SCT-12, Env-7, TPM-9, SP-

22, SP-21

43

Rios Fachal, M., GP-19 Rodriguez, C., Kin-6 Roduit, B., Nrg-13, Kin-12 Rouchon, L., Kin-3 Safronava, N., Kin-11 Sairiala, M., Nrg-9 Sakamoto, K., Nrg-11 Salazar, Y., SP-20 Saraji-Bozorgzad, M., GP-18, SCT-7, SCT-2,

AIM-2 Sarbach, A., Nrg-13, Kin-12 Sato, R., Kin-2 Schawe, J., PNG-5, BW-11, AIM-3 Schick, C., PNG-7, BW-6, GP-15 Schweiger, M., Kin-6 Sciazko, M., Oxy-5 Sevinc, Z., GP-3, GP-4 Shah, M., Env-4 Shapiro, P., SCT-5 Sharma, D., BW-18, Gen-1 Shen, S., SP-4 Shevde, H., Kin-19 Shimada, K., GP-27 Shinohara, Y., Std-4 Shiu, S., Oxy-6 Shiue, G., SP-8, BW-20 Shu, C., BW-22, BW-23, SP-11, BW-17, BW-

21, BW-24, BW-26, SP-3, SP-4, SP-9, SP-8, BW-20, SP-5, SP-6, BW-25, BW-27

Silva, F., GP-22 Simon, S., SP-17, PNG-2, PNG-3, PNG-8,

PNG-6 Sims, J., Bio-5, Nrg-6 Singh, S., Nrg-4 Sit, S., Oxy-3 Smith, J., Nrg-8 Smith, P., Deg-6, Deg-2 Song, C., SP-32 Song, N., Env-5 Song, M., SP-22, SP-21, SCT-12 Stevens, C., SP-2 Stevens, E., SP-18 Streibel, T., SCT-7 Strobel, C., GP-3 Sugie, Y., Nrg-5 Sui, Z., SP-16

Sultan, A., Kin-18 Sun, L., GP-24, GP-25, Bio-6, IoM-4 Sun, W., Deg-8 Sun, Y., Oxy-7 Sun, Y., GP-17, GP-16 Sun, Z., SP-32 Tan, A., PNG-1 Tao, R., SP-17, PNG-2 Tarro-Saavedra, J., GP-19 Tatsuoka, T., GP-10 Tedesco, M., SP-22 Teng, Y., SP-16, Env-5, SP-32 Terada, K., FnP-1, GP-29 Thieme, C., Deg-6 Thoen, J., TPM-8 Tong, J., BW-17 Torkelson, J., PNG-1, BW-10 Tsai, F., SP-3 Tsai, Y., SP-3, SP-9, SP-11, BW-17, SP-4, BW-

23, BW-25 Tsugoshi, T., SCT-1 Turcotte, R., Nrg-4 Turpeinen, E., Nrg-9 Utsumi, T., Std-4 Vadlamudi, M., BW-12, GP-15 Vakiti, R., GP-2 Van Der Heijden, A., GP-9 Vargeese, A., Nrg-12 Varma-Nair, M., GP-15 Vaucher, S., PNG-7 Vyazovkin, S., Kin-15, GP-7, GP-23, Kin-7,

Kin-10 Wakai, K., IoM-3 Walker, A., SP-21 Walte, A., SCT-7, GP-18, AIM-2 Walters, R., Deg-1 Wang, K., FnP-5 Wang, T., SP-4 Wang, W., AIM-7 Wang, X., BW-9 Webb, C., SP-30, GP-2 Weng, S., SP-5, BW-25, BW-27, SP-6 Wen-Lian, L., TPM-5 Wingard, D., TPM-1 Wohlfahrt, S., SCT-2 Wörner, A., Kin-5

44

Wu, D., SP-15 Wu, H., GP-20 Wu, H., Oxy-6 Wu, S., SP-12 Wurm, A., PNG-7, BW-6, GP-15 Xiang, C., Bio-6, IoM-4 Xiang, M., TPM-4 Xu, D., SP-32 Xu, F., GP-24, GP-25, IoM-4, Bio-6 Xu, H., SP-32 Xue, G., BW-9 Yamada, N., Std-3 Yan, B., GP-2, SP-2 Yancey, B., Kin-7, Kin-10 Yang, F., Oxy-7 Yang, L., GP-21 Yang, W., GP-20 Yashiro, K., IoM-3 Yo, J., TPM-5 Yonemochi, E., GP-29, FnP-1 Yoshida, H., Pln-3 Yoshihashi, Y., FnP-1, GP-29 Yoshiizumi, M., GP-27 Yoshikawa, M., Kin-16, GP-10 Yoshino, S., Nrg-11 Yoshizawa, R., Kin-2 You, M., BW-25, SP-3 Yu, J., TPM-4 Yu, Y., SP-6, SP-5, BW-27 Yuan, X., SP-25 Zang, N., BW-26 Zaragoza-Fernández, S., SCT-8 Zemo, M., AIM-3 Zhang, H., GP-25, IoM-4 Zhang, K., SP-16 Zhang, L., Deg-7 Zhang, M., SP-1 Zhang, R., Env-2 Zhang, T., Deg-2 Zhang, Y., Env-5, Env-6 Zhao, H., Oxy-4, SCT-10, Oxy-3 Zhao, K., Oxy-2 Zheng, A., Oxy-2 Zhong, L., SP-16, SP-32 Zhou, D., BW-9 Zhou, H., IoM-4

Zhu, W., TPM-11 Zhu, Y., Nrg-2, GP-1, TPM-4 Zhu, Y., PNG-4 Zhuravlev, E., GP-15, BW-6 Zimmermann, R., SCT-2, GP-18, AIM-2, SCT-

7 Zou, Y., Bio-6, IoM-4 Zulker, E., BW-15 Zvetkov, V., Kin-9

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technical program of the 41th north american thermal … · 2016. 6. 29. · yoshida (tokyo...

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