tlc2 potem absorb ccc1,2 tlc1 sa,aas

AAS-ASINDICEAS mg/25 mlg/100 mlA278A308SA A278SA A3080.10.00040.0250.123A11(g/100ml)=58.167304.76pendiente0.30.00120.0670.354a=A11/10=5.816730.4760.50.0020.1150.587MW=138.1138.1304.762569832410.0040.2341.217e=A11*MW/10=803.286274208.7356AAS mg/25ml.AAS A278AAS A3080.50.0020.1590.015A11(g/100ml)=76.017410.0040.3050.018a=A11/10=7.60170.41.50.0060.4560.026MW=180.2180.220.0080.6060.039e=A11*MW/10=1369.8263472.08

AAS-AS

AS, 278 nmA1cm1%(p/v)

%T-A-ABSORCION

A1cm1%(p/v)

BHT-MASSLAB-MSC32INDICEAbsorcin %%TAbsorbanciaintroducir valor"=SUMA(100;-(A2))""=2-LOG10(B2)"75250.602059991310900.04575749064960.017728767

INDICE

A-T%INDICE293.E+042.90E+01,3.10E+04413.E+044.10E+01,2.60E+04531.E+045.30E+01,1.00E+04553.E+045.50E+01,3.40E+04561.E+045.60E+01,1.40E+04577.E+045.70E+01,6.80E+04581.E+045.80E+01,1.10E+04672.E+046.70E+01,2.10E+04771.E+047.70E+01,1.00E+04791.E+047.90E+01,1.00E+04806.E+038.00E+01,6.00E+03813.E+048.10E+01,2.80E+04835.E+038.30E+01,5.00E+03911.E+049.10E+01,1.40E+04935.E+039.30E+01,5.00E+03952.E+049.50E+01,1.50E+041052.E+041.05E+02,1.70E+041159.E+031.15E+02,9.00E+031164.E+031.16E+02,4.00E+031175.E+031.17E+02,5.00E+031191.E+041.19E+02,1.00E+041218.E+031.21E+02,8.00E+031286.E+031.28E+02,6.00E+031296.E+031.29E+02,6.00E+031303.E+031.30E+02,3.00E+031318.E+031.31E+02,8.00E+031336.E+031.33E+02,6.00E+031353.E+031.35E+02,3.00E+031415.E+031.41E+02,5.00E+031424.E+031.42E+02,4.00E+031432.E+031.43E+02,2.00E+031453.E+041.45E+02,2.60E+041464.E+031.46E+02,4.00E+031474.E+031.47E+02,4.00E+031498.E+031.49E+02,8.00E+031572.E+031.57E+02,2.00E+031594.E+031.59E+02,4.00E+031617.E+031.61E+02,7.00E+031635.E+031.63E+02,5.00E+031753.E+031.75E+02,3.00E+031771.E+041.77E+02,1.40E+041891.E+041.89E+02,1.00E+041912.E+031.91E+02,2.00E+032032.E+032.03E+02,2.00E+032053.E+052.05E+02,2.55E+052064.E+042.06E+02,3.90E+042075.E+032.07E+02,5.00E+032192.E+032.19E+02,2.00E+032207.E+042.20E+02,7.00E+042211.E+042.21E+02,1.20E+04

INDICE

ConcentracionINDICE10120.00000000015010060.0001-410.00499.08319448931.2176.06736329590.7830.50.00299.54054173520.58725.88212915151.4130.30.001299.72407117420.35444.25883723631.6460.10.000499.90793899840.12375.33555637341.877AT%AT%

Concentracion

A-neta

AAS-plomo

IR-mtodosINDICECL40AH0.42CMAM0.650.01080.04CH80AL0.850.01030.106Este clculo sirve tambien para corregir tambin la linea base em espectrometras y para establecer el Punto Estequiomtrico en las PotenciometrasRESULTADO56.4814814815con paso por el origen=63.1067961165

IR-mtodos

interpolacinCONC en mg/LAbsorbanciaCLCULO DE CONCENTRACIN

vitab12 bisINDICEValores.2 A=50 pixel256,771-275,759-265,7210.036Absorbancia neta estimada

INDICE

ccc2INDICEPara El Plomo, absorcin: mostrando la longitud de onda en AnstrongUNICAMSP.pifhttp://jersey.uoregon.edu/vlab/elements/Elements.html

INDICEhttp://jersey.uoregon.edu/vlab/elements/Elements.htmlUNICAMSP.pif

envolventeINDICE%TAbsorbancia51.301GRAB.pifRelacin longitud de onda m yfrecuencia, nmero de onda en cm-11190cm-10.00084cm8.4micras11901305160516951750610B (1)Acido acetilsalicilicoLa figura siguiente muestra PARTE DE ESTA PGINA 610, letra B,con el espectro de Nujol superpuesto para poder descontar sus bandas2 parteConfirme la identidad de esta sustancia

INDICEGRAB.pif

TLCunidimensionalINDICECCC1.BASCyanocobalamin, Vitamina B121a7b0+7a6b1+21a5b2+35a4b3+35a3b4+21a2b5+7a1b6+1a0b7N de tuboAmbas fasesfase inferiorfase superiorK(coeficiente de reparto)a+b=1; a/b=1.2 ( a=.5454,b=.4545)10.014370.006530.007841.200612557435a4b30.290757041720.08380.038090.045711.2000525072coef3530.209490.095220.114271.200063012a4=0.088483141740.290960.132250.158711.2000756144b3=0.093886178650.242470.110210.132251.199981852835a4b3=0.290757041760.121230.055110.066131.19996370890.290757041770.033680.015310.018371.1998693664"=35*POTENCIA(0.5454;4)*POTENCIA(0.4545;3)"80.004010.001820.002191.2032967033corregir en ccc2 la fase orgnicaEl tringulo de Pascal es el tringulo generado por dos nmeros de la siguiente forma:Cuando a y b son 1, se obtiene el llamado tringulo de Tartaglia, que representa los coeficientes combinatorioscoeficiente..1..1 11 2 11 3 3 11 4 6 4 11 5 10 10 5 11 6 15 20 15 6 11 7 21 35 35 21 7 11 8 28 56 70 56 28 8 1ambas fasesfase benzyl alcoholfase acuosaK=1.210.01440.0070.0081.20120.08380.0380.0461.20030.20950.0950.1141.20040.29100.1320.1591.20050.24250.1100.1321.20060.12120.0550.0661.20070.03370.0150.0181.20080.00400.0020.0021.2031.00001.200clsdefint h,p,n,mdefdbl y,f,cdef fnfact(p)fact=1while p0fact=fact*pp=p-1wendfnfact=factend definput"NOMBRE DEL FICHERO SIN EXTENSION:";NAMEF$ :IF NAMEF$= " "THEN RETURN'OPEN NAMEF$+" .wk1" FOR OUTPUT AS #1 'EXTENSION PARA IMPORTAR AL QPROopen namef$+".prn" for output as #1 'O al HG version color como ASCIIINPUT"Cantidad de soluto:",cinput"Coeficiente de reparto:",kinput "Grado=numero de tubos -1:";na=c*k/(1+k)b=c/(1+k)clsdim y(n+1)for h2=0 to nh1=-(h2-n)m=n+1ncoef=h2+1ynum=fnfact(m)ydenom=m*fnfact(m-ncoef)*fnfact(ncoef-1)coeff=ynum/ydenomy(h2)=coeff*(a^h1*b^h2)print #1,using"####.####";(h2)+1,'print #1,";";print #1,using"####.#####"; y(h2),'print #1,";";print #1,using"####.#####";Y(h2)/(1+k),'print #1,";";print #1,using"####.#####";(y(h2)-y(h2)/(1+k))print using"###.";(h2)+1,print,USING"#.####";y(h2),print,using"#.####"; y(h2)/(1+k),print,using"#.###"; (y(h2)-Y(H2)/(1+K)),print,using"#####";coeffnextclose #1

TLCunidimensional

ambas fasescapa superiorcapa inferior

TLC resolucinINDICECCC2.BAS100000200000Autores (p.o. de firma): SIMAL GNDARA, M; SIMAL LOZANO, J; Y SIMAL GNDARA, J300000clsTtulo: Simulacin de la distribucin en contracorriente por ordenador400000Ref. revista Tcnicas de Laboratorio Libro:500000defint h,p,n,mClave: A Volumen: 170 Pginas, inicial: 194 final: 201 Fecha: 1.992600000defdbl y,f,cEditorial (si libro): Lugar de publicacin: Espaa70000080000090000.00010.0001def fnfact(p)100000.00020.0002fact=1110000.00060.0006while p0120000.00140.0014fact=fact*p130000.00290.0029p=p-1140000.00570.0057wend150000.01010.0101fnfact=fact160000.01670.0167end def17000.00010.02560.025718000.00030.03670.037input"NOMBRE DEL FICHERO SIN EXTENSION:";NAMEF$ :IF NAMEF$= " "THEN RETURN19000.00050.04930.0498INPUT "GRADO=";n20000.00110.06230.0634INPUT "NUMERO DE SUSTANCIAS:";nsust21000.0020.07420.0762DIM y(n+1),c(nsust),k(nsust)22000.00360.08350.0871PRINT:PRINT23000.0060.0890.095FOR pp=1 TO nsust24000.00960.09010.0997INPUT"CANTIDAD DE SOLUTO:",c(pp)25000.01440.08660.101INPUT"COEFICIENTE DE REPARTO:",k(pp)26000.02080.07940.1002PRINT27000.02860.06940.098NEXT28000.03750.0580.0955CLS29000.04710.04630.0934OPEN NAMEF$+" .PRN" FOR OUTPUT AS #1 'EXTENSION PARA IMPORTAR AL QPRO30000.05660.03540.09231000.06520.0260.091232000.07210.01830.0904'INPUT"Cantidad de soluto:",c33000.07660.01240.089'input"Coeficiente de reparto:",k34000.07830.0080.0863'input "Grado=numero de tubos -1:";n35000.07690.0050.081936000.07290.0030.0759'a=c*k/(1+k)37000.06650.00180.0683'b=c/(1+k)38000.05850.0010.05953900.00010.04970.00050.0503'cls4000.00010.04080.00030.04124100.00020.03240.00010.0327'dim y(n+1)4200.00040.02480.00010.02534300.00070.018400.0191304400.00110.013200.0143'OPEN "B18"+right$(str$(int(k)),len(str$(int(k)))-1)+".DAT" FOR OUTPUT AS #14500.00180.009200.0114600.00280.006200.009for h2=0 to n4700.00420.00400.00824800.00620.002500.0087h1=-(h2-n)4900.00890.001600.01055000.01240.000900.0133m=n+15100.01670.000500.0172ncoef=h2+15200.02180.000300.0221ynum=fnfact(m)5300.02770.000200.0279ydenom=m*fnfact(m-ncoef)*fnfact(ncoef-1)5400.03410.000100.0342coeff=ynum/ydenom5500.0408000.04085600.0475000.0475'y(h2)=coeff*(a^h1*b^h2)5700.0537000.05375800.0591000.0591'print,using"####.###"; y(h2)5900.0631000.06316000.0656000.0656print".";6100.0664000.0664'To use with HG you have to supress the remark comand6200.0653000.0653PRINT #1,USING"####";NCOEF,6300.0625000.0625'PRINT #1,";";6400.0582000.05826500.0527000.0527FOR pp=1 TO nsust6600.0465000.04656700.0399000.0399A=k(pp)/(1+k(pp))6800.0334000.0334B=1/(1+k(pp))6900.0272000.0272y(h2)=coeff*(a^h1*b^h2)*c(pp)7000.0215000.0215PRINT #1,USING"####.####";y(h2),7100.0166000.0166'print #1,";";7200.0125000.01257300.0091000.0091next7400.0065000.0065print #1,7500.0045000.0045next7600.003000.003close #17700.002000.0027800.0013000.0013790.00010.0008000.0009800.00010.0005000.0006810.00020.0003000.0005820.00040.0002000.0006830.00060.0001000.0007840.0010.0001000.0011850.00170000.0017860.00260000.0026870.00390000.0039880.00570000.0057890.00820000.0082900.01140000.0114910.01550000.0155920.02040000.0204930.02620000.0262940.03260000.0326950.03960000.0396960.04660000.0466970.05340000.0534980.05950000.0595990.06440000.06441000.06760000.06761010.0690000.0691020.06830000.06831030.06560000.06561040.06110000.06111050.05530000.05531060.04840000.04841070.04110000.04111080.03380000.03381090.02690000.02691100.02080000.02081110.01550000.01551120.01110000.01111130.00780000.00781140.00520000.00521150.00340000.00341160.00210000.00211170.00130000.00131180.00070000.00071190.00040000.00041200.00020000.00021210.00010000.00011220.00010000.00011230000012400000125000001260000012700000128000001290000013000000131000001320000013300000134000001350000013600000137000001380000013900000140000001410000014200000143000001440000014500000146000001470000014800000149000001500000015100000

TLC resolucin

tlc bidi 1-2INDICE100000200000../../Bromatologia/CAA/Seminarios/TB.pif30000040000050000060000070000080000090000.00010.0001100000.00020.0002110000.00060.0006120000.00140.0014130000.00290.0029140000.00570.0057150000.01010.0101envolvente160000.01670.016717000.00010.02560.025718000.00030.03670.03719000.00050.04930.049820000.00110.06230.063421000.0020.07420.076222000.00360.08350.087123000.0060.0890.09524000.00960.09010.099725000.01440.08660.10126000.02080.07940.100227000.02860.06940.09828000.03750.0580.095529000.04710.04630.093430000.05660.03540.09231000.06520.0260.091232000.07210.01830.090433000.07660.01240.08934000.07830.0080.086335000.07690.0050.081936000.07290.0030.075937000.06650.00180.068338000.05850.0010.05953900.00010.04970.00050.05034000.00010.04080.00030.04124100.00020.03240.00010.03274200.00040.02480.00010.02534300.00070.018400.01914400.00110.013200.01434500.00180.009200.0114600.00280.006200.0094700.00420.00400.00824800.00620.002500.00874900.00890.001600.01055000.01240.000900.01335100.01670.000500.01725200.02180.000300.02215300.02770.000200.02795400.03410.000100.03425500.0408000.04085600.0475000.04755700.0537000.05375800.0591000.05915900.0631000.06316000.0656000.06566100.0664000.06646200.0653000.06536300.0625000.06256400.0582000.05826500.0527000.05276600.0465000.04656700.0399000.03996800.0334000.03346900.0272000.02727000.0215000.02157100.0166000.01667200.0125000.01257300.0091000.00917400.0065000.00657500.0045000.00457600.003000.0037700.002000.0027800.0013000.0013790.00010.0008000.0009800.00010.0005000.0006810.00020.0003000.0005820.00040.0002000.0006830.00060.0001000.0007840.0010.0001000.0011850.00170000.0017860.00260000.0026870.00390000.0039880.00570000.0057890.00820000.0082900.01140000.0114910.01550000.0155920.02040000.0204930.02620000.0262940.03260000.0326950.03960000.0396960.04660000.0466970.05340000.0534980.05950000.0595990.06440000.06441000.06760000.06761010.0690000.0691020.06830000.06831030.06560000.06561040.06110000.06111050.05530000.05531060.04840000.04841070.04110000.04111080.03380000.03381090.02690000.02691100.02080000.02081110.01550000.01551120.01110000.01111130.00780000.00781140.00520000.00521150.00340000.00341160.00210000.00211170.00130000.00131180.00070000.00071190.00040000.00041200.00020000.00021210.00010000.00011220.00010000.00011230000012400000125000001260000012700000128000001290000013000000131000001320000013300000134000001350000013600000137000001380000013900000140000001410000014200000143000001440000014500000146000001470000014800000149000001500000015100000

tlc bidi 1-20000000000000000000000000000000000.000100.000100.000200.000200.000600.000600.001400.001400.002900.002900.005700.005700.010100.010100.016700.016700.02570.00010.025600.0370.00030.036700.04980.00050.049300.06340.00110.062300.07620.0020.074200.08710.00360.083500.0950.0060.08900.09970.00960.090100.1010.01440.086600.10020.02080.079400.0980.02860.069400.09550.03750.05800.09340.04710.046300.0920.05660.035400.09120.06520.02600.09040.07210.018300.0890.07660.012400.08630.07830.00800.08190.07690.00500.07590.07290.00300.06830.06650.001800.05950.05850.00100.05030.04970.000500.04120.04080.000300.03270.03240.000100.02530.02480.000100.01910.0184000.01430.0132000.0110.0092000.0090.0062000.00820.004000.00870.0025000.01050.0016000.01330.0009000.01720.0005000.02210.0003000.02790.0002000.03420.0001000.04080000.04750000.05370000.05910000.06310000.06560000.06640000.06530000.06250000.05820000.05270000.04650000.03990000.03340000.02720000.02150000.01660000.01250000.00910000.00650000.00450000.0030000.0020000.0013000.00010.0009000.00010.0006000.00020.0005000.00040.0006000.00060.0007000.0010.0011000.00170.0017000.00260.0026000.00390.0039000.00570.0057000.00820.0082000.01140.0114000.01550.0155000.02040.0204000.02620.0262000.03260.0326000.03960.0396000.04660.0466000.05340.0534000.05950.0595000.06440.0644000.06760.0676000.0690.069000.06830.0683000.06560.0656000.06110.0611000.05530.0553000.04840.0484000.04110.0411000.03380.0338000.02690.0269000.02080.0208000.01550.0155000.01110.0111000.00780.0078000.00520.0052000.00340.0034000.00210.0021000.00130.0013000.00070.0007000.00040.0004000.00020.0002000.00010.0001000.00010.000100000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000000

TLC bidimensional-aflatoxinINDICERf123distancia 23 desarrollo1desarrorrollo2esarrolloincremento 30.110.90.811.92.713.86223.23.860.332.11.475.16.5740.662.40.968.49.360.63631.50.630.990.90.099.99.9980.212.11.6591.310613.7595.069611.922761.21.7521.922760.333.32.2111.481375.5116.99237Autores (p.o. de firma): VILLAR DAZ, J.; SIMAL LOZANO, J. y VILA ABAD, J.Ttulo: Cromatografa de desarrollo mltiple unidimensionalRef. revista Tcnicas de Laboratorio Libro:Clave: A Volumen: 128 Pginas, inicial:99 final: 107 Fecha: 1.986Editorial (si libro):Lugar de publicacin: Espaaexcel: convertir texto en columnas

TLC bidimensional-aflatoxin

CROMATOGRAFA MLTIPLE UNIDIMENSIONAL

teofilina

CROMATOGRAFA MLTIPLE UNIDIMENSIONAL 2 desarrollo

CyTA


potenciometra


rrt brew1INDICEPaloma Canzos AchiricaResolucinRfDistancia libre por recorrerDist. migradaDist migrada total10.2102220.281.63.630.26.41.284.8840.25.121.0245.90450.24.0960.81926.723260.23.27680.655367.3785670.22.621440.5242887.90284880.22.0971520.41943048.322278490.21.67772160.335544328.65782272100.21.342177280.2684354568.926258176110.21.0737418240.21474836489.1410065408120.20.85899345920.17179869189.3128052326Diferenciacinentre resoluciones10.31033120.372.15.11.530.34.91.476.571.6940.33.431.0297.5991.69550.32.4010.72038.31931.596160.31.68070.504218.823511.4449570.31.176490.3529479.1764571.27360980.30.8235430.24706299.42351991.101241590.30.57648010.172944039.596463930.93864121100.30.403536070.1210608219.7175247510.791266575110.30.2824752490.08474257479.80226732570.6612607849120.30.19773267430.05931980239.8615871280.548781895310.8108820.821.69.630.80.40.329.9240.80.080.0649.98410.91099120.910.99.90.330.90.10.099.990.0740.90.010.0099.9990.015

rrt brew111.51.691.6951.59611.444951.2736091.10124150.938641210.7912665750.66126078490.5487818953

Rf 0,2Rf 0,3dDiferenciacin entre resolucionesNmero de resolucinDistancia de migracinResolucin de sustancias con Rf distintos

FACTOR DE ASIMETRA

Nmero de resolucinDistancia de migracinResolucin de sustancias con Rf distintos

sst-RP-USP

rrt-hINDICExydistanciadisolventerfavance22120.224220.557220.668220.88102222222222yxrf216120.20.35045.522130.10.180.8833.810.82120.5007222100.9001122220220220220220x2.861.431.000.506.430.5013.431.434.700.506.430.5014.292.575.000.907.570.5015.143.715.301.308.710.5016.004.865.601.709.860.5016.866.005.902.1011.000.5013.4316.864.705.9021.860.503.4317.147.860.203.436.577.867.891.310.204.575.718.147.201.490.205.714.868.436.511.660.206.864.008.715.831.830.208.003.149.005.142.000.2016.866.5713.437.891.310.20

JSL:avance con los distintos RfJSL:rf de diferentes mezclasJSL: Eje Xconvierte el valor grfico de C en real sobre 20 cm.JSL:eje yJSL:valor grfico en el dibujo de nuestro trabajoJSL:eje yJSL: avance nueva YJSL: rf 1 desarrolloJSL:patrn 2 desarrJSL:patrn 2 desarrJSL:rf del segundo desarrolloJSL:20 - valor X valor de x, ahora ser YJSL:avance 2eje Y 13.14 (10+ 3.14)-posicin inicialAnterior valor de Y ; ahora es el de eje X

rrt-h427810

MTODOS-CUANT.45.510.833.87121110

2 desarrollo mostrando dos o tres componentes en un punto del 1e r deassarollo

%REA-017.14287147.8851964646.571495587.19948565.7143576.5137747364.857218425.8280638724.000079845.1423530083.142941267.8851964646.57149558

NORM.INDENE-11.42856436.42856431.42856436.42856432.571415747.571415743.714267188.714267184.857118629.857118625.9999700610.9999700616.8570587413.42850442

inicial

IS-INDENE-2Autores (p.o. de firma): SIMAL, J.; LPEZ, J.; GARRIDOydistanciadisolventerfavanceTtulo: Investigacin de Aflatoxinas en leches, cacahuetes y piensos2120.224Ref. revista Trabajos Compostelanos de Biologa Libro:211012Clave: A Volumen :12 Pginas, inicial: 5 final: 12 Fecha: 198520.668Editorial (si libro):20.8810Lugar de publicacin: Espaa222222222yxrf216120.20.35045.52280.10.180.8833.810.82120.5007222100.9001122220220220220220INDICE7.00xyRf2.861.431.003.430.503.430.2013.431.434.703.430.503.430.2014.292.575.004.340.904.570.2015.143.715.305.261.305.710.2016.004.865.606.171.706.860.2016.866.005.907.092.108.000.2013.4316.864.7016.865.9018.860.20x2-posicin inicial girada 90y22desrrollox=DRf 2 desarrollo1.4317.1417.140.401.436.578.519.202.630.402.575.718.008.682.970.403.714.867.498.173.310.404.864.006.977.663.660.406.003.146.467.144.000.4016.866.578.519.202.630.40x2y2conc2.001.002.003.004.005.006.00

JSL:avance con los distintos RfJSL:rf de diferentes mezclasJSL: Eje Xconvierte el valor grfico de C en real sobre 20 cm.JSL:eje yJSL:valor grfico en el dibujo de nuestro trabajoJSL: avance nueva YJSL: rf 1 desarrolloJSL:patrn 2 desarrJSL:patrn 2 desarrJSL:rf del segundo desarrolloJSL:20 - valor X se establece restando de 20JSL:avance 2eje Y 13.14 (10+ 3.14)-posicin inicialAnterior valor de Y ; ahora es el de eje XPC: valor de y despues de un desarrolloJSL:eje yAnterior valor de Y ; ahora es el de eje X

IS-INDENE-2427810

ES-INDENE-545.510.833.87121110

2 desarrollo mostrando dos o tres componentes en un punto del 1e r deassarollo

Temas20051.42856432.85712861.428564313.428504422.5714157414.2856433.7142671815.142781584.8571186215.999920165.9999700616.8570587416.8570587413.42850442

inicial y 1er desarrollo

ejercicios Excel

INDICEMETROHM 686TITRATORdate91-08-12 time0.5708333333METU******** #6mV(init) 415V/mlmVEP15.580stopVreached========GETU******** #6V/mlmV0415141043575.43939393944.53305.43939393945265205.43939393945.124530-105.221550-205.316575-255.490140-65VESUV.pif5.5-50401005.6-9030105.7-12015155.8-1356-1458-17010-180=======USER0P FOR REPORT#1 5.425 ml : 55.46 mV

-65100

punto estequiomtricoml

-65100

METROHM 682 TITRATORdate 01-04-01 time 22:17GET pH ******** # 7C00 1dummy sample size!pH(init) 9.05V/ml pHEP1 2.460 7.55RS1 .2460stop V reached========GET pH ******** # 70.065V/ml pH2.63709.0700.1429.050.02-0.020.2849.040.010.010.4279.020.02-0.010.5699.010.010.010.7118.990.02-0.010.8538.970.0200.9958.940.03-0.011,1378.90.04-0.011,2808.860.04-01,4228.810.05-0.011,5648.760.05-01,7068.690.07-0.021,8488.610.08-0.011,9918.510.1-0.022,1338.390.12-0.022,2758.230.16-0.042.4177.890.34-0.18INDICE2.5596.950.94-0.62.7026.730.220.722,8446.590.140.082,2758.230.342,9866.480.110.032.4177.89-0.60.943,1286.390.090.022.5596.950.720.223,2706.310.080.012.7026.733,4126.240.070.013,5556.170.07-03,6976.10.0703,8396.040.060.013,9815.980.0604,1235.920.06-04,2665.860.0604,4085.810.050.014,5505.740.07-0.024,6925.680.060.014,8345.620.060========USER-EP FOR REPORT #1 2.282 ml : 8.21 pH

-0.60.72

00-0.020.1420.020.010.2840.01-0.010.4270.020.010.5690.01-0.010.7110.0200.8530.02-0.010.9950.03-0.0111370.04-012800.04-0.0114220.05-015640.05-0.0217060.07-0.0118480.08-0.0219910.1-0.0221330.12-0.0422750.16-0.182.4170.34-0.62.5590.940.722.7020.220.0828440.140.0329860.110.0231280.090.0132700.080.0134120.07-035550.07036970.070.0138390.06039810.06-041230.06042660.060.0144080.05-0.0245500.070.0146920.06048340.06

INDICEMETROHM 682 TITRATORdate 01-04-01 time 22:17GET pH ******** # 7C00 1dummy sample size!pH(init) 9.05V/ml pHEP1 2.460 7.55RS1 .2460stop V reached========GET pH ******** # 70.065V/ml pH-0.022.63709.0700.010.1429.050.02-0.010.2849.040.010.010.4279.020.02-0.010.5699.010.0100.7118.990.02-0.010.8538.970.02-0.010.9958.940.03-01,1378.90.04-0.011,2808.860.04-01,4228.810.05-0.021,5648.760.05-0.011,7068.690.07-0.021,8488.610.08-0.021,9918.510.1-0.042,1338.390.12-0.182,2758.230.162,2758.230.342.4177.890.34-0.62.4177.89-0.60.942.5596.950.940.722.5596.950.720.222.7026.730.220.082.7026.732,8446.590.140.032,9866.480.110.023,1286.390.090.010.013,2706.310.08-03,4126.240.0703,5556.170.070.013,6976.10.0703,8396.040.06-03,9815.980.0604,1235.920.060.014,2665.860.064,4085.810.054,5505.740.07-0.024,6925.680.060.014,8345.620.060========USER-EP FOR REPORT #1 2.282 ml : 8.21 pH

-0.60.72

00-0.020.1420.020.010.2840.01-0.010.4270.020.010.5690.01-0.010.7110.0200.8530.02-0.010.9950.03-0.0111370.04-012800.04-0.0114220.05-015640.05-0.0217060.07-0.0118480.08-0.0219910.1-0.0221330.12-0.0422750.16-0.182.4170.34-0.62.5590.940.722.7020.220.0828440.140.0329860.110.0231280.090.0132700.080.0134120.07-035550.07036970.070.0138390.06039810.06-041230.06042660.060.0144080.05-0.0245500.070.0146920.06048340.06

-0.60.72

mlsegunda derivadaP.estequimtrico

INDICEDISK FILE:BADGE1.RAWINJECTEDAT: / /1:23:37REPROCESSED: Method: LocalDefault MethodCH=PS=1FILE 1METHOD 2RUN 1INDEX 1CALIBANALYST:RRTobtenido directamente en esta hojaNAMECONCRTPK HTRFRRTISDTRRT102.25920.1937.451.20.168203.3146900.3597.451.20.338304.25127740.5047.451.20.488404.9149040.6077.451.20.594505.4311350.6877.451.20.677aflato16.47713380.5670.8497.451.20.843isINTERNAL STD7.4540428117.451.21.000808.4629411.1577.451.21.162909.2536141.287.451.21.28810011.6138371.6457.451.21.666TOTALS2145753NEW FILE:NAMERFRTaflato0.5676.47isINT STD7.45

INDICEC:\Documents and Settings\PC\Escritorio\Paint (2).lnkPaint (2).lnk16.4701.67592163990.9236111111543183360valor de Wb213valor de f63valor de 2f126valor de Wb/2f1.6904761905

Paint (2).lnkINDICE

INDICEPaint.lnkSST.pif1.691.693877551FILENAME: BADGE1.RAW METHOD: BADGE2.FIL EPPEAK RET. RESOLUTION TAILING TH. PLATE CAPACITYTIME FACTOR FACTOR NUMBER FACTORestearico 6.46 1.69 4608 5.46oleico 7.44 2.52 1.58 5600 6.44SYSTEM SUITABILITY TESTFILENAME: BADGE1.RAW METHOD: BADGE2.FIL USPPEAK RET. RESOLUTION TAILING TH. PLATE CAPACITYTIME FACTOR FACTOR NUMBER FACTORestearico 6.46 1.69 4528 5.46oleico 7.44 2.48 1.58 5373 6.441.-REVISAR LOS DIFERENTES FACTORES DE LA SEPARACIN CROMOTGRFICA2.-Estimar la relacin entre el ancho de la base (USP) y el ancho a media altura de la EP.Wb/W1/2=1.70RF (USP)/(EP)=1.69

Paint.lnkSST.pifINDICE

INDICEDISK FILE:BADGE1.RAWINJECTEDAT: / /1:23:37REPROCESSED: Method: LocalDefault MethodCH=PS=14.4FILE 1 METHOD 2RUN 1INDEX 1CALIBANALYST:NAME CONCRTPK HTRFRRT1 0.0002.25920.2282 0.0003.3146900.4233 0.0004.25127740.5944 0.0004.9149040.7155 0.0005.4311350.81estearico INTERNAL STD6.477133811oleico 2.0007.45404283.5291.1788 0.0008.4629411.3639 0.0009.2536141.50810 0.00011.6138371.938TOTALS 3.000145753DISK FILE:BADGE1.RAWINJECTEDAT: / /1:23:37REPROCESSED: Method: LocalestericoCH=PS=1FILE 1METHOD 2RUN 1INDEX 1CALIBDT=1ANALYST:NAMECONCRTPK HTRFRRT102.25920.193203.3146900.359304.25127740.504404.9149040.607505.4311350.687estearico16.47713380.5670.849isINTERNAL STD7.454042811808.4629411.157WW09.2536141.2810011.6138371.645TOTALS2145753NEW FILE:NAMERFRTestearico0.5676.47isINT STD7.44WW09.63

92469012774490411357133840428294136143837

rrt corregidos/altura

INDICE

INDICEPeak #AREA%RTAREADT=110.2650.16930320.0570.47201930.1222.19428241,8693.326565050.1453.69508967,1674.2625169072,2274.937821280.3815.4513369947,8126.4816791241031,9237.451121118112,1298.4874752122,8589.25100381133,04511.6106944TOTALS100,0003511933

INDICE

INDICEPeak#AREA%RTAREADT=110.1222.19428221,8753.326565030.1453.69508947,1904.2625169052,2344.937821260.3825.4513369747,9676.481679124832,0267.45112111892,1358.4874752102,8689.25100381113,05511.6106944TOTALS100,0003500611

INDICE

INDICEDISK FILE:BADGE1,RAWINJECTEDAT: / /1:23:37REPROCESSED:Method: LocalEXTERNAL-STD,-SIMALCH=PS=1FILE 1METHOD 5RUN 1INDEX 1CALIBANALYST:NAMECONCRTAREARFRRTDT=valor introducido en la celda siguiente102.2523340.22810.2285191956203.311582520.42310.4223034735304.253723140.59410.5941499086404.911333240.71510.7148080439505.43479960.8110.8098720293ES16.4722906132290613111INDENE17.45143014614301461.17811.1791590494808.461261621.36311.3638025594909.251497041.50811.50822669110011.612612201.93811.9396709324TOTALS24972065FILE 1METHOD 2RUN 1

INDICE

INDICEDISK FILE:BADGE1,RAWINJECTEDAT: / /1:23:37REPROCESSED: Method: LocalEXTERNALSTANDART-SIMALCH=PS=1FILE 1METHOD 5RUN 1INDEX 1CALIBANALYST:NAMECONCRTAREARFRRT102.2523340.228DT=valor introducido en la celda siguiente203.311582520.42310.3581395349304.253723140.5941.30.4796747967404.911333240.7151.30.5869918699505.43479960.811.30.6715447154IS16.472290613229061311.30.8406504065INDENE17.45143014614301461.1781.31808.461261621.3631.31.1642276423909.251497041.5081.31.292682926810011.612612201.9381.31.67642276421.3-0.2113821138TOTALS24972065NEW FILE:NAMERFRTIS22906136.47INDENE14301467.44

INDICE

INDICETEMAS:CURSO 2005-2006 (CONTAMINANTES EN FONDO BLANCO ; ADITIVOS EN FONDO AMARILLO; RESIDUOS DE FRMACOS EN LILA)CONTAMINANTESPESTICIDAS1POLICLOROBIFENILOS (PCBs) Y POLICLOROTERFENILOS (PCTs)2(HBS.ALIFTICOS) Hidrocarburos alifticos3( PAHs) Policiclicos Aromtcos Hidrocarburos4MICOTOXINAS5FENOLES6MONMEROS7TENSIOACTIVOS8RESIDUOS DE FRMACOS9METALES10ADITIVOSEDULCORANTES-CON CUERPO12EDULCORANTES-ADMITIDOS13COLORANTES-INORGNICOS14COLORANTES-NATURALES15aditivos distintos de edulcorates y colorantesConservadores18Antioxidante.19Emulgente.20Sales de fundido.21Espesante.22Gelificante.23Estabilizador (se incluyen en esta categora los estabilizadores de espuma).24Potenciador del sabor.25Acidulante.26Corrector de la acidez (las regulaciones de pH pueden realizarse en ambos sentidos).27Antiaglomerante.28Almidn modificado.29Gasificante.30Antiespumante.31Agente de recubrimiento (se incluyen en esta categora los agentes desmoldeadores).32Agente de tratamiento de la harina.33Endurecedor.34Humectante.35Secuestrante.36Enzimas (slo se incluyen en esta categora las enzimas que tienen funcin de aditivos).37Agente de carga.38Gas propulsor y gas de envasado.39RESIDUOS DE FRMACOSHIDRRXI-BENZOICOS41CARBOHIDRATOS42GLUCXIDOS43ESTEROIDES44BARBITURICOS45AMINOCIDOS46SULFAMIDAS47ALCALOIDES48ANTIPIRTICOS Y ANALGSICOS49ANTIBITICOS50VITAMINAS HIDROSOLUBLES51VITAMINAS LIPOSOLUBLES52ORGANOMETLICOS10

INDICERESIDUOS DE FRMACOS1423567891012131510484644

..\..\broma\caa\seminari\WOW.lnkALGUNOS DE LOS EJERCICIOS MS REPRESENTATIVOS QUE SE HACEN A LO LARGO DEL CURSOAAS-AS-mezcla (cido acetilsaliclico-cido saliclico, mezcla)%Absocin-%T-AA-T%ConcentracinA-neta-PaintAbsorcion Atmica- PlomoIR-mtodosBHT-MASSLAB-MSC32Distribucin en dos capas y ocho tubos de vitamina B12-Aplicacin del programa CCC1-cifras significatrivas,etcCCC2 Distribucin en contracorriente de varios componentes, mximo 150 tubos-envolvente,etcTLC multiple UnidimensionalResolucin TLC multiple UnidimensionalTLC Bidimensionaltlc bidi 1-2'!A1TLC Bidimensional-multicomponentes- AflatoxinasEjemplos de Potenciometras- punto estequiomtricosRRTRetencin relativa y corregida en Cromatografa-electroforesisSystem Suitability Text (Factor de Asimetra-Paint; Factor de capacidad; Resolucin; EficaciaMtodos de cuantificacin en Cromatografa: (WOW) WINNER ON WINDOWS%REA- Metodo-0, de WOWNORMALIZACION %-.INDENE- Metodo-1, de WOWIS(INTERNAL STANDARD)-INDENE- Metodo-2, de WOWES (EXTERNAL STANDARD)-INDENE- Metodo-5, de WOWTEMAS CURSO 2005 PARA:CONTAMINACIN ABITICA DE LOS ALIMENTOS (FARMACIA)MATERIAS PRIMAS Y ADITIVOS ALIMENTARIOS (BIOTECNOLOGA)PROBLEMTICA ANALTICA DE LOS ALIMENTOS (TODOS-TERCER CICLO)

tlc bidi 1-2'!A1AAS-AS-mezcla (cido acetilsaliclico-cido saliclico, mezcla)%Absocin-%T-AA-T%ConcentracinA-neta-PaintAbsorcion Atmica- PlomoIR-mtodosDistribucin en dos capas y ocho tubos de vitamina B12-Aplicacin del programa CCC1-cifras significatrivas,etcCCC2 Distribucin en contracorriente de varios componentes, mximo 150 tubos-envolvente,etcTLC multiple UnidimensionalResolucin TLC multiple UnidimensionalTLC BidimensionalTLC Bidimensional-multicomponentes- AflatoxinasEjemplos de Potenciometras- punto estequiomtricosRRTRetencin relativa y corregida en Cromatografa-electroforesisSystem Suitability Text (Factor de Asimetra-Paint; Factor de capacidad; Resolucin; EficaciaMtodos de cuantificacin en Cromatografa: (WOW) WINNER ON WINDOWS%REA- Metodo-0, de WOWNORMALIZACION %-.INDENE- Metodo-1, de WOWIS(INTERNAL STANDARD)-INDENE- Metodo-2, de WOWES (EXTERNAL STANDARD)-INDENE- Metodo-5, de WOWTEMAS CURSO 2005 PARA:BHT-MASSLAB-MSC32..\..\broma\caa\seminari\WOW.lnk

MBD0004A290.docAutores (p.o. de firma): SIMAL, J.; LPEZ, J.; GARRIDO

Ttulo: Investigacin de Aflatoxinas en leches, cacahuetes y piensos

Ref. revista Trabajos Compostelanos de Biologa Libro:

Clave: A Volumen :12 Pginas, inicial: 5 final: 12 Fecha: 1985

Editorial (si libro):

Lugar de publicacin: Espaa

MBD000E2E31/UNICAMSP.EXE.pif