test report...test report report no. scl01i118709 report issued date : page 2 of 14 jan. 5, 2017...

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Test Report Report No. SCL01I118709 Report Issued Date : Page 1 of 14 Jan. 5, 2017 The following sample(s) and sample information was/were submitted and identified by/on the behalf of the client Sample Description 1000HNX Hardener Amount of Sample 2 oz Buyers Name / Division Adidas Apparel INKCUPS NOW CORPS 310 ANDOVER STREET DANVERS MA 01923, USA Applicant & Address Contact Person Joe S. Tel No. 978-646-8980 Mail Box [email protected] Pass Summary Report Failure Test Items --- Age Group Adults/Infants/Children Material Name/ Code 1000HNX Hardener Color Name/ Code --- Supplier Name --- Country of Origin --- Country of Destination --- Material Component --- Sample Classification Miscellaneous&Others Material key code under adidas-Group A-01 test standard (2016) 509&Cement RSL based on The adidas-Group A-01 RSL (2016) Report Type (FT) Full Test Report No. --- P.O. No. --- Item No. --- Additional Information Size:S-XXL Sample Received Date Dec. 30, 2016 Testing Period Dec. 30, 2016 to Jan. 5, 2017 Full Test (FT)/ First Order (FO)/ Separate Colors (SC*)/ New version update test items (NT*)/ Improvement Test (IT*)/ Random Test (RT)/ Supplier Internal (SI)/ Special Test (ST*) Tested by Approved by Reviewed by Date Jan. 5, 2017 No. S198449155 Yanna Cao Lab Manager Centre Testing International Group Co.,Ltd. Hongwei Industrial Zone, Baoan 70 District, Shenzhen, Guangdong, China

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Page 1: Test Report...Test Report Report No. SCL01I118709 Report Issued Date : Page 2 of 14 Jan. 5, 2017 Summary of Test Result(s) Test Item(s) Pre-Treatment Test Method Test Result/ Conclusion

Test Report Report No. SCL01I118709

Report Issued Date :

Page 1 of 14

Jan. 5, 2017

The following sample(s) and sample information was/were submitted and identified by/on the behalf of the client

Sample Description 1000HNX Hardener Amount of Sample 2 oz Buyer’s Name / Division Adidas Apparel

INKCUPS NOW CORPS 310 ANDOVER STREET DANVERS MA 01923, USA

Applicant & Address

Contact Person Joe S. Tel No. 978-646-8980 Mail Box [email protected]

Pass Summary Report Failure Test Items --- Age Group Adults/Infants/Children Material Name/ Code 1000HNX Hardener Color Name/ Code --- Supplier Name --- Country of Origin --- Country of Destination --- Material Component --- Sample Classification Miscellaneous&Others Material key code under adidas-Group A-01 test standard (2016)

509&Cement

RSL based on The adidas-Group A-01 RSL (2016) Report Type (FT) Full Test Report No. --- P.O. No. --- Item No. --- Additional Information Size:S-XXL

Sample Received Date Dec. 30, 2016 Testing Period Dec. 30, 2016 to Jan. 5, 2017 Full Test (FT)/ First Order (FO)/ Separate Colors (SC*)/ New version update test items (NT*)/ Improvement Test (IT*)/ Random Test (RT)/ Supplier Internal (SI)/ Special Test (ST*)

Tested by

Approved by

Reviewed by

Date Jan. 5, 2017

No. S198449155Yanna Cao

Lab Manager Centre Testing International Group Co.,Ltd. Hongwei Industrial Zone, Bao’an 70 District, Shenzhen, Guangdong, China

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Test Report Report No. SCL01I118709

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Summary of Test Result(s)

Test Item(s) Pre-Treatment Test Method Test Result/ Conclusion

PASS Cadmium-Extraction DIN EN ISO 11885 (2009) DIN EN ISO 105-E04 (2013) in acid solution (1 hour extraction with 37℃)

PASS Cadmium-Total DIN EN ISO 11885 (2009) Microwave digestion

PASS Chromium-Extraction DIN EN ISO 11885 (2009) DIN EN ISO 105-E04 (2013) in acid solution (1 hour extraction with 37℃)

PASS Lead-Extraction DIN EN ISO 11885 (2009) DIN EN ISO 105-E04 (2013) in acid solution (1 hour extraction with 37℃)

PASS Lead-Total DIN EN ISO 11885 (2009) Non-metal parts:Microwave digestion with H2O2 /HNO3 (or HF in case of silicone polymers) ;Metal parts:Aqua regia

PASS Mercury-Extraction DIN EN ISO 12846(2012) DIN EN ISO 105-E04 (2013) in acid solution (1 hour extraction with 37℃)

PASS Formaldehyde DIN EN ISO 14184-1, (2011)

PASS ΣPentachlorophenol (PCP), Tetrachlorophenol (TeCP) and Trichlorophenol (TriCP)

GCMS Extraction with KOH

PASS o-Phenylphenol (o-PP) GCMS Extraction with KOH

PASS Dibutyltin (DBT) ISO/TS 16179 (2012)

PASS Dioctyltin (DOT) ISO/TS 16179 (2012)

PASS Tributyltin (TBT) ISO/TS 16179 (2012)

PASS Triphenyltin (TPhT) ISO/TS 16179 (2012)

PASS Monobutyl Tin (MBT) ISO/TS 16179 (2012)

PASS Monooctyltin (MOT) ISO/TS 16179 (2012)

PASS Trioctyltin (TOT) ISO/TS 16179 (2012)

PASS Σ of NP, OP, NPEO, OPEO NP,OP: GCMS or LCMS NPEO,OPEO: DIN EN ISO 18254-1:2016-09

NP,OP:Extraction with THF;NPEO,OPEO:DIN EN ISO 18254-1:2016-09

N/A Azo-Amines prEN ISO 14362-1 :2015&prEN ISO 14362-3 :2015

PASS Σ Phthalates GCMS Extraction with THF with ASE or Soxhlet

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N/A Regulated Polycyclic Aromatic Hydrocarbons (PAHs) of high concern

AfPS GS 2014:01 AfPS GS 2014:01

N/A Σ of Polycyclic Aromatic Hydrocarbons (PAHs)

AfPS GS 2014:01 AfPS GS 2014:01

N/A Disperse Dyes and Dyestuffs DIN 54231 (2005)

PASS Benzene Solvent Extraction, Analysis by Headspace GCMS/ GCMS/ HPLC

PASS Phenol DIN EN 71-10(2006)

PASS Tetrachloroethane Solvent Extraction, Analysis by Headspace GCMS/ GCMS/ HPLC

PASS Toluene Solvent Extraction, Analysis by Headspace GCMS/ GCMS/ HPLC

PASS Xylene Solvent Extraction, Analysis by Headspace GCMS/ GCMS/ HPLC

PASS Trichloroethylene Solvent Extraction, Analysis by Headspace GCMS/ GCMS/ HPLC

PASS Tetrachloroethylene Solvent Extraction, Analysis by Headspace GCMS/ GCMS/ HPLC

PASS Dichloromethane Solvent Extraction, Analysis by Headspace GCMS/ GCMS/ HPLC

PASS Methylphenol Solvent Extraction, Analysis by Headspace GCMS/ GCMS/ HPLC

PASS Dimethylformamide (DMFA) Solvent Extraction, Analysis by Headspace GCMS/ GCMS/ HPLC

PASS Trichloromethane (Chloroform) Solvent Extraction, Analysis by Headspace GCMS/ GCMS/ HPLC

PASS Cyclohexane Solvent Extraction, Analysis by Headspace GCMS/ GCMS/ HPLC

PASS THF Solvent Extraction, Analysis by Headspace GCMS/ GCMS/ HPLC

PASS Σ Short Chained Chloroparaffines C10 to C13 (SCCP)

DIN EN ISO 18219(2016-02)

Note: Photo of submitted sample appendix was included.

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Photo(s) of the sample(s)

************ For Further Details, Please Refer To the Following Page(s) *************

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Test Conducted (As Requested By The Client)

Cadmium-Extraction 1

Test Result (mg/kg) Threshold Limit Value (TLV) (mg/kg)

Test Item(s) 001*

MDL (mg/kg)

0.1 0.02 N.D. Cadmium-Extraction

Cadmium-Total 2

Test Result (mg/kg) Threshold Limit Value (TLV) (mg/kg)

Test Item(s) 001*

MDL (mg/kg)

40 5 N.D. Cadmium-Total

3 Chromium-Extraction

Tested Item(s) Test Result (mg/kg)

MDL (mg/kg) Threshold Limit Value (TLV) (mg/kg) 001*

Chromium-Extraction N.D. 0.02 Adults:2 Infants:1

4 Lead-Extraction

Tested Item(s) Test Result (mg/kg)

MDL (mg/kg) Threshold Limit Value (TLV) (mg/kg) 001*

Lead-Extraction N.D. 0.02 Adults:1 Infants:0.2

Lead-Total 5

Test Result (mg/kg) Threshold Limit Value (TLV) (mg/kg)

Test Item(s) 001*

MDL (mg/kg)

40 5 N.D. Lead-Total

Mercury-Extraction 6

Test Result (mg/kg) Threshold Limit Value (TLV) (mg/kg)

Test Item(s) 001*

MDL (mg/kg)

0.02 0.01 N.D. Mercury-Extraction

Formaldehyde 7

Test Result (mg/kg) Threshold Limit Value (TLV) (mg/kg)

Test Item(s) 001

MDL (mg/kg)

13 13 N.D. Formaldehyde

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ΣPentachlorophenol (PCP), Tetrachlorophenol (TeCP) and Trichlorophenol (TriCP) 8

Test Result (mg/kg) Threshold Limit Value (TLV) (mg/kg)

Test Item(s) 001

MDL (mg/kg)

Adults: 0.5 Infants: 0.05

0.05 N.D. Pentachlorophenol (PCP)

0.05 N.D. 2.3.5.6-Tetrachlorophenol

0.05 N.D. 2.3.4.6-Tetrachlorophenol

0.05 N.D. 2.3.4.5-Tetrachlorophenol

0.05 N.D. 2.4.6-Trichlorophenol

0.05 N.D. 2.3.6-Trichlorophenol

0.05 N.D. 2.3.5-Trichlorophenol

0.05 N.D. 2.4.5-Trichlorophenol

0.05 N.D. 2.3.4-Trichlorophenol

0.05 N.D. 3.4.5-Trichlorophenol

9 o-Phenylphenol (o-PP)

Tested Item(s) Test Result (mg/kg)

MDL (mg/kg) Threshold Limit Value (TLV) (mg/kg) 001

o-Phenylphenol (o-PP) N.D. 0.5 Adults:1000 Infants: 500

Dibutyltin (DBT) 10

Test Result (mg/kg) Threshold Limit Value (TLV) (mg/kg)

Test Item(s) 001

MDL (mg/kg)

1 0.05 N.D. Dibutyltin(DBT)

Dioctyltin (DOT) 11

Test Result (mg/kg) Threshold Limit Value (TLV) (mg/kg)

Test Item(s) 001

MDL (mg/kg)

1 0.05 N.D. Dioctyltin (DOT)

Tributyltin (TBT) 12

Test Result (mg/kg) Threshold Limit Value (TLV) (mg/kg)

Test Item(s) 001

MDL (mg/kg)

0.05 0.025 N.D. Tributyltin(TBT)

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13 Triphenyltin (TPhT)

Tested Item(s) Test Result (mg/kg) MDL (mg/kg) Threshold Limit Value (TLV) (mg/kg) 001

Triphenyltin (TPhT) N.D. 0.05 Adults:1 Infants: 0.5

Monobutyl Tin (MBT) 14

Test Result (mg/kg) Threshold Limit Value (TLV) (mg/kg)

Test Item(s) 001

MDL (mg/kg)

1 0.05 N.D. Monobutyltin(MBT)

Monooctyltin (MOT) 15

Test Result (mg/kg) Threshold Limit Value (TLV) (mg/kg)

Test Item(s) 001

MDL (mg/kg)

1 0.05 N.D. Monooctyltin(MOT)

Trioctyltin (TOT) 16

Test Result (mg/kg) Threshold Limit Value (TLV) (mg/kg)

Test Item(s) 001

MDL (mg/kg)

1 0.05 N.D. Trioctyltin(TOT)

Σ of NP, OP, NPEO, OPEO 17

Test Result (mg/kg) Threshold Limit Value (TLV) (mg/kg)

Test Item(s) 001

MDL (mg/kg)

250 (10 for NP,OP as single

parameters)

10 N.D. Octylphenol(OP)

10 N.D. Nonylphenol(NP)

50 N.D. Octylphenol Ethoxylate(OPEO)

50 N.D. Nonylphenol Ethoxylate(NPEO)

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Azo-Amines 18

Test Item(s) 001

Test Result (mg/kg) Cas No. MDL (mg/kg)

N/A 5 137-17-7 2,4,5-trimethylaniline

N/A 5 615-05-4 2,4-diaminoanisole

N/A 5 95-80-7 2,4-diaminotoluene

N/A 5 95-68-1 2,4-xylidine

N/A 5 87-62-7 2,6-xylidine

N/A 5 90-04-0 2-methoxyaniline

N/A 5 91-59-8 2-naphthylamine

N/A 5 91-94-1 3,3'-dichlorobenzidine

N/A 5 119-90-4 3,3'-dimethoxybenzidine

N/A 5 119-93-7 3,3'-dimethylbenzidine

N/A 5 101-77-9 4,4'-diaminodiphenylmethane

N/A 5 101-14-4 4,4'-methylene-bis-(2-chloro-aniline)

N/A 5 838-88-0 4,4'-methylenedi-o-toluidine

N/A 5 101-80-4 4,4'-oxydianiline

N/A 5 139-65-1 4,4'-thiodianiline

N/A 5 60-09-3 4-aminoazobenzene

N/A 5 92-67-1 4-aminobiphenyl

N/A 5 95-69-2 4-chloro-o-toluidine

N/A 5 106-47-8 4-chloroaniline

N/A 5 99-55-8 5-nitro-o-toluidine

N/A 5 120-71-8 6-methoxy-m-toluidine

N/A 5 92-87-5 Benzidine

N/A 5 97-56-3 o-aminoazotoluene

N/A 5 95-53-4 o-toluidine

Threshold Limit Value(TLV) = 20 mg/kg

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Σ Phthalates 19

Test Result (mg/kg) Threshold Limit Value (TLV) (mg/kg)

Test Item(s) 001*

MDL (mg/kg)

500

50 N.D. Dibutylphthalate (DBP)

50 N.D. Butylbenzylphthalate (BBP)

50 N.D. Di(2-ethylhexyl)-phthalate (DEHP)

50 N.D. Di-n-octylphthalate (DNOP)

50 N.D. Di-Iso-nonylphthalate (DINP)

50 N.D. Diisodecylphthalate (DIDP)

50 N.D. Diisobutylphthalate (DIBP)

100 N.D. Di-C6-8-branched alkylphthalates(DIHP)

100 N.D. Di-C711-branched alkylphthalates(DHNUP)

50 N.D. Di-n-hexylphthalate(DHP)

50 N.D. Di-(2-methoxymethyl)-phthalate(DMEP)

50 N.D. Di-n-Pentyl Phthalate (DPP)

50 N.D. Dicyclohexyl phthalate(DCHP)

Regulated Polycyclic Aromatic Hydrocarbons (PAHs) of high concern 20

Test Result (mg/kg) Threshold Limit Value (TLV) (mg/kg)

Test Item(s) 001

MDL (mg/kg)

1 0.2 N/A Benzo(a)anthracene

1 0.2 N/A Chrysene

1 0.2 N/A Benzo(b)fluoranthene

1 0.2 N/A Benzo(k)fluoranthene

1 0.2 N/A Benzo(a)pyrene

1 0.2 N/A Dibenzo(a,h)anthracene

1 0.2 N/A Benzo (j) fluoranthene

1 0.2 N/A Benzo (e) pyrene

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Σ of Polycyclic Aromatic Hydrocarbons (PAHs) 21

Test Result (mg/kg) Threshold Limit Value (TLV) (mg/kg)

Test Item(s) 001

MDL (mg/kg)

10

0.2 N/A Naphthalene

0.2 N/A Acenaphthylene

0.2 N/A Acenaphthene

0.2 N/A Fluorene

0.2 N/A Phenanthrene

0.2 N/A Anthracene

0.2 N/A Fluoranthene

0.2 N/A Pyrene

0.2 N/A Benzo[a]anthracene

0.2 N/A Chrysene

0.2 N/A Benzo[b]fluoranthene

0.2 N/A Benzo[k]fluoranthene

0.2 N/A Benzo[a]pyrene

0.2 N/A Indeno[1,2,3-cd]pyrene

0.2 N/A Dibenzo[a,h]anthracene

0.2 N/A Benzo[g,h,i]perylene

0.2 N/A Benzo[j]fluoranthene

0.2 N/A Benzo[e]pyrene

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Disperse Dyes and Dyestuffs 22

001

Test Result (mg/kg) MDL (mg/kg) Test Item(s) C.I. No. Cas No.

N/A 15 16150 3761-53-3 Acid Red 26

N/A 15 30235 1937-37-7 Basic Black 38

N/A 15 42500 569-61-9 Basic Red 9

N/A 15 42510 632-99-5 Basic Violet 14

N/A 15 22610 2602-46-2 Direct Blue 6

N/A 15 22120 573-58-0 Direct Red 28

N/A 15 64500 2475-45-8 Disperse Blue 1

N/A 15 / 12222-97-8 Disperse Blue 102

N/A 15 / 12223-01-7 Disperse Blue 106

N/A 15 / 61951-51-7 Disperse Blue 124

N/A 15 63305 3860-63-7 Disperse Blue 26

N/A 15 61505 2475-46-9 Disperse Blue 3

N/A 15 / 12222-75-2 Disperse Blue 35

N/A 15 62500 3179-90-6 Disperse Blue 7

N/A 15 / 23355-64-8 Disperse Brown 1

N/A 15 11080 2581-69-3 Disperse Orange 1

N/A 15 60700 82-28-0 Disperse Orange 11

N/A 15 / 85136-74-9 Disperse Orange 149

N/A 15 11005 730-40-5 Disperse Orange 3

N/A 15 / 12223-33-5/13301-61-6/5181

1-42-8

Disperse Orange 37/59/76

N/A 15 11110 2872-52-8 Disperse Red 1

N/A 15 62015 2872-48-2 Disperse Red 11

N/A 15 11210 3179-89-3 Disperse Red 17

N/A 15 10345 119-15-3 Disperse Yellow 1

N/A 15 26070 6250-23-3 Disperse Yellow 23

N/A 15 11855 2832-40-8 Disperse Yellow 3

N/A 15 / 12236-29-2 Disperse Yellow 39

N/A 15 / 54824-37-2 Disperse Yellow 49

N/A 15 10375 6373-73-5 Disperse Yellow 9

Threshold Limit Value(TLV) = 50 mg/kg

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Benzene 23

Test Result (mg/kg) Threshold Limit Value (TLV) (mg/kg)

Test Item(s) 001

MDL (mg/kg)

5 1 N.D. Benzene

Phenol 24

Test Result (mg/kg) Threshold Limit Value (TLV) (mg/kg)

Test Item(s) 001

MDL (mg/kg)

15 5 N.D. Phenol

Tetrachloroethane 25

Test Result (%) Threshold Limit Value (TLV) (%)

Test Item(s) 001

MDL (%)

0.1 0.001 N.D. Tetrachloroethane

Toluene 26

Test Result (%) Threshold Limit Value (TLV) (%)

Test Item(s) 001

MDL (%)

0.1 0.001 N.D. Toluene

Xylene 27

Test Result (%) Threshold Limit Value (TLV) (%)

Test Item(s) 001

MDL (%)

0.1 0.001 N.D. Xylene

Trichloroethylene 28

Test Result (%) Threshold Limit Value (TLV) (%)

Test Item(s) 001

MDL (%)

0.1 0.001 N.D. Trichloroethylene

Tetrachloroethylene 29

Test Result (%) Threshold Limit Value (TLV) (%)

Test Item(s) 001

MDL (%)

0.1 0.001 N.D. Tetrachloroethylene

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Dichloromethane 30

Test Result (%) Threshold Limit Value (TLV) (%)

Test Item(s) 001

MDL (%)

0.1 0.001 N.D. Dichloromethane

Methylphenol 31

Test Result (%) Threshold Limit Value (TLV) (%)

Test Item(s) 001

MDL (%)

0.1 0.001 N.D. Methylphenol

Dimethylformamide (DMFA) 32

Test Result (%) Threshold Limit Value (TLV) (%)

Test Item(s) 001

MDL (%)

0.1 0.001 N.D. Dimethylformamide (DMFA)

Trichloromethane (Chloroform) 33

Test Result (%) Threshold Limit Value (TLV) (%)

Test Item(s) 001

MDL (%)

0.1 0.001 N.D. Trichloromethane (Chloroform)

Cyclohexane 34

Test Result (%) Threshold Limit Value (TLV) (%)

Test Item(s) 001

MDL (%)

0.1 0.001 N.D. Cyclohexane

THF 35

Test Result (%) Threshold Limit Value (TLV) (%)

Test Item(s) 001

MDL (%)

0.1 0.001 N.D. THF

Σ Short Chained Chloroparaffines C10 to C13 (SCCP) 36

Test Result (mg/kg) Threshold Limit Value (TLV) (mg/kg)

Test Item(s) 001

MDL (mg/kg)

1000 100 N.D. Σ Short Chained Chloroparaffines C10 to C13 (SCCP)

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Remark: -MDL = Method Detection Limit

-N.D. = Not Detected (<MDL)

-mg/kg = ppm = parts per million

-N/A = Not Applicable -*= As specified by the client, the test result(s) was/ were based on the dry weight of the submitted sample(s).The result is to be calculated on a dry weight basis.

Tested Sample/Part Description 001 Transparent ink(1000HNX Hardener)

*** End of Report *** The test report is effective only with both signature and specialized stamp, The result(s) shown in this report refer only to the sample(s) tested. Without written approval of CTI, this report can’t be reproduced except in full.