variable head permeability test contract 42103 bh10 … · a3.1.2 any discussion in this report is...

VARIABLE HEAD PERMEABILITY TEST

42103 Variable Head (Falling) Permeability Test in BH10

SITE Western Link

CONTRACT 42103 BH10 DEPTH< mBGL 4.70

INITIAL CONDITIONSBase of Response Zone 4.70 mBGL Operator HSTop of Reponse Zone 1.70 mBGL DateDiameter of casing 50.00 mm Time 11:20Height of casing 0.00 mAGL Weather SunnyElevation of Borehole mAOD CalculatedGroundwater Level 2.16 mBGL 3.00 m

TEST CALCULATION Elapsed Total Water Head H/Ho(minutes) seconds Depth (m) (metres)

0.0 0 0.040 2.120 1.000Intake Factor, F 0.5 30 0.280 1.880 0.887

1.0 60 0.460 1.700 0.802F= 3.94 (i) 2.0 120 0.720 1.440 0.679

3.0 180 0.950 1.210 0.571Borehole Case d 4.0 240 1.110 1.050 0.495BS 5930: 1999 Figure 6 5.0 300 1.280 0.880 0.415

6.0 360 1.380 0.780 0.3687.0 420 1.470 0.690 0.3258.0 480 1.550 0.610 0.2889.0 540 1.600 0.560 0.264

10.0 600 1.650 0.510 0.241Permeability, K 15.0 900 1.780 0.380 0.179

20.0 1200 1.820 0.340 0.160K= A (iii) 25.0 1500 1.840 0.320 0.151

F . T 30.0 1800 1.840 0.320 0.15140.0 2400 1.850 0.310 0.146

Where T is the Basic Time Lag Factor 50.0 3000 1.860 0.300 0.142corresponding to an H/Ho value of 0.37 60 3600 1.860 0.300 0.142

L= 3.00 mD= 0.050 m

L/D= 60

A= 0.00196 m^2F= 3.9388 From (i)T= 360 s

K= 1.39E-06 m/s From (iii)

Remarks

31/08/2017

APPENDIX 3

GEOTECHNICAL LABORATORY TEST RESULTS

Appendix 10 pages x/i-x/ii x/i

APPENDIX 3

GENERAL NOTES ON LABORATORY TESTS ON SOILS

A3.1 GENERAL

A3.1.1 Where applicable all tests are carried out in accordance with the relevant British Standard. The laboratory test procedures are as below:

Test Name Procedures BS1377:1990 Part:Clause

Moisture Content 2:3 Liquid Limit 2:4 Plastic Limit and Plastic Index 2:5 Linear Shrinkage 2:6 Particle Size Distribution 2:9

Loss on Ignition 3:4* Sulphate content 3:5 Chloride Content 3:7* pH Value 3:9

Compaction Test 4:3* Moisture condition Value 4:5 California Bearing Ratio 4:7

Consolidation 5:3

Bulk Density 7:2* Laboratory Vane Tests 7:3* Shear Box 7:4* Triaxial Compression

Total Stress Single-Stage 7:8 Total Stress Multi-Stage 7:9 Effective Stress Note 1*

Permeability Note 2* Desiccation Note 3*

In-situ density by Sand replacement Part 9 Core Cutter Part 9 Nuclear density Part 9

BS812 Part:Clause

Ten % fines (Dry and Soaked) 111 Aggregate crushing value 110 Particle density and water absorption 2 Particle size distribution 103 Moisture content – oven drying 109 Soundness 121

Appendix 10 pages x/i-x/ii x/ii

BS:1881 Part:Clause Chloride Content 124:10.2 Sulphate content 124:10.3 Curing/density and compressive strength of concrete tubes 116-111-114 Location of reinforcement 204 Carbonation Note 4 Resistivity Note 5 Sampling of concrete dust by drilling Note 6 Half cell potential Note 7 Note 1 - Manual of soils laboratory testing volume 3: 1985, section 19.2 by K.H. Head Note 2 - Manual of soils laboratory testing volume 2: 1985, section 10.7 by K.H. Head Note 3 - BRE Information paper IP4 issued February 1993 Note 4 - BRE Information paper IP6/81 Note 5 - In-house document number 109 Note 6 - In-house document number 112 Note 7 - ASTM C876-91 * Tests are not included in UKAS accreditation

A3.1.2 Any discussion in this report is based on the values and results obtained from the appropriate tests. Due allowance should be made, when considering any result in isolation, of the possible inaccuracy of any such individual result. Details of the accuracy of results are included in this section, where applicable.

Figure A3.1

Results of Soil Testing

Site:

Job Number:

Originating Client:

Originating Reference:

Date Sampled:

Date Scheduled:

Date Testing Started:

Date Testing Finished:

Remarks:

Authorised By:

Page. 1

Ian Farmer Associates (1998) Limited. Registered in England and Wales No. 3661447Registered Office: Unit 4 Faraday Close, Pattinson North Industrial Estate, Washington, NE38 8QJ

Offices in: Coventry (024) 7630 3422. Harpenden, Herts. (01582) 460 018. Llanelli (01554) 566 566.Motherwell (01698) 230 231. Newcastle upon Tyne (0191) 482 8500. Truro (01827) 261 775.

Warrington (01925) 855 440.

24/07/2017

04/08/2017

Paul CathcartQuality Manager Date: 24/08/2017

Warrington Western Link

42103

Warrington Borough Council

42103

Not Given

Unit 4 Faraday Close, Pattinson North Industrial Estate, Washington, Tyne & Wear, NE38 8QJTel. 0191 482 8500 Fax. 0191 482 8520 Email. [email protected] Internet. www.ianfarmer.co.uk

F.A.O.

Test Report - 42103 / 2

27/07/2017

3.50 14.7 93 15.0 24 14 10

4.50 12.3 98 12.0 23 11 12

6.00 10.2 99 10.0 18 17 1

10.00 11.2 94 12.0 22 10 12

13.00 13.4 95 14.0 21 11 10

6.20 31.1 100 31.0 35 23 12

8.20 37 100 37.0 45 24 21

9.20 15.4

11.50 11.8 99 12.0 24 11 13

13.50 10.5 94 11.0 21 10 11

15.50 12.4 93 13.0 22 11 11

3.00 20.1 100 20.0 27 19 8

3.50 21.2 100 21.0 28 10 18

5.50 29.5 100 30.0 35 17 18

8.00 7.3 10 29.0 27 14 13

2.20 26.8

4.20 14.8

7.20 12.6

9.20 20.8

1.20 24.5

2.00 24.5

4.00 12.1

5.00 16.7

4.20 11.6

Site: Warrington Western Link Job Number: 42103

Natural / Sieved

Natural Water

Content %

Laboratory Test Report 42103 / 2

Liquidity Index Class

Client: Warrington Borough Council Page: 2

Determination of Water Content, Liquid Limit and Plastic Limit and Derivation of Plasticity and Liquidity Index

Borehole / Trial Pit Depth (m) Sample Description / Remarks

Percentage %

Water Content %

Sample Passing425 µm Sieve Liquid Limit

%Plastic Limit

%Plasticity Index %

BH03 B9 Natural 0.15 CL Brown slightly sandy CLAY

BH03 U11 Natural 0.12 CL Brown CLAY

BH03 D14 Natural -6.73 ML Brown slightly sandy CLAY


BH03 D24 Natural 0.29 CL Brown slightly gravelly CLAY

BH04 U18 Natural 0.68 CL/CI Grey/Brown slightly sandy, CLAY/SILT

BH04 U21 Natural 0.62 CI Grey CLAY

BH04 B23 Brown SAND


BH04 D31 Natural 0.08 CL Brown slightly sandy CLAY

BH04 U33 Natural 0.18 CL Brown sandy CLAY

BH05 U8 Natural 0.14 CL Brown slightly sandy CLAY

BH05 D9 Natural 0.62 CL Brown CLAY

BH05 D14 Natural 0.69 CL/CI Brown silty CLAY

BH05 B17 Sieved 1.16 CL Brown slightly clayey GRAVEL

BH06 B5 Brown slightly clayey, very silty SAND

BH06 B9 Brown SAND

BH06 UT15 Brown CLAY

BH06 UT19 Brown sandy CLAY

BH10 B5 Brown slightly gravelly, clayey, sandy SILT

BH10 D8 Brown clayey, sandy SILT

BH10 UT10Brown slightly gravelly, slightly clayey, very

silty SAND

BH10 B12 Brown CLAY

BH12A B13 Brown gravelly SAND

Method of Preparation: BS EN ISO 17892 : Part 1 : 2014 : Clause 5.1 Water content test preparationBS 1377 : Part 1 : 2016 : Clause 8.4.3 Preparation of samples for plasticity testsBS 1377 : Part 2 : 1990 : Clause 4.2 Preparation of samples for plastic limit tests

Method of Test: BS EN ISO 17892 : Part 1 : 2014 : Clause 5.2 Water content test executionBS 1377 : Part 2 : 1990 : Clause 4.3 or 4.4 Determination of the liquid limitBS 1377 : Part 2 : 1990 : Clause 5.3 Determination of the plastic limit and plasticity index

mmmmmmmm

RemarksPreparation and testing in accordance with BS1377 unless noted below




DETERMINATION OF PARTICLE SIZE DISTRIBUTION

Borehole / Trial Pit Depth (m) Sample Testing Type Description

BH03 2.00 B7 Wet Sieve + Pipette Brown slightly gravelly, clayey, very silty SAND

Sieving Sedimentation Dry Mass of sample, g 1994Particle Size

mm % Passing Particle Size mm % Passing

0.0201 42 Sample Proportions % dry mass0.0060 32 Very coarse 00.0020 14 Gravel 5

Sand 44Silt 37Clay 14

20 100 Grading Analysis14 100 D100 2010 99 D60 0.1276.3 98 D30 0.005365 98 D10

3.35 96 Uniformity Coefficient2 95 Curvature Coefficient

1.18 940.6 90 Particle density (assumed)

0.425 87 2.65 Mg/m30.3 80

0.212 720.15 620.063 51

Method of Preparation: BS 1377:Part 1:1990, clause 7 3 Initial preparationBS 1377:Part 1:1990, clause 7.4.5 Preparation of particle size tests

Method of Test: BS1377:Part 2:1990, clause 9.2 Determination of particle size distribution by wet sieving methodBS1377:Part 2:1990, clause 9.4 Determination of sedimentation by pipette method

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SILTFine Medium Coarse

SANDFine Medium Coarse

GRAVELFine Medium CoarseCLAY COBBLES BOULDERS

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BH04 3.20 B10 Wet Sieve + Pipette Brown slightly silty, sandy GRAVEL




Sand 2550 100 Silt 12

37.5 79 Clay 128 7920 70 Grading Analysis14 57 D100 5010 54 D60 15.26.3 49 D30 0.8695 47 D10 0.0294

3.35 43 Uniformity Coefficient 5202 38 Curvature Coefficient 1.7


0.425 24 2.65 Mg/m30.3 19

0.212 180.15 150.063 13



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BH04 9.20 B23 Wet Sieve Brown SAND



Sample Proportions % dry massVery coarse 0Gravel 6Sand 91

Fines <0.063mm 228 10020 98 Grading Analysis14 98 D100 2810 96 D60 0.486.3 95 D30 0.335 95 D10 0.22

3.35 95 Uniformity Coefficient 2.22 94 Curvature Coefficient 1

1.18 920.6 74

0.425 520.3 22

0.212 90.15 40.063 2


Method of Test: BS1377:Part 2:1990, clause 9.2 Determination of particle size distribution by wet sieving method

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BH05 8.00 B17 Wet Sieve Brown slightly clayey GRAVEL




50 10037.5 93 Fines <0.063mm 628 8220 66 Grading Analysis14 44 D100 5010 32 D60 18.16.3 19 D30 9.435 14 D10 2.36

3.35 11 Uniformity Coefficient 7.72 10 Curvature Coefficient 2.1

1.18 90.6 9

0.425 90.3 9

0.212 80.15 80.063 6



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BH06 2.20 B5 Wet Sieve + Pipette Brown slightly clayey, very silty, SAND





Grading AnalysisD100 10

10 100 D60 0.07126.3 100 D30 0.02415 100 D10



0.425 99 2.65 Mg/m30.3 99

0.212 990.15 980.063 54



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Fines <0.063mm 928 10020 99 Grading Analysis14 99 D100 2810 98 D60 0.446.3 98 D30 0.3095 98 D10 0.0712

3.35 98 Uniformity Coefficient 6.22 97 Curvature Coefficient 3

1.18 960.6 80

0.425 580.3 27

0.212 190.15 160.063 9



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BH10 1.20 B5 Wet Sieve + Pipette Brown slightly gravelly, clayey, sandy, SILT





20 100 Grading Analysis14 100 D100 2010 99 D60 0.02296.3 98 D30 0.004985 98 D10



0.425 91 2.65 Mg/m30.3 85

0.212 810.15 790.063 77



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BH10 2.00 D8 Wet Sieve + Pipette Brown clayey, sandy SILT





Grading Analysis14 100 D100 1410 100 D60 0.03196.3 99 D30 0.002255 99 D10



0.425 94 2.65 Mg/m30.3 89

0.212 860.15 810.063 67



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BH10 5.00 B12 Wet Sieve + Pipette Brown slightly gravelly, slightly clayey, very silty, SAND





20 100 Grading Analysis14 99 D100 2010 97 D60 0.2236.3 96 D30 0.01785 95 D10 0.00455



0.425 81 2.65 Mg/m30.3 65

0.212 590.15 520.063 46



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BH12A 4.20 B13 Wet Sieve Brown gravelly SAND



Sample Proportions % dry mass90 100 Very coarse 1575 85 Gravel 1963 85 Sand 6450 85

37.5 79 Fines <0.063mm 228 7920 78 Grading Analysis14 77 D100 9010 75 D60 1.056.3 73 D30 0.4245 70 D10 0.247

3.35 69 Uniformity Coefficient 4.22 67 Curvature Coefficient 0.7

1.18 630.6 46

0.425 300.3 13

0.212 70.15 50.063 2



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DETERMINATION OF THE ONE-DIMENSIONAL CONSOLIDATION PROPERTIES

Borehole / Trial Pit Depth (m) Sample Description

BH03 1.2 U5 Brown sandy, silty CLAY

Initi

al S

peci

men Length of Sample (mm) 350.00 Diameter (mm) 74.98

Depth from top of specimen (mm) 12.81 Particle density (Mg/m³) 2.65 assumed

Condition of Sample: Undisturbed Swelling Pressure (kPa)

Orientation: Vertical Lab Temp. (°C) 21

Applied Pressure

kPa

Mvm2/MN

Cv(t50, log)

m2/yr

Cv(t90, root)

m2/yrCsec Voids ratio Initial Final

Height (mm) 19.00 18.340.0 - - - - 0.34530 0.37 0.95 1.2 0.00047 0.330

12.1 11.360 0.2 0.92 1.7 0.00059 0.322

0.17 1.4 2.6 0.00093 0.308

Water Content (%)

Bulk density (Mg/m³) 2.21 2.27240 0.11 1.7 3.9 0.00089 0.290120

1.97 2.0430 0.058 0.298

120 0.0064Dry density (Mg/m³)

0.291

Voids Ratio 0.345 0.298

Degree of Saturation (%) 93 101

Method of Preparation: BS 1377:Part 5:1990, clause 3.3 Preparation of specimenBS 1377:Part 5:1990, clause 3.4 Preparation and assembly of apparatus

Method of Test: BS 1377:Part 5:1990, clause 3.5 Determination of the one-dimensional consolidation properties

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Applied Pressure kPa






BH05 3 U8 Brown slightly sandy CLAY

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Applied Pressure

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m2/yr

Cv(t90, root)


Height (mm) 19.10 18.000.0 - - - - 0.48560 0.58 0.68 0.8 0.00057 0.434

17.6 15.3100 0.17 0.61 0.82 0.0013 0.424

0.17 0.62 1.1 0.0014 0.411

Water Content (%)

Bulk density (Mg/m³) 2.10 2.18200 0.13 0.31 0.81 0.0013 0.402150

1.78 1.89100 0.014 0.397250 0.11

0.04 0.399

Dry density (Mg/m³)0.28 0.88 0.0016 0.394





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Unconsolidated Undrained Triaxial Compression Test without measurement of pore pressure - single specimen (Definitive Method)

Borehole / Trial Pit

Depth (m) Sample Description

Orientation

BH03 4.50 U11 Brown CLAY

Original Length (mm) 280.00

Depth from Top (mm) 20.00

Condition Undisturbed

Vertical

Length (mm) 206.62

Diameter (mm) 102.18

Moisture Content (%) 12.30

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Test Number 1

Bulk Density (Mg/m3) 2.32

Dry Density (Mg/m3) 2.07

Membrane Thickness (mm) 0.34

Membrane Type Latex

Rate of Strain (%/min) 1.9

Test

Res

ults

Cell Pressure (kPa) 100

Axial Strain (%) 13

Membrane Corr. (kPa) 0.91

Deviator Stress, ( σ1 - σ3 )f

(kPa) 131

Undrained Shear Strength, cu = ½( σ1 - σ3 )f (kPa)

65

Mode of Failure Compound

Deviator stress corrected for area change and membrane effects

Mohr circles and their interpretation is not covered by BS1377.This is provided for information only.

Method of Preparation: BS 1377:PT1:1990:8.3 Preparation of undisturbed samples for testing orBS 1377:PT1:1990:7.7.5.2 Preparation of disturbed samples for testing

Method of Test: BS 1377:PT2:1990:7.2 Determination of density by linear measurement. BS 1377:PT7:1990:8.4 Determination of undrained shear strength in triaxial compression without measurement of pore pressure (Definitive method) 1464

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Length (mm) 206.23



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Axial Strain (%) 14



(kPa) 225


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BH04 4.20 U13 Brown slightly gravelly CLAY




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Length (mm) 207.68



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Axial Strain (%) 13



(kPa) 44


22






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BH04 8.20 U21 Grey CLAY




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Length (mm) 208.32



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Axial Strain (%) 13



(kPa) 69


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Length (mm) 207.85



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Axial Strain (%) 16



(kPa) 605


303






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BH04 15.50 U33 Brown sandy CLAY




Vertical

Length (mm) 207.74



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Axial Strain (%) 20



(kPa) 243


122






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BH06 7.20 UT15 Brown CLAY




Vertical

Length (mm) 208.16



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Axial Strain (%) 20



(kPa) 261


131

Mode of Failure Plastic





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BH06 9.20 UT19 Brown sandy CLAY




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Length (mm) 207.18



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Axial Strain (%) 6.8



(kPa) 114


57

Mode of Failure Brittle





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BH10 4.00 UT10 Brown silty CLAY




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Length (mm) 207.59



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Axial Strain (%) 20



(kPa) 157


79






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Site:

Job Number:

Originating Client:

Page. 24


42103


All opinions and interpretations contained within this report are outside of our Scope of Accreditation.

This test report shall not be reproduced, except in full and only with the written permission of Ian Farmer Associates Ltd

Date: 24/08/2017

Test Report - 42103 / 2

Site:

Job Number:

Originating Client:


Date Sampled:

Date Scheduled:



Remarks:

Authorised By:

Page. 1



Warrington (01925) 855 440.



F.A.O.

Test Report - 42103A / 1


42103A

Warrington Borough Council 42103

Not Given

24/07/2017

28/07/2017

03/08/2017

Paul Cathcart

2.90 47.6 100 48.0 37 27 10

Site: Warrington Western Link Job Number: 42103A

Natural / Sieved

Natural Water

Content %

Laboratory Test Report 42103A / 1





Percentage %

Water Content %


%Plastic Limit

%Plasticity Index %

CPT14A D9 Natural 2.06 MI Grey slightly sandy CLAY



mmmmmmmm







CPT14A 1.00 D3 Wet Sieve + Pipette Brown slightly gravelly, silty SAND (CLAY pockets noted)





Grading Analysis14 100 D100 1410 99 D60 0.1056.3 99 D30 0.03825 99 D10 0.00878



0.425 84 2.65 Mg/m30.3 79

0.212 750.15 730.063 42



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CPT14A 2.20 D7 Wet Sieve + Pipette Brown slightly silty SAND





Grading AnalysisD100 5D60 0.0949D30 0.0651

5 100 D10 0.02493.35 100 Uniformity Coefficient 3.8

2 100 Curvature Coefficient 1.81.18 1000.6 99 Particle density (assumed)

0.425 99 2.65 Mg/m30.3 99

0.212 980.15 960.063 27



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CPT14A 4.10 D13 Wet Sieve + Pipette Grey silty SAND





Grading AnalysisD100 5D60 0.108D30 0.0688

5 100 D10 0.02493.35 100 Uniformity Coefficient 4.4

2 99 Curvature Coefficient 1.81.18 990.6 97 Particle density (assumed)

0.425 94 2.65 Mg/m30.3 88

0.212 840.15 820.063 24



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Site:

Job Number:

Originating Client:

Page. 6


42103A




Date: 03/08/2017

Test Report - 42103A / 1

Site:

Job Number:

Originating Client:


Date Sampled:

Date Scheduled:



Remarks:

Authorised By:

Page. 1



Warrington (01925) 855 440.



F.A.O.

Test Report - 42103B / 1


42103B


42103B

Not Given

02/08/2017

10/08/2017

21/08/2017

13.00 10.4 70 13 27 16 11

1.20 40.7 100 41 49 29 20

1.65 76.1

2.20 49.3 100 49 53 32 21

3.65 59.7

4.20 94.0 100 94 NP

6.20 21.9

7.20 28.4 100 28 NP

7.65 28.6

8.20 33.6

10.20 20.0

14.20 9.1 100 9.1 20 11 9

0.55 28.6

1.70 24.9 78 30 NP

2.40 13.6

3.40 10.5 96 11 25 14 11

4.60 9.8

0.20 15.9 99 16 NP

1.00 14.8

2.08 5.3

3.03 10.5 94 11 22 11 11

3.80 11.3

4.60 8.7 94 8.9 21 11 10

1.70 22.6 100 23 NP

3.15 34.6

3.60 21.2 69 28 37 29 8

5.80 29.5

7.00 26.6

0.70 33.0 100 33 48 35 13

1.70 6.8

2.40 21.2 99 21 NP

2.92 15.3

4.10 12.7 43 23 NP

4.80 19.0

6.50 16.7 23 56 NP

7.00 31.4



CPT15A D33 Brown sandy GRAVEL

CPT15A D30 Sieved Brown SAND

CPT15A D24 Brown SAND

CPT15A D20 Sieved Brown gravelly SAND




CPT15A D5 Natural -0.15 MI Brown sandy SILT

CPT14A D22 Brown gravelly SAND

CPT14A D17 Brown sandy SILT

CPT14A D12 Sieved -0.08 MI Brown sandy SILT



CPT03A D26 Natural -0.21 CL Brown slightly gravelly, slighty sandy CLAY

CPT03A D21 Brown slightly sandy CLAY

CPT03A D17 Natural -0.02 CL Brown slightly sandy, slightly gravelly CLAY



CPT03A D2 Natural Brown silty SAND

CPT01A D24 Brown sandy, slightly gravelly CLAY

CPT01A D18 Natural -0.30 CL Brown slightly sandy CLAY

CPT01A D12 Brown slightly gravelly, sandy SILT

CPT01A D8 Sieved Brown slightly gravelly, sandy SILT


BH07 U26 Natural -0.21 CL Brown sandy, slightly gravelly CLAY

BH07 D22 Brown SAND

BH07 D18 Brown silty CLAY

BH07 D17 Brown silty CLAY

BH07 U16 Natural Brown sandy, clayey SILT

BH07 D14 Brown sandy, silty CLAY

BH07 D10 Natural Brown sandy SILT

BH07 D9 Brown slightly sandy CLAY

BH07 D6 Natural 0.82 MH Brown silty CLAY

BH07 D5 Brown slightly organic SILT

BH07 U4 Natural 0.59 MI Brown silty, gravelly SAND

BH06A D1 Sieved -0.30 CL Brown clayey, silty SAND

Description / RemarksPercentage

%Water

Content %


%Plastic Limit

%Plasticity Index %




Borehole / Trial Pit Depth (m) Sample Natural /

Sieved

Natural Water

Content %

Laboratory Test Report 42103B / 1

Site: Warrington Western Link Job Number: 42103B

8.20 23.4


Natural / Sieved

Natural Water

Content %






Percentage %

Water Content %


%Plastic Limit

%Plasticity Index %


Method of Preparation: BS EN ISO 17892 : Part 1 : 2014 : Clause 5.1 Water content test preparation

Method of Test: BS EN ISO 17892 : Part 1 : 2014 : Clause 5.2 Water content test execution

mmmmmmmm







BH06A 14.20 B2 Wet Sieve Brown sandy GRAVEL

Sieving SedimentationParticle Size

mm % Passing Particle Size mm % Passing Dry Mass of sample, g 10847

Sample Proportions % dry mass125 100 Very coarse 3690 80 Gravel 2075 73 Sand 3663 6450 62 Fines <0.063mm 8

37.5 5928 58 Grading Analysis20 54 D100 12514 51 D60 42.710 50 D30 0.366.3 48 D10 0.08715 47 Uniformity Coefficient 490

3.35 45 Curvature Coefficient 0.0352 44

1.18 430.6 40

0.425 360.3 24

0.212 180.15 140.063 8



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mmmmmmmm







BH07 1.20 U4 Wet Sieve + Pipette Brown silty, clayey SAND



0.0201 550.0060 48 Sample Proportions % dry mass0.0020 32 Very coarse 0

Gravel 1Sand 35Silt 31Clay 32

Grading AnalysisD100 6.3D60 0.0394D30

6.3 100 D105 100 Uniformity Coefficient

3.35 100 Curvature Coefficient2 99 Particle density (assumed)

1.18 98 2.65 Mg/m30.6 97

0.425 970.3 96

0.212 950.15 930.063 64



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mmmmmmmm







BH07 3.20 U8 Wet Sieve + Pipette Brown/Black slightly gravelly, silty SAND





Grading AnalysisD100 10D60 0.168

10 100 D30 0.02876.3 98 D10 0.002435 96 Uniformity Coefficient 69

3.35 95 Curvature Coefficient 22 92 Particle density (assumed)

1.18 84 2.65 Mg/m30.6 81

0.425 790.3 78

0.212 710.15 550.063 40



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mmmmmmmm







BH07 5.20 U12 Wet Sieve + Pipette Brown/Blackish slightly gravelly, silty SAND





Grading Analysis20 100 D100 2014 98 D60 0.12610 95 D30 0.0476.3 90 D10 0.003355 88 Uniformity Coefficient 38

3.35 86 Curvature Coefficient 5.22 84 Particle density (assumed)

1.18 82 2.65 Mg/m30.6 80

0.425 790.3 78

0.212 770.15 670.063 33



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mmmmmmmm







BH07 7.20 U16 Wet Sieve + Pipette Brown sandy, clayey SILT





Grading AnalysisD100 2D60 0.0508D30 0.00715D10Uniformity CoefficientCurvature Coefficient

2 100 Particle density (assumed)1.18 100 2.65 Mg/m30.6 99

0.425 990.3 98

0.212 970.15 960.063 65



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BH07 9.20 U20 Wet Sieve + Pipette Brown sandy SILT





Grading AnalysisD100 6.3D60 0.049D30 0.025

6.3 100 D10 0.00745 100 Uniformity Coefficient 6.6


1.18 99 2.65 Mg/m30.6 98

0.425 970.3 96

0.212 950.15 940.063 71



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mmmmmmmm











Fines <0.063mm 4

Grading AnalysisD100 10D60 0.54

10 100 D30 0.3676.3 100 D10 0.2255 100 Uniformity Coefficient 2.4


1.18 970.6 69

0.425 400.3 16

0.212 90.15 60.063 4



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Fines <0.063mm 2

Grading AnalysisD100 14

14 100 D60 0.46910 100 D30 0.3556.3 100 D10 0.2775 99 Uniformity Coefficient 1.7


1.18 980.6 86

0.425 500.3 12

0.212 40.15 30.063 2



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BH07 16.20 B29 Wet Sieve + Pipette Brown slightly clayey, silty SAND





Grading Analysis20 100 D100 2014 99 D60 0.12910 98 D30 0.02526.3 97 D105 96 Uniformity Coefficient


1.18 93 2.65 Mg/m30.6 90

0.425 850.3 75

0.212 690.15 620.063 51



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BH07 3.2 U8

Initi

al S

peci





Applied Pressure

kPa

Mvm2/MN

Cv(t50, log)

m2/yr

Cv(t90, root)


Height (mm) 18.94 15.580.0 - - - - 1.37425 1.6 6 7.4 0.0036 1.281

51.2 37.650 0.74 0.87 3.1 0.0025 1.239

0.82 3.2 3.2 0.0062 1.147

Water Content (%)

Bulk density (Mg/m³) 1.69 1.87200 0.5 3 4.1 0.0072 1.040100

1.12 1.36200 0.0091 0.931400 0.28

0.077 0.953

Dry density (Mg/m³)2.4 5.1 0.0061 0.927





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1.000

1.050

1.100

1.150

1.200

1.250

1.300

1.350

1.400

Void

s R

atio

0.002.004.006.008.00

10.00

1 10 100 1000 10000

Cv

m2 /y

r(lo

g tim

e)


Brown/Black slightly gravelly, silty SAND






BH07 7.2 U16

Initi

al S

peci





Applied Pressure

kPa

Mvm2/MN

Cv(t50, log)

m2/yr

Cv(t90, root)


Height (mm) 18.99 17.500.0 - - - - 0.71250 0.73 2.9 3.5 0.0014 0.650

27.4 23.4100 0.25 1.9 4.7 0.0009 0.630

0.17 3.2 5.8 0.0019 0.602

Water Content (%)

Bulk density (Mg/m³) 1.97 2.07400 0.11 3.6 6.3 0.002 0.567200

1.55 1.6850 0.043 0.578


0.568





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0.001.002.003.004.005.00

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Brown sandy, clayey SILT







Orientation

BH07 14.20 U26 Brown sandy, slightly gravelly CLAY




Vertical

Length (mm) 207.76



Initi

al S

ampl

e

Test Number 1




Membrane Type Latex


Test

Res

ults


Axial Strain (%) 20



(kPa) 485


243

Mode of Failure Plastic





0

100

200

300

400

500

600

0 5 10 15 20 25

Cor

rect

ed D

evia

tor S

tress

kPa

Axial Strain %


0

100

200

300

400

500

600

700

800

900

0 500 1000

Shea

r Stre

ngth

kPa

Normal Stresses kPa

Mohr Circles

Height mm Diameter mm Bulk Density Mg/m³ Water Content % Dry Density Mg/m³

Cvi

Mvi

kvi

Method of Test: BS EN ISO 17892 : Part 1 : 2014 : Clause 5.2. Water content test executionBS EN ISO 17892 : Part 2 : 2014 : Clause 5.1. Density by linear measurement methodBS 1377 : Part 8 : 1990 : Clause 5.3, 6.2, 7 Determination of consolidated-undrained triaxial compression test with measurement of pore pressure 1464

Coefficient of Permeability ( Calculated ) N/A m/s

Method of Preparation: BS EN ISO 17892 : Part 1 : 2014 : Clause 5.1 Water content test specimenBS 1377 : Part 1 : 1990 : Clause 7.7.5.2 Preparation of disturbed samples for testing

Pore Pressure Dissipation at End of Consolidation 96 % Consolidation Parameters( see note to BS1377 : pt 8, clause 6.3.4 )

Coefficient of Consolidation 0.30 m2/year Coefficient of Compressibility 1.444 m2/MN

50 kPa Pore Pressure at Start of Consolidation 351 kPa Pore Pressure at End of Consolidation 312 kPa

Consolidation Details

Drainage Conditions From one end and radial boundary Cell Pressure Applied 360 kPa Back Pressure Applied 310 kPa Effective Pressure

70.0 35.1 Final Pore Water Pressure 351 kPa1.06 1.37 Final B Value 0.97

103.0 Differential Pressure 10 kPa1.80 1.88 Final Cell Pressure 360 kPa

Increments of Cell and Back Pressure209.2 Cell Pressure Increments 30 kPa

Specimen Orientation, Type and Preparation Vertical sample, Undisturbed as BS 1377

Specimen Details Initial Final Saturation DetailsMethod of Saturation

BH07 3.20 U8 Brown/Black slightly gravelly, silty SAND

Test Method Singlestage test based on BS1377 : Part 8 : 1990, clauses 1 to 6 and 7


Consolidated Undrained Triaxial Compression Test with Measurement of Pore Pressure( Singlestage Test on a Single Specimen )




0.0

0.5

1.0

0 50 100 150 200 250 300 350

B V

alue

Applied Cell Pressure kPa

0

20

40

60

80

100

120

0 10 20 30 40 50 60 70

Volu

me

Cha

nge

(ml)

Root Time (mins)

Compression Stages - Graphical Data

Sheet No. 2 of 3




Site: Warrington Western Link Job Number: 42103BClient: Warrington Borough Council Page: 17


0

20

40

60

80

100

120

0 2 4 6 8 10 12 14 16 18 20

Devia

tor

Str

ess

( σ

1' -σ

3' )

kP

a

ε %

Maximum Deviator Stress

1.00

2.00

3.00

4.00

5.00

6.00

7.00

8.00

9.00

0 2 4 6 8 10 12 14 16 18 20

Princip

al S

tress R

atio (

σ1' /

σ3' )

ε %

305

310

315

320

325

330

335

340

345

350

355

0 2 4 6 8 10 12 14 16 18 20

Pore

Wat

er P

ress

ure

kPa

Axial Strain, ε % ( All Plots )

Mohr Circles ______ Peak Deviator Stress

MIT Stress Field

Remarks General

Stage

Test Duration (days) 2 3 1

All symbols used above are defined in BS1377 Sheet No. 3 of 3

Deviator stresses corrected for area change, vertical side drains and 0.71 mm thick rubber membrane/

Saturation Consolidation Shearing Plastic

kPa 0.0 -Ø ' Degrees 45.8 -

Mode of Failure

Shear Strength Parameters Linear Regression ManualRe-assessment

c '

0.28Conditions at Maximum Deviator Stress 18.4 6.02 101 340 20 121 0.28

18.4 6.02 101 340 20 121kPa kPa kPa kPa

1 360 312 48 1.20kPa kPa kPa %/hr %

Effective Principle

Stress Ratio,( σ1' / σ3' ) f

Deviator Stress,

( σ1 - σ3 ) f

Pore Pressure,

uf

Minor Effective Principle

Stress, σ3' f

Major Effective Principle

Stress, σ1' f

Pore Pressure Parameter,

Af

End of Stage Criterion :Maximum Deviator Stress Compression Stages - Table of results and interpretation

StageCell

Pressure Initial PWPInitial

Effective Stress, σ3'

Rate of Strain

Axial Strain, εf






0

100

0 100 200 300

Shea

r stre

ss

kPa

Effective stresses kPa

0

100

0 100 200 300

t',

( σ

1' -σ

3' )

/ 2

kP

a

s', ( σ1' + σ3' ) / 2 kPa


Cvi

Mvi

kvi














BH07 5.20 U12 Brown/Blackish slightly gravelly, silty SAND







0.0

0.5

1.0

0 50 100 150 200 250 300 350 400

B V

alue


0

20

40

60

80

100

120

140

160

0 5 10 15 20 25 30 35 40

Volu

me

Cha

nge

(ml)

Root Time (mins)


Sheet No. 2 of 3






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10

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40

50

60

70

80

90

100

0 2 4 6 8 10 12 14 16 18

Devia

tor

Str

ess

( σ

1' -σ

3' )

kP

a

ε %


1.00

1.50

2.00

2.50

3.00

3.50

4.00

4.50

0 2 4 6 8 10 12 14 16 18

Princip

al S

tress R

atio (

σ1' /

σ3' )

ε %

300

310

320

330

340

350

360

370

0 2 4 6 8 10 12 14 16 18

Pore

Wat

er P

ress

ure

kPa



MIT Stress Field

Remarks General

Stage




Saturation Consolidation Shearing Plastic


Mode of Failure


c '


14.6 3.99 92 359 31 122kPa kPa kPa kPa

1 390 310 80 1.50kPa kPa kPa %/hr %

Effective Principle


Deviator Stress,

( σ1 - σ3 ) f

Pore Pressure,

uf


Stress, σ3' f


Stress, σ1' f


Af


StageCell



Rate of Strain

Axial Strain, εf






0

100

0 100 200 300

Shea

r stre

ss

kPa


0

100

0 100 200 300

t',

( σ

1' -σ

3' )

/ 2

kP

a

s', ( σ1' + σ3' ) / 2 kPa

Site:

Job Number:

Originating Client:

Page. 22


42103B



This test report shall not be reproduced, except in full and only with the written permission of Ian Farmer Associates Ltd.

Date: 22/08/2017

Test Report - 42103B / 1

Site:

Job Number:

Originating Client:


Date Sampled:

Date Scheduled:



Remarks:

Authorised By:

Page. 1



Warrington (01925) 855 440.



F.A.O.

Test Report - 42103C / 1


42103C


42103C

Not Given

02/08/2017

10/08/2017

22/08/2017

19.50 10.7

11.00 17.4

16.00 12.3

1.20 22.9

1.20 32.6 100 33.0 40 22 18

2.00 27.2 100 27.0 34 25 9

0.50 16.3

0.50 14.3

1.10 50.4

Site: Warrington Western Link Job Number: 42103C

Natural / Sieved

Natural Water

Content %

Laboratory Test Report 42103C / 1





Percentage %

Water Content %


%Plastic Limit

%Plasticity Index %

BH04 U39 Brown silty, sandy, gravelly CLAY

BH05 D22 Brown silty SAND

BH05 D29 Brown sandy CLAY

BH06 UT2 Brown slightly clayey, silty SAND

BH10 D6 Natural 0.59 CI Brown sandy, slightly gravelly, silty CLAY

BH10 B7 Natural 0.24 ML Brown sandy SILT

CPT01 D3 Brown sandy GRAVEL

CPT02 D3 Brown gravelly, silty SAND

CPT15A D6 Brown sandy SILT



mmmmmmmm







BH04 1.20 B4 Wet Sieve + Pipette Brown/Red slightly silty, slightly sandy GRAVEL (BRICKS noted)




Gravel 4775 100 Sand 2663 93 Silt 1750 90 Clay 4

37.5 8928 86 Grading Analysis20 81 D100 7514 74 D60 5.8110 69 D30 0.2496.3 62 D10 0.005335 57 Uniformity Coefficient 1100


1.18 42 2.65 Mg/m30.6 38

0.425 360.3 32

0.212 280.15 250.063 21



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mmmmmmmm







BH05 0.50 B2 Wet Sieve




50 100 Fines <0.063mm 737.5 9728 87 Grading Analysis20 79 D100 5014 63 D60 12.910 50 D30 4.436.3 37 D10 0.2775 32 Uniformity Coefficient 46


1.18 160.6 12

0.425 110.3 11

0.212 80.15 80.063 7



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Brown sandy GRAVEL

mmmmmmmm







BH05 3.00 U8 Wet Sieve + Pipette Brown slightly sandy, clayey SILT





Grading AnalysisD100 5D60 0.0283D30 0.00563D10

5 100 Uniformity Coefficient3.35 100 Curvature Coefficient


0.425 990.3 98

0.212 980.15 970.063 86



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mmmmmmmm







BH06 1.20 UT2 Wet Sieve + Pipette Brown slightly clayey, silty SAND





Grading AnalysisD100 5D60 0.0755D30 0.027D10

5 100 Uniformity Coefficient3.35 100 Curvature Coefficient


0.425 990.3 99

0.212 980.15 980.063 50



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Particle Size mm

mmmmmmmm







BH06 7.20 UT15 Wet Sieve + Pipette Brown slightly gravelly, silty SAND





Grading Analysis20 100 D100 2014 98 D60 0.19410 95 D30 0.01866.3 93 D10 0.005075 93 Uniformity Coefficient 38


1.18 88 2.65 Mg/m30.6 85

0.425 810.3 70

0.212 620.15 540.063 45



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mmmmmmmm







BH12A 1.20 B4 Wet Sieve + Pipette Brown silty, sandy GRAVEL (GLASS/CONCRETE noted)





37.5 10028 98 Grading Analysis20 94 D100 37.514 86 D60 3.9410 78 D30 0.1736.3 66 D10 0.008685 63 Uniformity Coefficient 450


1.18 51 2.65 Mg/m30.6 48

0.425 450.3 40

0.212 330.15 280.063 23



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Particle Size mm

mmmmmmmm







BH12A 3.20 B10 Wet Sieve Brown gravelly SAND (GLASS/CHINA noted)




Fines <0.063mm 037.5 10028 92 Grading Analysis20 88 D100 37.514 86 D60 0.8710 84 D30 0.3686.3 81 D10 0.2095 78 Uniformity Coefficient 4.2


1.18 650.6 54

0.425 380.3 19

0.212 100.15 50.063 1



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Particle Size mm

mmmmmmmm







CPT01 1.10 D5 Wet Sieve + Pipette Brown slightly silty, sandy GRAVEL





37.5 10028 92 Grading Analysis20 82 D100 37.514 76 D60 5.9410 69 D30 0.3126.3 61 D10 0.00415 57 Uniformity Coefficient 1400


1.18 44 2.65 Mg/m30.6 37

0.425 340.3 30

0.212 270.15 230.063 19



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Particle Size mm

mmmmmmmm







CPT02 1.00 D5 Wet Sieve + Pipette Brown slightly silty, gravelly SAND





28 100 Grading Analysis20 94 D100 2814 91 D60 1.7210 84 D30 0.1746.3 75 D10 0.01685 71 Uniformity Coefficient 100


1.18 56 2.69 Mg/m30.6 49

0.425 450.3 39

0.212 330.15 280.063 21



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mmmmmmmm







CPT14A 0.50 D4 Wet Sieve + Pipette Brown silty SAND






6.3 100 D10 0.00275 100 Uniformity Coefficient 30


1.18 99 2.65 Mg/m30.6 99

0.425 990.3 98

0.212 970.15 910.063 48



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Particle Size mm

mmmmmmmm







CPT15A 0.50 D4 Wet Sieve + Pipette Brown silty SAND






6.3 100 D105 100 Uniformity Coefficient


1.18 96 2.65 Mg/m30.6 94

0.425 930.3 91

0.212 890.15 780.063 29



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BH05 9 UT18 Brown slightly gravelly, sandy CLAY

Initi

al S

peci





Applied Pressure

kPa

Mvm2/MN

Cv(t50, log)

m2/yr

Cv(t90, root)


Height (mm) 19.02 17.480.0 - - - - 0.28175 0.69 42 26 0.00029 0.214

10.1 10.2150 0.089 1.8 50 0.0011 0.206

0.073 2.9 49 0.00075 0.193

Water Content (%)

Bulk density (Mg/m³) 2.28 2.48600 0.056 2.3 9 0.0008 0.173300

2.07 2.25150 0.017 0.177300 0.0033

Dry density (Mg/m³)0.174





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s R

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0.0010.0020.0030.0040.0050.00

1 10 100 1000 10000

Cv

m2 /y

r(lo

g tim

e)







BH06 7.2 UT15 Brown slightly gravelly, silty SAND

Initi

al S

peci





Applied Pressure

kPa

Mvm2/MN

Cv(t50, log)

m2/yr

Cv(t90, root)


Height (mm) 19.04 17.860.0 - - - - 0.31675 0.33 0.89 1.1 0.00088 0.284

13.2 11.2150 0.14 1.2 2.4 0.00088 0.271

0.097 1.7 3.3 0.001 0.252

Water Content (%)

Bulk density (Mg/m³) 2.28 2.39600 0.057 2.1 5.7 0.0014 0.231300

2.01 2.15150 0.018 0.235300 0.0019

Dry density (Mg/m³)0.231





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0.000.501.001.502.002.50

1 10 100 1000 10000

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r(lo

g tim

e)







BH10 4 UT10 Brown slightly sandy, slightly gravelly CLAY

Initi

al S

peci





Applied Pressure

kPa

Mvm2/MN

Cv(t50, log)

m2/yr

Cv(t90, root)


Height (mm) 19.02 18.180.0 - - - - 0.26650 0.43 1.2 3.2 0.00088 0.239

11.4 10.2100 0.14 1.7 2.6 0.00088 0.230

0.1 2 5.2 0.00063 0.218

Water Content (%)

Bulk density (Mg/m³) 2.33 2.41400 0.06 2.8 6.3 0.0011 0.203200

2.09 2.1950 0.034 0.210


0.204





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atio

0.001.002.003.004.005.00

1 10 100 1000 10000

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r(lo

g tim

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Cvi

Mvi

kvi














BH04 19.50 U39 Brown silty, sandy, gravelly CLAY







0.0

0.5

1.0

0 50 100 150 200 250 300 350 400 450 500 550 600 650 700 750

B V

alue


0

5

10

15

20

25

30

35

40

45

50

0 5 10 15 20 25 30 35 40

Volu

me

Cha

nge

(ml)

Root Time (mins)


Sheet No. 2 of 3




Site: Warrington Western Link Job Number: 42103CClient: Warrington Borough Council Page: 18


0

100

200

300

400

500

600

700

800

0 2 4 6 8 10 12 14 16 18 20

Devia

tor

Str

ess

( σ

1' -σ

3' )

kP

a

ε %


1.00

1.50

2.00

2.50

3.00

3.50

4.00

0 2 4 6 8 10 12 14 16 18 20

Princip

al S

tress R

atio (

σ1' /

σ3' )

ε %

0

100

200

300

400

500

600

0 2 4 6 8 10 12 14 16 18 20

Pore

Wat

er P

ress

ure

kPa



MIT Stress Field

Remarks General

Stage




Saturation Consolidation Shearing Compound


Mode of Failure


c '


13.8 3.04 736 390 360 1096kPa kPa kPa kPa

1 750 358 392 1.40kPa kPa kPa %/hr %

Effective Principle


Deviator Stress,

( σ1 - σ3 ) f

Pore Pressure,

uf


Stress, σ3' f


Stress, σ1' f


Af


StageCell



Rate of Strain

Axial Strain, εf




Site: Warrington Western Link Job Number: 42103CClient: Warrington Borough Council Page: 19


0

100

200

300

400

0 100 200 300 400 500 600 700 800 900 1000 1100 1200

Shea

r stre

ss

kPa


0

100

200

300

400

0 100 200 300 400 500 600 700 800 900 1000 1100 1200

t',

( σ

1' -σ

3' )

/ 2

kP

a

s', ( σ1' + σ3' ) / 2 kPa

Site:

Job Number:

Originating Client:

Page. 20


42103C




Date: 29/08/2017

Test Report - 42103C / 1

Site:

Job Number:

Originating Client:


Date Sampled:

Date Scheduled:



Remarks:

Authorised By:

Page. 1



Warrington (01925) 855 440.



F.A.O.

Test Report - 42103D / 1


42103D


42103

Not Given

10/08/2017

16/08/2017

25/08/2017

Paul Cathcart

25.20 8.7 83 9.5 21 12 9

27.20 12.7

29.20 7.8 97 7.9 NP

33.20 9.9 96 10.0 17 8 9

35.20 9.1

36.00 12.2 60 17.0 21 11 10

19.20 11.3

21.20 11.5 96 12.0 NP

23.20 15.8

24.20 14.8

Site: Warrington Western Link Job Number: 42103D

Natural / Sieved

Natural Water

Content %

Laboratory Test Report 42103D / 1





Percentage %

Water Content %


%Plastic Limit

%Plasticity Index %

BH04A D3 Natural -0.28 CL Brown sandy CLAY

BH04A D6 Brown sandy CLAY

BH04A D9 Natural Brown clayey SAND

BH04A D15 Natural 0.23 CL Brown sandy CLAY

BH04A D18 Brown slightly sandy CLAY

BH04A D20 Natural 0.59 CL Brown sandy CLAY

BH05A D3 Brown sandy CLAY

BH05A D6 Natural Brown clayey SAND

BH05A D9 Reddish-Brown SAND

BH05A D12 Reddish-Brown sandy CLAY



mmmmmmmm







BH05A 18.00 B1 Wet Sieve Brown slightly gravelly, clayey SAND




Fines <0.063mm 39

Grading Analysis20 100 D100 2014 99 D60 0.19410 98 D306.3 97 D105 97 Uniformity Coefficient

3.35 96 Curvature Coefficient2 95

1.18 950.6 93

0.425 890.3 78

0.212 640.15 490.063 39



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Particle Size mm

mmmmmmmm







BH05A 23.80 B11 Wet Sieve Reddish-Brown slightly gravelly, clayey SAND




Fines <0.063mm 3837.5 10028 96 Grading Analysis20 96 D100 37.514 96 D60 0.13210 95 D306.3 95 D105 95 Uniformity Coefficient

3.35 95 Curvature Coefficient2 94

1.18 940.6 93

0.425 920.3 85

0.212 760.15 640.063 38



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Site:

Job Number:

Originating Client:

Page. 5


42103D




Date: 25/08/2017

Test Report - 42103D / 1

Certificate Number 25-Jul-17Client

Our Reference

Client Reference

Order No

Contract Title

Description

Date Received

Date Started

Date Completed

Test Procedures

Notes

Approved By

Adam Fenwick

Opinions and interpretations are outside the laboratory's scope of ISO 10725

accreditation. This certificate is issued in accordance with the accreditation

requirements of the United Kingdom Accreditation Service. The results reported herein

relate only to the material supplied to the laboratory. This certificate shall not be

reproduced except in full, without the prior written approval of the laboratory.

Contracts Manager


4 Soil samples.

21-Jul-17

21-Jul-17

25-Jul-17

Identified by prefix DETSn (details on request).

Certificate of Analysis

17-05850

Ian Farmer Associates

14-15 Rufford Court

Hardwick Grange

Woolston

Warrington

Cheshire

WA1 4RF

17-05850

42103

43037

Derwentside Environmental Testing Services LimitedUnit 2, Park Road Industrial Estate South, Consett, Co Durham, DH8 5PY

Tel: 01207 582333 • email: [email protected] • www.dets.co.uk Page 1 of 6 .

Summary of Chemical AnalysisMatrix Descriptions

Our Ref 17-05850Client Ref 42103

Contract Title Warrington Western Link

Sample ID Other ID Depth Lab No Completed Matrix DescriptionBH03 6 1.7 1207334 25/07/2017 Brown gravelly, sandy CLAY

BH04 4 1.2 1207335 25/07/2017 Dark brown gravelly, sandy CLAY (Possible made ground - brick)

BH04 11 3.2 1207336 25/07/2017 Black gravelly, sandy CLAY

BH10 6 1.2 1207337 25/07/2017 Brown sandy CLAY

Page 2 of 6

Summary of Chemical AnalysisSoil Samples


Contract Title Warrington Western LinkLab No 1207334 1207335 1207336 1207337

Sample ID BH03 BH04 BH04 BH10Depth 1.70 1.20 3.20 1.20

Other ID 6 4 11 6

Sample Type D B D D

Sampling Date n/s n/s n/s n/s

Sampling Time n/s n/s n/s n/s

Test Method LOD Units

DETSC 2008# 8.3 8.1 7.2 7.3DETSC 2076# 10 mg/l 13 170 860 50

pHSulphate Aqueous Extract as SO4

Inorganics

Page 3 of 6Key: # -MCERTS (accreditation only applies if report carries the MCERTS logo). n/s -not supplied.

Information in Support of the Analytical ResultsOur Ref 17-05850

Client Ref 42103Contract Warrington Western Link

Containers Received & Deviating Samples

Lab No Sample ID

Date

Sampled Containers Received Holding time exceeded for tests

Inappropriate

container for

tests1207334 BH03 1.70 SOIL PT 1L Sample date not supplied, Anions 2:1 (365 days), pH

+ Conductivity (7 days)

1207335 BH04 1.20 SOIL PT 1L Sample date not supplied, Anions 2:1 (365 days), pH






Soil Analysis NotesInorganic soil analysis was carried out on a dried sample, crushed to pass a 425µm sieve, in accordance with BS1377.

Organic soil analysis was carried out on an 'as received' sample. Organics results are corrected for moisture and expressed on a dry weight basis.

The Loss on Drying, used to express organics analysis on an air dried basis, is carried out at a temperature of 28°C +/-2°C.

DisposalFrom the issue date of this test certificate, samples will be held for the following times prior to disposal :-

Soils - 1 month, Liquids - 2 weeks, Asbestos (test portion) - 6 months

Key: P-Plastic T-Tub

DETS cannot be held responsible for the integrity of samples received whereby the laboratory did not undertake the sampling. In this instance samples received may

be deviating. Deviating Sample criteria are based on British and International standards and laboratory trials in conjunction with the UKAS note 'Guidance on

Deviating Samples'. All samples received are listed above. However, those samples that have additional comments in relation to hold time, inappropriate containers

etc are deviating due to the reasons stated. This means that the analysis is accredited where applicable, but results may be compromised due to sample deviations. If

no sampled date (soils) or date+time (waters) has been supplied then samples are deviating. However, if you are able to supply a sampled date (and time for waters)

this will prevent samples being reported as deviating where specific hold times are not exceeded and where the container supplied is suitable.

Page 4 of 6

Appendix A - Details of Analysis

Method Parameter Units

Limit of

Detection

Sample

Preparation Sub-Contracted UKAS MCERTSDETSC 2002 Organic matter % 0.1 Air Dried No Yes Yes

DETSC 2003 Loss on ignition % 0.01 Air Dried No Yes Yes

DETSC 2008 pH pH Units 1 Air Dried No Yes Yes

DETSC 2024 Sulphide mg/kg 10 Air Dried No Yes Yes

DETSC 2076 Sulphate Aqueous Extract as SO4 mg/l 10 Air Dried No Yes Yes

DETSC 2084 Total Carbon % 0.5 Air Dried No Yes Yes

DETSC 2084 Total Organic Carbon % 0.5 Air Dried No Yes Yes

DETSC 2119 Ammoniacal Nitrogen as N mg/kg 0.5 Air Dried No Yes Yes

DETSC 2130 Cyanide free mg/kg 0.1 Air Dried No Yes Yes

DETSC 2130 Cyanide total mg/kg 0.1 Air Dried No Yes Yes

DETSC 2130 Phenol - Monohydric mg/kg 0.3 Air Dried No Yes Yes

DETSC 2130 Thiocyanate mg/kg 0.6 Air Dried No Yes Yes

DETSC 2321 Total Sulphate as SO4 % 0.01 Air Dried No Yes Yes

DETSC 2325 Mercury mg/kg 0.05 Air Dried No Yes Yes

DETSC 3049 Sulphur (free) mg/kg 0.75 Air Dried No Yes Yes

DETSC2123 Boron (water soluble) mg/kg 0.2 Air Dried No Yes Yes

DETSC2301 Arsenic mg/kg 0.2 Air Dried No Yes Yes

DETSC2301 Barium mg/kg 1.5 Air Dried No Yes Yes

DETSC2301 Beryllium mg/kg 0.2 Air Dried No Yes Yes

DETSC2301 Cadmium Available mg/kg 0.1 Air Dried No Yes Yes

DETSC2301 Cadmium mg/kg 0.1 Air Dried No Yes Yes

DETSC2301 Cobalt mg/kg 0.7 Air Dried No Yes Yes

DETSC2301 Chromium mg/kg 0.15 Air Dried No Yes Yes

DETSC2301 Copper mg/kg 0.2 Air Dried No Yes Yes

DETSC2301 Manganese mg/kg 20 Air Dried No Yes Yes

DETSC2301 Molybdenum mg/kg 0.4 Air Dried No Yes Yes

DETSC2301 Nickel mg/kg 1 Air Dried No Yes Yes

DETSC2301 Lead mg/kg 0.3 Air Dried No Yes Yes

DETSC2301 Selenium mg/kg 0.5 Air Dried No Yes Yes

DETSC2301 Zinc mg/kg 1 Air Dried No Yes Yes

DETSC 3072 Ali/Aro C10-C35 mg/kg 10 As Received No Yes Yes

DETSC 3072 Aliphatic C10-C12 mg/kg 1.5 As Received No Yes Yes

DETSC 3072 Aliphatic C10-C12 mg/kg 10 As Received No Yes Yes








DETSC 3072 Aromatic C10-C12 mg/kg 0.9 As Received No Yes Yes

DETSC 3072 Aromatic C10-C12 mg/kg 10 As Received No Yes Yes








DETS 062 Benzene mg/kg 0.01 As Received No Yes Yes

DETS 062 Ethylbenzene mg/kg 0.01 As Received No Yes Yes

DETS 062 Toluene mg/kg 0.01 As Received No Yes Yes

DETS 062 Xylene mg/kg 0.01 As Received No Yes Yes

DETS 062 m+p Xylene mg/kg 0.01 As Received No Yes Yes

DETS 062 o Xylene mg/kg 0.01 As Received No Yes Yes

DETSC 3311 C10-C24 Diesel Range Organics (DRO) mg/kg 10 As Received No Yes Yes

DETSC 3311 C24-C40 Lube Oil Range Organics (LORO) mg/kg 10 As Received No Yes Yes

DETSC 3311 EPH (C10-C40) mg/kg 10 As Received No Yes Yes

Page 5 of 6



Limit of

Detection

Sample

Preparation Sub-Contracted UKAS MCERTSDETSC 3303 Acenaphthene mg/kg 0.03 As Received No Yes Yes

DETSC 3303 Acenaphthylene mg/kg 0.03 As Received No Yes Yes

DETSC 3303 Benzo(a)pyrene mg/kg 0.03 As Received No Yes Yes

DETSC 3303 Benzo(a)anthracene mg/kg 0.03 As Received No Yes Yes

DETSC 3303 Benzo(b)fluoranthene mg/kg 0.03 As Received No Yes Yes

DETSC 3303 Benzo(k)fluoranthene mg/kg 0.03 As Received No Yes Yes

DETSC 3303 Benzo(g,h,i)perylene mg/kg 0.03 As Received No Yes Yes

DETSC 3303 Dibenzo(a,h)anthracene mg/kg 0.03 As Received No Yes Yes

DETSC 3303 Fluoranthene mg/kg 0.03 As Received No Yes Yes

DETSC 3303 Indeno(1,2,3-c,d)pyrene mg/kg 0.03 As Received No Yes Yes

DETSC 3303 Naphthalene mg/kg 0.03 As Received No Yes Yes

DETSC 3303 Phenanthrene mg/kg 0.03 As Received No Yes Yes

DETSC 3303 Pyrene mg/kg 0.03 As Received No Yes Yes

DETSC 3401 PCB 28 + PCB 31 mg/kg 0.01 As Received No Yes Yes

DETSC 3401 PCB 52 mg/kg 0.01 As Received No Yes Yes






DETSC 3401 PCB Total mg/kg 0.01 As Received No Yes Yes

Method details are shown only for those determinands listed in Annex A of the MCERTS standard. Anything not included on this list falls outside the scope of

MCERTS. No Recovery Factors are used in the determination of results. Results reported assume 100% recovery. Full method statements are available on

request.

Page 6 of 6

Certificate Number 04-Aug-17Client

Our Reference

Client Reference

Order No

Contract Title

Description

Date Received

Date Started

Date Completed

Test Procedures

Notes

Approved By

Adam Fenwick






Contracts Manager


5 Soil samples.

Wednesday, August 2, 2017


Friday, August 4, 2017



17-06867


14-15 Rufford Court

Hardwick Grange

Woolston

Warrington

Cheshire

WA1 4RF

17-06867

42103

43100






Sample ID Other ID Depth Lab No Completed Matrix DescriptionCPT01A 14 2.66 1212347 04-Aug-17 Brown gravelly, sandy CLAY

CPT03A 9 1.7 1212348 04-Aug-17 Brown gravelly, sandy CLAY

CPT14A 22 7 1212349 04-Aug-17 Dark brown gravelly, clayey SAND

CPT15A 14 2.7 1212350 04-Aug-17 Brown gravelly, clayey SAND (Made ground - brick)

CPT15A 34 7.2 1212351 04-Aug-17 Dark brown clayey, gravelly SAND (Made ground - brick)

Page 2 of 6



Contract Title Warrington Western LinkLab No 1212347 1212348 1212349 1212350 1212351

Sample ID CPT01A CPT03A CPT14A CPT15A CPT15ADepth 2.66 1.70 7.00 2.70 7.20

Other ID 14 9 22 14 34

Sample Type D D D D D

Sampling Date n/s n/s n/s n/s n/s

Sampling Time n/s n/s n/s n/s n/s


DETSC 2008# 8.0 8.1 7.6 7.0 5.8DETSC 2076# 10 mg/l 73 39 54 56 45


Inorganics





Lab No Sample ID

Date


Inappropriate

container for

tests1212347 CPT01A 2.66 SOIL PT 1L Sample date not supplied, Anions 2:1 (365 days), pH


1212348 CPT03A 1.70 SOIL PT 1L Sample date not supplied, Anions 2:1 (365 days), pH




















Page 4 of 6



Limit of

Detection

Sample



























































Page 5 of 6



Limit of

Detection

Sample
























request.

Page 6 of 6


Our Reference

Client Reference

Order No

Contract Title

Description

Date Received

Date Started

Date Completed

Test Procedures

Notes

Approved By

Adam Fenwick






Contracts Manager

Warrington

5 Soil samples.

10-Aug-17

10-Aug-17

15-Aug-17



17-07515


4 Faraday Close

District 15

Pattinson North Industrial Est

Washington

Tyne & Wear

NE38 8QJ

17-07515

42103B

(not supplied)




Our Ref 17-07515Client Ref 42103B

Contract Title WarringtonLab No 1215642 1215643 1215644 1215645 1215646

Sample ID CPT01A CPT14A CPT14A CPT15A CPT15ADepth 0.80 3.40 6.65 1.85 5.38

Other ID 5 11 20 9 26

Sample Type D D D D D

Sampling Date n/s n/s n/s n/s n/s

Sampling Time n/s n/s n/s n/s n/s


DETSC 2003# 0.01 % 27 2.1 1.4 0.90 3.1DETSC 2002# 0.1 % 6.9 1.5 0.9 < 0.1 2.7

Loss on Ignition at 440oCOrganic matter

Inorganics



Client Ref 42103BContract Warrington


Lab No Sample ID

Date


Inappropriate

container for

tests1215642 CPT01A 0.80 SOIL PT 1L Sample date not supplied, Loss on Ignition (730

days), Organic Matter (Manual) (730 days)

1215643 CPT14A 3.40 SOIL PT 1L Sample date not supplied, Loss on Ignition (730




















Page 3 of 3


Our Reference

Client Reference

Order No

Contract Title

Description

Date Received

Date Started

Date Completed

Test Procedures

Notes

Approved By

Adam Fenwick






Contracts Manager


2 Soil samples.



Friday, August 4, 2017



17-06861


14-15 Rufford Court

Hardwick Grange

Woolston

Warrington

Cheshire

WA1 4RF

17-06861

42103

43100






Sample ID Other ID Depth Lab No Completed Matrix DescriptionBH04 11 3.2 1212317 04-Aug-17 Dark brown gravelly, sandy CLAY (Made ground - coal)

BH06 6 2.2 1212318 04-Aug-17 Brown, slightly gravelly, sandy CLAY

Page 2 of 6



Contract Title Warrington Western LinkLab No 1212317 1212318

Sample ID BH04 BH06Depth 3.20 2.20

Other ID 11 6

Sample Type D D

Sampling Date n/s n/s

Sampling Time n/s n/s


DETSC 2008# 7.6 8.4DETSC 2076# 10 mg/l 1100 32


Inorganics





Lab No Sample ID

Date


Inappropriate

container for

tests1212317 BH04 3.20 SOIL PT 1L Sample date not supplied, Anions 2:1 (365 days), pH
















Page 4 of 6



Limit of

Detection

Sample



























































Page 5 of 6



Limit of

Detection

Sample
























request.

Page 6 of 6


Our Reference

Client Reference

Order No

Contract Title

Description

Date Received

Date Started

Date Completed

Test Procedures

Notes

Approved By

Adam Fenwick






Contracts Manager

Warrington

2 Soil samples.

10-Aug-17

10-Aug-17

14-Aug-17



17-07493


4 Faraday Close

District 15


Washington

Tyne & Wear

NE38 8QJ

17-07493

42103C

(not supplied)




Our Ref 17-07493Client Ref 42103C

Contract Title WarringtonLab No 1215552 1215553

Sample ID BH12A CPT02Depth 2.20 0.50

Other ID 8 3

Sample Type D D

Sampling Date n/s n/s

Sampling Time n/s n/s


DETSC 2003# 0.01 % 9.8 8.5DETSC 2002# 0.1 % 4.3 6.4


Inorganics



Client Ref 42103CContract Warrington


Lab No Sample ID

Date


Inappropriate

container for

tests1215552 BH12A 2.20 SOIL PT 1L Sample date not supplied, Loss on Ignition (730


1215553 CPT02 0.50 SOIL PT 1L Sample date not supplied, Loss on Ignition (730














Page 3 of 3


Our Reference

Client Reference

Order No

Contract Title

Description

Date Received

Date Started

Date Completed

Test Procedures

Notes

Approved By

Adam Fenwick






Contracts Manager

Warrington

One Soil sample.

10-Aug-17

10-Aug-17

14-Aug-17



17-07599


4 Faraday Close

District 15


Washington

Tyne & Wear

NE38 8QJ

17-07599

42103C

(not supplied)




Our Ref 17-07599Client Ref 42103C

Contract Title WarringtonLab No 1216047

Sample ID CPT01Depth 0.50

Other ID 3

Sample Type D

Sampling Date n/s

Sampling Time n/s


DETSC 2003# 0.01 % 7.5DETSC 2002# 0.1 % 4.0


Inorganics



Client Ref 42103CContract Warrington


Lab No Sample ID

Date


Inappropriate

container for

tests1216047 CPT01 0.50 SOIL PB 1L Sample date not supplied, Loss on Ignition (730







Key: P-Plastic B-Bottle







Page 3 of 3


Our Reference

Client Reference

Order No

Contract Title

Description

Date Received

Date Started

Date Completed

Test Procedures

Notes

Approved By

Adam Fenwick






Contracts Manager

Western Link

One Soil sample.

10-Aug-17

10-Aug-17

15-Aug-17



17-07495


14-15 Rufford Court

Hardwick Grange

Woolston

Warrington

Cheshire

WA1 4RF

17-07495

42103

43146





Contract Title Western LinkLab No 1215555

Sample ID BH04ADepth 26.00

Other ID 5

Sample Type D

Sampling Date n/s

Sampling Time n/s


DETSC 2008# 8.3DETSC 2076# 10 mg/l 890


Inorganics



Client Ref 42103Contract Western Link


Lab No Sample ID

Date


Inappropriate

container for

tests1215555 BH04A 26.00 SOIL PT 1L Sample date not supplied, Anions 2:1 (365 days), pH














Page 3 of 3


Our Reference

Client Reference

Order No

Contract Title

Description

Date Received

Date Started

Date Completed

Test Procedures

Notes

Approved By

Adam Fenwick






Contracts Manager


One Soil sample.

23-Aug-17

23-Aug-17

29-Aug-17



17-08461


14-15 Rufford Court

Hardwick Grange

Woolston

Warrington

Cheshire

WA1 4RF

17-08461

42103

(not supplied)






Sample ID Other ID Depth Lab No Completed Matrix DescriptionCPT14A TUB 2 OF 3 1 1220745 29/08/2017 Dark brown sandy CLAY

Page 2 of 6



Contract Title Warrington Western LinkLab No 1220745

Sample ID CPT14ADepth 1.00

Other ID TUB 2 OF 3

Sample Type D

Sampling Date 12/07/17

Sampling Time n/s


DETSC 2008# 8.2DETSC 2076# 10 mg/l 23


Inorganics





Lab No Sample ID

Date


Inappropriate

container for

tests1220745 CPT14A 1.00 SOIL 12/07/17 PT 500ml pH + Conductivity (7 days)













Page 4 of 6



Limit of

Detection

Sample



























































Page 5 of 6



Limit of

Detection

Sample
























request.

Page 6 of 6

Figure A3.2

Split, Photograph and Describe Records

Western Link

Split and Describe Samples BH04

Contract No. 42103

BH04 - U18 - 6.20m – 6.65m

Description: Soft, greyish brown, slightly sandy clayey SILT

Western Link


Contract No. 42103

B2 – 0.50m – 1.00m

Description: MADE GROUND: Brown, slightly silty, very sandy GRAVEL with occasional inclusions of soft brown slightly sandy slightly gravelly clay. Gravel is angular fine to coarse (dark grey) limestone.

Western Link


Contract No. 42103

Sample 5 – 2.00m- 2.45m

Description: MADE GROUND: Very soft, black CLAY and clayey SAND with inclusions of rubber and metal (nails). Pungent odour of hydrocarbons.

Western Link


Contract No. 42103

U26 – 14.00m – 14.45

Description: (Stiff) light brown slightly sandy slightly gravelly CLAY. Gravel is angular to subrounded fine to coarse sandstone and mudstone.

Western Link


Contract No. 42103

UT2 – 1.20m – 1.65m

Description: (Firm) orangey brown, slightly sandy CLAY. Root noted.

Western Link


Contract No. 42103

U7 - 1.20m – 1.65m

Description: Soft, black, locally light brown, slightly sandy organic CLAY with occasional decaying roots/rootlets. Organic odour noted.

Western Link


Contract No. 42103

U20 - 9.20m – 9.65m

Description: Brown, silty fine and medium SAND, thinly and thickly interlaminated with soft brown CLAY.

Western Link

Split and Describe Samples BH12A

Contract No. 42103

BH12A – 2.00m to 2.65m

Description: Dark, orangey brown, silty SAND and GRAVEL. Sand is fine to coarse. Gravel is angular and subangular fine to coarse of coal, burnt shale and occasional brick.

Figure A3.3

Results of Rock Testing

Site:

Job Number:

Originating Client:


Date Sampled:

Date Scheduled:



Remarks:

Authorised By:

Page. 1



Warrington (01925) 855 440.



F.A.O.

Test Report - 42103R / 2


42103R


42103

Not Given

03/08/2017

15/08/2017

16/08/2017

Paul Cathcart

Site:

Client:

Lne W Dps Dps'

Is

.

Is

(50)

mm mm mm mm kN mm MPa MPa

BH10 14.10 D PL YES 35.7 86.0 86.0 85.0 0.1 86.0 0.016 0.021

BH10 14.10 A PD YES 85.3 38.3 34.3 0.1 64.5 0.024 0.027

BH10 20.21 D PL YES 36.1 84.1 84.1 82.1 0.4 84.1 0.059 0.075

BH10 20.21 A PD NO 84.6 70.6 57.6 0.2 87.2 0.024 0.031

BH10 20.80 D PL YES 103.0 85.5 85.5 82.5 0.6 85.5 0.085 0.109

BH10 20.80 A PD YES 85.7 108.4 96.4 2.0 108.7 0.166 0.235

BH10 21.78 D PL YES 51.0 86.2 86.2 84.2 0.5 86.2 0.070 0.089

BH10 21.78 A PD YES 86.0 50.1 46.1 0.0 74.0 0.004 0.005

BH10 22.25 D PL YES 85.2 85.4 85.4 81.4 1.1 85.4 0.145 0.184

BH10 22.25 A PD YES 85.5 101.3 93.3 0.0 105.0 0.002 0.003

BH10 22.80 l U YES 24.2 50.2 31.5 28.5 0.0 44.9 0.007 0.007

BH10 22.80 l U YES 27.6 56.5 25.5 21.5 0.0 42.9 0.006 0.006

BH10 22.80 l U YES 27.3 54.3 25.7 22.7 0.0 42.1 0.005 0.005

BH10 23.38 D PL YES 53.8 84.9 84.9 82.9 0.0 84.9 0.004 0.005

BH10 23.38 A PD YES 86.6 52.0 47.0 0.7 75.7 0.124 0.150

BH12 6.82 D PL YES 43.7 84.7 84.7 83.7 0.0 84.7 0.004 0.005

BH12 6.82 A PD YES 85.5 55.5 53.5 0.1 77.7 0.024 0.029

BH12 7.60 D PL YES 19.6 84.4 84.4 82.4 0.2 84.4 0.022 0.028

BH12 7.60 A PD YES 84.1 47.3 31.3 0.2 71.2 0.041 0.048

BH12 8.84 D PL YES 28.8 85.2 85.2 82.2 0.0 85.2 0.004 0.005

Laboratory Test Report 42103R / 2

Warrington Western Link Job Number: 42103R

Warrington Borough Council Page: 2

Point Load Strength Index TestsSummary of Results

BoreholeNo. Depth

m

SampleRock Type

andTest condition

Test Typesee ISRM

Failu

re V

alid

(Y/N

)

DimensionsForce

P

Equi

vale

nt

diam

eter

, De Point Load

Strength Index Remarks(including water

content if measured)Ty

pe(D

, A, I

, B)

Dire

ctio

n(L

, P o

r U)

C19 Brown SANDSTONEAs received




















Test TypeD - Diametral, A - Axial, I - Irregular Lump, B - BlockDirection L - parallel to planes of weaknessP - perpendicular to planes of weaknessU - unknown or randomDimensions Dps - Distance between platens ( platen separation )Dps' - at failure ( see ISRM note 6)Lne - Length from platens to nearest free endW - Width of shortest dimension perpendicular to load, PSize factor, F = (De/50)0.45 for all tests.

Detailed legend for test and dimensions, based on ISRM

Method of Preparation: ISRM 2007 Suggested method for point load strength index (pages 125 - 132)

Method of Test: ISRM 2007 Suggested method for point load strength index (pages 125 - 132)

P

WDps

Axial

P

W

Lne Dps

Block/irregular lumpDiametral

Dps

P

Lne

W

Site:

Client:

Lne W Dps Dps'

Is

.

Is

(50)


BH12 8.84 A PD YES 86.0 29.2 27.2 0.0 56.5 0.009 0.010

BH12 9.66 D PL YES 27.6 86.6 86.6 84.6 0.0 86.6 0.004 0.005

BH12 9.66 A PD YES 84.5 28.9 26.9 0.1 55.8 0.039 0.041

BH12 13.50 D PL YES 45.5 85.6 85.6 82.6 0.0 85.6 0.000 0.010

BH12 13.50 A PD YES 87.3 48.7 45.7 0.0 73.6 0.000 0.010

BH12 15.39 D PL YES 31.8 83.4 83.4 79.4 0.1 83.4 0.020 0.020

BH12 15.39 A PD YES 85.1 31.9 30.9 0.1 58.8 0.020 0.030

BH12 15.70 D PL YES 30.6 84.6 84.6 82.6 0.1 84.6 0.020 0.020

BH12 15.70 A PD YES 86.3 57.3 48.3 0.2 79.4 0.040 0.050

Laboratory Test Report 42103R / 2

Warrington Western Link Job Number: 42103R



BoreholeNo. Depth

m

SampleRock Type

andTest condition

Test Typesee ISRM

Failu

re V

alid

(Y/N

)

DimensionsForce

P

Equi

vale

nt

diam

eter

, De Point Load



pe(D

, A, I

, B)

Dire

ctio

n(L

, P o

r U)














P

WDps

Axial

P

W

Lne Dps


Dps

P

Lne

W

Dia. Length H/D Condition Stress Rate UCS

mm mm Mg/m3 % MPa/s MPa

85.8 140.7 *1.6 2.25 11.2 as received 0.5015 AC 5.6

ISRM p87 test 1, water content at 105 ± 3 oC, specimen as tested for UCS *Denotes length diameter ratio outside ISRM specification2 ISRM p86 clause (vii), Caliper method used for determination of bulk volume and derivation of bulk density Mode of failure :3 ISRM p153 part 1, determination of Uniaxial Compressive Strength ( UCS ) of Rock Materials S - Single shear MS - multiple shear

above notes apply unless annotated otherwise in the remarks AC - Axial cleavage F - Fragmented

42103R / 2

Site: Warrington Western Link Job Number: 42103R

Depth

m

Sample Rock Type

Specimen Dimensions2

Laboratory Test Report

Uniaxial Compression3

RemarksMode of

failure


UNIAXIAL COMPRESSION TEST ON ROCK - SUMMARY OF RESULTS

Hole No.

BH10 22.80 C24 Brown SANDSTONE

Bulk Density2

Water Content

1

Notes 1

Method of Preparation: International Society for Rock Mechanics, The complete ISRM suggested methods for Rock Characterization Testing and Monitoring, 2007

Method of Test: International Society for Rock Mechanics, The complete ISRM suggested methods for Rock Characterization Testing and Monitoring, 2007

Site:

Job Number:

Originating Client:

Page. 5


42103R




Date: 22/08/2017

Test Report - 42103R / 2

Site:

Job Number:

Originating Client:


Date Sampled:

Date Scheduled:



Remarks:

Authorised By:

Page. 1



Warrington (01925) 855 440.



F.A.O.

Test Report - 42103R2 / 1


42103R2


42103

Not Given

10/08/2017

15/08/2017

16/08/2017

Paul Cathcart

Site:

Client:

Lne W Dps Dps'

Is

.

Is

(50)


BH07 21.00 D PL YES 35.3 83.9 83.9 80.9 0.0 83.9 0.002 0.002

BH07 21.00 A PD YES 85.0 39.3 37.3 0.0 65.2 0.003 0.003

BH07 22.66 D PL YES 27.0 84.9 84.9 82.9 0.2 84.9 0.024 0.031

BH07 22.66 A PD YES 85.8 31.2 28.2 0.2 58.4 0.048 0.051

BH07 23.87 D PL YES 38.9 85.0 85.0 82.0 0.3 85.0 0.048 0.061

BH07 23.87 A PD YES 82.3 32.6 29.6 0.0 58.4 0.005 0.005

BH07 24.17 D PL YES 43.1 86.1 86.1 83.1 0.0 86.1 0.002 0.003

BH07 24.17 A PD YES 86.4 69.2 56.2 0.0 87.3 0.003 0.003

Laboratory Test Report 42103R2 / 1

Warrington Western Link Job Number: 42103R2



BoreholeNo. Depth

m

SampleRock Type

andTest condition

Test Typesee ISRM

Failu

re V

alid

(Y/N

)

DimensionsForce

P

Equi

vale

nt

diam

eter

, De Point Load



pe(D

, A, I

, B)

Dire

ctio

n(L

, P o

r U)













P

WDps

Axial

P

W

Lne Dps


Dps

P

Lne

W

Site:

Job Number:

Originating Client:

Page. 3


42103R2




Date: 16/08/2017

Test Report - 42103R2 / 1

APPENDIX 4

CHEMICAL LABORATORY TEST RESULTS

Figure A4.1

Results of Chemical Tests – Soil and Leachate

Concept Life Sciences


Hadfield HouseHadfield Street

CornbrookManchester

M16 9FETel : 0161 874 2400Fax : 0161 874 2468

Report Number: 666658-1

Date of Report: 27-Jul-2017

Customer: Ian Farmer Associates14-15 Rufford CourtHardwick GrangeWarringtonCheshireWA1 4RF

Customer Contact: Ms Michelle Hirst-Watson

Customer Job Reference: 42103Customer Purchase Order: 42961Customer Site Reference: Western Link

Date Job Received at Concept: 06-Jul-2017Date Analysis Started: 11-Jul-2017

Date Analysis Completed: 27-Jul-2017

The results reported relate to samples received in the laboratory and may not be representative of a wholebatch.Opinions and interpretations expressed herein are outside the scope of UKAS accreditationThis report should not be reproduced except in full without the written approval of the laboratoryTests covered by this certificate were conducted in accordance with Concept SOPsAll results have been reviewed in accordance with Section 25 of the Concept, Analytical Quality QualityManual

This document has been printed from a digitally signed master copy

Concept Life Sciences is a trading name of

Scientific Analysis Laboratories registered in England and

Wales (No 2514788)

1549

Report checkedand authorised by :Stefan KondzielaProject Manager

Issued by :Stefan KondzielaProject Manager

Page 1 of 18

666658-1

Concept Reference: 666658

Project Site: Western Link

Customer Reference: 42103

Soil Analysed as Soil

MCERTS Preparation

Concept Reference 666658 001 666658 002 666658 003 666658 004 666658 005

Customer Sample Reference CPT01A CPT03A CPT14A CPT14A CPT14A

Test Sample AR AR AR AR AR

Bottom Depth 2.20 2.20 2.20 3.40 5.80

Top Depth 1.20 1.20 1.20 2.40 4.80

Date Sampled 30-JUN-2017 28-JUN-2017 03-JUL-2017 03-JUL-2017 03-JUL-2017

Matrix Class Sandy Soil Sandy Soil Sandy Soil Sandy Soil Sandy Soil

Determinand Method LOD Units Symbol

Moisture @105C Grav (1 Dec) (105 C) 0.1 % N 22 14 5.7 24 24





MCERTS Preparation

Concept Reference 666658 006 666658 007 666658 008

Customer Sample Reference CPT15A CPT15A CPT15A

Test Sample AR AR AR

Bottom Depth 2.20 4.60 7.00

Top Depth 1.20 3.60 6.00

Date Sampled 30-JUN-2017 30-JUN-2017 30-JUN-2017

Matrix Class Sandy Soil Sandy Soil Sandy Soil


Moisture @105C Grav (1 Dec) (105 C) 0.1 % N 30 20 16





MCERTS Preparation



Test Sample M40 M40 M40 M40 M40

Bottom Depth 2.20 2.20 2.20 3.40 5.80

Top Depth 1.20 1.20 1.20 2.40 4.80




Retained on 10mm sieve Grav 0.1 % N <0.1 <0.1 <0.1 <0.1 <0.1





MCERTS Preparation



Test Sample M40 M40 M40


Top Depth 1.20 3.60 6.00




Retained on 10mm sieve Grav 0.1 % N <0.1 <0.1 <0.1


Produced by Concept Life Sciences, Hadfield House, Hadfield Street, Cornbrook, Manchester, M16 9FE Page 2 of 18

666658-1





Soil Suite



Test Sample A40 A40 A40 A40 A40

Bottom Depth 2.20 2.20 2.20 3.40 5.80

Top Depth 1.20 1.20 1.20 2.40 4.80




Sulphate (Total) ICP/OES 0.01 % N 1.2 0.02 0.09 0.19 0.16

Sulphur (total) ICP/OES 0.01 % N 0.52 0.01 0.06 0.13 0.10

Total Organic Carbon OX/IR 0.1 % N 19 0.4 3.9 1.2 1.6





Soil Suite



Test Sample A40 A40 A40


Top Depth 1.20 3.60 6.00




Sulphate (Total) ICP/OES 0.01 % N 0.37 0.11 0.05

Sulphur (total) ICP/OES 0.01 % N 0.39 0.04 0.03

Total Organic Carbon OX/IR 0.1 % N 3.7 0.5 1.0





Soil Suite




Bottom Depth 2.20 2.20 2.20 3.40 5.80

Top Depth 1.20 1.20 1.20 2.40 4.80




Boron (water-soluble) ICP/OES 1 mg/kg N <1 <1 <1 <1 <1

Cyanide (Total) Colorimetry (CF) 1 mg/kg M <1 <1 <1 7 8

Total Phenols GC/MS (MCERTS) 0.1 mg/kg N <0.1 <0.1 <0.1 <0.1 <0.1

Sulphide Colorimetry 10 mg/kg N 95 20 160 200 38

Asbestos ID PLM SU N.D. N.D. N.D. N.D. N.D.

pH Probe M 6.9 7.7 7.9 7.8 7.5



666658-1





Soil Suite



Test Sample AR AR AR


Top Depth 1.20 3.60 6.00




Boron (water-soluble) ICP/OES 1 mg/kg N <1 <1 <1

Cyanide (Total) Colorimetry (CF) 1 mg/kg M 15 2 <1

Total Phenols GC/MS (MCERTS) 0.1 mg/kg N <0.1 <0.1 <0.1

Sulphide Colorimetry 10 mg/kg N <10 <10 <10

Asbestos ID PLM SU N.D. N.D. N.D.

pH Probe M 7.3 7.4 7.5





Soil Suite




Bottom Depth 2.20 2.20 2.20 3.40 5.80

Top Depth 1.20 1.20 1.20 2.40 4.80




Arsenic ICP/OES 2 mg/kg M 140 6 22 24 47

Cadmium ICP/OES 1 mg/kg M 2 <1 1 4 2

Chromium ICP/OES 1 mg/kg M 56 29 33 39 84

Copper ICP/OES 1 mg/kg M 620 20 57 87 85

Lead ICP/OES 1 mg/kg M 370 28 96 110 150

Nickel ICP/OES 1 mg/kg M 160 28 34 18 25

Mercury ICP/OES 1 mg/kg M <1 <1 <1 <1 2

Selenium ICP/OES 3 mg/kg M <3 <3 <3 <3 <3

Vanadium ICP/OES 1 mg/kg M 120 27 31 17 25

Zinc ICP/OES 1 mg/kg M 950 47 270 760 720



666658-1





Soil Suite





Top Depth 1.20 3.60 6.00




Arsenic ICP/OES 2 mg/kg M 48 21 69

Cadmium ICP/OES 1 mg/kg M 5 2 2

Chromium ICP/OES 1 mg/kg M 85 33 73

Copper ICP/OES 1 mg/kg M 140 45 48

Lead ICP/OES 1 mg/kg M 180 65 100

Nickel ICP/OES 1 mg/kg M 32 14 19

Mercury ICP/OES 1 mg/kg M 2 <1 <1

Selenium ICP/OES 3 mg/kg M <3 <3 <3

Vanadium ICP/OES 1 mg/kg M 31 14 15

Zinc ICP/OES 1 mg/kg M 900 470 490





PAH USEPA16




Bottom Depth 2.20 2.20 2.20 3.40 5.80

Top Depth 1.20 1.20 1.20 2.40 4.80




Naphthalene GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1 0.1

Acenaphthylene GC/MS (MCERTS) 0.1 mg/kg U <0.1 <0.1 <0.1 <0.1 <0.1

Acenaphthene GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1 <0.1

Fluorene GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1 <0.1

Phenanthrene GC/MS (MCERTS) 0.1 mg/kg M 0.3 <0.1 <0.1 0.2 0.3

Anthracene GC/MS (MCERTS) 0.1 mg/kg U <0.1 <0.1 <0.1 <0.1 <0.1

Fluoranthene GC/MS (MCERTS) 0.1 mg/kg M 0.8 <0.1 <0.1 0.5 0.4

Pyrene GC/MS (MCERTS) 0.1 mg/kg M 0.8 <0.1 <0.1 0.5 0.3

Benzo(a)Anthracene GC/MS (MCERTS) 0.1 mg/kg M 0.4 <0.1 <0.1 0.2 0.2

Chrysene GC/MS (MCERTS) 0.1 mg/kg M 0.5 <0.1 <0.1 0.3 0.2

Benzo(b)fluoranthene GC/MS (MCERTS) 0.1 mg/kg M 0.5 <0.1 <0.1 0.2 0.1

Benzo(k)fluoranthene GC/MS (MCERTS) 0.1 mg/kg M 0.5 <0.1 <0.1 0.2 0.2

Benzo(a)Pyrene GC/MS (MCERTS) 0.1 mg/kg M 0.5 <0.1 <0.1 0.2 0.1

Indeno(123-cd)Pyrene GC/MS (MCERTS) 0.1 mg/kg M 0.3 <0.1 <0.1 0.1 <0.1

Dibenzo(ah)Anthracene GC/MS (MCERTS) 0.1 mg/kg M 0.1 <0.1 <0.1 <0.1 <0.1

Benzo(ghi)Perylene GC/MS (MCERTS) 0.1 mg/kg M 0.3 <0.1 <0.1 0.1 <0.1

Polyaromatic Hydrocarbons (Total) GC/MS (MCERTS) 0.1 mg/kg U 4.9 <0.1 <0.1 2.7 1.9



666658-1





PAH USEPA16





Top Depth 1.20 3.60 6.00




Naphthalene GC/MS (MCERTS) 0.1 mg/kg M 0.2 <0.1 <0.1

Acenaphthylene GC/MS (MCERTS) 0.1 mg/kg U 0.3 <0.1 <0.1

Acenaphthene GC/MS (MCERTS) 0.1 mg/kg M 0.1 <0.1 <0.1

Fluorene GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1

Phenanthrene GC/MS (MCERTS) 0.1 mg/kg M 0.6 0.1 0.1

Anthracene GC/MS (MCERTS) 0.1 mg/kg U 0.2 <0.1 <0.1

Fluoranthene GC/MS (MCERTS) 0.1 mg/kg M 1.3 0.3 0.2

Pyrene GC/MS (MCERTS) 0.1 mg/kg M 1.2 0.3 0.2

Benzo(a)Anthracene GC/MS (MCERTS) 0.1 mg/kg M 0.7 0.2 0.2

Chrysene GC/MS (MCERTS) 0.1 mg/kg M 0.8 0.2 0.2

Benzo(b)fluoranthene GC/MS (MCERTS) 0.1 mg/kg M 1.0 0.2 0.1

Benzo(k)fluoranthene GC/MS (MCERTS) 0.1 mg/kg M 0.8 0.2 0.2

Benzo(a)Pyrene GC/MS (MCERTS) 0.1 mg/kg M 1.0 0.2 0.1

Indeno(123-cd)Pyrene GC/MS (MCERTS) 0.1 mg/kg M 0.7 0.1 <0.1

Dibenzo(ah)Anthracene GC/MS (MCERTS) 0.1 mg/kg M 0.2 <0.1 <0.1

Benzo(ghi)Perylene GC/MS (MCERTS) 0.1 mg/kg M 0.7 0.1 <0.1

Polyaromatic Hydrocarbons (Total) GC/MS (MCERTS) 0.1 mg/kg U 9.9 2.0 1.3





PCB EC7




Bottom Depth 2.20 2.20 2.20 3.40 5.80

Top Depth 1.20 1.20 1.20 2.40 4.80




Polychlorinated biphenyl BZ#28 GC/MS (HR) (MCERTS) 0.05 µg/kg M (9,26) <10 (26) <1.0 (26,9) <10 (26) <1.0 (26) <1.0









666658-1





PCB EC7





Top Depth 1.20 3.60 6.00




Polychlorinated biphenyl BZ#28 GC/MS (HR) (MCERTS) 0.05 µg/kg M (9,26) <10 (26) <1.0 (26) <1.0











TPH (CWG) with MTBE, BTEX

Concept Reference 666658001

666658002

666658003

666658004

666658005



Bottom Depth 2.20 2.20 2.20 3.40 5.80

Top Depth 1.20 1.20 1.20 2.40 4.80

Date Sampled 30-JUN-2017

28-JUN-2017

03-JUL-2017

03-JUL-2017

03-JUL-2017

Matrix Class SandySoil

SandySoil

SandySoil

SandySoil

SandySoil


Benzene GC/MS (Head Space)(MCERTS) 10 µg/kg M (110,13) <20 (13) <10 (13) <10 (13) <10 (13) <10

Toluene GC/MS (Head Space)(MCERTS) 10 µg/kg M (110) <20 <10 <10 <10 <10

EthylBenzene GC/MS (Head Space)(MCERTS) 10 µg/kg M (110) <20 <10 <10 <10 <10

Meta/Para-Xylene GC/MS (Head Space)(MCERTS) 10 µg/kg M (110) <20 <10 <10 <10 <10

Ortho-Xylene GC/MS (Head Space)(MCERTS) 10 µg/kg M (110) <20 <10 <10 <10 <10

Methyl tert-Butyl Ether GC/MS (Head Space)(MCERTS) 10 µg/kg M (110) <20 <10 <10 <10 <10

Total Petroleum Hydrocarbons (C5 - C6 aliphatic) GC/MS (Head Space)(MCERTS) 0.100 mg/kg N (110)

<0.200<0.100 <0.100 <0.100 <0.100

Total Petroleum Hydrocarbons (C6-C8 aliphatic) GC/MS (Head Space)(MCERTS) 0.10 mg/kg N (110) <0.20 <0.10 <0.10 <0.10 <0.10

Total Petroleum Hydrocarbons (C8-C10 aliphatic) GC/MS (Head Space)(MCERTS) 0.10 mg/kg N (110) <0.20 <0.10 <0.10 0.78 <0.10

Total Petroleum Hydrocarbons (C10-C12 aliphatic) GCxGC 1 mg/kg M (9,13) <10 (13) <1 (13,9) <10 (13) <1 (13) <1

Total Petroleum Hydrocarbons (C12-C16 aliphatic) GCxGC 1 mg/kg M (13) 12 (13) <1 (13,9) <10 (13) <1 (13) <1

Total Petroleum Hydrocarbons (C16-C21 aliphatic) GCxGC 1 mg/kg M (13,9) <10 (13) <1 (9,13) <10 (13) <1 (13) <1

Total Petroleum Hydrocarbons (C21-C35 aliphatic) GCxGC 2 mg/kg M (13) 98 (13) <2 (13) 18 (13) <2 (13) <2

Total Petroleum Hydrocarbons (C35-C40 aliphatic) GCxGC 1 mg/kg N (13) 37 (13) <1 (9,13) <10 (13) <1 (13) <1

Total Petroleum Hydrocarbons (Aliphatic) total Calc mg/kg N (13) 150 (13) N.D. (13) 18 (13) 0.78 (13) N.D.

Total Petroleum Hydrocarbons (C6 - C7 aromatic) GC/MS (Head Space)(MCERTS) 0.10 mg/kg N (110) <0.20 <0.10 <0.10 <0.10 <0.10

Total Petroleum Hydrocarbons (C7-C8 aromatic) GC/MS (Head Space)(MCERTS) 0.10 mg/kg N (110) <0.20 <0.10 <0.10 <0.10 <0.10

Total Petroleum Hydrocarbons (C8-C10 aromatic) GC/MS (Head Space)(MCERTS) 0.10 mg/kg N (110) <0.20 <0.10 <0.10 <0.10 <0.10

Total Petroleum Hydrocarbons (C10-C12 aromatic) GCxGC 2 mg/kg M (9,13) <10 (13) <2 (13,9) <10 (13) <2 (13) <2

Total Petroleum Hydrocarbons (C12-C16 aromatic) GCxGC 1 mg/kg M (13) 19 (13) <1 (9,13) <10 (13) 2 (13) 2

Total Petroleum Hydrocarbons (C16-C21 aromatic) GCxGC 1 mg/kg M (13) 26 (13) <1 (9,13) <10 (13) 5 (13) 5

Total Petroleum Hydrocarbons (C21-C35 aromatic) GCxGC 1 mg/kg M (13) 42 (13) <1 (13) 17 (13) 18 (13) 15

Total Petroleum Hydrocarbons (C35-C40 aromatic) GCxGC 1 mg/kg N (13,9) <10 (13) <1 (13,9) <10 (13) <1 (13) <1

Total Petroleum Hydrocarbons (Aromatic) total Calc mg/kg N (13) 42 (13) N.D. (13) 17 (13) 25 (13) 22

Total Petroleum Hydrocarbons (Aliphatic+Aromatic) Calc mg/kg N (13) 190 (13) N.D. (13) 35 (13) 26 (13) 22



666658-1







666658007

666658008




Top Depth 1.20 3.60 6.00


30-JUN-2017

30-JUN-2017


SandySoil

SandySoil


Benzene GC/MS (Head Space)(MCERTS) 10 µg/kg M (13) <10 (13) <10 (13) <10

Toluene GC/MS (Head Space)(MCERTS) 10 µg/kg M <10 <10 <10

EthylBenzene GC/MS (Head Space)(MCERTS) 10 µg/kg M <10 <10 <10

Meta/Para-Xylene GC/MS (Head Space)(MCERTS) 10 µg/kg M <10 <10 <10

Ortho-Xylene GC/MS (Head Space)(MCERTS) 10 µg/kg M <10 <10 <10

Methyl tert-Butyl Ether GC/MS (Head Space)(MCERTS) 10 µg/kg M <10 <10 <10

Total Petroleum Hydrocarbons (C5 - C6 aliphatic) GC/MS (Head Space)(MCERTS) 0.100 mg/kg N <0.100 <0.100 <0.100

Total Petroleum Hydrocarbons (C6-C8 aliphatic) GC/MS (Head Space)(MCERTS) 0.10 mg/kg N <0.10 <0.10 <0.10

Total Petroleum Hydrocarbons (C8-C10 aliphatic) GC/MS (Head Space)(MCERTS) 0.10 mg/kg N <0.10 <0.10 <0.10

Total Petroleum Hydrocarbons (C10-C12 aliphatic) GCxGC 1 mg/kg M (13) <1 (13) <1 (13) <1

Total Petroleum Hydrocarbons (C12-C16 aliphatic) GCxGC 1 mg/kg M (13) 3 (13) <1 (13) <1



Total Petroleum Hydrocarbons (C35-C40 aliphatic) GCxGC 1 mg/kg N (13) 2 (13) <1 (13) <1

Total Petroleum Hydrocarbons (Aliphatic) total Calc mg/kg N (13) 16 (13) N.D. (13) N.D.

Total Petroleum Hydrocarbons (C6 - C7 aromatic) GC/MS (Head Space)(MCERTS) 0.10 mg/kg N <0.10 <0.10 <0.10

Total Petroleum Hydrocarbons (C7-C8 aromatic) GC/MS (Head Space)(MCERTS) 0.10 mg/kg N <0.10 <0.10 <0.10

Total Petroleum Hydrocarbons (C8-C10 aromatic) GC/MS (Head Space)(MCERTS) 0.10 mg/kg N <0.10 <0.10 <0.10

Total Petroleum Hydrocarbons (C10-C12 aromatic) GCxGC 2 mg/kg M (13) <2 (13) <2 (13) <2

Total Petroleum Hydrocarbons (C12-C16 aromatic) GCxGC 1 mg/kg M (13) 6 (13) 2 (13) <1

Total Petroleum Hydrocarbons (C16-C21 aromatic) GCxGC 1 mg/kg M (13) 25 (13) 6 (13) 2

Total Petroleum Hydrocarbons (C21-C35 aromatic) GCxGC 1 mg/kg M (13) 88 (13) 22 (13) 9

Total Petroleum Hydrocarbons (C35-C40 aromatic) GCxGC 1 mg/kg N (13) <1 (13) <1 (13) <1

Total Petroleum Hydrocarbons (Aromatic) total Calc mg/kg N (13) 120 (13) 30 (13) 11

Total Petroleum Hydrocarbons (Aliphatic+Aromatic) Calc mg/kg N (13) 140 (13) 30 (13) 11



666658-1





Volatile Organic Compounds (USEPA 624)




Bottom Depth 2.20 2.20 2.20 3.40 5.80

Top Depth 1.20 1.20 1.20 2.40 4.80




Dichlorodifluoromethane GC/MS (Head Space)(MCERTS) 50 µg/kg M (110) <100 <50 <50 <50 <50

Chloromethane GC/MS (Head Space)(MCERTS) 50 µg/kg U (110) <100 <50 <50 <50 <50

Vinyl chloride monomer GC/MS (Head Space)(MCERTS) 50 µg/kg M (110) <100 <50 <50 <50 <50

Bromomethane GC/MS (Head Space)(MCERTS) 50 µg/kg U (110) <100 <50 <50 <50 <50

Chloroethane GC/MS (Head Space)(MCERTS) 50 µg/kg M (110) <100 <50 <50 <50 <50

Trichlorofluoromethane GC/MS (Head Space)(MCERTS) 50 µg/kg M (110) <100 <50 <50 <50 <50

1,1-Dichloroethylene GC/MS (Head Space)(MCERTS) 50 µg/kg M (110) <100 <50 <50 <50 <50

Dichloromethane GC/MS (Head Space)(MCERTS) 50 µg/kg U (110) <100 <50 <50 <50 <50

Trans-1,2-Dichloroethylene GC/MS (Head Space)(MCERTS) 50 µg/kg M (110) <100 <50 <50 <50 <50

1,1-Dichloroethane GC/MS (Head Space)(MCERTS) 50 µg/kg M (110) <100 <50 <50 <50 <50

Cis-1,2-Dichloroethylene GC/MS (Head Space)(MCERTS) 50 µg/kg M (110) <100 <50 <50 <50 <50

2,2-Dichloropropane GC/MS (Head Space)(MCERTS) 50 µg/kg U (110) <100 <50 <50 <50 <50

Chloroform GC/MS (Head Space)(MCERTS) 50 µg/kg M (110) <100 <50 <50 <50 <50

Bromochloromethane GC/MS (Head Space)(MCERTS) 50 µg/kg M (110) <100 <50 <50 <50 <50

1,1,1-Trichloroethane GC/MS (Head Space)(MCERTS) 50 µg/kg M (110) <100 <50 <50 <50 <50

1,1-Dichloropropene GC/MS (Head Space)(MCERTS) 50 µg/kg M (110) <100 <50 <50 <50 <50

Carbon tetrachloride GC/MS (Head Space)(MCERTS) 50 µg/kg M (110) <100 <50 <50 <50 <50



1,2-Dichloropropane GC/MS (Head Space)(MCERTS) 50 µg/kg M (110) <100 <50 <50 <50 <50

Trichloroethylene GC/MS (Head Space)(MCERTS) 50 µg/kg M (110) <100 <50 <50 <50 <50

Bromodichloromethane GC/MS (Head Space)(MCERTS) 50 µg/kg M (110) <100 <50 <50 <50 <50

Dibromomethane GC/MS (Head Space)(MCERTS) 50 µg/kg M (110) <100 <50 <50 <50 <50

Cis-1,3-Dichloropropene GC/MS (Head Space)(MCERTS) 50 µg/kg M (110) <100 <50 <50 <50 <50


Trans-1,3-Dichloropropene GC/MS (Head Space)(MCERTS) 50 µg/kg M (110) <100 <50 <50 <50 <50



Tetrachloroethylene GC/MS (Head Space)(MCERTS) 50 µg/kg M (110) <100 <50 <50 <50 <50

Chlorodibromomethane GC/MS (Head Space)(MCERTS) 50 µg/kg M (110) <100 <50 <50 <50 <50

1,2-dibromoethane GC/MS (Head Space)(MCERTS) 50 µg/kg M (110) <100 <50 <50 <50 <50

Chlorobenzene GC/MS (Head Space)(MCERTS) 50 µg/kg M (110) <100 <50 <50 <50 <50

1,1,1,2-Tetrachloroethane GC/MS (Head Space)(MCERTS) 50 µg/kg M (110) <100 <50 <50 <50 <50


Meta/Para-Xylene GC/MS (Head Space)(MCERTS) 10 µg/kg M (110) <20 <10 <10 <10 <10


Styrene GC/MS (Head Space)(MCERTS) 50 µg/kg U (110) <100 <50 <50 <50 <50

Bromoform GC/MS (Head Space)(MCERTS) 50 µg/kg M (110) <100 <50 <50 <50 <50

Isopropyl benzene GC/MS (Head Space)(MCERTS) 50 µg/kg M (110) <100 <50 <50 <50 <50

1,1,2,2-Tetrachloroethane GC/MS (Head Space)(MCERTS) 50 µg/kg U (110) <100 <50 <50 <50 <50

1,2,3-Trichloropropane GC/MS (Head Space)(MCERTS) 50 µg/kg U (110) <100 <50 <50 <50 <50

n-Propylbenzene GC/MS (Head Space)(MCERTS) 50 µg/kg M (110) <100 <50 <50 <50 <50

Bromobenzene GC/MS (Head Space)(MCERTS) 50 µg/kg M (110) <100 <50 <50 <50 <50

1,3,5-Trimethylbenzene GC/MS (Head Space)(MCERTS) 50 µg/kg M (110) <100 <50 <50 <50 <50

Tert-Butylbenzene GC/MS (Head Space)(MCERTS) 50 µg/kg M (110) <100 <50 <50 <50 <50


Sec-Butylbenzene GC/MS (Head Space)(MCERTS) 50 µg/kg M (110) <100 <50 <50 <50 <50

p-Isopropyltoluene GC/MS (Head Space)(MCERTS) 50 µg/kg M (110) <100 <50 <50 <50 <50

2-Chlorotoluene GC/MS (Head Space)(MCERTS) 50 µg/kg U (110) <100 <50 <50 <50 <50


1,3-Dichlorobenzene GC/MS (Head Space)(MCERTS) 50 µg/kg M (110) <100 <50 <50 <50 <50





666658-1










Top Depth 1.20 3.60 6.00




Dichlorodifluoromethane GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50

Chloromethane GC/MS (Head Space)(MCERTS) 50 µg/kg U <50 <50 <50

Vinyl chloride monomer GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50

Bromomethane GC/MS (Head Space)(MCERTS) 50 µg/kg U <50 <50 <50

Chloroethane GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50

Trichlorofluoromethane GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50

1,1-Dichloroethylene GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50

Dichloromethane GC/MS (Head Space)(MCERTS) 50 µg/kg U <50 <50 <50

Trans-1,2-Dichloroethylene GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50

1,1-Dichloroethane GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50

Cis-1,2-Dichloroethylene GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50

2,2-Dichloropropane GC/MS (Head Space)(MCERTS) 50 µg/kg U <50 <50 <50

Chloroform GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50

Bromochloromethane GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50

1,1,1-Trichloroethane GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50

1,1-Dichloropropene GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50

Carbon tetrachloride GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50

1,2-Dichloroethane GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50

Benzene GC/MS (Head Space)(MCERTS) 10 µg/kg M (13) <10 (13) <10 (13) <10

1,2-Dichloropropane GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50

Trichloroethylene GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50

Bromodichloromethane GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50

Dibromomethane GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50

Cis-1,3-Dichloropropene GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50

Toluene GC/MS (Head Space)(MCERTS) 10 µg/kg M <10 <10 <10

Trans-1,3-Dichloropropene GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50

1,1,2-Trichloroethane GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50

1,3-Dichloropropane GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50

Tetrachloroethylene GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50

Chlorodibromomethane GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50

1,2-dibromoethane GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50

Chlorobenzene GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50

1,1,1,2-Tetrachloroethane GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50

EthylBenzene GC/MS (Head Space)(MCERTS) 10 µg/kg M <10 <10 <10

Meta/Para-Xylene GC/MS (Head Space)(MCERTS) 10 µg/kg M <10 <10 <10

Ortho-Xylene GC/MS (Head Space)(MCERTS) 10 µg/kg M <10 <10 <10

Styrene GC/MS (Head Space)(MCERTS) 50 µg/kg U <50 <50 <50

Bromoform GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50

Isopropyl benzene GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50

1,1,2,2-Tetrachloroethane GC/MS (Head Space)(MCERTS) 50 µg/kg U <50 <50 <50

1,2,3-Trichloropropane GC/MS (Head Space)(MCERTS) 50 µg/kg U <50 <50 <50

n-Propylbenzene GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50

Bromobenzene GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50

1,3,5-Trimethylbenzene GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50

Tert-Butylbenzene GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50

1,2,4-Trimethylbenzene GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50

Sec-Butylbenzene GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50

p-Isopropyltoluene GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50

2-Chlorotoluene GC/MS (Head Space)(MCERTS) 50 µg/kg U <50 <50 <50

4-Chlorotoluene GC/MS (Head Space)(MCERTS) 50 µg/kg U <50 <50 <50

1,3-Dichlorobenzene GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50





666658-1





Semi-Volatile Organic Compounds (USEPA 625) (excl PAH)




Bottom Depth 2.20 2.20 2.20 3.40 5.80

Top Depth 1.20 1.20 1.20 2.40 4.80




Phenol GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1 <0.1

Bis (2-chloroethyl) ether GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1 <0.1

2-Chlorophenol GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1 <0.1

1,3-Dichlorobenzene GC/MS (MCERTS) 0.1 mg/kg M (162) <0.2 (162) <0.2 (162) <0.2 (162) <0.2 (162) <0.2

1,4-Dichlorobenzene GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1 <0.1


Bis (2-chloroisopropyl) ether GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1 <0.1

2-methyl phenol GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1 <0.1

3/4-Methylphenol GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1 <0.1

Hexachloroethane GC/MS (MCERTS) 0.1 mg/kg U (162) <0.2 (162) <0.2 (162) <0.2 (162) <0.2 (162) <0.2

Nitrobenzene GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1 <0.1

Isophorone GC/MS (MCERTS) 0.1 mg/kg U <0.1 <0.1 <0.1 <0.1 <0.1

2-Nitrophenol GC/MS (MCERTS) 0.1 mg/kg U <0.1 <0.1 <0.1 <0.1 <0.1

2,4-Dimethylphenol GC/MS (MCERTS) 0.1 mg/kg U <0.1 <0.1 <0.1 <0.1 <0.1

Bis (2-chloroethoxy) methane GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1 <0.1

2,4-Dichlorophenol GC/MS (MCERTS) 0.1 mg/kg U <0.1 <0.1 <0.1 <0.1 <0.1

1,2,4-Trichlorobenzene GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1 <0.1

4-Chloroaniline GC/MS (MCERTS) 0.1 mg/kg U (162) <0.2 (162) <0.2 (162) <0.2 (162) <0.2 (162) <0.2

Hexachlorobutadiene GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1 <0.1

4-Chloro-3-methylphenol GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1 <0.1

2-Methylnaphthalene GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1 <0.1

Hexachlorocyclopentadiene GC/MS (MCERTS) 0.1 mg/kg U (162) <0.5 (162) <0.5 (162) <0.5 (162) <0.5 (162) <0.5

2,4,6-Trichlorophenol GC/MS (MCERTS) 0.1 mg/kg U <0.1 <0.1 <0.1 <0.1 <0.1


2-Chloronaphthalene GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1 <0.1

2-Nitroaniline GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1 <0.1

Dimethyl phthalate GC/MS (MCERTS) 0.1 mg/kg U <0.1 <0.1 <0.1 <0.1 <0.1

2,6-Dinitrotoluene GC/MS (MCERTS) 0.1 mg/kg U <0.1 <0.1 <0.1 <0.1 <0.1

3-Nitroaniline GC/MS (MCERTS) 0.1 mg/kg U (162) <0.2 (162) <0.2 (162) <0.2 (162) <0.2 (162) <0.2

Dibenzofuran GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1 <0.1

2,4-Dinitrotoluene GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1 <0.1

Diethyl phthalate GC/MS (MCERTS) 0.1 mg/kg U <0.1 <0.1 <0.1 <0.1 <0.1

4-Chlorophenyl phenylether GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1 <0.1


Azobenzene GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1 <0.1

4-Bromophenyl phenylether GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1 <0.1

Hexachlorobenzene GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1 <0.1

Pentachlorophenol GC/MS (MCERTS) 0.1 mg/kg U <0.1 <0.1 <0.1 <0.1 <0.1

Carbazole GC/MS (MCERTS) 0.1 mg/kg U <0.1 <0.1 <0.1 <0.1 <0.1

Di-n-butylphthalate GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1 <0.1

Butyl benzylphthalate GC/MS (MCERTS) 0.1 mg/kg U <0.1 <0.1 <0.1 <0.1 <0.1

Bis (2-ethylhexyl)phthalate GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1 <0.1

Di-n-octylphthalate GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1 <0.1



666658-1










Top Depth 1.20 3.60 6.00




Phenol GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1

Bis (2-chloroethyl) ether GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1

2-Chlorophenol GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1

1,3-Dichlorobenzene GC/MS (MCERTS) 0.1 mg/kg M (162) <0.2 (162) <0.2 (162) <0.2

1,4-Dichlorobenzene GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1

1,2-Dichlorobenzene GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1

Bis (2-chloroisopropyl) ether GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1

2-methyl phenol GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1

3/4-Methylphenol GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1

Hexachloroethane GC/MS (MCERTS) 0.1 mg/kg U (162) <0.2 (162) <0.2 (162) <0.2

Nitrobenzene GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1

Isophorone GC/MS (MCERTS) 0.1 mg/kg U <0.1 <0.1 <0.1

2-Nitrophenol GC/MS (MCERTS) 0.1 mg/kg U <0.1 <0.1 <0.1

2,4-Dimethylphenol GC/MS (MCERTS) 0.1 mg/kg U <0.1 <0.1 <0.1

Bis (2-chloroethoxy) methane GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1

2,4-Dichlorophenol GC/MS (MCERTS) 0.1 mg/kg U <0.1 <0.1 <0.1

1,2,4-Trichlorobenzene GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1

4-Chloroaniline GC/MS (MCERTS) 0.1 mg/kg U (162) <0.2 (162) <0.2 (162) <0.2

Hexachlorobutadiene GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1

4-Chloro-3-methylphenol GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1

2-Methylnaphthalene GC/MS (MCERTS) 0.1 mg/kg M 0.1 <0.1 <0.1

Hexachlorocyclopentadiene GC/MS (MCERTS) 0.1 mg/kg U (162) <0.5 (162) <0.5 (162) <0.5

2,4,6-Trichlorophenol GC/MS (MCERTS) 0.1 mg/kg U <0.1 <0.1 <0.1

2,4,5-Trichlorophenol GC/MS (MCERTS) 0.1 mg/kg U <0.1 <0.1 <0.1

2-Chloronaphthalene GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1

2-Nitroaniline GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1

Dimethyl phthalate GC/MS (MCERTS) 0.1 mg/kg U <0.1 <0.1 <0.1

2,6-Dinitrotoluene GC/MS (MCERTS) 0.1 mg/kg U <0.1 <0.1 <0.1

3-Nitroaniline GC/MS (MCERTS) 0.1 mg/kg U (162) <0.2 (162) <0.2 (162) <0.2

Dibenzofuran GC/MS (MCERTS) 0.1 mg/kg M 0.1 <0.1 <0.1

2,4-Dinitrotoluene GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1

Diethyl phthalate GC/MS (MCERTS) 0.1 mg/kg U <0.1 <0.1 <0.1

4-Chlorophenyl phenylether GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1

4-Nitroaniline GC/MS (MCERTS) 0.1 mg/kg U (162) <0.2 (162) <0.2 (162) <0.2

Azobenzene GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1

4-Bromophenyl phenylether GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1

Hexachlorobenzene GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1

Pentachlorophenol GC/MS (MCERTS) 0.1 mg/kg U <0.1 <0.1 <0.1

Carbazole GC/MS (MCERTS) 0.1 mg/kg U <0.1 <0.1 <0.1

Di-n-butylphthalate GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1

Butyl benzylphthalate GC/MS (MCERTS) 0.1 mg/kg U <0.1 <0.1 <0.1

Bis (2-ethylhexyl)phthalate GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1

Di-n-octylphthalate GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1



666658-1




Leachate to BS EN12457-2 (10:1)

Analysed as Water

Leachate Suite

Concept Reference 666658 001 666658 002 666658 003 666658 006

Customer Sample Reference CPT01A CPT03A CPT14A CPT15A

Test Sample 10:1 10:1 10:1 10:1

Bottom Depth 2.20 2.20 2.20 2.20

Top Depth 1.20 1.20 1.20 1.20

Date Sampled 30-JUN-2017 28-JUN-2017 03-JUL-2017 30-JUN-2017

Matrix Class Sandy Soil Sandy Soil Sandy Soil Sandy Soil


Arsenic (Dissolved) ICP/MS (Filtered) 0.2 µg/l U 1.2 <0.2 14 17

Boron (Dissolved) ICP/OES (Filtered) 0.01 mg/l N 0.06 0.04 0.03 0.13

Cadmium (Dissolved) ICP/MS (Filtered) 0.02 µg/l U 0.06 <0.02 0.07 0.09

Chromium (Dissolved) ICP/MS (Filtered) 1 µg/l U <1 <1 2 1

Copper (Dissolved) ICP/MS (Filtered) 0.5 µg/l U 1.4 1.1 16 1.7

Lead (Dissolved) ICP/MS (Filtered) 0.3 µg/l U <0.3 <0.3 1.5 1.3

Nickel (Dissolved) ICP/MS (Filtered) 1 µg/l U 2 <1 2 4

Mercury (Dissolved) ICP/MS (Filtered) 0.05 µg/l U <0.05 <0.05 <0.05 0.08

Selenium (Dissolved) ICP/MS (Filtered) 0.5 µg/l U <0.5 <0.5 0.8 <0.5

Vanadium (Dissolved) ICP/MS (Filtered) 2 µg/l U <2 <2 4 <2

Zinc (Dissolved) ICP/MS (Filtered) 2 µg/l U 5 <2 9 8

Ammoniacal nitrogen Discrete Analyser 0.05 mg/l U 0.26 <0.05 0.22 0.05

Chloride Discrete Analyser 1 mg/l U 2 <1 <1 2

Cyanide (Total) Colorimetry 0.05 mg/l U <0.05 <0.05 <0.05 <0.05

Fluoride Discrete Analyser 0.05 mg/l U 0.28 0.35 0.46 0.68

Nitrate Discrete Analyser 0.5 mg/l U <0.5 <0.5 <0.5 78

Total Phenols GC/MS 0.5 µg/l U (13) <0.5 <0.5 (13) <0.5 (13) <0.5

Phosphate Discrete Analyser 0.5 mg/l U 7.3 2.8 0.7 6.5

Sulphate Discrete Analyser 0.5 mg/l U 140 2.8 9.3 87

Sulphide Colorimetry 0.05 mg/l N <0.05 <0.05 <0.05 <0.05

Dissolved Organic Carbon OX/IR 1 mg/l N 27 4 16 28

Electrical Conductivity Probe 10 µS/cm N 340 36 120 540

pH Probe U 7.6 7.3 7.6 7.6



666658-1





Analysed as Water

PAH USEPA16



Test Sample 10:1 10:1 10:1 10:1

Bottom Depth 2.20 2.20 2.20 2.20

Top Depth 1.20 1.20 1.20 1.20




Naphthalene GC/MS (SIR) 0.01 µg/l U (13) 0.01 (13) 0.06 (13) 0.16 (13) 0.04

Acenaphthylene GC/MS (SIR) 0.01 µg/l U 0.02 0.02 0.20 0.08

Acenaphthene GC/MS (SIR) 0.01 µg/l U (13) 0.02 (13) 0.02 (13) 0.12 (13) 0.44

Fluorene GC/MS (SIR) 0.01 µg/l U (13) 0.02 (13) 0.04 (13) 0.14 (13) 0.12

Phenanthrene GC/MS (SIR) 0.01 µg/l U (13) 0.02 (13) 0.10 (13) 0.32 (13) 0.06

Anthracene GC/MS (SIR) 0.01 µg/l U 0.01 0.02 0.26 0.12

Fluoranthene GC/MS (SIR) 0.01 µg/l U (13) <0.01 (13) 0.04 (13) 0.64 (13) 0.20

Pyrene GC/MS (SIR) 0.01 µg/l U (13) <0.01 (13) 0.02 (13) 0.58 (13) 0.12

Benzo(a)Anthracene GC/MS (SIR) 0.01 µg/l U 0.01 0.02 0.38 0.04

Chrysene GC/MS (SIR) 0.01 µg/l U 0.01 0.04 0.42 0.04

Benzo(b)fluoranthene GC/MS (SIR) 0.01 µg/l U 0.01 0.04 0.60 0.08

Benzo(k)fluoranthene GC/MS (SIR) 0.01 µg/l U 0.01 0.02 0.56 0.06

Benzo(a)Pyrene GC/MS (SIR) 0.01 µg/l U 0.01 0.02 0.70 0.08

Indeno(123-cd)Pyrene GC/MS (SIR) 0.01 µg/l U 0.01 0.02 0.62 0.06

Dibenzo(ah)Anthracene GC/MS (SIR) 0.01 µg/l U <0.01 0.02 0.12 0.02

Benzo(ghi)Perylene GC/MS (SIR) 0.01 µg/l U <0.01 0.02 0.80 0.08

Polyaromatic Hydrocarbons (Total) GC/MS (SIR) 0.01 µg/l U 0.16 0.52 6.6 1.6





Analysed as Water

PCB EC7



Test Sample 10:1 10:1 10:1 10:1

Bottom Depth 2.20 2.20 2.20 2.20

Top Depth 1.20 1.20 1.20 1.20




Polychlorinated biphenyl BZ#28 GC/MS (HR) 0.005 µg/l U <0.005 <0.005 <0.005 <0.005



Polychlorinated biphenyl BZ#118 GC/MS 0.005 µg/l U <0.005 <0.005 <0.005 <0.005






666658-1





Analysed as Water




Test Sample 10:1 10:1 10:1 10:1

Bottom Depth 2.20 2.20 2.20 2.20

Top Depth 1.20 1.20 1.20 1.20


28-JUN-2017

03-JUL-2017 30-JUN-2017



Benzene GC/MS (Headspace) 1 µg/l U (13) <1 (13) <1 (13) <1 (13) <1

Toluene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1

EthylBenzene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1

Meta/Para-Xylene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1

Ortho-Xylene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1

Methyl tert-Butyl Ether GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1

Total Petroleum Hydrocarbons (C5 - C6 aliphatic) GC/MS (Headspace)(LV) 0.010 mg/l N <0.010 <0.010 <0.010 <0.010

Total Petroleum Hydrocarbons (C6-C8 aliphatic) GC/MS (Headspace)(LV) 0.010 mg/l N <0.010 <0.010 <0.010 <0.010


Total Petroleum Hydrocarbons (C10-C12 aliphatic) GCxGC (LV) 0.01 mg/l N (13,100) <0.02 (13,100) <0.02 (13,100) <0.02 (100,13) <0.10


Total Petroleum Hydrocarbons (C16-C21 aliphatic) GCxGC (LV) 0.01 mg/l N (13,100) <0.02 (13,100) <0.02 (13) 0.03 (100,13) <0.10

Total Petroleum Hydrocarbons (C21-C35 aliphatic) GCxGC (LV) 0.01 mg/l N (13,100) <0.02 (13,100) <0.02 (13) 0.08 (100,13) <0.10

Total Petroleum Hydrocarbons (C6 - C7 aromatic) GC/MS (Headspace)(LV) 0.010 mg/l N <0.010 <0.010 <0.010 <0.010

Total Petroleum Hydrocarbons (C7-C8 aromatic) GC/MS (Headspace)(LV) 0.010 mg/l N <0.010 <0.010 <0.010 <0.010


Total Petroleum Hydrocarbons (C10-C12 aromatic) GCxGC (LV) 0.01 mg/l N (100,13) <0.02 (100,13) <0.02 (100,13) <0.02 (13,100) <0.10



Total Petroleum Hydrocarbons (C21-C35 aromatic) GCxGC (LV) 0.01 mg/l N (13,100) <0.02 (13,100) <0.02 (13) 0.03 (100,13) <0.10



666658-1





Analysed as Water




Test Sample 10:1 10:1 10:1 10:1

Bottom Depth 2.20 2.20 2.20 2.20

Top Depth 1.20 1.20 1.20 1.20




Dichlorodifluoromethane GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1

Chloromethane GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1

Vinyl chloride monomer GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1

Bromomethane GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1

Chloroethane GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1

Trichlorofluoromethane GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1

1,1-Dichloroethylene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1

Dichloromethane GC/MS (Headspace) 50 µg/l N <50 <50 <50 <50

Trans-1,2-Dichloroethylene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1

1,1-Dichloroethane GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1

Cis-1,2-Dichloroethylene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1

2,2-Dichloropropane GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1

Chloroform GC/MS (Headspace) 1 µg/l U (13) <1 (13) 32 (13) 49 (13) 39

Bromochloromethane GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1

1,1,1-Trichloroethane GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1

1,1-Dichloropropene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1

Carbon tetrachloride GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1


Benzene GC/MS (Headspace) 1 µg/l U (13) <1 (13) <1 (13) <1 (13) <1


1,1,2-Trichloroethylene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1

Bromodichloromethane GC/MS (Headspace) 1 µg/l U (13) <1 (13) <1 (13) 1 (13) <1

Dibromomethane GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1

Cis-1,3-Dichloropropene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1

Toluene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1

Trans-1,3-Dichloropropene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1



Tetrachloroethylene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1

Chlorodibromomethane GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1

1,2-dibromoethane GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1

Chlorobenzene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1

1,1,1,2-Tetrachloroethane GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1


Meta/Para-Xylene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1

Ortho-Xylene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1

Styrene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1

Bromoform GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1

Isopropyl benzene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1


1,2,3-Trichloropropane GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1

n-Propylbenzene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1

Bromobenzene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1

1,3,5-Trimethylbenzene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1

Tert-Butylbenzene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1


Sec-Butylbenzene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1

p-Isopropyltoluene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1

2-Chlorotoluene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1


1,3-Dichlorobenzene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1





666658-1

Index to symbols used in 666658-1





Analysed as Water




Test Sample 10:1 10:1 10:1 10:1

Bottom Depth 2.20 2.20 2.20 2.20

Top Depth 1.20 1.20 1.20 1.20




Phenol GC/MS 10 µg/l U <10 <10 <10 <10

Bis (2-chloroethyl) ether GC/MS 10 µg/l U <10 <10 <10 <10

2-Chlorophenol GC/MS 10 µg/l U <10 <10 <10 <10

1,3-Dichlorobenzene GC/MS 10 µg/l U <10 <10 <10 <10



Bis (2-chloroisopropyl) ether GC/MS 10 µg/l U <10 <10 <10 <10

2-methyl phenol GC/MS 10 µg/l U <10 <10 <10 <10

3/4-Methylphenol GC/MS 10 µg/l U <10 <10 <10 <10

Hexachloroethane GC/MS 10 µg/l U (162) <20 (162) <20 (162) <20 (162) <20

Nitrobenzene GC/MS 10 µg/l U <10 <10 <10 <10

Isophorone GC/MS 10 µg/l U <10 <10 <10 <10

2-Nitrophenol GC/MS 10 µg/l U <10 <10 <10 <10

2,4-Dimethylphenol GC/MS 10 µg/l U <10 <10 <10 <10

Bis (2-chloroethoxy) methane GC/MS 10 µg/l U <10 <10 <10 <10

2,4-Dichlorophenol GC/MS 10 µg/l U <10 <10 <10 <10

1,2,4-Trichlorobenzene GC/MS 10 µg/l U (162) <20 (162) <20 (162) <20 (162) <20

4-Chloroaniline GC/MS 10 µg/l U <10 <10 <10 <10

Hexachlorobutadiene GC/MS 10 µg/l U (162) <20 (162) <20 (162) <20 (162) <20

4-Chloro-3-methylphenol GC/MS 10 µg/l U <10 <10 <10 <10

2-Methylnaphthalene GC/MS 10 µg/l U <10 <10 <10 <10

Hexachlorocyclopentadiene GC/MS 10 µg/l U (162) <50 (162) <50 (162) <50 (162) <50

2,4,6-Trichlorophenol GC/MS 10 µg/l U <10 <10 <10 <10

2,4,5-Trichlorophenol GC/MS 10 µg/l U <10 <10 <10 <10

2-Chloronaphthalene GC/MS 10 µg/l U <10 <10 <10 <10

2-Nitroaniline GC/MS 10 µg/l U <10 <10 <10 <10

Dimethyl phthalate GC/MS 10 µg/l U (162) <20 (162) <20 (162) <20 (162) <20

2,6-Dinitrotoluene GC/MS 10 µg/l U <10 <10 <10 <10


Dibenzofuran GC/MS 10 µg/l U <10 <10 <10 <10

2,4-Dinitrotoluene GC/MS 10 µg/l U <10 <10 <10 <10

Diethyl phthalate GC/MS 10 µg/l U <10 <10 <10 <10

4-Chlorophenyl phenylether GC/MS 10 µg/l U <10 <10 <10 <10


Azobenzene GC/MS 10 µg/l U <10 <10 <10 <10

4-Bromophenyl phenylether GC/MS 10 µg/l U <10 <10 <10 <10

Hexachlorobenzene GC/MS 10 µg/l U <10 <10 <10 <10

Pentachlorophenol GC/MS 10 µg/l U <10 <10 <10 <10

Carbazole GC/MS 10 µg/l U <10 <10 <10 <10

Di-n-butylphthalate GC/MS 10 µg/l U <10 <10 <10 <10

Butyl benzylphthalate GC/MS 10 µg/l U <10 <10 <10 <10

Bis (2-ethylhexyl)phthalate GC/MS 10 µg/l U <10 <10 <10 <10

Di-n-octylphthalate GC/MS 10 µg/l U <10 <10 <10 <10

Value Description

M105 Analysis conducted on an "as received" aliquot. Results are reported on a dryweight basis where moisture content was determined by assisted drying of sampleat 105C

A40 Assisted dried < 40C

M40 Analysis conducted on sample assisted dried at no more than 40C. Results arereported on a dry weight basis.

10:1 Leachate to BS EN 12457-2 (10:1)

AR As Received

N.D. Not Detected



666658-1

Notes

9 LOD raised due to dilution of sample

162 LOD determined by matrix spike recovery

100 LOD determined by sample aliquot used for analysis

110 LOD raised due to low internal standard recovery.

26 LOD raised because the analysis was performed by an alternative technique

13 Results have been blank corrected.

S Analysis was subcontracted

M Analysis is MCERTS accredited

U Analysis is UKAS accredited

N Analysis is not UKAS accredited

Asbestos was subcontracted to REC Asbestos.

These samples have been analysed exceeding recommended holding times. It is possible therefore that the results provided may be compromised.



666658-1




CornbrookManchester

M16 9FETel : 0161 874 2400Fax : 0161 874 2468


Date of Report: 16-Aug-2017




Date Job Received at Concept: 28-Jun-2017Date Analysis Started: 13-Jul-2017

Date Analysis Completed: 16-Aug-2017

The results reported relate to samples received in the laboratory and may not be representative of a wholebatch.Opinions and interpretations expressed herein are outside the scope of UKAS accreditationThis report should not be reproduced except in full without the written approval of the laboratoryTests covered by this certificate were conducted in accordance with Concept Life Sciences SOPsAll results have been reviewed in accordance with Section 25 of the Concept Life Sciences, AnalyticalServices Quality Manual



Concept Life Sciences Analytical & Development

Services Limited registered in England and

Wales (No 2514788)

1549



Page 1 of 28

667517-3

Waste Acceptance Criteria

Following the recommendation from the Environment Agency (England and Wales)*, the leachate preparation in this report has been carried out to BS EN 12457-2 : One Stage

batch test at a liquid to solid ratio of 10 l/kg. This is also compliant with Schedule 10 of the Environmental Permitting Regulations 2010.

Note : This is the minimum amount of testing which is required.

Further testing may be required if :

- evidence of immediately leachable parameters becomes available.

- evidence to indicate that the sample could be classified as hazardous under H1-H14 of the Waste(England and Wales) Regulations 2011(as amended) becomes available.

Acceptance of waste at landfill is always at the discretion of the Landfill Operator.

* Waste Sampling and Testing for Disposal at Landfill, EBPRI 11507B, Environment Agency (England and Wales) March 2013

As detailed in- Waste Classification. Guidance on the classification and assessment of waste. Technical Guidance WM3:

https://www.gov.uk/government/uploads/system/uploads/attachment_data/file/427077/LIT_10121.pdf

Landfill WAC analysis (specifically leaching test results) should not be used for hazardous waste classification purposes. This analysis is only applicable for hazardous waste

landfill acceptance and does not give any indication as to whether a waste may be hazardous or non-hazardous.

Customer Sample Reference : BH12A ES4

SAL Sample Reference : 667517 001

Project Site : Western Link

Customer Reference : 42109

Bottom Depth : 2.00

Date Sampled : 03-JUL-2017

Matrix Class : Sandy Soil

Soil Result Inert WasteLandfill

Stable nonreactive

Hazardous WasteLandfill

Determinand Technique LOD Units Symbol

Acid Neutralising Capacity (pH 4) Titration 2 Mol/kg N <2


Loss on Ignition Grav 0.1 % N 18 10.0

BTEX (Sum) Calc 0.080 mg/kg U (110) <0.080 6.0

PAH (Sum) Calc 1.6 mg/kg N 3.2 100.0

PCB EC7 (Sum) Calc 0.007 mg/kg M <0.007 1.0

Total Petroleum Hydrocarbons C10-C40 (Sum) Calc 1 mg/kg N (13) 53 500.0

Data for BS EN 12457-2 (10:1) Result Inert WasteLandfill

Stable nonreactive



Antimony Calc WAC ICP/MS 0.010 mg/kg N 0.026 0.06 0.7 5.0

Arsenic Calc WAC ICP/MS 0.0020 mg/kg N 0.018 0.5 2.0 25.0

Barium Calc WAC ICP/MS 0.010 mg/kg N 0.77 20.0 100.0 300.0

Cadmium Calc WAC ICP/MS 0.00020 mg/kg N 0.00051 0.04 1.0 5.0

Chromium Calc WAC ICP/MS 0.010 mg/kg N 0.016 0.5 10.0 70.0

Copper Calc WAC ICP/MS 0.0050 mg/kg N 0.014 2.0 50.0 100.0

Lead Calc WAC ICP/MS 0.0030 mg/kg N <0.0030 0.5 10.0 50.0

Mercury Calc WAC ICP/MS 0.00050 mg/kg N <0.00050 0.01 0.2 2.0

Molybdenum Calc WAC ICP/MS 0.010 mg/kg N 0.20 0.5 10.0 30.0

Nickel Calc WAC ICP/MS 0.010 mg/kg N 0.019 0.4 10.0 40.0

Selenium Calc WAC ICP/MS 0.0050 mg/kg N 0.070 0.1 0.5 7.0

Zinc Calc WAC ICP/MS 0.020 mg/kg N 0.088 4.0 50.0 200.0

Chloride Calc (W) 10 mg/kg N <10 800.0 15000.0 25000.0

Fluoride Calc (W) 0.50 mg/kg N 2.5 10.0 150.0 500.0

Sulphate Calc (W) 5 mg/kg N 730 1000.0 20000.0 50000.0

Phenols (Total-Mono) Calc 1.0 mg/kg N <1.0 1.0

Dissolved Organic Carbon Calc 10 mg/kg N 270 500.0 800.0 1000.0

Total Dissolved Solids Calc WAC ICP/MS 1000 mg/kg N 2400 4000.0 60000.0 100000.0



667517-3














Customer Sample Reference : BH12A ES5




Bottom Depth : 3.00




Stable nonreactive





Loss on Ignition Grav 0.1 % N 12 10.0

BTEX (Sum) Calc 0.040 mg/kg U <0.040 6.0

PAH (Sum) Calc 1.6 mg/kg N 14 100.0




Stable nonreactive







Chromium Calc WAC ICP/MS 0.010 mg/kg N <0.010 0.5 10.0 70.0


Lead Calc WAC ICP/MS 0.0030 mg/kg N <0.0030 0.5 10.0 50.0







Fluoride Calc (W) 0.50 mg/kg N <0.50 10.0 150.0 500.0







667517-3














Customer Sample Reference : BH04 ES5




Bottom Depth : 3.00

Date Sampled : 27-JUN-2017



Stable nonreactive





Loss on Ignition Grav 0.1 % N 6.2 10.0


PAH (Sum) Calc 1.6 mg/kg N 57 100.0

PCB EC7 (Sum) Calc 0.070 mg/kg M (9) <0.070 1.0



Stable nonreactive









Lead Calc WAC ICP/MS 0.0030 mg/kg N 0.0091 0.5 10.0 50.0




Selenium Calc WAC ICP/MS 0.0050 mg/kg N <0.0050 0.1 0.5 7.0










667517-3














Customer Sample Reference : BH04




Bottom Depth : 1.00




Stable nonreactive





Loss on Ignition Grav 0.1 % N 5.0 10.0


PAH (Sum) Calc 1.6 mg/kg N <1.6 100.0




Stable nonreactive














Zinc Calc WAC ICP/MS 0.020 mg/kg N <0.020 4.0 50.0 200.0









667517-3





MCERTS Preparation


Customer Sample Reference BH12A ES4 BH12A ES5 BH12A ES6 BH03 ES4 BH04 ES5


Bottom Depth 2.00 3.00 4.00 1.20 3.00

Date Sampled 03-JUL-2017 03-JUL-2017 03-JUL-2017 27-JUN-2017 27-JUN-2017

Matrix Class Sandy Soil Sandy Soil Sandy Soil Clay Sandy Soil


Moisture @105C Grav (1 Dec) (105 C) 0.1 % N 28 24 31 14 20





MCERTS Preparation

Concept Reference 667517 006 667517 008

Customer Sample Reference BH04 ES6 BH04

Test Sample AR AR

Bottom Depth 4.00 1.00

Date Sampled 27-JUN-2017 18-JUL-2017

Matrix Class Clay Sandy Soil


Moisture @105C Grav (1 Dec) (105 C) 0.1 % N 15 16





MCERTS Preparation




Bottom Depth 2.00 3.00 4.00 1.20 3.00




Retained on 10mm sieve Grav 0.1 % N <0.1 <0.1 <0.1 <0.1 <0.1





MCERTS Preparation



Test Sample M40 M40





Retained on 10mm sieve Grav 0.1 % N <0.1 <0.1



667517-3





Soil Suite



Test Sample A40 A40 A40 A40 A40

Bottom Depth 2.00 3.00 4.00 1.20 3.00




Sulphate (Total) ICP/OES 0.01 % N 0.26 1.1 0.10 0.02 0.14

Sulphur (total) ICP/OES 0.01 % N 0.16 0.39 0.05 <0.01 0.13

Total Organic Carbon OX/IR 0.1 % N 16 14 1.4 0.4 3.2





Soil Suite



Test Sample A40 A40





Sulphate (Total) ICP/OES 0.01 % N 0.78 0.13

Sulphur (total) ICP/OES 0.01 % N 0.51 0.08

Total Organic Carbon OX/IR 0.1 % N 26 1.9





Soil Suite




Bottom Depth 2.00 3.00 4.00 1.20 3.00




Boron (water-soluble) ICP/OES 1 mg/kg N <1 <1 <1 <1 <1

Cyanide (Total) Colorimetry (CF) 1 mg/kg M <1 1 <1 <1 <1

Sulphide Colorimetry 10 mg/kg N <10 <10 <10 <10 <10

Total Phenols GC/MS (MCERTS) 0.1 mg/kg N <0.1 <0.1 <0.1 <0.1 <0.1

Asbestos ID PLM SU N.D. N.D. N.D. N.D. N.D.

pH Probe M 7.6 7.3 7.0 7.8 7.2



667517-3





Soil Suite



Test Sample AR AR





Boron (water-soluble) ICP/OES 1 mg/kg N <1 <1

Cyanide (Total) Colorimetry (CF) 1 mg/kg M <1 <1

Sulphide Colorimetry 10 mg/kg N 100 18

Total Phenols GC/MS (MCERTS) 0.1 mg/kg N <0.1 <0.1

Asbestos ID PLM SU N.D. N.D.

pH Probe M 6.9 7.5





Soil Suite




Bottom Depth 2.00 3.00 4.00 1.20 3.00




Arsenic ICP/OES 2 mg/kg M 150 92 26 10 12

Cadmium ICP/OES 1 mg/kg M 1 1 <1 <1 <1

Chromium ICP/OES 1 mg/kg M 38 28 11 28 29

Copper ICP/OES 1 mg/kg M 360 270 62 19 94

Lead ICP/OES 1 mg/kg M 720 530 210 16 120

Mercury ICP/OES 1 mg/kg M 1 <1 <1 <1 <1

Nickel ICP/OES 1 mg/kg M 140 110 29 30 32

Selenium ICP/OES 3 mg/kg M <3 <3 <3 <3 <3

Vanadium ICP/OES 1 mg/kg M 85 66 22 28 35

Zinc ICP/OES 1 mg/kg M 600 470 190 44 95



667517-3





Soil Suite



Test Sample M40 M40





Arsenic ICP/OES 2 mg/kg M 73 14

Cadmium ICP/OES 1 mg/kg M 2 <1

Chromium ICP/OES 1 mg/kg M 23 22

Copper ICP/OES 1 mg/kg M 730 55

Lead ICP/OES 1 mg/kg M 1900 160

Mercury ICP/OES 1 mg/kg M 1 <1

Nickel ICP/OES 1 mg/kg M 61 19

Selenium ICP/OES 3 mg/kg M <3 <3

Vanadium ICP/OES 1 mg/kg M 48 25

Zinc ICP/OES 1 mg/kg M 650 150





PAH USEPA16




Bottom Depth 2.00 3.00 4.00 1.20 3.00




Naphthalene GC/MS (MCERTS) 0.1 mg/kg M 0.1 0.2 <0.1 <0.1 <1.0

Acenaphthylene GC/MS (MCERTS) 0.1 mg/kg U <0.1 0.2 <0.1 <0.1 <1.0

Acenaphthene GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1 <1.0

Fluorene GC/MS (MCERTS) 0.1 mg/kg M <0.1 0.3 <0.1 <0.1 <1.0

Phenanthrene GC/MS (MCERTS) 0.1 mg/kg M 0.2 2.1 0.1 <0.1 6.8

Anthracene GC/MS (MCERTS) 0.1 mg/kg U <0.1 0.6 <0.1 <0.1 1.7

Fluoranthene GC/MS (MCERTS) 0.1 mg/kg M 0.5 2.3 0.2 <0.1 8.7

Pyrene GC/MS (MCERTS) 0.1 mg/kg M 0.5 2.1 0.2 <0.1 8.9

Benzo(a)Anthracene GC/MS (MCERTS) 0.1 mg/kg M 0.3 1.2 0.1 <0.1 5.3

Chrysene GC/MS (MCERTS) 0.1 mg/kg M 0.4 1.2 0.1 <0.1 6.2

Benzo(b)fluoranthene GC/MS (MCERTS) 0.1 mg/kg M 0.3 1.0 <0.1 <0.1 4.9

Benzo(k)fluoranthene GC/MS (MCERTS) 0.1 mg/kg M 0.4 1.3 0.1 <0.1 5.5

Benzo(a)Pyrene GC/MS (MCERTS) 0.1 mg/kg M 0.3 1.0 <0.1 <0.1 4.3

Indeno(123-cd)Pyrene GC/MS (MCERTS) 0.1 mg/kg M 0.2 0.5 <0.1 <0.1 2.6

Dibenzo(ah)Anthracene GC/MS (MCERTS) 0.1 mg/kg M <0.1 0.2 <0.1 <0.1 <1.0

Benzo(ghi)Perylene GC/MS (MCERTS) 0.1 mg/kg M 0.2 0.4 <0.1 <0.1 2.6

Coronene GC/MS 0.1 mg/kg N <0.1 <0.1 - - <0.1


Polyaromatic Hydrocarbons (Total) GC/MS (MCERTS) 0.1 mg/kg U 3.2 14 0.9 <0.1 57



667517-3





PAH USEPA16



Test Sample M105 M105





Naphthalene GC/MS (MCERTS) 0.1 mg/kg M <1.0 <0.1

Acenaphthylene GC/MS (MCERTS) 0.1 mg/kg U <1.0 <0.1

Acenaphthene GC/MS (MCERTS) 0.1 mg/kg M <1.0 <0.1

Fluorene GC/MS (MCERTS) 0.1 mg/kg M <1.0 <0.1

Phenanthrene GC/MS (MCERTS) 0.1 mg/kg M 1.5 0.1

Anthracene GC/MS (MCERTS) 0.1 mg/kg U <1.0 <0.1

Fluoranthene GC/MS (MCERTS) 0.1 mg/kg M 1.6 0.2

Pyrene GC/MS (MCERTS) 0.1 mg/kg M 1.7 0.3

Benzo(a)Anthracene GC/MS (MCERTS) 0.1 mg/kg M <1.0 <0.1

Chrysene GC/MS (MCERTS) 0.1 mg/kg M 1.2 0.1

Benzo(b)fluoranthene GC/MS (MCERTS) 0.1 mg/kg M <1.0 <0.1

Benzo(k)fluoranthene GC/MS (MCERTS) 0.1 mg/kg M 1.4 0.1

Benzo(a)Pyrene GC/MS (MCERTS) 0.1 mg/kg M <1.0 <0.1

Indeno(123-cd)Pyrene GC/MS (MCERTS) 0.1 mg/kg M <1.0 <0.1

Dibenzo(ah)Anthracene GC/MS (MCERTS) 0.1 mg/kg M <1.0 <0.1

Benzo(ghi)Perylene GC/MS (MCERTS) 0.1 mg/kg M <1.0 <0.1

Coronene GC/MS 0.1 mg/kg N - <0.1

Phenol GC/MS (MCERTS) 0.1 mg/kg M <1.0 <0.1

Polyaromatic Hydrocarbons (Total) GC/MS (MCERTS) 0.1 mg/kg U 7.3 0.9





PCB EC7




Bottom Depth 2.00 3.00 4.00 1.20 3.00




Polychlorinated biphenyl BZ#28 GC/MS (HR) (MCERTS) 0.00005

mg/kg M (26) <0.0010 (26) <0.0010 (26) <0.0010 (26) <0.0010 (26,9) <0.010


mg/kg M (26) <0.0010 (26) <0.0010 (26) <0.0010 (26) <0.0010 (26,9) <0.010


mg/kg M (26) <0.0010 (26) <0.0010 (26) <0.0010 (26) <0.0010 (26,9) <0.010


mg/kg M (26) <0.0010 (26) <0.0010 (26) <0.0010 (26) <0.0010 (26,9) <0.010


mg/kg M (26) <0.0010 (26) <0.0010 (26) <0.0010 (26) <0.0010 (26,9) <0.010


mg/kg M (26) <0.0010 (26) <0.0010 (26) <0.0010 (26) <0.0010 (9,26) <0.010


mg/kg M (26) <0.0010 (26) <0.0010 (26) <0.0010 (26) <0.0010 (26,9) <0.010



667517-3





PCB EC7









mg/kg M (26,9) <0.010 (26) <0.0010


mg/kg M (9,26) <0.010 (26) <0.0010


mg/kg M (26,9) <0.010 (26) <0.0010


mg/kg M (26,9) <0.010 (26) <0.0010


mg/kg M (26,9) <0.010 (26) <0.0010


mg/kg M (26,9) <0.010 (26) <0.0010


mg/kg M (26,9) <0.010 (26) <0.0010







667517002

667517003

667517004

667517005

Customer Sample Reference BH12AES4

BH12AES5

BH12AES6

BH03 ES4 BH04 ES5


Bottom Depth 2.00 3.00 4.00 1.20 3.00

Date Sampled 03-JUL-2017

03-JUL-2017

03-JUL-2017

27-JUN-2017

27-JUN-2017


SandySoil

SandySoil

Clay SandySoil





Meta/Para-Xylene GC/MS (Head Space)(MCERTS) 10 µg/kg M (110) <20 <10 <10 <10 15


Methyl tert-Butyl Ether GC/MS (Head Space)(MCERTS) 10 µg/kg M (110) <20 <10 <10 <10 <10

Total Petroleum Hydrocarbons (C5 - C6 aliphatic) GC/MS (Head Space)(MCERTS) 100 µg/kg N (110) <200 <100 <100 <100 <100

Total Petroleum Hydrocarbons (C6-C8 aliphatic) GC/MS (Head Space)(MCERTS) 100 µg/kg N (110) <200 <100 <100 <100 <100

Total Petroleum Hydrocarbons (C8-C10 aliphatic) GC/MS (Head Space)(MCERTS) 100 µg/kg N (110) <200 <100 <100 <100 <100

Total Petroleum Hydrocarbons (C10-C12 aliphatic) GCxGC 1 mg/kg M (13) <1 (13) <1 (13) <1 (13) <1 (13,9) <10

Total Petroleum Hydrocarbons (C12-C16 aliphatic) GCxGC 1 mg/kg M (13) 2 (13) 1 (13) 1 (13) <1 (13,9) <10

Total Petroleum Hydrocarbons (C16-C21 aliphatic) GCxGC 1 mg/kg M (13) 3 (13) 3 (13) 2 (13) <1 (13) 14

Total Petroleum Hydrocarbons (C21-C35 aliphatic) GCxGC 2 mg/kg M (13) <2 (13) <2 (13) 4 (13) <2 (13) 67

Total Petroleum Hydrocarbons (C35-C40 aliphatic) GCxGC 1 mg/kg N (13) <1 (13) <1 (13) <1 (13) <1 (13,9) <10

Total Petroleum Hydrocarbons (Aliphatic) total Calc mg/kg N (13) 5.0 (13) 4.0 (13) 7.0 (13) N.D. (13) 81

Total Petroleum Hydrocarbons (C6 - C7 aromatic) GC/MS (Head Space)(MCERTS) 100 µg/kg N (110) <200 <100 <100 <100 <100

Total Petroleum Hydrocarbons (C7-C8 aromatic) GC/MS (Head Space)(MCERTS) 100 µg/kg N (110) <200 <100 <100 <100 <100

Total Petroleum Hydrocarbons (C8-C10 aromatic) GC/MS (Head Space)(MCERTS) 100 µg/kg N (110) <200 <100 <100 <100 <100

Total Petroleum Hydrocarbons (C10-C12 aromatic) GCxGC 2 mg/kg M (13) <2 (13) <2 (13) <2 (13) <2 (9,13) <10

Total Petroleum Hydrocarbons (C12-C16 aromatic) GCxGC 1 mg/kg M (13) 3 (13) 3 (13) 1 (13) <1 (13) 42



Total Petroleum Hydrocarbons (C35-C40 aromatic) GCxGC 1 mg/kg N (13) <1 (13) <1 (13) <1 (13) <1 (9,13) <10

Total Petroleum Hydrocarbons (Aromatic) total Calc mg/kg N (13) 21 (13) 20 (13) 8.0 (13) N.D. (13) 1100

Total Petroleum Hydrocarbons (Aliphatic+Aromatic) Calc mg/kg N (13) 26 (13) 24 (13) 15 (13) N.D. (13) 1200



667517-3







667517008





18-JUL-2017

Matrix Class Clay SandySoil


Benzene GC/MS (Head Space)(MCERTS) 10 µg/kg M (13) <10 (13) <10

Toluene GC/MS (Head Space)(MCERTS) 10 µg/kg M <10 <10

EthylBenzene GC/MS (Head Space)(MCERTS) 10 µg/kg M <10 <10

Meta/Para-Xylene GC/MS (Head Space)(MCERTS) 10 µg/kg M <10 <10

Ortho-Xylene GC/MS (Head Space)(MCERTS) 10 µg/kg M <10 <10

Methyl tert-Butyl Ether GC/MS (Head Space)(MCERTS) 10 µg/kg M <10 <10

Total Petroleum Hydrocarbons (C5 - C6 aliphatic) GC/MS (Head Space)(MCERTS) 100 µg/kg N <100 <100

Total Petroleum Hydrocarbons (C6-C8 aliphatic) GC/MS (Head Space)(MCERTS) 100 µg/kg N <100 <100

Total Petroleum Hydrocarbons (C8-C10 aliphatic) GC/MS (Head Space)(MCERTS) 100 µg/kg N <100 <100

Total Petroleum Hydrocarbons (C10-C12 aliphatic) GCxGC 1 mg/kg M (13) <1 (13) <1

Total Petroleum Hydrocarbons (C12-C16 aliphatic) GCxGC 1 mg/kg M (13) <1 (13) 2

Total Petroleum Hydrocarbons (C16-C21 aliphatic) GCxGC 1 mg/kg M (13) 2 (13) 3

Total Petroleum Hydrocarbons (C21-C35 aliphatic) GCxGC 2 mg/kg M (13) 9 (13) 5

Total Petroleum Hydrocarbons (C35-C40 aliphatic) GCxGC 1 mg/kg N (13) <1 (13) <1

Total Petroleum Hydrocarbons (Aliphatic) total Calc mg/kg N (13) 11 (13) 11

Total Petroleum Hydrocarbons (C6 - C7 aromatic) GC/MS (Head Space)(MCERTS) 100 µg/kg N <100 <100

Total Petroleum Hydrocarbons (C7-C8 aromatic) GC/MS (Head Space)(MCERTS) 100 µg/kg N <100 <100

Total Petroleum Hydrocarbons (C8-C10 aromatic) GC/MS (Head Space)(MCERTS) 100 µg/kg N <100 <100

Total Petroleum Hydrocarbons (C10-C12 aromatic) GCxGC 2 mg/kg M (13) <2 (13) <2

Total Petroleum Hydrocarbons (C12-C16 aromatic) GCxGC 1 mg/kg M (13) 6 (13) 2



Total Petroleum Hydrocarbons (C35-C40 aromatic) GCxGC 1 mg/kg N (13) <1 (13) <1

Total Petroleum Hydrocarbons (Aromatic) total Calc mg/kg N (13) 230 (13) 18

Total Petroleum Hydrocarbons (Aliphatic+Aromatic) Calc mg/kg N (13) 240 (13) 29





TPH


Customer Sample Reference BH12A ES4 BH12A ES5 BH04 ES5 BH04

Test Sample M105 M105 M105 M105

Bottom Depth 2.00 3.00 3.00 1.00

Date Sampled 03-JUL-2017 03-JUL-2017 27-JUN-2017 18-JUL-2017



Total Petroleum Hydrocarbons (C35-C40) GC/FID 1 mg/kg N (13) 6 (13) 2 (13) 100 (13) 7

Total Petroleum Hydrocarbons GC/FID 1 mg/kg M (13) 47 (13) 18 (13) 1200 (13) 140



667517-3









Bottom Depth 2.00 3.00 4.00 1.20 3.00




Dichlorodifluoromethane GC/MS (Head Space)(MCERTS) 50 µg/kg M (110) <100 <50 <50 <50 <50

Chloromethane GC/MS (Head Space)(MCERTS) 50 µg/kg U (110) <100 <50 <50 <50 <50

Vinyl chloride monomer GC/MS (Head Space)(MCERTS) 50 µg/kg M (110) <100 <50 <50 <50 <50

Bromomethane GC/MS (Head Space)(MCERTS) 50 µg/kg U (110) <100 <50 <50 <50 <50

Chloroethane GC/MS (Head Space)(MCERTS) 50 µg/kg M (110) <100 <50 <50 <50 <50

Trichlorofluoromethane GC/MS (Head Space)(MCERTS) 50 µg/kg M (110) <100 <50 <50 <50 <50

1,1-Dichloroethylene GC/MS (Head Space)(MCERTS) 50 µg/kg M (110) <100 <50 <50 <50 <50

Dichloromethane GC/MS (Head Space)(MCERTS) 50 µg/kg U (110) <100 <50 <50 <50 <50

Trans-1,2-Dichloroethylene GC/MS (Head Space)(MCERTS) 50 µg/kg M (110) <100 <50 <50 <50 <50


Cis-1,2-Dichloroethylene GC/MS (Head Space)(MCERTS) 50 µg/kg M (110) <100 <50 <50 <50 <50

2,2-Dichloropropane GC/MS (Head Space)(MCERTS) 50 µg/kg U (110) <100 <50 <50 <50 <50

Chloroform GC/MS (Head Space)(MCERTS) 50 µg/kg M (110) <100 <50 <50 <50 <50

Bromochloromethane GC/MS (Head Space)(MCERTS) 50 µg/kg M (110) <100 <50 <50 <50 <50


1,1-Dichloropropene GC/MS (Head Space)(MCERTS) 50 µg/kg M (110) <100 <50 <50 <50 <50

Carbon tetrachloride GC/MS (Head Space)(MCERTS) 50 µg/kg M (110) <100 <50 <50 <50 <50




Trichloroethylene GC/MS (Head Space)(MCERTS) 50 µg/kg M (110) <100 <50 <50 <50 <50

Bromodichloromethane GC/MS (Head Space)(MCERTS) 50 µg/kg M (110) <100 <50 <50 <50 <50

Dibromomethane GC/MS (Head Space)(MCERTS) 50 µg/kg M (110) <100 <50 <50 <50 <50

Cis-1,3-Dichloropropene GC/MS (Head Space)(MCERTS) 50 µg/kg M (110) <100 <50 <50 <50 <50


Trans-1,3-Dichloropropene GC/MS (Head Space)(MCERTS) 50 µg/kg M (110) <100 <50 <50 <50 <50



Tetrachloroethylene GC/MS (Head Space)(MCERTS) 50 µg/kg M (110) <100 <50 <50 <50 <50

Chlorodibromomethane GC/MS (Head Space)(MCERTS) 50 µg/kg M (110) <100 <50 <50 <50 <50

1,2-dibromoethane GC/MS (Head Space)(MCERTS) 50 µg/kg M (110) <100 <50 <50 <50 <50

Chlorobenzene GC/MS (Head Space)(MCERTS) 50 µg/kg M (110) <100 <50 <50 <50 <50

1,1,1,2-Tetrachloroethane GC/MS (Head Space)(MCERTS) 50 µg/kg M (110) <100 <50 <50 <50 <50


Meta/Para-Xylene GC/MS (Head Space)(MCERTS) 10 µg/kg M (110) <20 <10 <10 <10 15


Styrene GC/MS (Head Space)(MCERTS) 50 µg/kg U (110) <100 <50 <50 <50 <50

Bromoform GC/MS (Head Space)(MCERTS) 50 µg/kg M (110) <100 <50 <50 <50 <50

Isopropyl benzene GC/MS (Head Space)(MCERTS) 50 µg/kg M (110) <100 <50 <50 <50 <50

1,1,2,2-Tetrachloroethane GC/MS (Head Space)(MCERTS) 50 µg/kg U (110) <100 <50 <50 <50 <50

1,2,3-Trichloropropane GC/MS (Head Space)(MCERTS) 50 µg/kg U (110) <100 <50 <50 <50 <50

n-Propylbenzene GC/MS (Head Space)(MCERTS) 50 µg/kg M (110) <100 <50 <50 <50 <50

Bromobenzene GC/MS (Head Space)(MCERTS) 50 µg/kg M (110) <100 <50 <50 <50 <50


Tert-Butylbenzene GC/MS (Head Space)(MCERTS) 50 µg/kg M (110) <100 <50 <50 <50 <50


Sec-Butylbenzene GC/MS (Head Space)(MCERTS) 50 µg/kg M (110) <100 <50 <50 <50 <50

p-Isopropyltoluene GC/MS (Head Space)(MCERTS) 50 µg/kg M (110) <100 <50 <50 <50 <50








667517-3













Dichlorodifluoromethane GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50

Chloromethane GC/MS (Head Space)(MCERTS) 50 µg/kg U <50 <50

Vinyl chloride monomer GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50

Bromomethane GC/MS (Head Space)(MCERTS) 50 µg/kg U <50 <50

Chloroethane GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50

Trichlorofluoromethane GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50

1,1-Dichloroethylene GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50

Dichloromethane GC/MS (Head Space)(MCERTS) 50 µg/kg U <50 <50

Trans-1,2-Dichloroethylene GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50

1,1-Dichloroethane GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50

Cis-1,2-Dichloroethylene GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50

2,2-Dichloropropane GC/MS (Head Space)(MCERTS) 50 µg/kg U <50 <50

Chloroform GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50

Bromochloromethane GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50

1,1,1-Trichloroethane GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50

1,1-Dichloropropene GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50

Carbon tetrachloride GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50

1,2-Dichloroethane GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50

Benzene GC/MS (Head Space)(MCERTS) 10 µg/kg M (13) <10 (13) <10

1,2-Dichloropropane GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50

Trichloroethylene GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50

Bromodichloromethane GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50

Dibromomethane GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50

Cis-1,3-Dichloropropene GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50

Toluene GC/MS (Head Space)(MCERTS) 10 µg/kg M <10 <10

Trans-1,3-Dichloropropene GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50

1,1,2-Trichloroethane GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50

1,3-Dichloropropane GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50

Tetrachloroethylene GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50

Chlorodibromomethane GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50

1,2-dibromoethane GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50

Chlorobenzene GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50

1,1,1,2-Tetrachloroethane GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50

EthylBenzene GC/MS (Head Space)(MCERTS) 10 µg/kg M <10 <10

Meta/Para-Xylene GC/MS (Head Space)(MCERTS) 10 µg/kg M <10 <10

Ortho-Xylene GC/MS (Head Space)(MCERTS) 10 µg/kg M <10 <10

Styrene GC/MS (Head Space)(MCERTS) 50 µg/kg U <50 <50

Bromoform GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50

Isopropyl benzene GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50

1,1,2,2-Tetrachloroethane GC/MS (Head Space)(MCERTS) 50 µg/kg U <50 <50

1,2,3-Trichloropropane GC/MS (Head Space)(MCERTS) 50 µg/kg U <50 <50

n-Propylbenzene GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50

Bromobenzene GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50

1,3,5-Trimethylbenzene GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50

Tert-Butylbenzene GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50

1,2,4-Trimethylbenzene GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50

Sec-Butylbenzene GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50

p-Isopropyltoluene GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50

2-Chlorotoluene GC/MS (Head Space)(MCERTS) 50 µg/kg U <50 <50

4-Chlorotoluene GC/MS (Head Space)(MCERTS) 50 µg/kg U <50 <50

1,3-Dichlorobenzene GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50

1,4-Dichlorobenzene GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50

1,2-Dichlorobenzene GC/MS (Head Space)(MCERTS) 50 µg/kg M 59 <50



667517-3









Bottom Depth 2.00 3.00 4.00 1.20 3.00





Bis (2-chloroethyl) ether GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1 <1.0

2-Chlorophenol GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1 <1.0




Bis (2-chloroisopropyl) ether GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1 <1.0

2-methyl phenol GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1 <1.0

3/4-Methylphenol GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1 <1.0

Hexachloroethane GC/MS (MCERTS) 0.1 mg/kg U (162) <0.2 (162) <0.2 (162) <0.2 (162) <0.2 (162) <2.0

Nitrobenzene GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1 <1.0

Isophorone GC/MS (MCERTS) 0.1 mg/kg U <0.1 <0.1 <0.1 <0.1 <1.0

2-Nitrophenol GC/MS (MCERTS) 0.1 mg/kg U <0.1 <0.1 <0.1 <0.1 <1.0

2,4-Dimethylphenol GC/MS (MCERTS) 0.1 mg/kg U <0.1 <0.1 <0.1 <0.1 <1.0

Bis (2-chloroethoxy) methane GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1 <1.0

2,4-Dichlorophenol GC/MS (MCERTS) 0.1 mg/kg U <0.1 <0.1 <0.1 <0.1 <1.0

1,2,4-Trichlorobenzene GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1 <1.0

4-Chloroaniline GC/MS (MCERTS) 0.1 mg/kg U (162) <0.2 (162) <0.2 (162) <0.2 (162) <0.2 (162) <2.0

Hexachlorobutadiene GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1 <1.0

4-Chloro-3-methylphenol GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1 <1.0

2-Methylnaphthalene GC/MS (MCERTS) 0.1 mg/kg M 0.1 0.1 <0.1 <0.1 <1.0

Hexachlorocyclopentadiene GC/MS (MCERTS) 0.1 mg/kg U (162) <0.5 (162) <0.5 (162) <0.5 (162) <0.5 (162) <5.0



2-Chloronaphthalene GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1 <1.0

2-Nitroaniline GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1 <1.0

Dimethyl phthalate GC/MS (MCERTS) 0.1 mg/kg U <0.1 <0.1 <0.1 <0.1 <1.0

2,6-Dinitrotoluene GC/MS (MCERTS) 0.1 mg/kg U <0.1 <0.1 <0.1 <0.1 <1.0

3-Nitroaniline GC/MS (MCERTS) 0.1 mg/kg U <0.1 <0.1 <0.1 <0.1 <1.0

Dibenzofuran GC/MS (MCERTS) 0.1 mg/kg M <0.1 0.1 <0.1 <0.1 <1.0

2,4-Dinitrotoluene GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1 <1.0

Diethyl phthalate GC/MS (MCERTS) 0.1 mg/kg U <0.1 <0.1 <0.1 <0.1 <1.0

4-Chlorophenyl phenylether GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1 <1.0


Azobenzene GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1 <1.0

4-Bromophenyl phenylether GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1 <1.0

Hexachlorobenzene GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1 <1.0

Pentachlorophenol GC/MS (MCERTS) 0.1 mg/kg U <0.1 <0.1 <0.1 <0.1 <1.0

Carbazole GC/MS (MCERTS) 0.1 mg/kg U <0.1 0.1 <0.1 <0.1 <1.0

Di-n-butylphthalate GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1 <1.0

Butyl benzylphthalate GC/MS (MCERTS) 0.1 mg/kg U <0.1 <0.1 <0.1 <0.1 <1.0

Bis (2-ethylhexyl)phthalate GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1 <1.0

Di-n-octylphthalate GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1 <1.0



667517-3













Phenol GC/MS (MCERTS) 0.1 mg/kg M <1.0 <0.1

Bis (2-chloroethyl) ether GC/MS (MCERTS) 0.1 mg/kg M <1.0 <0.1

2-Chlorophenol GC/MS (MCERTS) 0.1 mg/kg M <1.0 <0.1

1,3-Dichlorobenzene GC/MS (MCERTS) 0.1 mg/kg M <1.0 <0.1



Bis (2-chloroisopropyl) ether GC/MS (MCERTS) 0.1 mg/kg M <1.0 <0.1

2-methyl phenol GC/MS (MCERTS) 0.1 mg/kg M <1.0 <0.1

3/4-Methylphenol GC/MS (MCERTS) 0.1 mg/kg M <1.0 <0.1

Hexachloroethane GC/MS (MCERTS) 0.1 mg/kg U (162) <2.0 (162) <0.2

Nitrobenzene GC/MS (MCERTS) 0.1 mg/kg M <1.0 <0.1

Isophorone GC/MS (MCERTS) 0.1 mg/kg U <1.0 <0.1

2-Nitrophenol GC/MS (MCERTS) 0.1 mg/kg U <1.0 <0.1

2,4-Dimethylphenol GC/MS (MCERTS) 0.1 mg/kg U <1.0 <0.1

Bis (2-chloroethoxy) methane GC/MS (MCERTS) 0.1 mg/kg M <1.0 <0.1

2,4-Dichlorophenol GC/MS (MCERTS) 0.1 mg/kg U <1.0 <0.1

1,2,4-Trichlorobenzene GC/MS (MCERTS) 0.1 mg/kg M <1.0 <0.1

4-Chloroaniline GC/MS (MCERTS) 0.1 mg/kg U (162) <2.0 (162) <0.5

Hexachlorobutadiene GC/MS (MCERTS) 0.1 mg/kg M <1.0 <0.1

4-Chloro-3-methylphenol GC/MS (MCERTS) 0.1 mg/kg M <1.0 <0.1

2-Methylnaphthalene GC/MS (MCERTS) 0.1 mg/kg M <1.0 <0.1

Hexachlorocyclopentadiene GC/MS (MCERTS) 0.1 mg/kg U (162) <5.0 (162) <0.5

2,4,6-Trichlorophenol GC/MS (MCERTS) 0.1 mg/kg U <1.0 <0.1

2,4,5-Trichlorophenol GC/MS (MCERTS) 0.1 mg/kg U <1.0 <0.1

2-Chloronaphthalene GC/MS (MCERTS) 0.1 mg/kg M <1.0 <0.1

2-Nitroaniline GC/MS (MCERTS) 0.1 mg/kg M <1.0 <0.1

Dimethyl phthalate GC/MS (MCERTS) 0.1 mg/kg U <1.0 <0.1

2,6-Dinitrotoluene GC/MS (MCERTS) 0.1 mg/kg U <1.0 <0.1

3-Nitroaniline GC/MS (MCERTS) 0.1 mg/kg U <1.0 (162) <0.2

Dibenzofuran GC/MS (MCERTS) 0.1 mg/kg M <1.0 <0.1

2,4-Dinitrotoluene GC/MS (MCERTS) 0.1 mg/kg M <1.0 <0.1

Diethyl phthalate GC/MS (MCERTS) 0.1 mg/kg U <1.0 <0.1

4-Chlorophenyl phenylether GC/MS (MCERTS) 0.1 mg/kg M <1.0 <0.1

4-Nitroaniline GC/MS (MCERTS) 0.1 mg/kg U (162) <2.0 (162) <0.2

Azobenzene GC/MS (MCERTS) 0.1 mg/kg M <1.0 <0.1

4-Bromophenyl phenylether GC/MS (MCERTS) 0.1 mg/kg M <1.0 <0.1

Hexachlorobenzene GC/MS (MCERTS) 0.1 mg/kg M <1.0 <0.1

Pentachlorophenol GC/MS (MCERTS) 0.1 mg/kg U <1.0 <0.1

Carbazole GC/MS (MCERTS) 0.1 mg/kg U <1.0 <0.1

Di-n-butylphthalate GC/MS (MCERTS) 0.1 mg/kg M <1.0 <0.1

Butyl benzylphthalate GC/MS (MCERTS) 0.1 mg/kg U <1.0 <0.1

Bis (2-ethylhexyl)phthalate GC/MS (MCERTS) 0.1 mg/kg M <1.0 <0.1

Di-n-octylphthalate GC/MS (MCERTS) 0.1 mg/kg M <1.0 <0.1



667517-3





Analysed as Water

Leachate Suite



Test Sample 10:1 10:1 10:1 10:1 10:1

Bottom Depth 2.00 3.00 4.00 1.20 3.00




Arsenic (Dissolved) ICP/MS (Filtered) 0.2 µg/l U 1.8 1.0 0.5 0.3 1.6

Boron (Dissolved) ICP/OES (Filtered) 10 µg/l N 92 98 67 31 340

Cadmium (Dissolved) ICP/MS (Filtered) 0.02 µg/l U 0.05 0.04 0.02 <0.02 0.04

Chromium (Dissolved) ICP/MS (Filtered) 1 µg/l U 2 <1 <1 <1 <1

Copper (Dissolved) ICP/MS (Filtered) 0.5 µg/l U 1.4 1.4 1.0 <0.5 0.6

Lead (Dissolved) ICP/MS (Filtered) 0.3 µg/l U <0.3 <0.3 <0.3 <0.3 0.9

Mercury (Dissolved) ICP/MS (Filtered) 0.05 µg/l U <0.05 <0.05 <0.05 <0.05 <0.05

Nickel (Dissolved) ICP/MS (Filtered) 1 µg/l U 2 4 <1 <1 5

Selenium (Dissolved) ICP/MS (Filtered) 0.5 µg/l U 7.0 3.4 <0.5 <0.5 <0.5

Vanadium (Dissolved) ICP/MS (Filtered) 2 µg/l U <2 <2 <2 <2 <2

Zinc (Dissolved) ICP/MS (Filtered) 2 µg/l U 9 6 9 <2 16

Ammoniacal nitrogen Discrete Analyser 0.05 mg/l U 0.05 0.06 <0.05 0.08 0.80

Chloride Discrete Analyser 1 mg/l U <1 <1 4 <1 <1

Cyanide (Total) Colorimetry 0.05 mg/l U <0.05 <0.05 <0.05 <0.05 <0.05

Fluoride Discrete Analyser 0.05 mg/l U 0.25 <0.05 0.08 0.45 0.16

Nitrate Discrete Analyser 0.5 mg/l U 8.8 4.5 <0.5 10 <0.5

Phosphate Discrete Analyser 0.5 mg/l U <0.5 <0.5 <0.5 <0.5 <0.5

Sulphate Discrete Analyser 0.5 mg/l U 73 550 45 2.0 340

Sulphide Colorimetry 0.05 mg/l N 0.07 0.08 0.08 0.08 0.07

Total Phenols GC/MS 0.5 µg/l U (13) <0.5 (13) <0.5 (13) <0.5 (13) <0.5 (13) <0.5

Dissolved Organic Carbon OX/IR 1 mg/l N 27 17 10 9 36

Electrical Conductivity Probe 10 µS/cm N 390 1100 210 86 950

pH Probe U 7.83 7.85 7.45 8.04 7.59



667517-3





Analysed as Water

Leachate Suite



Test Sample 10:1 10:1





Arsenic (Dissolved) ICP/MS (Filtered) 0.2 µg/l U 4.5 3.6

Boron (Dissolved) ICP/OES (Filtered) 10 µg/l N 120 32

Cadmium (Dissolved) ICP/MS (Filtered) 0.02 µg/l U 0.03 0.03

Chromium (Dissolved) ICP/MS (Filtered) 1 µg/l U 1 <1

Copper (Dissolved) ICP/MS (Filtered) 0.5 µg/l U <0.5 1.4

Lead (Dissolved) ICP/MS (Filtered) 0.3 µg/l U 0.3 0.5

Mercury (Dissolved) ICP/MS (Filtered) 0.05 µg/l U <0.05 <0.05

Nickel (Dissolved) ICP/MS (Filtered) 1 µg/l U 1 2

Selenium (Dissolved) ICP/MS (Filtered) 0.5 µg/l U <0.5 0.7

Vanadium (Dissolved) ICP/MS (Filtered) 2 µg/l U 3 <2

Zinc (Dissolved) ICP/MS (Filtered) 2 µg/l U <2 <2

Ammoniacal nitrogen Discrete Analyser 0.05 mg/l U 2.5 0.94

Chloride Discrete Analyser 1 mg/l U <1 <1

Cyanide (Total) Colorimetry 0.05 mg/l U <0.05 <0.05

Fluoride Discrete Analyser 0.05 mg/l U 0.29 0.80

Nitrate Discrete Analyser 0.5 mg/l U <0.5 1.1

Phosphate Discrete Analyser 0.5 mg/l U <0.5 <0.5

Sulphate Discrete Analyser 0.5 mg/l U 25 34

Sulphide Colorimetry 0.05 mg/l N 0.08 0.06

Total Phenols GC/MS 0.5 µg/l U (13,100) <2.5 <0.5

Dissolved Organic Carbon OX/IR 1 mg/l N 14 22

Electrical Conductivity Probe 10 µS/cm N 130 220

pH Probe U 7.55 7.78



667517-3





Analysed as Water

PAH USEPA16



Test Sample 10:1 10:1 10:1 10:1 10:1

Bottom Depth 2.00 3.00 4.00 1.20 3.00




Naphthalene GC/MS (SIR) 0.01 µg/l U (13) 0.07 (13) 0.10 (13) 0.02 (13) 0.14 (13) 0.15

Acenaphthylene GC/MS (SIR) 0.01 µg/l U (13) 0.01 (13) <0.01 (13) 0.01 (13) 0.01 (13) 0.02

Acenaphthene GC/MS (SIR) 0.01 µg/l U (13) 0.02 (13) 0.02 (13) 0.02 (13) 0.03 (13) 0.03

Fluorene GC/MS (SIR) 0.01 µg/l U (13) 0.03 (13) 0.03 (13) 0.03 (13) 0.04 (13) 0.03

Phenanthrene GC/MS (SIR) 0.01 µg/l U (13) 0.05 (13) 0.05 (13) 0.03 (13) 0.08 (13) 0.06

Anthracene GC/MS (SIR) 0.01 µg/l U (13) 0.01 (13) <0.01 (13) 0.01 (13) <0.01 (13) 0.01

Fluoranthene GC/MS (SIR) 0.01 µg/l U (13) 0.02 (13) 0.03 (13) 0.01 (13) 0.03 (13) 0.07

Pyrene GC/MS (SIR) 0.01 µg/l U (13) 0.02 (13) 0.02 (13) 0.01 (13) 0.02 (13) 0.07

Benzo(a)Anthracene GC/MS (SIR) 0.01 µg/l U (13) 0.01 (13) 0.01 (13) 0.01 (13) 0.01 (13) 0.03

Chrysene GC/MS (SIR) 0.01 µg/l U (13) 0.01 (13) 0.02 (13) 0.01 (13) 0.01 (13) 0.04

Benzo(b)fluoranthene GC/MS (SIR) 0.01 µg/l U (13) 0.01 (13) 0.01 (13) 0.01 (13) 0.01 (13) 0.03

Benzo(k)fluoranthene GC/MS (SIR) 0.01 µg/l U (13) 0.01 (13) 0.02 (13) 0.01 (13) 0.01 (13) 0.04

Benzo(a)Pyrene GC/MS (SIR) 0.01 µg/l U (13) 0.01 (13) 0.01 (13) 0.01 (13) 0.01 (13) 0.03

Indeno(123-cd)Pyrene GC/MS (SIR) 0.01 µg/l U (13) 0.01 (13) 0.01 (13) 0.01 (13) 0.01 (13) 0.02

Dibenzo(ah)Anthracene GC/MS (SIR) 0.01 µg/l U (13) <0.01 (13) 0.01 (13) 0.01 (13) <0.01 (13) 0.01

Benzo(ghi)Perylene GC/MS (SIR) 0.01 µg/l U (13) 0.01 (13) 0.01 (13) 0.01 (13) 0.01 (13) 0.02

Polyaromatic Hydrocarbons (Total) GC/MS (SIR) 0.01 µg/l U 0.30 0.35 0.22 0.42 0.66





Analysed as Water

PAH USEPA16








Naphthalene GC/MS (SIR) 0.01 µg/l U (13) 2.9 (13) 0.02

Acenaphthylene GC/MS (SIR) 0.01 µg/l U (13) 0.10 (13) <0.01

Acenaphthene GC/MS (SIR) 0.01 µg/l U (13) 0.35 (13) <0.01

Fluorene GC/MS (SIR) 0.01 µg/l U (13) 0.50 (13) 0.01

Phenanthrene GC/MS (SIR) 0.01 µg/l U (13) 1.3 (13) 0.03

Anthracene GC/MS (SIR) 0.01 µg/l U (13) 0.15 (13) 0.01

Fluoranthene GC/MS (SIR) 0.01 µg/l U (13) 0.70 (13) 0.01

Pyrene GC/MS (SIR) 0.01 µg/l U (13) 0.60 (13) 0.01

Benzo(a)Anthracene GC/MS (SIR) 0.01 µg/l U (13) 0.20 (13) 0.01

Chrysene GC/MS (SIR) 0.01 µg/l U (13) 0.30 (13) 0.01

Benzo(b)fluoranthene GC/MS (SIR) 0.01 µg/l U (13) 0.20 (13) 0.01

Benzo(k)fluoranthene GC/MS (SIR) 0.01 µg/l U (13) 0.20 (13) 0.01

Benzo(a)Pyrene GC/MS (SIR) 0.01 µg/l U (13) 0.15 (13) 0.01

Indeno(123-cd)Pyrene GC/MS (SIR) 0.01 µg/l U (13) 0.15 (13) 0.01

Dibenzo(ah)Anthracene GC/MS (SIR) 0.01 µg/l U (13) 0.05 (13) <0.01

Benzo(ghi)Perylene GC/MS (SIR) 0.01 µg/l U (13) 0.15 (13) 0.01

Polyaromatic Hydrocarbons (Total) GC/MS (SIR) 0.01 µg/l U 7.9 0.16



667517-3





Analysed as Water

PCB EC7



Test Sample 10:1 10:1 10:1 10:1 10:1

Bottom Depth 2.00 3.00 4.00 1.20 3.00




Polychlorinated biphenyl BZ#28 GC/MS (HR) 0.005 µg/l U <0.005 <0.005 <0.005 <0.005 <0.005



Polychlorinated biphenyl BZ#118 GC/MS 0.005 µg/l U <0.005 <0.005 <0.005 <0.005 <0.005








Analysed as Water

PCB EC7








Polychlorinated biphenyl BZ#28 GC/MS (HR) 0.005 µg/l U (100) <0.020 <0.005



Polychlorinated biphenyl BZ#118 GC/MS 0.005 µg/l U (100) <0.020 <0.005






667517-3





Analysed as Water




Test Sample 10:1 10:1 10:1 10:1 10:1

Bottom Depth 2.00 3.00 4.00 1.20 3.00

Date Sampled 03-JUL-2017 03-JUL-2017 03-JUL-2017 27-JUN-2017

27-JUN-2017



Benzene GC/MS (Headspace) 1 µg/l U (13) <1 (13) <1 (13) <1 (13) <1 (13) <1

Toluene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1 <1

EthylBenzene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1 <1

Meta/Para-Xylene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1 <1

Ortho-Xylene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1 <1

Methyl tert-Butyl Ether GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1 <1

Total Petroleum Hydrocarbons (C5 - C6 aliphatic) GC/MS (Headspace)(LV) 10 µg/l N <10 <10 <10 <10 <10

Total Petroleum Hydrocarbons (C6-C8 aliphatic) GC/MS (Headspace)(LV) 10 µg/l N <10 <10 <10 <10 <10

Total Petroleum Hydrocarbons (C8-C10 aliphatic) GC/MS (Headspace)(LV) 10 µg/l N <10 <10 <10 <10 <10

Total Petroleum Hydrocarbons (C10-C12 aliphatic) GCxGC (LV) 0.01 mg/l N (100,13) <0.03 (13,100) <0.02 (13,100) <0.02 (13,100) <0.02 (100,13) <0.03




Total Petroleum Hydrocarbons (C6 - C7 aromatic) GC/MS (Headspace)(LV) 10 µg/l N <10 <10 <10 <10 <10

Total Petroleum Hydrocarbons (C7-C8 aromatic) GC/MS (Headspace)(LV) 10 µg/l N <10 <10 <10 <10 <10

Total Petroleum Hydrocarbons (C8-C10 aromatic) GC/MS (Headspace)(LV) 10 µg/l N <10 <10 <10 <10 <10

Total Petroleum Hydrocarbons (C10-C12 aromatic) GCxGC (LV) 0.01 mg/l N (13,100) <0.03 (100,13) <0.02 (100,13) <0.02 (13,100) <0.02 (100,13) <0.03






667517-3





Analysed as Water







18-JUL-2017



Benzene GC/MS (Headspace) 1 µg/l U (13) <1 (13) <1

Toluene GC/MS (Headspace) 1 µg/l U <1 <1

EthylBenzene GC/MS (Headspace) 1 µg/l U <1 <1

Meta/Para-Xylene GC/MS (Headspace) 1 µg/l U <1 <1

Ortho-Xylene GC/MS (Headspace) 1 µg/l U <1 <1

Methyl tert-Butyl Ether GC/MS (Headspace) 1 µg/l U <1 <1

Total Petroleum Hydrocarbons (C5 - C6 aliphatic) GC/MS (Headspace)(LV) 10 µg/l N <10 <10

Total Petroleum Hydrocarbons (C6-C8 aliphatic) GC/MS (Headspace)(LV) 10 µg/l N <10 <10

Total Petroleum Hydrocarbons (C8-C10 aliphatic) GC/MS (Headspace)(LV) 10 µg/l N <10 <10

Total Petroleum Hydrocarbons (C10-C12 aliphatic) GCxGC (LV) 0.01 mg/l N (13) <0.01 (13) <0.01




Total Petroleum Hydrocarbons (C6 - C7 aromatic) GC/MS (Headspace)(LV) 10 µg/l N <10 <10

Total Petroleum Hydrocarbons (C7-C8 aromatic) GC/MS (Headspace)(LV) 10 µg/l N <10 <10

Total Petroleum Hydrocarbons (C8-C10 aromatic) GC/MS (Headspace)(LV) 10 µg/l N <10 <10

Total Petroleum Hydrocarbons (C10-C12 aromatic) GCxGC (LV) 0.01 mg/l N (13) <0.01 (13) 0.03



Total Petroleum Hydrocarbons (C21-C35 aromatic) GCxGC (LV) 0.01 mg/l N (13) <0.01 (13) <0.01



667517-3





Analysed as Water




Test Sample 10:1 10:1 10:1 10:1 10:1

Bottom Depth 2.00 3.00 4.00 1.20 3.00




Dichlorodifluoromethane GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1 <1

Chloromethane GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1 <1

Vinyl chloride monomer GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1 <1

Bromomethane GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1 <1

Chloroethane GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1 <1

Trichlorofluoromethane GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1 <1

1,1-Dichloroethylene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1 <1

Dichloromethane GC/MS (Headspace) 50 µg/l N <50 <50 <50 <50 <50

Trans-1,2-Dichloroethylene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1 <1

1,1-Dichloroethane GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1 <1

Cis-1,2-Dichloroethylene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1 <1

2,2-Dichloropropane GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1 <1

Chloroform GC/MS (Headspace) 1 µg/l U (13) 1 (13) 17 (13) 29 (13) 33 (13) <1

Bromochloromethane GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1 <1

1,1,1-Trichloroethane GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1 <1

1,1-Dichloropropene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1 <1

Carbon tetrachloride GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1 <1

1,2-Dichloroethane GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1 <1

Benzene GC/MS (Headspace) 1 µg/l U (13) <1 (13) <1 (13) <1 (13) <1 (13) <1


1,1,2-Trichloroethylene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1 <1

Bromodichloromethane GC/MS (Headspace) 1 µg/l U (13) <1 (13) <1 (13) <1 (13) <1 (13) <1

Dibromomethane GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1 <1

Cis-1,3-Dichloropropene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1 <1

Toluene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1 <1

Trans-1,3-Dichloropropene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1 <1

1,1,2-Trichloroethane GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1 <1


Tetrachloroethylene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1 <1

Chlorodibromomethane GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1 <1

1,2-dibromoethane GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1 <1

Chlorobenzene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1 <1

1,1,1,2-Tetrachloroethane GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1 <1

EthylBenzene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1 <1

Meta/Para-Xylene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1 <1

Ortho-Xylene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1 <1

Styrene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1 <1

Bromoform GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1 <1

Isopropyl benzene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1 <1

1,1,2,2-Tetrachloroethane GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1 <1

1,2,3-Trichloropropane GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1 <1

n-Propylbenzene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1 <1

Bromobenzene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1 <1

1,3,5-Trimethylbenzene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1 <1

Tert-Butylbenzene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1 <1

1,2,4-Trimethylbenzene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1 <1

Sec-Butylbenzene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1 <1

p-Isopropyltoluene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1 <1

2-Chlorotoluene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1 <1

4-Chlorotoluene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1 <1

1,3-Dichlorobenzene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1 <1





667517-3





Analysed as Water









Dichlorodifluoromethane GC/MS (Headspace) 1 µg/l U <1 <1

Chloromethane GC/MS (Headspace) 1 µg/l U <1 <1

Vinyl chloride monomer GC/MS (Headspace) 1 µg/l U <1 <1

Bromomethane GC/MS (Headspace) 1 µg/l U <1 <1

Chloroethane GC/MS (Headspace) 1 µg/l U <1 <1

Trichlorofluoromethane GC/MS (Headspace) 1 µg/l U <1 <1

1,1-Dichloroethylene GC/MS (Headspace) 1 µg/l U <1 <1

Dichloromethane GC/MS (Headspace) 50 µg/l N <50 <50

Trans-1,2-Dichloroethylene GC/MS (Headspace) 1 µg/l U <1 <1

1,1-Dichloroethane GC/MS (Headspace) 1 µg/l U <1 <1

Cis-1,2-Dichloroethylene GC/MS (Headspace) 1 µg/l U <1 <1

2,2-Dichloropropane GC/MS (Headspace) 1 µg/l U <1 <1

Chloroform GC/MS (Headspace) 1 µg/l U (13) 35 <1

Bromochloromethane GC/MS (Headspace) 1 µg/l U <1 <1

1,1,1-Trichloroethane GC/MS (Headspace) 1 µg/l U <1 <1

1,1-Dichloropropene GC/MS (Headspace) 1 µg/l U <1 <1

Carbon tetrachloride GC/MS (Headspace) 1 µg/l U <1 <1

1,2-Dichloroethane GC/MS (Headspace) 1 µg/l U <1 <1

Benzene GC/MS (Headspace) 1 µg/l U (13) <1 (13) <1


1,1,2-Trichloroethylene GC/MS (Headspace) 1 µg/l U <1 <1

Bromodichloromethane GC/MS (Headspace) 1 µg/l U (13) <1 (13) <1

Dibromomethane GC/MS (Headspace) 1 µg/l U <1 <1

Cis-1,3-Dichloropropene GC/MS (Headspace) 1 µg/l U <1 <1

Toluene GC/MS (Headspace) 1 µg/l U <1 <1

Trans-1,3-Dichloropropene GC/MS (Headspace) 1 µg/l U <1 <1

1,1,2-Trichloroethane GC/MS (Headspace) 1 µg/l U <1 <1


Tetrachloroethylene GC/MS (Headspace) 1 µg/l U <1 <1

Chlorodibromomethane GC/MS (Headspace) 1 µg/l U <1 <1

1,2-dibromoethane GC/MS (Headspace) 1 µg/l U <1 <1

Chlorobenzene GC/MS (Headspace) 1 µg/l U <1 <1

1,1,1,2-Tetrachloroethane GC/MS (Headspace) 1 µg/l U <1 <1

EthylBenzene GC/MS (Headspace) 1 µg/l U <1 <1

Meta/Para-Xylene GC/MS (Headspace) 1 µg/l U <1 <1

Ortho-Xylene GC/MS (Headspace) 1 µg/l U <1 <1

Styrene GC/MS (Headspace) 1 µg/l U <1 <1

Bromoform GC/MS (Headspace) 1 µg/l U <1 <1

Isopropyl benzene GC/MS (Headspace) 1 µg/l U <1 <1

1,1,2,2-Tetrachloroethane GC/MS (Headspace) 1 µg/l U <1 <1

1,2,3-Trichloropropane GC/MS (Headspace) 1 µg/l U <1 <1

n-Propylbenzene GC/MS (Headspace) 1 µg/l U <1 <1

Bromobenzene GC/MS (Headspace) 1 µg/l U <1 <1

1,3,5-Trimethylbenzene GC/MS (Headspace) 1 µg/l U <1 <1

Tert-Butylbenzene GC/MS (Headspace) 1 µg/l U <1 <1

1,2,4-Trimethylbenzene GC/MS (Headspace) 1 µg/l U <1 <1

Sec-Butylbenzene GC/MS (Headspace) 1 µg/l U <1 <1

p-Isopropyltoluene GC/MS (Headspace) 1 µg/l U <1 <1

2-Chlorotoluene GC/MS (Headspace) 1 µg/l U <1 <1

4-Chlorotoluene GC/MS (Headspace) 1 µg/l U <1 <1

1,3-Dichlorobenzene GC/MS (Headspace) 1 µg/l U <1 <1





667517-3





Analysed as Water




Test Sample 10:1 10:1 10:1 10:1 10:1

Bottom Depth 2.00 3.00 4.00 1.20 3.00




Phenol GC/MS 10 µg/l U <10 <10 <10 <10 <10

Bis (2-chloroethyl) ether GC/MS 10 µg/l U <10 <10 <10 <10 <10

2-Chlorophenol GC/MS 10 µg/l U <10 <10 <10 <10 <10

1,3-Dichlorobenzene GC/MS 10 µg/l U <10 <10 <10 <10 <10



Bis (2-chloroisopropyl) ether GC/MS 10 µg/l U <10 <10 <10 <10 <10

2-methyl phenol GC/MS 10 µg/l U <10 <10 <10 <10 <10

3/4-Methylphenol GC/MS 10 µg/l U <10 <10 <10 <10 <10

Hexachloroethane GC/MS 10 µg/l U (162) <20 (162) <20 (162) <20 (162) <20 (162) <20

Nitrobenzene GC/MS 10 µg/l U <10 <10 <10 <10 <10

Isophorone GC/MS 10 µg/l U <10 <10 <10 <10 <10

2-Nitrophenol GC/MS 10 µg/l U <10 <10 <10 <10 <10

2,4-Dimethylphenol GC/MS 10 µg/l U <10 <10 <10 <10 <10

Bis (2-chloroethoxy) methane GC/MS 10 µg/l U <10 <10 <10 <10 <10

2,4-Dichlorophenol GC/MS 10 µg/l U <10 <10 <10 <10 <10

1,2,4-Trichlorobenzene GC/MS 10 µg/l U (162) <20 (162) <20 (162) <20 (162) <20 (162) <20

4-Chloroaniline GC/MS 10 µg/l U <10 <10 <10 <10 <10

Hexachlorobutadiene GC/MS 10 µg/l U (162) <20 (162) <20 (162) <20 (162) <20 (162) <20

4-Chloro-3-methylphenol GC/MS 10 µg/l U <10 <10 <10 <10 <10

2-Methylnaphthalene GC/MS 10 µg/l U <10 <10 <10 <10 <10

Hexachlorocyclopentadiene GC/MS 10 µg/l U (162) <50 (162) <50 (162) <50 (162) <50 (162) <50

2,4,6-Trichlorophenol GC/MS 10 µg/l U <10 <10 <10 <10 <10

2,4,5-Trichlorophenol GC/MS 10 µg/l U <10 <10 <10 <10 <10

2-Chloronaphthalene GC/MS 10 µg/l U <10 <10 <10 <10 <10

2-Nitroaniline GC/MS 10 µg/l U <10 <10 <10 <10 <10

Dimethyl phthalate GC/MS 10 µg/l U <10 <10 <10 <10 <10

2,6-Dinitrotoluene GC/MS 10 µg/l U <10 <10 <10 <10 <10


Dibenzofuran GC/MS 10 µg/l U <10 <10 <10 <10 <10

2,4-Dinitrotoluene GC/MS 10 µg/l U <10 <10 <10 <10 <10

Diethyl phthalate GC/MS 10 µg/l U <10 <10 <10 <10 <10

4-Chlorophenyl phenylether GC/MS 10 µg/l U <10 <10 <10 <10 <10


Azobenzene GC/MS 10 µg/l U <10 <10 <10 <10 <10

4-Bromophenyl phenylether GC/MS 10 µg/l U <10 <10 <10 <10 <10

Hexachlorobenzene GC/MS 10 µg/l U <10 <10 <10 <10 <10

Pentachlorophenol GC/MS 10 µg/l U <10 <10 <10 <10 <10

Carbazole GC/MS 10 µg/l U <10 <10 <10 <10 <10

Di-n-butylphthalate GC/MS 10 µg/l U <10 <10 <10 <10 <10

Butyl benzylphthalate GC/MS 10 µg/l U <10 <10 <10 <10 <10

Bis (2-ethylhexyl)phthalate GC/MS 10 µg/l U <10 <10 <10 <10 <10

Di-n-octylphthalate GC/MS 10 µg/l U <10 <10 <10 <10 <10



667517-3





Analysed as Water









Phenol GC/MS 10 µg/l U <10 <10

Bis (2-chloroethyl) ether GC/MS 10 µg/l U <10 <10

2-Chlorophenol GC/MS 10 µg/l U <10 <10

1,3-Dichlorobenzene GC/MS 10 µg/l U <10 (162) <20



Bis (2-chloroisopropyl) ether GC/MS 10 µg/l U <10 <10

2-methyl phenol GC/MS 10 µg/l U <10 <10

3/4-Methylphenol GC/MS 10 µg/l U <10 <10

Hexachloroethane GC/MS 10 µg/l U (162) <20 (162) <20

Nitrobenzene GC/MS 10 µg/l U <10 <10

Isophorone GC/MS 10 µg/l U <10 <10

2-Nitrophenol GC/MS 10 µg/l U <10 (162) <20

2,4-Dimethylphenol GC/MS 10 µg/l U <10 <10

Bis (2-chloroethoxy) methane GC/MS 10 µg/l U <10 <10

2,4-Dichlorophenol GC/MS 10 µg/l U <10 <10

1,2,4-Trichlorobenzene GC/MS 10 µg/l U (162) <20 (162) <20

4-Chloroaniline GC/MS 10 µg/l U <10 (162) <50

Hexachlorobutadiene GC/MS 10 µg/l U (162) <20 (162) <50

4-Chloro-3-methylphenol GC/MS 10 µg/l U <10 <10

2-Methylnaphthalene GC/MS 10 µg/l U <10 (162) <20

Hexachlorocyclopentadiene GC/MS 10 µg/l U (162) <50 (162) <50

2,4,6-Trichlorophenol GC/MS 10 µg/l U <10 (162) <20

2,4,5-Trichlorophenol GC/MS 10 µg/l U <10 (162) <20

2-Chloronaphthalene GC/MS 10 µg/l U <10 <10

2-Nitroaniline GC/MS 10 µg/l U <10 <10

Dimethyl phthalate GC/MS 10 µg/l U <10 <10

2,6-Dinitrotoluene GC/MS 10 µg/l U <10 <10

3-Nitroaniline GC/MS 10 µg/l U <10 (162) <20

Dibenzofuran GC/MS 10 µg/l U <10 <10

2,4-Dinitrotoluene GC/MS 10 µg/l U <10 <10

Diethyl phthalate GC/MS 10 µg/l U <10 <10

4-Chlorophenyl phenylether GC/MS 10 µg/l U <10 <10

4-Nitroaniline GC/MS 10 µg/l U <10 <10

Azobenzene GC/MS 10 µg/l U <10 <10

4-Bromophenyl phenylether GC/MS 10 µg/l U <10 <10

Hexachlorobenzene GC/MS 10 µg/l U <10 <10

Pentachlorophenol GC/MS 10 µg/l U <10 (162) <20

Carbazole GC/MS 10 µg/l U <10 <10

Di-n-butylphthalate GC/MS 10 µg/l U <10 <10

Butyl benzylphthalate GC/MS 10 µg/l U <10 <10

Bis (2-ethylhexyl)phthalate GC/MS 10 µg/l U <10 <10

Di-n-octylphthalate GC/MS 10 µg/l U <10 <10



667517-3


Notes





Analysed as Water

Waste Acceptance Criteria (reduced)



Test Sample 10:1 10:1 10:1 10:1 10:1

Bottom Depth 2.00 3.00 4.00 1.20 3.00




Antimony (Dissolved) ICP/MS (Filtered) 1 µg/l U 3 3 1 <1 1

Barium (Dissolved) ICP/MS (Filtered) 1 µg/l U 77 37 59 11 76

Molybdenum (Dissolved) ICP/MS (Filtered) 1 µg/l N 20 9 3 3 17

Phenols (Total-Mono) Colorimetry 0.1 mg/l U <0.1 <0.1 <0.1 <0.1 <0.1

Electrical Conductivity Probe 10 µS/cm N 390 1100 210 86 950

Total Dissolved Solids Grav 100 mg/l N 240 670 120 <100 570





Analysed as Water









Antimony (Dissolved) ICP/MS (Filtered) 1 µg/l U <1 4

Barium (Dissolved) ICP/MS (Filtered) 1 µg/l U 26 41

Molybdenum (Dissolved) ICP/MS (Filtered) 1 µg/l N 11 10

Phenols (Total-Mono) Colorimetry 0.1 mg/l U <0.1 <0.1

Electrical Conductivity Probe 10 µS/cm N 130 220

Total Dissolved Solids Grav 100 mg/l N <100 130

Value Description

AR As Received

10:1 Leachate to BS EN 12457-2 (10:1)

10:1 S Data for BS EN 12457-2 (10:1)




N.D. Not Detected



110 LOD raised due to low internal standard recovery.










667517-3


These samples will be analysed exceeding recommended holding times. It is possible therefore that the results provided may be compromised.



667517-3




CornbrookManchester

M16 9FETel : 0161 874 2400Fax : 0161 874 2468






Date Job Received at Concept: 06-Jul-2017Date Analysis Started: 13-Jul-2017







Wales (No 2514788)

1549



Page 1 of 14

667902-1














Customer Sample Reference : BH05




Bottom Depth : 1.80



Soil Result Inert Waste Landfill Stable non reactive Hazardous WasteLandfill


Total Organic Carbon OX/IR 0.1 % N 6.3 3.0 5.0 6.0

pH Probe M 7.6 > 6.0

Data for BS EN 12457-2 (10:1) Result Inert Waste Landfill Stable non reactive Hazardous WasteLandfill







Copper Calc WAC ICP/MS 0.0050 mg/kg N <0.0050 2.0 50.0 100.0


Mercury Calc WAC ICP/MS 0.00050 mg/kg N 0.00051 0.01 0.2 2.0



Selenium Calc WAC ICP/MS 0.0050 mg/kg N <0.0050 0.1 0.5 7.0


Chloride Calc (W) 10 mg/kg N 110 800.0 15000.0 25000.0

Fluoride Calc (W) 0.50 mg/kg N 12 10.0 150.0 500.0







667902-1





MCERTS Preparation


Customer Sample Reference BH05 BH05 BH06 BH10

Test Sample AR AR AR AR

Bottom Depth 1.80 2.50 2.00 0.50

Date Sampled 06-JUL-2017 06-JUL-2017 06-JUL-2017 03-JUL-2017

Matrix Class Sandy Soil Sandy Soil Clay Sandy Soil


Moisture @105C Grav (1 Dec) (105 C) 0.1 % N 10 23 16 9.8





MCERTS Preparation




Bottom Depth 1.80 2.50 2.00 0.50




Retained on 10mm sieve Grav 0.1 % N <0.1 <0.1 <0.1 <0.1





Soil Suite



Test Sample A40 A40 A40 A40

Bottom Depth 1.80 2.50 2.00 0.50




Sulphate (Total) ICP/OES 0.01 % N 0.13 0.12 0.03 0.05

Sulphur (total) ICP/OES 0.01 % N 0.15 0.20 0.01 0.02

Total Organic Carbon OX/IR 0.1 % N 6.3 8.7 0.3 1.5



667902-1





Soil Suite



Test Sample AR AR AR AR

Bottom Depth 1.80 2.50 2.00 0.50




Boron (water-soluble) ICP/OES 1 mg/kg N 1 1 <1 <1

Cyanide (Total) Colorimetry (CF) 1 mg/kg M 2 2 <1 <1

Sulphide Colorimetry 10 mg/kg N <10 <10 <10 <10

Total Phenols GC/MS (MCERTS) 0.1 mg/kg N <0.1 <0.1 <0.1 <0.1

Asbestos ID PLM SU N.D. N.D. N.D. N.D.

pH Probe M 7.6 7.8 8.1 8.1





Soil Suite




Bottom Depth 1.80 2.50 2.00 0.50




Arsenic ICP/OES 2 mg/kg M 18 25 7 110

Cadmium ICP/OES 1 mg/kg M 2 1 <1 <1

Chromium ICP/OES 1 mg/kg M 49 36 20 12

Copper ICP/OES 1 mg/kg M 88 100 8 39

Lead ICP/OES 1 mg/kg M 340 340 13 50

Mercury ICP/OES 1 mg/kg M 1 <1 <1 <1

Nickel ICP/OES 1 mg/kg M 27 31 18 16

Selenium ICP/OES 3 mg/kg M <3 <3 <3 <3

Vanadium ICP/OES 1 mg/kg M 36 42 23 16

Zinc ICP/OES 1 mg/kg M 470 550 45 81



667902-1





PAH USEPA16




Bottom Depth 1.80 2.50 2.00 0.50




Naphthalene GC/MS (MCERTS) 0.1 mg/kg M 0.5 <0.1 <0.1 <0.1

Acenaphthylene GC/MS (MCERTS) 0.1 mg/kg U <0.1 <0.1 <0.1 <0.1

Acenaphthene GC/MS (MCERTS) 0.1 mg/kg M 0.2 <0.1 <0.1 <0.1

Fluorene GC/MS (MCERTS) 0.1 mg/kg M 0.2 <0.1 <0.1 <0.1

Phenanthrene GC/MS (MCERTS) 0.1 mg/kg M 1.2 <0.1 <0.1 <0.1

Anthracene GC/MS (MCERTS) 0.1 mg/kg U 0.3 <0.1 <0.1 <0.1

Fluoranthene GC/MS (MCERTS) 0.1 mg/kg M 1.2 <0.1 <0.1 0.1

Pyrene GC/MS (MCERTS) 0.1 mg/kg M 1.1 <0.1 <0.1 <0.1

Benzo(a)Anthracene GC/MS (MCERTS) 0.1 mg/kg M 0.5 <0.1 <0.1 <0.1

Chrysene GC/MS (MCERTS) 0.1 mg/kg M 0.6 <0.1 <0.1 <0.1

Benzo(b)fluoranthene GC/MS (MCERTS) 0.1 mg/kg M 0.4 <0.1 <0.1 <0.1

Benzo(k)fluoranthene GC/MS (MCERTS) 0.1 mg/kg M 0.4 <0.1 <0.1 <0.1

Benzo(a)Pyrene GC/MS (MCERTS) 0.1 mg/kg M 0.4 <0.1 <0.1 <0.1

Indeno(123-cd)Pyrene GC/MS (MCERTS) 0.1 mg/kg M 0.2 <0.1 <0.1 <0.1

Dibenzo(ah)Anthracene GC/MS (MCERTS) 0.1 mg/kg M 0.1 <0.1 <0.1 <0.1

Benzo(ghi)Perylene GC/MS (MCERTS) 0.1 mg/kg M 0.2 <0.1 <0.1 <0.1

Polyaromatic Hydrocarbons (Total) GC/MS (MCERTS) 0.1 mg/kg U 7.5 <0.1 <0.1 0.1





PCB EC7




Bottom Depth 1.80 2.50 2.00 0.50





mg/kg M (26,9) <0.010 (26) <0.0010 (26) <0.0010 (26) <0.0010


mg/kg M (26,9) <0.010 (26) <0.0010 (26) <0.0010 (26) <0.0010


mg/kg M (9,26) <0.010 (26) <0.0010 (26) <0.0010 (26) <0.0010


mg/kg M (26,9) <0.010 (26) <0.0010 (26) <0.0010 (26) <0.0010


mg/kg M (9,26) <0.010 (26) <0.0010 (26) <0.0010 (26) <0.0010


mg/kg M (26,9) <0.010 (26) <0.0010 (26) <0.0010 (26) <0.0010


mg/kg M (26,9) <0.010 (26) <0.0010 (26) <0.0010 (26) <0.0010



667902-1







667902002

667902003

667902004



Bottom Depth 1.80 2.50 2.00 0.50


06-JUL-2017

06-JUL-2017

03-JUL-2017


SandySoil

Clay SandySoil


Benzene GC/MS (Head Space)(MCERTS) 10 µg/kg M <10 <10 <10 <10

Toluene GC/MS (Head Space)(MCERTS) 10 µg/kg M 70 <10 <10 <10

EthylBenzene GC/MS (Head Space)(MCERTS) 10 µg/kg M (175) 12000 <10 <10 <10

Meta/Para-Xylene GC/MS (Head Space)(MCERTS) 10 µg/kg M (175) 24000 62 16 <10

Ortho-Xylene GC/MS (Head Space)(MCERTS) 10 µg/kg M (175) 3700 <10 <10 <10

Methyl tert-Butyl Ether GC/MS (Head Space)(MCERTS) 10 µg/kg M <10 <10 <10 <10

Total Petroleum Hydrocarbons (C5 - C6 aliphatic) GC/MS (Head Space)(MCERTS) 0.100 mg/kg N <0.100 <0.100 <0.100 <0.100

Total Petroleum Hydrocarbons (C6-C8 aliphatic) GC/MS (Head Space)(MCERTS) 0.10 mg/kg N 0.67 <0.10 <0.10 <0.10

Total Petroleum Hydrocarbons (C8-C10 aliphatic) GC/MS (Head Space)(MCERTS) 0.10 mg/kg N 27 <0.10 <0.10 <0.10

Total Petroleum Hydrocarbons (C10-C12 aliphatic) GCxGC 1 mg/kg M (13) 43 (13) <1 (13) <1 (13) <1



Total Petroleum Hydrocarbons (C21-C35 aliphatic) GCxGC 2 mg/kg M (13) 40 (13) <2 (13) 2 (13) 2

Total Petroleum Hydrocarbons (C35-C40 aliphatic) GCxGC 1 mg/kg N (13) 4 (13) <1 (13) <1 (13) <1

Total Petroleum Hydrocarbons (Aliphatic) total Calc mg/kg N (13) 130 (13) N.D. (13) 2.0 (13) 2.0

Total Petroleum Hydrocarbons (C6 - C7 aromatic) GC/MS (Head Space)(MCERTS) 0.10 mg/kg N <0.10 <0.10 <0.10 <0.10

Total Petroleum Hydrocarbons (C7-C8 aromatic) GC/MS (Head Space)(MCERTS) 0.10 mg/kg N <0.10 <0.10 <0.10 <0.10

Total Petroleum Hydrocarbons (C8-C10 aromatic) GC/MS (Head Space)(MCERTS) 0.10 mg/kg N 100 <0.10 <0.10 <0.10

Total Petroleum Hydrocarbons (C10-C12 aromatic) GCxGC 2 mg/kg M (13) 43 (13) <2 (13) <2 (13) <2

Total Petroleum Hydrocarbons (C12-C16 aromatic) GCxGC 1 mg/kg M (13) 20 (13) <1 (13) <1 (13) <1

Total Petroleum Hydrocarbons (C16-C21 aromatic) GCxGC 1 mg/kg M (13) 21 (13) <1 (13) 1 (13) 1

Total Petroleum Hydrocarbons (C21-C35 aromatic) GCxGC 1 mg/kg M (13) 25 (13) <1 (13) 4 (13) 2

Total Petroleum Hydrocarbons (C35-C40 aromatic) GCxGC 1 mg/kg N (13) <1 (13) <1 (13) <1 (13) <1

Total Petroleum Hydrocarbons (Aromatic) total Calc mg/kg N (13) 210 (13) N.D. (13) 5.0 (13) 3.0

Total Petroleum Hydrocarbons (Aliphatic+Aromatic) Calc mg/kg N (13) 340 (13) N.D. (13) 7.0 (13) 5.0



667902-1









Bottom Depth 1.80 2.50 2.00 0.50




Dichlorodifluoromethane GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50 <50

Chloromethane GC/MS (Head Space)(MCERTS) 50 µg/kg U <50 <50 <50 <50

Vinyl chloride monomer GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50 <50

Bromomethane GC/MS (Head Space)(MCERTS) 50 µg/kg U <50 <50 <50 <50

Chloroethane GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50 <50

Trichlorofluoromethane GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50 <50

1,1-Dichloroethylene GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50 <50

Dichloromethane GC/MS (Head Space)(MCERTS) 50 µg/kg U <50 <50 <50 <50

Trans-1,2-Dichloroethylene GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50 <50

1,1-Dichloroethane GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50 <50

Cis-1,2-Dichloroethylene GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50 <50

2,2-Dichloropropane GC/MS (Head Space)(MCERTS) 50 µg/kg U <50 <50 <50 <50

Chloroform GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50 <50

Bromochloromethane GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50 <50

1,1,1-Trichloroethane GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50 <50

1,1-Dichloropropene GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50 <50

Carbon tetrachloride GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50 <50

1,2-Dichloroethane GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50 <50

Benzene GC/MS (Head Space)(MCERTS) 10 µg/kg M <10 <10 <10 <10

1,2-Dichloropropane GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50 <50

Trichloroethylene GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50 <50

Bromodichloromethane GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50 <50

Dibromomethane GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50 <50

Cis-1,3-Dichloropropene GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50 <50

Toluene GC/MS (Head Space)(MCERTS) 10 µg/kg M 70 <10 <10 <10

Trans-1,3-Dichloropropene GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50 <50

1,1,2-Trichloroethane GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50 <50

1,3-Dichloropropane GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50 <50

Tetrachloroethylene GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50 <50

Chlorodibromomethane GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50 <50

1,2-dibromoethane GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50 <50

Chlorobenzene GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50 <50

1,1,1,2-Tetrachloroethane GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50 <50

EthylBenzene GC/MS (Head Space)(MCERTS) 10 µg/kg M (175) 12000 <10 <10 <10

Meta/Para-Xylene GC/MS (Head Space)(MCERTS) 10 µg/kg M (175) 24000 62 16 <10

Ortho-Xylene GC/MS (Head Space)(MCERTS) 10 µg/kg M (175) 3700 <10 <10 <10

Styrene GC/MS (Head Space)(MCERTS) 50 µg/kg U <50 <50 <50 <50

Bromoform GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50 <50

Isopropyl benzene GC/MS (Head Space)(MCERTS) 50 µg/kg M 1400 <50 <50 <50

1,1,2,2-Tetrachloroethane GC/MS (Head Space)(MCERTS) 50 µg/kg U <50 <50 <50 <50

1,2,3-Trichloropropane GC/MS (Head Space)(MCERTS) 50 µg/kg U <50 <50 <50 <50

n-Propylbenzene GC/MS (Head Space)(MCERTS) 50 µg/kg M (175) 5400 <50 <50 <50

Bromobenzene GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50 <50

1,3,5-Trimethylbenzene GC/MS (Head Space)(MCERTS) 50 µg/kg M (175) 8600 <50 <50 <50

Tert-Butylbenzene GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50 <50

1,2,4-Trimethylbenzene GC/MS (Head Space)(MCERTS) 50 µg/kg M (175) 18000 <50 <50 <50

Sec-Butylbenzene GC/MS (Head Space)(MCERTS) 50 µg/kg M 910 <50 <50 <50

p-Isopropyltoluene GC/MS (Head Space)(MCERTS) 50 µg/kg M 2600 <50 <50 <50

2-Chlorotoluene GC/MS (Head Space)(MCERTS) 50 µg/kg U <50 <50 <50 <50

4-Chlorotoluene GC/MS (Head Space)(MCERTS) 50 µg/kg U <50 <50 <50 <50

1,3-Dichlorobenzene GC/MS (Head Space)(MCERTS) 50 µg/kg M <50 <50 <50 <50





667902-1









Bottom Depth 1.80 2.50 2.00 0.50




Phenol GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1

Bis (2-chloroethyl) ether GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1

2-Chlorophenol GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1

1,3-Dichlorobenzene GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1



Bis (2-chloroisopropyl) ether GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1

2-methyl phenol GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1

3/4-Methylphenol GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1

Hexachloroethane GC/MS (MCERTS) 0.1 mg/kg U <0.1 <0.1 <0.1 <0.1

Nitrobenzene GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1

Isophorone GC/MS (MCERTS) 0.1 mg/kg U <0.1 <0.1 <0.1 <0.1

2-Nitrophenol GC/MS (MCERTS) 0.1 mg/kg U <0.1 <0.1 <0.1 <0.1

2,4-Dimethylphenol GC/MS (MCERTS) 0.1 mg/kg U <0.1 <0.1 <0.1 <0.1

Bis (2-chloroethoxy) methane GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1

2,4-Dichlorophenol GC/MS (MCERTS) 0.1 mg/kg U <0.1 <0.1 <0.1 <0.1

1,2,4-Trichlorobenzene GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1

4-Chloroaniline GC/MS (MCERTS) 0.1 mg/kg U (162) <0.5 (162) <0.5 (162) <0.5 (162) <0.5

Hexachlorobutadiene GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1

4-Chloro-3-methylphenol GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1

2-Methylnaphthalene GC/MS (MCERTS) 0.1 mg/kg M 0.4 <0.1 <0.1 <0.1

Hexachlorocyclopentadiene GC/MS (MCERTS) 0.1 mg/kg U (162) <0.5 (162) <0.5 (162) <0.5 (162) <0.5

2,4,6-Trichlorophenol GC/MS (MCERTS) 0.1 mg/kg U <0.1 <0.1 <0.1 <0.1

2,4,5-Trichlorophenol GC/MS (MCERTS) 0.1 mg/kg U <0.1 <0.1 <0.1 <0.1

2-Chloronaphthalene GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1

2-Nitroaniline GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1

Dimethyl phthalate GC/MS (MCERTS) 0.1 mg/kg U <0.1 <0.1 <0.1 <0.1

2,6-Dinitrotoluene GC/MS (MCERTS) 0.1 mg/kg U <0.1 <0.1 <0.1 <0.1

3-Nitroaniline GC/MS (MCERTS) 0.1 mg/kg U (162) <0.2 (162) <0.2 (162) <0.2 (162) <0.2

Dibenzofuran GC/MS (MCERTS) 0.1 mg/kg M 0.2 <0.1 <0.1 <0.1

2,4-Dinitrotoluene GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1

Diethyl phthalate GC/MS (MCERTS) 0.1 mg/kg U <0.1 <0.1 <0.1 <0.1

4-Chlorophenyl phenylether GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1

4-Nitroaniline GC/MS (MCERTS) 0.1 mg/kg U (162) <0.2 (162) <0.2 (162) <0.2 (162) <0.2

Azobenzene GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1

4-Bromophenyl phenylether GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1

Hexachlorobenzene GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1

Pentachlorophenol GC/MS (MCERTS) 0.1 mg/kg U <0.1 <0.1 <0.1 <0.1

Carbazole GC/MS (MCERTS) 0.1 mg/kg U 0.1 <0.1 <0.1 <0.1

Di-n-butylphthalate GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1

Butyl benzylphthalate GC/MS (MCERTS) 0.1 mg/kg U <0.1 <0.1 <0.1 <0.1

Bis (2-ethylhexyl)phthalate GC/MS (MCERTS) 0.1 mg/kg M 0.4 <0.1 <0.1 0.3

Di-n-octylphthalate GC/MS (MCERTS) 0.1 mg/kg M <0.1 <0.1 <0.1 <0.1



667902-1





Analysed as Water

Leachate Suite



Test Sample 10:1 10:1 10:1 10:1

Bottom Depth 1.80 2.50 2.00 0.50




Arsenic (Dissolved) ICP/MS (Filtered) 0.2 µg/l U 8.6 5.7 0.5 38

Boron (Dissolved) ICP/OES (Filtered) 0.01 mg/l N 0.63 0.81 0.03 0.05

Cadmium (Dissolved) ICP/MS (Filtered) 0.02 µg/l U 0.14 0.05 0.03 0.03

Chromium (Dissolved) ICP/MS (Filtered) 1 µg/l U <1 3 1 1

Copper (Dissolved) ICP/MS (Filtered) 0.5 µg/l U <0.5 6.7 0.7 1.1

Lead (Dissolved) ICP/MS (Filtered) 0.3 µg/l U 2.0 2.1 <0.3 <0.3

Mercury (Dissolved) ICP/MS (Filtered) 0.05 µg/l U 0.05 <0.05 <0.05 <0.05

Nickel (Dissolved) ICP/MS (Filtered) 1 µg/l U 5 5 <1 <1

Selenium (Dissolved) ICP/MS (Filtered) 0.5 µg/l U <0.5 0.8 0.6 0.6

Vanadium (Dissolved) ICP/MS (Filtered) 2 µg/l U 3 11 <2 <2

Zinc (Dissolved) ICP/MS (Filtered) 2 µg/l U 7 4 <2 3

Ammoniacal nitrogen Discrete Analyser 0.05 mg/l U 6.8 13 0.05 <0.05

Chloride Discrete Analyser 1 mg/l U 11 7 5 7

Cyanide (Total) Colorimetry 0.05 mg/l U <0.05 <0.05 <0.05 <0.05

Fluoride Discrete Analyser 0.05 mg/l U 1.2 1.7 0.92 0.31

Nitrate Discrete Analyser 0.5 mg/l U <0.5 <0.5 <0.5 1.3

Phosphate Discrete Analyser 0.5 mg/l U 3.8 4.0 3.2 3.1

Sulphate Discrete Analyser 0.5 mg/l U 54 25 7.0 8.4

Sulphide Colorimetry 0.05 mg/l N 0.08 0.08 0.08 0.08

Total Phenols GC/MS 0.5 µg/l U 54 (100) <2.5 <0.5 <0.5

Dissolved Organic Carbon OX/IR 1 mg/l N 28 18 6 5

Electrical Conductivity Probe 10 µS/cm N 520 340 150 130

pH Probe U 8.11 8.38 7.92 7.99



667902-1





Analysed as Water

PAH USEPA16



Test Sample 10:1 10:1 10:1 10:1

Bottom Depth 1.80 2.50 2.00 0.50




Naphthalene GC/MS (SIR) 0.01 µg/l U (NR) - (13,100) <0.05 (13,100) <0.05 (100,13) <0.05

Acenaphthylene GC/MS (SIR) 0.01 µg/l U (NR) - (13,100) <0.05 (13,100) <0.05 (100,13) <0.05

Acenaphthene GC/MS (SIR) 0.01 µg/l U (NR) - (100,13) <0.05 (100,13) <0.05 (100,13) <0.05

Fluorene GC/MS (SIR) 0.01 µg/l U (NR) - (100,13) <0.05 (100,13) <0.05 (100,13) <0.05

Phenanthrene GC/MS (SIR) 0.01 µg/l U (NR) - (100,13) <0.05 (100,13) <0.05 (100,13) <0.05

Anthracene GC/MS (SIR) 0.01 µg/l U (NR) - (13) 0.05 (13) 0.05 (100,13) <0.05

Fluoranthene GC/MS (SIR) 0.01 µg/l U (NR) - (13) 0.05 (13) 0.05 (13,100) <0.05

Pyrene GC/MS (SIR) 0.01 µg/l U (NR) - (13,100) <0.05 (13) 0.05 (13,100) <0.05

Benzo(a)Anthracene GC/MS (SIR) 0.01 µg/l U (NR) - (13) 0.05 (13) 0.05 (13) 0.05

Chrysene GC/MS (SIR) 0.01 µg/l U (NR) - (13) 0.05 (13) 0.05 (13) 0.05

Benzo(b)fluoranthene GC/MS (SIR) 0.01 µg/l U (NR) - (13) 0.05 (13) 0.05 (13) 0.05

Benzo(k)fluoranthene GC/MS (SIR) 0.01 µg/l U (NR) - (100,13) <0.05 (13) 0.05 (13) 0.05

Benzo(a)Pyrene GC/MS (SIR) 0.01 µg/l U (NR) - (100,13) <0.05 (13) 0.05 (13) 0.05

Indeno(123-cd)Pyrene GC/MS (SIR) 0.01 µg/l U (NR) - (100,13) <0.05 (13,100) <0.05 (13) 0.05

Dibenzo(ah)Anthracene GC/MS (SIR) 0.01 µg/l U (NR) - (13,100) <0.05 (13,100) <0.05 (100,13) <0.05

Benzo(ghi)Perylene GC/MS (SIR) 0.01 µg/l U (NR) - (100,13) <0.05 (13,100) <0.05 (13) 0.05

Polyaromatic Hydrocarbons (Total) GC/MS (SIR) 0.01 µg/l U (NR) - 0.25 0.40 0.35





Analysed as Water

PCB EC7



Test Sample 10:1 10:1 10:1 10:1

Bottom Depth 1.80 2.50 2.00 0.50




Polychlorinated biphenyl BZ#28 GC/MS (HR) 0.005 µg/l U (100) <0.010 (100) <0.010 (100) <0.010 (100) <0.010



Polychlorinated biphenyl BZ#118 GC/MS 0.005 µg/l U (100) <0.010 (100) <0.010 (100) <0.010 (100) <0.010






667902-1





Analysed as Water




Test Sample 10:1 10:1 10:1 10:1

Bottom Depth 1.80 2.50 2.00 0.50




Benzene GC/MS (Headspace) 1 µg/l U (13) 1 (13) <1 (13) <1 (13) <1

Toluene GC/MS (Headspace) 1 µg/l U (13) <1 (13) <1 (13) <1 (13) <1


Meta/Para-Xylene GC/MS (Headspace) 1 µg/l U 110 <1 <1 <1

Ortho-Xylene GC/MS (Headspace) 1 µg/l U 240 <1 <1 <1

Methyl tert-Butyl Ether GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1

Total Petroleum Hydrocarbons (C5 - C6 aliphatic) GC/MS (Headspace)(LV) 0.010 mg/l N <0.010 <0.010 <0.010 <0.010




Total Petroleum Hydrocarbons (C12-C16 aliphatic) GCxGC (LV) 0.01 mg/l N (100,13) <0.02 (13) 0.04 (13,100) <0.02 (100,13) <0.02

Total Petroleum Hydrocarbons (C16-C21 aliphatic) GCxGC (LV) 0.01 mg/l N (100,13) <0.02 (13) 0.05 (100,13) <0.02 (13,100) <0.02

Total Petroleum Hydrocarbons (C21-C35 aliphatic) GCxGC (LV) 0.01 mg/l N (13) 0.06 (13) 0.12 (13) 0.03 (13) 0.07

Total Petroleum Hydrocarbons (C6 - C7 aromatic) GC/MS (Headspace)(LV) 0.010 mg/l N <0.010 <0.010 <0.010 <0.010


Total Petroleum Hydrocarbons (C8-C10 aromatic) GC/MS (Headspace)(LV) 0.010 mg/l N 0.50 <0.010 <0.010 <0.010

Total Petroleum Hydrocarbons (C10-C12 aromatic) GCxGC (LV) 0.01 mg/l N (13) 0.22 (100,13) <0.04 (100,13) <0.02 (13,100) <0.02

Total Petroleum Hydrocarbons (C12-C16 aromatic) GCxGC (LV) 0.01 mg/l N (13) 0.26 (100,13) <0.04 (13) 0.02 (100,13) <0.02

Total Petroleum Hydrocarbons (C16-C21 aromatic) GCxGC (LV) 0.01 mg/l N (13,100) <0.02 (100,13) <0.04 (13) 0.03 (13) 0.03

Total Petroleum Hydrocarbons (C21-C35 aromatic) GCxGC (LV) 0.01 mg/l N (13) 0.03 (100,13) <0.04 (13) 0.02 (13) 0.02



667902-1





Analysed as Water




Test Sample 10:1 10:1 10:1 10:1

Bottom Depth 1.80 2.50 2.00 0.50




Dichlorodifluoromethane GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1

Chloromethane GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1

Vinyl chloride monomer GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1

Bromomethane GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1

Chloroethane GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1

Trichlorofluoromethane GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1

1,1-Dichloroethylene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1

Dichloromethane GC/MS (Headspace) 50 µg/l N <50 <50 <50 <50

Trans-1,2-Dichloroethylene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1


Cis-1,2-Dichloroethylene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1

2,2-Dichloropropane GC/MS (Headspace) 1 µg/l U (13) 1 (13) <1 (13) <1 (13) <1

Chloroform GC/MS (Headspace) 1 µg/l U (13) 33 (13) 49 (13) 38 (13) 45

Bromochloromethane GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1


1,1-Dichloropropene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1

Carbon tetrachloride GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1


Benzene GC/MS (Headspace) 1 µg/l U (13) 1 (13) <1 (13) <1 (13) <1


1,1,2-Trichloroethylene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1

Bromodichloromethane GC/MS (Headspace) 1 µg/l U (13) 2 (13) 5 (13) 4 (13) 5

Dibromomethane GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1

Cis-1,3-Dichloropropene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1

Toluene GC/MS (Headspace) 1 µg/l U (13) <1 (13) <1 (13) <1 (13) <1

Trans-1,3-Dichloropropene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1



Tetrachloroethylene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1

Chlorodibromomethane GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1

1,2-dibromoethane GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1

Chlorobenzene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1



Meta/Para-Xylene GC/MS (Headspace) 1 µg/l U 110 <1 <1 <1

Ortho-Xylene GC/MS (Headspace) 1 µg/l U 240 <1 <1 <1

Styrene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1

Bromoform GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1

Isopropyl benzene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1


1,2,3-Trichloropropane GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1

n-Propylbenzene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1

Bromobenzene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1

1,3,5-Trimethylbenzene GC/MS (Headspace) 1 µg/l U 27 <1 <1 <1

Tert-Butylbenzene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1


Sec-Butylbenzene GC/MS (Headspace) 1 µg/l U <1 <1 <1 <1

p-Isopropyltoluene GC/MS (Headspace) 1 µg/l U 4 <1 <1 <1








667902-1





Analysed as Water




Test Sample 10:1 10:1 10:1 10:1

Bottom Depth 1.80 2.50 2.00 0.50




Phenol GC/MS 10 µg/l U (100) <20 (100) <20 (100) <20 (100) <20

Bis (2-chloroethyl) ether GC/MS 10 µg/l U (100) <20 (100) <20 (100) <20 (100) <20

2-Chlorophenol GC/MS 10 µg/l U (100) <20 (100) <20 (100) <20 (100) <20

1,3-Dichlorobenzene GC/MS 10 µg/l U (100) <20 (100) <20 (100) <20 (100) <20



Bis (2-chloroisopropyl) ether GC/MS 10 µg/l U (100) <20 (100) <20 (100) <20 (100) <20

2-methyl phenol GC/MS 10 µg/l U (100) <20 (100) <20 (100) <20 (100) <20

3/4-Methylphenol GC/MS 10 µg/l U (100) <20 (100) <20 (100) <20 (100) <20

Hexachloroethane GC/MS 10 µg/l U (162) <40 (162) <40 (162) <40 (162) <40

Nitrobenzene GC/MS 10 µg/l U (100) <20 (100) <20 (100) <20 (100) <20

Isophorone GC/MS 10 µg/l U (100) <20 (100) <20 (100) <20 (100) <20

2-Nitrophenol GC/MS 10 µg/l U (100) <20 (100) <20 (100) <20 (100) <20

2,4-Dimethylphenol GC/MS 10 µg/l U (100) <20 (100) <20 (100) <20 (100) <20

Bis (2-chloroethoxy) methane GC/MS 10 µg/l U (100) <20 (100) <20 (100) <20 (100) <20

2,4-Dichlorophenol GC/MS 10 µg/l U (100) <20 (100) <20 (100) <20 (100) <20

1,2,4-Trichlorobenzene GC/MS 10 µg/l U (162) <40 (162) <40 (162) <40 (162) <40

4-Chloroaniline GC/MS 10 µg/l U (100) <20 (100) <20 (100) <20 (100) <20

Hexachlorobutadiene GC/MS 10 µg/l U (162) <80 (162) <80 (162) <80 (162) <80

4-Chloro-3-methylphenol GC/MS 10 µg/l U (100) <20 (100) <20 (100) <20 (100) <20

2-Methylnaphthalene GC/MS 10 µg/l U (100) <20 (100) <20 (100) <20 (100) <20

Hexachlorocyclopentadiene GC/MS 10 µg/l U (162) <80 (162) <80 (162) <80 (162) <80

2,4,6-Trichlorophenol GC/MS 10 µg/l U (100) <20 (100) <20 (100) <20 (100) <20

2,4,5-Trichlorophenol GC/MS 10 µg/l U (100) <20 (100) <20 (100) <20 (100) <20

2-Chloronaphthalene GC/MS 10 µg/l U (100) <20 (100) <20 (100) <20 (100) <20

2-Nitroaniline GC/MS 10 µg/l U (100) <20 (100) <20 (100) <20 (100) <20

Dimethyl phthalate GC/MS 10 µg/l U (100) <20 (100) <20 (100) <20 (100) <20

2,6-Dinitrotoluene GC/MS 10 µg/l U (100) <20 (100) <20 (100) <20 (100) <20


Dibenzofuran GC/MS 10 µg/l U (100) <20 (100) <20 (100) <20 (100) <20

2,4-Dinitrotoluene GC/MS 10 µg/l U (100) <20 (100) <20 (100) <20 (100) <20

Diethyl phthalate GC/MS 10 µg/l U (100) <20 (100) <20 (100) <20 (100) <20

4-Chlorophenyl phenylether GC/MS 10 µg/l U (100) <20 (100) <20 (100) <20 (100) <20


Azobenzene GC/MS 10 µg/l U (100) <20 (100) <20 (100) <20 (100) <20

4-Bromophenyl phenylether GC/MS 10 µg/l U (100) <20 (100) <20 (100) <20 (100) <20

Hexachlorobenzene GC/MS 10 µg/l U (100) <20 (100) <20 (100) <20 (100) <20

Pentachlorophenol GC/MS 10 µg/l U (162) <40 (162) <40 (162) <40 (162) <40

Carbazole GC/MS 10 µg/l U (100) <20 (100) <20 (100) <20 (100) <20

Di-n-butylphthalate GC/MS 10 µg/l U (100) <20 (100) <20 (100) <20 (100) <20

Butyl benzylphthalate GC/MS 10 µg/l U (100) <20 (100) <20 (100) <20 (100) <20

Bis (2-ethylhexyl)phthalate GC/MS 10 µg/l U (100) <20 (100) <20 (100) <20 (100) <20

Di-n-octylphthalate GC/MS 10 µg/l U (100) <20 (100) <20 (100) <20 (100) <20



667902-1


Notes





Analysed as Water


Concept Reference 667902 001

Customer Sample Reference BH05

Test Sample 10:1

Bottom Depth 1.80


Matrix Class Sandy Soil


Volume Vol 1 ml U -

Antimony (Dissolved) ICP/MS (Filtered) 1 µg/l U 11

Barium (Dissolved) ICP/MS (Filtered) 1 µg/l U 150

Molybdenum (Dissolved) ICP/MS (Filtered) 1 µg/l N 92

Phenols (Total-Mono) Colorimetry 0.1 mg/l U <0.1

Electrical Conductivity Probe 10 µS/cm N 520

Total Dissolved Solids Grav 100 mg/l N 310

Value Description


M40 Analysis conducted on sample assisted dried at no more than 40C. Results are reported on a dryweight basis.

10:1 S Data for BS EN 12457-2 (10:1)

M105 Analysis conducted on an "as received" aliquot. Results are reported on a dry weight basis wheremoisture content was determined by assisted drying of sample at 105C

AR As Received

10:1 Leachate to BS EN 12457-2 (10:1)

N.D. Not Detected



175 Results should be viewed with caution due to being outside of the instrument calibration range




NR No Result





These samples have been analysed exceeding recommended holding times. It is possible therefore that the results provided may be compromised.


Please note; The recoveries for PCB congeners 28 and 52 in samples 001 and 002 were <50% however the signal to noise is greater than 20:1, therefore the data are considered as valid.



667902-1




CornbrookManchester

M16 9FETel : 0161 874 2400Fax : 0161 874 2468






Date Job Received at Concept: 21-Jul-2017Date Analysis Started: 01-Aug-2017







Wales (No 2514788)

1549



Page 1 of 16

672474-1





MCERTS Preparation




Determinand Method TestSample LOD Units

Moisture @105C T162 AR 0.1 % 39

Retained on 10mm sieve T2 M40 0.1 % <0.1





Soil Suite





Arsenic T6 M40 2 mg/kg 64

Boron (water-soluble) T6 AR 1 mg/kg <1

Cadmium T6 M40 1 mg/kg 6

Chromium T6 M40 1 mg/kg 96

Copper T6 M40 1 mg/kg 190

Lead T6 M40 1 mg/kg 230

Nickel T6 M40 1 mg/kg 31

Mercury T6 M40 1 mg/kg 3

Selenium T6 M40 3 mg/kg <3

Vanadium T6 M40 1 mg/kg 33

Zinc T6 M40 1 mg/kg 1100

Cyanide(Total) T546 AR 1 mg/kg 18

SO4(Total) T6 A40 0.01 % 0.50

Sulphide T4 AR 10 mg/kg <10

Sulphur (total) T6 A40 0.01 % 0.20

Total Phenols T207 AR 0.1 mg/kg <0.1

Asbestos ID T27 AR N.D.

Total Organic Carbon T21 A40 0.1 % 2.4

pH T7 AR 7.2



672474-1





PAH USEPA16





Naphthalene T207 M105 0.1 mg/kg 0.6

Acenaphthylene T207 M105 0.1 mg/kg 0.4

Acenaphthene T207 M105 0.1 mg/kg 0.3

Fluorene T207 M105 0.1 mg/kg 0.2

Phenanthrene T207 M105 0.1 mg/kg 0.8

Anthracene T207 M105 0.1 mg/kg 0.4

Fluoranthene T207 M105 0.1 mg/kg 1.4

Pyrene T207 M105 0.1 mg/kg 1.2

Benzo(a)Anthracene T207 M105 0.1 mg/kg 0.8

Chrysene T207 M105 0.1 mg/kg 0.9

Benzo(b)fluoranthene T207 M105 0.1 mg/kg 0.9

Benzo(k)fluoranthene T207 M105 0.1 mg/kg 0.8

Benzo(a)Pyrene T207 M105 0.1 mg/kg 1.1

Indeno(123-cd)Pyrene T207 M105 0.1 mg/kg 0.8

Dibenzo(ah)Anthracene T207 M105 0.1 mg/kg 0.3

Benzo(ghi)Perylene T207 M105 0.1 mg/kg 0.9

PAH(total) T207 M105 0.1 mg/kg 12





PCB EC7





PCB BZ#28 T208 M105 0.05 µg/kg (26) <1.0

PCB BZ#52 T208 M105 0.05 µg/kg (26) 2.1

PCB BZ#101 T208 M105 0.05 µg/kg (26) <1.0

PCB BZ#118 T208 M105 0.05 µg/kg (26) <1.0

PCB BZ#138 T208 M105 0.05 µg/kg (26) <1.0

PCB BZ#153 T208 M105 0.05 µg/kg (26) <1.0

PCB BZ#180 T208 M105 0.05 µg/kg (26) <7.0



672474-1










Benzene T209 M105 10 µg/kg (13) <10

Toluene T209 M105 10 µg/kg <10

EthylBenzene T209 M105 10 µg/kg <10

M/P Xylene T209 M105 10 µg/kg <10

O Xylene T209 M105 10 µg/kg <10

Methyl tert-Butyl Ether T209 M105 10 µg/kg <10

TPH (C5-C6 aliphatic) T209 M105 100 µg/kg <100



TPH (C10-C12 aliphatic) T909 M105 1 mg/kg (13) <1

TPH (C12-C16 aliphatic) T909 M105 1 mg/kg (13) 5




TPH (Aliphatic) total T85 M105 mg/kg 32

TPH (C6-C7 aromatic) T209 M105 100 µg/kg <100



TPH (C10-C12 aromatic) T909 M105 2 mg/kg (13) <2

TPH (C12-C16 aromatic) T909 M105 1 mg/kg (13) 8



TPH (C35-C40 aromatic) T909 M105 1 mg/kg (13) <1

TPH (Aromatic) total T85 M105 mg/kg 100

TPH (Aliphatic+Aromatic) (sum) T85 M105 mg/kg 130



672474-1










Dichlorodifluoromethane T209 M105 50 µg/kg <50

Chloromethane T209 M105 50 µg/kg <50

Vinyl chloride T209 M105 50 µg/kg <50

Bromomethane T209 M105 50 µg/kg <50

Chloroethane T209 M105 50 µg/kg <50

Trichlorofluoromethane T209 M105 50 µg/kg <50

1,1-Dichloroethylene T209 M105 50 µg/kg <50

Dichloromethane T209 M105 50 µg/kg <50

Trans-1,2-Dichloroethene T209 M105 50 µg/kg <50

1,1-Dichloroethane T209 M105 50 µg/kg <50

Cis-1,2-Dichloroethylene T209 M105 50 µg/kg <50

2,2-Dichloropropane T209 M105 50 µg/kg <50

Chloroform T209 M105 50 µg/kg <50

Bromochloromethane T209 M105 50 µg/kg <50

1,1,1-Trichloroethane T209 M105 50 µg/kg <50

1,1-Dichloropropene T209 M105 50 µg/kg <50

Carbon tetrachloride T209 M105 50 µg/kg <50

1,2-Dichloroethane T209 M105 50 µg/kg <50

Benzene T209 M105 10 µg/kg (13) <10


Trichloroethene T209 M105 50 µg/kg <50

Bromodichloromethane T209 M105 50 µg/kg <50

Dibromomethane T209 M105 50 µg/kg <50

Cis-1,3-Dichloropropene T209 M105 50 µg/kg <50

Toluene T209 M105 10 µg/kg <10

Trans-1,3-Dichloropropene T209 M105 50 µg/kg <50

1,1,2-Trichloroethane T209 M105 50 µg/kg <50


Tetrachloroethene T209 M105 50 µg/kg <50

Chlorodibromomethane T209 M105 50 µg/kg <50

1,2-dibromoethane T209 M105 50 µg/kg <50

Chlorobenzene T209 M105 50 µg/kg <50

1,1,1,2-Tetrachloroethane T209 M105 50 µg/kg <50

EthylBenzene T209 M105 10 µg/kg <10

M/P Xylene T209 M105 10 µg/kg <10

O Xylene T209 M105 10 µg/kg <10

Styrene T209 M105 50 µg/kg <50

Bromoform T209 M105 50 µg/kg <50

Isopropyl benzene T209 M105 50 µg/kg <50

1,1,2,2-Tetrachloroethane T209 M105 50 µg/kg <50

1,2,3-Trichloropropane T209 M105 50 µg/kg <50

n-Propylbenzene T209 M105 50 µg/kg <50

Bromobenzene T209 M105 50 µg/kg <50

1,3,5-Trimethylbenzene T209 M105 50 µg/kg <50

T-Butylbenzene T209 M105 50 µg/kg <50

1,2,4-Trimethylbenzene T209 M105 50 µg/kg <50

S-Butylbenzene T209 M105 50 µg/kg <50

p-Isopropyltoluene T209 M105 50 µg/kg <50

2-Chlorotoluene T209 M105 50 µg/kg <50

4-Chlorotoluene T209 M105 50 µg/kg <50

1,3-Dichlorobenzene T209 M105 50 µg/kg <50





672474-1










Phenol T207 M105 0.1 mg/kg <0.1

Bis (2-chloroethyl) ether T207 M105 0.1 mg/kg <0.1

2-Chlorophenol T207 M105 0.1 mg/kg <0.1

1,3-Dichlorobenzene T207 M105 0.1 mg/kg <0.1

1,4-Dichlorobenzene T207 M105 0.1 mg/kg 0.2

1,2-Dichlorobenzene T207 M105 0.1 mg/kg <0.1

Bis (2-chloroisopropyl) ether T207 M105 0.1 mg/kg <0.1

2-methyl phenol T207 M105 0.1 mg/kg <0.1

3/4-Methylphenol T207 M105 0.1 mg/kg <0.1

Hexachloroethane T207 M105 0.1 mg/kg <0.1

Nitrobenzene T207 M105 0.1 mg/kg <0.1

Isophorone T207 M105 0.1 mg/kg <0.1

2-Nitrophenol T207 M105 0.1 mg/kg <0.1

2,4-Dimethylphenol T207 M105 0.1 mg/kg <0.1

Bis (2-chloroethoxy) methane T207 M105 0.1 mg/kg <0.1

2,4-Dichlorophenol T207 M105 0.1 mg/kg <0.1

1,2,4-Trichlorobenzene T207 M105 0.1 mg/kg <0.1

4-Chloroaniline T207 M105 0.1 mg/kg (162) <0.5

Hexachlorobutadiene T207 M105 0.1 mg/kg <0.1

4-Chloro-3-methylphenol T207 M105 0.1 mg/kg <0.1

2-Methylnaphthalene T207 M105 0.1 mg/kg 0.3

Hexachlorocyclopentadiene T207 M105 0.1 mg/kg (162) <0.5

2,4,6-Trichlorophenol T207 M105 0.1 mg/kg <0.1

2,4,5-Trichlorophenol T207 M105 0.1 mg/kg <0.1

2-Chloronaphthalene T207 M105 0.1 mg/kg <0.1

2-Nitroaniline T207 M105 0.1 mg/kg <0.1

Dimethyl phthalate T207 M105 0.1 mg/kg <0.1

2,6-Dinitrotoluene T207 M105 0.1 mg/kg <0.1


Dibenzofuran T207 M105 0.1 mg/kg 0.4

2,4-Dinitrotoluene T207 M105 0.1 mg/kg <0.1

Diethyl phthalate T207 M105 0.1 mg/kg <0.1

4-Chlorophenyl phenylether T207 M105 0.1 mg/kg <0.1


Azobenzene T207 M105 0.1 mg/kg <0.1

4-Bromophenyl phenylether T207 M105 0.1 mg/kg <0.1

Hexachlorobenzene T207 M105 0.1 mg/kg <0.1

Pentachlorophenol T207 M105 0.1 mg/kg <0.1

Carbazole T207 M105 0.1 mg/kg <0.1

Di-n-butylphthalate T207 M105 0.1 mg/kg <0.1

Butyl benzylphthalate T207 M105 0.1 mg/kg <0.1

Bis (2-ethylhexyl)phthalate T207 M105 0.1 mg/kg <0.1

Di-n-octylphthalate T207 M105 0.1 mg/kg <0.1



672474-1




Leachate to BS EN 12457-2 (10:1) Analysed as Water

Leachate Suite





As (Dissolved) T281 10:1 0.2 µg/l 3.0

B (Dissolved) T373 10:1 0.01 mg/l 0.06

Cd (Dissolved) T281 10:1 0.02 µg/l 1.0

Cr (Dissolved) T281 10:1 1 µg/l <1

Cu (Dissolved) T281 10:1 0.5 µg/l 12

Pb (Dissolved) T281 10:1 0.3 µg/l <0.3

Ni (Dissolved) T281 10:1 1 µg/l 5

Hg (Dissolved) T281 10:1 0.05 µg/l <0.05

Se (Dissolved) T281 10:1 0.5 µg/l <0.5

V (Dissolved) T281 10:1 2 µg/l <2

Zn (Dissolved) T281 10:1 2 µg/l 120

Ammoniacal nitrogen T686 10:1 0.05 mg/l 0.10

Chloride T686 10:1 1 mg/l 2

Cyanide(Total) T4 10:1 0.05 mg/l 0.06

Fluoride T686 10:1 0.05 mg/l 0.52

Nitrate T686 10:1 0.5 mg/l 0.6

Phosphate T686 10:1 0.5 mg/l 1.7

Sulphate T686 10:1 0.5 mg/l 360

Total Phenols T16 10:1 0.5 µg/l <0.5

Sulphide T4 10:1 0.05 mg/l 0.11

Dissolved Organic Carbon T21 10:1 1 mg/l 15

Electrical Conductivity T7 10:1 10 µS/cm 800

pH T7 10:1 7.99





PAH USEPA16





Naphthalene T149 10:1 0.01 µg/l (13) 0.01

Acenaphthylene T149 10:1 0.01 µg/l (13) 0.05

Acenaphthene T149 10:1 0.01 µg/l (13) 0.01

Fluorene T149 10:1 0.01 µg/l (13) <0.01

Phenanthrene T149 10:1 0.01 µg/l (13) <0.01

Anthracene T149 10:1 0.01 µg/l (13) 0.07

Fluoranthene T149 10:1 0.01 µg/l (13) <0.01

Pyrene T149 10:1 0.01 µg/l (13) <0.01

Benzo(a)Anthracene T149 10:1 0.01 µg/l (13) <0.01

Chrysene T149 10:1 0.01 µg/l (13) <0.01

Benzo(b)fluoranthene T149 10:1 0.01 µg/l (13) 0.01

Benzo(k)fluoranthene T149 10:1 0.01 µg/l (13) <0.01

Benzo(a)Pyrene T149 10:1 0.01 µg/l (13) 0.01

Indeno(123-cd)Pyrene T149 10:1 0.01 µg/l (13) 0.01

Dibenzo(ah)Anthracene T149 10:1 0.01 µg/l (13) <0.01

Benzo(ghi)Perylene T149 10:1 0.01 µg/l (13) 0.01

PAH(total) T149 10:1 0.01 µg/l 0.18



672474-1





PCB EC7





PCB BZ#28 T1 10:1 0.005 µg/l <0.005

PCB BZ#52 T1 10:1 0.005 µg/l <0.005

PCB BZ#101 T1 10:1 0.005 µg/l <0.005

PCB BZ#118 T16 10:1 0.005 µg/l <0.005

PCB BZ#138 T1 10:1 0.005 µg/l <0.005

PCB BZ#153 T1 10:1 0.005 µg/l <0.005

PCB BZ#180 T1 10:1 0.005 µg/l <0.005










Benzene T54 10:1 1 µg/l (13) <1

Toluene T54 10:1 1 µg/l <1

EthylBenzene T54 10:1 1 µg/l <1

M/P Xylene T54 10:1 1 µg/l <1

O Xylene T54 10:1 1 µg/l <1

Methyl tert-Butyl Ether T54 10:1 1 µg/l <1

TPH (C5-C6 aliphatic) T215 10:1 10 µg/l <10



TPH (C10-C12 aliphatic) T910 10:1 0.01 mg/l (13) <0.01



TPH (C21-C35 aliphatic) T910 10:1 0.01 mg/l (13) 0.02

TPH (C6-C7 aromatic) T215 10:1 10 µg/l <10



TPH (C10-C12 aromatic) T910 10:1 0.01 mg/l (13) <0.01



TPH (C21-C35 aromatic) T910 10:1 0.01 mg/l (13) 0.02



672474-1










Dichlorodifluoromethane T54 10:1 1 µg/l <1

Chloromethane T54 10:1 1 µg/l <1

Vinyl chloride T54 10:1 1 µg/l <1

Bromomethane T54 10:1 1 µg/l <1

Chloroethane T54 10:1 1 µg/l <1

Trichlorofluoromethane T54 10:1 1 µg/l <1

1,1-Dichloroethylene T54 10:1 1 µg/l <1

Dichloromethane T54 10:1 50 µg/l <50

Trans-1,2-Dichloroethene T54 10:1 1 µg/l <1

1,1-Dichloroethane T54 10:1 1 µg/l <1

Cis-1,2-Dichloroethylene T54 10:1 1 µg/l <1

2,2-Dichloropropane T54 10:1 1 µg/l <1

Chloroform T54 10:1 1 µg/l (13) 18

Bromochloromethane T54 10:1 1 µg/l <1

1,1,1-Trichloroethane T54 10:1 1 µg/l <1

1,1-Dichloropropene T54 10:1 1 µg/l <1

Carbon tetrachloride T54 10:1 1 µg/l <1

1,2-Dichloroethane T54 10:1 1 µg/l <1

Benzene T54 10:1 1 µg/l (13) <1


1,1,2-Trichloroethylene T54 10:1 1 µg/l <1

Bromodichloromethane T54 10:1 1 µg/l <1

Dibromomethane T54 10:1 1 µg/l <1

Cis-1,3-Dichloropropene T54 10:1 1 µg/l <1

Toluene T54 10:1 1 µg/l <1

Trans-1,3-Dichloropropene T54 10:1 1 µg/l <1

1,1,2-Trichloroethane T54 10:1 1 µg/l <1


Tetrachloroethene T54 10:1 1 µg/l <1

Chlorodibromomethane T54 10:1 1 µg/l <1

1,2-dibromoethane T54 10:1 1 µg/l <1

Chlorobenzene T54 10:1 1 µg/l <1

1,1,1,2-Tetrachloroethane T54 10:1 1 µg/l <1

EthylBenzene T54 10:1 1 µg/l <1

M/P Xylene T54 10:1 1 µg/l <1

O Xylene T54 10:1 1 µg/l <1

Styrene T54 10:1 1 µg/l <1

Bromoform T54 10:1 1 µg/l <1

Isopropyl benzene T54 10:1 1 µg/l <1

1,1,2,2-Tetrachloroethane T54 10:1 1 µg/l <1

1,2,3-Trichloropropane T54 10:1 1 µg/l <1

n-Propylbenzene T54 10:1 1 µg/l <1

Bromobenzene T54 10:1 1 µg/l <1

1,3,5-Trimethylbenzene T54 10:1 1 µg/l <1

T-Butylbenzene T54 10:1 1 µg/l <1

1,2,4-Trimethylbenzene T54 10:1 1 µg/l <1

S-Butylbenzene T54 10:1 1 µg/l <1

p-Isopropyltoluene T54 10:1 1 µg/l <1

2-Chlorotoluene T54 10:1 1 µg/l <1

4-Chlorotoluene T54 10:1 1 µg/l <1

1,3-Dichlorobenzene T54 10:1 1 µg/l <1





672474-1











Phenol T16 10:1 10 µg/l <10

Bis (2-chloroethyl) ether T16 10:1 10 µg/l <10

2-Chlorophenol T16 10:1 10 µg/l <10

1,3-Dichlorobenzene T16 10:1 10 µg/l (162) <20



Bis (2-chloroisopropyl) ether T16 10:1 10 µg/l <10

2-methyl phenol T16 10:1 10 µg/l <10

3/4-Methylphenol T16 10:1 10 µg/l <10

Hexachloroethane T16 10:1 10 µg/l (162) <20

Nitrobenzene T16 10:1 10 µg/l <10

Isophorone T16 10:1 10 µg/l <10

2-Nitrophenol T16 10:1 10 µg/l (162) <20

2,4-Dimethylphenol T16 10:1 10 µg/l <10

Bis (2-chloroethoxy) methane T16 10:1 10 µg/l <10

2,4-Dichlorophenol T16 10:1 10 µg/l <10

1,2,4-Trichlorobenzene T16 10:1 10 µg/l (162) <20

4-Chloroaniline T16 10:1 10 µg/l (162) <50

Hexachlorobutadiene T16 10:1 10 µg/l (162) <50

4-Chloro-3-methylphenol T16 10:1 10 µg/l <10

2-Methylnaphthalene T16 10:1 10 µg/l (162) <20

Hexachlorocyclopentadiene T16 10:1 10 µg/l (162) <50

2,4,6-Trichlorophenol T16 10:1 10 µg/l (162) <20

2,4,5-Trichlorophenol T16 10:1 10 µg/l (162) <20

2-Chloronaphthalene T16 10:1 10 µg/l <10

2-Nitroaniline T16 10:1 10 µg/l <10

Dimethyl phthalate T16 10:1 10 µg/l <10

2,6-Dinitrotoluene T16 10:1 10 µg/l <10

3-Nitroaniline T16 10:1 10 µg/l (162) <20

Dibenzofuran T16 10:1 10 µg/l <10

2,4-Dinitrotoluene T16 10:1 10 µg/l <10

Diethyl phthalate T16 10:1 10 µg/l <10

4-Chlorophenyl phenylether T16 10:1 10 µg/l <10

4-Nitroaniline T16 10:1 10 µg/l <10

Azobenzene T16 10:1 10 µg/l <10

4-Bromophenyl phenylether T16 10:1 10 µg/l <10

Hexachlorobenzene T16 10:1 10 µg/l <10

Pentachlorophenol T16 10:1 10 µg/l (162) <20

Carbazole T16 10:1 10 µg/l <10

Di-n-butylphthalate T16 10:1 10 µg/l <10

Butyl benzylphthalate T16 10:1 10 µg/l <10

Bis (2-ethylhexyl)phthalate T16 10:1 10 µg/l <10

Di-n-octylphthalate T16 10:1 10 µg/l <10

Value Description



AR As Received

10:1 Leachate to BS EN 12457-2 (10:1)


N.D. Not Detected







672474-1

Notes

Method Index

Accreditation Summary




These samples will be analysed exceeding recommended holding times. It is possible therefore that the results provided may be compromised.


Value Description

T281 ICP/MS (Filtered)

T6 ICP/OES

T207 GC/MS (MCERTS)

T2 Grav

T909 GCxGC

T4 Colorimetry

T7 Probe

T16 GC/MS

T54 GC/MS (Headspace)

T546 Colorimetry (CF)

T1 GC/MS (HR)

T85 Calc

T686 Discrete Analyser

T27 PLM

T209 GC/MS (Head Space)(MCERTS)

T373 ICP/OES (Filtered)

T162 Grav (1 Dec) (105 C)

T208 GC/MS (HR) (MCERTS)

T215 GC/MS (Headspace)(LV)

T21 OX/IR

T149 GC/MS (SIR)

T910 GCxGC (LV)

Determinand Method TestSample LOD Units Symbol Concept References

Moisture @105C T162 AR 0.1 % N 001

Retained on 10mm sieve T2 M40 0.1 % N 001

As (Dissolved) T281 10:1 0.2 µg/l U 002

B (Dissolved) T373 10:1 0.01 mg/l N 002

Cd (Dissolved) T281 10:1 0.02 µg/l U 002

Cr (Dissolved) T281 10:1 1 µg/l U 002

Cu (Dissolved) T281 10:1 0.5 µg/l U 002

Pb (Dissolved) T281 10:1 0.3 µg/l U 002

Ni (Dissolved) T281 10:1 1 µg/l U 002

Hg (Dissolved) T281 10:1 0.05 µg/l U 002

Se (Dissolved) T281 10:1 0.5 µg/l U 002

V (Dissolved) T281 10:1 2 µg/l U 002

Zn (Dissolved) T281 10:1 2 µg/l U 002

Ammoniacal nitrogen T686 10:1 0.05 mg/l U 002

Chloride T686 10:1 1 mg/l U 002

Cyanide(Total) T4 10:1 0.05 mg/l U 002

Fluoride T686 10:1 0.05 mg/l U 002

Nitrate T686 10:1 0.5 mg/l U 002

Phosphate T686 10:1 0.5 mg/l U 002

Sulphate T686 10:1 0.5 mg/l U 002

Sulphide T4 10:1 0.05 mg/l N 002

Total Phenols T16 10:1 0.5 µg/l U 002

Dissolved Organic Carbon T21 10:1 1 mg/l N 002

Electrical Conductivity T7 10:1 10 µS/cm N 002

pH T7 10:1 U 002

Naphthalene T149 10:1 0.01 µg/l U 002

Acenaphthylene T149 10:1 0.01 µg/l U 002

Acenaphthene T149 10:1 0.01 µg/l U 002

Fluorene T149 10:1 0.01 µg/l U 002

Phenanthrene T149 10:1 0.01 µg/l U 002



672474-1


Anthracene T149 10:1 0.01 µg/l U 002

Fluoranthene T149 10:1 0.01 µg/l U 002

Pyrene T149 10:1 0.01 µg/l U 002

Benzo(a)Anthracene T149 10:1 0.01 µg/l U 002

Chrysene T149 10:1 0.01 µg/l U 002

Benzo(b)fluoranthene T149 10:1 0.01 µg/l U 002

Benzo(k)fluoranthene T149 10:1 0.01 µg/l U 002

Benzo(a)Pyrene T149 10:1 0.01 µg/l U 002

Indeno(123-cd)Pyrene T149 10:1 0.01 µg/l U 002

Dibenzo(ah)Anthracene T149 10:1 0.01 µg/l U 002

Benzo(ghi)Perylene T149 10:1 0.01 µg/l U 002

PAH(total) T149 10:1 0.01 µg/l U 002

Phenol T16 10:1 10 µg/l U 002

Bis (2-chloroethyl) ether T16 10:1 10 µg/l U 002

2-Chlorophenol T16 10:1 10 µg/l U 002

1,3-Dichlorobenzene T16 10:1 10 µg/l U 002



Bis (2-chloroisopropyl) ether T16 10:1 10 µg/l U 002

2-methyl phenol T16 10:1 10 µg/l U 002

3/4-Methylphenol T16 10:1 10 µg/l U 002

Hexachloroethane T16 10:1 10 µg/l U 002

Nitrobenzene T16 10:1 10 µg/l U 002

Isophorone T16 10:1 10 µg/l U 002

2-Nitrophenol T16 10:1 10 µg/l U 002

2,4-Dimethylphenol T16 10:1 10 µg/l U 002

Bis (2-chloroethoxy) methane T16 10:1 10 µg/l U 002

2,4-Dichlorophenol T16 10:1 10 µg/l U 002

1,2,4-Trichlorobenzene T16 10:1 10 µg/l U 002

4-Chloroaniline T16 10:1 10 µg/l U 002

Hexachlorobutadiene T16 10:1 10 µg/l U 002

4-Chloro-3-methylphenol T16 10:1 10 µg/l U 002

2-Methylnaphthalene T16 10:1 10 µg/l U 002

Hexachlorocyclopentadiene T16 10:1 10 µg/l U 002

2,4,6-Trichlorophenol T16 10:1 10 µg/l U 002

2,4,5-Trichlorophenol T16 10:1 10 µg/l U 002

2-Chloronaphthalene T16 10:1 10 µg/l U 002

2-Nitroaniline T16 10:1 10 µg/l U 002

Dimethyl phthalate T16 10:1 10 µg/l U 002

2,6-Dinitrotoluene T16 10:1 10 µg/l U 002


Dibenzofuran T16 10:1 10 µg/l U 002

2,4-Dinitrotoluene T16 10:1 10 µg/l U 002

Diethyl phthalate T16 10:1 10 µg/l U 002

4-Chlorophenyl phenylether T16 10:1 10 µg/l U 002


Azobenzene T16 10:1 10 µg/l U 002

4-Bromophenyl phenylether T16 10:1 10 µg/l U 002

Hexachlorobenzene T16 10:1 10 µg/l U 002

Pentachlorophenol T16 10:1 10 µg/l U 002

Carbazole T16 10:1 10 µg/l U 002

Di-n-butylphthalate T16 10:1 10 µg/l U 002

Butyl benzylphthalate T16 10:1 10 µg/l U 002

Bis (2-ethylhexyl)phthalate T16 10:1 10 µg/l U 002

Di-n-octylphthalate T16 10:1 10 µg/l U 002

Dichlorodifluoromethane T54 10:1 1 µg/l U 002

Chloromethane T54 10:1 1 µg/l U 002

Vinyl chloride T54 10:1 1 µg/l U 002

Bromomethane T54 10:1 1 µg/l U 002

Chloroethane T54 10:1 1 µg/l U 002

Trichlorofluoromethane T54 10:1 1 µg/l U 002

1,1-Dichloroethylene T54 10:1 1 µg/l U 002

Dichloromethane T54 10:1 50 µg/l N 002

Trans-1,2-Dichloroethene T54 10:1 1 µg/l U 002

1,1-Dichloroethane T54 10:1 1 µg/l U 002

Cis-1,2-Dichloroethylene T54 10:1 1 µg/l U 002

2,2-Dichloropropane T54 10:1 1 µg/l U 002

Chloroform T54 10:1 1 µg/l U 002

Bromochloromethane T54 10:1 1 µg/l U 002

1,1,1-Trichloroethane T54 10:1 1 µg/l U 002



672474-1


1,1-Dichloropropene T54 10:1 1 µg/l U 002

Carbon tetrachloride T54 10:1 1 µg/l U 002

1,2-Dichloroethane T54 10:1 1 µg/l U 002

Benzene T54 10:1 1 µg/l U 002


1,1,2-Trichloroethylene T54 10:1 1 µg/l U 002

Bromodichloromethane T54 10:1 1 µg/l U 002

Dibromomethane T54 10:1 1 µg/l U 002

Cis-1,3-Dichloropropene T54 10:1 1 µg/l U 002

Toluene T54 10:1 1 µg/l U 002

Trans-1,3-Dichloropropene T54 10:1 1 µg/l U 002

1,1,2-Trichloroethane T54 10:1 1 µg/l U 002


Tetrachloroethene T54 10:1 1 µg/l U 002

Chlorodibromomethane T54 10:1 1 µg/l U 002

1,2-dibromoethane T54 10:1 1 µg/l U 002

Chlorobenzene T54 10:1 1 µg/l U 002

1,1,1,2-Tetrachloroethane T54 10:1 1 µg/l U 002

O Xylene T54 10:1 1 µg/l U 002

Styrene T54 10:1 1 µg/l U 002

Bromoform T54 10:1 1 µg/l U 002

Isopropyl benzene T54 10:1 1 µg/l U 002

1,1,2,2-Tetrachloroethane T54 10:1 1 µg/l U 002

1,2,3-Trichloropropane T54 10:1 1 µg/l U 002

n-Propylbenzene T54 10:1 1 µg/l U 002

Bromobenzene T54 10:1 1 µg/l U 002

1,3,5-Trimethylbenzene T54 10:1 1 µg/l U 002

T-Butylbenzene T54 10:1 1 µg/l U 002

1,2,4-Trimethylbenzene T54 10:1 1 µg/l U 002

S-Butylbenzene T54 10:1 1 µg/l U 002

p-Isopropyltoluene T54 10:1 1 µg/l U 002

2-Chlorotoluene T54 10:1 1 µg/l U 002

4-Chlorotoluene T54 10:1 1 µg/l U 002




PCB BZ#28 T1 10:1 0.005 µg/l U 002

PCB BZ#52 T1 10:1 0.005 µg/l U 002

PCB BZ#101 T1 10:1 0.005 µg/l U 002

PCB BZ#118 T16 10:1 0.005 µg/l U 002

PCB BZ#138 T1 10:1 0.005 µg/l U 002

PCB BZ#153 T1 10:1 0.005 µg/l U 002

PCB BZ#180 T1 10:1 0.005 µg/l U 002

EthylBenzene T54 10:1 1 µg/l U 002

M/P Xylene T54 10:1 1 µg/l U 002

Methyl tert-Butyl Ether T54 10:1 1 µg/l U 002

TPH (C5-C6 aliphatic) T215 10:1 10 µg/l N 002



TPH (C10-C12 aliphatic) T910 10:1 0.01 mg/l N 002




TPH (C6-C7 aromatic) T215 10:1 10 µg/l N 002



TPH (C10-C12 aromatic) T910 10:1 0.01 mg/l N 002




Arsenic T6 M40 2 mg/kg M 001

Boron (water-soluble) T6 AR 1 mg/kg N 001

Cadmium T6 M40 1 mg/kg M 001

Chromium T6 M40 1 mg/kg M 001

Copper T6 M40 1 mg/kg M 001

Lead T6 M40 1 mg/kg M 001

Nickel T6 M40 1 mg/kg M 001

Mercury T6 M40 1 mg/kg M 001

Selenium T6 M40 3 mg/kg M 001

Vanadium T6 M40 1 mg/kg M 001



672474-1


Zinc T6 M40 1 mg/kg M 001

Cyanide(Total) T546 AR 1 mg/kg M 001

SO4(Total) T6 A40 0.01 % N 001

Sulphide T4 AR 10 mg/kg N 001

Sulphur (total) T6 A40 0.01 % N 001

Total Phenols T207 AR 0.1 mg/kg N 001

Asbestos ID T27 AR SU 001

Total Organic Carbon T21 A40 0.1 % N 001

pH T7 AR M 001

PCB BZ#28 T208 M105 0.05 µg/kg M 001

PCB BZ#52 T208 M105 0.05 µg/kg M 001

PCB BZ#101 T208 M105 0.05 µg/kg M 001

PCB BZ#118 T208 M105 0.05 µg/kg M 001

PCB BZ#138 T208 M105 0.05 µg/kg M 001

PCB BZ#153 T208 M105 0.05 µg/kg M 001

PCB BZ#180 T208 M105 0.05 µg/kg M 001

EthylBenzene T209 M105 10 µg/kg M 001

M/P Xylene T209 M105 10 µg/kg M 001

Methyl tert-Butyl Ether T209 M105 10 µg/kg M 001

TPH (C5-C6 aliphatic) T209 M105 100 µg/kg N 001



TPH (C10-C12 aliphatic) T909 M105 1 mg/kg M 001




TPH (C35-C40 aliphatic) T909 M105 1 mg/kg N 001

TPH (Aliphatic) total T85 M105 mg/kg N 001

TPH (C6-C7 aromatic) T209 M105 100 µg/kg N 001



TPH (C10-C12 aromatic) T909 M105 2 mg/kg M 001




TPH (C35-C40 aromatic) T909 M105 1 mg/kg N 001

TPH (Aromatic) total T85 M105 mg/kg N 001

TPH (Aliphatic+Aromatic) (sum) T85 M105 mg/kg N 001

Naphthalene T207 M105 0.1 mg/kg M 001

Acenaphthylene T207 M105 0.1 mg/kg U 001

Acenaphthene T207 M105 0.1 mg/kg M 001

Fluorene T207 M105 0.1 mg/kg M 001

Phenanthrene T207 M105 0.1 mg/kg M 001

Anthracene T207 M105 0.1 mg/kg U 001

Fluoranthene T207 M105 0.1 mg/kg M 001

Pyrene T207 M105 0.1 mg/kg M 001

Benzo(a)Anthracene T207 M105 0.1 mg/kg M 001

Chrysene T207 M105 0.1 mg/kg M 001

Benzo(b)fluoranthene T207 M105 0.1 mg/kg M 001

Benzo(k)fluoranthene T207 M105 0.1 mg/kg M 001

Benzo(a)Pyrene T207 M105 0.1 mg/kg M 001

Indeno(123-cd)Pyrene T207 M105 0.1 mg/kg M 001

Dibenzo(ah)Anthracene T207 M105 0.1 mg/kg M 001

Benzo(ghi)Perylene T207 M105 0.1 mg/kg M 001

PAH(total) T207 M105 0.1 mg/kg U 001

Phenol T207 M105 0.1 mg/kg M 001

Bis (2-chloroethyl) ether T207 M105 0.1 mg/kg M 001

2-Chlorophenol T207 M105 0.1 mg/kg M 001

1,3-Dichlorobenzene T207 M105 0.1 mg/kg M 001



Bis (2-chloroisopropyl) ether T207 M105 0.1 mg/kg M 001

2-methyl phenol T207 M105 0.1 mg/kg M 001

3/4-Methylphenol T207 M105 0.1 mg/kg M 001

Hexachloroethane T207 M105 0.1 mg/kg U 001

Nitrobenzene T207 M105 0.1 mg/kg M 001

Isophorone T207 M105 0.1 mg/kg U 001

2-Nitrophenol T207 M105 0.1 mg/kg U 001

2,4-Dimethylphenol T207 M105 0.1 mg/kg U 001

Bis (2-chloroethoxy) methane T207 M105 0.1 mg/kg M 001



672474-1


2,4-Dichlorophenol T207 M105 0.1 mg/kg U 001

1,2,4-Trichlorobenzene T207 M105 0.1 mg/kg M 001

4-Chloroaniline T207 M105 0.1 mg/kg U 001

Hexachlorobutadiene T207 M105 0.1 mg/kg M 001

4-Chloro-3-methylphenol T207 M105 0.1 mg/kg M 001

2-Methylnaphthalene T207 M105 0.1 mg/kg M 001

Hexachlorocyclopentadiene T207 M105 0.1 mg/kg U 001

2,4,6-Trichlorophenol T207 M105 0.1 mg/kg U 001

2,4,5-Trichlorophenol T207 M105 0.1 mg/kg U 001

2-Chloronaphthalene T207 M105 0.1 mg/kg M 001

2-Nitroaniline T207 M105 0.1 mg/kg M 001

Dimethyl phthalate T207 M105 0.1 mg/kg U 001

2,6-Dinitrotoluene T207 M105 0.1 mg/kg U 001

3-Nitroaniline T207 M105 0.1 mg/kg U 001

Dibenzofuran T207 M105 0.1 mg/kg M 001

2,4-Dinitrotoluene T207 M105 0.1 mg/kg M 001

Diethyl phthalate T207 M105 0.1 mg/kg U 001

4-Chlorophenyl phenylether T207 M105 0.1 mg/kg M 001

4-Nitroaniline T207 M105 0.1 mg/kg U 001

Azobenzene T207 M105 0.1 mg/kg M 001

4-Bromophenyl phenylether T207 M105 0.1 mg/kg M 001

Hexachlorobenzene T207 M105 0.1 mg/kg M 001

Pentachlorophenol T207 M105 0.1 mg/kg U 001

Carbazole T207 M105 0.1 mg/kg U 001

Di-n-butylphthalate T207 M105 0.1 mg/kg M 001

Butyl benzylphthalate T207 M105 0.1 mg/kg U 001

Bis (2-ethylhexyl)phthalate T207 M105 0.1 mg/kg M 001

Di-n-octylphthalate T207 M105 0.1 mg/kg M 001

Dichlorodifluoromethane T209 M105 50 µg/kg M 001

Chloromethane T209 M105 50 µg/kg U 001

Vinyl chloride T209 M105 50 µg/kg M 001

Bromomethane T209 M105 50 µg/kg U 001

Chloroethane T209 M105 50 µg/kg M 001

Trichlorofluoromethane T209 M105 50 µg/kg M 001

1,1-Dichloroethylene T209 M105 50 µg/kg M 001

Dichloromethane T209 M105 50 µg/kg U 001

Trans-1,2-Dichloroethene T209 M105 50 µg/kg M 001

1,1-Dichloroethane T209 M105 50 µg/kg M 001

Cis-1,2-Dichloroethylene T209 M105 50 µg/kg M 001

2,2-Dichloropropane T209 M105 50 µg/kg U 001

Chloroform T209 M105 50 µg/kg M 001

Bromochloromethane T209 M105 50 µg/kg M 001

1,1,1-Trichloroethane T209 M105 50 µg/kg M 001

1,1-Dichloropropene T209 M105 50 µg/kg M 001

Carbon tetrachloride T209 M105 50 µg/kg M 001

1,2-Dichloroethane T209 M105 50 µg/kg M 001

Benzene T209 M105 10 µg/kg M 001

1,2-Dichloropropane T209 M105 50 µg/kg M 001

Trichloroethene T209 M105 50 µg/kg M 001

Bromodichloromethane T209 M105 50 µg/kg M 001

Dibromomethane T209 M105 50 µg/kg M 001

Cis-1,3-Dichloropropene T209 M105 50 µg/kg M 001

Toluene T209 M105 10 µg/kg M 001

Trans-1,3-Dichloropropene T209 M105 50 µg/kg M 001

1,1,2-Trichloroethane T209 M105 50 µg/kg M 001

1,3-Dichloropropane T209 M105 50 µg/kg M 001

Tetrachloroethene T209 M105 50 µg/kg M 001

Chlorodibromomethane T209 M105 50 µg/kg M 001

1,2-dibromoethane T209 M105 50 µg/kg M 001

Chlorobenzene T209 M105 50 µg/kg M 001

1,1,1,2-Tetrachloroethane T209 M105 50 µg/kg M 001

O Xylene T209 M105 10 µg/kg M 001

Styrene T209 M105 50 µg/kg U 001

Bromoform T209 M105 50 µg/kg M 001

Isopropyl benzene T209 M105 50 µg/kg M 001

1,1,2,2-Tetrachloroethane T209 M105 50 µg/kg U 001

1,2,3-Trichloropropane T209 M105 50 µg/kg U 001

n-Propylbenzene T209 M105 50 µg/kg M 001

Bromobenzene T209 M105 50 µg/kg M 001

1,3,5-Trimethylbenzene T209 M105 50 µg/kg M 001



672474-1


T-Butylbenzene T209 M105 50 µg/kg M 001

1,2,4-Trimethylbenzene T209 M105 50 µg/kg M 001

S-Butylbenzene T209 M105 50 µg/kg M 001

p-Isopropyltoluene T209 M105 50 µg/kg M 001

2-Chlorotoluene T209 M105 50 µg/kg U 001

4-Chlorotoluene T209 M105 50 µg/kg U 001

1,3-Dichlorobenzene T209 M105 50 µg/kg M 001





672474-1

Figure A4.2

Results of Chemical Tests – Groundwater




CornbrookManchester

M16 9FETel : 0161 874 2400Fax : 0161 874 2468


Date of Report: 07-Sep-2017




Date Job Received at Concept: 10-Aug-2017Date Analysis Started: 16-Aug-2017

Date Analysis Completed: 07-Sep-2017






Wales (No 2514788)

1549

Report checkedand authorised by :Stefan KondzielaCustomer Service Advisor

Issued by :Stefan KondzielaCustomer Service Advisor

Page 1 of 17

674893-1




Water Analysed as Water

Groundwater Suite


Customer Sample Reference BH5 BH4A BH3 BH6A BH7

Date Sampled 10-AUG-2017 10-AUG-2017 10-AUG-2017 10-AUG-2017 10-AUG-2017


As (Dissolved) T281 AR 0.2 µg/l 2.4 26 10 2.3 3.1

B (Dissolved) T373 AR 0.01 mg/l 2.9 0.13 0.09 0.16 0.40

Cd (Dissolved) T281 AR 0.02 µg/l <0.02 0.07 0.07 <0.02 0.05

Cr (Dissolved) T281 AR 1 µg/l 2 22 18 <1 1

Cu (Dissolved) T281 AR 0.5 µg/l 0.8 79 21 1.0 2.8

Pb (Dissolved) T281 AR 0.3 µg/l <0.3 1.4 <0.3 <0.3 <0.3

Hg (Dissolved) T281 AR 0.05 µg/l <0.05 0.06 <0.05 <0.05 <0.05

Ni (Dissolved) T281 AR 1 µg/l 6 20 25 8 11

Se (Dissolved) T281 AR 0.5 µg/l 0.8 42 14 1.7 62

V (Dissolved) T281 AR 2 µg/l <2 94 43 <2 <2

Zn (Dissolved) T281 AR 2 µg/l 18 5 4 5 58

Ammoniacal nitrogen T686 F 0.05 mg/l 34 1.8 0.79 0.18 23

Chloride T686 F 1 mg/l 150 38 27 76 130

Cyanide(Total) T4 AR 0.05 mg/l <0.05 <0.05 <0.05 <0.05 <0.05

Fluoride T686 F 0.05 mg/l 1.0 0.74 0.39 0.27 0.20

Methane T8 AR 0.04 mg/l <0.04 <0.04 <0.04 <0.04 <0.04

Nitrate T686 F 0.5 mg/l <0.5 <0.5 13 <0.5 <0.5

Phosphate T686 F 0.5 mg/l <0.5 <0.5 <0.5 <0.5 <0.5

Sulphate T686 F 0.5 mg/l 13 180 91 110 140

Sulphide T4 AR 0.05 mg/l <0.05 0.16 0.13 0.09 0.06

Total Phenols T16 AR 0.5 µg/l (13) 3.1 (13) 0.9 (13) 4.2 (13) 0.6 (13) 0.8

Electrical Conductivity T7 AR 10 µS/cm 2400 1700 1000 1400 2600

Total Organic Carbon T21 AR 1 mg/l 230 120 60 100 240

pH T7 AR 6.70 10.1 10.8 7.05 7.24





PAH USEPA16





Naphthalene T149 AR 0.01 µg/l (13) 0.30 (13) 0.14 (13) 0.09 (13) <0.01 (13) 0.01

Acenaphthylene T149 AR 0.01 µg/l 0.01 0.01 0.02 <0.01 0.02

Acenaphthene T149 AR 0.01 µg/l 0.22 0.06 0.02 0.01 0.01

Fluorene T149 AR 0.01 µg/l 0.10 0.06 0.03 0.01 0.01

Phenanthrene T149 AR 0.01 µg/l (13) 0.22 (13) 0.13 (13) 0.14 (13) 0.02 (13) 0.02

Anthracene T149 AR 0.01 µg/l 0.09 0.14 0.08 0.02 0.05

Fluoranthene T149 AR 0.01 µg/l 0.08 0.10 0.29 0.08 0.06

Pyrene T149 AR 0.01 µg/l 0.07 0.09 0.28 0.07 0.09

Benzo(a)Anthracene T149 AR 0.01 µg/l 0.02 0.02 0.12 0.01 0.02

Chrysene T149 AR 0.01 µg/l 0.02 0.04 0.15 0.02 0.03

Benzo(b)fluoranthene T149 AR 0.01 µg/l 0.01 0.01 0.12 0.01 0.02

Benzo(k)fluoranthene T149 AR 0.01 µg/l 0.01 0.01 0.13 0.01 0.02

Benzo(a)Pyrene T149 AR 0.01 µg/l 0.01 0.01 0.12 <0.01 0.01

Indeno(123-cd)Pyrene T149 AR 0.01 µg/l 0.01 0.01 0.08 <0.01 0.01

Dibenzo(ah)Anthracene T149 AR 0.01 µg/l <0.01 <0.01 0.02 <0.01 0.01

Benzo(ghi)Perylene T149 AR 0.01 µg/l 0.01 0.01 0.10 <0.01 0.01

PAH(total) T149 AR 0.01 µg/l 1.2 0.84 1.8 0.26 0.40



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PCB EC7





PCB BZ#28 T1 AR 0.005 µg/l 0.27 <0.005 <0.005 <0.005 <0.005

PCB BZ#52 T1 AR 0.005 µg/l 0.11 <0.005 <0.005 <0.005 <0.005

PCB BZ#101 T1 AR 0.005 µg/l (100) <0.050 <0.005 <0.005 <0.005 <0.005

PCB BZ#118 T16 AR 0.005 µg/l (100) <0.050 <0.005 <0.005 <0.005 <0.005

PCB BZ#138 T1 AR 0.005 µg/l (100) <0.050 <0.005 <0.005 <0.005 <0.005

PCB BZ#153 T1 AR 0.005 µg/l 0.074 <0.005 <0.005 <0.005 <0.005

PCB BZ#180 T1 AR 0.005 µg/l 0.071 <0.005 <0.005 <0.005 <0.005










Benzene T54 AR 1 µg/l (13) 4 (13) <1 (13) <1 (13) <1 (13) <1

Toluene T54 AR 1 µg/l 3 <1 <1 <1 <1

EthylBenzene T54 AR 1 µg/l 8 <1 <1 <1 <1

M/P Xylene T54 AR 1 µg/l 53 <1 <1 <1 <1

O Xylene T54 AR 1 µg/l 4 <1 <1 <1 <1

Methyl tert-Butyl Ether T54 AR 1 µg/l <1 <1 <1 <1 <1

TPH (C5-C6 aliphatic) T215 AR 10 µg/l <10 <10 <10 <10 <10



TPH (C10-C12 aliphatic) T910 AR 0.01 mg/l (13) <0.01 (13) <0.01 (13) <0.01 (13) <0.01 (13) <0.01

TPH (C12-C16 aliphatic) T910 AR 0.01 mg/l (13) <0.01 (13) 0.01 (13) <0.01 (13) <0.01 (13) <0.01

TPH (C16-C21 aliphatic) T910 AR 0.01 mg/l (13) <0.01 (13) 0.01 (13) 0.01 (13) <0.01 (13) 0.01

TPH (C21-C35 aliphatic) T910 AR 0.01 mg/l (13) 0.02 (13) 0.04 (13) 0.10 (13) <0.01 (13) 0.05

TPH (C6-C7 aromatic) T215 AR 10 µg/l <10 <10 <10 <10 <10

TPH (C7-C8 aromatic) T215 AR 10 µg/l <10 <10 <10 <10 <10

TPH (C8-C10 aromatic) T215 AR 10 µg/l 76 <10 <10 <10 <10

TPH (C10-C12 aromatic) T910 AR 0.01 mg/l (13) 0.02 (13) <0.01 (13) <0.01 (13) <0.01 (13) <0.01

TPH (C12-C16 aromatic) T910 AR 0.01 mg/l (13) 0.03 (13) <0.01 (13) 0.03 (13) <0.01 (13) 0.01

TPH (C16-C21 aromatic) T910 AR 0.01 mg/l (13) <0.01 (13) <0.01 (13) 0.05 (13) <0.01 (13) <0.01

TPH (C21-C35 aromatic) T910 AR 0.01 mg/l (13) 0.03 (13) <0.01 (13) 0.09 (13) <0.01 (13) <0.01



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Dichlorodifluoromethane T54 AR 1 µg/l <1 <1 <1 <1 <1

Chloromethane T54 AR 1 µg/l <1 <1 <1 <1 <1

Vinyl chloride T54 AR 1 µg/l <1 <1 <1 <1 <1

Bromomethane T54 AR 1 µg/l <1 <1 <1 <1 <1

Chloroethane T54 AR 1 µg/l <1 <1 <1 <1 <1

Trichlorofluoromethane T54 AR 1 µg/l <1 <1 <1 <1 <1

1,1-Dichloroethylene T54 AR 1 µg/l <1 <1 <1 <1 <1

Dichloromethane T54 AR 50 µg/l <50 <50 <50 <50 <50

Trans-1,2-Dichloroethene T54 AR 1 µg/l <1 <1 <1 <1 <1

1,1-Dichloroethane T54 AR 1 µg/l <1 <1 <1 <1 <1

Cis-1,2-Dichloroethylene T54 AR 1 µg/l <1 <1 <1 <1 <1

2,2-Dichloropropane T54 AR 1 µg/l <1 <1 <1 <1 <1

Chloroform T54 AR 1 µg/l <1 <1 <1 <1 2

Bromochloromethane T54 AR 1 µg/l <1 <1 <1 <1 <1

1,1,1-Trichloroethane T54 AR 1 µg/l <1 <1 <1 <1 <1

1,1-Dichloropropene T54 AR 1 µg/l <1 <1 <1 <1 <1

Carbon tetrachloride T54 AR 1 µg/l <1 <1 <1 <1 <1

1,2-Dichloroethane T54 AR 1 µg/l <1 <1 <1 <1 <1

Benzene T54 AR 1 µg/l (13) 4 (13) <1 (13) <1 (13) <1 (13) <1


1,1,2-Trichloroethylene T54 AR 1 µg/l <1 <1 <1 <1 <1

Bromodichloromethane T54 AR 1 µg/l <1 <1 <1 <1 <1

Dibromomethane T54 AR 1 µg/l <1 <1 <1 <1 <1

Cis-1,3-Dichloropropene T54 AR 1 µg/l <1 <1 <1 <1 <1

Toluene T54 AR 1 µg/l 3 <1 <1 <1 <1

Trans-1,3-Dichloropropene T54 AR 1 µg/l <1 <1 <1 <1 <1

1,1,2-Trichloroethane T54 AR 1 µg/l <1 <1 <1 <1 <1


Tetrachloroethene T54 AR 1 µg/l <1 <1 <1 <1 <1

Chlorodibromomethane T54 AR 1 µg/l <1 <1 <1 <1 <1

1,2-dibromoethane T54 AR 1 µg/l <1 <1 <1 <1 <1

Chlorobenzene T54 AR 1 µg/l 48 <1 <1 <1 <1

1,1,1,2-Tetrachloroethane T54 AR 1 µg/l <1 <1 <1 <1 <1

EthylBenzene T54 AR 1 µg/l 8 <1 <1 <1 <1

M/P Xylene T54 AR 1 µg/l 53 <1 <1 <1 <1

O Xylene T54 AR 1 µg/l 4 <1 <1 <1 <1

Styrene T54 AR 1 µg/l <1 <1 <1 <1 <1

Bromoform T54 AR 1 µg/l <1 <1 <1 <1 <1

Isopropyl benzene T54 AR 1 µg/l 2 <1 <1 <1 <1

1,1,2,2-Tetrachloroethane T54 AR 1 µg/l <1 <1 <1 <1 <1

1,2,3-Trichloropropane T54 AR 1 µg/l <1 <1 <1 <1 <1

n-Propylbenzene T54 AR 1 µg/l 1 <1 <1 <1 <1

Bromobenzene T54 AR 1 µg/l <1 <1 <1 <1 <1

1,3,5-Trimethylbenzene T54 AR 1 µg/l <1 <1 <1 <1 <1

T-Butylbenzene T54 AR 1 µg/l <1 <1 <1 <1 <1

1,2,4-Trimethylbenzene T54 AR 1 µg/l 5 <1 <1 <1 <1

S-Butylbenzene T54 AR 1 µg/l <1 <1 <1 <1 <1

p-Isopropyltoluene T54 AR 1 µg/l <1 <1 <1 <1 <1

2-Chlorotoluene T54 AR 1 µg/l <1 <1 <1 <1 <1

4-Chlorotoluene T54 AR 1 µg/l <1 <1 <1 <1 <1

1,3-Dichlorobenzene T54 AR 1 µg/l <1 <1 <1 <1 <1





674893-1










Phenol T16 AR 10 µg/l <10 <10 <10 <10 <10

Bis (2-chloroethyl) ether T16 AR 10 µg/l <10 <10 <10 <10 <10

2-Chlorophenol T16 AR 10 µg/l <10 <10 <10 <10 <10

1,3-Dichlorobenzene T16 AR 10 µg/l (162) <20 (162) <20 (162) <20 (162) <20 (162) <20

1,4-Dichlorobenzene T16 AR 10 µg/l (162) <20 (162) <20 (162) <20 (162) <20 (162) <20


Bis (2-chloroisopropyl) ether T16 AR 10 µg/l <10 <10 <10 <10 <10

2-methyl phenol T16 AR 10 µg/l <10 <10 <10 <10 <10

3/4-Methylphenol T16 AR 10 µg/l <10 <10 <10 <10 <10

Hexachloroethane T16 AR 10 µg/l (162) <20 (162) <20 (162) <20 (162) <20 (162) <20

Nitrobenzene T16 AR 10 µg/l <10 <10 <10 <10 <10

Isophorone T16 AR 10 µg/l <10 <10 <10 <10 <10

2-Nitrophenol T16 AR 10 µg/l <10 <10 <10 <10 <10

2,4-Dimethylphenol T16 AR 10 µg/l <10 <10 <10 <10 <10

Bis (2-chloroethoxy) methane T16 AR 10 µg/l <10 <10 <10 <10 <10

2,4-Dichlorophenol T16 AR 10 µg/l <10 <10 <10 <10 <10

1,2,4-Trichlorobenzene T16 AR 10 µg/l (162) <20 (162) <20 (162) <20 (162) <20 (162) <20

4-Chloroaniline T16 AR 10 µg/l <10 <10 <10 <10 <10

Hexachlorobutadiene T16 AR 10 µg/l (162) <50 (162) <50 (162) <50 (162) <50 (162) <50

4-Chloro-3-methylphenol T16 AR 10 µg/l <10 <10 <10 <10 <10

2-Methylnaphthalene T16 AR 10 µg/l (162) <20 (162) <20 (162) <20 (162) <20 (162) <20

Hexachlorocyclopentadiene T16 AR 10 µg/l (162) <50 (162) <50 (162) <50 (162) <50 (162) <50

2,4,6-Trichlorophenol T16 AR 10 µg/l <10 <10 <10 <10 <10

2,4,5-Trichlorophenol T16 AR 10 µg/l <10 <10 <10 <10 <10

2-Chloronaphthalene T16 AR 10 µg/l <10 <10 <10 <10 <10

2-Nitroaniline T16 AR 10 µg/l <10 <10 <10 <10 <10

Dimethyl phthalate T16 AR 10 µg/l <10 <10 <10 <10 <10

2,6-Dinitrotoluene T16 AR 10 µg/l <10 <10 <10 <10 <10


Dibenzofuran T16 AR 10 µg/l <10 <10 <10 <10 <10

2,4-Dinitrotoluene T16 AR 10 µg/l <10 <10 <10 <10 <10

Diethyl phthalate T16 AR 10 µg/l <10 <10 <10 <10 <10

4-Chlorophenyl phenylether T16 AR 10 µg/l <10 <10 <10 <10 <10


Azobenzene T16 AR 10 µg/l <10 <10 <10 <10 <10

4-Bromophenyl phenylether T16 AR 10 µg/l <10 <10 <10 <10 <10

Hexachlorobenzene T16 AR 10 µg/l <10 <10 <10 <10 <10

Pentachlorophenol T16 AR 10 µg/l <10 <10 <10 <10 <10

Carbazole T16 AR 10 µg/l <10 <10 <10 <10 <10

Di-n-butylphthalate T16 AR 10 µg/l <10 <10 <10 <10 <10

Butyl benzylphthalate T16 AR 10 µg/l <10 <10 <10 <10 <10

Bis (2-ethylhexyl)phthalate T16 AR 10 µg/l <10 <10 <10 <10 <10

Di-n-octylphthalate T16 AR 10 µg/l <10 <10 <10 <10 <10



674893-1





MRPS by GC (CSOPP611)


Customer Sample Reference BH5 BH7

Date Sampled 10-AUG-2017 10-AUG-2017


2,4,6-Trichlorophenol T826 AR 0.1 µg/l <0.1 <0.1

2-Phenylphenol T826 AR 0.1 µg/l <0.1 <0.1

Acetochlor T826 AR 0.1 µg/l <0.1 <0.1

Aclonifen T826 AR 0.1 µg/l <0.1 <0.1

Acrinathrin T826 AR 0.1 µg/l <0.1 <0.1

Alachlor T826 AR 0.1 µg/l <0.1 <0.1

Aldrin T826 AR 0.1 µg/l <0.1 <0.1

Ametryn T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Atraton T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Atrazine T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Azaconazole T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Azobenzene T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Azoxystrobin T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Benalaxyl T826 AR 0.1 µg/l <0.1 <0.1

Benfluralin T826 AR 0.1 µg/l <0.1 <0.1

Bifenox T826 AR 0.1 µg/l <0.1 <0.1

Bifenthrin T826 AR 0.1 µg/l <0.1 <0.1

Binapacryl T826 AR 0.1 µg/l <0.1 <0.1

Biphenyl T826 AR 0.1 µg/l <10 <10

Bitertanol T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Boscalid T826 AR 0.1 µg/l <0.1 <0.1

Bromacil T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Bromophos T826 AR 0.1 µg/l <0.1 <0.1

Bromophos-Ethyl T826 AR 0.1 µg/l <0.1 <0.1

Bromopropylate T826 AR 0.1 µg/l <0.1 <0.1

Bupirimate T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Buprofezine T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Butachlor T826 AR 0.1 µg/l <0.1 <0.1

Cadusafos T826 AR 0.1 µg/l <0.1 <0.1

Carbaryl T826 AR 0.1 µg/l <0.1 <0.1

Carbophenothion T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Carboxine T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Carfentrazone Ethyl T826 AR 0.1 µg/l <0.1 <0.1

Chlorbenzilate T826 AR 0.1 µg/l <0.1 <0.1

Chlordane T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Chlordimeform T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Chlorethoxyfos T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Chlorfenapyr T826 AR 0.1 µg/l <0.1 <0.1

Chlorfenvinphos T826 AR 0.1 µg/l <0.1 <0.1

Chlormephos T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Chloropropylate T826 AR 0.1 µg/l <0.1 <0.1

Chlorothalonil T826 AR 0.1 µg/l <0.1 <0.1

Chlorpropham T826 AR 0.1 µg/l <0.1 <0.1

Chlorpyrifos T826 AR 0.1 µg/l <0.1 <0.1

Chlorpyrifos methyl T826 AR 0.1 µg/l <0.1 <0.1

Chlorthal Dimethyl T826 AR 0.1 µg/l <0.1 <0.1

Chlorthion T826 AR 0.1 µg/l <0.1 <0.1

Chlorthiophos T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Chlozolinate T826 AR 0.1 µg/l <0.1 <0.1

Clodinafop propargy T826 AR 0.1 µg/l <0.1 <0.1

Clomazone T826 AR 0.1 µg/l <0.1 <0.1

Cloquintocet mexyl T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Coumaphos T826 AR 0.1 µg/l <0.1 <0.1

Cyflufenamid T826 AR 0.1 µg/l <0.1 <0.1

Cyfluthrin T826 AR 0.1 µg/l <0.1 <0.1

Cypermethrin T826 AR 0.1 µg/l <0.1 <0.1

Cyphenothrin T826 AR 0.1 µg/l <0.1 <0.1

Cyproconazole T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Cyprodinil T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Deltamethrin T826 AR 0.1 µg/l <0.1 <0.1



674893-1










Desmetryn T826 AR 0.1 µg/l <0.1 <0.1

Diafenthiuron T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Dialifos T826 AR 0.1 µg/l <0.1 <0.1

Diazinon T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Dichlobenil T826 AR 0.1 µg/l <0.1 <0.1

Dichlofenthion T826 AR 0.1 µg/l <0.1 <0.1

Dichlorvos T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Diclobutrazol T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Dicloran T826 AR 0.1 µg/l <0.1 <0.1

Dicofol T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Dieldrin T826 AR 0.1 µg/l <0.1 <0.1

Difenoconazole T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Diflufenican T826 AR 0.1 µg/l <0.1 <0.1

Dimethenamid T826 AR 0.1 µg/l <0.1 <0.1

Dimethomorph T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Dimoxystrobin T826 AR 0.1 µg/l <0.1 <0.1

Dioxabenzofos T826 AR 0.1 µg/l <0.1 <0.1

Diphenamid T826 AR 0.1 µg/l <0.1 <0.1

Diphenylamine T826 AR 0.1 µg/l <0.1 <0.1

Disulfoton T826 AR 0.1 µg/l <0.1 <0.1

Ditalimfos T826 AR 0.1 µg/l <0.1 <0.1

Edifenphos T826 AR 0.1 µg/l <0.1 <0.1

Endosulphan alpha T826 AR 0.1 µg/l <0.1 <0.1

Endosulphan beta T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Endosulphan sulphate T826 AR 0.1 µg/l <0.1 <0.1

Endrin T826 AR 0.1 µg/l <0.1 <0.1

Epn T826 AR 0.1 µg/l <0.1 <0.1

Epoxiconazole T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

EPTC T826 AR 0.1 µg/l <0.1 <0.1

Etaconazole T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Ethion T826 AR 0.1 µg/l <0.1 <0.1

Ethofumesate T826 AR 0.1 µg/l <0.1 <0.1

Ethoprophos T826 AR 0.1 µg/l <0.1 <0.1

Ethoxyquin T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Etofenprox T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Etoxazole T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Etridiazole T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Etrimfos T826 AR 0.1 µg/l <0.1 <0.1

Famoxadone T826 AR 0.1 µg/l <0.1 <0.1

Famphur T826 AR 0.1 µg/l <0.1 <0.1

Fenamidone T826 AR 0.1 µg/l <0.1 <0.1

Fenamiphos T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Fenarimol T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Fenbuconazole T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Fenchlorphos T826 AR 0.1 µg/l <0.1 <0.1

Fenitrothion T826 AR 0.1 µg/l <0.1 <0.1

Fenpiclonil T826 AR 0.1 µg/l <0.1 <0.1

Fenpropathrin T826 AR 0.1 µg/l <0.1 <0.1

Fenpropimorph T826 AR 0.1 µg/l <0.1 <0.1

Fenson T826 AR 0.1 µg/l <0.1 <0.1

Fensulfothion T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Fenthion T826 AR 0.1 µg/l <0.1 <0.1

Fenvalerate T826 AR 0.1 µg/l <0.1 <0.1

Fipronil T826 AR 0.1 µg/l <0.1 <0.1

Fipronil sulphone T826 AR 0.1 µg/l <0.1 <0.1

Flamprop isopropyl T826 AR 0.1 µg/l <0.1 <0.1

Fluazifop-P-Butyl T826 AR 0.1 µg/l <0.1 <0.1

Flucythrinate T826 AR 0.1 µg/l <0.1 <0.1

Fludioxonil T826 AR 0.1 µg/l <0.1 <0.1

Flufenacet T826 AR 0.1 µg/l <0.1 <0.1



674893-1










Flumetralin T826 AR 0.1 µg/l <0.1 <0.1

Flumioxazin T826 AR 0.1 µg/l <0.1 <0.1

Flumorph T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Fluopyram T826 AR 0.1 µg/l <0.1 <0.1

Fluquinconazole T826 AR 0.1 µg/l <0.1 <0.1

Fluroxypyr-1-methylheptyl ester T826 AR 0.1 µg/l <0.1 <0.1

Flusilazole T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Flutolanil T826 AR 0.1 µg/l <0.1 <0.1

Fluxapyroxad T826 AR 0.1 µg/l <0.1 <0.1

Fonophos T826 AR 0.1 µg/l <0.1 <0.1

Formothion T826 AR 0.1 µg/l <0.1 <0.1

Furalaxyl T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Haloxyfop etotyl T826 AR 0.1 µg/l <0.1 <0.1

Haloxyfop Methyl T826 AR 0.1 µg/l <0.1 <0.1

Heptachlor T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Heptachlor epoxide T826 AR 0.1 µg/l <0.1 <0.1

Heptachlor exo Epoxide T826 AR 0.1 µg/l <0.1 <0.1

Heptenophos T826 AR 0.1 µg/l <0.1 <0.1

Hexachlorobenzene T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Hexachlorocyclohexane (alpha) T826 AR 0.1 µg/l <0.1 <0.1

Hexachlorocyclohexane (beta) T826 AR 0.1 µg/l <0.1 <0.1

Hexachlorocyclohexane (delta) T826 AR 0.1 µg/l <0.1 <0.1

Hexaconazole T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Hexazinone T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Iodofenphos T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Iprodione T826 AR 0.1 µg/l <0.1 <0.1

Isazofos T826 AR 0.1 µg/l <0.1 <0.1

Isocarbophos T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Isodrin T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Isofenphos T826 AR 0.1 µg/l <0.1 <0.1

Isofenphos Methyl T826 AR 0.1 µg/l <0.1 <0.1

Isomethiozin T826 AR 0.1 µg/l <0.1 <0.1

Isoprothiolane T826 AR 0.1 µg/l <0.1 <0.1

Isopyrazam T826 AR 0.1 µg/l <0.1 <0.1

Kresoxim Methyl T826 AR 0.1 µg/l <0.1 <0.1

Lambda Cyhalothrin T826 AR 0.1 µg/l <0.1 <0.1

Lenacil T826 AR 0.1 µg/l <0.1 <0.1

Leptophos T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Lindane T826 AR 0.1 µg/l <0.1 <0.1

Malathion T826 AR 0.1 µg/l <0.1 <0.1

MCPA-thioethyl T826 AR 0.1 µg/l <0.1 <0.1

Mecarbam T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Mepanipyrim T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Mephosfolan T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Mepronil T826 AR 0.1 µg/l <0.1 <0.1

Metalaxyl T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Metazachlor T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Methacrifos T826 AR 0.1 µg/l <0.1 <0.1

Methidathion T826 AR 0.1 µg/l <0.1 <0.1

Methoxychlor T826 AR 0.1 µg/l <0.1 <0.1

Methyl Paraoxon T826 AR 0.1 µg/l <0.1 <0.1

Metolachlor T826 AR 0.1 µg/l <0.1 <0.1

Metolcarb T826 AR 0.1 µg/l <0.1 <0.1

Metrafenone T826 AR 0.1 µg/l <0.1 <0.1

Metribuzin T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Mevinphos T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Mirex T826 AR 0.1 µg/l <0.1 <0.1

Molinate T826 AR 0.1 µg/l <0.1 <0.1

Myclobutanil T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Napropamide T826 AR 0.1 µg/l <0.1 <0.1



674893-1










Nitrofen T826 AR 0.1 µg/l <0.1 <0.1

Nitrothal isopropyl T826 AR 0.1 µg/l <0.1 <0.1

Nuarimol T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

o,p'-DDT T826 AR 0.1 µg/l <0.1 <0.1

o,p-DDD T826 AR 0.1 µg/l <0.1 <0.1

o,p-DDE T826 AR 0.1 µg/l <0.1 <0.1

Octylisothiazolon T826 AR 0.1 µg/l <0.1 <0.1

Ofurace T826 AR 0.1 µg/l <0.1 <0.1

Orysastrobin T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Oxadiazon T826 AR 0.1 µg/l <0.1 <0.1

Oxadixyl T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Oxyfluorfen T826 AR 0.1 µg/l <0.1 <0.1

p,p-DDD T826 AR 0.1 µg/l <0.1 <0.1

p,p-DDE T826 AR 0.1 µg/l <0.1 <0.1

p,p-DDT T826 AR 0.1 µg/l <0.1 <0.1

Paclobutrazol T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Paraoxon T826 AR 0.1 µg/l <0.1 <0.1

Parathion T826 AR 0.1 µg/l <0.1 <0.1

Parathion methyl T826 AR 0.1 µg/l <0.1 <0.1

Penconazole T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Pendimethalin T826 AR 0.1 µg/l <0.1 <0.1

Pentachloroaniline T826 AR 0.1 µg/l <0.1 <0.1

Pentachlorophenol T826 AR 0.1 µg/l <0.1 <0.1

Pentanochlor T826 AR 0.1 µg/l <0.1 <0.1

Permethrin T826 AR 0.1 µg/l <0.1 <0.1

Pethoxamid T826 AR 0.1 µg/l <0.1 <0.1

Phenothrin T826 AR 0.1 µg/l <0.1 <0.1

Phenthoate T826 AR 0.1 µg/l <0.1 <0.1

Phorate T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Phosalone T826 AR 0.1 µg/l <0.1 <0.1

Phosfolan T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Picoxystrobin T826 AR 0.1 µg/l <0.1 <0.1

Piperonyl Butoxide T826 AR 0.1 µg/l <0.1 <0.1

Pirimicarb T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Pirimiphos Ethyl T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Pirimiphos methyl T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Pretilachlor T826 AR 0.1 µg/l <0.1 <0.1

Procymidone T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Profenofos T826 AR 0.1 µg/l <0.1 <0.1

Prometon T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Prometryn T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Propachlor T826 AR 0.1 µg/l <0.1 <0.1

Propanil T826 AR 0.1 µg/l <0.1 <0.1

Propaphos T826 AR 0.1 µg/l <0.1 <0.1

Propargite T826 AR 0.1 µg/l <0.1 <0.1

Propazine T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Propetamphos T826 AR 0.1 µg/l <0.1 <0.1

Propham T826 AR 0.1 µg/l <0.1 <0.1

Propiconazole T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Propyzamide T826 AR 0.1 µg/l <0.1 <0.1

Proquinazid T826 AR 0.1 µg/l <0.1 <0.1

Prosulfocarb T826 AR 0.1 µg/l <0.1 <0.1

Prothiofos T826 AR 0.1 µg/l <0.1 <0.1

Pyraclostrobin T826 AR 0.1 µg/l <0.1 <0.1

Pyraflufen ethyl T826 AR 0.1 µg/l <0.1 <0.1

Pyrazophos T826 AR 0.1 µg/l <0.1 <0.1

Pyridaben T826 AR 0.1 µg/l <0.1 <0.1

Pyridaphenthion T826 AR 0.1 µg/l <0.1 <0.1

Pyrimethanil T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Pyriproxyfen T826 AR 0.1 µg/l (278) <0.1 (278) <0.1



674893-1










Quinalphos T826 AR 0.1 µg/l <0.1 <0.1

Quinoxyfen T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Quintozene T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Quizalofop-ethyl T826 AR 0.1 µg/l <0.1 <0.1

Secbumeton T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Silafluofen T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Simazine T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Simeconazole T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Sulfallate T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Sulprofos T826 AR 0.1 µg/l <0.1 <0.1

Tebuconazole T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Tebufenpyrad T826 AR 0.1 µg/l <0.1 <0.1

Tebupirimiphos T826 AR 0.1 µg/l <0.1 <0.1

Tecnazene T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Tefluthrin T826 AR 0.1 µg/l <0.1 <0.1

Terbacil T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Terbufos T826 AR 0.1 µg/l <0.1 <0.1

Terbumeton T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Terbuthylazine T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Terbutryn T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Tetrachlorvinphos T826 AR 0.1 µg/l <0.1 <0.1

Tetraconazole T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Tetradifon T826 AR 0.1 µg/l <0.1 <0.1

sulfotep T826 AR 0.1 µg/l <0.1 <0.1

Tetramethrin T826 AR 0.1 µg/l <0.1 <0.1

Tetrasul T826 AR 0.1 µg/l <0.1 <0.1

Thiamethoxam T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Thiobencarb T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Tolclofos methyl T826 AR 0.1 µg/l <0.1 <0.1

Triadimefon T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Triadimenol T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Triallate T826 AR 0.1 µg/l <0.1 <0.1

Triazamate T826 AR 0.1 µg/l <0.1 <0.1

Triazophos T826 AR 0.1 µg/l <0.1 <0.1

Trifloxystrobin T826 AR 0.1 µg/l <0.1 <0.1

Triflumizole T826 AR 0.1 µg/l (278) <0.1 (278) <0.1

Trifluralin T826 AR 0.1 µg/l <0.1 <0.1

Vinclozolin T826 AR 0.1 µg/l <0.1 <0.1

Vinclozolin metabolite 3,5-Dichloroaniline T826 AR 0.1 µg/l <0.1 <0.1





Pesticide Suite





Bentazone T310 AR 0.1 µg/l <0.1 <0.1

Diuron T569 AR 0.1 µg/l <0.1 <0.1

Isoproturon T569 AR 0.1 µg/l <0.1 <0.1

Linuron T569 AR 0.1 µg/l <0.1 <0.1

Mecoprop T16 AR 0.1 µg/l <0.1 <0.1



674893-1


Method Index


Value Description

F Filtered

AR As Received



278 Data reported is qualitative as recovery is outside the 60 to 140% range




Value Description

T21 OX/IR

T910 GCxGC (LV)

T1 GC/MS (HR)

T569 LC MS MS 1L


T8 GC/FID

T16 GC/MS

T7 Probe

T149 GC/MS (SIR)

T310 LC/MS/MS

T826 SOP611 (GC MSMS)

T4 Colorimetry






As (Dissolved) T281 AR 0.2 µg/l U 001-005

B (Dissolved) T373 AR 0.01 mg/l N 001-005

Cd (Dissolved) T281 AR 0.02 µg/l U 001-005

Cr (Dissolved) T281 AR 1 µg/l U 001-005

Cu (Dissolved) T281 AR 0.5 µg/l U 001-005

Pb (Dissolved) T281 AR 0.3 µg/l U 001-005

Hg (Dissolved) T281 AR 0.05 µg/l U 001-005

Ni (Dissolved) T281 AR 1 µg/l U 001-005

Se (Dissolved) T281 AR 0.5 µg/l U 001-005

V (Dissolved) T281 AR 2 µg/l U 001-005

Zn (Dissolved) T281 AR 2 µg/l U 001-005

Ammoniacal nitrogen T686 F 0.05 mg/l U 001-005

Chloride T686 F 1 mg/l U 001-005

Cyanide(Total) T4 AR 0.05 mg/l U 001-005

Fluoride T686 F 0.05 mg/l U 001-005

Methane T8 AR 0.04 mg/l N 001-005

Nitrate T686 F 0.5 mg/l U 001-005

Phosphate T686 F 0.5 mg/l U 001-005

Sulphate T686 F 0.5 mg/l U 001-005

Sulphide T4 AR 0.05 mg/l N 001-005

Total Phenols T16 AR 0.5 µg/l U 001-005

Electrical Conductivity T7 AR 10 µS/cm N 001-005

Total Organic Carbon T21 AR 1 mg/l U 001-005

pH T7 AR U 001-005

Naphthalene T149 AR 0.01 µg/l U 001-005

Acenaphthylene T149 AR 0.01 µg/l U 001-005

Acenaphthene T149 AR 0.01 µg/l U 001-005

Fluorene T149 AR 0.01 µg/l U 001-005

Phenanthrene T149 AR 0.01 µg/l U 001-005

Anthracene T149 AR 0.01 µg/l U 001-005

Fluoranthene T149 AR 0.01 µg/l U 001-005

Pyrene T149 AR 0.01 µg/l U 001-005

Benzo(a)Anthracene T149 AR 0.01 µg/l U 001-005



674893-1


Chrysene T149 AR 0.01 µg/l U 001-005

Benzo(b)fluoranthene T149 AR 0.01 µg/l U 001-005

Benzo(k)fluoranthene T149 AR 0.01 µg/l U 001-005

Benzo(a)Pyrene T149 AR 0.01 µg/l U 001-005

Indeno(123-cd)Pyrene T149 AR 0.01 µg/l U 001-005

Dibenzo(ah)Anthracene T149 AR 0.01 µg/l U 001-005

Benzo(ghi)Perylene T149 AR 0.01 µg/l U 001-005

PAH(total) T149 AR 0.01 µg/l U 001-005

Phenol T16 AR 10 µg/l U 001-005

Bis (2-chloroethyl) ether T16 AR 10 µg/l U 001-005

2-Chlorophenol T16 AR 10 µg/l U 001-005

1,3-Dichlorobenzene T16 AR 10 µg/l U 001-005



Bis (2-chloroisopropyl) ether T16 AR 10 µg/l U 001-005

2-methyl phenol T16 AR 10 µg/l U 001-005

3/4-Methylphenol T16 AR 10 µg/l U 001-005

Hexachloroethane T16 AR 10 µg/l U 001-005

Nitrobenzene T16 AR 10 µg/l U 001-005

Isophorone T16 AR 10 µg/l U 001-005

2-Nitrophenol T16 AR 10 µg/l U 001-005

2,4-Dimethylphenol T16 AR 10 µg/l U 001-005

Bis (2-chloroethoxy) methane T16 AR 10 µg/l U 001-005

2,4-Dichlorophenol T16 AR 10 µg/l U 001-005

1,2,4-Trichlorobenzene T16 AR 10 µg/l U 001-005

4-Chloroaniline T16 AR 10 µg/l U 001-005

Hexachlorobutadiene T16 AR 10 µg/l U 001-005

4-Chloro-3-methylphenol T16 AR 10 µg/l U 001-005

2-Methylnaphthalene T16 AR 10 µg/l U 001-005

Hexachlorocyclopentadiene T16 AR 10 µg/l U 001-005

2,4,6-Trichlorophenol T16 AR 10 µg/l U 001-005

2,4,5-Trichlorophenol T16 AR 10 µg/l U 001-005

2-Chloronaphthalene T16 AR 10 µg/l U 001-005

2-Nitroaniline T16 AR 10 µg/l U 001-005

Dimethyl phthalate T16 AR 10 µg/l U 001-005

2,6-Dinitrotoluene T16 AR 10 µg/l U 001-005


Dibenzofuran T16 AR 10 µg/l U 001-005

2,4-Dinitrotoluene T16 AR 10 µg/l U 001-005

Diethyl phthalate T16 AR 10 µg/l U 001-005

4-Chlorophenyl phenylether T16 AR 10 µg/l U 001-005


Azobenzene T16 AR 10 µg/l U 001-005

4-Bromophenyl phenylether T16 AR 10 µg/l U 001-005

Hexachlorobenzene T16 AR 10 µg/l U 001-005

Pentachlorophenol T16 AR 10 µg/l U 001-005

Carbazole T16 AR 10 µg/l U 001-005

Di-n-butylphthalate T16 AR 10 µg/l U 001-005

Butyl benzylphthalate T16 AR 10 µg/l U 001-005

Bis (2-ethylhexyl)phthalate T16 AR 10 µg/l U 001-005

Di-n-octylphthalate T16 AR 10 µg/l U 001-005

Dichlorodifluoromethane T54 AR 1 µg/l U 001-005

Chloromethane T54 AR 1 µg/l U 001-005

Vinyl chloride T54 AR 1 µg/l U 001-005

Bromomethane T54 AR 1 µg/l U 001-005

Chloroethane T54 AR 1 µg/l U 001-005

Trichlorofluoromethane T54 AR 1 µg/l U 001-005

1,1-Dichloroethylene T54 AR 1 µg/l U 001-005

Dichloromethane T54 AR 50 µg/l N 001-005

Trans-1,2-Dichloroethene T54 AR 1 µg/l U 001-005

1,1-Dichloroethane T54 AR 1 µg/l U 001-005

Cis-1,2-Dichloroethylene T54 AR 1 µg/l U 001-005

2,2-Dichloropropane T54 AR 1 µg/l U 001-005

Chloroform T54 AR 1 µg/l U 001-005

Bromochloromethane T54 AR 1 µg/l U 001-005

1,1,1-Trichloroethane T54 AR 1 µg/l U 001-005

1,1-Dichloropropene T54 AR 1 µg/l U 001-005

Carbon tetrachloride T54 AR 1 µg/l U 001-005

1,2-Dichloroethane T54 AR 1 µg/l U 001-005

Benzene T54 AR 1 µg/l U 001-005



674893-1



1,1,2-Trichloroethylene T54 AR 1 µg/l U 001-005

Bromodichloromethane T54 AR 1 µg/l U 001-005

Dibromomethane T54 AR 1 µg/l U 001-005

Cis-1,3-Dichloropropene T54 AR 1 µg/l U 001-005

Trans-1,3-Dichloropropene T54 AR 1 µg/l U 001-005

1,1,2-Trichloroethane T54 AR 1 µg/l U 001-005


Tetrachloroethene T54 AR 1 µg/l U 001-005

Chlorodibromomethane T54 AR 1 µg/l U 001-005

1,2-dibromoethane T54 AR 1 µg/l U 001-005

Chlorobenzene T54 AR 1 µg/l U 001-005

1,1,1,2-Tetrachloroethane T54 AR 1 µg/l U 001-005

M/P Xylene T54 AR 1 µg/l U 001-005

Styrene T54 AR 1 µg/l U 001-005

Bromoform T54 AR 1 µg/l U 001-005

Isopropyl benzene T54 AR 1 µg/l U 001-005

1,1,2,2-Tetrachloroethane T54 AR 1 µg/l U 001-005

1,2,3-Trichloropropane T54 AR 1 µg/l U 001-005

n-Propylbenzene T54 AR 1 µg/l U 001-005

Bromobenzene T54 AR 1 µg/l U 001-005

1,3,5-Trimethylbenzene T54 AR 1 µg/l U 001-005

T-Butylbenzene T54 AR 1 µg/l U 001-005

1,2,4-Trimethylbenzene T54 AR 1 µg/l U 001-005

S-Butylbenzene T54 AR 1 µg/l U 001-005

p-Isopropyltoluene T54 AR 1 µg/l U 001-005

2-Chlorotoluene T54 AR 1 µg/l U 001-005

4-Chlorotoluene T54 AR 1 µg/l U 001-005




PCB BZ#28 T1 AR 0.005 µg/l U 001-005

PCB BZ#52 T1 AR 0.005 µg/l U 001-005

PCB BZ#101 T1 AR 0.005 µg/l U 001-005

PCB BZ#118 T16 AR 0.005 µg/l U 001-005

PCB BZ#138 T1 AR 0.005 µg/l U 001-005

PCB BZ#153 T1 AR 0.005 µg/l U 001-005

PCB BZ#180 T1 AR 0.005 µg/l U 001-005

Toluene T54 AR 1 µg/l U 001-005

EthylBenzene T54 AR 1 µg/l U 001-005

O Xylene T54 AR 1 µg/l U 001-005

Methyl tert-Butyl Ether T54 AR 1 µg/l U 001-005

TPH (C5-C6 aliphatic) T215 AR 10 µg/l N 001-005



TPH (C10-C12 aliphatic) T910 AR 0.01 mg/l N 001-005




TPH (C6-C7 aromatic) T215 AR 10 µg/l N 001-005



TPH (C10-C12 aromatic) T910 AR 0.01 mg/l N 001-005




Bentazone T310 AR 0.1 µg/l N 001,005

Diuron T569 AR 0.1 µg/l N 001,005

Isoproturon T569 AR 0.1 µg/l N 001,005

Linuron T569 AR 0.1 µg/l N 001,005

Mecoprop T16 AR 0.1 µg/l N 001,005

2,4,6-Trichlorophenol T826 AR 0.1 µg/l N 001,005

2-Phenylphenol T826 AR 0.1 µg/l N 001,005

Acetochlor T826 AR 0.1 µg/l N 001,005

Aclonifen T826 AR 0.1 µg/l N 001,005

Acrinathrin T826 AR 0.1 µg/l N 001,005

Alachlor T826 AR 0.1 µg/l N 001,005

Aldrin T826 AR 0.1 µg/l N 001,005

Ametryn T826 AR 0.1 µg/l N 001,005

Atraton T826 AR 0.1 µg/l N 001,005



674893-1


Atrazine T826 AR 0.1 µg/l N 001,005

Azaconazole T826 AR 0.1 µg/l N 001,005

Azobenzene T826 AR 0.1 µg/l N 001,005

Azoxystrobin T826 AR 0.1 µg/l N 001,005

Benalaxyl T826 AR 0.1 µg/l N 001,005

Benfluralin T826 AR 0.1 µg/l N 001,005

Bifenox T826 AR 0.1 µg/l N 001,005

Bifenthrin T826 AR 0.1 µg/l N 001,005

Binapacryl T826 AR 0.1 µg/l N 001,005

Biphenyl T826 AR 0.1 µg/l N 001,005

Bitertanol T826 AR 0.1 µg/l N 001,005

Boscalid T826 AR 0.1 µg/l N 001,005

Bromacil T826 AR 0.1 µg/l N 001,005

Bromophos T826 AR 0.1 µg/l N 001,005

Bromophos-Ethyl T826 AR 0.1 µg/l N 001,005

Bromopropylate T826 AR 0.1 µg/l N 001,005

Bupirimate T826 AR 0.1 µg/l N 001,005

Buprofezine T826 AR 0.1 µg/l N 001,005

Butachlor T826 AR 0.1 µg/l N 001,005

Cadusafos T826 AR 0.1 µg/l N 001,005

Carbaryl T826 AR 0.1 µg/l N 001,005

Carbophenothion T826 AR 0.1 µg/l N 001,005

Carboxine T826 AR 0.1 µg/l N 001,005

Carfentrazone Ethyl T826 AR 0.1 µg/l N 001,005

Chlorbenzilate T826 AR 0.1 µg/l N 001,005

Chlordane T826 AR 0.1 µg/l N 001,005

Chlordimeform T826 AR 0.1 µg/l N 001,005

Chlorethoxyfos T826 AR 0.1 µg/l N 001,005

Chlorfenapyr T826 AR 0.1 µg/l N 001,005

Chlorfenvinphos T826 AR 0.1 µg/l N 001,005

Chlormephos T826 AR 0.1 µg/l N 001,005

Chloropropylate T826 AR 0.1 µg/l N 001,005

Chlorothalonil T826 AR 0.1 µg/l N 001,005

Chlorpropham T826 AR 0.1 µg/l N 001,005

Chlorpyrifos T826 AR 0.1 µg/l N 001,005

Chlorpyrifos methyl T826 AR 0.1 µg/l N 001,005

Chlorthal Dimethyl T826 AR 0.1 µg/l N 001,005

Chlorthion T826 AR 0.1 µg/l N 001,005

Chlorthiophos T826 AR 0.1 µg/l N 001,005

Chlozolinate T826 AR 0.1 µg/l N 001,005

Clodinafop propargy T826 AR 0.1 µg/l N 001,005

Clomazone T826 AR 0.1 µg/l N 001,005

Cloquintocet mexyl T826 AR 0.1 µg/l N 001,005

Coumaphos T826 AR 0.1 µg/l N 001,005

Cyflufenamid T826 AR 0.1 µg/l N 001,005

Cyfluthrin T826 AR 0.1 µg/l N 001,005

Cypermethrin T826 AR 0.1 µg/l N 001,005

Cyphenothrin T826 AR 0.1 µg/l N 001,005

Cyproconazole T826 AR 0.1 µg/l N 001,005

Cyprodinil T826 AR 0.1 µg/l N 001,005

Deltamethrin T826 AR 0.1 µg/l N 001,005

Desmetryn T826 AR 0.1 µg/l N 001,005

Diafenthiuron T826 AR 0.1 µg/l N 001,005

Dialifos T826 AR 0.1 µg/l N 001,005

Diazinon T826 AR 0.1 µg/l N 001,005

Dichlobenil T826 AR 0.1 µg/l N 001,005

Dichlofenthion T826 AR 0.1 µg/l N 001,005

Dichlorvos T826 AR 0.1 µg/l N 001,005

Diclobutrazol T826 AR 0.1 µg/l N 001,005

Dicloran T826 AR 0.1 µg/l N 001,005

Dicofol T826 AR 0.1 µg/l N 001,005

Dieldrin T826 AR 0.1 µg/l N 001,005

Difenoconazole T826 AR 0.1 µg/l N 001,005

Diflufenican T826 AR 0.1 µg/l N 001,005

Dimethenamid T826 AR 0.1 µg/l N 001,005

Dimethomorph T826 AR 0.1 µg/l N 001,005

Dimoxystrobin T826 AR 0.1 µg/l N 001,005

Dioxabenzofos T826 AR 0.1 µg/l N 001,005

Diphenamid T826 AR 0.1 µg/l N 001,005

Diphenylamine T826 AR 0.1 µg/l N 001,005



674893-1


Disulfoton T826 AR 0.1 µg/l N 001,005

Ditalimfos T826 AR 0.1 µg/l N 001,005

Edifenphos T826 AR 0.1 µg/l N 001,005

Endosulphan alpha T826 AR 0.1 µg/l N 001,005

Endosulphan beta T826 AR 0.1 µg/l N 001,005

Endosulphan sulphate T826 AR 0.1 µg/l N 001,005

Endrin T826 AR 0.1 µg/l N 001,005

Epn T826 AR 0.1 µg/l N 001,005

Epoxiconazole T826 AR 0.1 µg/l N 001,005

EPTC T826 AR 0.1 µg/l N 001,005

Etaconazole T826 AR 0.1 µg/l N 001,005

Ethion T826 AR 0.1 µg/l N 001,005

Ethofumesate T826 AR 0.1 µg/l N 001,005

Ethoprophos T826 AR 0.1 µg/l N 001,005

Ethoxyquin T826 AR 0.1 µg/l N 001,005

Etofenprox T826 AR 0.1 µg/l N 001,005

Etoxazole T826 AR 0.1 µg/l N 001,005

Etridiazole T826 AR 0.1 µg/l N 001,005

Etrimfos T826 AR 0.1 µg/l N 001,005

Famoxadone T826 AR 0.1 µg/l N 001,005

Famphur T826 AR 0.1 µg/l N 001,005

Fenamidone T826 AR 0.1 µg/l N 001,005

Fenamiphos T826 AR 0.1 µg/l N 001,005

Fenarimol T826 AR 0.1 µg/l N 001,005

Fenbuconazole T826 AR 0.1 µg/l N 001,005

Fenchlorphos T826 AR 0.1 µg/l N 001,005

Fenitrothion T826 AR 0.1 µg/l N 001,005

Fenpiclonil T826 AR 0.1 µg/l N 001,005

Fenpropathrin T826 AR 0.1 µg/l N 001,005

Fenpropimorph T826 AR 0.1 µg/l N 001,005

Fenson T826 AR 0.1 µg/l N 001,005

Fensulfothion T826 AR 0.1 µg/l N 001,005

Fenthion T826 AR 0.1 µg/l N 001,005

Fenvalerate T826 AR 0.1 µg/l N 001,005

Fipronil T826 AR 0.1 µg/l N 001,005

Fipronil sulphone T826 AR 0.1 µg/l N 001,005

Flamprop isopropyl T826 AR 0.1 µg/l N 001,005

Fluazifop-P-Butyl T826 AR 0.1 µg/l N 001,005

Flucythrinate T826 AR 0.1 µg/l N 001,005

Fludioxonil T826 AR 0.1 µg/l N 001,005

Flufenacet T826 AR 0.1 µg/l N 001,005

Flumetralin T826 AR 0.1 µg/l N 001,005

Flumioxazin T826 AR 0.1 µg/l N 001,005

Flumorph T826 AR 0.1 µg/l N 001,005

Fluopyram T826 AR 0.1 µg/l N 001,005

Fluquinconazole T826 AR 0.1 µg/l N 001,005

Fluroxypyr-1-methylheptyl ester T826 AR 0.1 µg/l N 001,005

Flusilazole T826 AR 0.1 µg/l N 001,005

Flutolanil T826 AR 0.1 µg/l N 001,005

Fluxapyroxad T826 AR 0.1 µg/l N 001,005

Fonophos T826 AR 0.1 µg/l N 001,005

Formothion T826 AR 0.1 µg/l N 001,005

Furalaxyl T826 AR 0.1 µg/l N 001,005

Haloxyfop etotyl T826 AR 0.1 µg/l N 001,005

Haloxyfop Methyl T826 AR 0.1 µg/l N 001,005

Heptachlor T826 AR 0.1 µg/l N 001,005

Heptachlor epoxide T826 AR 0.1 µg/l N 001,005

Heptachlor exo Epoxide T826 AR 0.1 µg/l N 001,005

Heptenophos T826 AR 0.1 µg/l N 001,005

Hexachlorobenzene T826 AR 0.1 µg/l N 001,005

Hexachlorocyclohexane (alpha) T826 AR 0.1 µg/l N 001,005

Hexachlorocyclohexane (beta) T826 AR 0.1 µg/l N 001,005

Hexachlorocyclohexane (delta) T826 AR 0.1 µg/l N 001,005

Hexaconazole T826 AR 0.1 µg/l N 001,005

Hexazinone T826 AR 0.1 µg/l N 001,005

Iodofenphos T826 AR 0.1 µg/l N 001,005

Iprodione T826 AR 0.1 µg/l N 001,005

Isazofos T826 AR 0.1 µg/l N 001,005

Isocarbophos T826 AR 0.1 µg/l N 001,005

Isodrin T826 AR 0.1 µg/l N 001,005



674893-1


Isofenphos T826 AR 0.1 µg/l N 001,005

Isofenphos Methyl T826 AR 0.1 µg/l N 001,005

Isomethiozin T826 AR 0.1 µg/l N 001,005

Isoprothiolane T826 AR 0.1 µg/l N 001,005

Isopyrazam T826 AR 0.1 µg/l N 001,005

Kresoxim Methyl T826 AR 0.1 µg/l N 001,005

Lambda Cyhalothrin T826 AR 0.1 µg/l N 001,005

Lenacil T826 AR 0.1 µg/l N 001,005

Leptophos T826 AR 0.1 µg/l N 001,005

Lindane T826 AR 0.1 µg/l N 001,005

Malathion T826 AR 0.1 µg/l N 001,005

MCPA-thioethyl T826 AR 0.1 µg/l N 001,005

Mecarbam T826 AR 0.1 µg/l N 001,005

Mepanipyrim T826 AR 0.1 µg/l N 001,005

Mephosfolan T826 AR 0.1 µg/l N 001,005

Mepronil T826 AR 0.1 µg/l N 001,005

Metalaxyl T826 AR 0.1 µg/l N 001,005

Metazachlor T826 AR 0.1 µg/l N 001,005

Methacrifos T826 AR 0.1 µg/l N 001,005

Methidathion T826 AR 0.1 µg/l N 001,005

Methoxychlor T826 AR 0.1 µg/l N 001,005

Methyl Paraoxon T826 AR 0.1 µg/l N 001,005

Metolachlor T826 AR 0.1 µg/l N 001,005

Metolcarb T826 AR 0.1 µg/l N 001,005

Metrafenone T826 AR 0.1 µg/l N 001,005

Metribuzin T826 AR 0.1 µg/l N 001,005

Mevinphos T826 AR 0.1 µg/l N 001,005

Mirex T826 AR 0.1 µg/l N 001,005

Molinate T826 AR 0.1 µg/l N 001,005

Myclobutanil T826 AR 0.1 µg/l N 001,005

Napropamide T826 AR 0.1 µg/l N 001,005

Nitrofen T826 AR 0.1 µg/l N 001,005

Nitrothal isopropyl T826 AR 0.1 µg/l N 001,005

Nuarimol T826 AR 0.1 µg/l N 001,005

o,p'-DDT T826 AR 0.1 µg/l N 001,005

o,p-DDD T826 AR 0.1 µg/l N 001,005

o,p-DDE T826 AR 0.1 µg/l N 001,005

Octylisothiazolon T826 AR 0.1 µg/l N 001,005

Ofurace T826 AR 0.1 µg/l N 001,005

Orysastrobin T826 AR 0.1 µg/l N 001,005

Oxadiazon T826 AR 0.1 µg/l N 001,005

Oxadixyl T826 AR 0.1 µg/l N 001,005

Oxyfluorfen T826 AR 0.1 µg/l N 001,005

p,p-DDD T826 AR 0.1 µg/l N 001,005

p,p-DDE T826 AR 0.1 µg/l N 001,005

p,p-DDT T826 AR 0.1 µg/l N 001,005

Paclobutrazol T826 AR 0.1 µg/l N 001,005

Paraoxon T826 AR 0.1 µg/l N 001,005

Parathion T826 AR 0.1 µg/l N 001,005

Parathion methyl T826 AR 0.1 µg/l N 001,005

Penconazole T826 AR 0.1 µg/l N 001,005

Pendimethalin T826 AR 0.1 µg/l N 001,005

Pentachloroaniline T826 AR 0.1 µg/l N 001,005

Pentachlorophenol T826 AR 0.1 µg/l N 001,005

Pentanochlor T826 AR 0.1 µg/l N 001,005

Permethrin T826 AR 0.1 µg/l N 001,005

Pethoxamid T826 AR 0.1 µg/l N 001,005

Phenothrin T826 AR 0.1 µg/l N 001,005

Phenthoate T826 AR 0.1 µg/l N 001,005

Phorate T826 AR 0.1 µg/l N 001,005

Phosalone T826 AR 0.1 µg/l N 001,005

Phosfolan T826 AR 0.1 µg/l N 001,005

Picoxystrobin T826 AR 0.1 µg/l N 001,005

Piperonyl Butoxide T826 AR 0.1 µg/l N 001,005

Pirimicarb T826 AR 0.1 µg/l N 001,005

Pirimiphos Ethyl T826 AR 0.1 µg/l N 001,005

Pirimiphos methyl T826 AR 0.1 µg/l N 001,005

Pretilachlor T826 AR 0.1 µg/l N 001,005

Procymidone T826 AR 0.1 µg/l N 001,005

Profenofos T826 AR 0.1 µg/l N 001,005



674893-1


Prometon T826 AR 0.1 µg/l N 001,005

Prometryn T826 AR 0.1 µg/l N 001,005

Propachlor T826 AR 0.1 µg/l N 001,005

Propanil T826 AR 0.1 µg/l N 001,005

Propaphos T826 AR 0.1 µg/l N 001,005

Propargite T826 AR 0.1 µg/l N 001,005

Propazine T826 AR 0.1 µg/l N 001,005

Propetamphos T826 AR 0.1 µg/l N 001,005

Propham T826 AR 0.1 µg/l N 001,005

Propiconazole T826 AR 0.1 µg/l N 001,005

Propyzamide T826 AR 0.1 µg/l N 001,005

Proquinazid T826 AR 0.1 µg/l N 001,005

Prosulfocarb T826 AR 0.1 µg/l N 001,005

Prothiofos T826 AR 0.1 µg/l N 001,005

Pyraclostrobin T826 AR 0.1 µg/l N 001,005

Pyraflufen ethyl T826 AR 0.1 µg/l N 001,005

Pyrazophos T826 AR 0.1 µg/l N 001,005

Pyridaben T826 AR 0.1 µg/l N 001,005

Pyridaphenthion T826 AR 0.1 µg/l N 001,005

Pyrimethanil T826 AR 0.1 µg/l N 001,005

Pyriproxyfen T826 AR 0.1 µg/l N 001,005

Quinalphos T826 AR 0.1 µg/l N 001,005

Quinoxyfen T826 AR 0.1 µg/l N 001,005

Quintozene T826 AR 0.1 µg/l N 001,005

Quizalofop-ethyl T826 AR 0.1 µg/l N 001,005

Secbumeton T826 AR 0.1 µg/l N 001,005

Silafluofen T826 AR 0.1 µg/l N 001,005

Simazine T826 AR 0.1 µg/l N 001,005

Simeconazole T826 AR 0.1 µg/l N 001,005

Sulfallate T826 AR 0.1 µg/l N 001,005

Sulprofos T826 AR 0.1 µg/l N 001,005

Tebuconazole T826 AR 0.1 µg/l N 001,005

Tebufenpyrad T826 AR 0.1 µg/l N 001,005

Tebupirimiphos T826 AR 0.1 µg/l N 001,005

Tecnazene T826 AR 0.1 µg/l N 001,005

Tefluthrin T826 AR 0.1 µg/l N 001,005

Terbacil T826 AR 0.1 µg/l N 001,005

Terbufos T826 AR 0.1 µg/l N 001,005

Terbumeton T826 AR 0.1 µg/l N 001,005

Terbuthylazine T826 AR 0.1 µg/l N 001,005

Terbutryn T826 AR 0.1 µg/l N 001,005

Tetrachlorvinphos T826 AR 0.1 µg/l N 001,005

Tetraconazole T826 AR 0.1 µg/l N 001,005

Tetradifon T826 AR 0.1 µg/l N 001,005

sulfotep T826 AR 0.1 µg/l N 001,005

Tetramethrin T826 AR 0.1 µg/l N 001,005

Tetrasul T826 AR 0.1 µg/l N 001,005

Thiamethoxam T826 AR 0.1 µg/l N 001,005

Thiobencarb T826 AR 0.1 µg/l N 001,005

Tolclofos methyl T826 AR 0.1 µg/l N 001,005

Triadimefon T826 AR 0.1 µg/l N 001,005

Triadimenol T826 AR 0.1 µg/l N 001,005

Triallate T826 AR 0.1 µg/l N 001,005

Triazamate T826 AR 0.1 µg/l N 001,005

Triazophos T826 AR 0.1 µg/l N 001,005

Trifloxystrobin T826 AR 0.1 µg/l N 001,005

Triflumizole T826 AR 0.1 µg/l N 001,005

Trifluralin T826 AR 0.1 µg/l N 001,005

Vinclozolin T826 AR 0.1 µg/l N 001,005

Vinclozolin metabolite 3,5-Dichloroaniline T826 AR 0.1 µg/l N 001,005



674893-1




CornbrookManchester

M16 9FETel : 0161 874 2400Fax : 0161 874 2468






Date Job Received at Concept: 24-Aug-2017Date Analysis Started: 25-Aug-2017







Wales (No 2514788)

1549



Page 1 of 8

678085-1





Groundwater Suite


Customer Sample Reference BH12A

Date Sampled 24-AUG-2017


As (Dissolved) T281 AR 0.2 µg/l 1.2

B (Dissolved) T373 AR 0.01 mg/l 0.51

Cd (Dissolved) T281 AR 0.02 µg/l 0.18

Cr (Dissolved) T281 AR 1 µg/l 6

Cu (Dissolved) T281 AR 0.5 µg/l 3.0

Pb (Dissolved) T281 AR 0.3 µg/l <0.3

Hg (Dissolved) T281 AR 0.05 µg/l 0.09

Ni (Dissolved) T281 AR 1 µg/l 10

Se (Dissolved) T281 AR 0.5 µg/l 2.4

V (Dissolved) T281 AR 2 µg/l <2

Zn (Dissolved) T281 AR 2 µg/l 29

Ammoniacal nitrogen T686 F 0.05 mg/l 0.11

Chloride T686 F 1 mg/l 550

Cyanide(Total) T4 AR 0.05 mg/l <0.05

Fluoride T686 F 0.05 mg/l <0.05

Nitrate T686 F 0.5 mg/l 19

Phosphate T686 F 0.5 mg/l 2.5

Sulphate T686 F 0.5 mg/l 75

Sulphide T4 AR 0.05 mg/l <0.05

Total Phenols T16 AR 0.5 µg/l (13) <0.5

Electrical Conductivity T7 AR 10 µS/cm 3000

Total Organic Carbon T21 AR 1 mg/l 80

pH T7 AR 6.95





PAH USEPA16





Naphthalene T149 AR 0.01 µg/l (13,3,131)

<0.67

Acenaphthylene T149 AR 0.01 µg/l (13) 0.02

Acenaphthene T149 AR 0.01 µg/l (13) 0.01

Fluorene T149 AR 0.01 µg/l (13) 0.02

Phenanthrene T149 AR 0.01 µg/l (13) 0.13

Anthracene T149 AR 0.01 µg/l (13) 0.04

Fluoranthene T149 AR 0.01 µg/l (13) 0.31

Pyrene T149 AR 0.01 µg/l (13) 0.33

Benzo(a)Anthracene T149 AR 0.01 µg/l (13) 0.16

Chrysene T149 AR 0.01 µg/l (13) 0.18

Benzo(b)fluoranthene T149 AR 0.01 µg/l (13) 0.17

Benzo(k)fluoranthene T149 AR 0.01 µg/l (13) 0.15

Benzo(a)Pyrene T149 AR 0.01 µg/l (13) 0.18

Indeno(123-cd)Pyrene T149 AR 0.01 µg/l (13) 0.12

Dibenzo(ah)Anthracene T149 AR 0.01 µg/l (13) 0.03

Benzo(ghi)Perylene T149 AR 0.01 µg/l (13) 0.15

PAH(total) T149 AR 0.01 µg/l 2.0



678085-1





PCB EC7





PCB BZ#28 T1 AR 0.005 µg/l <0.005

PCB BZ#52 T1 AR 0.005 µg/l <0.005

PCB BZ#101 T1 AR 0.005 µg/l <0.005

PCB BZ#118 T16 AR 0.005 µg/l <0.005

PCB BZ#138 T1 AR 0.005 µg/l <0.005

PCB BZ#153 T1 AR 0.005 µg/l <0.005

PCB BZ#180 T1 AR 0.005 µg/l <0.005










Benzene T54 AR 1 µg/l (13) <1

Toluene T54 AR 1 µg/l <1

EthylBenzene T54 AR 1 µg/l <1

M/P Xylene T54 AR 1 µg/l <1

O Xylene T54 AR 1 µg/l <1

Methyl tert-Butyl Ether T54 AR 1 µg/l <1

TPH (C5-C6 aliphatic) T215 AR 10 µg/l <10



TPH (C10-C12 aliphatic) T910 AR 0.01 mg/l (13) <0.01



TPH (C21-C35 aliphatic) T910 AR 0.01 mg/l (13) 0.06

TPH (C6-C7 aromatic) T215 AR 10 µg/l <10



TPH (C10-C12 aromatic) T910 AR 0.01 mg/l (13) <0.01






678085-1










Dichlorodifluoromethane T54 AR 1 µg/l <1

Chloromethane T54 AR 1 µg/l <1

Vinyl chloride T54 AR 1 µg/l <1

Bromomethane T54 AR 1 µg/l <1

Chloroethane T54 AR 1 µg/l <1

Trichlorofluoromethane T54 AR 1 µg/l <1

1,1-Dichloroethylene T54 AR 1 µg/l <1

Dichloromethane T54 AR 50 µg/l <50

Trans-1,2-Dichloroethene T54 AR 1 µg/l <1

1,1-Dichloroethane T54 AR 1 µg/l <1

Cis-1,2-Dichloroethylene T54 AR 1 µg/l <1

2,2-Dichloropropane T54 AR 1 µg/l <1

Chloroform T54 AR 1 µg/l <1

Bromochloromethane T54 AR 1 µg/l <1

1,1,1-Trichloroethane T54 AR 1 µg/l <1

1,1-Dichloropropene T54 AR 1 µg/l <1

Carbon tetrachloride T54 AR 1 µg/l <1




1,1,2-Trichloroethylene T54 AR 1 µg/l <1

Bromodichloromethane T54 AR 1 µg/l <1

Dibromomethane T54 AR 1 µg/l <1

Cis-1,3-Dichloropropene T54 AR 1 µg/l <1


Trans-1,3-Dichloropropene T54 AR 1 µg/l <1



Tetrachloroethene T54 AR 1 µg/l <1

Chlorodibromomethane T54 AR 1 µg/l <1

1,2-dibromoethane T54 AR 1 µg/l <1

Chlorobenzene T54 AR 1 µg/l <1

1,1,1,2-Tetrachloroethane T54 AR 1 µg/l <1




Styrene T54 AR 1 µg/l <1

Bromoform T54 AR 1 µg/l <1

Isopropyl benzene T54 AR 1 µg/l <1


1,2,3-Trichloropropane T54 AR 1 µg/l <1

n-Propylbenzene T54 AR 1 µg/l <1

Bromobenzene T54 AR 1 µg/l <1

1,3,5-Trimethylbenzene T54 AR 1 µg/l <1

T-Butylbenzene T54 AR 1 µg/l <1


S-Butylbenzene T54 AR 1 µg/l <1

p-Isopropyltoluene T54 AR 1 µg/l <1

2-Chlorotoluene T54 AR 1 µg/l <1


1,3-Dichlorobenzene T54 AR 1 µg/l <1





678085-1











Phenol T16 AR 10 µg/l <10

Bis (2-chloroethyl) ether T16 AR 10 µg/l <10

2-Chlorophenol T16 AR 10 µg/l <10




Bis (2-chloroisopropyl) ether T16 AR 10 µg/l <10

2-methyl phenol T16 AR 10 µg/l <10

3/4-Methylphenol T16 AR 10 µg/l <10

Hexachloroethane T16 AR 10 µg/l <10

Nitrobenzene T16 AR 10 µg/l <10

Isophorone T16 AR 10 µg/l <10

2-Nitrophenol T16 AR 10 µg/l <10

2,4-Dimethylphenol T16 AR 10 µg/l <10

Bis (2-chloroethoxy) methane T16 AR 10 µg/l <10

2,4-Dichlorophenol T16 AR 10 µg/l <10

1,2,4-Trichlorobenzene T16 AR 10 µg/l <10

4-Chloroaniline T16 AR 10 µg/l <10

Hexachlorobutadiene T16 AR 10 µg/l (162) <20

4-Chloro-3-methylphenol T16 AR 10 µg/l <10

2-Methylnaphthalene T16 AR 10 µg/l <10

Hexachlorocyclopentadiene T16 AR 10 µg/l (162) <50

2,4,6-Trichlorophenol T16 AR 10 µg/l <10


2-Chloronaphthalene T16 AR 10 µg/l <10

2-Nitroaniline T16 AR 10 µg/l <10

Dimethyl phthalate T16 AR 10 µg/l <10

2,6-Dinitrotoluene T16 AR 10 µg/l <10


Dibenzofuran T16 AR 10 µg/l <10


Diethyl phthalate T16 AR 10 µg/l <10

4-Chlorophenyl phenylether T16 AR 10 µg/l <10


Azobenzene T16 AR 10 µg/l <10

4-Bromophenyl phenylether T16 AR 10 µg/l <10

Hexachlorobenzene T16 AR 10 µg/l <10

Pentachlorophenol T16 AR 10 µg/l <10

Carbazole T16 AR 10 µg/l <10

Di-n-butylphthalate T16 AR 10 µg/l <10

Butyl benzylphthalate T16 AR 10 µg/l <10

Bis (2-ethylhexyl)phthalate T16 AR 10 µg/l <10

Di-n-octylphthalate T16 AR 10 µg/l <10

Value Description

F Filtered

AR As Received


131 Result is outside of the scope of accreditation due to a QC Failure

3 LOD Raised Due to Elevated Blank






678085-1

Notes

Method Index


These samples have been analysed exceeding recommended PAH and TPH holding times. It is possible therefore that the results provided may be compromised.

Value Description

T4 Colorimetry

T910 GCxGC (LV)




T21 OX/IR

T7 Probe


T16 GC/MS

T1 GC/MS (HR)

T149 GC/MS (SIR)



As (Dissolved) T281 AR 0.2 µg/l U 001

B (Dissolved) T373 AR 0.01 mg/l N 001

Cd (Dissolved) T281 AR 0.02 µg/l U 001

Cr (Dissolved) T281 AR 1 µg/l U 001

Cu (Dissolved) T281 AR 0.5 µg/l U 001

Pb (Dissolved) T281 AR 0.3 µg/l U 001

Hg (Dissolved) T281 AR 0.05 µg/l U 001

Ni (Dissolved) T281 AR 1 µg/l U 001

Se (Dissolved) T281 AR 0.5 µg/l U 001

V (Dissolved) T281 AR 2 µg/l U 001

Zn (Dissolved) T281 AR 2 µg/l U 001

Ammoniacal nitrogen T686 F 0.05 mg/l U 001

Chloride T686 F 1 mg/l U 001

Cyanide(Total) T4 AR 0.05 mg/l U 001

Fluoride T686 F 0.05 mg/l U 001

Nitrate T686 F 0.5 mg/l U 001

Phosphate T686 F 0.5 mg/l U 001

Sulphate T686 F 0.5 mg/l U 001

Sulphide T4 AR 0.05 mg/l N 001

Total Phenols T16 AR 0.5 µg/l U 001

Electrical Conductivity T7 AR 10 µS/cm N 001

Total Organic Carbon T21 AR 1 mg/l U 001

pH T7 AR U 001

Naphthalene T149 AR 0.01 µg/l U 001

Acenaphthylene T149 AR 0.01 µg/l U 001

Acenaphthene T149 AR 0.01 µg/l U 001

Fluorene T149 AR 0.01 µg/l U 001

Phenanthrene T149 AR 0.01 µg/l U 001

Anthracene T149 AR 0.01 µg/l U 001

Fluoranthene T149 AR 0.01 µg/l U 001

Pyrene T149 AR 0.01 µg/l U 001

Benzo(a)Anthracene T149 AR 0.01 µg/l U 001

Chrysene T149 AR 0.01 µg/l U 001

Benzo(b)fluoranthene T149 AR 0.01 µg/l U 001

Benzo(k)fluoranthene T149 AR 0.01 µg/l U 001

Benzo(a)Pyrene T149 AR 0.01 µg/l U 001

Indeno(123-cd)Pyrene T149 AR 0.01 µg/l U 001

Dibenzo(ah)Anthracene T149 AR 0.01 µg/l U 001

Benzo(ghi)Perylene T149 AR 0.01 µg/l U 001

PAH(total) T149 AR 0.01 µg/l U 001

PCB BZ#28 T1 AR 0.005 µg/l U 001

PCB BZ#52 T1 AR 0.005 µg/l U 001

PCB BZ#101 T1 AR 0.005 µg/l U 001

PCB BZ#118 T16 AR 0.005 µg/l U 001

PCB BZ#138 T1 AR 0.005 µg/l U 001



678085-1


PCB BZ#153 T1 AR 0.005 µg/l U 001

PCB BZ#180 T1 AR 0.005 µg/l U 001

Benzene T54 AR 1 µg/l U 001

Toluene T54 AR 1 µg/l U 001

EthylBenzene T54 AR 1 µg/l U 001

O Xylene T54 AR 1 µg/l U 001

Methyl tert-Butyl Ether T54 AR 1 µg/l U 001

TPH (C5-C6 aliphatic) T215 AR 10 µg/l N 001



TPH (C10-C12 aliphatic) T910 AR 0.01 mg/l N 001




TPH (C6-C7 aromatic) T215 AR 10 µg/l N 001



TPH (C10-C12 aromatic) T910 AR 0.01 mg/l N 001




Dichlorodifluoromethane T54 AR 1 µg/l U 001

Chloromethane T54 AR 1 µg/l U 001

Vinyl chloride T54 AR 1 µg/l U 001

Bromomethane T54 AR 1 µg/l U 001

Chloroethane T54 AR 1 µg/l U 001

Trichlorofluoromethane T54 AR 1 µg/l U 001

1,1-Dichloroethylene T54 AR 1 µg/l U 001

Dichloromethane T54 AR 50 µg/l N 001

Trans-1,2-Dichloroethene T54 AR 1 µg/l U 001

1,1-Dichloroethane T54 AR 1 µg/l U 001

Cis-1,2-Dichloroethylene T54 AR 1 µg/l U 001

2,2-Dichloropropane T54 AR 1 µg/l U 001

Chloroform T54 AR 1 µg/l U 001

Bromochloromethane T54 AR 1 µg/l U 001

1,1,1-Trichloroethane T54 AR 1 µg/l U 001

1,1-Dichloropropene T54 AR 1 µg/l U 001

Carbon tetrachloride T54 AR 1 µg/l U 001



1,1,2-Trichloroethylene T54 AR 1 µg/l U 001

Bromodichloromethane T54 AR 1 µg/l U 001

Dibromomethane T54 AR 1 µg/l U 001

Cis-1,3-Dichloropropene T54 AR 1 µg/l U 001

Trans-1,3-Dichloropropene T54 AR 1 µg/l U 001



Tetrachloroethene T54 AR 1 µg/l U 001

Chlorodibromomethane T54 AR 1 µg/l U 001

1,2-dibromoethane T54 AR 1 µg/l U 001

Chlorobenzene T54 AR 1 µg/l U 001

1,1,1,2-Tetrachloroethane T54 AR 1 µg/l U 001

M/P Xylene T54 AR 1 µg/l U 001

Styrene T54 AR 1 µg/l U 001

Bromoform T54 AR 1 µg/l U 001

Isopropyl benzene T54 AR 1 µg/l U 001


1,2,3-Trichloropropane T54 AR 1 µg/l U 001

n-Propylbenzene T54 AR 1 µg/l U 001

Bromobenzene T54 AR 1 µg/l U 001

1,3,5-Trimethylbenzene T54 AR 1 µg/l U 001

T-Butylbenzene T54 AR 1 µg/l U 001


S-Butylbenzene T54 AR 1 µg/l U 001

p-Isopropyltoluene T54 AR 1 µg/l U 001

2-Chlorotoluene T54 AR 1 µg/l U 001


1,3-Dichlorobenzene T54 AR 1 µg/l U 001





678085-1


Phenol T16 AR 10 µg/l U 001

Bis (2-chloroethyl) ether T16 AR 10 µg/l U 001

2-Chlorophenol T16 AR 10 µg/l U 001




Bis (2-chloroisopropyl) ether T16 AR 10 µg/l U 001

2-methyl phenol T16 AR 10 µg/l U 001

3/4-Methylphenol T16 AR 10 µg/l U 001

Hexachloroethane T16 AR 10 µg/l U 001

Nitrobenzene T16 AR 10 µg/l U 001

Isophorone T16 AR 10 µg/l U 001

2-Nitrophenol T16 AR 10 µg/l U 001

2,4-Dimethylphenol T16 AR 10 µg/l U 001

Bis (2-chloroethoxy) methane T16 AR 10 µg/l U 001

2,4-Dichlorophenol T16 AR 10 µg/l U 001

1,2,4-Trichlorobenzene T16 AR 10 µg/l U 001

4-Chloroaniline T16 AR 10 µg/l U 001

Hexachlorobutadiene T16 AR 10 µg/l U 001

4-Chloro-3-methylphenol T16 AR 10 µg/l U 001

2-Methylnaphthalene T16 AR 10 µg/l U 001

Hexachlorocyclopentadiene T16 AR 10 µg/l U 001

2,4,6-Trichlorophenol T16 AR 10 µg/l U 001


2-Chloronaphthalene T16 AR 10 µg/l U 001

2-Nitroaniline T16 AR 10 µg/l U 001

Dimethyl phthalate T16 AR 10 µg/l U 001

2,6-Dinitrotoluene T16 AR 10 µg/l U 001


Dibenzofuran T16 AR 10 µg/l U 001


Diethyl phthalate T16 AR 10 µg/l U 001

4-Chlorophenyl phenylether T16 AR 10 µg/l U 001


Azobenzene T16 AR 10 µg/l U 001

4-Bromophenyl phenylether T16 AR 10 µg/l U 001

Hexachlorobenzene T16 AR 10 µg/l U 001

Pentachlorophenol T16 AR 10 µg/l U 001

Carbazole T16 AR 10 µg/l U 001

Di-n-butylphthalate T16 AR 10 µg/l U 001

Butyl benzylphthalate T16 AR 10 µg/l U 001

Bis (2-ethylhexyl)phthalate T16 AR 10 µg/l U 001

Di-n-octylphthalate T16 AR 10 µg/l U 001



678085-1




CornbrookManchester

M16 9FETel : 0161 874 2400Fax : 0161 874 2468




Customer Contact: Ms Hannah Hadwin


Date Job Received at Concept: 31-Aug-2017Date Analysis Started: 01-Sep-2017







Wales (No 2514788)

1549



Page 1 of 18

679268-1





Groundwater Suite





As (Dissolved) T281 AR 0.2 µg/l 2.3

B (Dissolved) T373 AR 0.01 mg/l 0.32

Cd (Dissolved) T281 AR 0.02 µg/l <0.02

Cr (Dissolved) T281 AR 1 µg/l <1

Cu (Dissolved) T281 AR 0.5 µg/l 1.3

Pb (Dissolved) T281 AR 0.3 µg/l <0.3

Hg (Dissolved) T281 AR 0.05 µg/l <0.05

Ni (Dissolved) T281 AR 1 µg/l 7

Se (Dissolved) T281 AR 0.5 µg/l <0.5

V (Dissolved) T281 AR 2 µg/l 2

Zn (Dissolved) T281 AR 2 µg/l 8

Ammoniacal nitrogen T686 F 0.05 mg/l 4.4

Chloride T686 F 1 mg/l 300

Cyanide(Total) T4 AR 0.05 mg/l <0.05

Fluoride T686 F 0.05 mg/l 0.25

Nitrate T686 F 0.5 mg/l 78

Phosphate T686 F 0.5 mg/l 18

Sulphate T686 F 0.5 mg/l 32

Sulphide T4 AR 0.05 mg/l 0.11

Total Phenols T16 AR 0.5 µg/l <0.5

Electrical Conductivity T7 AR 10 µS/cm 2100

Total Organic Carbon T21 AR 1 mg/l 170

pH T7 AR 7.01





PAH USEPA16





Naphthalene T149 AR 0.01 µg/l (3,13,131)

<0.35

Acenaphthylene T149 AR 0.01 µg/l (13) <0.01

Acenaphthene T149 AR 0.01 µg/l (13) 0.01

Fluorene T149 AR 0.01 µg/l (13) 0.02

Phenanthrene T149 AR 0.01 µg/l (13) 0.03

Anthracene T149 AR 0.01 µg/l (13) 0.02

Fluoranthene T149 AR 0.01 µg/l (13) 0.02

Pyrene T149 AR 0.01 µg/l (13) 0.02

Benzo(a)Anthracene T149 AR 0.01 µg/l (13) 0.01

Chrysene T149 AR 0.01 µg/l (13) 0.01

Benzo(b)fluoranthene T149 AR 0.01 µg/l (13) 0.01

Benzo(k)fluoranthene T149 AR 0.01 µg/l (13) 0.01

Benzo(a)Pyrene T149 AR 0.01 µg/l (13) 0.01

Indeno(123-cd)Pyrene T149 AR 0.01 µg/l (13) 0.01

Dibenzo(ah)Anthracene T149 AR 0.01 µg/l (13) <0.01

Benzo(ghi)Perylene T149 AR 0.01 µg/l (13) 0.01

PAH(total) T149 AR 0.01 µg/l <0.35



679268-1





PCB EC7





PCB BZ#28 T1 AR 0.005 µg/l <0.005

PCB BZ#52 T1 AR 0.005 µg/l <0.005

PCB BZ#101 T1 AR 0.005 µg/l <0.005

PCB BZ#118 T16 AR 0.005 µg/l <0.005

PCB BZ#138 T1 AR 0.005 µg/l <0.005

PCB BZ#153 T1 AR 0.005 µg/l <0.005

PCB BZ#180 T1 AR 0.005 µg/l <0.005















Methyl tert-Butyl Ether T54 AR 1 µg/l <1

















679268-1










Dichlorodifluoromethane T54 AR 1 µg/l <1

Chloromethane T54 AR 1 µg/l <1

Vinyl chloride T54 AR 1 µg/l <1

Bromomethane T54 AR 1 µg/l <1

Chloroethane T54 AR 1 µg/l <1

Trichlorofluoromethane T54 AR 1 µg/l <1

1,1-Dichloroethylene T54 AR 1 µg/l <1

Dichloromethane T54 AR 50 µg/l <50

Trans-1,2-Dichloroethene T54 AR 1 µg/l <1


Cis-1,2-Dichloroethylene T54 AR 1 µg/l <1


Chloroform T54 AR 1 µg/l <1

Bromochloromethane T54 AR 1 µg/l <1


1,1-Dichloropropene T54 AR 1 µg/l <1

Carbon tetrachloride T54 AR 1 µg/l <1




1,1,2-Trichloroethylene T54 AR 1 µg/l <1

Bromodichloromethane T54 AR 1 µg/l <1

Dibromomethane T54 AR 1 µg/l <1

Cis-1,3-Dichloropropene T54 AR 1 µg/l <1


Trans-1,3-Dichloropropene T54 AR 1 µg/l <1



Tetrachloroethene T54 AR 1 µg/l <1

Chlorodibromomethane T54 AR 1 µg/l <1

1,2-dibromoethane T54 AR 1 µg/l <1

Chlorobenzene T54 AR 1 µg/l <1





Styrene T54 AR 1 µg/l <1

Bromoform T54 AR 1 µg/l <1

Isopropyl benzene T54 AR 1 µg/l <1


1,2,3-Trichloropropane T54 AR 1 µg/l <1

n-Propylbenzene T54 AR 1 µg/l <1

Bromobenzene T54 AR 1 µg/l <1


T-Butylbenzene T54 AR 1 µg/l <1


S-Butylbenzene T54 AR 1 µg/l <1

p-Isopropyltoluene T54 AR 1 µg/l <1








679268-1










Phenol T16 AR 10 µg/l <10

Bis (2-chloroethyl) ether T16 AR 10 µg/l <10

2-Chlorophenol T16 AR 10 µg/l (162) <20




Bis (2-chloroisopropyl) ether T16 AR 10 µg/l <10

2-methyl phenol T16 AR 10 µg/l <10

3/4-Methylphenol T16 AR 10 µg/l <10

Hexachloroethane T16 AR 10 µg/l <10

Nitrobenzene T16 AR 10 µg/l <10

Isophorone T16 AR 10 µg/l <10

2-Nitrophenol T16 AR 10 µg/l <10

2,4-Dimethylphenol T16 AR 10 µg/l <10

Bis (2-chloroethoxy) methane T16 AR 10 µg/l <10

2,4-Dichlorophenol T16 AR 10 µg/l <10

1,2,4-Trichlorobenzene T16 AR 10 µg/l <10

4-Chloroaniline T16 AR 10 µg/l <10

Hexachlorobutadiene T16 AR 10 µg/l (162) <20

4-Chloro-3-methylphenol T16 AR 10 µg/l (162) <20

2-Methylnaphthalene T16 AR 10 µg/l <10

Hexachlorocyclopentadiene T16 AR 10 µg/l (162) <50



2-Chloronaphthalene T16 AR 10 µg/l <10


Dimethyl phthalate T16 AR 10 µg/l (162) <20



Dibenzofuran T16 AR 10 µg/l <10


Diethyl phthalate T16 AR 10 µg/l <10

4-Chlorophenyl phenylether T16 AR 10 µg/l <10


Azobenzene T16 AR 10 µg/l <10

4-Bromophenyl phenylether T16 AR 10 µg/l <10

Hexachlorobenzene T16 AR 10 µg/l <10

Pentachlorophenol T16 AR 10 µg/l <10

Carbazole T16 AR 10 µg/l <10

Di-n-butylphthalate T16 AR 10 µg/l <10

Butyl benzylphthalate T16 AR 10 µg/l <10

Bis (2-ethylhexyl)phthalate T16 AR 10 µg/l <10

Di-n-octylphthalate T16 AR 10 µg/l <10



679268-1





Pesticide Suite





Bentazone T310 AR 0.1 µg/l <0.1

Diuron T569 AR 0.1 µg/l (NR)

Isoproturon T569 AR 0.1 µg/l (NR)

Linuron T569 AR 0.1 µg/l (NR)

Mecoprop T16 AR 0.1 µg/l <0.1



679268-1










2,4,6-Trichlorophenol T826 AR 0.1 µg/l <0.1

2-Phenylphenol T826 AR 0.1 µg/l <0.1

Acetochlor T826 AR 0.1 µg/l <0.1

Aclonifen T826 AR 0.1 µg/l <0.1

Acrinathrin T826 AR 0.1 µg/l <0.1

Alachlor T826 AR 0.1 µg/l <0.1

Aldrin T826 AR 0.1 µg/l (278) <0.1

Ametryn T826 AR 0.1 µg/l (278) <0.1

Atraton T826 AR 0.1 µg/l (278) <0.1

Atrazine T826 AR 0.1 µg/l (278) <0.1

Azaconazole T826 AR 0.1 µg/l (278) <0.1

Azobenzene T826 AR 0.1 µg/l (278) <0.1

Azoxystrobin T826 AR 0.1 µg/l (278) <0.1

Benalaxyl T826 AR 0.1 µg/l <0.1

Benfluralin T826 AR 0.1 µg/l <0.1

Bifenox T826 AR 0.1 µg/l <0.1

Bifenthrin T826 AR 0.1 µg/l <0.1

Binapacryl T826 AR 0.1 µg/l <0.1

Biphenyl T826 AR 0.1 µg/l (278) <10

Bitertanol T826 AR 0.1 µg/l (278) <0.1

Boscalid T826 AR 0.1 µg/l <0.1

Bromacil T826 AR 0.1 µg/l (278) <0.1

Bromophos T826 AR 0.1 µg/l <0.1

Bromophos-Ethyl T826 AR 0.1 µg/l <0.1

Bromopropylate T826 AR 0.1 µg/l <0.1

Bupirimate T826 AR 0.1 µg/l (278) <0.1

Buprofezine T826 AR 0.1 µg/l (278) <0.1

Butachlor T826 AR 0.1 µg/l <0.1

Cadusafos T826 AR 0.1 µg/l <0.1

Carbaryl T826 AR 0.1 µg/l <0.1

Carbophenothion T826 AR 0.1 µg/l (278) <0.1

Carboxine T826 AR 0.1 µg/l (278) <0.1

Carfentrazone Ethyl T826 AR 0.1 µg/l <0.1

Chlorbenzilate T826 AR 0.1 µg/l <0.1

Chlordane T826 AR 0.1 µg/l (278) <0.1

Chlordimeform T826 AR 0.1 µg/l (278) <0.1

Chlorethoxyfos T826 AR 0.1 µg/l (278) <0.1

Chlorfenapyr T826 AR 0.1 µg/l <0.1

Chlorfenvinphos T826 AR 0.1 µg/l <0.1

Chlormephos T826 AR 0.1 µg/l (278) <0.1

Chloropropylate T826 AR 0.1 µg/l <0.1

Chlorothalonil T826 AR 0.1 µg/l <0.1

Chlorpropham T826 AR 0.1 µg/l <0.1

Chlorpyrifos T826 AR 0.1 µg/l <0.1

Chlorpyrifos methyl T826 AR 0.1 µg/l <0.1

Chlorthal Dimethyl T826 AR 0.1 µg/l <0.1

Chlorthion T826 AR 0.1 µg/l <0.1

Chlorthiophos T826 AR 0.1 µg/l (278) <0.1

Chlozolinate T826 AR 0.1 µg/l <0.1

Clodinafop propargy T826 AR 0.1 µg/l <0.1

Clomazone T826 AR 0.1 µg/l <0.1

Cloquintocet mexyl T826 AR 0.1 µg/l (278) <0.1

Coumaphos T826 AR 0.1 µg/l <0.1

Cyflufenamid T826 AR 0.1 µg/l <0.1

Cyfluthrin T826 AR 0.1 µg/l <0.1

Cypermethrin T826 AR 0.1 µg/l <0.1

Cyphenothrin T826 AR 0.1 µg/l <0.1

Cyproconazole T826 AR 0.1 µg/l (278) <0.1

Cyprodinil T826 AR 0.1 µg/l (278) <0.1

Deltamethrin T826 AR 0.1 µg/l <0.1



679268-1










Desmetryn T826 AR 0.1 µg/l (278) <0.1

Diafenthiuron T826 AR 0.1 µg/l (278) <0.1

Dialifos T826 AR 0.1 µg/l <0.1

Diazinon T826 AR 0.1 µg/l (278) <0.1

Dichlobenil T826 AR 0.1 µg/l <0.1

Dichlofenthion T826 AR 0.1 µg/l <0.1

Dichlorvos T826 AR 0.1 µg/l (278) <0.1

Diclobutrazol T826 AR 0.1 µg/l (278) <0.1

Dicloran T826 AR 0.1 µg/l <0.1

Dicofol T826 AR 0.1 µg/l (278) <0.1

Dieldrin T826 AR 0.1 µg/l <0.1

Difenoconazole T826 AR 0.1 µg/l (278) <0.1

Diflufenican T826 AR 0.1 µg/l <0.1

Dimethenamid T826 AR 0.1 µg/l <0.1

Dimethomorph T826 AR 0.1 µg/l (278) <0.1

Dimoxystrobin T826 AR 0.1 µg/l <0.1

Dioxabenzofos T826 AR 0.1 µg/l <0.1

Diphenamid T826 AR 0.1 µg/l <0.1

Diphenylamine T826 AR 0.1 µg/l <0.1

Disulfoton T826 AR 0.1 µg/l <0.1

Ditalimfos T826 AR 0.1 µg/l <0.1

Edifenphos T826 AR 0.1 µg/l <0.1

Endosulphan alpha T826 AR 0.1 µg/l <0.1

Endosulphan beta T826 AR 0.1 µg/l (278) <0.1

Endosulphan sulphate T826 AR 0.1 µg/l <0.1

Endrin T826 AR 0.1 µg/l <0.1

Epn T826 AR 0.1 µg/l <0.1

Epoxiconazole T826 AR 0.1 µg/l (278) <0.1

EPTC T826 AR 0.1 µg/l <0.1

Etaconazole T826 AR 0.1 µg/l (278) <0.1

Ethion T826 AR 0.1 µg/l <0.1

Ethofumesate T826 AR 0.1 µg/l <0.1

Ethoprophos T826 AR 0.1 µg/l <0.1

Ethoxyquin T826 AR 0.1 µg/l (278) <0.1

Etofenprox T826 AR 0.1 µg/l (278) <0.1

Etoxazole T826 AR 0.1 µg/l (278) <0.1

Etridiazole T826 AR 0.1 µg/l (278) <0.1

Etrimfos T826 AR 0.1 µg/l <0.1

Famoxadone T826 AR 0.1 µg/l <0.1

Famphur T826 AR 0.1 µg/l <0.1

Fenamidone T826 AR 0.1 µg/l <0.1

Fenamiphos T826 AR 0.1 µg/l (278) <0.1

Fenarimol T826 AR 0.1 µg/l (278) <0.1

Fenbuconazole T826 AR 0.1 µg/l (278) <0.1

Fenchlorphos T826 AR 0.1 µg/l <0.1

Fenitrothion T826 AR 0.1 µg/l <0.1

Fenpiclonil T826 AR 0.1 µg/l <0.1

Fenpropathrin T826 AR 0.1 µg/l <0.1

Fenpropimorph T826 AR 0.1 µg/l <0.1

Fenson T826 AR 0.1 µg/l <0.1

Fensulfothion T826 AR 0.1 µg/l (278) <0.1

Fenthion T826 AR 0.1 µg/l <0.1

Fenvalerate T826 AR 0.1 µg/l <0.1

Fipronil T826 AR 0.1 µg/l <0.1

Fipronil sulphone T826 AR 0.1 µg/l <0.1

Flamprop isopropyl T826 AR 0.1 µg/l <0.1

Fluazifop-P-Butyl T826 AR 0.1 µg/l <0.1

Flucythrinate T826 AR 0.1 µg/l <0.1

Fludioxonil T826 AR 0.1 µg/l <0.1

Flufenacet T826 AR 0.1 µg/l <0.1



679268-1










Flumetralin T826 AR 0.1 µg/l <0.1

Flumioxazin T826 AR 0.1 µg/l <0.1

Flumorph T826 AR 0.1 µg/l (278) <0.1

Fluopyram T826 AR 0.1 µg/l <0.1

Fluquinconazole T826 AR 0.1 µg/l <0.1

Fluroxypyr-1-methylheptyl ester T826 AR 0.1 µg/l <0.1

Flusilazole T826 AR 0.1 µg/l (278) <0.1

Flutolanil T826 AR 0.1 µg/l <0.1

Fluxapyroxad T826 AR 0.1 µg/l <0.1

Fonophos T826 AR 0.1 µg/l <0.1

Formothion T826 AR 0.1 µg/l <0.1

Furalaxyl T826 AR 0.1 µg/l (278) <0.1

Haloxyfop etotyl T826 AR 0.1 µg/l <0.1

Haloxyfop Methyl T826 AR 0.1 µg/l <0.1

Heptachlor T826 AR 0.1 µg/l (278) <0.1

Heptachlor epoxide T826 AR 0.1 µg/l <0.1

Heptachlor exo Epoxide T826 AR 0.1 µg/l <0.1

Heptenophos T826 AR 0.1 µg/l <0.1

Hexachlorobenzene T826 AR 0.1 µg/l (278) <0.1

Hexachlorocyclohexane (alpha) T826 AR 0.1 µg/l <0.1

Hexachlorocyclohexane (beta) T826 AR 0.1 µg/l <0.1

Hexachlorocyclohexane (delta) T826 AR 0.1 µg/l <0.1

Hexaconazole T826 AR 0.1 µg/l (278) <0.1

Hexazinone T826 AR 0.1 µg/l (278) <0.1

Iodofenphos T826 AR 0.1 µg/l <0.1

Iprodione T826 AR 0.1 µg/l <0.1

Isazofos T826 AR 0.1 µg/l <0.1

Isocarbophos T826 AR 0.1 µg/l <0.1

Isodrin T826 AR 0.1 µg/l <0.1

Isofenphos T826 AR 0.1 µg/l <0.1

Isofenphos Methyl T826 AR 0.1 µg/l <0.1

Isomethiozin T826 AR 0.1 µg/l <0.1

Isoprothiolane T826 AR 0.1 µg/l <0.1

Isopyrazam T826 AR 0.1 µg/l <0.1

Kresoxim Methyl T826 AR 0.1 µg/l <0.1

Lambda Cyhalothrin T826 AR 0.1 µg/l <0.1

Lenacil T826 AR 0.1 µg/l <0.1

Leptophos T826 AR 0.1 µg/l <0.1

Lindane T826 AR 0.1 µg/l <0.1

Malathion T826 AR 0.1 µg/l <0.1

MCPA-thioethyl T826 AR 0.1 µg/l <0.1

Mecarbam T826 AR 0.1 µg/l (278) <0.1

Mepanipyrim T826 AR 0.1 µg/l (278) <0.1

Mephosfolan T826 AR 0.1 µg/l (278) <0.1

Mepronil T826 AR 0.1 µg/l <0.1

Metalaxyl T826 AR 0.1 µg/l (278) <0.1

Metazachlor T826 AR 0.1 µg/l (278) <0.1

Methacrifos T826 AR 0.1 µg/l <0.1

Methidathion T826 AR 0.1 µg/l <0.1

Methoxychlor T826 AR 0.1 µg/l <0.1

Methyl Paraoxon T826 AR 0.1 µg/l <0.1

Metolachlor T826 AR 0.1 µg/l <0.1

Metolcarb T826 AR 0.1 µg/l <0.1

Metrafenone T826 AR 0.1 µg/l <0.1

Metribuzin T826 AR 0.1 µg/l (278) <0.1

Mevinphos T826 AR 0.1 µg/l (278) <0.1

Mirex T826 AR 0.1 µg/l <0.1

Molinate T826 AR 0.1 µg/l <0.1

Myclobutanil T826 AR 0.1 µg/l (278) <0.1

Napropamide T826 AR 0.1 µg/l <0.1



679268-1










Nitrofen T826 AR 0.1 µg/l <0.1

Nitrothal isopropyl T826 AR 0.1 µg/l <0.1

Nuarimol T826 AR 0.1 µg/l (278) <0.1

o,p'-DDT T826 AR 0.1 µg/l <0.1

o,p-DDD T826 AR 0.1 µg/l <0.1

o,p-DDE T826 AR 0.1 µg/l <0.1

Octylisothiazolon T826 AR 0.1 µg/l <0.1

Ofurace T826 AR 0.1 µg/l <0.1

Orysastrobin T826 AR 0.1 µg/l (278) <0.1

Oxadiazon T826 AR 0.1 µg/l <0.1

Oxadixyl T826 AR 0.1 µg/l (278) <0.1

Oxyfluorfen T826 AR 0.1 µg/l <0.1

p,p-DDD T826 AR 0.1 µg/l <0.1

p,p-DDE T826 AR 0.1 µg/l <0.1

p,p-DDT T826 AR 0.1 µg/l <0.1

Paclobutrazol T826 AR 0.1 µg/l (278) <0.1

Paraoxon T826 AR 0.1 µg/l <0.1

Parathion T826 AR 0.1 µg/l <0.1

Parathion methyl T826 AR 0.1 µg/l <0.1

Penconazole T826 AR 0.1 µg/l (278) <0.1

Pendimethalin T826 AR 0.1 µg/l <0.1

Pentachloroaniline T826 AR 0.1 µg/l <0.1

Pentachlorophenol T826 AR 0.1 µg/l <0.1

Pentanochlor T826 AR 0.1 µg/l <0.1

Permethrin T826 AR 0.1 µg/l <0.1

Pethoxamid T826 AR 0.1 µg/l <0.1

Phenothrin T826 AR 0.1 µg/l <0.1

Phenthoate T826 AR 0.1 µg/l <0.1

Phorate T826 AR 0.1 µg/l (278) <0.1

Phosalone T826 AR 0.1 µg/l <0.1

Phosfolan T826 AR 0.1 µg/l (278) <0.1

Picoxystrobin T826 AR 0.1 µg/l <0.1

Piperonyl Butoxide T826 AR 0.1 µg/l <0.1

Pirimicarb T826 AR 0.1 µg/l (278) <0.1

Pirimiphos Ethyl T826 AR 0.1 µg/l (278) <0.1

Pirimiphos methyl T826 AR 0.1 µg/l (278) <0.1

Pretilachlor T826 AR 0.1 µg/l <0.1

Procymidone T826 AR 0.1 µg/l (278) <0.1

Profenofos T826 AR 0.1 µg/l <0.1

Prometon T826 AR 0.1 µg/l (278) <0.1

Prometryn T826 AR 0.1 µg/l (278) <0.1

Propachlor T826 AR 0.1 µg/l <0.1

Propanil T826 AR 0.1 µg/l <0.1

Propaphos T826 AR 0.1 µg/l <0.1

Propargite T826 AR 0.1 µg/l (278) <0.1

Propazine T826 AR 0.1 µg/l (278) <0.1

Propetamphos T826 AR 0.1 µg/l <0.1

Propham T826 AR 0.1 µg/l <0.1

Propiconazole T826 AR 0.1 µg/l (278) <0.1

Propyzamide T826 AR 0.1 µg/l <0.1

Proquinazid T826 AR 0.1 µg/l <0.1

Prosulfocarb T826 AR 0.1 µg/l <0.1

Prothiofos T826 AR 0.1 µg/l <0.1

Pyraclostrobin T826 AR 0.1 µg/l <0.1

Pyraflufen ethyl T826 AR 0.1 µg/l <0.1

Pyrazophos T826 AR 0.1 µg/l <0.1

Pyridaben T826 AR 0.1 µg/l <0.1

Pyridaphenthion T826 AR 0.1 µg/l <0.1

Pyrimethanil T826 AR 0.1 µg/l (278) <0.1

Pyriproxyfen T826 AR 0.1 µg/l (278) <0.1



679268-1


Notes










Quinalphos T826 AR 0.1 µg/l <0.1

Quinoxyfen T826 AR 0.1 µg/l (278) <0.1

Quintozene T826 AR 0.1 µg/l (278) <0.1

Quizalofop-ethyl T826 AR 0.1 µg/l <0.1

Secbumeton T826 AR 0.1 µg/l (278) <0.1

Silafluofen T826 AR 0.1 µg/l (278) <0.1

Simazine T826 AR 0.1 µg/l (278) <0.1

Simeconazole T826 AR 0.1 µg/l (278) <0.1

Sulfallate T826 AR 0.1 µg/l (278) <0.1

Sulprofos T826 AR 0.1 µg/l <0.1

Tebuconazole T826 AR 0.1 µg/l (278) <0.1

Tebufenpyrad T826 AR 0.1 µg/l <0.1

Tebupirimiphos T826 AR 0.1 µg/l <0.1

Tecnazene T826 AR 0.1 µg/l (278) <0.1

Tefluthrin T826 AR 0.1 µg/l <0.1

Terbacil T826 AR 0.1 µg/l (278) <0.1

Terbufos T826 AR 0.1 µg/l <0.1

Terbumeton T826 AR 0.1 µg/l (278) <0.1

Terbuthylazine T826 AR 0.1 µg/l (278) <0.1

Terbutryn T826 AR 0.1 µg/l (278) <0.1

Tetrachlorvinphos T826 AR 0.1 µg/l <0.1

Tetraconazole T826 AR 0.1 µg/l (278) <0.1

Tetradifon T826 AR 0.1 µg/l <0.1

sulfotep T826 AR 0.1 µg/l <0.1

Tetramethrin T826 AR 0.1 µg/l <0.1

Tetrasul T826 AR 0.1 µg/l <0.1

Thiamethoxam T826 AR 0.1 µg/l (278) <0.1

Thiobencarb T826 AR 0.1 µg/l (278) <0.1

Tolclofos methyl T826 AR 0.1 µg/l <0.1

Triadimefon T826 AR 0.1 µg/l (278) <0.1

Triadimenol T826 AR 0.1 µg/l (278) <0.1

Triallate T826 AR 0.1 µg/l <0.1

Triazamate T826 AR 0.1 µg/l <0.1

Triazophos T826 AR 0.1 µg/l <0.1

Trifloxystrobin T826 AR 0.1 µg/l <0.1

Triflumizole T826 AR 0.1 µg/l (278) <0.1

Trifluralin T826 AR 0.1 µg/l <0.1

Vinclozolin T826 AR 0.1 µg/l <0.1

Vinclozolin metabolite 3,5-Dichloroaniline T826 AR 0.1 µg/l <0.1

Value Description

AR As Received

F Filtered



131 Result is outside of the scope of accreditation due to a QC Failure

3 LOD Raised Due to Elevated Blank

278 Data reported is qualitative as recovery is outside the 60 to 140% range

NR No Result





679268-1

Method Index


Pesticide testing is transferred to CLS Cambridge.

Value Description


T826 SOP611 (GC MSMS)


T21 OX/IR


T149 GC/MS (SIR)


T569 LC MS MS 1L

T310 LC/MS/MS

T16 GC/MS

T4 Colorimetry

T1 GC/MS (HR)


T7 Probe

T910 GCxGC (LV)


As (Dissolved) T281 AR 0.2 µg/l U 001

B (Dissolved) T373 AR 0.01 mg/l N 001

Cd (Dissolved) T281 AR 0.02 µg/l U 001

Cr (Dissolved) T281 AR 1 µg/l U 001

Cu (Dissolved) T281 AR 0.5 µg/l U 001

Pb (Dissolved) T281 AR 0.3 µg/l U 001

Hg (Dissolved) T281 AR 0.05 µg/l U 001

Ni (Dissolved) T281 AR 1 µg/l U 001

Se (Dissolved) T281 AR 0.5 µg/l U 001

V (Dissolved) T281 AR 2 µg/l U 001

Zn (Dissolved) T281 AR 2 µg/l U 001

Ammoniacal nitrogen T686 F 0.05 mg/l U 001

Chloride T686 F 1 mg/l U 001

Cyanide(Total) T4 AR 0.05 mg/l U 001

Fluoride T686 F 0.05 mg/l U 001

Nitrate T686 F 0.5 mg/l U 001

Phosphate T686 F 0.5 mg/l U 001

Sulphate T686 F 0.5 mg/l U 001

Sulphide T4 AR 0.05 mg/l N 001

Total Phenols T16 AR 0.5 µg/l U 001

Electrical Conductivity T7 AR 10 µS/cm N 001

Total Organic Carbon T21 AR 1 mg/l U 001

pH T7 AR U 001

Naphthalene T149 AR 0.01 µg/l U 001

Acenaphthylene T149 AR 0.01 µg/l U 001

Acenaphthene T149 AR 0.01 µg/l U 001

Fluorene T149 AR 0.01 µg/l U 001

Phenanthrene T149 AR 0.01 µg/l U 001

Anthracene T149 AR 0.01 µg/l U 001

Fluoranthene T149 AR 0.01 µg/l U 001

Pyrene T149 AR 0.01 µg/l U 001

Benzo(a)Anthracene T149 AR 0.01 µg/l U 001

Chrysene T149 AR 0.01 µg/l U 001

Benzo(b)fluoranthene T149 AR 0.01 µg/l U 001

Benzo(k)fluoranthene T149 AR 0.01 µg/l U 001

Benzo(a)Pyrene T149 AR 0.01 µg/l U 001

Indeno(123-cd)Pyrene T149 AR 0.01 µg/l U 001

Dibenzo(ah)Anthracene T149 AR 0.01 µg/l U 001

Benzo(ghi)Perylene T149 AR 0.01 µg/l U 001

PAH(total) T149 AR 0.01 µg/l U 001

PCB BZ#28 T1 AR 0.005 µg/l U 001

PCB BZ#52 T1 AR 0.005 µg/l U 001

PCB BZ#101 T1 AR 0.005 µg/l U 001

PCB BZ#118 T16 AR 0.005 µg/l U 001

PCB BZ#138 T1 AR 0.005 µg/l U 001



679268-1


PCB BZ#153 T1 AR 0.005 µg/l U 001

PCB BZ#180 T1 AR 0.005 µg/l U 001

Benzene T54 AR 1 µg/l U 001

Methyl tert-Butyl Ether T54 AR 1 µg/l U 001















Dichlorodifluoromethane T54 AR 1 µg/l U 001

Chloromethane T54 AR 1 µg/l U 001

Vinyl chloride T54 AR 1 µg/l U 001

Bromomethane T54 AR 1 µg/l U 001

Chloroethane T54 AR 1 µg/l U 001

Trichlorofluoromethane T54 AR 1 µg/l U 001

1,1-Dichloroethylene T54 AR 1 µg/l U 001

Dichloromethane T54 AR 50 µg/l N 001

Trans-1,2-Dichloroethene T54 AR 1 µg/l U 001


Cis-1,2-Dichloroethylene T54 AR 1 µg/l U 001


Chloroform T54 AR 1 µg/l U 001

Bromochloromethane T54 AR 1 µg/l U 001


1,1-Dichloropropene T54 AR 1 µg/l U 001

Carbon tetrachloride T54 AR 1 µg/l U 001



1,1,2-Trichloroethylene T54 AR 1 µg/l U 001

Bromodichloromethane T54 AR 1 µg/l U 001

Dibromomethane T54 AR 1 µg/l U 001

Cis-1,3-Dichloropropene T54 AR 1 µg/l U 001

Toluene T54 AR 1 µg/l U 001

Trans-1,3-Dichloropropene T54 AR 1 µg/l U 001



Tetrachloroethene T54 AR 1 µg/l U 001

Chlorodibromomethane T54 AR 1 µg/l U 001

1,2-dibromoethane T54 AR 1 µg/l U 001

Chlorobenzene T54 AR 1 µg/l U 001


EthylBenzene T54 AR 1 µg/l U 001

M/P Xylene T54 AR 1 µg/l U 001

O Xylene T54 AR 1 µg/l U 001

Styrene T54 AR 1 µg/l U 001

Bromoform T54 AR 1 µg/l U 001

Isopropyl benzene T54 AR 1 µg/l U 001


1,2,3-Trichloropropane T54 AR 1 µg/l U 001

n-Propylbenzene T54 AR 1 µg/l U 001

Bromobenzene T54 AR 1 µg/l U 001


T-Butylbenzene T54 AR 1 µg/l U 001


S-Butylbenzene T54 AR 1 µg/l U 001

p-Isopropyltoluene T54 AR 1 µg/l U 001








679268-1


Phenol T16 AR 10 µg/l U 001

Bis (2-chloroethyl) ether T16 AR 10 µg/l U 001

2-Chlorophenol T16 AR 10 µg/l U 001




Bis (2-chloroisopropyl) ether T16 AR 10 µg/l U 001

2-methyl phenol T16 AR 10 µg/l U 001

3/4-Methylphenol T16 AR 10 µg/l U 001

Hexachloroethane T16 AR 10 µg/l U 001

Nitrobenzene T16 AR 10 µg/l U 001

Isophorone T16 AR 10 µg/l U 001

2-Nitrophenol T16 AR 10 µg/l U 001

2,4-Dimethylphenol T16 AR 10 µg/l U 001

Bis (2-chloroethoxy) methane T16 AR 10 µg/l U 001

2,4-Dichlorophenol T16 AR 10 µg/l U 001

1,2,4-Trichlorobenzene T16 AR 10 µg/l U 001

4-Chloroaniline T16 AR 10 µg/l U 001

Hexachlorobutadiene T16 AR 10 µg/l U 001

4-Chloro-3-methylphenol T16 AR 10 µg/l U 001

2-Methylnaphthalene T16 AR 10 µg/l U 001

Hexachlorocyclopentadiene T16 AR 10 µg/l U 001



2-Chloronaphthalene T16 AR 10 µg/l U 001


Dimethyl phthalate T16 AR 10 µg/l U 001



Dibenzofuran T16 AR 10 µg/l U 001


Diethyl phthalate T16 AR 10 µg/l U 001

4-Chlorophenyl phenylether T16 AR 10 µg/l U 001


Azobenzene T16 AR 10 µg/l U 001

4-Bromophenyl phenylether T16 AR 10 µg/l U 001

Hexachlorobenzene T16 AR 10 µg/l U 001

Pentachlorophenol T16 AR 10 µg/l U 001

Carbazole T16 AR 10 µg/l U 001

Di-n-butylphthalate T16 AR 10 µg/l U 001

Butyl benzylphthalate T16 AR 10 µg/l U 001

Bis (2-ethylhexyl)phthalate T16 AR 10 µg/l U 001

Di-n-octylphthalate T16 AR 10 µg/l U 001

Bentazone T310 AR 0.1 µg/l N 001

Diuron T569 AR 0.1 µg/l N 001

Isoproturon T569 AR 0.1 µg/l N 001

Linuron T569 AR 0.1 µg/l N 001

Mecoprop T16 AR 0.1 µg/l N 001

2,4,6-Trichlorophenol T826 AR 0.1 µg/l N 001

2-Phenylphenol T826 AR 0.1 µg/l N 001

Acetochlor T826 AR 0.1 µg/l N 001

Aclonifen T826 AR 0.1 µg/l N 001

Acrinathrin T826 AR 0.1 µg/l N 001

Alachlor T826 AR 0.1 µg/l N 001

Aldrin T826 AR 0.1 µg/l N 001

Ametryn T826 AR 0.1 µg/l N 001

Atraton T826 AR 0.1 µg/l N 001

Atrazine T826 AR 0.1 µg/l N 001

Azaconazole T826 AR 0.1 µg/l N 001

Azobenzene T826 AR 0.1 µg/l N 001

Azoxystrobin T826 AR 0.1 µg/l N 001

Benalaxyl T826 AR 0.1 µg/l N 001

Benfluralin T826 AR 0.1 µg/l N 001

Bifenox T826 AR 0.1 µg/l N 001

Bifenthrin T826 AR 0.1 µg/l N 001

Binapacryl T826 AR 0.1 µg/l N 001

Biphenyl T826 AR 0.1 µg/l N 001

Bitertanol T826 AR 0.1 µg/l N 001

Boscalid T826 AR 0.1 µg/l N 001

Bromacil T826 AR 0.1 µg/l N 001



679268-1


Bromophos T826 AR 0.1 µg/l N 001

Bromophos-Ethyl T826 AR 0.1 µg/l N 001

Bromopropylate T826 AR 0.1 µg/l N 001

Bupirimate T826 AR 0.1 µg/l N 001

Buprofezine T826 AR 0.1 µg/l N 001

Butachlor T826 AR 0.1 µg/l N 001

Cadusafos T826 AR 0.1 µg/l N 001

Carbaryl T826 AR 0.1 µg/l N 001

Carbophenothion T826 AR 0.1 µg/l N 001

Carboxine T826 AR 0.1 µg/l N 001

Carfentrazone Ethyl T826 AR 0.1 µg/l N 001

Chlorbenzilate T826 AR 0.1 µg/l N 001

Chlordane T826 AR 0.1 µg/l N 001

Chlordimeform T826 AR 0.1 µg/l N 001

Chlorethoxyfos T826 AR 0.1 µg/l N 001

Chlorfenapyr T826 AR 0.1 µg/l N 001

Chlorfenvinphos T826 AR 0.1 µg/l N 001

Chlormephos T826 AR 0.1 µg/l N 001

Chloropropylate T826 AR 0.1 µg/l N 001

Chlorothalonil T826 AR 0.1 µg/l N 001

Chlorpropham T826 AR 0.1 µg/l N 001

Chlorpyrifos T826 AR 0.1 µg/l N 001

Chlorpyrifos methyl T826 AR 0.1 µg/l N 001

Chlorthal Dimethyl T826 AR 0.1 µg/l N 001

Chlorthion T826 AR 0.1 µg/l N 001

Chlorthiophos T826 AR 0.1 µg/l N 001

Chlozolinate T826 AR 0.1 µg/l N 001

Clodinafop propargy T826 AR 0.1 µg/l N 001

Clomazone T826 AR 0.1 µg/l N 001

Cloquintocet mexyl T826 AR 0.1 µg/l N 001

Coumaphos T826 AR 0.1 µg/l N 001

Cyflufenamid T826 AR 0.1 µg/l N 001

Cyfluthrin T826 AR 0.1 µg/l N 001

Cypermethrin T826 AR 0.1 µg/l N 001

Cyphenothrin T826 AR 0.1 µg/l N 001

Cyproconazole T826 AR 0.1 µg/l N 001

Cyprodinil T826 AR 0.1 µg/l N 001

Deltamethrin T826 AR 0.1 µg/l N 001

Desmetryn T826 AR 0.1 µg/l N 001

Diafenthiuron T826 AR 0.1 µg/l N 001

Dialifos T826 AR 0.1 µg/l N 001

Diazinon T826 AR 0.1 µg/l N 001

Dichlobenil T826 AR 0.1 µg/l N 001

Dichlofenthion T826 AR 0.1 µg/l N 001

Dichlorvos T826 AR 0.1 µg/l N 001

Diclobutrazol T826 AR 0.1 µg/l N 001

Dicloran T826 AR 0.1 µg/l N 001

Dicofol T826 AR 0.1 µg/l N 001

Dieldrin T826 AR 0.1 µg/l N 001

Difenoconazole T826 AR 0.1 µg/l N 001

Diflufenican T826 AR 0.1 µg/l N 001

Dimethenamid T826 AR 0.1 µg/l N 001

Dimethomorph T826 AR 0.1 µg/l N 001

Dimoxystrobin T826 AR 0.1 µg/l N 001

Dioxabenzofos T826 AR 0.1 µg/l N 001

Diphenamid T826 AR 0.1 µg/l N 001

Diphenylamine T826 AR 0.1 µg/l N 001

Disulfoton T826 AR 0.1 µg/l N 001

Ditalimfos T826 AR 0.1 µg/l N 001

Edifenphos T826 AR 0.1 µg/l N 001

Endosulphan alpha T826 AR 0.1 µg/l N 001

Endosulphan beta T826 AR 0.1 µg/l N 001

Endosulphan sulphate T826 AR 0.1 µg/l N 001

Endrin T826 AR 0.1 µg/l N 001

Epn T826 AR 0.1 µg/l N 001

Epoxiconazole T826 AR 0.1 µg/l N 001

EPTC T826 AR 0.1 µg/l N 001

Etaconazole T826 AR 0.1 µg/l N 001

Ethion T826 AR 0.1 µg/l N 001

Ethofumesate T826 AR 0.1 µg/l N 001



679268-1


Ethoprophos T826 AR 0.1 µg/l N 001

Ethoxyquin T826 AR 0.1 µg/l N 001

Etofenprox T826 AR 0.1 µg/l N 001

Etoxazole T826 AR 0.1 µg/l N 001

Etridiazole T826 AR 0.1 µg/l N 001

Etrimfos T826 AR 0.1 µg/l N 001

Famoxadone T826 AR 0.1 µg/l N 001

Famphur T826 AR 0.1 µg/l N 001

Fenamidone T826 AR 0.1 µg/l N 001

Fenamiphos T826 AR 0.1 µg/l N 001

Fenarimol T826 AR 0.1 µg/l N 001

Fenbuconazole T826 AR 0.1 µg/l N 001

Fenchlorphos T826 AR 0.1 µg/l N 001

Fenitrothion T826 AR 0.1 µg/l N 001

Fenpiclonil T826 AR 0.1 µg/l N 001

Fenpropathrin T826 AR 0.1 µg/l N 001

Fenpropimorph T826 AR 0.1 µg/l N 001

Fenson T826 AR 0.1 µg/l N 001

Fensulfothion T826 AR 0.1 µg/l N 001

Fenthion T826 AR 0.1 µg/l N 001

Fenvalerate T826 AR 0.1 µg/l N 001

Fipronil T826 AR 0.1 µg/l N 001

Fipronil sulphone T826 AR 0.1 µg/l N 001

Flamprop isopropyl T826 AR 0.1 µg/l N 001

Fluazifop-P-Butyl T826 AR 0.1 µg/l N 001

Flucythrinate T826 AR 0.1 µg/l N 001

Fludioxonil T826 AR 0.1 µg/l N 001

Flufenacet T826 AR 0.1 µg/l N 001

Flumetralin T826 AR 0.1 µg/l N 001

Flumioxazin T826 AR 0.1 µg/l N 001

Flumorph T826 AR 0.1 µg/l N 001

Fluopyram T826 AR 0.1 µg/l N 001

Fluquinconazole T826 AR 0.1 µg/l N 001

Fluroxypyr-1-methylheptyl ester T826 AR 0.1 µg/l N 001

Flusilazole T826 AR 0.1 µg/l N 001

Flutolanil T826 AR 0.1 µg/l N 001

Fluxapyroxad T826 AR 0.1 µg/l N 001

Fonophos T826 AR 0.1 µg/l N 001

Formothion T826 AR 0.1 µg/l N 001

Furalaxyl T826 AR 0.1 µg/l N 001

Haloxyfop etotyl T826 AR 0.1 µg/l N 001

Haloxyfop Methyl T826 AR 0.1 µg/l N 001

Heptachlor T826 AR 0.1 µg/l N 001

Heptachlor epoxide T826 AR 0.1 µg/l N 001

Heptachlor exo Epoxide T826 AR 0.1 µg/l N 001

Heptenophos T826 AR 0.1 µg/l N 001

Hexachlorobenzene T826 AR 0.1 µg/l N 001

Hexachlorocyclohexane (alpha) T826 AR 0.1 µg/l N 001

Hexachlorocyclohexane (beta) T826 AR 0.1 µg/l N 001

Hexachlorocyclohexane (delta) T826 AR 0.1 µg/l N 001

Hexaconazole T826 AR 0.1 µg/l N 001

Hexazinone T826 AR 0.1 µg/l N 001

Iodofenphos T826 AR 0.1 µg/l N 001

Iprodione T826 AR 0.1 µg/l N 001

Isazofos T826 AR 0.1 µg/l N 001

Isocarbophos T826 AR 0.1 µg/l N 001

Isodrin T826 AR 0.1 µg/l N 001

Isofenphos T826 AR 0.1 µg/l N 001

Isofenphos Methyl T826 AR 0.1 µg/l N 001

Isomethiozin T826 AR 0.1 µg/l N 001

Isoprothiolane T826 AR 0.1 µg/l N 001

Isopyrazam T826 AR 0.1 µg/l N 001

Kresoxim Methyl T826 AR 0.1 µg/l N 001

Lambda Cyhalothrin T826 AR 0.1 µg/l N 001

Lenacil T826 AR 0.1 µg/l N 001

Leptophos T826 AR 0.1 µg/l N 001

Lindane T826 AR 0.1 µg/l N 001

Malathion T826 AR 0.1 µg/l N 001

MCPA-thioethyl T826 AR 0.1 µg/l N 001

Mecarbam T826 AR 0.1 µg/l N 001



679268-1


Mepanipyrim T826 AR 0.1 µg/l N 001

Mephosfolan T826 AR 0.1 µg/l N 001

Mepronil T826 AR 0.1 µg/l N 001

Metalaxyl T826 AR 0.1 µg/l N 001

Metazachlor T826 AR 0.1 µg/l N 001

Methacrifos T826 AR 0.1 µg/l N 001

Methidathion T826 AR 0.1 µg/l N 001

Methoxychlor T826 AR 0.1 µg/l N 001

Methyl Paraoxon T826 AR 0.1 µg/l N 001

Metolachlor T826 AR 0.1 µg/l N 001

Metolcarb T826 AR 0.1 µg/l N 001

Metrafenone T826 AR 0.1 µg/l N 001

Metribuzin T826 AR 0.1 µg/l N 001

Mevinphos T826 AR 0.1 µg/l N 001

Mirex T826 AR 0.1 µg/l N 001

Molinate T826 AR 0.1 µg/l N 001

Myclobutanil T826 AR 0.1 µg/l N 001

Napropamide T826 AR 0.1 µg/l N 001

Nitrofen T826 AR 0.1 µg/l N 001

Nitrothal isopropyl T826 AR 0.1 µg/l N 001

Nuarimol T826 AR 0.1 µg/l N 001

o,p'-DDT T826 AR 0.1 µg/l N 001

o,p-DDD T826 AR 0.1 µg/l N 001

o,p-DDE T826 AR 0.1 µg/l N 001

Octylisothiazolon T826 AR 0.1 µg/l N 001

Ofurace T826 AR 0.1 µg/l N 001

Orysastrobin T826 AR 0.1 µg/l N 001

Oxadiazon T826 AR 0.1 µg/l N 001

Oxadixyl T826 AR 0.1 µg/l N 001

Oxyfluorfen T826 AR 0.1 µg/l N 001

p,p-DDD T826 AR 0.1 µg/l N 001

p,p-DDE T826 AR 0.1 µg/l N 001

p,p-DDT T826 AR 0.1 µg/l N 001

Paclobutrazol T826 AR 0.1 µg/l N 001

Paraoxon T826 AR 0.1 µg/l N 001

Parathion T826 AR 0.1 µg/l N 001

Parathion methyl T826 AR 0.1 µg/l N 001

Penconazole T826 AR 0.1 µg/l N 001

Pendimethalin T826 AR 0.1 µg/l N 001

Pentachloroaniline T826 AR 0.1 µg/l N 001

Pentachlorophenol T826 AR 0.1 µg/l N 001

Pentanochlor T826 AR 0.1 µg/l N 001

Permethrin T826 AR 0.1 µg/l N 001

Pethoxamid T826 AR 0.1 µg/l N 001

Phenothrin T826 AR 0.1 µg/l N 001

Phenthoate T826 AR 0.1 µg/l N 001

Phorate T826 AR 0.1 µg/l N 001

Phosalone T826 AR 0.1 µg/l N 001

Phosfolan T826 AR 0.1 µg/l N 001

Picoxystrobin T826 AR 0.1 µg/l N 001

Piperonyl Butoxide T826 AR 0.1 µg/l N 001

Pirimicarb T826 AR 0.1 µg/l N 001

Pirimiphos Ethyl T826 AR 0.1 µg/l N 001

Pirimiphos methyl T826 AR 0.1 µg/l N 001

Pretilachlor T826 AR 0.1 µg/l N 001

Procymidone T826 AR 0.1 µg/l N 001

Profenofos T826 AR 0.1 µg/l N 001

Prometon T826 AR 0.1 µg/l N 001

Prometryn T826 AR 0.1 µg/l N 001

Propachlor T826 AR 0.1 µg/l N 001

Propanil T826 AR 0.1 µg/l N 001

Propaphos T826 AR 0.1 µg/l N 001

Propargite T826 AR 0.1 µg/l N 001

Propazine T826 AR 0.1 µg/l N 001

Propetamphos T826 AR 0.1 µg/l N 001

Propham T826 AR 0.1 µg/l N 001

Propiconazole T826 AR 0.1 µg/l N 001

Propyzamide T826 AR 0.1 µg/l N 001

Proquinazid T826 AR 0.1 µg/l N 001

Prosulfocarb T826 AR 0.1 µg/l N 001



679268-1


Prothiofos T826 AR 0.1 µg/l N 001

Pyraclostrobin T826 AR 0.1 µg/l N 001

Pyraflufen ethyl T826 AR 0.1 µg/l N 001

Pyrazophos T826 AR 0.1 µg/l N 001

Pyridaben T826 AR 0.1 µg/l N 001

Pyridaphenthion T826 AR 0.1 µg/l N 001

Pyrimethanil T826 AR 0.1 µg/l N 001

Pyriproxyfen T826 AR 0.1 µg/l N 001

Quinalphos T826 AR 0.1 µg/l N 001

Quinoxyfen T826 AR 0.1 µg/l N 001

Quintozene T826 AR 0.1 µg/l N 001

Quizalofop-ethyl T826 AR 0.1 µg/l N 001

Secbumeton T826 AR 0.1 µg/l N 001

Silafluofen T826 AR 0.1 µg/l N 001

Simazine T826 AR 0.1 µg/l N 001

Simeconazole T826 AR 0.1 µg/l N 001

Sulfallate T826 AR 0.1 µg/l N 001

Sulprofos T826 AR 0.1 µg/l N 001

Tebuconazole T826 AR 0.1 µg/l N 001

Tebufenpyrad T826 AR 0.1 µg/l N 001

Tebupirimiphos T826 AR 0.1 µg/l N 001

Tecnazene T826 AR 0.1 µg/l N 001

Tefluthrin T826 AR 0.1 µg/l N 001

Terbacil T826 AR 0.1 µg/l N 001

Terbufos T826 AR 0.1 µg/l N 001

Terbumeton T826 AR 0.1 µg/l N 001

Terbuthylazine T826 AR 0.1 µg/l N 001

Terbutryn T826 AR 0.1 µg/l N 001

Tetrachlorvinphos T826 AR 0.1 µg/l N 001

Tetraconazole T826 AR 0.1 µg/l N 001

Tetradifon T826 AR 0.1 µg/l N 001

sulfotep T826 AR 0.1 µg/l N 001

Tetramethrin T826 AR 0.1 µg/l N 001

Tetrasul T826 AR 0.1 µg/l N 001

Thiamethoxam T826 AR 0.1 µg/l N 001

Thiobencarb T826 AR 0.1 µg/l N 001

Tolclofos methyl T826 AR 0.1 µg/l N 001

Triadimefon T826 AR 0.1 µg/l N 001

Triadimenol T826 AR 0.1 µg/l N 001

Triallate T826 AR 0.1 µg/l N 001

Triazamate T826 AR 0.1 µg/l N 001

Triazophos T826 AR 0.1 µg/l N 001

Trifloxystrobin T826 AR 0.1 µg/l N 001

Triflumizole T826 AR 0.1 µg/l N 001

Trifluralin T826 AR 0.1 µg/l N 001

Vinclozolin T826 AR 0.1 µg/l N 001

Vinclozolin metabolite 3,5-Dichloroaniline T826 AR 0.1 µg/l N 001



679268-1

APPENDIX 5

PHOTOGRAPHS

Figure A5.1

Photographs of Rock Core

Western Link

Core Photographs BH07

Contract No. 42103

Western Link

Core Photographs BH10

Contract No. 42103

Western Link

Core Photographs BH12A

Contract No. 42103

Figure A5.2

Photographs of MOSTAP Samples

Western Link

MOSTAP Sampler Photographs CPT01A

Contract No. 42103

0.00m

1.00m

Western Link


Contract No. 42103

Western Link Warrington

42103


Mott Macdonald

17th July 2017

CPT01A

MOSTAP SAMPLE B

1.70m

2.20m

Western Link


Contract No. 42103


42103


Mott Macdonald

17th July 2017

CPT01A

MOSTAP SAMPLE C

2.40m

3.40m

Western Link


Contract No. 42103


42103


Mott Macdonald

17th July 2017

CPT01A

MOSTAP SAMPLE D

3.60m

4.60m

Western Link


Contract No. 42103

Western Link


Contract No. 42103


42103


Mott Macdonald

18th July 2017

CPT3A

MOSTAP SAMPLE D

3.60m

4.60m

Western Link

MOSTAP Sampler Photographs

CPT14

Contract No. 42103

Western Link


Contract No. 42103

APPENDIX 6

MONITORING

O2% CO2% CH4% CO H2S

v/v v/v v/v ppm ppm

Hole No:VOC ppm

CO2% v/v

H2S ppm

RelPressure

(mb)

Gas flow Rate (l/hr)

Depth to base of

well SWL

LNAPL or

DNAPL

Steady Steady Peak Steady Steady Steady Range mBGL mBGL mBGL

BH05A 0.0 15.6 61.9 52.5 0 3.29 0.1 7.40 1.88 NDBH06A 0.0 3.0 0.0 0.0 0 3.29 0.2 5.15 1.73 NDBH10 0.0 0.0 0.2 0.1 0 3.23 0.4 4.43 2.00 NDCPT14A 0.0 7.3 29.5 20.3 0 2.10 -0.1 5.00 5.00 NDCPT15A 0.0 0.3 0.0 0.0 0 0.01 -0.1 6.28 5.43 ND

>>>> = Flow above detection limit of 30 l/hr, <<< = Negative flow greater than -10 l/hr. >Max = In excess of lower explosive limit.

Remarks: BH03 - unable to take readings as top of well flooded.

20.5 0

CH4% v/v

1.3 0

O2% v/v

CO ppm

Steady Steady

113.5 25.4

19.6 0

Background Ground Conditions (dry / wet etc):

Readings: Atmospheric Pressure (Start):

Time (Start): NR Time (Finish):

Atmospheric Pressure (Finish):

Wet1001mb1001mb

NR0.020.9 0.0 0.0 0.0

Date: 28th July 2017Weather Conditions:

Checked By: MHWDry, overcast

Contract Name: Western LinkContract Number: 42103

Gas and Groundwater Monitoring Results

Gas Monitor: GA2000Readings Taken By: BL


v/v v/v v/v ppm ppm

Hole No:VOC ppm

CO2% v/v

H2S ppm

RelPressure

(mb)


Depth to base of

well SWL

LNAPL or

DNAPL


BH03 0.0 0.0 0.0 0.0 0 5.97 0.1 11.50 2.02 NDBH04A 0.0 0.0 0.0 0.0 0 0.21 0.0 11.65 3.12 NDBH05A 0.0 0.0 0.2 0.1 0 3.23 0.4 4.43 2.00 NDBH0 6A 0.0 2.7 0.0 0.0 0 -0.05 0.0 5.20 2.17 NDBH07 0.0 2.6 5.1 5.0 0 0.05 0.0 30.25 9.30 NDBH10


Remarks: BH12A was inaccessible.

Unable to locate 5



Damp1026mb

19.6 0

O2% v/v

CH4% v/v

CO ppm

15.2 017.6

Steady

19.8 016.9 2

Contract Number: 42103

Date: 10th August 2017Weather Conditions:

Checked By:

Time (Start): 09.50 Time (Finish):

Atmospheric Pressure (Finish): 1026mb12:00

Steady


Gas Monitor: GA5000Contract Name: Western Link Readings Taken By: DM

MHWCloudy, breezy, dry 19 ⁰C

21.1 0.0 0.0 0.00.0


v/v v/v v/v ppm ppm

Hole No:VOC ppm

CO2% v/v

H2S ppm

RelPressure

(mb)


Depth to base of

well SWL

LNAPL or

DNAPL


BH03 0.0 0.0 0.0 0.0 0 7.50 -1.3 10.50 4.34 NDBH04A 0.0 0.1 0.0 0.0 0 0.07 0.0 11.38 3.02 NDBH05A 0.0 0.0 0.2 0.1 0 3.23 0.4 7.36 1.88 NDBH06A 0.0 1.6 0.0 0.0 0 0.55 0.0 5.12 2.14 NDBH07 0.0 0.8 0.9 0.7 0 0.05 0.0 30.40 9.46 NDBH10BH12A 0.0 13.5 0.1 0.1 0 0.09 0.0 5.40 3.28 ND


Remarks:

Unable to locate 2.7 0

0.0

0

20.3 0

O2% v/v

CH4% v/v

CO ppm

21.1 0



Dry1013

20.2 0

Time (Start): 07:00 Time (Finish):


Steady Steady

16.8 019.6



Gas Monitor: GA5000

0.0101410:00

Contract Name: Western Link Readings Taken By: DMDate: 24th August 2017

Weather Conditions:

Checked By: MHWDull, mild, dry15-18⁰C

21.2 0.0 0.0


v/v v/v v/v ppm ppm

Hole No:VOC ppm

CO2% v/v

H2S ppm

RelPressure

(mb)


Depth to base of

well SWL

LNAPL or

DNAPL

Steady Steady Peak Steady Steady Steady Steady mBGL mBGL mBGL

BH03 0.0 0.1 0.0 0.0 0 0.67 0.1 10.55 0.44 NDBH04A 0.0 0.1 0.0 0.0 0 0.22 0.0 11.24 3.73 NDBH05A 0.0 0.0 0.2 0.1 0 3.23 0.4 4.43 2.00 NDBH06A 0.0 1.8 0.0 0.0 0 0.05 0.0 5.17 2.62 NDBH07 0.0 2.1 1.0 0.9 0 0.00 0.0 30.13 9.57 NDBH10 0.0 2.7 0.0 0.0 0 0.14 0.0 4.38 2.30 NDBH12A 0.0 0.9 0.0 0.0 0 -0.03 0.0 5.38 3.32 ND


Remarks:

O2% v/v

CH4% v/v

CO ppm

20.4 0

18.1 021.1

0.0

09.5 0

21.0 019.6 0



Steady Steady

20.7 0



Wet1016mb



Gas Monitor: GA5000

01014mb12:00

Contract Name: Western Link Readings Taken By: DMDate: 31st August 2017

Weather Conditions:

Checked By: HHDull/rain

21.4 0.0 0


v/v v/v v/v ppm ppm

Hole No:VOC ppm

CO2% v/v

H2S ppm

RelPressure

(mb)


Depth to base of

well SWL

LNAPL or

DNAPL


BH03 0.0 18.9 0.0 0.0 0 -6.04 -0.7 10.62 0.88 NDBH04 0.0 0.1 0.0 0.0 0 0.17 0.0 11.22 3.00 NDBH05 0.0 0.2 0.0 0.0 0 1.21 -0.3 7.38 1.84 NDBH06 0.0 3.5 0.0 0.0 0 0.79 0.0 5.20 2.35 NDBH07 0.0 7.5 2.1 2.1 0 0.39 0.0 30.20 9.66 NDBH10 0.0 0.3 0.0 0.0 0 0.12 0.0 4.35 2.18 NDBH12 0.0 3.1 0.0 0.0 0 -0.05 0.0 5.40 3.30 ND


Remarks: Borehole's 03,04,05,06,07 results taken 07.09.17. Borehole 10 & 12 taken 08.09.17.

O2% v/v

CH4% v/v

CO ppm

14.5 0

10.8 015.5

0.0

320.4 0

21.0 020.5 0

Time (Start): 14.00 Time (Finish):


Steady Steady

0.0 0



Damp1012mb



Gas Monitor: GA5000

0.01012mb16:00

Contract Name: Western Link Readings Taken By: DMDate: 7th September 2017

Weather Conditions:

Checked By:

Dull, breezy, dry 14-17 c

21.0 0.0 0.0


v/v v/v v/v ppm ppm

Hole No:VOC ppm

CO2% v/v

H2S ppm

RelPressure

(mb)


Depth to base of

well SWL

LNAPL or

DNAPL


BH03 0.0 0.0 0.0 0.0 0 11.50 -1.9 10.60 0.87 NDBH04A 0.0 0.1 0.0 0.0 0 0.15 0.0 11.24 2.87 NDBH05A 0.0 0.2 0.2 0.2 0 0.09 0.0 7.38 4.73 NDBH06A 0.0 1.3 0.0 0.0 0 0.29 0.0 5.03 1.92 NDBH07 0.0 10.2 2.3 2.3 0 0.14 0.0 3.02 9.35 NDBH10 0.0 0.1 0.1 0.1 0 -0.12 0.0 4.32 1.85 NDBH12A 0.0 0.1 0.0 0.0 0 -0.70 0.0 5.41 3.24 ND


Remarks:

200

0002

Date: 14th September 2017 Checked By:

Weather Conditions:

Steady

O2% v/v

CH4% v/v

CO ppm

Contract Name: Western Link Readings Taken By:GA5000DM

Contract Number: 42103 Gas Monitor:

21.3 0.0 0.0 0


HH

0

19.5





Dull and Brezzey

Wet1009mb1008mb

15:00

13.013.412.920.3

20.9

Steady

18.5

Base of Well

SWL pHRedox

Potential Dissolved Oxygen

Electrical Conductivity

mBGL mBGL mV ppm µs/cm

BH03 11.50 2.02 9.66 91.2 5.65 9.61BH04A 11.65 3.12 10.69 85.4 6.31 14.38BH05A 7.37 1.88 7.63 9.9 3.97 21.39BH6A 5.20 2.17 8.33 188.8 3.80 12.00BH07 30.25 9.30 7.98 200.8 4.03 22.97BH10 4.32 4.32 8.24 163.1 4.02 10.87

Remarks:

Groundwater Monitoring Results

Contract Number: 42103Contract Name: Western Link

Date: 10th August 2017Weather Conditions: Cloudy, breezy and dry

Borehole Number

Temperature

Steady

13.613.314.5

13.811.615.7

Checked By: MHW

Readings Taken By: DM

Base of Well

SWL pHRedox



mBGL mBGL mV ppm µs/cm

BH12A 5.40 3.28 9.21 189 4.9 1425

0000

Remarks:



Date: 10th August 2017Weather Conditions: Dull, mild, dry 15-18⁰C

Borehole Number

Temperature

Steady

17.3


Checked By: MHW

Base of Well

SWL pHRedox



mBGL mBGL mv ppm μs/cm

BH05A 7.36 1.88 7.55 55.5 6.03 300BH07 30.13 9.57 6.89 -64.3 4.22 1679BH10 4.38 2.30 6.70 -57.7 4.84 1730

Remarks:



Date: 31st August 2017Weather Conditions:

Borehole Number

Temperature

Steady

14.911.515.3


Checked By: MHW

Mott MacDonald | Western Link

50

Ground Investigation Report

382900-WL-MMD-07-ZZ-RP-N-0002 | 20 October 2017 https://mottmac.sharepoint.com/teams/pj-b1092/Shared Documents/12 - Geotechnics/Reports/Documents/382900-WL-MMD-07-ZZ-RP-N-0002 GIR.docx

F. HazWaste Online report

www.hazwasteonline.com CHABL-27J58-NKP2U Page 1 of 89

Waste Classification Report

CHABL-27J58-NKP2U

Job name

Western Link

Description/Comments

Project

Site

Waste Stream Template

Comprehesive Waste Stream - TEMPLATE

Classified by

Name:Louis McGgovernDate:07/09/2017 14:01:32 UTCTelephone:01223 463500

Company:Mott MacDonaldSpring Bank House33 Stamford StreetAltrinchamWA14 1ES

Report

Created by: Louis McGgovernCreated date: 07/09/2017 14:01 UTC

Job summary# Sample Name Depth [m] Classification Result Hazard properties Page1 BH7 Potentially Hazardous HP 3(i) 3

2 BH12A ES4 Potentially Hazardous HP 3(i) 8



5 BH03 ES4 Non Hazardous 23

6 BH04 ES5 Hazardous HP 3(i), HP 7, HP 11 28

7 BH04 ES6 Potentially Hazardous HP 3(i) 33

8 BH04 Non Hazardous 38

9 CPT 01A Potentially Hazardous HP 3(i) 43

10 CPT 03A Non Hazardous 48


12 CPT 14A[1] Potentially Hazardous HP 3(i) 58





Report created by Louis McGgovern on 07/09/2017

Page 2 of 89 CHABL-27J58-NKP2U www.hazwasteonline.com

Appendices PageAppendix A: Classifier defined and non CLP determinands 83Appendix B: Rationale for selection of metal species 88Appendix C: Version 89



Classification of sample: BH7

Potentially Hazardous WasteClassified as 17 05 04 or 17 05 03 *

in the List of Waste

Sample details

Sample Name:BH7

LoW Code:Chapter: 17: Construction and Demolition Wastes (including excavated soil

from contaminated sites)Entry: 17 05 04 or 17 05 03 * (Soil and stones other than those

mentioned in 17 05 03 or Soil and stones containing hazardoussubstances)

Hazard properties (substances considered hazardous until shown otherwise)

HP 3(i): Flammable "flammable liquid waste: liquid waste having a flash point below 60°C or waste gas oil, diesel and light heating oilshaving a flash point > 55°C and <= 75°C"

Hazard Statements hit:

Flam. Liq. 3; H226 "Flammable liquid and vapour."

Because of determinand:

TPH (C6 to C40) petroleum group: (conc.: 0.019%)

Determinands

Moisture content: 0% No Moisture Correction applied (MC)

#Determinand

CLP

Not

e

User entered dataConv.Factor

Compound conc.Classification

value

MC

App

lied

Conc. NotUsed

CLP index number EC Number CAS Number

1acenaphthene

0.3 mg/kg 0.3 mg/kg 0.00003 % 201-469-6 83-32-9

2acenaphthylene

0.4 mg/kg 0.4 mg/kg 0.00004 % 205-917-1 208-96-8

3anthracene

0.4 mg/kg 0.4 mg/kg 0.00004 % 204-371-1 120-12-7

4

antimony { antimony compounds, with the exception ofthe tetroxide (Sb2O4), pentoxide (Sb2O5), trisulphide(Sb2S3), pentasulphide (Sb2S5) and those specifiedelsewhere in this Annex }

1 <0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD

051-003-00-9

5arsenic { arsenic trioxide }

64 mg/kg 1.32 84.501 mg/kg 0.00845 %033-003-00-0 215-481-4 1327-53-3

6benzene

<10 mg/kg <10 mg/kg <0.001 % <LOD601-020-00-8 200-753-7 71-43-2

7benzo[a]anthracene

0.8 mg/kg 0.8 mg/kg 0.00008 %601-033-00-9 200-280-6 56-55-3

8benzo[a]pyrene; benzo[def]chrysene

1.1 mg/kg 1.1 mg/kg 0.00011 %601-032-00-3 200-028-5 50-32-8

9benzo[b]fluoranthene

0.9 mg/kg 0.9 mg/kg 0.00009 %601-034-00-4 205-911-9 205-99-2

10benzo[ghi]perylene

0.9 mg/kg 0.9 mg/kg 0.00009 % 205-883-8 191-24-2

11benzo[k]fluoranthene

0.8 mg/kg 0.8 mg/kg 0.00008 %601-036-00-5 205-916-6 207-08-9



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed


12beryllium { beryllium oxide }

<0.1 mg/kg 2.775 <0.278 mg/kg <0.0000278 % <LOD004-003-00-8 215-133-1 1304-56-9

13

boron { boron tribromide/trichloride/trifluoride(combined) }

<1 mg/kg 13.43 <13.43 mg/kg <0.00134 % <LOD 10294-33-4,10294-34-5,7637-07-2

14cadmium { cadmium sulfide }

1 6 mg/kg 1.285 7.711 mg/kg 0.0006 %048-010-00-4 215-147-8 1306-23-6

15chromium in chromium(III) compounds { chromium(III)oxide } 96 mg/kg 1.462 140.309 mg/kg 0.014 %

215-160-9 1308-38-9

16chromium in chromium(VI) compounds { chromium(VI)oxide } <0.1 mg/kg 1.923 <0.192 mg/kg <0.0000192 % <LOD

024-001-00-0 215-607-8 1333-82-0

17chrysene

0.9 mg/kg 0.9 mg/kg 0.00009 %601-048-00-0 205-923-4 218-01-9

18 copper { dicopper oxide; copper (I) oxide } 190 mg/kg 1.126 213.919 mg/kg 0.0214 %029-002-00-X 215-270-7 1317-39-1

19

cyanides { salts of hydrogen cyanide with theexception of complex cyanides such as ferrocyanides,ferricyanides and mercuric oxycyanide and thosespecified elsewhere in this Annex }

18 mg/kg 1.884 33.912 mg/kg 0.00339 %

006-007-00-5

20dibenz[a,h]anthracene

0.3 mg/kg 0.3 mg/kg 0.00003 %601-041-00-2 200-181-8 53-70-3

21

dichloroethane { 1,1-dichloroethane and1,2-dichloroethane (combined) } <0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD

203-458-1,200-863-5

107-06-2, 75-34-3

22

diesel petroleum group

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 68334-30-5,

68476-34-6,94114-59-7,1159170-26-9

23ethylbenzene

<10 mg/kg <10 mg/kg <0.001 % <LOD601-023-00-4 202-849-4 100-41-4

24fluoranthene

1.4 mg/kg 1.4 mg/kg 0.00014 % 205-912-4 206-44-0

25fluorene

0.2 mg/kg 0.2 mg/kg 0.00002 % 201-695-5 86-73-7

26indeno[123-cd]pyrene

0.8 mg/kg 0.8 mg/kg 0.00008 % 205-893-2 193-39-5

27lead { lead compounds with the exception of thosespecified elsewhere in this Annex } 1 230 mg/kg 230 mg/kg 0.023 %

082-001-00-6

28manganese { manganese sulphate }

<0.1 mg/kg 2.749 <0.275 mg/kg <0.0000275 % <LOD025-003-00-4 232-089-9 7785-87-7

29mercury { mercury dichloride }

3 mg/kg 1.353 4.06 mg/kg 0.000406 %080-010-00-X 231-299-8 7487-94-7

30molybdenum { molybdenum(VI) oxide }

<0.1 mg/kg 1.5 <0.15 mg/kg <0.000015 % <LOD042-001-00-9 215-204-7 1313-27-5

31naphthalene

0.6 mg/kg 0.6 mg/kg 0.00006 %601-052-00-2 202-049-5 91-20-3

32nickel { nickel dihydroxide }

31 mg/kg 1.579 48.964 mg/kg 0.0049 %028-008-00-X 235-008-5 [1]234-348-1 [2]

12054-48-7 [1]11113-74-9 [2]

33pH

7.2 pH 7.2 pH 7.2 pH PH

34phenanthrene

0.8 mg/kg 0.8 mg/kg 0.00008 % 201-581-5 85-01-8



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed


35phenol

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD604-001-00-2 203-632-7 108-95-2

36pyrene

1.2 mg/kg 1.2 mg/kg 0.00012 % 204-927-3 129-00-0

37

selenium { selenium compounds with the exception ofcadmium sulphoselenide and those specified elsewherein this Annex } <3 mg/kg 2.554 <7.661 mg/kg <0.000766 % <LOD

034-002-00-8

38tetrachloroethylene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-028-00-4 204-825-9 127-18-4

39carbon tetrachloride; tetrachloromethane

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-008-00-5 200-262-8 56-23-5

40toluene

<10 mg/kg <10 mg/kg <0.001 % <LOD601-021-00-3 203-625-9 108-88-3

41TPH (C6 to C40) petroleum group

190 mg/kg 190 mg/kg 0.019 % TPH

42trichloroethylene; trichloroethene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-027-00-9 201-167-4 79-01-6

43vinyl chloride; chloroethylene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-023-00-7 200-831-0 75-01-4

44

xylene

<10 mg/kg <10 mg/kg <0.001 % <LOD601-022-00-9 202-422-2 [1]

203-396-5 [2]203-576-3 [3]215-535-7 [4]

95-47-6 [1]106-42-3 [2]108-38-3 [3]1330-20-7 [4]

45zinc { zinc oxide }

1100 mg/kg 1.245 1369.185 mg/kg 0.137 %030-013-00-7 215-222-5 1314-13-2

46

DDT (ISO); clofenotane (INN); dicophane;1,1,1-trichloro-2,2-bis(4-chlorophenyl)ethane;dichlorodiphenyltrichloroethane <0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD

602-045-00-7 200-024-3 50-29-3

47

chlordane (ISO);1,2,4,5,6,7,8,8-octachloro-3a,4,7,7a-tetrahydro-4,7-methanoindan <0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD

602-047-00-8 200-349-0 57-74-9

48

hexachlorocyclohexanes, including lindane

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-043-00-6 210-168-9,

200-401-2,206-270-8,206-271-3

58-89-9, 319-84-6,319-85-7, 608-73-1

49dieldrin (ISO)

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-049-00-9 200-484-5 60-57-1

50

endrin (ISO);1,2,3,4,10,10-hexachloro-6,7-epoxy-1,4,4a,5,6,7,8,8a-octahydro-1,4:5,8-dimethanonaphthalene <0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD

602-051-00-X 200-775-7 72-20-8

51

heptachlor (ISO);1,4,5,6,7,8,8-heptachloro-3a,4,7,7a-tetrahydro-4,7-methanoindene <0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD

602-046-00-2 200-962-3 76-44-8

52hexachlorobenzene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-065-00-6 204-273-9 118-74-1

53

chlordecone (ISO);perchloropentacyclo[5,3,0,02,6,03,9,04,8]decan-5-one;decachloropentacyclo[5,2,1,02,6,03,9,05,8]decan-4-one <0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD

606-019-00-6 205-601-3 143-50-0

54aldrin (ISO)

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-048-00-3 206-215-8 309-00-2

55pentachlorobenzene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-074-00-5 210-172-0 608-93-5

56polychlorobiphenyls; PCB

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-039-00-4 215-648-1 1336-36-3



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed


57dodecachloropentacyclo[5.2.1.02,6.03,9.05,8]decane;mirex <0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD

602-077-00-1 219-196-6 2385-85-5

58camphechlor (ISO); toxaphene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-044-00-1 232-283-3 8001-35-2

59hexabromobiphenyl

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 252-994-2 36355-01-8

602,3,7,8-TeCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 217-122-7 1746-01-6

611,2,3,7,8-PeCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 40321-76-4

621,2,3,4,7,8-HxCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 39227-28-6

631,2,3,6,7,8-HxCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57653-85-7

641,2,3,7,8,9-HxCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 19408-74-3

651,2,3,4,6,7,8-HpCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 35822-46-9

66OCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 3268-87-9

672,3,7,8-TeCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 51207-31-9

681,2,3,7,8-PeCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57117-41-6

692,3,4,7,8-PeCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57117-31-4

701,2,3,4,7,8-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 70648-26-9

711,2,3,6,7,8-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57117-44-9

721,2,3,7,8,9-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 72918-21-9

732,3,4,6,7,8-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 60851-34-5

741,2,3,4,6,7,8-HpCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 67562-39-4

751,2,3,4,7,8,9-HpCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 55673-89-7

76OCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 39001-02-0

77pH: acid/alkali reserve

<0.1gNaOH

<0.1gNaOH

<0.1 gNaOH <LOD

78 barium { barium chromate } <0.1 mg/kg 1.845 <0.184 mg/kg <0.0000184 % <LOD 233-660-5 10294-40-3

79calcium { calcium chromate }

<0.1 mg/kg 3.894 <0.389 mg/kg <0.0000389 % <LOD024-008-00-9 237-366-8 13765-19-0

80cobalt { cobalt sulfate }

1 <0.1 mg/kg 2.63 <0.263 mg/kg <0.00001 % <LOD027-005-00-0 233-334-2 10124-43-3

81 iron { iron (III) oxide (worst case) } <0.1 mg/kg 1.43 <0.143 mg/kg <0.0000143 % <LOD 215-168-2 1309-37-1

82potassium { potassium chromate }

<0.1 mg/kg 2.483 <0.248 mg/kg <0.0000248 % <LOD024-006-00-8 232-140-5 7789-00-6

83silver { silver nitrate }

<0.1 mg/kg 1.575 <0.157 mg/kg <0.0000157 % <LOD047-001-00-2 231-853-9 7761-88-8

84sodium { sodium chromate }

<0.1 mg/kg 3.523 <0.352 mg/kg <0.0000352 % <LOD024-018-00-3 231-889-5 7775-11-3



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed


85thallium { thallium compounds, with the exception ofthose specified elsewhere in this Annex } <0.1 mg/kg 1.284 <0.128 mg/kg <0.0000128 % <LOD

081-002-00-9

86tin { tin(II) methanesulphonate }

<0.1 mg/kg 2.602 <0.26 mg/kg <0.000026 % <LOD050-018-00-8 401-640-7 53408-94-9

87vanadium { divanadium pentaoxide; vanadium pentoxide }

85 mg/kg 1.785 151.741 mg/kg 0.0152 %023-001-00-8 215-239-8 1314-62-1

881,2,4-trimethylbenzene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-043-00-3 202-436-9 95-63-6

89mesitylene; 1,3,5-trimethylbenzene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-025-00-5 203-604-4 108-67-8

90chloroform; trichloromethane

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-006-00-4 200-663-8 67-66-3

Total: 0.255 %

KeyUser supplied data

Determinand values ignored for classification, see column 'Conc. Not Used' for reason

Potentially Hazardous result

Determinand defined or amended by HazWasteOnline (see Appendix A)

Speciated Deteminand - Unless the Determinand is Note 1, the Conversion Factor is used to calculate the compoundconcentration

<LOD Below limit of detectionCLP: Note 1 Only the metal concentration has been used for classification



Classification of sample: BH12A ES4



Sample details

Sample Name:BH12A ES4










Determinands


#Determinand

CLP

Not

e



valueM

CA

pplie

dConc. Not

UsedCLP index number EC Number CAS Number

1acenaphthene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 201-469-6 83-32-9

2acenaphthylene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 205-917-1 208-96-8

3anthracene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 204-371-1 120-12-7

4


1 <0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD

051-003-00-9


150 mg/kg 1.32 198.049 mg/kg 0.0198 %033-003-00-0 215-481-4 1327-53-3

6benzene

<20 mg/kg <20 mg/kg <0.002 % <LOD601-020-00-8 200-753-7 71-43-2

7benzo[a]anthracene

0.3 mg/kg 0.3 mg/kg 0.00003 %601-033-00-9 200-280-6 56-55-3


0.3 mg/kg 0.3 mg/kg 0.00003 %601-032-00-3 200-028-5 50-32-8


0.3 mg/kg 0.3 mg/kg 0.00003 %601-034-00-4 205-911-9 205-99-2


0.2 mg/kg 0.2 mg/kg 0.00002 % 205-883-8 191-24-2


0.4 mg/kg 0.4 mg/kg 0.00004 %601-036-00-5 205-916-6 207-08-9



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed



<0.1 mg/kg 2.775 <0.278 mg/kg <0.0000278 % <LOD004-003-00-8 215-133-1 1304-56-9

13


<1 mg/kg 13.43 <13.43 mg/kg <0.00134 % <LOD 10294-33-4,10294-34-5,7637-07-2


1 1 mg/kg 1.285 1.285 mg/kg 0.0001 %048-010-00-4 215-147-8 1306-23-6


215-160-9 1308-38-9


024-001-00-0 215-607-8 1333-82-0

17chrysene

0.4 mg/kg 0.4 mg/kg 0.00004 %601-048-00-0 205-923-4 218-01-9


19


<0.1 mg/kg 1.884 <0.188 mg/kg <0.0000188 % <LOD

006-007-00-5


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-041-00-2 200-181-8 53-70-3

21


203-458-1,200-863-5

107-06-2, 75-34-3

22


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 68334-30-5,

68476-34-6,94114-59-7,1159170-26-9

23ethylbenzene

<20 mg/kg <20 mg/kg <0.002 % <LOD601-023-00-4 202-849-4 100-41-4

24fluoranthene

0.5 mg/kg 0.5 mg/kg 0.00005 % 205-912-4 206-44-0

25fluorene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 201-695-5 86-73-7


0.2 mg/kg 0.2 mg/kg 0.00002 % 205-893-2 193-39-5


082-001-00-6


<0.1 mg/kg 2.749 <0.275 mg/kg <0.0000275 % <LOD025-003-00-4 232-089-9 7785-87-7


1 mg/kg 1.353 1.353 mg/kg 0.000135 %080-010-00-X 231-299-8 7487-94-7


<0.1 mg/kg 1.5 <0.15 mg/kg <0.000015 % <LOD042-001-00-9 215-204-7 1313-27-5

31naphthalene

0.1 mg/kg 0.1 mg/kg 0.00001 %601-052-00-2 202-049-5 91-20-3


140 mg/kg 1.579 221.13 mg/kg 0.0221 %028-008-00-X 235-008-5 [1]234-348-1 [2]

12054-48-7 [1]11113-74-9 [2]

33pH

7.6 pH 7.6 pH 7.6 pH PH

34phenanthrene

0.2 mg/kg 0.2 mg/kg 0.00002 % 201-581-5 85-01-8



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed


35phenol

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD604-001-00-2 203-632-7 108-95-2

36pyrene

0.5 mg/kg 0.5 mg/kg 0.00005 % 204-927-3 129-00-0

37


034-002-00-8


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-028-00-4 204-825-9 127-18-4


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-008-00-5 200-262-8 56-23-5

40toluene

<20 mg/kg <20 mg/kg <0.002 % <LOD601-021-00-3 203-625-9 108-88-3


26 mg/kg 26 mg/kg 0.0026 % TPH


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-027-00-9 201-167-4 79-01-6


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-023-00-7 200-831-0 75-01-4

44

xylene

<20 mg/kg <20 mg/kg <0.002 % <LOD601-022-00-9 202-422-2 [1]

203-396-5 [2]203-576-3 [3]215-535-7 [4]

95-47-6 [1]106-42-3 [2]108-38-3 [3]1330-20-7 [4]


600 mg/kg 1.245 746.828 mg/kg 0.0747 %030-013-00-7 215-222-5 1314-13-2

46


602-045-00-7 200-024-3 50-29-3

47


602-047-00-8 200-349-0 57-74-9

48


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-043-00-6 210-168-9,

200-401-2,206-270-8,206-271-3

58-89-9, 319-84-6,319-85-7, 608-73-1

49dieldrin (ISO)

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-049-00-9 200-484-5 60-57-1

50


602-051-00-X 200-775-7 72-20-8

51


602-046-00-2 200-962-3 76-44-8

52hexachlorobenzene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-065-00-6 204-273-9 118-74-1

53


606-019-00-6 205-601-3 143-50-0

54aldrin (ISO)

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-048-00-3 206-215-8 309-00-2


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-074-00-5 210-172-0 608-93-5


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-039-00-4 215-648-1 1336-36-3



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed



602-077-00-1 219-196-6 2385-85-5


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-044-00-1 232-283-3 8001-35-2

59hexabromobiphenyl

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 252-994-2 36355-01-8

602,3,7,8-TeCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 217-122-7 1746-01-6

611,2,3,7,8-PeCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 40321-76-4

621,2,3,4,7,8-HxCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 39227-28-6

631,2,3,6,7,8-HxCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57653-85-7

641,2,3,7,8,9-HxCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 19408-74-3

651,2,3,4,6,7,8-HpCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 35822-46-9

66OCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 3268-87-9

672,3,7,8-TeCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 51207-31-9

681,2,3,7,8-PeCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57117-41-6

692,3,4,7,8-PeCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57117-31-4

701,2,3,4,7,8-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 70648-26-9

711,2,3,6,7,8-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57117-44-9

721,2,3,7,8,9-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 72918-21-9

732,3,4,6,7,8-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 60851-34-5

741,2,3,4,6,7,8-HpCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 67562-39-4

751,2,3,4,7,8,9-HpCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 55673-89-7

76OCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 39001-02-0


<0.1gNaOH

<0.1gNaOH

<0.1 gNaOH <LOD



<0.1 mg/kg 3.894 <0.389 mg/kg <0.0000389 % <LOD024-008-00-9 237-366-8 13765-19-0


1 <0.1 mg/kg 2.63 <0.263 mg/kg <0.00001 % <LOD027-005-00-0 233-334-2 10124-43-3



<0.1 mg/kg 2.483 <0.248 mg/kg <0.0000248 % <LOD024-006-00-8 232-140-5 7789-00-6


<0.1 mg/kg 1.575 <0.157 mg/kg <0.0000157 % <LOD047-001-00-2 231-853-9 7761-88-8


<0.1 mg/kg 3.523 <0.352 mg/kg <0.0000352 % <LOD024-018-00-3 231-889-5 7775-11-3



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed



081-002-00-9


<0.1 mg/kg 2.602 <0.26 mg/kg <0.000026 % <LOD050-018-00-8 401-640-7 53408-94-9


66 mg/kg 1.785 117.822 mg/kg 0.0118 %023-001-00-8 215-239-8 1314-62-1


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-043-00-3 202-436-9 95-63-6


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-025-00-5 203-604-4 108-67-8


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-006-00-4 200-663-8 67-66-3

Total: 0.26 %












Sample details











Determinands


#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed


1acenaphthene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 201-469-6 83-32-9

2acenaphthylene

0.2 mg/kg 0.2 mg/kg 0.00002 % 205-917-1 208-96-8

3anthracene

0.6 mg/kg 0.6 mg/kg 0.00006 % 204-371-1 120-12-7

4


1 <0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD

051-003-00-9


92 mg/kg 1.32 121.47 mg/kg 0.0121 %033-003-00-0 215-481-4 1327-53-3

6benzene

<10 mg/kg <10 mg/kg <0.001 % <LOD601-020-00-8 200-753-7 71-43-2

7benzo[a]anthracene

1.2 mg/kg 1.2 mg/kg 0.00012 %601-033-00-9 200-280-6 56-55-3


1 mg/kg 1 mg/kg 0.0001 %601-032-00-3 200-028-5 50-32-8


1 mg/kg 1 mg/kg 0.0001 %601-034-00-4 205-911-9 205-99-2


0.4 mg/kg 0.4 mg/kg 0.00004 % 205-883-8 191-24-2


1.3 mg/kg 1.3 mg/kg 0.00013 %601-036-00-5 205-916-6 207-08-9



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed



<0.1 mg/kg 2.775 <0.278 mg/kg <0.0000278 % <LOD004-003-00-8 215-133-1 1304-56-9

13


<1 mg/kg 13.43 <13.43 mg/kg <0.00134 % <LOD 10294-33-4,10294-34-5,7637-07-2


1 1 mg/kg 1.285 1.285 mg/kg 0.0001 %048-010-00-4 215-147-8 1306-23-6


215-160-9 1308-38-9


024-001-00-0 215-607-8 1333-82-0

17chrysene

1.2 mg/kg 1.2 mg/kg 0.00012 %601-048-00-0 205-923-4 218-01-9


19


<0.1 mg/kg 1.884 <0.188 mg/kg <0.0000188 % <LOD

006-007-00-5


0.2 mg/kg 0.2 mg/kg 0.00002 %601-041-00-2 200-181-8 53-70-3

21


203-458-1,200-863-5

107-06-2, 75-34-3

22


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 68334-30-5,

68476-34-6,94114-59-7,1159170-26-9

23ethylbenzene

<10 mg/kg <10 mg/kg <0.001 % <LOD601-023-00-4 202-849-4 100-41-4

24fluoranthene

2.3 mg/kg 2.3 mg/kg 0.00023 % 205-912-4 206-44-0

25fluorene

0.3 mg/kg 0.3 mg/kg 0.00003 % 201-695-5 86-73-7


0.5 mg/kg 0.5 mg/kg 0.00005 % 205-893-2 193-39-5


082-001-00-6


<0.1 mg/kg 2.749 <0.275 mg/kg <0.0000275 % <LOD025-003-00-4 232-089-9 7785-87-7


<1 mg/kg 1.353 <1.353 mg/kg <0.000135 % <LOD080-010-00-X 231-299-8 7487-94-7


<0.1 mg/kg 1.5 <0.15 mg/kg <0.000015 % <LOD042-001-00-9 215-204-7 1313-27-5

31naphthalene

0.2 mg/kg 0.2 mg/kg 0.00002 %601-052-00-2 202-049-5 91-20-3


110 mg/kg 1.579 173.745 mg/kg 0.0174 %028-008-00-X 235-008-5 [1]234-348-1 [2]

12054-48-7 [1]11113-74-9 [2]

33pH

7.3 pH 7.3 pH 7.3 pH PH

34phenanthrene

2.1 mg/kg 2.1 mg/kg 0.00021 % 201-581-5 85-01-8



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed


35phenol

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD604-001-00-2 203-632-7 108-95-2

36pyrene

2.1 mg/kg 2.1 mg/kg 0.00021 % 204-927-3 129-00-0

37


034-002-00-8


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-028-00-4 204-825-9 127-18-4


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-008-00-5 200-262-8 56-23-5

40toluene

<10 mg/kg <10 mg/kg <0.001 % <LOD601-021-00-3 203-625-9 108-88-3


24 mg/kg 24 mg/kg 0.0024 % TPH


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-027-00-9 201-167-4 79-01-6


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-023-00-7 200-831-0 75-01-4

44

xylene

<10 mg/kg <10 mg/kg <0.001 % <LOD601-022-00-9 202-422-2 [1]

203-396-5 [2]203-576-3 [3]215-535-7 [4]

95-47-6 [1]106-42-3 [2]108-38-3 [3]1330-20-7 [4]


470 mg/kg 1.245 585.016 mg/kg 0.0585 %030-013-00-7 215-222-5 1314-13-2

46


602-045-00-7 200-024-3 50-29-3

47


602-047-00-8 200-349-0 57-74-9

48


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-043-00-6 210-168-9,

200-401-2,206-270-8,206-271-3

58-89-9, 319-84-6,319-85-7, 608-73-1

49dieldrin (ISO)

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-049-00-9 200-484-5 60-57-1

50


602-051-00-X 200-775-7 72-20-8

51


602-046-00-2 200-962-3 76-44-8

52hexachlorobenzene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-065-00-6 204-273-9 118-74-1

53


606-019-00-6 205-601-3 143-50-0

54aldrin (ISO)

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-048-00-3 206-215-8 309-00-2


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-074-00-5 210-172-0 608-93-5


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-039-00-4 215-648-1 1336-36-3



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed



602-077-00-1 219-196-6 2385-85-5


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-044-00-1 232-283-3 8001-35-2

59hexabromobiphenyl

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 252-994-2 36355-01-8

602,3,7,8-TeCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 217-122-7 1746-01-6

611,2,3,7,8-PeCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 40321-76-4

621,2,3,4,7,8-HxCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 39227-28-6

631,2,3,6,7,8-HxCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57653-85-7

641,2,3,7,8,9-HxCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 19408-74-3

651,2,3,4,6,7,8-HpCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 35822-46-9

66OCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 3268-87-9

672,3,7,8-TeCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 51207-31-9

681,2,3,7,8-PeCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57117-41-6

692,3,4,7,8-PeCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57117-31-4

701,2,3,4,7,8-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 70648-26-9

711,2,3,6,7,8-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57117-44-9

721,2,3,7,8,9-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 72918-21-9

732,3,4,6,7,8-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 60851-34-5

741,2,3,4,6,7,8-HpCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 67562-39-4

751,2,3,4,7,8,9-HpCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 55673-89-7

76OCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 39001-02-0


<0.1gNaOH

<0.1gNaOH

<0.1 gNaOH <LOD



<0.1 mg/kg 3.894 <0.389 mg/kg <0.0000389 % <LOD024-008-00-9 237-366-8 13765-19-0


1 <0.1 mg/kg 2.63 <0.263 mg/kg <0.00001 % <LOD027-005-00-0 233-334-2 10124-43-3



<0.1 mg/kg 2.483 <0.248 mg/kg <0.0000248 % <LOD024-006-00-8 232-140-5 7789-00-6


<0.1 mg/kg 1.575 <0.157 mg/kg <0.0000157 % <LOD047-001-00-2 231-853-9 7761-88-8


<0.1 mg/kg 3.523 <0.352 mg/kg <0.0000352 % <LOD024-018-00-3 231-889-5 7775-11-3



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed



081-002-00-9


<0.1 mg/kg 2.602 <0.26 mg/kg <0.000026 % <LOD050-018-00-8 401-640-7 53408-94-9


22 mg/kg 1.785 39.274 mg/kg 0.00393 %023-001-00-8 215-239-8 1314-62-1


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-043-00-3 202-436-9 95-63-6


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-025-00-5 203-604-4 108-67-8


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-006-00-4 200-663-8 67-66-3

Total: 0.19 %












Sample details











Determinands


#Determinand

CLP

Not

e



valueM

CA

pplie

dConc. Not


1acenaphthene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 201-469-6 83-32-9

2acenaphthylene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 205-917-1 208-96-8

3anthracene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 204-371-1 120-12-7

4


1 <0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD

051-003-00-9


26 mg/kg 1.32 34.328 mg/kg 0.00343 %033-003-00-0 215-481-4 1327-53-3

6benzene

<10 mg/kg <10 mg/kg <0.001 % <LOD601-020-00-8 200-753-7 71-43-2

7benzo[a]anthracene

0.1 mg/kg 0.1 mg/kg 0.00001 %601-033-00-9 200-280-6 56-55-3


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-032-00-3 200-028-5 50-32-8


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-034-00-4 205-911-9 205-99-2


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 205-883-8 191-24-2


0.1 mg/kg 0.1 mg/kg 0.00001 %601-036-00-5 205-916-6 207-08-9



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed



<0.1 mg/kg 2.775 <0.278 mg/kg <0.0000278 % <LOD004-003-00-8 215-133-1 1304-56-9

13


<1 mg/kg 13.43 <13.43 mg/kg <0.00134 % <LOD 10294-33-4,10294-34-5,7637-07-2


1 <1 mg/kg 1.285 <1.285 mg/kg <0.0001 % <LOD048-010-00-4 215-147-8 1306-23-6


215-160-9 1308-38-9


024-001-00-0 215-607-8 1333-82-0

17chrysene

0.1 mg/kg 0.1 mg/kg 0.00001 %601-048-00-0 205-923-4 218-01-9


19


<0.1 mg/kg 1.884 <0.188 mg/kg <0.0000188 % <LOD

006-007-00-5


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-041-00-2 200-181-8 53-70-3

21


203-458-1,200-863-5

107-06-2, 75-34-3

22


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 68334-30-5,

68476-34-6,94114-59-7,1159170-26-9

23ethylbenzene

<10 mg/kg <10 mg/kg <0.001 % <LOD601-023-00-4 202-849-4 100-41-4

24fluoranthene

0.2 mg/kg 0.2 mg/kg 0.00002 % 205-912-4 206-44-0

25fluorene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 201-695-5 86-73-7


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 205-893-2 193-39-5


082-001-00-6


<0.1 mg/kg 2.749 <0.275 mg/kg <0.0000275 % <LOD025-003-00-4 232-089-9 7785-87-7


<1 mg/kg 1.353 <1.353 mg/kg <0.000135 % <LOD080-010-00-X 231-299-8 7487-94-7


<0.1 mg/kg 1.5 <0.15 mg/kg <0.000015 % <LOD042-001-00-9 215-204-7 1313-27-5

31naphthalene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-052-00-2 202-049-5 91-20-3


29 mg/kg 1.579 45.805 mg/kg 0.00458 %028-008-00-X 235-008-5 [1]234-348-1 [2]

12054-48-7 [1]11113-74-9 [2]

33pH

7 pH 7 pH 7pH PH

34phenanthrene

0.1 mg/kg 0.1 mg/kg 0.00001 % 201-581-5 85-01-8



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed


35phenol

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD604-001-00-2 203-632-7 108-95-2

36pyrene

0.2 mg/kg 0.2 mg/kg 0.00002 % 204-927-3 129-00-0

37


034-002-00-8


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-028-00-4 204-825-9 127-18-4


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-008-00-5 200-262-8 56-23-5

40toluene

<10 mg/kg <10 mg/kg <0.001 % <LOD601-021-00-3 203-625-9 108-88-3


15 mg/kg 15 mg/kg 0.0015 % TPH


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-027-00-9 201-167-4 79-01-6


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-023-00-7 200-831-0 75-01-4

44

xylene

<10 mg/kg <10 mg/kg <0.001 % <LOD601-022-00-9 202-422-2 [1]

203-396-5 [2]203-576-3 [3]215-535-7 [4]

95-47-6 [1]106-42-3 [2]108-38-3 [3]1330-20-7 [4]


190 mg/kg 1.245 236.496 mg/kg 0.0236 %030-013-00-7 215-222-5 1314-13-2

46


602-045-00-7 200-024-3 50-29-3

47


602-047-00-8 200-349-0 57-74-9

48


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-043-00-6 210-168-9,

200-401-2,206-270-8,206-271-3

58-89-9, 319-84-6,319-85-7, 608-73-1

49dieldrin (ISO)

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-049-00-9 200-484-5 60-57-1

50


602-051-00-X 200-775-7 72-20-8

51


602-046-00-2 200-962-3 76-44-8

52hexachlorobenzene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-065-00-6 204-273-9 118-74-1

53


606-019-00-6 205-601-3 143-50-0

54aldrin (ISO)

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-048-00-3 206-215-8 309-00-2


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-074-00-5 210-172-0 608-93-5


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-039-00-4 215-648-1 1336-36-3



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed



602-077-00-1 219-196-6 2385-85-5


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-044-00-1 232-283-3 8001-35-2

59hexabromobiphenyl

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 252-994-2 36355-01-8

602,3,7,8-TeCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 217-122-7 1746-01-6

611,2,3,7,8-PeCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 40321-76-4

621,2,3,4,7,8-HxCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 39227-28-6

631,2,3,6,7,8-HxCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57653-85-7

641,2,3,7,8,9-HxCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 19408-74-3

651,2,3,4,6,7,8-HpCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 35822-46-9

66OCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 3268-87-9

672,3,7,8-TeCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 51207-31-9

681,2,3,7,8-PeCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57117-41-6

692,3,4,7,8-PeCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57117-31-4

701,2,3,4,7,8-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 70648-26-9

711,2,3,6,7,8-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57117-44-9

721,2,3,7,8,9-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 72918-21-9

732,3,4,6,7,8-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 60851-34-5

741,2,3,4,6,7,8-HpCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 67562-39-4

751,2,3,4,7,8,9-HpCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 55673-89-7

76OCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 39001-02-0


<0.1gNaOH

<0.1gNaOH

<0.1 gNaOH <LOD



<0.1 mg/kg 3.894 <0.389 mg/kg <0.0000389 % <LOD024-008-00-9 237-366-8 13765-19-0


1 <0.1 mg/kg 2.63 <0.263 mg/kg <0.00001 % <LOD027-005-00-0 233-334-2 10124-43-3



<0.1 mg/kg 2.483 <0.248 mg/kg <0.0000248 % <LOD024-006-00-8 232-140-5 7789-00-6


<0.1 mg/kg 1.575 <0.157 mg/kg <0.0000157 % <LOD047-001-00-2 231-853-9 7761-88-8


<0.1 mg/kg 3.523 <0.352 mg/kg <0.0000352 % <LOD024-018-00-3 231-889-5 7775-11-3



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed



081-002-00-9


<0.1 mg/kg 2.602 <0.26 mg/kg <0.000026 % <LOD050-018-00-8 401-640-7 53408-94-9


28 mg/kg 1.785 49.985 mg/kg 0.005 %023-001-00-8 215-239-8 1314-62-1


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-043-00-3 202-436-9 95-63-6


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-025-00-5 203-604-4 108-67-8


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-006-00-4 200-663-8 67-66-3

Total: 0.0748 %









Classification of sample: BH03 ES4

Non Hazardous WasteClassified as 17 05 04


Sample details

Sample Name:BH03 ES4


from contaminated sites)Entry: 17 05 04 (Soil and stones other than those mentioned in 17 05

03)

Hazard properties

None identified

Determinands


#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed


1acenaphthene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 201-469-6 83-32-9

2acenaphthylene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 205-917-1 208-96-8

3anthracene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 204-371-1 120-12-7

4


1 <0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD

051-003-00-9


10 mg/kg 1.32 13.203 mg/kg 0.00132 %033-003-00-0 215-481-4 1327-53-3

6benzene

<10 mg/kg <10 mg/kg <0.001 % <LOD601-020-00-8 200-753-7 71-43-2

7benzo[a]anthracene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-033-00-9 200-280-6 56-55-3


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-032-00-3 200-028-5 50-32-8


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-034-00-4 205-911-9 205-99-2


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 205-883-8 191-24-2


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-036-00-5 205-916-6 207-08-9


<0.1 mg/kg 2.775 <0.278 mg/kg <0.0000278 % <LOD004-003-00-8 215-133-1 1304-56-9

13


<1 mg/kg 13.43 <13.43 mg/kg <0.00134 % <LOD 10294-33-4,10294-34-5,7637-07-2


1 <1 mg/kg 1.285 <1.285 mg/kg <0.0001 % <LOD048-010-00-4 215-147-8 1306-23-6



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed



215-160-9 1308-38-9


024-001-00-0 215-607-8 1333-82-0

17chrysene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-048-00-0 205-923-4 218-01-9


19


<0.1 mg/kg 1.884 <0.188 mg/kg <0.0000188 % <LOD

006-007-00-5


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-041-00-2 200-181-8 53-70-3

21


203-458-1,200-863-5

107-06-2, 75-34-3

22


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 68334-30-5,

68476-34-6,94114-59-7,1159170-26-9

23ethylbenzene

<10 mg/kg <10 mg/kg <0.001 % <LOD601-023-00-4 202-849-4 100-41-4

24fluoranthene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 205-912-4 206-44-0

25fluorene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 201-695-5 86-73-7


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 205-893-2 193-39-5


082-001-00-6


<0.1 mg/kg 2.749 <0.275 mg/kg <0.0000275 % <LOD025-003-00-4 232-089-9 7785-87-7


<1 mg/kg 1.353 <1.353 mg/kg <0.000135 % <LOD080-010-00-X 231-299-8 7487-94-7


<0.1 mg/kg 1.5 <0.15 mg/kg <0.000015 % <LOD042-001-00-9 215-204-7 1313-27-5

31naphthalene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-052-00-2 202-049-5 91-20-3


30 mg/kg 1.579 47.385 mg/kg 0.00474 %028-008-00-X 235-008-5 [1]234-348-1 [2]

12054-48-7 [1]11113-74-9 [2]

33pH

7.8 pH 7.8 pH 7.8 pH PH

34phenanthrene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 201-581-5 85-01-8

35phenol

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD604-001-00-2 203-632-7 108-95-2

36pyrene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 204-927-3 129-00-0

37


034-002-00-8



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed



<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-028-00-4 204-825-9 127-18-4


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-008-00-5 200-262-8 56-23-5

40toluene

<10 mg/kg <10 mg/kg <0.001 % <LOD601-021-00-3 203-625-9 108-88-3


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD TPH


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-027-00-9 201-167-4 79-01-6


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-023-00-7 200-831-0 75-01-4

44

xylene

<10 mg/kg <10 mg/kg <0.001 % <LOD601-022-00-9 202-422-2 [1]

203-396-5 [2]203-576-3 [3]215-535-7 [4]

95-47-6 [1]106-42-3 [2]108-38-3 [3]1330-20-7 [4]


44 mg/kg 1.245 54.767 mg/kg 0.00548 %030-013-00-7 215-222-5 1314-13-2

46


602-045-00-7 200-024-3 50-29-3

47


602-047-00-8 200-349-0 57-74-9

48


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-043-00-6 210-168-9,

200-401-2,206-270-8,206-271-3

58-89-9, 319-84-6,319-85-7, 608-73-1

49dieldrin (ISO)

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-049-00-9 200-484-5 60-57-1

50


602-051-00-X 200-775-7 72-20-8

51


602-046-00-2 200-962-3 76-44-8

52hexachlorobenzene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-065-00-6 204-273-9 118-74-1

53


606-019-00-6 205-601-3 143-50-0

54aldrin (ISO)

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-048-00-3 206-215-8 309-00-2


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-074-00-5 210-172-0 608-93-5


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-039-00-4 215-648-1 1336-36-3


602-077-00-1 219-196-6 2385-85-5


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-044-00-1 232-283-3 8001-35-2

59hexabromobiphenyl

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 252-994-2 36355-01-8

602,3,7,8-TeCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 217-122-7 1746-01-6



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed


611,2,3,7,8-PeCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 40321-76-4

621,2,3,4,7,8-HxCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 39227-28-6

631,2,3,6,7,8-HxCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57653-85-7

641,2,3,7,8,9-HxCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 19408-74-3

651,2,3,4,6,7,8-HpCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 35822-46-9

66OCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 3268-87-9

672,3,7,8-TeCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 51207-31-9

681,2,3,7,8-PeCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57117-41-6

692,3,4,7,8-PeCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57117-31-4

701,2,3,4,7,8-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 70648-26-9

711,2,3,6,7,8-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57117-44-9

721,2,3,7,8,9-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 72918-21-9

732,3,4,6,7,8-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 60851-34-5

741,2,3,4,6,7,8-HpCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 67562-39-4

751,2,3,4,7,8,9-HpCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 55673-89-7

76OCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 39001-02-0


<0.1gNaOH

<0.1gNaOH

<0.1 gNaOH <LOD



<0.1 mg/kg 3.894 <0.389 mg/kg <0.0000389 % <LOD024-008-00-9 237-366-8 13765-19-0


1 <0.1 mg/kg 2.63 <0.263 mg/kg <0.00001 % <LOD027-005-00-0 233-334-2 10124-43-3



<0.1 mg/kg 2.483 <0.248 mg/kg <0.0000248 % <LOD024-006-00-8 232-140-5 7789-00-6


<0.1 mg/kg 1.575 <0.157 mg/kg <0.0000157 % <LOD047-001-00-2 231-853-9 7761-88-8


<0.1 mg/kg 3.523 <0.352 mg/kg <0.0000352 % <LOD024-018-00-3 231-889-5 7775-11-3


081-002-00-9


<0.1 mg/kg 2.602 <0.26 mg/kg <0.000026 % <LOD050-018-00-8 401-640-7 53408-94-9


35 mg/kg 1.785 62.481 mg/kg 0.00625 %023-001-00-8 215-239-8 1314-62-1


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-043-00-3 202-436-9 95-63-6


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-025-00-5 203-604-4 108-67-8



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed



<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-006-00-4 200-663-8 67-66-3

Total: 0.0327 %









Hazardous WasteClassified as 17 05 03 *


Sample details



from contaminated sites)Entry: 17 05 03 * (Soil and stones containing hazardous substances)

Hazard properties

HP 7: Carcinogenic "waste which induces cancer or increases its incidence"


Carc. 1B; H350 "May cause cancer [state route of exposure if it is conclusively proven that no other routes of exposure cause thehazard]."



HP 11: Mutagenic "waste which may cause a mutation, that is a permanent change in the amount or structure of the genetic material ina cell"


Muta. 1B; H340 "May cause genetic defects [state route of exposure if it is conclusively proven that no other routes of exposure causethe hazard]."









Determinands


#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed


1acenaphthene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 201-469-6 83-32-9

2acenaphthylene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 205-917-1 208-96-8

3anthracene

1.7 mg/kg 1.7 mg/kg 0.00017 % 204-371-1 120-12-7

4 antimony { antimony compounds, with the exception ofthe tetroxide (Sb2O4), pentoxide (Sb2O5), trisulphide

1 <0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed


(Sb2S3), pentasulphide (Sb2S5) and those specifiedelsewhere in this Annex }

051-003-00-9


12 mg/kg 1.32 15.844 mg/kg 0.00158 %033-003-00-0 215-481-4 1327-53-3

6benzene

<10 mg/kg <10 mg/kg <0.001 % <LOD601-020-00-8 200-753-7 71-43-2

7benzo[a]anthracene

6.2 mg/kg 6.2 mg/kg 0.00062 %601-033-00-9 200-280-6 56-55-3


4.3 mg/kg 4.3 mg/kg 0.00043 %601-032-00-3 200-028-5 50-32-8


4.9 mg/kg 4.9 mg/kg 0.00049 %601-034-00-4 205-911-9 205-99-2


2.6 mg/kg 2.6 mg/kg 0.00026 % 205-883-8 191-24-2


5.5 mg/kg 5.5 mg/kg 0.00055 %601-036-00-5 205-916-6 207-08-9


<0.1 mg/kg 2.775 <0.278 mg/kg <0.0000278 % <LOD004-003-00-8 215-133-1 1304-56-9

13


<1 mg/kg 13.43 <13.43 mg/kg <0.00134 % <LOD 10294-33-4,10294-34-5,7637-07-2


1 <1 mg/kg 1.285 <1.285 mg/kg <0.0001 % <LOD048-010-00-4 215-147-8 1306-23-6


215-160-9 1308-38-9


024-001-00-0 215-607-8 1333-82-0

17chrysene

6.2 mg/kg 6.2 mg/kg 0.00062 %601-048-00-0 205-923-4 218-01-9


19


<0.1 mg/kg 1.884 <0.188 mg/kg <0.0000188 % <LOD

006-007-00-5


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-041-00-2 200-181-8 53-70-3

21


203-458-1,200-863-5

107-06-2, 75-34-3

22


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 68334-30-5,

68476-34-6,94114-59-7,1159170-26-9

23ethylbenzene

<10 mg/kg <10 mg/kg <0.001 % <LOD601-023-00-4 202-849-4 100-41-4

24fluoranthene

8.7 mg/kg 8.7 mg/kg 0.00087 % 205-912-4 206-44-0

25fluorene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 201-695-5 86-73-7


2.6 mg/kg 2.6 mg/kg 0.00026 % 205-893-2 193-39-5



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed



082-001-00-6


<0.1 mg/kg 2.749 <0.275 mg/kg <0.0000275 % <LOD025-003-00-4 232-089-9 7785-87-7


<1 mg/kg 1.353 <1.353 mg/kg <0.000135 % <LOD080-010-00-X 231-299-8 7487-94-7


<0.1 mg/kg 1.5 <0.15 mg/kg <0.000015 % <LOD042-001-00-9 215-204-7 1313-27-5

31naphthalene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-052-00-2 202-049-5 91-20-3


32 mg/kg 1.579 50.544 mg/kg 0.00505 %028-008-00-X 235-008-5 [1]234-348-1 [2]

12054-48-7 [1]11113-74-9 [2]

33pH

7.2 pH 7.2 pH 7.2 pH PH

34phenanthrene

6.8 mg/kg 6.8 mg/kg 0.00068 % 201-581-5 85-01-8

35phenol

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD604-001-00-2 203-632-7 108-95-2

36pyrene

8.9 mg/kg 8.9 mg/kg 0.00089 % 204-927-3 129-00-0

37


034-002-00-8


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-028-00-4 204-825-9 127-18-4


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-008-00-5 200-262-8 56-23-5

40toluene

<10 mg/kg <10 mg/kg <0.001 % <LOD601-021-00-3 203-625-9 108-88-3


1200 mg/kg 1200 mg/kg 0.12 % TPH


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-027-00-9 201-167-4 79-01-6


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-023-00-7 200-831-0 75-01-4

44

xylene

<10 mg/kg <10 mg/kg <0.001 % <LOD601-022-00-9 202-422-2 [1]

203-396-5 [2]203-576-3 [3]215-535-7 [4]

95-47-6 [1]106-42-3 [2]108-38-3 [3]1330-20-7 [4]


95 mg/kg 1.245 118.248 mg/kg 0.0118 %030-013-00-7 215-222-5 1314-13-2

46


602-045-00-7 200-024-3 50-29-3

47


602-047-00-8 200-349-0 57-74-9

48


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-043-00-6 210-168-9,

200-401-2,206-270-8,206-271-3

58-89-9, 319-84-6,319-85-7, 608-73-1

49dieldrin (ISO)

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-049-00-9 200-484-5 60-57-1



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed


50


602-051-00-X 200-775-7 72-20-8

51


602-046-00-2 200-962-3 76-44-8

52hexachlorobenzene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-065-00-6 204-273-9 118-74-1

53


606-019-00-6 205-601-3 143-50-0

54aldrin (ISO)

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-048-00-3 206-215-8 309-00-2


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-074-00-5 210-172-0 608-93-5


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-039-00-4 215-648-1 1336-36-3


602-077-00-1 219-196-6 2385-85-5


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-044-00-1 232-283-3 8001-35-2

59hexabromobiphenyl

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 252-994-2 36355-01-8

602,3,7,8-TeCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 217-122-7 1746-01-6

611,2,3,7,8-PeCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 40321-76-4

621,2,3,4,7,8-HxCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 39227-28-6

631,2,3,6,7,8-HxCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57653-85-7

641,2,3,7,8,9-HxCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 19408-74-3

651,2,3,4,6,7,8-HpCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 35822-46-9

66OCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 3268-87-9

672,3,7,8-TeCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 51207-31-9

681,2,3,7,8-PeCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57117-41-6

692,3,4,7,8-PeCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57117-31-4

701,2,3,4,7,8-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 70648-26-9

711,2,3,6,7,8-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57117-44-9

721,2,3,7,8,9-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 72918-21-9

732,3,4,6,7,8-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 60851-34-5

741,2,3,4,6,7,8-HpCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 67562-39-4

751,2,3,4,7,8,9-HpCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 55673-89-7

76OCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 39001-02-0



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed



<0.1gNaOH

<0.1gNaOH

<0.1 gNaOH <LOD



<0.1 mg/kg 3.894 <0.389 mg/kg <0.0000389 % <LOD024-008-00-9 237-366-8 13765-19-0


1 <0.1 mg/kg 2.63 <0.263 mg/kg <0.00001 % <LOD027-005-00-0 233-334-2 10124-43-3



<0.1 mg/kg 2.483 <0.248 mg/kg <0.0000248 % <LOD024-006-00-8 232-140-5 7789-00-6


<0.1 mg/kg 1.575 <0.157 mg/kg <0.0000157 % <LOD047-001-00-2 231-853-9 7761-88-8


<0.1 mg/kg 3.523 <0.352 mg/kg <0.0000352 % <LOD024-018-00-3 231-889-5 7775-11-3


081-002-00-9


<0.1 mg/kg 2.602 <0.26 mg/kg <0.000026 % <LOD050-018-00-8 401-640-7 53408-94-9


48 mg/kg 1.785 85.689 mg/kg 0.00857 %023-001-00-8 215-239-8 1314-62-1


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-043-00-3 202-436-9 95-63-6


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-025-00-5 203-604-4 108-67-8


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-006-00-4 200-663-8 67-66-3

Total: 0.187 %



Hazardous result









Sample details











Determinands


#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed


1acenaphthene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 201-469-6 83-32-9

2acenaphthylene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 205-917-1 208-96-8

3anthracene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 204-371-1 120-12-7

4


1 <0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD

051-003-00-9


73 mg/kg 1.32 96.384 mg/kg 0.00964 %033-003-00-0 215-481-4 1327-53-3

6benzene

<10 mg/kg <10 mg/kg <0.001 % <LOD601-020-00-8 200-753-7 71-43-2

7benzo[a]anthracene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-033-00-9 200-280-6 56-55-3


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-032-00-3 200-028-5 50-32-8


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-034-00-4 205-911-9 205-99-2


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 205-883-8 191-24-2


1.4 mg/kg 1.4 mg/kg 0.00014 %601-036-00-5 205-916-6 207-08-9



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed



<0.1 mg/kg 2.775 <0.278 mg/kg <0.0000278 % <LOD004-003-00-8 215-133-1 1304-56-9

13


<1 mg/kg 13.43 <13.43 mg/kg <0.00134 % <LOD 10294-33-4,10294-34-5,7637-07-2


1 2 mg/kg 1.285 2.57 mg/kg 0.0002 %048-010-00-4 215-147-8 1306-23-6


215-160-9 1308-38-9


024-001-00-0 215-607-8 1333-82-0

17chrysene

1.2 mg/kg 1.2 mg/kg 0.00012 %601-048-00-0 205-923-4 218-01-9


19


<0.1 mg/kg 1.884 <0.188 mg/kg <0.0000188 % <LOD

006-007-00-5


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-041-00-2 200-181-8 53-70-3

21


203-458-1,200-863-5

107-06-2, 75-34-3

22


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 68334-30-5,

68476-34-6,94114-59-7,1159170-26-9

23ethylbenzene

<10 mg/kg <10 mg/kg <0.001 % <LOD601-023-00-4 202-849-4 100-41-4

24fluoranthene

1.6 mg/kg 1.6 mg/kg 0.00016 % 205-912-4 206-44-0

25fluorene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 201-695-5 86-73-7


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 205-893-2 193-39-5


082-001-00-6


<0.1 mg/kg 2.749 <0.275 mg/kg <0.0000275 % <LOD025-003-00-4 232-089-9 7785-87-7


1 mg/kg 1.353 1.353 mg/kg 0.000135 %080-010-00-X 231-299-8 7487-94-7


<0.1 mg/kg 1.5 <0.15 mg/kg <0.000015 % <LOD042-001-00-9 215-204-7 1313-27-5

31naphthalene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-052-00-2 202-049-5 91-20-3


61 mg/kg 1.579 96.349 mg/kg 0.00963 %028-008-00-X 235-008-5 [1]234-348-1 [2]

12054-48-7 [1]11113-74-9 [2]

33pH

6.9 pH 6.9 pH 6.9 pH PH

34phenanthrene

1.5 mg/kg 1.5 mg/kg 0.00015 % 201-581-5 85-01-8



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed


35phenol

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD604-001-00-2 203-632-7 108-95-2

36pyrene

1.7 mg/kg 1.7 mg/kg 0.00017 % 204-927-3 129-00-0

37


034-002-00-8


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-028-00-4 204-825-9 127-18-4


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-008-00-5 200-262-8 56-23-5

40toluene

<10 mg/kg <10 mg/kg <0.001 % <LOD601-021-00-3 203-625-9 108-88-3


240 mg/kg 240 mg/kg 0.024 % TPH


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-027-00-9 201-167-4 79-01-6


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-023-00-7 200-831-0 75-01-4

44

xylene

<10 mg/kg <10 mg/kg <0.001 % <LOD601-022-00-9 202-422-2 [1]

203-396-5 [2]203-576-3 [3]215-535-7 [4]

95-47-6 [1]106-42-3 [2]108-38-3 [3]1330-20-7 [4]


650 mg/kg 1.245 809.064 mg/kg 0.0809 %030-013-00-7 215-222-5 1314-13-2

46


602-045-00-7 200-024-3 50-29-3

47


602-047-00-8 200-349-0 57-74-9

48


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-043-00-6 210-168-9,

200-401-2,206-270-8,206-271-3

58-89-9, 319-84-6,319-85-7, 608-73-1

49dieldrin (ISO)

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-049-00-9 200-484-5 60-57-1

50


602-051-00-X 200-775-7 72-20-8

51


602-046-00-2 200-962-3 76-44-8

52hexachlorobenzene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-065-00-6 204-273-9 118-74-1

53


606-019-00-6 205-601-3 143-50-0

54aldrin (ISO)

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-048-00-3 206-215-8 309-00-2


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-074-00-5 210-172-0 608-93-5


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-039-00-4 215-648-1 1336-36-3



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed



602-077-00-1 219-196-6 2385-85-5


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-044-00-1 232-283-3 8001-35-2

59hexabromobiphenyl

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 252-994-2 36355-01-8

602,3,7,8-TeCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 217-122-7 1746-01-6

611,2,3,7,8-PeCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 40321-76-4

621,2,3,4,7,8-HxCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 39227-28-6

631,2,3,6,7,8-HxCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57653-85-7

641,2,3,7,8,9-HxCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 19408-74-3

651,2,3,4,6,7,8-HpCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 35822-46-9

66OCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 3268-87-9

672,3,7,8-TeCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 51207-31-9

681,2,3,7,8-PeCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57117-41-6

692,3,4,7,8-PeCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57117-31-4

701,2,3,4,7,8-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 70648-26-9

711,2,3,6,7,8-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57117-44-9

721,2,3,7,8,9-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 72918-21-9

732,3,4,6,7,8-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 60851-34-5

741,2,3,4,6,7,8-HpCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 67562-39-4

751,2,3,4,7,8,9-HpCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 55673-89-7

76OCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 39001-02-0


<0.1gNaOH

<0.1gNaOH

<0.1 gNaOH <LOD



<0.1 mg/kg 3.894 <0.389 mg/kg <0.0000389 % <LOD024-008-00-9 237-366-8 13765-19-0


1 <0.1 mg/kg 2.63 <0.263 mg/kg <0.00001 % <LOD027-005-00-0 233-334-2 10124-43-3



<0.1 mg/kg 2.483 <0.248 mg/kg <0.0000248 % <LOD024-006-00-8 232-140-5 7789-00-6


<0.1 mg/kg 1.575 <0.157 mg/kg <0.0000157 % <LOD047-001-00-2 231-853-9 7761-88-8


<0.1 mg/kg 3.523 <0.352 mg/kg <0.0000352 % <LOD024-018-00-3 231-889-5 7775-11-3



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed



081-002-00-9


<0.1 mg/kg 2.602 <0.26 mg/kg <0.000026 % <LOD050-018-00-8 401-640-7 53408-94-9


25 mg/kg 1.785 44.63 mg/kg 0.00446 %023-001-00-8 215-239-8 1314-62-1


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-043-00-3 202-436-9 95-63-6


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-025-00-5 203-604-4 108-67-8


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-006-00-4 200-663-8 67-66-3

Total: 0.412 %









Classification of sample: BH04



Sample details

Sample Name:BH04



03)

Hazard properties

None identified

Determinands


#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed


1acenaphthene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 201-469-6 83-32-9

2acenaphthylene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 205-917-1 208-96-8

3anthracene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 204-371-1 120-12-7

4


1 <0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD

051-003-00-9


14 mg/kg 1.32 18.485 mg/kg 0.00185 %033-003-00-0 215-481-4 1327-53-3

6benzene

<10 mg/kg <10 mg/kg <0.001 % <LOD601-020-00-8 200-753-7 71-43-2

7benzo[a]anthracene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-033-00-9 200-280-6 56-55-3


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-032-00-3 200-028-5 50-32-8


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-034-00-4 205-911-9 205-99-2


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 205-883-8 191-24-2


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-036-00-5 205-916-6 207-08-9


<0.1 mg/kg 2.775 <0.278 mg/kg <0.0000278 % <LOD004-003-00-8 215-133-1 1304-56-9

13


<1 mg/kg 13.43 <13.43 mg/kg <0.00134 % <LOD 10294-33-4,10294-34-5,7637-07-2


1 <1 mg/kg 1.285 <1.285 mg/kg <0.0001 % <LOD048-010-00-4 215-147-8 1306-23-6



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed



215-160-9 1308-38-9


024-001-00-0 215-607-8 1333-82-0

17chrysene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-048-00-0 205-923-4 218-01-9


19


<0.1 mg/kg 1.884 <0.188 mg/kg <0.0000188 % <LOD

006-007-00-5


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-041-00-2 200-181-8 53-70-3

21


203-458-1,200-863-5

107-06-2, 75-34-3

22


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 68334-30-5,

68476-34-6,94114-59-7,1159170-26-9

23ethylbenzene

<10 mg/kg <10 mg/kg <0.001 % <LOD601-023-00-4 202-849-4 100-41-4

24fluoranthene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 205-912-4 206-44-0

25fluorene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 201-695-5 86-73-7


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 205-893-2 193-39-5


082-001-00-6


<0.1 mg/kg 2.749 <0.275 mg/kg <0.0000275 % <LOD025-003-00-4 232-089-9 7785-87-7


<1 mg/kg 1.353 <1.353 mg/kg <0.000135 % <LOD080-010-00-X 231-299-8 7487-94-7


<0.1 mg/kg 1.5 <0.15 mg/kg <0.000015 % <LOD042-001-00-9 215-204-7 1313-27-5

31naphthalene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-052-00-2 202-049-5 91-20-3


19 mg/kg 1.579 30.01 mg/kg 0.003 %028-008-00-X 235-008-5 [1]234-348-1 [2]

12054-48-7 [1]11113-74-9 [2]

33pH

7.5 pH 7.5 pH 7.5 pH PH

34phenanthrene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 201-581-5 85-01-8

35phenol

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD604-001-00-2 203-632-7 108-95-2

36pyrene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 204-927-3 129-00-0

37


034-002-00-8



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed



<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-028-00-4 204-825-9 127-18-4


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-008-00-5 200-262-8 56-23-5

40toluene

<10 mg/kg <10 mg/kg <0.001 % <LOD601-021-00-3 203-625-9 108-88-3


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD TPH


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-027-00-9 201-167-4 79-01-6


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-023-00-7 200-831-0 75-01-4

44

xylene

<10 mg/kg <10 mg/kg <0.001 % <LOD601-022-00-9 202-422-2 [1]

203-396-5 [2]203-576-3 [3]215-535-7 [4]

95-47-6 [1]106-42-3 [2]108-38-3 [3]1330-20-7 [4]


150 mg/kg 1.245 186.707 mg/kg 0.0187 %030-013-00-7 215-222-5 1314-13-2

46


602-045-00-7 200-024-3 50-29-3

47


602-047-00-8 200-349-0 57-74-9

48


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-043-00-6 210-168-9,

200-401-2,206-270-8,206-271-3

58-89-9, 319-84-6,319-85-7, 608-73-1

49dieldrin (ISO)

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-049-00-9 200-484-5 60-57-1

50


602-051-00-X 200-775-7 72-20-8

51


602-046-00-2 200-962-3 76-44-8

52hexachlorobenzene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-065-00-6 204-273-9 118-74-1

53


606-019-00-6 205-601-3 143-50-0

54aldrin (ISO)

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-048-00-3 206-215-8 309-00-2


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-074-00-5 210-172-0 608-93-5


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-039-00-4 215-648-1 1336-36-3


602-077-00-1 219-196-6 2385-85-5


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-044-00-1 232-283-3 8001-35-2

59hexabromobiphenyl

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 252-994-2 36355-01-8

602,3,7,8-TeCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 217-122-7 1746-01-6



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed


611,2,3,7,8-PeCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 40321-76-4

621,2,3,4,7,8-HxCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 39227-28-6

631,2,3,6,7,8-HxCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57653-85-7

641,2,3,7,8,9-HxCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 19408-74-3

651,2,3,4,6,7,8-HpCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 35822-46-9

66OCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 3268-87-9

672,3,7,8-TeCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 51207-31-9

681,2,3,7,8-PeCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57117-41-6

692,3,4,7,8-PeCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57117-31-4

701,2,3,4,7,8-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 70648-26-9

711,2,3,6,7,8-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57117-44-9

721,2,3,7,8,9-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 72918-21-9

732,3,4,6,7,8-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 60851-34-5

741,2,3,4,6,7,8-HpCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 67562-39-4

751,2,3,4,7,8,9-HpCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 55673-89-7

76OCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 39001-02-0


<0.1gNaOH

<0.1gNaOH

<0.1 gNaOH <LOD



<0.1 mg/kg 3.894 <0.389 mg/kg <0.0000389 % <LOD024-008-00-9 237-366-8 13765-19-0


1 <0.1 mg/kg 2.63 <0.263 mg/kg <0.00001 % <LOD027-005-00-0 233-334-2 10124-43-3



<0.1 mg/kg 2.483 <0.248 mg/kg <0.0000248 % <LOD024-006-00-8 232-140-5 7789-00-6


<0.1 mg/kg 1.575 <0.157 mg/kg <0.0000157 % <LOD047-001-00-2 231-853-9 7761-88-8


<0.1 mg/kg 3.523 <0.352 mg/kg <0.0000352 % <LOD024-018-00-3 231-889-5 7775-11-3


081-002-00-9


<0.1 mg/kg 2.602 <0.26 mg/kg <0.000026 % <LOD050-018-00-8 401-640-7 53408-94-9


<0.1 mg/kg 1.785 <0.179 mg/kg <0.0000179 % <LOD023-001-00-8 215-239-8 1314-62-1


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-043-00-3 202-436-9 95-63-6


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-025-00-5 203-604-4 108-67-8



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed



<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-006-00-4 200-663-8 67-66-3

Total: 0.056 %








Classification of sample: CPT 01A



Sample details

Sample Name:CPT 01A










Determinands


#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed


1acenaphthene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 201-469-6 83-32-9

2acenaphthylene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 205-917-1 208-96-8

3anthracene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 204-371-1 120-12-7

4


1 <0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD

051-003-00-9


140 mg/kg 1.32 184.846 mg/kg 0.0185 %033-003-00-0 215-481-4 1327-53-3

6benzene

<20 mg/kg <20 mg/kg <0.002 % <LOD601-020-00-8 200-753-7 71-43-2

7benzo[a]anthracene

0.4 mg/kg 0.4 mg/kg 0.00004 %601-033-00-9 200-280-6 56-55-3


0.5 mg/kg 0.5 mg/kg 0.00005 %601-032-00-3 200-028-5 50-32-8


0.5 mg/kg 0.5 mg/kg 0.00005 %601-034-00-4 205-911-9 205-99-2


0.3 mg/kg 0.3 mg/kg 0.00003 % 205-883-8 191-24-2


0.5 mg/kg 0.5 mg/kg 0.00005 %601-036-00-5 205-916-6 207-08-9



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed



<0.1 mg/kg 2.775 <0.278 mg/kg <0.0000278 % <LOD004-003-00-8 215-133-1 1304-56-9

13


<1 mg/kg 13.43 <13.43 mg/kg <0.00134 % <LOD 10294-33-4,10294-34-5,7637-07-2


1 2 mg/kg 1.285 2.57 mg/kg 0.0002 %048-010-00-4 215-147-8 1306-23-6


215-160-9 1308-38-9


024-001-00-0 215-607-8 1333-82-0

17chrysene

0.5 mg/kg 0.5 mg/kg 0.00005 %601-048-00-0 205-923-4 218-01-9


19


<1 mg/kg 1.884 <1.884 mg/kg <0.000188 % <LOD

006-007-00-5


0.1 mg/kg 0.1 mg/kg 0.00001 %601-041-00-2 200-181-8 53-70-3

21


203-458-1,200-863-5

107-06-2, 75-34-3

22


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 68334-30-5,

68476-34-6,94114-59-7,1159170-26-9

23ethylbenzene

<20 mg/kg <20 mg/kg <0.002 % <LOD601-023-00-4 202-849-4 100-41-4

24fluoranthene

0.8 mg/kg 0.8 mg/kg 0.00008 % 205-912-4 206-44-0

25fluorene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 201-695-5 86-73-7


0.3 mg/kg 0.3 mg/kg 0.00003 % 205-893-2 193-39-5


082-001-00-6


<0.1 mg/kg 2.749 <0.275 mg/kg <0.0000275 % <LOD025-003-00-4 232-089-9 7785-87-7


<1 mg/kg 1.353 <1.353 mg/kg <0.000135 % <LOD080-010-00-X 231-299-8 7487-94-7


<0.1 mg/kg 1.5 <0.15 mg/kg <0.000015 % <LOD042-001-00-9 215-204-7 1313-27-5

31naphthalene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-052-00-2 202-049-5 91-20-3


160 mg/kg 1.579 252.72 mg/kg 0.0253 %028-008-00-X 235-008-5 [1]234-348-1 [2]

12054-48-7 [1]11113-74-9 [2]

33pH

6.9 pH 6.9 pH 6.9 pH PH

34phenanthrene

0.3 mg/kg 0.3 mg/kg 0.00003 % 201-581-5 85-01-8



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed


35phenol

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD604-001-00-2 203-632-7 108-95-2

36pyrene

0.8 mg/kg 0.8 mg/kg 0.00008 % 204-927-3 129-00-0

37


034-002-00-8


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-028-00-4 204-825-9 127-18-4


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-008-00-5 200-262-8 56-23-5

40toluene

<20 mg/kg <20 mg/kg <0.002 % <LOD601-021-00-3 203-625-9 108-88-3


190 mg/kg 190 mg/kg 0.019 % TPH


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-027-00-9 201-167-4 79-01-6


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-023-00-7 200-831-0 75-01-4

44

xylene

<20 mg/kg <20 mg/kg <0.002 % <LOD601-022-00-9 202-422-2 [1]

203-396-5 [2]203-576-3 [3]215-535-7 [4]

95-47-6 [1]106-42-3 [2]108-38-3 [3]1330-20-7 [4]


950 mg/kg 1.245 1182.478 mg/kg 0.118 %030-013-00-7 215-222-5 1314-13-2

46


602-045-00-7 200-024-3 50-29-3

47


602-047-00-8 200-349-0 57-74-9

48


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-043-00-6 210-168-9,

200-401-2,206-270-8,206-271-3

58-89-9, 319-84-6,319-85-7, 608-73-1

49dieldrin (ISO)

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-049-00-9 200-484-5 60-57-1

50


602-051-00-X 200-775-7 72-20-8

51


602-046-00-2 200-962-3 76-44-8

52hexachlorobenzene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-065-00-6 204-273-9 118-74-1

53


606-019-00-6 205-601-3 143-50-0

54aldrin (ISO)

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-048-00-3 206-215-8 309-00-2


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-074-00-5 210-172-0 608-93-5


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-039-00-4 215-648-1 1336-36-3



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed



602-077-00-1 219-196-6 2385-85-5


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-044-00-1 232-283-3 8001-35-2

59hexabromobiphenyl

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 252-994-2 36355-01-8

602,3,7,8-TeCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 217-122-7 1746-01-6

611,2,3,7,8-PeCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 40321-76-4

621,2,3,4,7,8-HxCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 39227-28-6

631,2,3,6,7,8-HxCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57653-85-7

641,2,3,7,8,9-HxCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 19408-74-3

651,2,3,4,6,7,8-HpCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 35822-46-9

66OCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 3268-87-9

672,3,7,8-TeCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 51207-31-9

681,2,3,7,8-PeCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57117-41-6

692,3,4,7,8-PeCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57117-31-4

701,2,3,4,7,8-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 70648-26-9

711,2,3,6,7,8-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57117-44-9

721,2,3,7,8,9-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 72918-21-9

732,3,4,6,7,8-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 60851-34-5

741,2,3,4,6,7,8-HpCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 67562-39-4

751,2,3,4,7,8,9-HpCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 55673-89-7

76OCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 39001-02-0


<0.1gNaOH

<0.1gNaOH

<0.1 gNaOH <LOD



<0.1 mg/kg 3.894 <0.389 mg/kg <0.0000389 % <LOD024-008-00-9 237-366-8 13765-19-0


1 <0.1 mg/kg 2.63 <0.263 mg/kg <0.00001 % <LOD027-005-00-0 233-334-2 10124-43-3



<0.1 mg/kg 2.483 <0.248 mg/kg <0.0000248 % <LOD024-006-00-8 232-140-5 7789-00-6


<0.1 mg/kg 1.575 <0.157 mg/kg <0.0000157 % <LOD047-001-00-2 231-853-9 7761-88-8


<0.1 mg/kg 3.523 <0.352 mg/kg <0.0000352 % <LOD024-018-00-3 231-889-5 7775-11-3



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed



081-002-00-9


<0.1 mg/kg 2.602 <0.26 mg/kg <0.000026 % <LOD050-018-00-8 401-640-7 53408-94-9


120 mg/kg 1.785 214.222 mg/kg 0.0214 %023-001-00-8 215-239-8 1314-62-1


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-043-00-3 202-436-9 95-63-6


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-025-00-5 203-604-4 108-67-8


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-006-00-4 200-663-8 67-66-3

Total: 0.329 %












Sample details

Sample Name:CPT 03A



03)

Hazard properties

None identified

Determinands


#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed


1acenaphthene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 201-469-6 83-32-9

2acenaphthylene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 205-917-1 208-96-8

3anthracene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 204-371-1 120-12-7

4


1 <0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD

051-003-00-9


6 mg/kg 1.32 7.922 mg/kg 0.000792 %033-003-00-0 215-481-4 1327-53-3

6benzene

<10 mg/kg <10 mg/kg <0.001 % <LOD601-020-00-8 200-753-7 71-43-2

7benzo[a]anthracene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-033-00-9 200-280-6 56-55-3


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-032-00-3 200-028-5 50-32-8


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-034-00-4 205-911-9 205-99-2


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 205-883-8 191-24-2


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-036-00-5 205-916-6 207-08-9


<0.1 mg/kg 2.775 <0.278 mg/kg <0.0000278 % <LOD004-003-00-8 215-133-1 1304-56-9

13


<1 mg/kg 13.43 <13.43 mg/kg <0.00134 % <LOD 10294-33-4,10294-34-5,7637-07-2


1 <1 mg/kg 1.285 <1.285 mg/kg <0.0001 % <LOD048-010-00-4 215-147-8 1306-23-6



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed



215-160-9 1308-38-9


024-001-00-0 215-607-8 1333-82-0

17chrysene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-048-00-0 205-923-4 218-01-9


19


<1 mg/kg 1.884 <1.884 mg/kg <0.000188 % <LOD

006-007-00-5


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-041-00-2 200-181-8 53-70-3

21


203-458-1,200-863-5

107-06-2, 75-34-3

22


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 68334-30-5,

68476-34-6,94114-59-7,1159170-26-9

23ethylbenzene

<10 mg/kg <10 mg/kg <0.001 % <LOD601-023-00-4 202-849-4 100-41-4

24fluoranthene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 205-912-4 206-44-0

25fluorene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 201-695-5 86-73-7


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 205-893-2 193-39-5


082-001-00-6


<0.1 mg/kg 2.749 <0.275 mg/kg <0.0000275 % <LOD025-003-00-4 232-089-9 7785-87-7


<1 mg/kg 1.353 <1.353 mg/kg <0.000135 % <LOD080-010-00-X 231-299-8 7487-94-7


<0.1 mg/kg 1.5 <0.15 mg/kg <0.000015 % <LOD042-001-00-9 215-204-7 1313-27-5

31naphthalene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-052-00-2 202-049-5 91-20-3


28 mg/kg 1.579 44.226 mg/kg 0.00442 %028-008-00-X 235-008-5 [1]234-348-1 [2]

12054-48-7 [1]11113-74-9 [2]

33pH

7.7 pH 7.7 pH 7.7 pH PH

34phenanthrene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 201-581-5 85-01-8

35phenol

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD604-001-00-2 203-632-7 108-95-2

36pyrene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 204-927-3 129-00-0

37


034-002-00-8



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed



<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-028-00-4 204-825-9 127-18-4


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-008-00-5 200-262-8 56-23-5

40toluene

<10 mg/kg <10 mg/kg <0.001 % <LOD601-021-00-3 203-625-9 108-88-3


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-027-00-9 201-167-4 79-01-6


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-023-00-7 200-831-0 75-01-4

43

xylene

<10 mg/kg <10 mg/kg <0.001 % <LOD601-022-00-9 202-422-2 [1]

203-396-5 [2]203-576-3 [3]215-535-7 [4]

95-47-6 [1]106-42-3 [2]108-38-3 [3]1330-20-7 [4]


47 mg/kg 1.245 58.502 mg/kg 0.00585 %030-013-00-7 215-222-5 1314-13-2

45


602-045-00-7 200-024-3 50-29-3

46


602-047-00-8 200-349-0 57-74-9

47


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-043-00-6 210-168-9,

200-401-2,206-270-8,206-271-3

58-89-9, 319-84-6,319-85-7, 608-73-1

48dieldrin (ISO)

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-049-00-9 200-484-5 60-57-1

49


602-051-00-X 200-775-7 72-20-8

50


602-046-00-2 200-962-3 76-44-8

51hexachlorobenzene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-065-00-6 204-273-9 118-74-1

52

chlordecone (ISO);perchloropentacyclo[5,3,0,02,6,03,9,04,8]decan-5-one;decachloropentacyclo[5,2,1,02,6,03,9,05,8]decan-4-one

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD

606-019-00-6 205-601-3 143-50-0

53aldrin (ISO)

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-048-00-3 206-215-8 309-00-2


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-074-00-5 210-172-0 608-93-5


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-039-00-4 215-648-1 1336-36-3


602-077-00-1 219-196-6 2385-85-5


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-044-00-1 232-283-3 8001-35-2

58hexabromobiphenyl

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 252-994-2 36355-01-8

592,3,7,8-TeCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 217-122-7 1746-01-6

601,2,3,7,8-PeCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 40321-76-4



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed


611,2,3,4,7,8-HxCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 39227-28-6

621,2,3,6,7,8-HxCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57653-85-7

631,2,3,7,8,9-HxCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 19408-74-3

641,2,3,4,6,7,8-HpCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 35822-46-9

65OCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 3268-87-9

662,3,7,8-TeCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 51207-31-9

671,2,3,7,8-PeCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57117-41-6

682,3,4,7,8-PeCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57117-31-4

691,2,3,4,7,8-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 70648-26-9

701,2,3,6,7,8-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57117-44-9

711,2,3,7,8,9-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 72918-21-9

722,3,4,6,7,8-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 60851-34-5

731,2,3,4,6,7,8-HpCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 67562-39-4

741,2,3,4,7,8,9-HpCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 55673-89-7

75OCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 39001-02-0


<0.1gNaOH

<0.1gNaOH

<0.1 gNaOH <LOD



<0.1 mg/kg 3.894 <0.389 mg/kg <0.0000389 % <LOD024-008-00-9 237-366-8 13765-19-0


1 <0.1 mg/kg 2.63 <0.263 mg/kg <0.00001 % <LOD027-005-00-0 233-334-2 10124-43-3



<0.1 mg/kg 2.483 <0.248 mg/kg <0.0000248 % <LOD024-006-00-8 232-140-5 7789-00-6


<0.1 mg/kg 1.575 <0.157 mg/kg <0.0000157 % <LOD047-001-00-2 231-853-9 7761-88-8


<0.1 mg/kg 3.523 <0.352 mg/kg <0.0000352 % <LOD024-018-00-3 231-889-5 7775-11-3


081-002-00-9


<0.1 mg/kg 2.602 <0.26 mg/kg <0.000026 % <LOD050-018-00-8 401-640-7 53408-94-9


27 mg/kg 1.785 48.2 mg/kg 0.00482 %023-001-00-8 215-239-8 1314-62-1


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-043-00-3 202-436-9 95-63-6


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-025-00-5 203-604-4 108-67-8


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-006-00-4 200-663-8 67-66-3



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed


Total: 0.0324 %











Sample details

Sample Name:CPT 14A










Determinands


#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed


1acenaphthene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 201-469-6 83-32-9

2acenaphthylene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 205-917-1 208-96-8

3anthracene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 204-371-1 120-12-7

4


1 <0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD

051-003-00-9


22 mg/kg 1.32 29.047 mg/kg 0.0029 %033-003-00-0 215-481-4 1327-53-3

6benzene

<10 mg/kg <10 mg/kg <0.001 % <LOD601-020-00-8 200-753-7 71-43-2

7benzo[a]anthracene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-033-00-9 200-280-6 56-55-3


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-032-00-3 200-028-5 50-32-8


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-034-00-4 205-911-9 205-99-2


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 205-883-8 191-24-2


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-036-00-5 205-916-6 207-08-9



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed



<0.1 mg/kg 2.775 <0.278 mg/kg <0.0000278 % <LOD004-003-00-8 215-133-1 1304-56-9

13


<1 mg/kg 13.43 <13.43 mg/kg <0.00134 % <LOD 10294-33-4,10294-34-5,7637-07-2


1 1 mg/kg 1.285 1.285 mg/kg 0.0001 %048-010-00-4 215-147-8 1306-23-6


215-160-9 1308-38-9


024-001-00-0 215-607-8 1333-82-0

17chrysene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-048-00-0 205-923-4 218-01-9


19


<1 mg/kg 1.884 <1.884 mg/kg <0.000188 % <LOD

006-007-00-5


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-041-00-2 200-181-8 53-70-3

21


203-458-1,200-863-5

107-06-2, 75-34-3

22


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 68334-30-5,

68476-34-6,94114-59-7,1159170-26-9

23ethylbenzene

<10 mg/kg <10 mg/kg <0.001 % <LOD601-023-00-4 202-849-4 100-41-4

24fluoranthene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 205-912-4 206-44-0

25fluorene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 201-695-5 86-73-7


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 205-893-2 193-39-5


082-001-00-6


<0.1 mg/kg 2.749 <0.275 mg/kg <0.0000275 % <LOD025-003-00-4 232-089-9 7785-87-7


<1 mg/kg 1.353 <1.353 mg/kg <0.000135 % <LOD080-010-00-X 231-299-8 7487-94-7


<0.1 mg/kg 1.5 <0.15 mg/kg <0.000015 % <LOD042-001-00-9 215-204-7 1313-27-5

31naphthalene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-052-00-2 202-049-5 91-20-3


34 mg/kg 1.579 53.703 mg/kg 0.00537 %028-008-00-X 235-008-5 [1]234-348-1 [2]

12054-48-7 [1]11113-74-9 [2]

33pH

7.9 pH 7.9 pH 7.9 pH PH

34phenanthrene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 201-581-5 85-01-8



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed


35phenol

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD604-001-00-2 203-632-7 108-95-2

36pyrene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 204-927-3 129-00-0

37


034-002-00-8


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-028-00-4 204-825-9 127-18-4


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-008-00-5 200-262-8 56-23-5

40toluene

<10 mg/kg <10 mg/kg <0.001 % <LOD601-021-00-3 203-625-9 108-88-3


35 mg/kg 35 mg/kg 0.0035 % TPH


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-027-00-9 201-167-4 79-01-6


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-023-00-7 200-831-0 75-01-4

44

xylene

<10 mg/kg <10 mg/kg <0.001 % <LOD601-022-00-9 202-422-2 [1]

203-396-5 [2]203-576-3 [3]215-535-7 [4]

95-47-6 [1]106-42-3 [2]108-38-3 [3]1330-20-7 [4]


270 mg/kg 1.245 336.073 mg/kg 0.0336 %030-013-00-7 215-222-5 1314-13-2

46


602-045-00-7 200-024-3 50-29-3

47


602-047-00-8 200-349-0 57-74-9

48


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-043-00-6 210-168-9,

200-401-2,206-270-8,206-271-3

58-89-9, 319-84-6,319-85-7, 608-73-1

49dieldrin (ISO)

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-049-00-9 200-484-5 60-57-1

50


602-051-00-X 200-775-7 72-20-8

51


602-046-00-2 200-962-3 76-44-8

52hexachlorobenzene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-065-00-6 204-273-9 118-74-1

53


606-019-00-6 205-601-3 143-50-0

54aldrin (ISO)

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-048-00-3 206-215-8 309-00-2


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-074-00-5 210-172-0 608-93-5


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-039-00-4 215-648-1 1336-36-3



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed



602-077-00-1 219-196-6 2385-85-5


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-044-00-1 232-283-3 8001-35-2

59hexabromobiphenyl

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 252-994-2 36355-01-8

602,3,7,8-TeCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 217-122-7 1746-01-6

611,2,3,7,8-PeCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 40321-76-4

621,2,3,4,7,8-HxCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 39227-28-6

631,2,3,6,7,8-HxCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57653-85-7

641,2,3,7,8,9-HxCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 19408-74-3

651,2,3,4,6,7,8-HpCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 35822-46-9

66OCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 3268-87-9

672,3,7,8-TeCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 51207-31-9

681,2,3,7,8-PeCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57117-41-6

692,3,4,7,8-PeCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57117-31-4

701,2,3,4,7,8-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 70648-26-9

711,2,3,6,7,8-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57117-44-9

721,2,3,7,8,9-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 72918-21-9

732,3,4,6,7,8-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 60851-34-5

741,2,3,4,6,7,8-HpCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 67562-39-4

751,2,3,4,7,8,9-HpCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 55673-89-7

76OCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 39001-02-0


<0.1gNaOH

<0.1gNaOH

<0.1 gNaOH <LOD



<0.1 mg/kg 3.894 <0.389 mg/kg <0.0000389 % <LOD024-008-00-9 237-366-8 13765-19-0


1 <0.1 mg/kg 2.63 <0.263 mg/kg <0.00001 % <LOD027-005-00-0 233-334-2 10124-43-3



<0.1 mg/kg 2.483 <0.248 mg/kg <0.0000248 % <LOD024-006-00-8 232-140-5 7789-00-6


<0.1 mg/kg 1.575 <0.157 mg/kg <0.0000157 % <LOD047-001-00-2 231-853-9 7761-88-8


<0.1 mg/kg 3.523 <0.352 mg/kg <0.0000352 % <LOD024-018-00-3 231-889-5 7775-11-3



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed



081-002-00-9


<0.1 mg/kg 2.602 <0.26 mg/kg <0.000026 % <LOD050-018-00-8 401-640-7 53408-94-9


31 mg/kg 1.785 55.341 mg/kg 0.00553 %023-001-00-8 215-239-8 1314-62-1


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-043-00-3 202-436-9 95-63-6


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-025-00-5 203-604-4 108-67-8


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-006-00-4 200-663-8 67-66-3

Total: 0.079 %









Classification of sample: CPT 14A[1]



Sample details

Sample Name:CPT 14A[1]










Determinands


#Determinand

CLP

Not

e



valueM

CA

pplie

dConc. Not


1acenaphthene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 201-469-6 83-32-9

2acenaphthylene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 205-917-1 208-96-8

3anthracene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 204-371-1 120-12-7

4


1 <0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD

051-003-00-9


24 mg/kg 1.32 31.688 mg/kg 0.00317 %033-003-00-0 215-481-4 1327-53-3

6benzene

<10 mg/kg <10 mg/kg <0.001 % <LOD601-020-00-8 200-753-7 71-43-2

7benzo[a]anthracene

0.2 mg/kg 0.2 mg/kg 0.00002 %601-033-00-9 200-280-6 56-55-3


0.2 mg/kg 0.2 mg/kg 0.00002 %601-032-00-3 200-028-5 50-32-8


0.2 mg/kg 0.2 mg/kg 0.00002 %601-034-00-4 205-911-9 205-99-2


0.1 mg/kg 0.1 mg/kg 0.00001 % 205-883-8 191-24-2


0.2 mg/kg 0.2 mg/kg 0.00002 %601-036-00-5 205-916-6 207-08-9



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed



<0.1 mg/kg 2.775 <0.278 mg/kg <0.0000278 % <LOD004-003-00-8 215-133-1 1304-56-9

13


<1 mg/kg 13.43 <13.43 mg/kg <0.00134 % <LOD 10294-33-4,10294-34-5,7637-07-2


1 4 mg/kg 1.285 5.141 mg/kg 0.0004 %048-010-00-4 215-147-8 1306-23-6


215-160-9 1308-38-9


024-001-00-0 215-607-8 1333-82-0

17chrysene

0.3 mg/kg 0.3 mg/kg 0.00003 %601-048-00-0 205-923-4 218-01-9


19


7 mg/kg 1.884 13.188 mg/kg 0.00132 %

006-007-00-5


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-041-00-2 200-181-8 53-70-3

21


203-458-1,200-863-5

107-06-2, 75-34-3

22


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 68334-30-5,

68476-34-6,94114-59-7,1159170-26-9

23ethylbenzene

<10 mg/kg <10 mg/kg <0.001 % <LOD601-023-00-4 202-849-4 100-41-4

24fluoranthene

0.5 mg/kg 0.5 mg/kg 0.00005 % 205-912-4 206-44-0

25fluorene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 201-695-5 86-73-7


0.1 mg/kg 0.1 mg/kg 0.00001 % 205-893-2 193-39-5


082-001-00-6


<0.1 mg/kg 2.749 <0.275 mg/kg <0.0000275 % <LOD025-003-00-4 232-089-9 7785-87-7


<1 mg/kg 1.353 <1.353 mg/kg <0.000135 % <LOD080-010-00-X 231-299-8 7487-94-7


<0.1 mg/kg 1.5 <0.15 mg/kg <0.000015 % <LOD042-001-00-9 215-204-7 1313-27-5

31naphthalene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-052-00-2 202-049-5 91-20-3


18 mg/kg 1.579 28.431 mg/kg 0.00284 %028-008-00-X 235-008-5 [1]234-348-1 [2]

12054-48-7 [1]11113-74-9 [2]

33pH

7.8 pH 7.8 pH 7.8 pH PH

34phenanthrene

0.2 mg/kg 0.2 mg/kg 0.00002 % 201-581-5 85-01-8



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed


35phenol

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD604-001-00-2 203-632-7 108-95-2

36pyrene

0.5 mg/kg 0.5 mg/kg 0.00005 % 204-927-3 129-00-0

37


034-002-00-8


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-028-00-4 204-825-9 127-18-4


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-008-00-5 200-262-8 56-23-5

40toluene

<10 mg/kg <10 mg/kg <0.001 % <LOD601-021-00-3 203-625-9 108-88-3


26 mg/kg 26 mg/kg 0.0026 % TPH


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-027-00-9 201-167-4 79-01-6


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-023-00-7 200-831-0 75-01-4

44

xylene

<10 mg/kg <10 mg/kg <0.001 % <LOD601-022-00-9 202-422-2 [1]

203-396-5 [2]203-576-3 [3]215-535-7 [4]

95-47-6 [1]106-42-3 [2]108-38-3 [3]1330-20-7 [4]


760 mg/kg 1.245 945.983 mg/kg 0.0946 %030-013-00-7 215-222-5 1314-13-2

46


602-045-00-7 200-024-3 50-29-3

47


602-047-00-8 200-349-0 57-74-9

48


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-043-00-6 210-168-9,

200-401-2,206-270-8,206-271-3

58-89-9, 319-84-6,319-85-7, 608-73-1

49dieldrin (ISO)

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-049-00-9 200-484-5 60-57-1

50


602-051-00-X 200-775-7 72-20-8

51


602-046-00-2 200-962-3 76-44-8

52hexachlorobenzene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-065-00-6 204-273-9 118-74-1

53


606-019-00-6 205-601-3 143-50-0

54aldrin (ISO)

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-048-00-3 206-215-8 309-00-2


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-074-00-5 210-172-0 608-93-5


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-039-00-4 215-648-1 1336-36-3



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed



602-077-00-1 219-196-6 2385-85-5


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-044-00-1 232-283-3 8001-35-2

59hexabromobiphenyl

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 252-994-2 36355-01-8

602,3,7,8-TeCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 217-122-7 1746-01-6

611,2,3,7,8-PeCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 40321-76-4

621,2,3,4,7,8-HxCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 39227-28-6

631,2,3,6,7,8-HxCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57653-85-7

641,2,3,7,8,9-HxCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 19408-74-3

651,2,3,4,6,7,8-HpCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 35822-46-9

66OCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 3268-87-9

672,3,7,8-TeCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 51207-31-9

681,2,3,7,8-PeCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57117-41-6

692,3,4,7,8-PeCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57117-31-4

701,2,3,4,7,8-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 70648-26-9

711,2,3,6,7,8-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57117-44-9

721,2,3,7,8,9-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 72918-21-9

732,3,4,6,7,8-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 60851-34-5

741,2,3,4,6,7,8-HpCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 67562-39-4

751,2,3,4,7,8,9-HpCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 55673-89-7

76OCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 39001-02-0


<0.1gNaOH

<0.1gNaOH

<0.1 gNaOH <LOD



<0.1 mg/kg 3.894 <0.389 mg/kg <0.0000389 % <LOD024-008-00-9 237-366-8 13765-19-0


1 <0.1 mg/kg 2.63 <0.263 mg/kg <0.00001 % <LOD027-005-00-0 233-334-2 10124-43-3



<0.1 mg/kg 2.483 <0.248 mg/kg <0.0000248 % <LOD024-006-00-8 232-140-5 7789-00-6


<0.1 mg/kg 1.575 <0.157 mg/kg <0.0000157 % <LOD047-001-00-2 231-853-9 7761-88-8


<0.1 mg/kg 3.523 <0.352 mg/kg <0.0000352 % <LOD024-018-00-3 231-889-5 7775-11-3



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed



081-002-00-9


<0.1 mg/kg 2.602 <0.26 mg/kg <0.000026 % <LOD050-018-00-8 401-640-7 53408-94-9


17 mg/kg 1.785 30.348 mg/kg 0.00303 %023-001-00-8 215-239-8 1314-62-1


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-043-00-3 202-436-9 95-63-6


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-025-00-5 203-604-4 108-67-8


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-006-00-4 200-663-8 67-66-3

Total: 0.142 %












Sample details











Determinands


#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed


1acenaphthene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 201-469-6 83-32-9

2acenaphthylene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 205-917-1 208-96-8

3anthracene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 204-371-1 120-12-7

4


1 <0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD

051-003-00-9


47 mg/kg 1.32 62.055 mg/kg 0.00621 %033-003-00-0 215-481-4 1327-53-3

6benzene

<10 mg/kg <10 mg/kg <0.001 % <LOD601-020-00-8 200-753-7 71-43-2

7benzo[a]anthracene

0.2 mg/kg 0.2 mg/kg 0.00002 %601-033-00-9 200-280-6 56-55-3


0.1 mg/kg 0.1 mg/kg 0.00001 %601-032-00-3 200-028-5 50-32-8


0.1 mg/kg 0.1 mg/kg 0.00001 %601-034-00-4 205-911-9 205-99-2


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 205-883-8 191-24-2


0.2 mg/kg 0.2 mg/kg 0.00002 %601-036-00-5 205-916-6 207-08-9



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed



<0.1 mg/kg 2.775 <0.278 mg/kg <0.0000278 % <LOD004-003-00-8 215-133-1 1304-56-9

13


<1 mg/kg 13.43 <13.43 mg/kg <0.00134 % <LOD 10294-33-4,10294-34-5,7637-07-2


1 2 mg/kg 1.285 2.57 mg/kg 0.0002 %048-010-00-4 215-147-8 1306-23-6


215-160-9 1308-38-9


024-001-00-0 215-607-8 1333-82-0

17chrysene

0.2 mg/kg 0.2 mg/kg 0.00002 %601-048-00-0 205-923-4 218-01-9


19


8 mg/kg 1.884 15.072 mg/kg 0.00151 %

006-007-00-5


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-041-00-2 200-181-8 53-70-3

21


203-458-1,200-863-5

107-06-2, 75-34-3

22


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 68334-30-5,

68476-34-6,94114-59-7,1159170-26-9

23ethylbenzene

<10 mg/kg <10 mg/kg <0.001 % <LOD601-023-00-4 202-849-4 100-41-4

24fluoranthene

0.4 mg/kg 0.4 mg/kg 0.00004 % 205-912-4 206-44-0

25fluorene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 201-695-5 86-73-7


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 205-893-2 193-39-5


082-001-00-6


<0.1 mg/kg 2.749 <0.275 mg/kg <0.0000275 % <LOD025-003-00-4 232-089-9 7785-87-7


2 mg/kg 1.353 2.707 mg/kg 0.000271 %080-010-00-X 231-299-8 7487-94-7


<0.1 mg/kg 1.5 <0.15 mg/kg <0.000015 % <LOD042-001-00-9 215-204-7 1313-27-5

31naphthalene

0.1 mg/kg 0.1 mg/kg 0.00001 %601-052-00-2 202-049-5 91-20-3


25 mg/kg 1.579 39.487 mg/kg 0.00395 %028-008-00-X 235-008-5 [1]234-348-1 [2]

12054-48-7 [1]11113-74-9 [2]

33pH

7.5 pH 7.5 pH 7.5 pH PH

34phenanthrene

0.3 mg/kg 0.3 mg/kg 0.00003 % 201-581-5 85-01-8



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed


35phenol

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD604-001-00-2 203-632-7 108-95-2

36pyrene

0.3 mg/kg 0.3 mg/kg 0.00003 % 204-927-3 129-00-0

37


034-002-00-8


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-028-00-4 204-825-9 127-18-4


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-008-00-5 200-262-8 56-23-5

40toluene

<10 mg/kg <10 mg/kg <0.001 % <LOD601-021-00-3 203-625-9 108-88-3


22 mg/kg 22 mg/kg 0.0022 % TPH


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-027-00-9 201-167-4 79-01-6


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-023-00-7 200-831-0 75-01-4

44

xylene

<10 mg/kg <10 mg/kg <0.001 % <LOD601-022-00-9 202-422-2 [1]

203-396-5 [2]203-576-3 [3]215-535-7 [4]

95-47-6 [1]106-42-3 [2]108-38-3 [3]1330-20-7 [4]


720 mg/kg 1.245 896.194 mg/kg 0.0896 %030-013-00-7 215-222-5 1314-13-2

46


602-045-00-7 200-024-3 50-29-3

47


602-047-00-8 200-349-0 57-74-9

48


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-043-00-6 210-168-9,

200-401-2,206-270-8,206-271-3

58-89-9, 319-84-6,319-85-7, 608-73-1

49dieldrin (ISO)

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-049-00-9 200-484-5 60-57-1

50


602-051-00-X 200-775-7 72-20-8

51


602-046-00-2 200-962-3 76-44-8

52hexachlorobenzene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-065-00-6 204-273-9 118-74-1

53


606-019-00-6 205-601-3 143-50-0

54aldrin (ISO)

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-048-00-3 206-215-8 309-00-2


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-074-00-5 210-172-0 608-93-5


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-039-00-4 215-648-1 1336-36-3



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed



602-077-00-1 219-196-6 2385-85-5


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-044-00-1 232-283-3 8001-35-2

59hexabromobiphenyl

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 252-994-2 36355-01-8

602,3,7,8-TeCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 217-122-7 1746-01-6

611,2,3,7,8-PeCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 40321-76-4

621,2,3,4,7,8-HxCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 39227-28-6

631,2,3,6,7,8-HxCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57653-85-7

641,2,3,7,8,9-HxCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 19408-74-3

651,2,3,4,6,7,8-HpCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 35822-46-9

66OCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 3268-87-9

672,3,7,8-TeCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 51207-31-9

681,2,3,7,8-PeCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57117-41-6

692,3,4,7,8-PeCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57117-31-4

701,2,3,4,7,8-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 70648-26-9

711,2,3,6,7,8-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57117-44-9

721,2,3,7,8,9-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 72918-21-9

732,3,4,6,7,8-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 60851-34-5

741,2,3,4,6,7,8-HpCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 67562-39-4

751,2,3,4,7,8,9-HpCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 55673-89-7

76OCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 39001-02-0


<0.1gNaOH

<0.1gNaOH

<0.1 gNaOH <LOD



<0.1 mg/kg 3.894 <0.389 mg/kg <0.0000389 % <LOD024-008-00-9 237-366-8 13765-19-0


1 <0.1 mg/kg 2.63 <0.263 mg/kg <0.00001 % <LOD027-005-00-0 233-334-2 10124-43-3



<0.1 mg/kg 2.483 <0.248 mg/kg <0.0000248 % <LOD024-006-00-8 232-140-5 7789-00-6


<0.1 mg/kg 1.575 <0.157 mg/kg <0.0000157 % <LOD047-001-00-2 231-853-9 7761-88-8


<0.1 mg/kg 3.523 <0.352 mg/kg <0.0000352 % <LOD024-018-00-3 231-889-5 7775-11-3



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed



081-002-00-9


<0.1 mg/kg 2.602 <0.26 mg/kg <0.000026 % <LOD050-018-00-8 401-640-7 53408-94-9


25 mg/kg 1.785 44.63 mg/kg 0.00446 %023-001-00-8 215-239-8 1314-62-1


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-043-00-3 202-436-9 95-63-6


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-025-00-5 203-604-4 108-67-8


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-006-00-4 200-663-8 67-66-3

Total: 0.152 %












Sample details

Sample Name:CPT 15A










Determinands


#Determinand

CLP

Not

e



valueM

CA

pplie

dConc. Not


1acenaphthene

0.1 mg/kg 0.1 mg/kg 0.00001 % 201-469-6 83-32-9

2acenaphthylene

0.3 mg/kg 0.3 mg/kg 0.00003 % 205-917-1 208-96-8

3anthracene

0.2 mg/kg 0.2 mg/kg 0.00002 % 204-371-1 120-12-7

4


1 <0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD

051-003-00-9


48 mg/kg 1.32 63.376 mg/kg 0.00634 %033-003-00-0 215-481-4 1327-53-3

6benzene

<10 mg/kg <10 mg/kg <0.001 % <LOD601-020-00-8 200-753-7 71-43-2

7benzo[a]anthracene

0.7 mg/kg 0.7 mg/kg 0.00007 %601-033-00-9 200-280-6 56-55-3


1 mg/kg 1 mg/kg 0.0001 %601-032-00-3 200-028-5 50-32-8


1 mg/kg 1 mg/kg 0.0001 %601-034-00-4 205-911-9 205-99-2


0.7 mg/kg 0.7 mg/kg 0.00007 % 205-883-8 191-24-2


0.8 mg/kg 0.8 mg/kg 0.00008 %601-036-00-5 205-916-6 207-08-9



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed



<0.1 mg/kg 2.775 <0.278 mg/kg <0.0000278 % <LOD004-003-00-8 215-133-1 1304-56-9

13


<1 mg/kg 13.43 <13.43 mg/kg <0.00134 % <LOD 10294-33-4,10294-34-5,7637-07-2


1 5 mg/kg 1.285 6.426 mg/kg 0.0005 %048-010-00-4 215-147-8 1306-23-6


215-160-9 1308-38-9


024-001-00-0 215-607-8 1333-82-0

17chrysene

0.8 mg/kg 0.8 mg/kg 0.00008 %601-048-00-0 205-923-4 218-01-9


19


15 mg/kg 1.884 28.26 mg/kg 0.00283 %

006-007-00-5


0.2 mg/kg 0.2 mg/kg 0.00002 %601-041-00-2 200-181-8 53-70-3

21


203-458-1,200-863-5

107-06-2, 75-34-3

22


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 68334-30-5,

68476-34-6,94114-59-7,1159170-26-9

23ethylbenzene

<10 mg/kg <10 mg/kg <0.001 % <LOD601-023-00-4 202-849-4 100-41-4

24fluoranthene

1.3 mg/kg 1.3 mg/kg 0.00013 % 205-912-4 206-44-0

25fluorene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 201-695-5 86-73-7


0.7 mg/kg 0.7 mg/kg 0.00007 % 205-893-2 193-39-5


082-001-00-6


<0.1 mg/kg 2.749 <0.275 mg/kg <0.0000275 % <LOD025-003-00-4 232-089-9 7785-87-7


2 mg/kg 1.353 2.707 mg/kg 0.000271 %080-010-00-X 231-299-8 7487-94-7


<0.1 mg/kg 1.5 <0.15 mg/kg <0.000015 % <LOD042-001-00-9 215-204-7 1313-27-5

31naphthalene

0.2 mg/kg 0.2 mg/kg 0.00002 %601-052-00-2 202-049-5 91-20-3


32 mg/kg 1.579 50.544 mg/kg 0.00505 %028-008-00-X 235-008-5 [1]234-348-1 [2]

12054-48-7 [1]11113-74-9 [2]

33pH

7.3 pH 7.3 pH 7.3 pH PH

34phenanthrene

0.6 mg/kg 0.6 mg/kg 0.00006 % 201-581-5 85-01-8



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed


35phenol

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD604-001-00-2 203-632-7 108-95-2

36pyrene

1.2 mg/kg 1.2 mg/kg 0.00012 % 204-927-3 129-00-0

37


034-002-00-8


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-028-00-4 204-825-9 127-18-4


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-008-00-5 200-262-8 56-23-5

40toluene

<10 mg/kg <10 mg/kg <0.001 % <LOD601-021-00-3 203-625-9 108-88-3


140 mg/kg 140 mg/kg 0.014 % TPH


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-027-00-9 201-167-4 79-01-6


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-023-00-7 200-831-0 75-01-4

44

xylene

<10 mg/kg <10 mg/kg <0.001 % <LOD601-022-00-9 202-422-2 [1]

203-396-5 [2]203-576-3 [3]215-535-7 [4]

95-47-6 [1]106-42-3 [2]108-38-3 [3]1330-20-7 [4]


900 mg/kg 1.245 1120.243 mg/kg 0.112 %030-013-00-7 215-222-5 1314-13-2

46


602-045-00-7 200-024-3 50-29-3

47


602-047-00-8 200-349-0 57-74-9

48


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-043-00-6 210-168-9,

200-401-2,206-270-8,206-271-3

58-89-9, 319-84-6,319-85-7, 608-73-1

49dieldrin (ISO)

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-049-00-9 200-484-5 60-57-1

50


602-051-00-X 200-775-7 72-20-8

51


602-046-00-2 200-962-3 76-44-8

52hexachlorobenzene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-065-00-6 204-273-9 118-74-1

53


606-019-00-6 205-601-3 143-50-0

54aldrin (ISO)

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-048-00-3 206-215-8 309-00-2


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-074-00-5 210-172-0 608-93-5


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-039-00-4 215-648-1 1336-36-3



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed



602-077-00-1 219-196-6 2385-85-5


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-044-00-1 232-283-3 8001-35-2

59hexabromobiphenyl

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 252-994-2 36355-01-8

602,3,7,8-TeCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 217-122-7 1746-01-6

611,2,3,7,8-PeCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 40321-76-4

621,2,3,4,7,8-HxCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 39227-28-6

631,2,3,6,7,8-HxCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57653-85-7

641,2,3,7,8,9-HxCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 19408-74-3

651,2,3,4,6,7,8-HpCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 35822-46-9

66OCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 3268-87-9

672,3,7,8-TeCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 51207-31-9

681,2,3,7,8-PeCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57117-41-6

692,3,4,7,8-PeCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57117-31-4

701,2,3,4,7,8-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 70648-26-9

711,2,3,6,7,8-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57117-44-9

721,2,3,7,8,9-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 72918-21-9

732,3,4,6,7,8-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 60851-34-5

741,2,3,4,6,7,8-HpCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 67562-39-4

751,2,3,4,7,8,9-HpCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 55673-89-7

76OCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 39001-02-0


<0.1gNaOH

<0.1gNaOH

<0.1 gNaOH <LOD



<0.1 mg/kg 3.894 <0.389 mg/kg <0.0000389 % <LOD024-008-00-9 237-366-8 13765-19-0


1 <0.1 mg/kg 2.63 <0.263 mg/kg <0.00001 % <LOD027-005-00-0 233-334-2 10124-43-3



<0.1 mg/kg 2.483 <0.248 mg/kg <0.0000248 % <LOD024-006-00-8 232-140-5 7789-00-6


<0.1 mg/kg 1.575 <0.157 mg/kg <0.0000157 % <LOD047-001-00-2 231-853-9 7761-88-8


<0.1 mg/kg 3.523 <0.352 mg/kg <0.0000352 % <LOD024-018-00-3 231-889-5 7775-11-3



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed



081-002-00-9


<0.1 mg/kg 2.602 <0.26 mg/kg <0.000026 % <LOD050-018-00-8 401-640-7 53408-94-9


31 mg/kg 1.785 55.341 mg/kg 0.00553 %023-001-00-8 215-239-8 1314-62-1


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-043-00-3 202-436-9 95-63-6


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-025-00-5 203-604-4 108-67-8


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-006-00-4 200-663-8 67-66-3

Total: 0.2 %












Sample details











Determinands


#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed


1acenaphthene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 201-469-6 83-32-9

2acenaphthylene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 205-917-1 208-96-8

3anthracene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 204-371-1 120-12-7

4


1 <0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD

051-003-00-9


21 mg/kg 1.32 27.727 mg/kg 0.00277 %033-003-00-0 215-481-4 1327-53-3

6benzene

<10 mg/kg <10 mg/kg <0.001 % <LOD601-020-00-8 200-753-7 71-43-2

7benzo[a]anthracene

0.2 mg/kg 0.2 mg/kg 0.00002 %601-033-00-9 200-280-6 56-55-3


0.2 mg/kg 0.2 mg/kg 0.00002 %601-032-00-3 200-028-5 50-32-8


0.2 mg/kg 0.2 mg/kg 0.00002 %601-034-00-4 205-911-9 205-99-2


0.1 mg/kg 0.1 mg/kg 0.00001 % 205-883-8 191-24-2


0.2 mg/kg 0.2 mg/kg 0.00002 %601-036-00-5 205-916-6 207-08-9



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed



<0.1 mg/kg 2.775 <0.278 mg/kg <0.0000278 % <LOD004-003-00-8 215-133-1 1304-56-9

13


<1 mg/kg 13.43 <13.43 mg/kg <0.00134 % <LOD 10294-33-4,10294-34-5,7637-07-2


1 2 mg/kg 1.285 2.57 mg/kg 0.0002 %048-010-00-4 215-147-8 1306-23-6


215-160-9 1308-38-9


024-001-00-0 215-607-8 1333-82-0

17chrysene

0.2 mg/kg 0.2 mg/kg 0.00002 %601-048-00-0 205-923-4 218-01-9


19


42 mg/kg 1.884 79.128 mg/kg 0.00791 %

006-007-00-5


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-041-00-2 200-181-8 53-70-3

21


203-458-1,200-863-5

107-06-2, 75-34-3

22


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 68334-30-5,

68476-34-6,94114-59-7,1159170-26-9

23ethylbenzene

<10 mg/kg <10 mg/kg <0.001 % <LOD601-023-00-4 202-849-4 100-41-4

24fluoranthene

0.3 mg/kg 0.3 mg/kg 0.00003 % 205-912-4 206-44-0

25fluorene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 201-695-5 86-73-7


0.1 mg/kg 0.1 mg/kg 0.00001 % 205-893-2 193-39-5


082-001-00-6


<0.1 mg/kg 2.749 <0.275 mg/kg <0.0000275 % <LOD025-003-00-4 232-089-9 7785-87-7


<1 mg/kg 1.353 <1.353 mg/kg <0.000135 % <LOD080-010-00-X 231-299-8 7487-94-7


<0.1 mg/kg 1.5 <0.15 mg/kg <0.000015 % <LOD042-001-00-9 215-204-7 1313-27-5

31naphthalene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-052-00-2 202-049-5 91-20-3


14 mg/kg 1.579 22.113 mg/kg 0.00221 %028-008-00-X 235-008-5 [1]234-348-1 [2]

12054-48-7 [1]11113-74-9 [2]

33pH

7.4 pH 7.4 pH 7.4 pH PH

34phenanthrene

0.1 mg/kg 0.1 mg/kg 0.00001 % 201-581-5 85-01-8



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed


35phenol

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD604-001-00-2 203-632-7 108-95-2

36pyrene

0.3 mg/kg 0.3 mg/kg 0.00003 % 204-927-3 129-00-0

37


034-002-00-8


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-028-00-4 204-825-9 127-18-4


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-008-00-5 200-262-8 56-23-5

40toluene

<10 mg/kg <10 mg/kg <0.001 % <LOD601-021-00-3 203-625-9 108-88-3


30 mg/kg 30 mg/kg 0.003 % TPH


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-027-00-9 201-167-4 79-01-6


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-023-00-7 200-831-0 75-01-4

44

xylene

<10 mg/kg <10 mg/kg <0.001 % <LOD601-022-00-9 202-422-2 [1]

203-396-5 [2]203-576-3 [3]215-535-7 [4]

95-47-6 [1]106-42-3 [2]108-38-3 [3]1330-20-7 [4]


470 mg/kg 1.245 585.016 mg/kg 0.0585 %030-013-00-7 215-222-5 1314-13-2

46


602-045-00-7 200-024-3 50-29-3

47


602-047-00-8 200-349-0 57-74-9

48


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-043-00-6 210-168-9,

200-401-2,206-270-8,206-271-3

58-89-9, 319-84-6,319-85-7, 608-73-1

49dieldrin (ISO)

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-049-00-9 200-484-5 60-57-1

50


602-051-00-X 200-775-7 72-20-8

51


602-046-00-2 200-962-3 76-44-8

52hexachlorobenzene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-065-00-6 204-273-9 118-74-1

53


606-019-00-6 205-601-3 143-50-0

54aldrin (ISO)

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-048-00-3 206-215-8 309-00-2


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-074-00-5 210-172-0 608-93-5


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-039-00-4 215-648-1 1336-36-3



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed



602-077-00-1 219-196-6 2385-85-5


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-044-00-1 232-283-3 8001-35-2

59hexabromobiphenyl

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 252-994-2 36355-01-8

602,3,7,8-TeCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 217-122-7 1746-01-6

611,2,3,7,8-PeCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 40321-76-4

621,2,3,4,7,8-HxCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 39227-28-6

631,2,3,6,7,8-HxCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57653-85-7

641,2,3,7,8,9-HxCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 19408-74-3

651,2,3,4,6,7,8-HpCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 35822-46-9

66OCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 3268-87-9

672,3,7,8-TeCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 51207-31-9

681,2,3,7,8-PeCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57117-41-6

692,3,4,7,8-PeCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57117-31-4

701,2,3,4,7,8-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 70648-26-9

711,2,3,6,7,8-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57117-44-9

721,2,3,7,8,9-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 72918-21-9

732,3,4,6,7,8-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 60851-34-5

741,2,3,4,6,7,8-HpCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 67562-39-4

751,2,3,4,7,8,9-HpCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 55673-89-7

76OCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 39001-02-0


<0.1gNaOH

<0.1gNaOH

<0.1 gNaOH <LOD



<0.1 mg/kg 3.894 <0.389 mg/kg <0.0000389 % <LOD024-008-00-9 237-366-8 13765-19-0


1 <0.1 mg/kg 2.63 <0.263 mg/kg <0.00001 % <LOD027-005-00-0 233-334-2 10124-43-3



<0.1 mg/kg 2.483 <0.248 mg/kg <0.0000248 % <LOD024-006-00-8 232-140-5 7789-00-6


<0.1 mg/kg 1.575 <0.157 mg/kg <0.0000157 % <LOD047-001-00-2 231-853-9 7761-88-8


<0.1 mg/kg 3.523 <0.352 mg/kg <0.0000352 % <LOD024-018-00-3 231-889-5 7775-11-3



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed



081-002-00-9


<0.1 mg/kg 2.602 <0.26 mg/kg <0.000026 % <LOD050-018-00-8 401-640-7 53408-94-9


14 mg/kg 1.785 24.993 mg/kg 0.0025 %023-001-00-8 215-239-8 1314-62-1


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-043-00-3 202-436-9 95-63-6


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-025-00-5 203-604-4 108-67-8


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-006-00-4 200-663-8 67-66-3

Total: 0.101 %












Sample details











Determinands


#Determinand

CLP

Not

e



valueM

CA

pplie

dConc. Not


1acenaphthene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 201-469-6 83-32-9

2acenaphthylene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 205-917-1 208-96-8

3anthracene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 204-371-1 120-12-7

4


1 <0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD

051-003-00-9


69 mg/kg 1.32 91.102 mg/kg 0.00911 %033-003-00-0 215-481-4 1327-53-3

6benzene

<10 mg/kg <10 mg/kg <0.001 % <LOD601-020-00-8 200-753-7 71-43-2

7benzo[a]anthracene

0.2 mg/kg 0.2 mg/kg 0.00002 %601-033-00-9 200-280-6 56-55-3


0.1 mg/kg 0.1 mg/kg 0.00001 %601-032-00-3 200-028-5 50-32-8


0.1 mg/kg 0.1 mg/kg 0.00001 %601-034-00-4 205-911-9 205-99-2


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 205-883-8 191-24-2


0.2 mg/kg 0.2 mg/kg 0.00002 %601-036-00-5 205-916-6 207-08-9



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed



<0.1 mg/kg 2.775 <0.278 mg/kg <0.0000278 % <LOD004-003-00-8 215-133-1 1304-56-9

13


<1 mg/kg 13.43 <13.43 mg/kg <0.00134 % <LOD 10294-33-4,10294-34-5,7637-07-2


1 2 mg/kg 1.285 2.57 mg/kg 0.0002 %048-010-00-4 215-147-8 1306-23-6


215-160-9 1308-38-9


024-001-00-0 215-607-8 1333-82-0

17chrysene

0.2 mg/kg 0.2 mg/kg 0.00002 %601-048-00-0 205-923-4 218-01-9


19


<1 mg/kg 1.884 <1.884 mg/kg <0.000188 % <LOD

006-007-00-5


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-041-00-2 200-181-8 53-70-3

21


203-458-1,200-863-5

107-06-2, 75-34-3

22


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 68334-30-5,

68476-34-6,94114-59-7,1159170-26-9

23ethylbenzene

<10 mg/kg <10 mg/kg <0.001 % <LOD601-023-00-4 202-849-4 100-41-4

24fluoranthene

0.2 mg/kg 0.2 mg/kg 0.00002 % 205-912-4 206-44-0

25fluorene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 201-695-5 86-73-7


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 205-893-2 193-39-5


082-001-00-6


<0.1 mg/kg 2.749 <0.275 mg/kg <0.0000275 % <LOD025-003-00-4 232-089-9 7785-87-7


<1 mg/kg 1.353 <1.353 mg/kg <0.000135 % <LOD080-010-00-X 231-299-8 7487-94-7


<0.1 mg/kg 1.5 <0.15 mg/kg <0.000015 % <LOD042-001-00-9 215-204-7 1313-27-5

31naphthalene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-052-00-2 202-049-5 91-20-3


19 mg/kg 1.579 30.01 mg/kg 0.003 %028-008-00-X 235-008-5 [1]234-348-1 [2]

12054-48-7 [1]11113-74-9 [2]

33pH

7.5 pH 7.5 pH 7.5 pH PH

34phenanthrene

0.1 mg/kg 0.1 mg/kg 0.00001 % 201-581-5 85-01-8



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed


35phenol

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD604-001-00-2 203-632-7 108-95-2

36pyrene

0.2 mg/kg 0.2 mg/kg 0.00002 % 204-927-3 129-00-0

37


034-002-00-8


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-028-00-4 204-825-9 127-18-4


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-008-00-5 200-262-8 56-23-5

40toluene

<10 mg/kg <10 mg/kg <0.001 % <LOD601-021-00-3 203-625-9 108-88-3


11 mg/kg 11 mg/kg 0.0011 % TPH


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-027-00-9 201-167-4 79-01-6


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-023-00-7 200-831-0 75-01-4

44

xylene

<10 mg/kg <10 mg/kg <0.001 % <LOD601-022-00-9 202-422-2 [1]

203-396-5 [2]203-576-3 [3]215-535-7 [4]

95-47-6 [1]106-42-3 [2]108-38-3 [3]1330-20-7 [4]


490 mg/kg 1.245 609.91 mg/kg 0.061 %030-013-00-7 215-222-5 1314-13-2

46


602-045-00-7 200-024-3 50-29-3

47


602-047-00-8 200-349-0 57-74-9

48


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-043-00-6 210-168-9,

200-401-2,206-270-8,206-271-3

58-89-9, 319-84-6,319-85-7, 608-73-1

49dieldrin (ISO)

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-049-00-9 200-484-5 60-57-1

50


602-051-00-X 200-775-7 72-20-8

51


602-046-00-2 200-962-3 76-44-8

52hexachlorobenzene

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-065-00-6 204-273-9 118-74-1

53


606-019-00-6 205-601-3 143-50-0

54aldrin (ISO)

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-048-00-3 206-215-8 309-00-2


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-074-00-5 210-172-0 608-93-5


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-039-00-4 215-648-1 1336-36-3



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed



602-077-00-1 219-196-6 2385-85-5


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-044-00-1 232-283-3 8001-35-2

59hexabromobiphenyl

<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD 252-994-2 36355-01-8

602,3,7,8-TeCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 217-122-7 1746-01-6

611,2,3,7,8-PeCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 40321-76-4

621,2,3,4,7,8-HxCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 39227-28-6

631,2,3,6,7,8-HxCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57653-85-7

641,2,3,7,8,9-HxCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 19408-74-3

651,2,3,4,6,7,8-HpCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 35822-46-9

66OCDD

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 3268-87-9

672,3,7,8-TeCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 51207-31-9

681,2,3,7,8-PeCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57117-41-6

692,3,4,7,8-PeCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57117-31-4

701,2,3,4,7,8-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 70648-26-9

711,2,3,6,7,8-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 57117-44-9

721,2,3,7,8,9-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 72918-21-9

732,3,4,6,7,8-HxCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 60851-34-5

741,2,3,4,6,7,8-HpCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 67562-39-4

751,2,3,4,7,8,9-HpCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 55673-89-7

76OCDF

<0.1 ng/kg <1.0e-07 mg/kg <1.0e-11 % <LOD 39001-02-0


<0.1gNaOH

<0.1gNaOH

<0.1 gNaOH <LOD



<0.1 mg/kg 3.894 <0.389 mg/kg <0.0000389 % <LOD024-008-00-9 237-366-8 13765-19-0


1 <0.1 mg/kg 2.63 <0.263 mg/kg <0.00001 % <LOD027-005-00-0 233-334-2 10124-43-3



<0.1 mg/kg 2.483 <0.248 mg/kg <0.0000248 % <LOD024-006-00-8 232-140-5 7789-00-6


<0.1 mg/kg 1.575 <0.157 mg/kg <0.0000157 % <LOD047-001-00-2 231-853-9 7761-88-8


<0.1 mg/kg 3.523 <0.352 mg/kg <0.0000352 % <LOD024-018-00-3 231-889-5 7775-11-3



#Determinand

CLP

Not

e



value

MC

App

lied

Conc. NotUsed



081-002-00-9


<0.1 mg/kg 2.602 <0.26 mg/kg <0.000026 % <LOD050-018-00-8 401-640-7 53408-94-9


15 mg/kg 1.785 26.778 mg/kg 0.00268 %023-001-00-8 215-239-8 1314-62-1


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-043-00-3 202-436-9 95-63-6


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD601-025-00-5 203-604-4 108-67-8


<0.1 mg/kg <0.1 mg/kg <0.00001 % <LOD602-006-00-4 200-663-8 67-66-3

Total: 0.11 %









Appendix A: Classifier defined and non CLP determinands

acenaphthene (EC Number: 201-469-6, CAS Number: 83-32-9)

Description/Comments: Data from C&L Inventory DatabaseData source: http://echa.europa.eu/web/guest/information-on-chemicals/cl-inventory-databaseData source date: 17/07/2015Risk Phrases: R36 , R37 , R38 , N R50/53 , N R51/53Hazard Statements: Eye Irrit. 2 H319 , STOT SE 3 H335 , Skin Irrit. 2 H315 , Aquatic Acute 1 H400 , Aquatic Chronic 1 H410 , AquaticChronic 2 H411

acenaphthylene (EC Number: 205-917-1, CAS Number: 208-96-8)

Description/Comments: Data from C&L Inventory DatabaseData source: http://echa.europa.eu/web/guest/information-on-chemicals/cl-inventory-databaseData source date: 17/07/2015Risk Phrases: R22 , R26 , R27 , R36 , R37 , R38Hazard Statements: Acute Tox. 4 H302 , Acute Tox. 1 H330 , Acute Tox. 1 H310 , Eye Irrit. 2 H319 , STOT SE 3 H335 , Skin Irrit. 2 H315

anthracene (EC Number: 204-371-1, CAS Number: 120-12-7)

Description/Comments: Data from C&L Inventory DatabaseData source: http://echa.europa.eu/web/guest/information-on-chemicals/cl-inventory-databaseData source date: 17/07/2015Risk Phrases: R36 , R37 , R38 , R43 , N R50/53Hazard Statements: Eye Irrit. 2 H319 , STOT SE 3 H335 , Skin Irrit. 2 H315 , Skin Sens. 1 H317 , Aquatic Acute 1 H400 , AquaticChronic 1 H410

benzo[ghi]perylene (EC Number: 205-883-8, CAS Number: 191-24-2)

Description/Comments: Data from C&L Inventory Database; SDS Sigma Aldrich 28/02/2015Data source: http://echa.europa.eu/web/guest/information-on-chemicals/cl-inventory-databaseData source date: 23/07/2015Risk Phrases: N R50/53Hazard Statements: Aquatic Acute 1 H400 , Aquatic Chronic 1 H410

boron tribromide/trichloride/trifluoride (combined) (CAS Number: 10294-33-4, 10294-34-5, 7637-07-2)

Conversion factor: 13.43Description/Comments: Combines the hazard statements and the average of the conversion factors for boron tribromide, borontrichloride and boron trifluorideData source: N/AData source date: 06/08/2015Risk Phrases: R14 , T+ R26/28 , C R34 , C R35Hazard Statements: EUH014 , Acute Tox. 2 H330 , Acute Tox. 2 H300 , Skin Corr. 1A H314 , Skin Corr. 1B H314

chromium(III) oxide (EC Number: 215-160-9, CAS Number: 1308-38-9)

Conversion factor: 1.462Description/Comments: Data from C&L Inventory DatabaseData source: http://echa.europa.eu/web/guest/information-on-chemicals/cl-inventory-databaseData source date: 17/07/2015Risk Phrases: R20 , R22 , R36 , R37 , R38 , R42 , R43 , R50/53 , R60 , R61Hazard Statements: Acute Tox. 4 H332 , Acute Tox. 4 H302 , Eye Irrit. 2 H319 , STOT SE 3 H335 , Skin Irrit. 2 H315 , Resp. Sens. 1H334 , Skin Sens. 1 H317 , Repr. 1B H360FD , Aquatic Acute 1 H400 , Aquatic Chronic 1 H410

dicopper oxide; copper (I) oxide (EC Number: 215-270-7, CAS Number: 1317-39-1)

CLP index number: 029-002-00-XData source: Regulation (EU) 2016/1179 of 19 July 2016 (ATP9)Additional Risk Phrases: N R50/53 , N R50/53 >= 0.25 %Additional Hazard Statement(s): None.Reason for additional Hazards Statement(s)/Risk Phrase(s):10/10/2016 - N R50/53 risk phrase sourced from: WM3 v1 still uses ecotoxic risk phrases10/10/2016 - N R50/53 >= 0.25 % risk phrase sourced from: WM3 v1 still uses ecotoxic risk phrases



salts of hydrogen cyanide with the exception of complex cyanides such as ferrocyanides, ferricyanides and mercuricoxycyanide and those specified elsewhere in this Annex

CLP index number: 006-007-00-5Data source: Commission Regulation (EC) No 790/2009 - 1st Adaptation to Technical Progress for Regulation (EC) No 1272/2008.(ATP1)Additional Risk Phrases: None.Additional Hazard Statement(s): EUH032 >= 0.2 %Reason for additional Hazards Statement(s)/Risk Phrase(s):14/12/2015 - EUH032 >= 0.2 % hazard statement sourced from: WM3, Table C12.2

1,1-dichloroethane and 1,2-dichloroethane (combined) (EC Number: 203-458-1, 200-863-5, CAS Number: 107-06-2, 75-34-3)

Description/Comments: Combines the hazard statements and risk phrases for 1,1-dichloroethane and 1,2-dichloroethaneData source: N/aData source date: 14/10/2016Risk Phrases: F R11 , Xn R22 , Xi R36/37/38 , Carc Cat 2 R45 , R52/53Hazard Statements: Flam. Liq. 2 H225 , Acute Tox. 4 H302 , Skin Irrit. 2 H315 , Eye Irrit. 2 H319 , STOT SE 3 H335 , Carc. 1B H350 ,Aquatic Chronic 3 H412

diesel petroleum group (CAS Number: 68334-30-5, 68476-34-6, 94114-59-7, 1159170-26-9)

Description/Comments: Hazard statements taken from WM3 1st Edition 2015; Risk phrases: WM2 3rd Edition 2013Data source: WM3 1st Edition 2015Data source date: 25/05/2015Risk Phrases: R40 , R51/53 , R65 , R66Hazard Statements: Flam. Liq. 3 H226 , Skin Irrit. 2 H315 , Acute Tox. 4 H332 , Carc. 2 H351 , Asp. Tox. 1 H304 , STOT RE 2 H373 ,Aquatic Chronic 2 H411

ethylbenzene (EC Number: 202-849-4, CAS Number: 100-41-4)

CLP index number: 601-023-00-4Data source: Commission Regulation (EU) No 605/2014 – 6th Adaptation to Technical Progress for Regulation (EC) No 1272/2008.(ATP6)Additional Risk Phrases: None.Additional Hazard Statement(s): Carc. 2 H351Reason for additional Hazards Statement(s)/Risk Phrase(s):03/06/2015 - Carc. 2 H351 hazard statement sourced from: IARC Group 2B (77) 2000

fluoranthene (EC Number: 205-912-4, CAS Number: 206-44-0)

Description/Comments: Data from C&L Inventory DatabaseData source: http://echa.europa.eu/web/guest/information-on-chemicals/cl-inventory-databaseData source date: 21/08/2015Risk Phrases: Xn R22 , N R50/53Hazard Statements: Acute Tox. 4 H302 , Aquatic Acute 1 H400 , Aquatic Chronic 1 H410

fluorene (EC Number: 201-695-5, CAS Number: 86-73-7)

Description/Comments: Data from C&L Inventory DatabaseData source: http://echa.europa.eu/web/guest/information-on-chemicals/cl-inventory-databaseData source date: 06/08/2015Risk Phrases: N R50/53Hazard Statements: Aquatic Acute 1 H400 , Aquatic Chronic 1 H410

indeno[123-cd]pyrene (EC Number: 205-893-2, CAS Number: 193-39-5)

Description/Comments: Data from C&L Inventory DatabaseData source: http://echa.europa.eu/web/guest/information-on-chemicals/cl-inventory-databaseData source date: 06/08/2015Risk Phrases: R40Hazard Statements: Carc. 2 H351

lead compounds with the exception of those specified elsewhere in this Annex

CLP index number: 082-001-00-6Data source: Regulation 1272/2008/EC - Classification, labelling and packaging of substances and mixtures. (CLP)Additional Risk Phrases: None.Additional Hazard Statement(s): Carc. 2 H351Reason for additional Hazards Statement(s)/Risk Phrase(s):03/06/2015 - Carc. 2 H351 hazard statement sourced from: IARC Group 2A (Sup 7, 87) 2006; Lead REACH Consortiumwww.reach-lead.eu/substanceinformation.html. Review date 29/09/2015



pH (CAS Number: PH)

Description/Comments: Appendix C4Data source: WM3 1st Edition 2015Data source date: 25/05/2015Risk Phrases: None.Hazard Statements: None.

phenanthrene (EC Number: 201-581-5, CAS Number: 85-01-8)

Description/Comments: Data from C&L Inventory DatabaseData source: http://echa.europa.eu/web/guest/information-on-chemicals/cl-inventory-databaseData source date: 06/08/2015Risk Phrases: R22 , R36 , R37 , R38 , R40 , R43 , N R50/53Hazard Statements: Acute Tox. 4 H302 , Eye Irrit. 2 H319 , STOT SE 3 H335 , Carc. 2 H351 , Skin Sens. 1 H317 , Aquatic Acute 1 H400, Aquatic Chronic 1 H410 , Skin Irrit. 2 H315

pyrene (EC Number: 204-927-3, CAS Number: 129-00-0)

Description/Comments: Data from C&L Inventory Database; SDS Sigma Aldrich 2014Data source: http://echa.europa.eu/web/guest/information-on-chemicals/cl-inventory-databaseData source date: 21/08/2015Risk Phrases: Xi R36/37/38 , N R50/53Hazard Statements: Skin Irrit. 2 H315 , Eye Irrit. 2 H319 , STOT SE 3 H335 , Aquatic Acute 1 H400 , Aquatic Chronic 1 H410

TPH (C6 to C40) petroleum group (CAS Number: TPH)

Description/Comments: Hazard statements taken from WM3 1st Edition 2015; Risk phrases: WM2 3rd Edition 2013Data source: WM3 1st Edition 2015Data source date: 25/05/2015Risk Phrases: R10 , R45 , R46 , R51/53 , R63 , R65Hazard Statements: Flam. Liq. 3 H226 , Asp. Tox. 1 H304 , STOT RE 2 H373 , Muta. 1B H340 , Carc. 1B H350 , Repr. 2 H361d ,Aquatic Chronic 2 H411

polychlorobiphenyls; PCB (EC Number: 215-648-1, CAS Number: 1336-36-3)

CLP index number: 602-039-00-4Data source: Regulation 1272/2008/EC - Classification, labelling and packaging of substances and mixtures. (CLP)Additional Risk Phrases: None.Additional Hazard Statement(s): Carc. 1A H350Reason for additional Hazards Statement(s)/Risk Phrase(s):29/09/2015 - Carc. 1A H350 hazard statement sourced from: IARC Group 1 (23, Sup 7, 100C) 2012

hexabromobiphenyl (EC Number: 252-994-2, CAS Number: 36355-01-8)

Description/Comments:Data source: POP specific threshold from ATP1 (Regulation (EU) 756/2010) to POPs Regulation (Regulation (EC) 850/2004).Data source date: 01/07/2013Risk Phrases: None.Hazard Statements: POP >= 0.005 %

2,3,7,8-TeCDD (EC Number: 217-122-7, CAS Number: 1746-01-6)

Description/Comments: 2,3,7,8-tetrachlorodibenzo-p-dioxin (TCDD)Data source: ATP1 (Regulation (EU) 756/2010) to POPs Regulation (Regulation (EC) 850/2004)Data source date: 24/08/2010Risk Phrases: None.Hazard Statements: PCDD/PCDF (TEF=1)

1,2,3,7,8-PeCDD (CAS Number: 40321-76-4)

Description/Comments: 1,2,3,7,8-pentachlorodibenzo-p-dioxinData source: ATP1 (Regulation (EU) 756/2010) to POPs Regulation (Regulation (EC) 850/2004)Data source date: 24/08/2010Risk Phrases: None.Hazard Statements: PCDD/PCDF (TEF=1)

1,2,3,4,7,8-HxCDD (CAS Number: 39227-28-6)

Description/Comments: 1,2,3,4,7,8-hexachlorodibenzo-p-dioxinData source: ATP1 (Regulation (EU) 756/2010) to POPs Regulation (Regulation (EC) 850/2004)Data source date: 24/08/2010Risk Phrases: None.Hazard Statements: PCDD/PCDF (TEF=0.1)



1,2,3,6,7,8-HxCDD (CAS Number: 57653-85-7)


1,2,3,7,8,9-HxCDD (CAS Number: 19408-74-3)


1,2,3,4,6,7,8-HpCDD (CAS Number: 35822-46-9)

Description/Comments: 1,2,3,4,6,7,8-heptachlorodibenzo-p-dioxinData source: ATP1 (Regulation (EU) 756/2010) to POPs Regulation (Regulation (EC) 850/2004)Data source date: 24/08/2010Risk Phrases: None.Hazard Statements: PCDD/PCDF (TEF=0.01)

OCDD (CAS Number: 3268-87-9)

Description/Comments: octachlorodibenzo-p-dioxinData source: ATP1 (Regulation (EU) 756/2010) to POPs Regulation (Regulation (EC) 850/2004)Data source date: 24/08/2010Risk Phrases: None.Hazard Statements: PCDD/PCDF (TEF=0.0003)

2,3,7,8-TeCDF (CAS Number: 51207-31-9)

Description/Comments: 2,3,7,8-tetrachlorodibenzofuranData source: ATP1 (Regulation (EU) 756/2010) to POPs Regulation (Regulation (EC) 850/2004)Data source date: 24/08/2010Risk Phrases: None.Hazard Statements: PCDD/PCDF (TEF=0.1)

1,2,3,7,8-PeCDF (CAS Number: 57117-41-6)

Description/Comments: 1,2,3,7,8-pentachlorodibenzofuranData source: ATP1 (Regulation (EU) 756/2010) to POPs Regulation (Regulation (EC) 850/2004)Data source date: 24/08/2010Risk Phrases: None.Hazard Statements: PCDD/PCDF (TEF=0.03)

2,3,4,7,8-PeCDF (CAS Number: 57117-31-4)

Description/Comments: 2,3,4,7,8-pentachlorodibenzofuranData source: ATP1 (Regulation (EU) 756/2010) to POPs Regulation (Regulation (EC) 850/2004)Data source date: 24/08/2010Risk Phrases: None.Hazard Statements: PCDD/PCDF (TEF=0.3)

1,2,3,4,7,8-HxCDF (CAS Number: 70648-26-9)

Description/Comments: 1,2,3,4,7,8-hexachlorodibenzofuranData source: ATP1 (Regulation (EU) 756/2010) to POPs Regulation (Regulation (EC) 850/2004)Data source date: 24/08/2010Risk Phrases: None.Hazard Statements: PCDD/PCDF (TEF=0.1)

1,2,3,6,7,8-HxCDF (CAS Number: 57117-44-9)




1,2,3,7,8,9-HxCDF (CAS Number: 72918-21-9)


2,3,4,6,7,8-HxCDF (CAS Number: 60851-34-5)


1,2,3,4,6,7,8-HpCDF (CAS Number: 67562-39-4)

Description/Comments: 1,2,3,4,6,7,8-heptachlorodibenzofuranData source: ATP1 (Regulation (EU) 756/2010) to POPs Regulation (Regulation (EC) 850/2004)Data source date: 24/08/2010Risk Phrases: None.Hazard Statements: PCDD/PCDF (TEF=0.01)

1,2,3,4,7,8,9-HpCDF (CAS Number: 55673-89-7)

Description/Comments: 1,2,3,4,7,8,9-heptachlorodibenzofuranData source: ATP1 (Regulation (EU) 756/2010) to POPs Regulation (Regulation (EC) 850/2004)Data source date: 24/08/2010Risk Phrases: None.Hazard Statements: PCDD/PCDF (TEF=0.01)

OCDF (CAS Number: 39001-02-0)

Description/Comments: octachlorodibenzo[b,d]furanData source: ATP1 (Regulation (EU) 756/2010) to POPs Regulation (Regulation (EC) 850/2004)Data source date: 24/08/2010Risk Phrases: None.Hazard Statements: PCDD/PCDF (TEF=0.0003)

pH: acid/alkali reserve

Description/Comments: Appendix C4; unit: grams of sodium hydroxide (equivalent) per 100g of substance required to adjust the pH tothe appropriate valueData source: WM3 1st Edition 2015Data source date: 25/05/2015Risk Phrases: None.Hazard Statements: None.

barium chromate (EC Number: 233-660-5, CAS Number: 10294-40-3)

Conversion factor: 1.845Description/Comments: Data from C&L Inventory DatabaseData source: http://echa.europa.eu/web/guest/information-on-chemicals/cl-inventory-databaseData source date: 28/09/2015Risk Phrases: O R8 , Xn R20/22 , T R25 , Xi R36/37/38 , R42 , R43 , Carc Cat 2 R45 , N R50/53 , Muta Cat 3 R68Hazard Statements: Acute Tox. 4 H302 , Acute Tox. 4 H332 , Acute Tox. 3 H301 , Skin Irrit. 2 H315 , Eye Irrit. 2 H319 , Resp. Sens. 1H334 , Muta. 2 H341 , Ox. Sol. 2 H272 , Skin Sens. 1 H317 , Carc. 1B H350 , STOT SE 3 H335 , Aquatic Acute 1 H400 , AquaticChronic 1 H410

iron (III) oxide (worst case) (EC Number: 215-168-2, CAS Number: 1309-37-1)

Conversion factor: 1.43Description/Comments:Data source: C&L Inventory, Registered Substances databaseData source date: 21/05/2015Risk Phrases: None.Hazard Statements: Skin Irrit. 2 H315 , Eye Dam. 1 H318 , Eye Irrit. 2 H319 , STOT SE 3 H335 , STOT RE 1 H372



thallium compounds, with the exception of those specified elsewhere in this Annex

CLP index number: 081-002-00-9Data source: Regulation 1272/2008/EC - Classification, labelling and packaging of substances and mixtures. (CLP)Additional Risk Phrases: None.Additional Hazard Statement(s): Carc. 1A H350Reason for additional Hazards Statement(s)/Risk Phrase(s):03/11/2015 - Carc. 1A H350 hazard statement sourced from: IARC Group 1 (23, Sup 7, 100C) 2012

Appendix B: Rationale for selection of metal species

antimony {antimony compounds, with the exception of the tetroxide (Sb2O4), pentoxide (Sb2O5), trisulphide (Sb2S3),pentasulphide (Sb2S5) and those specified elsewhere in this Annex}

Worst case species based on hazard statements

arsenic {arsenic trioxide}


beryllium {beryllium oxide}


boron {boron tribromide/trichloride/trifluoride (combined)}


cadmium {cadmium sulfide}


chromium in chromium(III) compounds {chromium(III) oxide}


chromium in chromium(VI) compounds {chromium(VI) oxide}


copper {dicopper oxide; copper (I) oxide}

Most likely common species

cyanides {salts of hydrogen cyanide with the exception of complex cyanides such as ferrocyanides, ferricyanides andmercuric oxycyanide and those specified elsewhere in this Annex}

Worst case species

dichloroethane {1,1-dichloroethane and 1,2-dichloroethane (combined)}


lead {lead compounds with the exception of those specified elsewhere in this Annex}

No Cr VI

manganese {manganese sulphate}


mercury {mercury dichloride}


molybdenum {molybdenum(VI) oxide}


nickel {nickel dihydroxide}


selenium {selenium compounds with the exception of cadmium sulphoselenide and those specified elsewhere in this Annex}


zinc {zinc oxide}

No Cr VI

barium {barium chromate}

Worst case species

calcium {calcium chromate}

Worst case species



cobalt {cobalt sulfate}

Worst case species

iron {iron (III) oxide (worst case)}

Worst case species

potassium {potassium chromate}

Worst case species

silver {silver nitrate}

Worst case species

sodium {sodium chromate}

Worst case species

thallium {thallium compounds, with the exception of those specified elsewhere in this Annex}

Worst case species

tin {tin(II) methanesulphonate}

Worst case species

vanadium {divanadium pentaoxide; vanadium pentoxide}

Worst case species

Appendix C: Version

HazWasteOnline Classification Engine: WM3 1st Edition, May 2015HazWasteOnline Classification Engine Version: 2017.248.3389.6849 (05 Sep 2017)HazWasteOnline Database: 2017.248.3389.6849 (05 Sep 2017)

This classification utilises the following guidance and legislation:WM3 - Waste Classification - May 2015CLP Regulation - Regulation 1272/2008/EC of 16 December 20081st ATP - Regulation 790/2009/EC of 10 August 20092nd ATP - Regulation 286/2011/EC of 10 March 20113rd ATP - Regulation 618/2012/EU of 10 July 20124th ATP - Regulation 487/2013/EU of 8 May 2013Correction to 1st ATP - Regulation 758/2013/EU of 7 August 20135th ATP - Regulation 944/2013/EU of 2 October 20136th ATP - Regulation 605/2014/EU of 5 June 2014WFD Annex III replacement - Regulation 1357/2014/EU of 18 December 2014Revised List of Wastes 2014 - Decision 2014/955/EU of 18 December 20147th ATP - Regulation 2015/1221/EU of 24 July 20158th ATP - Regulation (EU) 2016/918 of 19 May 20169th ATP - Regulation (EU) 2016/1179 of 19 July 201610th ATP - Regulation (EU) 2017/776 of 4 May 2017POPs Regulation 2004 - Regulation 850/2004/EC of 29 April 20041st ATP to POPs Regulation - Regulation 756/2010/EU of 24 August 20102nd ATP to POPs Regulation - Regulation 757/2010/EU of 24 August 2010


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G. Geotechnical risk register score tables

Health and

SafetyTime Cost Reputation Environment

1 very low negligible negligible negligible effect on programme negligible negligible negligible

2 low minor minor injury 5% effect on programme 1% budget

minor effect on local company

image/ business relationship

mildly affected

minor environmental incident

3 medium serious major injury 12% effect on programme 10%budgetlocal media exposure/

business relationship affected

environmental incident

requiring management input

4 high

threat to furture

work and client

relations

fatality 25% effect on programme 20% budget

nationwide media exposure /

business relationship greatly

affected

environmental incident leading

to prosecution or protestor

action

5 very high

threat to

business

survival and

credibility

multiple fatalities 50% effect on programme 50% budget

permanent nationwide affect

on company image/ significant

impact on business

relationship

major environmental incident

with irreversible effects and

threat to public health or

protected natural resource

NEGATIVE CONSEQUENCE SCORE TABLE

Impact

Probability

1 very lownegligible /

improbable<1%

2 lowunlikely /

remote>1%

3 medium likely / possible >10%

4 high probable >50%

5 very highvery likely /

almost certain>90%

LIKELIHOOD SCORE TABLELikelihood

Very Low Low Medium High Very High

Score 1 2 3 4 5

Very Low 1 n n n n t

Low 2 n n t t s

Medium 3 n t t s s

High 4 n t s s i

Very High 5 t s s i i

Risk Key

intolerable RED i 20 to 25significant AMBER s 10 to 16tolerable YELLOW t 5 to 9negligible / trivial GREEN n 1 to 4

LikelihoodN

egat

ive

Con

sequ

ence


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