excelchem environmental labs - california · 2017. 10. 26. · excelchem environmental lab. the...

RWQC Central Valley

RE: MUN/CV- SALTS Title 22 Monitoring

Rancho Cordova, CA 95670

11020 Sun Center Dr. #200

Cindy Au Yeung

Enclosed are the results of analyses for samples received by the laboratory on 06/25/14 15:30. All Quality Control results are

within acceptable limits except where noted as a case narrative. If you have any questions concerning this report, please feel free

to contact the laboratory.

Sincerely,

05 September 2014

Work order number:1406186

John Somers, Lab Director

ELAP Certificate No. : 2119

EXCELCHEM

Environmental Labs1135 W Sunset Boulevard

Suite A

Rocklin, CA 95765

Phone# 916-543-4445

Fax# 916-543-4449

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MUN/CV- SALTS Title 22 MonitoringRWQC Central Valley

11020 Sun Center Dr. #200 13-051-150

Cindy Au Yeung 09/05/14 16:01Rancho Cordova, CA 95670

Excelchem Environmental Labs

Date Reported:

Sample ID Laboratory ID Matrix Date Sampled

ANALYTICAL REPORT FOR SAMPLES

Date Received

CAY140625-37 1406186-01 06/25/14 10:05 06/25/14 15:30Water

CAY140625-38 1406186-02 06/25/14 12:09 06/25/14 15:30Water

CAY140625-39 1406186-03 06/25/14 09:01 06/25/14 15:30Water

CAY140625-40 1406186-04 06/25/14 13:07 06/25/14 15:30Water

CAY140625-3 1406186-05 06/25/14 12:09 06/25/14 15:30Water

CAY140625-4 1406186-06 06/25/14 07:00 06/25/14 15:30Water

Excelchem Environmental Lab. The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

Laboratory RepresentativePage 1 of 107

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11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-01 (Water)

CAY140625-37

Result Limit Notes MethodAnalyzedBatch PreparedUnitsAnalyteDate DateReporting

MDL DF

Volatile Organic Compounds by GC/MS

ND 06/28/14 06/28/14 ug/l AXG0011TBA 1.0 0.1 EPA 8260B1

ND " "" "Methyl tert-Butyl Ether 0.5 0.05 "1

ND " "" "Di-isopropyl ether 0.5 0.1 "1

ND " "" "Ethyl tert-Butyl Ether 0.5 0.04 "1

ND " "" "Tert-Amyl Methyl Ether 0.5 0.03 "1

ND " "" "Dichlorodifluoromethane 0.5 0.07 "1

ND " "" "Chloromethane 0.5 0.06 "1

ND " "" "Vinyl chloride 0.5 0.06 "1

ND " "" "Bromomethane 0.5 0.05 "1

ND " "" "Chloroethane 0.5 0.08 "1

ND " "" "Trichlorofluoromethane 0.5 0.05 "1

ND " "" "Trichlorotrifluoroethane 1.0 0.05 "1

ND " "" "Acetone 5.0 0.1 "1

ND " "" "1,1-Dichloroethene 0.5 0.05 "1

ND " "" "Iodomethane 0.5 0.03 "1

ND " "" "Methylene chloride 5.0 0.08 "1

ND " "" "Carbon disulfide 0.5 0.06 "1

ND " "" "trans-1,2-Dichloroethene 0.5 0.04 "1

ND " "" "1,1-Dichloroethane 0.5 0.04 "1

ND " "" "2-Butanone 5.0 0.1 "1

ND " "" "2,2-Dichloropropane 0.5 0.06 "1

ND " "" "cis-1,2-Dichloroethene 0.5 0.03 "1

ND " "" "Bromochloromethane 0.5 0.07 "1

ND " "" "Chloroform 0.5 0.05 "1

ND " "" "1,1,1-Trichloroethane 0.5 0.05 "1

ND " "" "Carbon tetrachloride 0.5 0.02 "1

ND " "" "1,1-Dichloropropene 0.5 0.03 "1

ND " "" "Benzene 0.5 0.03 "1

"0.1 " " ""1,2-Dichloroethane 0.5 Ja0.04 1

ND " "" "Dibromomethane 0.5 0.07 "1

ND " "" "Trichloroethene 0.5 0.06 "1

ND " "" "Bromodichloromethane 0.5 0.05 "1


ND " "" "cis-1,3-Dichloropropene 0.5 0.04 "1




Project:

Project Number:

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11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-01 (Water)

CAY140625-37


MDL DF


ND 06/28/14 06/28/14 ug/l AXG00114-Methyl-2-pentanone 5.0 0.05 "1

ND " "" "Toluene 0.5 0.04 "1

ND " "" "trans-1,3-Dichloropropene 0.5 0.04 "1


ND " "" "Tetrachloroethene 0.5 0.08 "1


ND " "" "2-Hexanone 5.0 0.1 "1

ND " "" "Dibromochloromethane 0.5 0.07 "1

ND " "" "1,2-Dibromoethane (EDB) 0.5 0.1 "1

ND " "" "Chlorobenzene 0.5 0.03 "1

ND " "" "1,1,1,2-Tetrachloroethane 0.5 0.08 "1

ND " "" "Ethylbenzene 0.5 0.03 "1

ND " "" "m,p-Xylene 1.0 0.09 "1

ND " "" "o-Xylene 0.5 0.04 "1

ND " "" "Xylenes, total 1.0 0.1 "1

ND " "" "Bromoform 0.5 0.03 "1

ND " "" "Isopropylbenzene 0.5 0.04 "1

ND " "" "Bromobenzene 0.5 0.05 "1


ND " "" "1,2,3-Trichloropropane 0.5 0.06 "1

ND " "" "n-Propylbenzene 0.5 0.04 "1

ND " "" "2-Chlorotoluene 0.5 0.03 "1


ND " "" "tert-Butylbenzene 0.5 0.02 "1

ND " "" "1,2,4-Trimethylbenzene 0.5 0.04 "1

"0.03 " " ""sec-Butylbenzene 0.5 Ja0.03 1

ND " "" "1,3-Dichlorobenzene 0.5 0.03 "1

ND " "" "4-Isopropyltoluene 0.5 0.04 "1



"0.05 " " ""n-Butylbenzene 0.5 Ja0.04 1

ND " "" "1,2-Dibromo-3-chloropropane 0.5 0.07 "1

"0.07 " " ""1,2,4-Trichlorobenzene 0.5 Ja0.02 1

ND " "" "Hexachlorobutadiene 0.5 0.07 "1




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-01 (Water)

CAY140625-37


MDL DF


"0.04 AXG0011 06/28/14 06/28/14 ug/lNaphthalene 0.5 Ja0.04 1

ND " "" "1,2,3-Trichlorobenzene 0.5 0.05 "1

Surrogate: Dibromofluoromethane "70-130105 % % Recovery Limits

Surrogate: Toluene-d8 "70-130104 % % Recovery Limits

Surrogate: 4-Bromofluorobenzene "70-13098.5 % % Recovery Limits

ND 07/28/14 08/04/14 " AXH0123TBA 1.0 0.1 EPA 5241




"0.2 " " ""Tert-Amyl Methyl Ether 0.5 Ja0.03 1







ND " "" "Total Trihalomethanes 0.5 0.5 "1




"0.3 " " ""Acetone 5.0 Ja0.1 1






ND " "" "2-Butanone 5.0 0.1 "1





ND " "" "Chloroform 0.5 Z-030.05 "1

ND " "" "Benzene 0.5 0.03 "1





Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-01 (Water)

CAY140625-37


MDL DF

Volatile Organic Compounds by GC/MS Z-01c

ND 07/28/14 08/04/14 ug/l AXH0123Trichloroethene 0.5 0.06 "1





ND " "" "Toluene 0.5 0.04 "1


"0.07 " " ""4-Methyl-2-pentanone 5.0 Ja0.05 1





ND " "" "2-Hexanone 5.0 0.1 "1





ND " "" "m,p-Xylene 0.5 0.09 "1

ND " "" "o-Xylene 0.5 0.04 "1


ND " "" "Styrene 0.5 0.09 "1

"0.04 " " ""Bromoform 0.5 Ja0.03 1
















Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-01 (Water)

CAY140625-37


MDL DF


ND 07/28/14 08/04/14 ug/l AXH01231,2,4-Trimethylbenzene 0.5 0.04 "1

ND " "" "sec-Butylbenzene 0.5 0.03 "1



ND " "" "n-Butylbenzene 0.5 0.04 "1

"0.09 " " ""1,2-Dibromo-3-chloropropane 0.5 Ja0.07 1


ND " "" "Naphthalene 0.5 0.04 "1




Surrogate: Toluene-d8 "70-13097.2 % % Recovery Limits


Pesticides by GC/ECD

ND 07/01/14 07/07/14 ug/l AXG0027alpha-BHC 0.100 0.011 EPA 8081A1

ND " "" "beta-BHC 0.100 0.011 "1

ND " "" "gamma-BHC (Lindane) 0.100 0.013 "1

ND " "" "delta-BHC 0.100 0.021 "1

ND " "" "Heptachlor 0.100 0.016 "1

ND " "" "Aldrin 0.100 0.011 "1

ND " "" "Heptachlor epoxide 0.100 0.020 "1

ND " "" "gamma-Chlordane 0.100 0.005 "1

ND " "" "Endosulfan I 0.100 0.007 "1

ND " "" "alpha-Chlordane 0.100 0.006 "1

ND " "" "4,4'-DDE 0.100 0.005 "1

ND " "" "Dieldrin 0.100 0.006 "1

ND " "" "Endrin 0.100 0.007 "1

ND " "" "Endosulfan II 0.100 0.021 "1

ND " "" "4,4'-DDD 0.100 0.006 "1

ND " "" "Endrin aldehyde 0.100 0.006 "1

"0.024 " " ""Endosulfan sulfate 0.100 Ja0.005 1

ND " "" "4,4'-DDT 0.100 0.004 "1

ND " "" "Endrin Ketone 0.100 0.005 "1

ND " "" "Methoxychlor 0.100 0.013 "1




Project:

Project Number:

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11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-01 (Water)

CAY140625-37


MDL DF


Surrogate: Decachlorobiphenyl "50-15085.9 % % Recovery Limits

Surrogate: Tetrachloro-meta-xylene "50-15058.9 % % Recovery Limits

PCBs by GC/ECD

ND " 07/07/14 ug/l AXG0027Aroclor 1016 1.00 0.0600 EPA 80821

ND " "" "PCBs 1.00 0.0800 "1

ND " "" "Aroclor 1221 1.00 0.130 "1

ND " "" "Aroclor 1232 1.00 0.100 "1

ND " "" "Aroclor 1242 1.00 0.0600 "1

ND " "" "Aroclor 1248 1.00 0.0600 "1

ND " "" "Aroclor 1254 1.00 0.0900 "1

ND " "" "Aroclor 1260 1.00 0.0800 "1



SemiVolatile Organic Compounds by GC/MS

ND 07/02/14 07/03/14 ug/l AXG0033N-Nitrosodimethylamine 2.0 0.4 EPA 8270C1

ND " "" "Aniline 2.0 0.3 "1

ND " "" "Bis(2-chloroethyl)ether 2.0 0.6 "1

ND " "" "Phenol 2.0 0.3 "1

ND " "" "2-Chlorophenol 2.0 0.8 "1


ND " "" "Benzyl alcohol 2.0 0.4 "1

ND " "" "Bis(2-chloroisopropyl)ether 2.0 0.4 "1

ND " "" "2-Methylphenol 2.0 0.4 "1

ND " "" "Hexachloroethane 2.0 0.5 "1

ND " "" "N-Nitrosodi-n-propylamine 2.0 0.3 "1

ND " "" "Nitrobenzene 2.0 0.7 "1

ND " "" "Isophorone 2.0 0.3 "1

ND " "" "2-Nitrophenol 5.0 1.2 "1

ND " "" "2,4-Dimethylphenol 2.0 0.8 "1

ND " "" "Bis(2-chloroethoxy)methane 2.0 0.4 "1

ND " "" "Benzoic acid 30.0 0.5 "1

ND " "" "2,4-Dichlorophenol 2.0 0.8 "1





Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-01 (Water)

CAY140625-37


MDL DF


ND 07/02/14 07/03/14 ug/l AXG0033Naphthalene 2.0 0.5 "1

ND " "" "4-Chloroaniline 2.0 0.5 "1


ND " "" "4-Chloro-3-methylphenol 2.0 0.6 "1

ND " "" "2-Methylnaphthalene 2.0 0.6 "1

ND " "" "Hexachlorocyclopentadiene 2.0 0.6 "1

ND " "" "2,4,6-Trichlorophenol 5.0 1.6 "1


ND " "" "2-Chloronaphthalene 2.0 0.2 "1

ND " "" "2-Nitroaniline 2.0 0.4 "1

ND " "" "Acenaphthylene 2.0 0.3 "1

ND " "" "Dimethyl phthalate 2.0 0.8 "1

ND " "" "2,6-Dinitrotoluene 2.0 0.8 "1

ND " "" "Acenaphthene 2.0 0.6 "1


ND " "" "2,4-Dinitrophenol 10.0 0.3 "1

ND " "" "Dibenzofuran 2.0 0.3 "1


ND " "" "4-Nitrophenol 5.0 0.1 "1

ND " "" "Fluorene 2.0 0.5 "1

ND " "" "4-Chlorophenyl phenyl ether 2.0 0.5 "1

ND " "" "Diethyl phthalate 2.0 0.6 "1


ND " "" "Azobenzene 2.0 0.4 "1

ND " "" "4,6-Dinitro-2-methylphenol 10.0 2.2 "1

ND " "" "N-Nitrosodiphenylamine 2.0 0.6 "1

ND " "" "4-Bromophenyl phenyl ether 2.0 0.8 "1

ND " "" "Hexachlorobenzene 2.0 0.6 "1

ND " "" "Pentachlorophenol 10.0 2.4 "1

ND " "" "Phenanthrene 2.0 0.4 "1

ND " "" "Anthracene 2.0 0.3 "1

ND " "" "Carbazole 2.0 0.6 "1

"0.5 " " ""Di-n-butyl phthalate 2.0 Ja0.4 1

ND " "" "Fluoranthene 2.0 0.6 "1




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-01 (Water)

CAY140625-37


MDL DF


ND 07/02/14 07/03/14 ug/l AXG0033Benzidine 5.0 0.2 "1

ND " "" "Pyrene 2.0 1.0 "1

ND " "" "Butyl benzyl phthalate 2.0 1.0 "1

ND " "" "3,3´-Dichlorobenzidine 5.0 0.8 "1

ND " "" "Benzo (a) anthracene 2.0 0.4 "1

ND " "" "Chrysene 2.0 0.5 "1

ND " "" "Bis(2-ethylhexyl)phthalate 5.0 0.7 "1

ND " "" "Di-n-octyl phthalate 5.0 0.7 "1

ND " "" "Benzo (b) fluoranthene 2.0 0.8 "1

ND " "" "Benzo (k) fluoranthene 2.0 1.0 "1

ND " "" "Benzo (a) pyrene 5.0 1.2 "1

ND " "" "Indeno (1,2,3-cd) pyrene 5.0 1.6 "1

ND " "" "Dibenz (a,h) anthracene 2.0 1.6 "1

ND " "" "Benzo (g,h,i) perylene 2.0 1.3 "1

Surrogate: 2-Fluorophenol "10-13015.3 % % Recovery Limits

Surrogate: Phenol-d6 "10-13015.6 % % Recovery Limits

Surrogate: Nitrobenzene-d5 "10-13044.7 % % Recovery Limits

Surrogate: 2-Fluorobiphenyl "10-13054.1 % % Recovery Limits

Surrogate: 2,4,6-Tribromophenol "10-13060.1 % % Recovery Limits

Surrogate: Terphenyl-dl4 "10-130106 % % Recovery Limits

Organophosphorus Pesticides

ND 07/01/14 07/10/14 ug/l AXG0046Dichlorvos 0.200 0.156 EPA 8141A1

ND " "" "Mevinphos 0.200 0.115 "1

ND " "" "TEPP 0.200 0.151 "1

ND " "" "Demeton 0.200 0.105 "1

ND " "" "Demeton-O 0.200 0.101 "1

ND " "" "Ethoprop 0.200 0.0770 "1

ND " "" "Naled 0.200 0.169 "1

ND " "" "Sulfotep 0.200 0.0950 "1

ND " "" "Monocrotophos 0.200 0.0150 "1

ND " "" "Phorate 0.200 0.0830 "1

ND " "" "Demeton-S 0.200 0.105 "1

ND " "" "Dimethoate 0.200 0.0710 "1




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-01 (Water)

CAY140625-37


MDL DF


ND 07/01/14 07/10/14 ug/l AXG0046Diazinon 0.250 0.0650 "1

ND " "" "Disulfoton 0.200 0.0690 "1

ND " "" "Parathion-methyl 0.200 0.0770 "1

ND " "" "Ronnel 0.200 0.0660 "1

ND " "" "Malathion 0.200 0.159 "1

ND " "" "Dursban (Chlorpyrifos) 0.200 0.0710 "1

ND " "" "Fenthion 0.200 0.0670 "1

ND " "" "Parathion 0.200 0.0790 "1

ND " "" "Trichloronate 0.200 0.0670 "1

ND " "" "Gardona (Stirophos) 0.200 0.110 "1

ND " "" "Tokuthion (Prothiofos) 0.200 0.0770 "1

ND " "" "Merphos 0.200 0.0970 "1

ND " "" "Fensulfothion 0.200 0.139 "1

ND " "" "Bolstar 0.200 0.0860 "1

ND " "" "EPN 0.200 0.124 "1

ND " "" "Azinphos-methyl 0.200 0.0270 "1

ND " "" "Coumaphos 0.200 0.168 "1

ND " "" "Molinate 0.200 0.0440 "1

Surrogate: Tributylphosphate "50-17091.7 % % Recovery Limits

Surrogate: Triphenyl phosphate "50-170120 % % Recovery Limits

Herbicides

EPA 8151A0.257 AXG0042 07/02/14 07/22/14 ug/lDalapon 0.600 Ja0.115 1

ND " "" "3,5-Dichlorobenzoic acid 0.800 0.170 "1

ND " "" "4-Nitrophenol 0.600 0.117 "1

"0.166 " " ""Dicamba 0.400 Ja0.0800 1

ND " "" "MCPP 10.0 0.891 "1

ND " "" "Dichloroprop 0.800 0.196 "1

ND " "" "2,4-D 0.400 0.0860 "1


ND " "" "2,4,5-TP (Silvex) 0.500 0.0950 "1

ND " "" "2,4,5-T 0.500 0.0970 "1

ND " "" "Chloramben 0.800 0.00800 "1

ND " "" "Dinoseb 0.400 0.0830 "1

ND " "" "2,4-DB 0.800 0.157 "1




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-01 (Water)

CAY140625-37


MDL DF

Herbicides

ND 07/02/14 07/22/14 ug/l AXG0042Bentazon 0.600 0.110 "1

ND " "" "DCPA 0.400 0.0150 "1

ND " "" "Picloram 0.800 0.0200 "1

ND " "" "Acifluorfen 0.800 0.157 "1

Surrogate: 2,4-Dichlorophenylacetic acid "43-16949.8 % % Recovery Limits

Ion Chromatography

EPA 300.025.8 AXG0062 06/26/14 06/26/14 mg/LChloride 0.5 0.04 1

"0.5 " " ""Fluoride 0.1 0.02 1

EPA 218.60.3 AXG0064 06/27/14 06/27/14 ug/lHexavalent Chromium 1.0 Ja0.1 1

EPA 300.00.02 AXG0062 06/26/14 06/26/14 mg/LNitrate as Nitrogen 0.11 Ja0.009 1

ND " "" "Nitrite as Nitrogen 0.15 0.03 "1

EPA 314.01.97 AXG0049 07/01/14 07/02/14 ug/lPerchlorate 2.00 Ja0.0940 1

Wet Chemistry

SM2320B234 AXF0233 06/27/14 06/27/14 mg/LTotal Alkalinity 5.00 2.37 1

SM 4500-NH3 B/H0.102 AXG0121 07/08/14 07/14/14 "Ammonia as N 0.100 0.0400 1

EPA 120.1655 AXF0223 06/26/14 06/26/14 uS/cmSpecific Conductance (EC) 5.00 1.09 1

ND 07/08/14 07/11/14 mg/L AXG0105Cyanide 0.00500 0.000900 SM 4500CN E1

SM5540C0.121 AXF0236 06/27/14 06/27/14 "MBAS 0.100 0.0600 1

SM 4500-H+ B8.05 AXF0224 06/26/14 06/26/14 pH UnitspH 0.100 Field0.100 1

SM 2540C387 AXG0054 06/26/14 06/26/14 mg/LTotal Dissolved Solids 15.0 7.68 1

SM2340B190 AXG0141 07/14/14 07/14/14 "Total Hardness 5.00 2.86 1

Total Recoverable Metals

EPA 200.71610 AXG0074 07/08/14 07/09/14 ug/lAluminum 50.0 24.5 1

ND " "" "Antimony 10.0 1.3 "1

"7.7 " " ""Arsenic 10.0 Ja1.0 1

"82.9 " " ""Barium 5.0 1.2 1

ND " "" "Beryllium 5.0 0.09 "1

"349 " " ""Boron 50.0 0.8 1

"0.4 " " ""Cadmium 5.0 Ja0.1 1

"31400 " " ""Calcium 100 79.0 1

"4.0 " " ""Chromium 5.0 Ja0.3 1

"4.6 " " ""Copper 5.0 Ja0.8 1

"1600 " " ""Iron 20.0 11.5 1




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-01 (Water)

CAY140625-37


MDL DF


ND 07/08/14 07/09/14 ug/l AXG0074Lead 5.0 0.9 "1

"21800 " " ""Magnesium 50.0 15.6 1

"231 " " ""Manganese 10.0 0.6 1

"6.5 " " ""Nickel 5.0 0.6 1

ND " "" "Selenium 20.0 1.3 "1

"0.4 " " ""Silver 5.0 Ja0.4 1

"73200 " " ""Sodium 200 120 1

ND " "" "Thallium 20.0 2.2 "1

"74.1 " " ""Titanium 50.0 1.2 1

"2.9 " " ""Zinc 10.0 Ja0.3 1

Dissolved Metals

ND 07/07/14 07/09/14 ug/l AXG0057Dissolved Aluminum 50.0 24.5 EPA 200.71

"7.2 " " ""Dissolved Arsenic 10.0 Ja1.0 1

"15.5 " " ""Dissolved Iron 20.0 Ja11.5 1

ND " "" "Dissolved Lead 5.0 0.9 "1

1613B

ND 07/13/14 07/15/14 pg/l 0001215Total PeCDF 50 2.58 1613B0

"0.115 " " ""TEQ 0

ND " "" "Total TCDF 10 2.01 "0

ND " "" "OCDF 100 6.25 "0

ND " "" "1,2,3,4,7,8-HxCDD 50 3.98 "0

ND " "" "1,2,3,4,7,8,9-HpCDF 50 4.61 "0

ND " "" "1,2,3,4,6,7,8-HpCDF 50 3.77 "0

"9.88 " " ""1,2,3,4,6,7,8-HpCDD 50 J2.17 0

"52.4 " " ""OCDD 100 J4.32 0

ND " "" "Total HxCDF 50 8.74 "0

ND " "" "2,3,7,8-TCDF 10 2.01 "0

ND " "" "2,3,7,8-TCDD 10 2.20 "0

ND " "" "2,3,4,7,8-PeCDF 50 2.36 "0

ND " "" "2,3,4,6,7,8-HxCDF 50 4.97 "0

ND " "" "Total TCDD 10 2.20 "0

ND " "" "1,2,3,7,8-PeCDD 50 2.29 "0

ND " "" "1,2,3,7,8,9-HxCDF 50 8.74 "0




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-01 (Water)

CAY140625-37


MDL DF

1613B

ND 07/13/14 07/15/14 pg/l 00012151,2,3,7,8,9-HxCDD 50 4.68 "0

ND " "" "1,2,3,6,7,8-HxCDF 50 3.97 "0

ND " "" "1,2,3,6,7,8-HxCDD 50 5.34 "0

ND " "" "Total PeCDD 50 2.29 "0

ND " "" "1,2,3,7,8-PeCDF 50 2.58 "0

ND " "" "1,2,3,4,7,8-HxCDF 50 3.66 "0

ND " "" "Total HpCDF 50 4.61 "0

ND " "" "Total HxCDD 50 5.34 "0

"16 " " ""Total HpCDD 50 J3.06 0

Surrogate: 37CL-2,3,7,8-TCDD "35-19798.5 % % Recovery Limits

Surrogate: 13C-1,2,3,7,8-PeCDD "25-18165.6 % % Recovery Limits

Surrogate: 13C-OCDD "17-15753.8 % % Recovery Limits

Surrogate: 13C-2,3,7,8-TCDF "24-16975.2 % % Recovery Limits

Surrogate: 13C-2,3,7,8-TCDD "25-16461.0 % % Recovery Limits

Surrogate: 13C-2,3,4,7,8-PeCDF "21-17877.9 % % Recovery Limits

Surrogate: 13C-2,3,4,6,7,8-HxCDF "28-13665.7 % % Recovery Limits


Surrogate: 13C-1,2,3,4,6,7,8-HpCDD "23-14063.0 % % Recovery Limits

Surrogate: 13C-1,2,3,4,6,7,8-HpCDF "28-14368.6 % % Recovery Limits


Surrogate: 13C-1,2,3,4,7,8-HxCDD "32-14174.9 % % Recovery Limits








Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-01RE1 (Water)

CAY140625-37


MDL DF

Ion Chromatography

EPA 300.087.6 AXG0062 07/08/14 07/08/14 mg/LSulfate as SO4 5.0 0.7 10




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-02 (Water)

CAY140625-38


MDL DF














ND " "" "Acetone 5.0 0.1 "1







ND " "" "2-Butanone 5.0 0.1 "1




ND " "" "Chloroform 0.5 0.05 "1




ND " "" "Benzene 0.5 0.03 "1










Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-02 (Water)

CAY140625-38


MDL DF



ND " "" "Toluene 0.5 0.04 "1





ND " "" "2-Hexanone 5.0 0.1 "1






ND " "" "m,p-Xylene 1.0 0.09 "1

ND " "" "o-Xylene 0.5 0.04 "1


ND " "" "Bromoform 0.5 0.03 "1















"0.04 " " ""n-Butylbenzene 0.5 Ja0.04 1







Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-02 (Water)

CAY140625-38


MDL DF




Surrogate: Dibromofluoromethane "70-13098.3 % % Recovery Limits



EPA 5240.1 AXH0123 07/28/14 08/04/14 "TBA 1.0 Ja0.1 1















"0.2 " " ""Acetone 5.0 Ja0.1 1






ND " "" "2-Butanone 5.0 0.1 "1





ND " "" "Chloroform 0.5 Z-030.05 "1

ND " "" "Benzene 0.5 0.03 "1





Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-02 (Water)

CAY140625-38


MDL DF







ND " "" "Toluene 0.5 0.04 "1


"0.05 " " ""4-Methyl-2-pentanone 5.0 Ja0.05 1






ND " "" "2-Hexanone 5.0 0.1 "1




ND " "" "m,p-Xylene 0.5 0.09 "1

ND " "" "o-Xylene 0.5 0.04 "1


ND " "" "Styrene 0.5 0.09 "1

ND " "" "Bromoform 0.5 0.03 "1
















Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-02 (Water)

CAY140625-38


MDL DF

















ND " "" "beta-BHC 0.100 0.011 "1


ND " "" "delta-BHC 0.100 0.021 "1

ND " "" "Heptachlor 0.100 0.016 "1

ND " "" "Aldrin 0.100 0.011 "1



ND " "" "Endosulfan I 0.100 0.007 "1


ND " "" "4,4'-DDE 0.100 0.005 "1

ND " "" "Dieldrin 0.100 0.006 "1

ND " "" "Endrin 0.100 0.007 "1

ND " "" "Endosulfan II 0.100 0.021 "1

ND " "" "4,4'-DDD 0.100 0.006 "1



ND " "" "4,4'-DDT 0.100 0.004 "1

ND " "" "Endrin Ketone 0.100 0.005 "1

ND " "" "Methoxychlor 0.100 0.013 "1




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-02 (Water)

CAY140625-38


MDL DF




PCBs by GC/ECD

ND " 07/07/14 ug/l AXG0027PCBs 1.00 0.0800 EPA 80821

ND " "" "Aroclor 1016 1.00 0.0600 "1

ND " "" "Aroclor 1221 1.00 0.130 "1

ND " "" "Aroclor 1232 1.00 0.100 "1

ND " "" "Aroclor 1242 1.00 0.0600 "1

ND " "" "Aroclor 1248 1.00 0.0600 "1

ND " "" "Aroclor 1254 1.00 0.0900 "1

ND " "" "Aroclor 1260 1.00 0.0800 "1





ND " "" "Aniline 2.0 0.3 "1


ND " "" "Phenol 2.0 0.3 "1










ND " "" "2-Nitrophenol 5.0 1.2 "1



ND " "" "Benzoic acid 30.0 0.5 "1






Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-02 (Water)

CAY140625-38


MDL DF




















ND " "" "4-Nitrophenol 5.0 0.1 "1

ND " "" "Fluorene 2.0 0.5 "1












ND " "" "Carbazole 2.0 0.6 "1

ND " "" "Di-n-butyl phthalate 2.0 0.4 "1





Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-02 (Water)

CAY140625-38


MDL DF



ND " "" "Pyrene 2.0 1.0 "1




ND " "" "Chrysene 2.0 0.5 "1





ND " "" "Benzo (a) pyrene 5.0 1.2 "1









Surrogate: Terphenyl-dl4 "10-13088.3 % % Recovery Limits



ND " "" "Mevinphos 0.200 0.115 "1

ND " "" "TEPP 0.200 0.151 "1

ND " "" "Demeton 0.200 0.105 "1

ND " "" "Demeton-O 0.200 0.101 "1

ND " "" "Ethoprop 0.200 0.0770 "1

ND " "" "Naled 0.200 0.169 "1

ND " "" "Sulfotep 0.200 0.0950 "1


ND " "" "Phorate 0.200 0.0830 "1

ND " "" "Demeton-S 0.200 0.105 "1

ND " "" "Dimethoate 0.200 0.0710 "1




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-02 (Water)

CAY140625-38


MDL DF



ND " "" "Disulfoton 0.200 0.0690 "1


ND " "" "Ronnel 0.200 0.0660 "1

ND " "" "Malathion 0.200 0.159 "1


ND " "" "Fenthion 0.200 0.0670 "1

ND " "" "Parathion 0.200 0.0790 "1




ND " "" "Merphos 0.200 0.0970 "1


ND " "" "Bolstar 0.200 0.0860 "1

ND " "" "EPN 0.200 0.124 "1


ND " "" "Coumaphos 0.200 0.168 "1

ND " "" "Molinate 0.200 0.0440 "1



Herbicides

ND 07/02/14 07/22/14 ug/l AXG0042Dalapon 0.600 0.115 EPA 8151A1


ND " "" "4-Nitrophenol 0.600 0.117 "1

ND " "" "Dicamba 0.400 0.0800 "1

ND " "" "MCPP 10.0 0.891 "1

"0.372 " " ""Dichloroprop 0.800 Ja0.196 1

"0.258 " " ""2,4-D 0.400 Ja0.0860 1


ND " "" "2,4,5-TP (Silvex) 0.500 0.0950 "1

ND " "" "2,4,5-T 0.500 0.0970 "1

ND " "" "Chloramben 0.800 0.00800 "1

ND " "" "Dinoseb 0.400 0.0830 "1

ND " "" "2,4-DB 0.800 0.157 "1




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-02 (Water)

CAY140625-38


MDL DF

Herbicides


ND " "" "DCPA 0.400 0.0150 "1

ND " "" "Picloram 0.800 0.0200 "1

ND " "" "Acifluorfen 0.800 0.157 "1


Ion Chromatography


"0.1 " " ""Fluoride 0.1 0.02 1



"0.08 " " ""Nitrite as Nitrogen 0.15 Ja0.03 1



Wet Chemistry





ND 06/27/14 06/27/14 " AXF0236MBAS 0.100 0.0600 SM5540C1





ND 07/08/14 07/09/14 ug/l AXG0074Antimony 20.0 2.6 EPA 200.72

"5.2 " " ""Arsenic 20.0 Ja1.9 2

"62.1 AXG0273 07/29/14 07/30/14 "Barium 5.0 1.2 1

ND 07/08/14 07/09/14 " AXG0074Beryllium 10.0 0.2 "2

"61.4 " " ""Boron 100 Ja1.5 2

"0.4 " " ""Cadmium 10.0 Ja0.2 2

"23400 " " ""Calcium 200 158 2

ND " "" "Chromium 10.0 0.6 "2

"4.4 " " ""Copper 10.0 Ja1.6 2

"1030 AXG0273 07/29/14 07/30/14 "Iron 20.0 11.5 1




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-02 (Water)

CAY140625-38


MDL DF


ND 07/08/14 07/09/14 ug/l AXG0074Lead 10.0 1.9 "2

"16300 " " ""Magnesium 100 31.2 2

"123 AXG0273 07/29/14 07/30/14 "Manganese 10.0 0.6 1

"2.9 AXG0074 07/08/14 07/09/14 "Nickel 10.0 Ja1.2 2

ND " "" "Selenium 40.0 2.6 "2

ND " "" "Silver 10.0 0.8 "2

"13400 " " ""Sodium 400 239 2

ND " "" "Thallium 40.0 4.4 "2

"5.8 " " ""Zinc 20.0 Ja0.5 2

Dissolved Metals

EPA 200.738.3 AXG0057 07/07/14 07/09/14 ug/lDissolved Aluminum 50.0 Ja24.5 1


"21.9 AXG0275 07/30/14 07/30/14 "Dissolved Iron 20.0 11.5 1

ND 07/07/14 07/09/14 " AXG0057Dissolved Lead 5.0 0.9 "1

1613B

ND 07/13/14 07/15/14 pg/l 00012152,3,7,8-TCDD 10 2.80 1613B0

ND " "" "1,2,3,7,8-PeCDF 50 2.99 "0

ND " "" "1,2,3,7,8-PeCDD 50 2.60 "0

ND " "" "Total HpCDD 50 5.91 "0

ND " "" "2,3,4,6,7,8-HxCDF 50 5.03 "0

ND " "" "Total HpCDF 50 3.11 "0

ND " "" "1,2,3,4,7,8-HxCDD 50 4.07 "0

ND " "" "1,2,3,6,7,8-HxCDD 50 5.09 "0

ND " "" "1,2,3,4,7,8-HxCDF 50 4.12 "0

ND " "" "Total HxCDD 50 5.09 "0

ND " "" "Total HxCDF 50 9.76 "0

ND " "" "Total PeCDD 50 2.60 "0

ND " "" "Total PeCDF 50 3.03 "0

ND " "" "Total TCDD 10 2.80 "0

ND " "" "Total TCDF 10 2.44 "0

"0.00582 " " ""TEQ 0

ND " "" "1,2,3,7,8,9-HxCDD 50 4.64 "0

ND " "" "2,3,7,8-TCDF 10 2.44 "0




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-02 (Water)

CAY140625-38


MDL DF

1613B

ND 07/13/14 07/15/14 pg/l 0001215OCDF 100 5.86 "0

"19.4 " " ""OCDD 100 J4.32 0

ND " "" "1,2,3,6,7,8-HxCDF 50 4.35 "0

ND " "" "1,2,3,7,8,9-HxCDF 50 9.76 "0

ND " "" "2,3,4,7,8-PeCDF 50 3.03 "0

ND " "" "1,2,3,4,6,7,8-HpCDF 50 2.85 "0

ND " "" "1,2,3,4,7,8,9-HpCDF 50 3.11 "0

ND " "" "1,2,3,4,6,7,8-HpCDD 50 5.91 "0
















Surrogate: 37CL-2,3,7,8-TCDD "35-197102 % % Recovery Limits




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-02RE1 (Water)

CAY140625-38


MDL DF



"61.6 " " ""Titanium 50.0 1.2 1




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-03 (Water)

CAY140625-39


MDL DF














"0.1 " " ""Acetone 5.0 Ja0.1 1







ND " "" "2-Butanone 5.0 0.1 "1




ND " "" "Chloroform 0.5 0.05 "1




ND " "" "Benzene 0.5 0.03 "1










Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-03 (Water)

CAY140625-39


MDL DF



ND " "" "Toluene 0.5 0.04 "1





ND " "" "2-Hexanone 5.0 0.1 "1






ND " "" "m,p-Xylene 1.0 0.09 "1

ND " "" "o-Xylene 0.5 0.04 "1


ND " "" "Bromoform 0.5 0.03 "1






















Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-03 (Water)

CAY140625-39


MDL DF







ND 07/28/14 08/04/14 " AXH0123TBA 1.0 0.1 EPA 5241














"0.2 " " ""Methylene chloride 1.0 Ja0.08 1

ND " "" "Acetone 5.0 0.1 "1






ND " "" "2-Butanone 5.0 0.1 "1





ND " "" "Chloroform 0.5 Z-030.05 "1

ND " "" "Benzene 0.5 0.03 "1





Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-03 (Water)

CAY140625-39


MDL DF







ND " "" "Toluene 0.5 0.04 "1


ND " "" "4-Methyl-2-pentanone 5.0 0.05 "1





ND " "" "2-Hexanone 5.0 0.1 "1





ND " "" "m,p-Xylene 0.5 0.09 "1

ND " "" "o-Xylene 0.5 0.04 "1


ND " "" "Styrene 0.5 0.09 "1

ND " "" "Bromoform 0.5 0.03 "1
















Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-03 (Water)

CAY140625-39


MDL DF

















ND " "" "beta-BHC 0.100 0.011 "1


ND " "" "delta-BHC 0.100 0.021 "1

ND " "" "Heptachlor 0.100 0.016 "1

ND " "" "Aldrin 0.100 0.011 "1



ND " "" "Endosulfan I 0.100 0.007 "1


ND " "" "4,4'-DDE 0.100 0.005 "1

ND " "" "Dieldrin 0.100 0.006 "1

ND " "" "Endrin 0.100 0.007 "1

ND " "" "Endosulfan II 0.100 0.021 "1

ND " "" "4,4'-DDD 0.100 0.006 "1


ND " "" "Endosulfan sulfate 0.100 0.005 "1

ND " "" "4,4'-DDT 0.100 0.004 "1

ND " "" "Endrin Ketone 0.100 0.005 "1

ND " "" "Methoxychlor 0.100 0.013 "1




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-03 (Water)

CAY140625-39


MDL DF




PCBs by GC/ECD


ND " "" "Aroclor 1016 1.00 0.0600 "1

ND " "" "Aroclor 1221 1.00 0.130 "1

ND " "" "Aroclor 1232 1.00 0.100 "1

ND " "" "Aroclor 1242 1.00 0.0600 "1

ND " "" "Aroclor 1248 1.00 0.0600 "1

ND " "" "Aroclor 1254 1.00 0.0900 "1

ND " "" "Aroclor 1260 1.00 0.0800 "1





ND " "" "Aniline 2.0 0.3 "1


ND " "" "Phenol 2.0 0.3 "1










ND " "" "2-Nitrophenol 5.0 1.2 "1



ND " "" "Benzoic acid 30.0 0.5 "1






Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-03 (Water)

CAY140625-39


MDL DF




















ND " "" "4-Nitrophenol 5.0 0.1 "1

ND " "" "Fluorene 2.0 0.5 "1












ND " "" "Carbazole 2.0 0.6 "1






Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-03 (Water)

CAY140625-39


MDL DF



ND " "" "Pyrene 2.0 1.0 "1




ND " "" "Chrysene 2.0 0.5 "1





ND " "" "Benzo (a) pyrene 5.0 1.2 "1












ND " "" "Mevinphos 0.200 0.115 "1

ND " "" "TEPP 0.200 0.151 "1

ND " "" "Demeton 0.200 0.105 "1

ND " "" "Demeton-O 0.200 0.101 "1

ND " "" "Ethoprop 0.200 0.0770 "1

ND " "" "Naled 0.200 0.169 "1

ND " "" "Sulfotep 0.200 0.0950 "1


ND " "" "Phorate 0.200 0.0830 "1

ND " "" "Demeton-S 0.200 0.105 "1

ND " "" "Dimethoate 0.200 0.0710 "1




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-03 (Water)

CAY140625-39


MDL DF



ND " "" "Disulfoton 0.200 0.0690 "1


ND " "" "Ronnel 0.200 0.0660 "1

ND " "" "Malathion 0.200 0.159 "1


ND " "" "Fenthion 0.200 0.0670 "1

ND " "" "Parathion 0.200 0.0790 "1




ND " "" "Merphos 0.200 0.0970 "1


ND " "" "Bolstar 0.200 0.0860 "1

ND " "" "EPN 0.200 0.124 "1


ND " "" "Coumaphos 0.200 0.168 "1

ND " "" "Molinate 0.200 0.0440 "1



Herbicides



ND " "" "4-Nitrophenol 0.600 0.117 "1

"0.213 " " ""Dicamba 0.400 Ja0.0800 1

ND " "" "MCPP 10.0 0.891 "1

"0.338 " " ""Dichloroprop 0.800 Ja0.196 1

ND " "" "2,4-D 0.400 0.0860 "1


ND " "" "2,4,5-TP (Silvex) 0.500 0.0950 "1

ND " "" "2,4,5-T 0.500 0.0970 "1

ND " "" "Chloramben 0.800 0.00800 "1

ND " "" "Dinoseb 0.400 0.0830 "1

ND " "" "2,4-DB 0.800 0.157 "1




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-03 (Water)

CAY140625-39


MDL DF

Herbicides


ND " "" "DCPA 0.400 0.0150 "1

ND " "" "Picloram 0.800 0.0200 "1

ND " "" "Acifluorfen 0.800 0.157 "1

Surrogate: 2,4-Dichlorophenylacetic acid " QR-07,

Z-01a

43-169 % % Recovery Limits

Ion Chromatography


"0.08 " " ""Fluoride 0.1 Ja0.02 1




ND 07/01/14 07/02/14 ug/l AXG0049Perchlorate 2.00 0.0940 EPA 314.01


Wet Chemistry

SM2320B62.0 AXF0233 06/27/14 06/27/14 mg/LTotal Alkalinity 5.00 2.37 1




ND 06/27/14 06/27/14 " AXF0236MBAS 0.100 0.0600 SM5540C1


SM 2540C90.0 AXG0054 06/26/14 06/26/14 mg/LTotal Dissolved Solids 15.0 7.68 1

SM2340B52.0 AXG0141 07/14/14 07/14/14 "Total Hardness 5.00 2.86 1



ND " "" "Antimony 10.0 1.3 "1

"2.0 " " ""Arsenic 10.0 Ja1.0 1

"17.8 " " ""Barium 5.0 1.2 1

ND " "" "Beryllium 5.0 0.09 "1

"48.8 " " ""Boron 50.0 Ja0.8 1

"0.2 " " ""Cadmium 5.0 Ja0.1 1

"10300 " " ""Calcium 100 79.0 1

"1.4 " " ""Chromium 5.0 Ja0.3 1

"3.1 " " ""Copper 5.0 Ja0.8 1




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-03 (Water)

CAY140625-39


MDL DF


"403 AXG0074 07/08/14 07/09/14 ug/lIron 20.0 11.5 1

ND " "" "Lead 5.0 0.9 "1

"4440 " " ""Magnesium 50.0 15.6 1

"14.0 " " ""Manganese 10.0 0.6 1

"1.4 " " ""Nickel 5.0 Ja0.6 1

ND " "" "Selenium 20.0 1.3 "1

ND " "" "Silver 5.0 0.4 "1

"6660 " " ""Sodium 200 120 1

ND " "" "Thallium 20.0 2.2 "1

"14.6 " " ""Titanium 50.0 Ja1.2 1

"1.0 " " ""Zinc 10.0 Ja0.3 1

Dissolved Metals

EPA 200.744.4 AXG0057 07/07/14 07/09/14 ug/lDissolved Aluminum 50.0 Ja24.5 1


"33.4 " " ""Dissolved Iron 20.0 11.5 1


1613B

ND 07/13/14 07/15/14 pg/l 00012151,2,3,6,7,8-HxCDD 50 8.03 1613B0

ND " "" "1,2,3,4,7,8-HxCDF 50 4.67 "0

ND " "" "1,2,3,4,7,8-HxCDD 50 5.34 "0

ND " "" "1,2,3,4,7,8,9-HpCDF 50 4.55 "0

ND " "" "OCDF 100 8.16 "0

ND " "" "1,2,3,7,8-PeCDD 50 3.71 "0

ND " "" "Total TCDF 10 2.63 "0

ND " "" "1,2,3,4,6,7,8-HpCDF 50 3.74 "0

ND " "" "1,2,3,4,6,7,8-HpCDD 50 7.40 "0

ND " "" "1,2,3,6,7,8-HxCDF 50 4.96 "0

ND " "" "1,2,3,7,8,9-HxCDD 50 6.63 "0

ND " "" "2,3,7,8-TCDD 10 3.02 "0

ND " "" "1,2,3,7,8,9-HxCDF 50 10.9 "0

ND " "" "Total HpCDF 50 4.55 "0

ND " "" "2,3,4,6,7,8-HxCDF 50 5.99 "0

ND " "" "Total TCDD 10 3.02 "0




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-03 (Water)

CAY140625-39


MDL DF

1613B

ND 07/13/14 07/15/14 pg/l 00012152,3,4,7,8-PeCDF 50 3.17 "0

ND " "" "2,3,7,8-TCDF 10 2.63 "0

"14.7 " " ""OCDD 100 J4.32 0

"0.00441 " " ""TEQ 0

ND " "" "Total HpCDD 50 7.40 "0

ND " "" "Total HxCDD 50 8.03 "0

ND " "" "Total PeCDD 50 3.71 "0

ND " "" "Total PeCDF 50 3.33 "0

ND " "" "Total HxCDF 50 10.9 "0

ND " "" "1,2,3,7,8-PeCDF 50 3.33 "0




















Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-04 (Water)

CAY140625-40


MDL DF














ND " "" "Acetone 5.0 0.1 "1







ND " "" "2-Butanone 5.0 0.1 "1




ND " "" "Chloroform 0.5 0.05 "1




ND " "" "Benzene 0.5 0.03 "1










Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-04 (Water)

CAY140625-40


MDL DF



ND " "" "Toluene 0.5 0.04 "1





ND " "" "2-Hexanone 5.0 0.1 "1






ND " "" "m,p-Xylene 1.0 0.09 "1

ND " "" "o-Xylene 0.5 0.04 "1


ND " "" "Bromoform 0.5 0.03 "1






















Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-04 (Water)

CAY140625-40


MDL DF







EPA 5240.2 AXH0123 07/28/14 08/04/14 "TBA 1.0 Ja0.1 1




"0.2 " " ""Tert-Amyl Methyl Ether 0.5 Ja0.03 1










"0.1 " " ""Acetone 5.0 Ja0.1 1







ND " "" "2-Butanone 5.0 0.1 "1





ND " "" "Chloroform 0.5 Z-030.05 "1

ND " "" "Benzene 0.5 0.03 "1





Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-04 (Water)

CAY140625-40


MDL DF







ND " "" "Toluene 0.5 0.04 "1








ND " "" "2-Hexanone 5.0 0.1 "1




ND " "" "m,p-Xylene 0.5 0.09 "1

ND " "" "o-Xylene 0.5 0.04 "1


ND " "" "Styrene 0.5 0.09 "1

"0.03 " " ""Bromoform 0.5 Ja0.03 1



"0.04 " " ""1,1,2,2-Tetrachloroethane 0.5 Ja0.04 1













Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-04 (Water)

CAY140625-40


MDL DF

















ND " "" "beta-BHC 0.100 0.011 "1


ND " "" "delta-BHC 0.100 0.021 "1

ND " "" "Heptachlor 0.100 0.016 "1

ND " "" "Aldrin 0.100 0.011 "1



ND " "" "Endosulfan I 0.100 0.007 "1


ND " "" "4,4'-DDE 0.100 0.005 "1

ND " "" "Dieldrin 0.100 0.006 "1

ND " "" "Endrin 0.100 0.007 "1

ND " "" "Endosulfan II 0.100 0.021 "1

ND " "" "4,4'-DDD 0.100 0.006 "1



ND " "" "4,4'-DDT 0.100 0.004 "1

ND " "" "Endrin Ketone 0.100 0.005 "1

ND " "" "Methoxychlor 0.100 0.013 "1




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-04 (Water)

CAY140625-40


MDL DF




PCBs by GC/ECD


ND " "" "PCBs 1.00 0.0800 "1

ND " "" "Aroclor 1221 1.00 0.130 "1

ND " "" "Aroclor 1232 1.00 0.100 "1

ND " "" "Aroclor 1242 1.00 0.0600 "1

ND " "" "Aroclor 1248 1.00 0.0600 "1

ND " "" "Aroclor 1254 1.00 0.0900 "1

ND " "" "Aroclor 1260 1.00 0.0800 "1





ND " "" "Aniline 2.0 0.3 "1


ND " "" "Phenol 2.0 0.3 "1










ND " "" "2-Nitrophenol 5.0 1.2 "1



ND " "" "Benzoic acid 30.0 0.5 "1






Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-04 (Water)

CAY140625-40


MDL DF




















ND " "" "4-Nitrophenol 5.0 0.1 "1

ND " "" "Fluorene 2.0 0.5 "1












ND " "" "Carbazole 2.0 0.6 "1






Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-04 (Water)

CAY140625-40


MDL DF



ND " "" "Pyrene 2.0 1.0 "1




ND " "" "Chrysene 2.0 0.5 "1





ND " "" "Benzo (a) pyrene 5.0 1.2 "1









Surrogate: Terphenyl-dl4 "10-130102 % % Recovery Limits



ND " "" "Mevinphos 0.200 0.115 "1

ND " "" "TEPP 0.200 0.151 "1

ND " "" "Demeton 0.200 0.105 "1

ND " "" "Demeton-O 0.200 0.101 "1

ND " "" "Ethoprop 0.200 0.0770 "1

ND " "" "Naled 0.200 0.169 "1

ND " "" "Sulfotep 0.200 0.0950 "1


ND " "" "Phorate 0.200 0.0830 "1

ND " "" "Demeton-S 0.200 0.105 "1

ND " "" "Dimethoate 0.200 0.0710 "1




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-04 (Water)

CAY140625-40


MDL DF



ND " "" "Disulfoton 0.200 0.0690 "1


ND " "" "Ronnel 0.200 0.0660 "1

ND " "" "Malathion 0.200 0.159 "1


ND " "" "Fenthion 0.200 0.0670 "1

ND " "" "Parathion 0.200 0.0790 "1




ND " "" "Merphos 0.200 0.0970 "1


ND " "" "Bolstar 0.200 0.0860 "1

ND " "" "EPN 0.200 0.124 "1


ND " "" "Coumaphos 0.200 0.168 "1

ND " "" "Molinate 0.200 0.0440 "1



Herbicides



ND " "" "4-Nitrophenol 0.600 0.117 "1

"0.0877 " " ""Dicamba 0.400 Ja0.0800 1

ND " "" "MCPP 10.0 0.891 "1

"0.248 " " ""Dichloroprop 0.800 Ja0.196 1

ND " "" "2,4-D 0.400 0.0860 "1


ND " "" "2,4,5-TP (Silvex) 0.500 0.0950 "1

ND " "" "2,4,5-T 0.500 0.0970 "1

ND " "" "Chloramben 0.800 0.00800 "1

ND " "" "Dinoseb 0.400 0.0830 "1

ND " "" "2,4-DB 0.800 0.157 "1




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-04 (Water)

CAY140625-40


MDL DF

Herbicides


ND " "" "DCPA 0.400 0.0150 "1

ND " "" "Picloram 0.800 0.0200 "1

ND " "" "Acifluorfen 0.800 0.157 "1


Ion Chromatography


"0.06 " " ""Fluoride 0.1 Ja0.02 1






Wet Chemistry

SM2320B48.0 AXF0233 06/27/14 06/27/14 mg/LTotal Alkalinity 5.00 2.37 1


EPA 120.198.1 AXF0223 06/26/14 06/26/14 uS/cmSpecific Conductance (EC) 5.00 1.09 1


ND 06/27/14 06/27/14 " AXF0236MBAS 0.100 0.0600 SM5540C1



SM2340B48.0 AXG0141 07/14/14 07/14/14 "Total Hardness 5.00 2.86 1



ND " "" "Antimony 10.0 1.3 "1

ND " "" "Arsenic 10.0 1.0 "1

"14.2 " " ""Barium 5.0 1.2 1

ND " "" "Beryllium 5.0 0.09 "1

"22.8 " " ""Boron 50.0 Ja0.8 1

"0.1 " " ""Cadmium 5.0 Ja0.1 1

"9300 " " ""Calcium 100 79.0 1

"1.3 " " ""Chromium 5.0 Ja0.3 1

"2.8 " " ""Copper 5.0 Ja0.8 1




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-04 (Water)

CAY140625-40


MDL DF


"386 AXG0074 07/08/14 07/09/14 ug/lIron 20.0 11.5 1

ND " "" "Lead 5.0 0.9 "1

"3470 " " ""Magnesium 50.0 15.6 1

"27.6 " " ""Manganese 10.0 0.6 1

"1.7 " " ""Nickel 5.0 Ja0.6 1

ND " "" "Selenium 20.0 1.3 "1

ND " "" "Silver 5.0 0.4 "1

"3860 " " ""Sodium 200 120 1

ND " "" "Thallium 20.0 2.2 "1

"16.2 " " ""Titanium 50.0 Ja1.2 1

"2.1 " " ""Zinc 10.0 Ja0.3 1

Dissolved Metals



"65.2 " " ""Dissolved Iron 20.0 11.5 1


1613B

ND 07/13/14 07/15/14 pg/l 00012152,3,7,8-TCDF 10 2.09 1613B0

ND " "" "1,2,3,6,7,8-HxCDF 50 3.94 "0

"0.0179 " " ""TEQ 0

ND " "" "OCDF 100 7.25 "0

ND " "" "2,3,4,7,8-PeCDF 50 3.24 "0

ND " "" "1,2,3,7,8,9-HxCDD 50 6.74 "0

ND " "" "1,2,3,4,6,7,8-HpCDD 50 9.21 "0

ND " "" "Total HpCDD 50 9.21 "0

ND " "" "1,2,3,6,7,8-HxCDD 50 7.84 "0

ND " "" "1,2,3,4,7,8-HxCDF 50 3.62 "0

ND " "" "1,2,3,4,7,8-HxCDD 50 5.62 "0

ND " "" "1,2,3,4,7,8,9-HpCDF 50 4.69 "0

ND " "" "Total HpCDF 50 4.69 "0

ND " "" "1,2,3,4,6,7,8-HpCDF 50 3.86 "0

"59.8 " " ""OCDD 100 J4.32 0

ND " "" "1,2,3,7,8,9-HxCDF 50 8.38 "0




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-04 (Water)

CAY140625-40


MDL DF

1613B

ND 07/13/14 07/15/14 pg/l 00012152,3,7,8-TCDD 10 1.76 "0

ND " "" "Total TCDD 10 1.76 "0

ND " "" "Total TCDF 10 2.09 "0

ND " "" "2,3,4,6,7,8-HxCDF 50 4.89 "0

ND " "" "Total HxCDF 50 8.38 "0

ND " "" "1,2,3,7,8-PeCDF 50 3.48 "0

ND " "" "1,2,3,7,8-PeCDD 50 3.06 "0

ND " "" "Total HxCDD 50 7.84 "0

ND " "" "Total PeCDF 50 3.48 "0

ND " "" "Total PeCDD 50 3.06 "0




















Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-05 (Water)

CAY140625-3


MDL DF














ND " "" "Acetone 5.0 0.1 "1







ND " "" "2-Butanone 5.0 0.1 "1




ND " "" "Chloroform 0.5 0.05 "1




ND " "" "Benzene 0.5 0.03 "1










Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-05 (Water)

CAY140625-3


MDL DF



"0.04 " " ""Toluene 0.5 Ja0.04 1





ND " "" "2-Hexanone 5.0 0.1 "1






ND " "" "m,p-Xylene 1.0 0.09 "1

ND " "" "o-Xylene 0.5 0.04 "1


ND " "" "Bromoform 0.5 0.03 "1






















Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-05 (Water)

CAY140625-3


MDL DF






Surrogate: 4-Bromofluorobenzene "70-130100 % % Recovery Limits

ND 07/28/14 08/04/14 " AXH0123TBA 1.0 0.1 EPA 5241















ND " "" "Acetone 5.0 0.1 "1






ND " "" "2-Butanone 5.0 0.1 "1





ND " "" "Chloroform 0.5 Z-030.05 "1

ND " "" "Benzene 0.5 0.03 "1





Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-05 (Water)

CAY140625-3


MDL DF







ND " "" "Toluene 0.5 0.04 "1







ND " "" "2-Hexanone 5.0 0.1 "1





ND " "" "m,p-Xylene 0.5 0.09 "1

ND " "" "o-Xylene 0.5 0.04 "1


ND " "" "Styrene 0.5 0.09 "1

ND " "" "Bromoform 0.5 0.03 "1
















Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-05 (Water)

CAY140625-3


MDL DF

















ND " "" "beta-BHC 0.100 0.011 "1


ND " "" "delta-BHC 0.100 0.021 "1

ND " "" "Heptachlor 0.100 0.016 "1

ND " "" "Aldrin 0.100 0.011 "1



ND " "" "Endosulfan I 0.100 0.007 "1


ND " "" "4,4'-DDE 0.100 0.005 "1

ND " "" "Dieldrin 0.100 0.006 "1

ND " "" "Endrin 0.100 0.007 "1

ND " "" "Endosulfan II 0.100 0.021 "1

ND " "" "4,4'-DDD 0.100 0.006 "1



ND " "" "4,4'-DDT 0.100 0.004 "1

ND " "" "Endrin Ketone 0.100 0.005 "1

ND " "" "Methoxychlor 0.100 0.013 "1




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-05 (Water)

CAY140625-3


MDL DF




PCBs by GC/ECD


ND " "" "PCBs 1.00 0.0800 "1

ND " "" "Aroclor 1221 1.00 0.130 "1

ND " "" "Aroclor 1232 1.00 0.100 "1

ND " "" "Aroclor 1242 1.00 0.0600 "1

ND " "" "Aroclor 1248 1.00 0.0600 "1

ND " "" "Aroclor 1254 1.00 0.0900 "1

ND " "" "Aroclor 1260 1.00 0.0800 "1





ND " "" "Aniline 2.0 0.3 "1


ND " "" "Phenol 2.0 0.3 "1










ND " "" "2-Nitrophenol 5.0 1.2 "1



ND " "" "Benzoic acid 30.0 0.5 "1






Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-05 (Water)

CAY140625-3


MDL DF




















ND " "" "4-Nitrophenol 5.0 0.1 "1

ND " "" "Fluorene 2.0 0.5 "1












ND " "" "Carbazole 2.0 0.6 "1

"0.4 " " ""Di-n-butyl phthalate 2.0 Ja0.4 1





Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-05 (Water)

CAY140625-3


MDL DF



ND " "" "Pyrene 2.0 1.0 "1




ND " "" "Chrysene 2.0 0.5 "1





ND " "" "Benzo (a) pyrene 5.0 1.2 "1












ND " "" "Mevinphos 0.200 0.115 "1

ND " "" "TEPP 0.200 0.151 "1

ND " "" "Demeton 0.200 0.105 "1

ND " "" "Demeton-O 0.200 0.101 "1

ND " "" "Ethoprop 0.200 0.0770 "1

ND " "" "Naled 0.200 0.169 "1

ND " "" "Sulfotep 0.200 0.0950 "1


ND " "" "Phorate 0.200 0.0830 "1

ND " "" "Demeton-S 0.200 0.105 "1

ND " "" "Dimethoate 0.200 0.0710 "1




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-05 (Water)

CAY140625-3


MDL DF



ND " "" "Disulfoton 0.200 0.0690 "1


ND " "" "Ronnel 0.200 0.0660 "1

ND " "" "Malathion 0.200 0.159 "1


ND " "" "Fenthion 0.200 0.0670 "1

ND " "" "Parathion 0.200 0.0790 "1




ND " "" "Merphos 0.200 0.0970 "1


ND " "" "Bolstar 0.200 0.0860 "1

ND " "" "EPN 0.200 0.124 "1


ND " "" "Coumaphos 0.200 0.168 "1

ND " "" "Molinate 0.200 0.0440 "1



Herbicides



ND " "" "4-Nitrophenol 0.600 0.117 "1

"0.207 " " ""Dicamba 0.400 Ja0.0800 1

ND " "" "MCPP 10.0 0.891 "1

ND " "" "Dichloroprop 0.800 0.196 "1

"0.135 " " ""2,4-D 0.400 Ja0.0860 1


ND " "" "2,4,5-TP (Silvex) 0.500 0.0950 "1

ND " "" "2,4,5-T 0.500 0.0970 "1

ND " "" "Chloramben 0.800 0.00800 "1

ND " "" "Dinoseb 0.400 0.0830 "1

ND " "" "2,4-DB 0.800 0.157 "1




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-05 (Water)

CAY140625-3


MDL DF

Herbicides


ND " "" "DCPA 0.400 0.0150 "1

ND " "" "Picloram 0.800 0.0200 "1

ND " "" "Acifluorfen 0.800 0.157 "1


Ion Chromatography


"0.1 " " ""Fluoride 0.1 0.02 1






Wet Chemistry





ND 06/27/14 06/27/14 " AXF0236MBAS 0.100 0.0600 SM5540C1






ND " "" "Antimony 10.0 1.3 "1

"5.4 " " ""Arsenic 10.0 Ja1.0 1

"64.8 AXG0273 07/29/14 07/30/14 "Barium 5.0 1.2 1

ND 07/08/14 07/09/14 " AXG0074Beryllium 5.0 0.09 "1

"62.4 " " ""Boron 50.0 0.8 1

"0.4 " " ""Cadmium 5.0 Ja0.1 1

"24200 " " ""Calcium 100 79.0 1

"3.8 " " ""Chromium 5.0 Ja0.3 1

"5.2 " " ""Copper 5.0 0.8 1




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-05 (Water)

CAY140625-3


MDL DF


"1270 AXG0273 07/29/14 07/30/14 ug/lIron 20.0 11.5 1

ND 07/08/14 07/09/14 " AXG0074Lead 5.0 0.9 "1

"17200 " " ""Magnesium 50.0 15.6 1

"123 AXG0273 07/29/14 07/30/14 "Manganese 10.0 0.6 1

"5.3 AXG0074 07/08/14 07/09/14 "Nickel 5.0 0.6 1

ND " "" "Selenium 20.0 1.3 "1

"0.4 " " ""Silver 5.0 Ja0.4 1

"14000 " " ""Sodium 200 120 1

ND " "" "Thallium 20.0 2.2 "1

"70.3 " " ""Titanium 50.0 1.2 1

"4.1 " " ""Zinc 10.0 Ja0.3 1

Dissolved Metals



ND 07/30/14 07/30/14 " AXG0275Dissolved Iron 20.0 11.5 "1

ND 07/07/14 07/09/14 " AXG0057Dissolved Lead 5.0 0.9 "1

1613B

ND 07/13/14 07/15/14 pg/l 00012151,2,3,6,7,8-HxCDD 50 6.40 1613B0

ND " "" "1,2,3,7,8,9-HxCDF 50 8.47 "0

ND " "" "1,2,3,6,7,8-HxCDF 50 3.85 "0

ND " "" "1,2,3,7,8-PeCDD 50 2.96 "0

ND " "" "1,2,3,7,8,9-HxCDD 50 5.37 "0

ND " "" "Total PeCDF 50 1.28 "0

ND " "" "Total PeCDD 50 2.96 "0

ND " "" "1,2,3,7,8-PeCDF 50 3.03 "0

ND " "" "Total TCDF 10 3.48 "0

ND " "" "Total HxCDD 50 6.40 "0

ND " "" "1,2,3,4,7,8-HxCDD 50 4.45 "0

ND " "" "1,2,3,4,6,7,8-HpCDD 50 9.83 "0

ND " "" "1,2,3,4,6,7,8-HpCDF 50 4.92 "0

ND " "" "1,2,3,4,7,8,9-HpCDF 50 6.19 "0

ND " "" "1,2,3,4,7,8-HxCDF 50 3.74 "0

ND " "" "2,3,4,6,7,8-HxCDF 50 5.30 "0




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-05 (Water)

CAY140625-3


MDL DF

1613B

"0.0113 0001215 07/13/14 07/15/14 pg/lTEQ 0

ND " "" "OCDF 100 8.69 "0

"37.7 " " ""OCDD 100 J4.32 0

ND " "" "2,3,7,8-TCDF 10 3.48 "0

ND " "" "2,3,4,7,8-PeCDF 50 2.80 "0

ND " "" "Total HxCDF 50 2.35 "0

ND " "" "Total TCDD 10 1.62 "0

ND " "" "Total HpCDD 50 9.83 "0

ND " "" "2,3,7,8-TCDD 10 1.62 "0

ND " "" "Total HpCDF 50 6.19 "0




















Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-06 (Water)

CAY140625-4


MDL DF














"0.1 " " ""Acetone 5.0 Ja0.1 1







ND " "" "2-Butanone 5.0 0.1 "1




"18.9 " " ""Chloroform 0.5 0.05 1




ND " "" "Benzene 0.5 0.03 "1










Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-06 (Water)

CAY140625-4


MDL DF



ND " "" "Toluene 0.5 0.04 "1





ND " "" "2-Hexanone 5.0 0.1 "1






ND " "" "m,p-Xylene 1.0 0.09 "1

ND " "" "o-Xylene 0.5 0.04 "1


ND " "" "Bromoform 0.5 0.03 "1






















Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-06 (Water)

CAY140625-4


MDL DF







ND 07/28/14 08/04/14 " AXH0123TBA 1.0 0.1 EPA 5241












"22.2 " " ""Total Trihalomethanes 0.5 0.5 1


"0.4 " " ""Acetone 5.0 Ja0.1 1

"1.9 " " ""Methylene chloride 1.0 Z-020.08 1






ND " "" "2-Butanone 5.0 0.1 "1





"22.2 " " ""Chloroform 0.5 Z-030.05 1

ND " "" "Benzene 0.5 0.03 "1





Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-06 (Water)

CAY140625-4


MDL DF


ND 07/28/14 08/04/14 ug/l AXH01231,1-Dichloropropene 0.5 0.03 "1





ND " "" "Toluene 0.5 0.04 "1







"0.1 " " ""2-Hexanone 5.0 Ja0.1 1





ND " "" "m,p-Xylene 0.5 0.09 "1

ND " "" "o-Xylene 0.5 0.04 "1


ND " "" "Styrene 0.5 0.09 "1

ND " "" "Bromoform 0.5 0.03 "1
















Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-06 (Water)

CAY140625-4


MDL DF

















ND " "" "beta-BHC 0.100 0.011 "1


ND " "" "delta-BHC 0.100 0.021 "1

ND " "" "Heptachlor 0.100 0.016 "1

ND " "" "Aldrin 0.100 0.011 "1



ND " "" "Endosulfan I 0.100 0.007 "1


ND " "" "4,4'-DDE 0.100 0.005 "1

ND " "" "Dieldrin 0.100 0.006 "1

ND " "" "Endrin 0.100 0.007 "1

ND " "" "Endosulfan II 0.100 0.021 "1

ND " "" "4,4'-DDD 0.100 0.006 "1



ND " "" "4,4'-DDT 0.100 0.004 "1

ND " "" "Endrin Ketone 0.100 0.005 "1

ND " "" "Methoxychlor 0.100 0.013 "1




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-06 (Water)

CAY140625-4


MDL DF




PCBs by GC/ECD


ND " "" "Aroclor 1016 1.00 0.0600 "1

ND " "" "Aroclor 1221 1.00 0.130 "1

ND " "" "Aroclor 1232 1.00 0.100 "1

ND " "" "Aroclor 1242 1.00 0.0600 "1

ND " "" "Aroclor 1248 1.00 0.0600 "1

ND " "" "Aroclor 1254 1.00 0.0900 "1

ND " "" "Aroclor 1260 1.00 0.0800 "1





ND " "" "Aniline 2.0 0.3 "1


ND " "" "Phenol 2.0 0.3 "1










ND " "" "2-Nitrophenol 5.0 1.2 "1



ND " "" "Benzoic acid 30.0 0.5 "1






Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-06 (Water)

CAY140625-4


MDL DF




















ND " "" "4-Nitrophenol 5.0 0.1 "1

ND " "" "Fluorene 2.0 0.5 "1












ND " "" "Carbazole 2.0 0.6 "1






Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-06 (Water)

CAY140625-4


MDL DF



ND " "" "Pyrene 2.0 1.0 "1




ND " "" "Chrysene 2.0 0.5 "1





ND " "" "Benzo (a) pyrene 5.0 1.2 "1












ND " "" "Mevinphos 0.200 0.115 "1

ND " "" "TEPP 0.200 0.151 "1

ND " "" "Demeton 0.200 0.105 "1

ND " "" "Demeton-O 0.200 0.101 "1

ND " "" "Ethoprop 0.200 0.0770 "1

ND " "" "Naled 0.200 0.169 "1

ND " "" "Sulfotep 0.200 0.0950 "1


ND " "" "Phorate 0.200 0.0830 "1

ND " "" "Demeton-S 0.200 0.105 "1

ND " "" "Dimethoate 0.200 0.0710 "1




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-06 (Water)

CAY140625-4


MDL DF



ND " "" "Disulfoton 0.200 0.0690 "1


ND " "" "Ronnel 0.200 0.0660 "1

ND " "" "Malathion 0.200 0.159 "1


ND " "" "Fenthion 0.200 0.0670 "1

ND " "" "Parathion 0.200 0.0790 "1




ND " "" "Merphos 0.200 0.0970 "1


ND " "" "Bolstar 0.200 0.0860 "1

ND " "" "EPN 0.200 0.124 "1


ND " "" "Coumaphos 0.200 0.168 "1

ND " "" "Molinate 0.200 0.0440 "1



Herbicides



ND " "" "4-Nitrophenol 0.600 0.117 "1

"0.400 " " ""Dicamba 0.400 0.0800 1

ND " "" "MCPP 10.0 0.891 "1

ND " "" "Dichloroprop 0.800 0.196 "1

ND " "" "2,4-D 0.400 0.0860 "1


ND " "" "2,4,5-TP (Silvex) 0.500 0.0950 "1

ND " "" "2,4,5-T 0.500 0.0970 "1

ND " "" "Chloramben 0.800 0.00800 "1

ND " "" "Dinoseb 0.400 0.0830 "1

ND " "" "2,4-DB 0.800 0.157 "1




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-06 (Water)

CAY140625-4


MDL DF

Herbicides


ND " "" "DCPA 0.400 0.0150 "1

ND " "" "Picloram 0.800 0.0200 "1

ND " "" "Acifluorfen 0.800 0.157 "1

Surrogate: 2,4-Dichlorophenylacetic acid " QR-07,

Z-01

43-16937.0 % % Recovery Limits

Ion Chromatography

EPA 300.00.1 AXG0062 06/26/14 06/26/14 mg/LChloride 0.5 Ja0.04 1

ND " "" "Fluoride 0.1 0.02 "1


ND 06/26/14 06/26/14 mg/L AXG0062Nitrate as Nitrogen 0.11 0.009 EPA 300.01



ND 06/26/14 06/26/14 mg/L AXG0062Sulfate as SO4 0.5 0.07 EPA 300.01

Wet Chemistry

ND 06/27/14 06/27/14 mg/L AXF0233Total Alkalinity 5.00 2.37 SM2320B1


EPA 120.14.52 AXF0223 06/26/14 06/26/14 uS/cmSpecific Conductance (EC) 5.00 Ja1.09 1

SM 4500CN E0.00168 AXG0105 07/08/14 07/11/14 mg/LCyanide 0.00500 Ja0.000900 1

ND 06/26/14 06/27/14 " AXF0236MBAS 0.100 0.0600 SM5540C1



ND 07/14/14 07/14/14 " AXG0141Total Hardness 5.00 2.86 SM2340B1


ND 07/08/14 07/09/14 ug/l AXG0074Aluminum 50.0 24.5 EPA 200.71

ND " "" "Antimony 10.0 1.3 "1

"1.0 " " ""Arsenic 10.0 Ja1.0 1

ND " "" "Barium 5.0 1.2 "1

ND " "" "Beryllium 5.0 0.09 "1

ND " "" "Boron 50.0 0.8 "1

"0.1 " " ""Cadmium 5.0 Ja0.1 1

ND " "" "Calcium 100 79.0 "1

"0.3 " " ""Chromium 5.0 Ja0.3 1

"1.1 " " ""Copper 5.0 Ja0.8 1




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-06 (Water)

CAY140625-4


MDL DF


ND 07/08/14 07/09/14 ug/l AXG0074Iron 20.0 11.5 "1

ND " "" "Lead 5.0 0.9 "1

ND " "" "Magnesium 50.0 15.6 "1

"6.5 " " ""Manganese 10.0 Ja0.6 1

ND " "" "Nickel 5.0 0.6 "1

ND " "" "Selenium 20.0 1.3 "1

ND " "" "Silver 5.0 0.4 "1

ND " "" "Sodium 200 120 "1

"2.5 " " ""Thallium 20.0 Ja2.2 1

ND " "" "Titanium 50.0 1.2 "1

"0.6 " " ""Zinc 10.0 Ja0.3 1

Dissolved Metals



ND " "" "Dissolved Iron 20.0 11.5 "1


1613B

ND 07/13/14 07/15/14 pg/l 00012151,2,3,7,8-PeCDF 50 2.38 1613B0

ND " "" "1,2,3,4,7,8-HxCDF 50 3.27 "0

ND " "" "1,2,3,6,7,8-HxCDD 50 5.18 "0

ND " "" "1,2,3,6,7,8-HxCDF 50 3.42 "0

ND " "" "1,2,3,7,8,9-HxCDD 50 4.46 "0

ND " "" "1,2,3,4,6,7,8-HpCDD 50 7.98 "0

"13.3 " " ""OCDD 100 J4.32 0

ND " "" "Total HpCDD 50 7.98 "0

ND " "" "1,2,3,7,8,9-HxCDF 50 7.73 "0

ND " "" "2,3,7,8-TCDD 10 1.51 "0

ND " "" "2,3,7,8-TCDF 10 1.92 "0

ND " "" "1,2,3,4,7,8-HxCDD 50 3.70 "0

ND " "" "1,2,3,4,6,7,8-HpCDF 50 2.07 "0

ND " "" "Total TCDF 10 1.92 "0

ND " "" "1,2,3,4,7,8,9-HpCDF 50 2.63 "0

ND " "" "1,2,3,7,8-PeCDD 50 3.29 "0




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

1406186-06 (Water)

CAY140625-4


MDL DF

1613B

ND 07/13/14 07/15/14 pg/l 00012152,3,4,6,7,8-HxCDF 50 4.44 "0

ND " "" "Total HxCDD 50 4.41 "0

ND " "" "Total HxCDF 50 4.38 "0

ND " "" "Total PeCDD 50 3.29 "0

ND " "" "Total PeCDF 50 2.32 "0

ND " "" "Total TCDD 10 1.51 "0

ND " "" "OCDF 100 4.80 "0

"0.00399 " " ""TEQ 0

ND " "" "2,3,4,7,8-PeCDF 50 2.26 "0

ND " "" "Total HpCDF 50 2.32 "0





Surrogate: 37CL-2,3,7,8-TCDD "35-19797.2 % % Recovery Limits















Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

Result LimitReporting

Units LevelSpike

ResultSource

%REC%RECLimits RPD

RPDLimit Notes Analyte

Volatile Organic Compounds by GC/MS - Quality Control

MDL

Batch AXG0011 - EPA 8260B

Blank (AXG0011-BLK1) Prepared & Analyzed: 06/28/14

Surrogate: Dibromofluoromethane ug/l 12.5 70-13010012.5

Surrogate: Toluene-d8 " 12.5 70-13010613.3

Surrogate: 4-Bromofluorobenzene " 12.5 70-13099.512.4

TBA "ND 1.0 0.1

Methyl tert-Butyl Ether "ND 0.5 0.05

Di-isopropyl ether "ND 0.5 0.1

Ethyl tert-Butyl Ether "ND 0.5 0.04

Tert-Amyl Methyl Ether "ND 0.5 0.03

Dichlorodifluoromethane "ND 0.5 0.07

Chloromethane "ND 0.5 0.06

Vinyl chloride "ND 0.5 0.06

Bromomethane "ND 0.5 0.05

Chloroethane "ND 0.5 0.08

Trichlorofluoromethane "ND 0.5 0.05

Trichlorotrifluoroethane "ND 1.0 0.05

Acetone "0.1 5.0 Ja0.1

1,1-Dichloroethene "ND 0.5 0.05

Iodomethane "ND 0.5 0.03

Methylene chloride "ND 5.0 0.08

Carbon disulfide "ND 0.5 0.06

trans-1,2-Dichloroethene "ND 0.5 0.04

1,1-Dichloroethane "ND 0.5 0.04

2-Butanone "ND 5.0 0.1

2,2-Dichloropropane "ND 0.5 0.06

cis-1,2-Dichloroethene "ND 0.5 0.03

Bromochloromethane "ND 0.5 0.07

Chloroform "0.4 0.5 Ja0.05

1,1,1-Trichloroethane "ND 0.5 0.05

Carbon tetrachloride "ND 0.5 0.02

1,1-Dichloropropene "ND 0.5 0.03

Benzene "ND 0.5 0.03


Dibromomethane "ND 0.5 0.07

Trichloroethene "ND 0.5 0.06

Bromodichloromethane "ND 0.5 0.05


cis-1,3-Dichloropropene "ND 0.5 0.04

4-Methyl-2-pentanone "ND 5.0 0.05

Toluene "ND 0.5 0.04




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:


Units LevelSpike

ResultSource

%REC%RECLimits RPD



MDL



trans-1,3-Dichloropropene ug/lND 0.5 0.04


Tetrachloroethene "ND 0.5 0.08


2-Hexanone "ND 5.0 0.1

Dibromochloromethane "ND 0.5 0.07

1,2-Dibromoethane (EDB) "ND 0.5 0.1

Chlorobenzene "ND 0.5 0.03

1,1,1,2-Tetrachloroethane "ND 0.5 0.08

Ethylbenzene "ND 0.5 0.03

m,p-Xylene "ND 1.0 0.09

o-Xylene "0.05 0.5 Ja0.04

Xylenes, total "ND 1.0 0.1

Bromoform "ND 0.5 0.03

Isopropylbenzene "ND 0.5 0.04

Bromobenzene "ND 0.5 0.05


1,2,3-Trichloropropane "ND 0.5 0.06

n-Propylbenzene "ND 0.5 0.04

2-Chlorotoluene "0.06 0.5 Ja0.03

4-Chlorotoluene "ND 0.5 0.05

tert-Butylbenzene "0.03 0.5 Ja0.02

1,2,4-Trimethylbenzene "ND 0.5 0.04

sec-Butylbenzene "0.05 0.5 Ja0.03

1,3-Dichlorobenzene "ND 0.5 0.03

4-Isopropyltoluene "0.05 0.5 Ja0.04



n-Butylbenzene "0.06 0.5 Ja0.04

1,2-Dibromo-3-chloropropane "ND 0.5 0.07

1,2,4-Trichlorobenzene "0.1 0.5 Ja0.02

Hexachlorobutadiene "ND 0.5 0.07

Naphthalene "0.08 0.5 Ja0.04





Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:


Units LevelSpike

ResultSource

%REC%RECLimits RPD



MDL


LCS (AXG0011-BS1) Prepared & Analyzed: 06/28/14


Surrogate: Toluene-d8 " 12.5 70-13010713.4


1,1-Dichloroethene "22.9 0.5 20.0 80-1201150.05

Benzene "24.4 0.5 20.0 Z-01b80-1201220.03

Trichloroethene "24.8 0.5 20.0 Z-01b80-1201240.06

Toluene "23.8 0.5 20.0 80-1201190.04

Chlorobenzene "21.6 0.5 20.0 80-1201080.03

LCS Dup (AXG0011-BSD1) Prepared & Analyzed: 06/28/14


Surrogate: Toluene-d8 " 12.5 70-13099.412.4


1,1-Dichloroethene "21.4 0.5 20.0 1580-120107 6.680.05

Benzene "24.7 0.5 20.0 15 Z-01b80-120124 1.180.03

Trichloroethene "19.5 0.5 20.0 15 Z-01b80-12097.7 23.90.06

Toluene "18.4 0.5 20.0 15 QR-0280-12092.0 25.50.04

Chlorobenzene "18.6 0.5 20.0 1580-12093.2 15.00.03

Batch AXH0123 - EPA 524

Blank (AXH0123-BLK1) Prepared: 07/28/14 Analyzed: 08/04/14




TBA "ND 1.0 0.1

Methyl tert-Butyl Ether "ND 0.5 0.05

Di-isopropyl ether "ND 0.5 0.1

Ethyl tert-Butyl Ether "ND 0.5 0.04

Tert-Amyl Methyl Ether "ND 0.5 0.03

Dichlorodifluoromethane "ND 0.5 0.07

Vinyl chloride "ND 0.5 0.06

Chloromethane "ND 0.5 0.06

Bromomethane "ND 0.5 0.05

Chloroethane "ND 0.5 0.08

1,1-Dichloroethene "ND 0.5 0.05

Total Trihalomethanes "ND 0.5 0.5

Trichlorofluoromethane "ND 0.5 0.05

Trichlorotrifluoroethane "ND 1.0 0.05




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:


Units LevelSpike

ResultSource

%REC%RECLimits RPD



MDL



Methylene chloride ug/l0.5 1.0 Ja0.08

Acetone "ND 5.0 0.1

Iodomethane "ND 0.5 0.03

Carbon disulfide "ND 0.5 0.06

trans-1,2-Dichloroethene "ND 0.5 0.04

cis-1,2-Dichloroethene "ND 0.5 0.03


2-Butanone "ND 5.0 0.1



Bromochloromethane "ND 0.5 0.07

Carbon tetrachloride "ND 0.5 0.02

Chloroform "ND 0.5 Z-030.05

Benzene "ND 0.5 0.03


Trichloroethene "ND 0.5 0.06

1,1-Dichloropropene "ND 0.5 0.03


Dibromomethane "ND 0.5 0.07

Bromodichloromethane "ND 0.5 0.05

Toluene "ND 0.5 0.04

cis-1,3-Dichloropropene "ND 0.5 0.04

4-Methyl-2-pentanone "0.06 5.0 Ja0.05


trans-1,3-Dichloropropene "ND 0.5 0.04

Tetrachloroethene "ND 0.5 0.08


Chlorobenzene "ND 0.5 0.03

2-Hexanone "ND 5.0 0.1

Dibromochloromethane "ND 0.5 0.07

Ethylbenzene "ND 0.5 0.03

1,2-Dibromoethane (EDB) "ND 0.5 0.1

m,p-Xylene "ND 0.5 0.09


o-Xylene "ND 0.5 0.04

Styrene "ND 0.5 0.09

Bromoform "ND 0.5 0.03

Isopropylbenzene "ND 0.5 0.04

Bromobenzene "ND 0.5 0.05




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:


Units LevelSpike

ResultSource

%REC%RECLimits RPD



MDL



1,1,2,2-Tetrachloroethane ug/lND 0.5 0.04

1,2,3-Trichloropropane "ND 0.5 0.06

n-Propylbenzene "ND 0.5 0.04






1,2,4-Trichlorobenzene "ND 0.5 0.02

tert-Butylbenzene "ND 0.5 0.02


sec-Butylbenzene "ND 0.5 0.03


4-Isopropyltoluene "ND 0.5 0.04

n-Butylbenzene "ND 0.5 0.04

1,2-Dibromo-3-chloropropane "ND 0.5 0.07

Hexachlorobutadiene "0.1 0.5 Ja0.07

Naphthalene "0.05 0.5 Ja0.04


Xylenes, total "ND 1.0 0.1

LCS (AXH0123-BS1) Prepared: 07/28/14 Analyzed: 08/04/14




1,1-Dichloroethene "21.7 0.5 20.0 80-1201080.05

Benzene "20.9 0.5 20.0 80-1201040.03

Trichloroethene "18.7 0.5 20.0 80-12093.60.06

Toluene "18.6 0.5 20.0 80-12093.10.04

Chlorobenzene "19.0 0.5 20.0 80-12095.00.03




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:


Units LevelSpike

ResultSource

%REC%RECLimits RPD



MDL


LCS Dup (AXH0123-BSD1) Prepared: 07/28/14 Analyzed: 08/04/14




1,1-Dichloroethene "21.9 0.5 20.0 1580-120110 1.050.05

Benzene "20.6 0.5 20.0 1580-120103 1.500.03

Trichloroethene "17.9 0.5 20.0 1580-12089.5 4.480.06

Toluene "18.0 0.5 20.0 1580-12090.2 3.110.04

Chlorobenzene "18.4 0.5 20.0 1580-12091.9 3.370.03




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:


Units LevelSpike

ResultSource

%REC%RECLimits RPD


Pesticides by GC/ECD - Quality Control

MDL

Batch AXG0027 - EPA 8081A

Blank (AXG0027-BLK1) Prepared: 07/02/14 Analyzed: 07/07/14

Surrogate: Decachlorobiphenyl ug/l 0.400 50-1501120.448

Surrogate: Tetrachloro-meta-xylene " 0.400 50-1501130.452

alpha-BHC "ND 0.100 0.011

beta-BHC "ND 0.100 0.011

gamma-BHC (Lindane) "ND 0.100 0.013

delta-BHC "ND 0.100 0.021

Heptachlor "ND 0.100 0.016

Aldrin "ND 0.100 0.011

Heptachlor epoxide "ND 0.100 0.020

gamma-Chlordane "ND 0.100 0.005

Endosulfan I "ND 0.100 0.007

alpha-Chlordane "ND 0.100 0.006

4,4'-DDE "ND 0.100 0.005

Dieldrin "ND 0.100 0.006

Endrin "ND 0.100 0.007

Endosulfan II "ND 0.100 0.021

4,4'-DDD "ND 0.100 0.006

Endrin aldehyde "ND 0.100 0.006

Endosulfan sulfate "0.008 0.100 Ja0.005

4,4'-DDT "ND 0.100 0.004

Endrin Ketone "ND 0.100 0.005

Methoxychlor "ND 0.100 0.013

Toxaphene "ND 1.00 0.018

LCS (AXG0027-BS1) Prepared: 07/02/14 Analyzed: 07/07/14

Surrogate: Decachlorobiphenyl ug/l 0.600 50-15076.30.458


gamma-BHC (Lindane) "0.573 0.100 0.600 50-15095.40.013

Heptachlor "0.518 0.100 0.600 50-15086.40.016

Aldrin "0.586 0.100 0.600 50-15097.60.011

Dieldrin "0.530 0.100 0.600 50-15088.40.006

Endrin "0.550 0.100 0.600 50-15091.60.007

4,4'-DDT "0.535 0.100 0.600 50-15089.20.004




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:


Units LevelSpike

ResultSource

%REC%RECLimits RPD


Pesticides by GC/ECD - Quality Control

MDL


LCS Dup (AXG0027-BSD1) Prepared: 07/02/14 Analyzed: 07/07/14



gamma-BHC (Lindane) "0.557 0.100 0.600 2550-15092.9 2.670.013

Heptachlor "0.504 0.100 0.600 2550-15083.9 2.870.016

Aldrin "0.588 0.100 0.600 2550-15098.0 0.4090.011

Dieldrin "0.524 0.100 0.600 2550-15087.3 1.190.006

Endrin "0.540 0.100 0.600 2550-15090.0 1.780.007

4,4'-DDT "0.530 0.100 0.600 2550-15088.3 1.020.004




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:


Units LevelSpike

ResultSource

%REC%RECLimits RPD


PCBs by GC/ECD - Quality Control

MDL

Batch AXG0027 - EPA 8082


Surrogate: Decachlorobiphenyl ug/l 0.400 50-1501060.425


Aroclor 1016 "ND 1.00 0.0600

PCBs "ND 1.00 0.0800

Aroclor 1221 "ND 1.00 0.130

Aroclor 1232 "ND 1.00 0.100

Aroclor 1242 "ND 1.00 0.0600

Aroclor 1248 "ND 1.00 0.0600

Aroclor 1254 "ND 1.00 0.0900

Aroclor 1260 "ND 1.00 0.0800




Aroclor 1260 "22.6 1.00 50-1500.0800




Aroclor 1260 "22.7 1.00 5050-150 0.6910.0800




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:


Units LevelSpike

ResultSource

%REC%RECLimits RPD


SemiVolatile Organic Compounds by GC/MS - Quality Control

MDL

Batch AXG0033 - EPA 8270C


Surrogate: 2-Fluorophenol ug/l 50.0 10-13021.010.5

Surrogate: Phenol-d6 " 50.0 10-13021.010.5

Surrogate: Nitrobenzene-d5 " 50.0 10-13053.226.6

Surrogate: 2-Fluorobiphenyl " 50.0 10-13051.025.5

Surrogate: 2,4,6-Tribromophenol " 50.0 10-13049.925.0

Surrogate: Terphenyl-dl4 " 50.0 10-13010050.0

N-Nitrosodimethylamine "ND 2.0 0.4

Aniline "ND 2.0 0.3

Bis(2-chloroethyl)ether "ND 2.0 0.6

Phenol "ND 2.0 0.3

2-Chlorophenol "ND 2.0 0.8


Benzyl alcohol "ND 2.0 0.4

Bis(2-chloroisopropyl)ether "ND 2.0 0.4

2-Methylphenol "ND 2.0 0.4

Hexachloroethane "ND 2.0 0.5

N-Nitrosodi-n-propylamine "ND 2.0 0.3

Nitrobenzene "ND 2.0 0.7

Isophorone "ND 2.0 0.3

2-Nitrophenol "ND 5.0 1.2

2,4-Dimethylphenol "ND 2.0 0.8

Bis(2-chloroethoxy)methane "ND 2.0 0.4

Benzoic acid "ND 30.0 0.5

2,4-Dichlorophenol "ND 2.0 0.8

1,2,4-Trichlorobenzene "ND 2.0 0.6

Naphthalene "ND 2.0 0.5

4-Chloroaniline "ND 2.0 0.5

Hexachlorobutadiene "ND 2.0 0.6

4-Chloro-3-methylphenol "ND 2.0 0.6

2-Methylnaphthalene "ND 2.0 0.6

Hexachlorocyclopentadiene "ND 2.0 0.6

2,4,6-Trichlorophenol "ND 5.0 1.6

2,4,5-Trichlorophenol "ND 5.0 1.6

2-Chloronaphthalene "ND 2.0 0.2

2-Nitroaniline "ND 2.0 0.4

Acenaphthylene "ND 2.0 0.3

Dimethyl phthalate "ND 2.0 0.8

2,6-Dinitrotoluene "ND 2.0 0.8

Acenaphthene "ND 2.0 0.6




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:


Units LevelSpike

ResultSource

%REC%RECLimits RPD



MDL



3-Nitroaniline ug/lND 2.0 0.5

2,4-Dinitrophenol "ND 10.0 0.3

Dibenzofuran "ND 2.0 0.3

2,4-Dinitrotoluene "ND 2.0 0.8


Fluorene "ND 2.0 0.5

4-Chlorophenyl phenyl ether "ND 2.0 0.5

Diethyl phthalate "ND 2.0 0.6

4-Nitroaniline "ND 2.0 0.6

Azobenzene "ND 2.0 0.4

4,6-Dinitro-2-methylphenol "ND 10.0 2.2

N-Nitrosodiphenylamine "ND 2.0 0.6

4-Bromophenyl phenyl ether "ND 2.0 0.8

Hexachlorobenzene "ND 2.0 0.6

Pentachlorophenol "ND 10.0 2.4

Phenanthrene "ND 2.0 0.4

Anthracene "ND 2.0 0.3

Carbazole "ND 2.0 0.6

Di-n-butyl phthalate "ND 2.0 0.4

Fluoranthene "ND 2.0 0.6

Benzidine "ND 5.0 0.2

Pyrene "ND 2.0 1.0

Butyl benzyl phthalate "ND 2.0 1.0

3,3´-Dichlorobenzidine "ND 5.0 0.8

Benzo (a) anthracene "ND 2.0 0.4

Chrysene "ND 2.0 0.5

Bis(2-ethylhexyl)phthalate "ND 5.0 0.7

Di-n-octyl phthalate "ND 5.0 0.7

Benzo (b) fluoranthene "ND 2.0 0.8

Benzo (k) fluoranthene "ND 2.0 1.0

Benzo (a) pyrene "ND 5.0 1.2

Indeno (1,2,3-cd) pyrene "ND 5.0 1.6

Dibenz (a,h) anthracene "ND 2.0 1.6

Benzo (g,h,i) perylene "ND 2.0 1.3




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:


Units LevelSpike

ResultSource

%REC%RECLimits RPD



MDL








Surrogate: Terphenyl-dl4 " 50.0 0-15089.244.6

Phenol "13.6 2.0 50.0 0-15027.30.3

2-Chlorophenol "24.8 2.0 50.0 0-15049.60.8

1,4-Dichlorobenzene "29.4 2.0 50.0 0-15058.80.4

N-Nitrosodi-n-propylamine "38.2 2.0 50.0 0-15076.40.3

1,2,4-Trichlorobenzene "32.3 2.0 50.0 0-15064.70.6

4-Chloro-3-methylphenol "35.6 2.0 50.0 0-15071.20.6

Acenaphthene "30.9 2.0 50.0 0-15061.70.6

2,4-Dinitrotoluene "35.0 2.0 50.0 0-15070.00.8

4-Nitrophenol "13.4 5.0 50.0 0-15026.80.1

Pentachlorophenol "35.5 10.0 50.0 0-15071.12.4

Pyrene "42.2 2.0 50.0 0-15084.41.0







Surrogate: Terphenyl-dl4 " 50.0 0-15087.543.8

Phenol "9.6 2.0 50.0 30 QR-020-15019.2 34.70.3

2-Chlorophenol "12.7 2.0 50.0 30 QR-020-15025.4 64.70.8

1,4-Dichlorobenzene "26.8 2.0 50.0 300-15053.6 9.360.4

N-Nitrosodi-n-propylamine "35.3 2.0 50.0 300-15070.7 7.800.3

1,2,4-Trichlorobenzene "30.2 2.0 50.0 300-15060.4 6.780.6

4-Chloro-3-methylphenol "27.4 2.0 50.0 300-15054.9 25.90.6

Acenaphthene "28.0 2.0 50.0 300-15055.9 9.860.6

2,4-Dinitrotoluene "31.1 2.0 50.0 300-15062.2 11.90.8

4-Nitrophenol "6.2 5.0 50.0 50 QR-020-15012.4 73.80.1

Pentachlorophenol "12.3 10.0 50.0 50 QR-020-15024.7 96.92.4

Pyrene "42.0 2.0 50.0 300-15084.0 0.4991.0




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:


Units LevelSpike

ResultSource

%REC%RECLimits RPD


Organophosphorus Pesticides - Quality Control

MDL



Surrogate: Tributylphosphate ug/l 0.400 50-17070.60.282

Surrogate: Triphenyl phosphate " 0.400 50-17080.50.322

Dichlorvos "ND 0.200 0.156

Mevinphos "ND 0.200 0.115

TEPP "ND 0.200 0.151

Demeton "ND 0.200 0.105

Demeton-O "ND 0.200 0.101

Ethoprop "ND 0.200 0.0770

Naled "ND 0.200 0.169

Sulfotep "ND 0.200 0.0950

Monocrotophos "ND 0.200 0.0150

Phorate "ND 0.200 0.0830

Demeton-S "ND 0.200 0.105

Dimethoate "ND 0.200 0.0710

Diazinon "ND 0.250 0.0650

Disulfoton "ND 0.200 0.0690

Parathion-methyl "ND 0.200 0.0770

Ronnel "ND 0.200 0.0660

Malathion "ND 0.200 0.159

Dursban (Chlorpyrifos) "ND 0.200 0.0710

Fenthion "ND 0.200 0.0670

Parathion "ND 0.200 0.0790

Trichloronate "ND 0.200 0.0670

Gardona (Stirophos) "ND 0.200 0.110

Tokuthion (Prothiofos) "ND 0.200 0.0770

Merphos "ND 0.200 0.0970

Fensulfothion "ND 0.200 0.139

Bolstar "ND 0.200 0.0860

EPN "ND 0.200 0.124

Azinphos-methyl "ND 0.200 0.0270

Coumaphos "ND 0.200 0.168

Molinate "ND 0.200 0.0440




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:


Units LevelSpike

ResultSource

%REC%RECLimits RPD


Organophosphorus Pesticides - Quality Control

MDL





Phorate "0.311 0.200 0.400 40-13077.80.0830

Diazinon "0.318 0.250 0.400 40-13079.40.0650

Dursban (Chlorpyrifos) "0.331 0.200 0.400 40-13082.80.0710

Trichloronate "0.322 0.200 0.400 40-13080.50.0670




Phorate "0.268 0.200 0.400 3040-13067.1 14.80.0830

Diazinon "0.318 0.250 0.400 3040-13079.5 0.04070.0650

Dursban (Chlorpyrifos) "0.325 0.200 0.400 3040-13081.2 1.870.0710

Trichloronate "0.324 0.200 0.400 3040-13080.9 0.4650.0670




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:


Units LevelSpike

ResultSource

%REC%RECLimits RPD


Herbicides - Quality Control

MDL



Surrogate: 2,4-Dichlorophenylacetic acid ug/l 3.20 43-16963.02.02

Dalapon "ND 0.600 0.115

3,5-Dichlorobenzoic acid "ND 0.800 0.170


Dicamba "ND 0.400 0.0800

MCPP "ND 10.0 0.891

Dichloroprop "0.249 0.800 Ja0.196

2,4-D "ND 0.400 0.0860

Pentachlorophenol "ND 0.300 0.0530

2,4,5-TP (Silvex) "ND 0.500 0.0950

2,4,5-T "ND 0.500 0.0970

Chloramben "ND 0.800 0.00800

Dinoseb "ND 0.400 0.0830

2,4-DB "ND 0.800 0.157

Bentazon "ND 0.600 0.110

DCPA "ND 0.400 0.0150

Picloram "ND 0.800 0.0200

Acifluorfen "ND 0.800 0.157



Dichloroprop "1.08 0.800 2.00 50-15054.10.196

2,4-D "1.16 0.400 2.00 50-15058.00.0860

2,4,5-TP (Silvex) "1.11 0.500 2.00 50-15055.50.0950

2,4,5-T "1.35 0.500 2.00 50-15067.40.0970

Dinoseb "1.42 0.400 2.00 50-15071.00.0830



Dichloroprop "1.37 0.800 2.00 3050-15068.5 23.60.196

2,4-D "1.38 0.400 2.00 3050-15069.1 17.50.0860

2,4,5-TP (Silvex) "1.13 0.500 2.00 3050-15056.6 1.890.0950

2,4,5-T "1.89 0.500 2.00 30 QR-0250-15094.5 33.40.0970

Dinoseb "2.37 0.400 2.00 30 QR-0250-150119 50.30.0830




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:


Units LevelSpike

ResultSource

%REC%RECLimits RPD


Ion Chromatography - Quality Control

MDL

Batch AXG0049 - EPA 314.0


Perchlorate ug/lND 2.00 0.0940


Perchlorate ug/l20.8 2.00 20.0 85-1151040.0940


Perchlorate ug/l22.7 2.00 20.0 2085-115113 8.490.0940

Duplicate (AXG0049-DUP1) Prepared: 07/01/14 Analyzed: 07/03/14 Source: 1406123-02

Perchlorate ug/lND 2.00 ND 150.0940

Matrix Spike (AXG0049-MS1) Prepared: 07/01/14 Analyzed: 07/03/14 Source: 1406123-02

Perchlorate ug/l10.5 2.00 10.0 ND 80-1201050.0940

Matrix Spike Dup (AXG0049-MSD1) Prepared: 07/01/14 Analyzed: 07/03/14 Source: 1406123-02

Perchlorate ug/l9.92 2.00 10.0 ND 2080-12099.2 6.080.0940



Fluoride mg/LND 0.1 0.02

Chloride "0.1 0.5 Ja0.04

Nitrite as Nitrogen "ND 0.15 0.03

Nitrate as Nitrogen "ND 0.11 0.009

Sulfate as SO4 "ND 0.5 0.07


Fluoride mg/L10.3 0.1 10.0 90-1101030.02

Chloride "10.2 0.5 10.0 90-1101020.04

Nitrite as Nitrogen "3.26 0.15 3.05 90-1101070.03

Nitrate as Nitrogen "2.36 0.11 2.26 90-1101040.009

Sulfate as SO4 "10.3 0.5 10.0 80-1201030.07




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:


Units LevelSpike

ResultSource

%REC%RECLimits RPD



MDL



Fluoride mg/L10.3 0.1 10.0 2090-110103 0.1260.02

Chloride "10.2 0.5 10.0 2090-110102 0.03920.04

Nitrite as Nitrogen "3.28 0.15 3.05 2090-110108 0.7070.03

Nitrate as Nitrogen "2.35 0.11 2.26 2090-110104 0.1250.009

Sulfate as SO4 "10.3 0.5 10.0 2080-120103 0.1160.07

Duplicate (AXG0062-DUP1) Prepared: 06/26/14 Analyzed: 06/27/14 Source: 1406186-06

Fluoride mg/LND 0.1 ND 200.02

Chloride "0.1 0.5 0.1 20 Ja0.7600.04

Nitrite as Nitrogen "ND 0.15 ND 200.03

Nitrate as Nitrogen "ND 0.11 ND 200.009

Sulfate as SO4 "ND 0.5 ND 200.07

Matrix Spike (AXG0062-MS1) Prepared & Analyzed: 06/26/14 Source: 1406186-03

Fluoride mg/L9.7 0.1 10.0 0.08 75-12596.30.02

Chloride "12.7 0.5 10.0 3.1 75-12596.40.04

Nitrite as Nitrogen "3.31 0.15 3.05 ND 75-1251080.03

Nitrate as Nitrogen "2.25 0.11 2.26 0.02 75-12598.40.009

Sulfate as SO4 "13.6 0.5 10.0 3.8 75-12597.90.07

Matrix Spike Dup (AXG0062-MSD1) Prepared & Analyzed: 06/26/14 Source: 1406186-03

Fluoride mg/L9.7 0.1 10.0 0.08 2075-12596.3 0.02060.02

Chloride "12.7 0.5 10.0 3.1 2075-12596.5 0.03140.04

Nitrate as Nitrogen "2.24 0.11 2.26 0.02 2075-12598.1 0.2620.009

Nitrite as Nitrogen "3.31 0.15 3.05 ND 2075-125108 0.07350.03

Sulfate as SO4 "13.6 0.5 10.0 3.8 2075-12598.0 0.08850.07




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:


Units LevelSpike

ResultSource

%REC%RECLimits RPD



MDL



Hexavalent Chromium ug/lND 1.0 0.1


Hexavalent Chromium ug/l10.5 1.0 10.0 80-1201050.1


Hexavalent Chromium ug/l10.6 1.0 10.0 2080-120106 0.9750.1

Duplicate (AXG0064-DUP1) Prepared & Analyzed: 06/27/14 Source: 1406186-03

Hexavalent Chromium ug/l0.4 1.0 0.4 200 Ja6.270.1


Hexavalent Chromium ug/l11.1 1.0 10.0 0.4 75-1251070.1


Hexavalent Chromium ug/l11.2 1.0 10.0 0.4 2075-125107 0.4940.1




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:


Units LevelSpike

ResultSource

%REC%RECLimits RPD


Wet Chemistry - Quality Control

MDL

Batch AXF0223 - EPA 120.1

Duplicate (AXF0223-DUP1) Prepared & Analyzed: 06/26/14 Source: 1406186-01

Specific Conductance (EC) uS/cm656 5.00 655 200.1531.09

Batch AXF0224 - SM 4500-H+ B


pH pH Units8.04 0.100 8.05 20 Field0.02490.100

Batch AXF0233 - SM2320B

Blank (AXF0233-BLK1) Prepared & Analyzed: 06/27/14

Total Alkalinity mg/LND 5.00 2.37

LCS (AXF0233-BS1) Prepared & Analyzed: 06/27/14

Total Alkalinity mg/L100 5.00 100 80-1201002.37

LCS Dup (AXF0233-BSD1) Prepared & Analyzed: 06/27/14

Total Alkalinity mg/L102 5.00 100 2080-120102 1.982.37


Total Alkalinity mg/LND 5.00 ND 202.37

Matrix Spike (AXF0233-MS1) Prepared & Analyzed: 06/27/14 Source: 1406186-06

Total Alkalinity mg/L106 5.00 100 ND 80-1201062.37

Matrix Spike Dup (AXF0233-MSD1) Prepared & Analyzed: 06/27/14 Source: 1406186-06

Total Alkalinity mg/L104 5.00 100 ND 2080-120104 1.902.37




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:


Units LevelSpike

ResultSource

%REC%RECLimits RPD



MDL

Batch AXF0236 - SM5540C

Blank (AXF0236-BLK1) Prepared & Analyzed: 06/27/14

MBAS mg/LND 0.100 0.0600

LCS (AXF0236-BS1) Prepared & Analyzed: 06/27/14

MBAS mg/L0.455 0.100 0.500 90-11091.00.0600

LCS Dup (AXF0236-BSD1) Prepared & Analyzed: 06/27/14

MBAS mg/L0.458 0.100 0.500 1590-11091.6 0.6570.0600

Batch AXG0054 - SM 2540C


Total Dissolved Solids mg/LND 15.0 7.68


Total Dissolved Solids mg/L24.0 15.0 24.0 200.007.68

Batch AXG0105 - SM 4500CN E


Cyanide mg/LND 0.00500 0.000900


Cyanide mg/L0.0970 0.00500 0.100 70-13097.00.000900


Cyanide mg/L0.0965 0.00500 0.100 3070-13096.5 0.5170.000900




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:


Units LevelSpike

ResultSource

%REC%RECLimits RPD



MDL

Batch AXG0105 - SM 4500CN E


Cyanide mg/L0.102 0.00500 0.100 ND 70-1301020.000900


Cyanide mg/L0.108 0.00500 0.100 ND 3070-130108 6.670.000900

Batch AXG0121 - SM 4500-NH3 B/H


Ammonia as N mg/LND 0.100 0.0400


Ammonia as N mg/L2.15 0.100 2.00 85-1151070.0400


Ammonia as N mg/L2.11 0.100 2.00 2085-115106 1.540.0400


Ammonia as N mg/L2.40 0.100 2.00 0.310 75-1251040.0400


Ammonia as N mg/L2.54 0.100 2.00 0.310 2075-125111 5.570.0400

Batch AXG0141 - SM2340B


Total Hardness mg/LND 5.00 2.86




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:


Units LevelSpike

ResultSource

%REC%RECLimits RPD



MDL

Batch AXG0141 - SM2340B


Total Hardness mg/L52.0 5.00 50.0 80-1201042.86


Total Hardness mg/L56.0 5.00 50.0 2080-120112 7.412.86


Total Hardness mg/L192 5.00 190 201.052.86


Total Hardness mg/L248 5.00 50.0 190 75-1251162.86


Total Hardness mg/L238 5.00 50.0 190 2075-12596.0 4.122.86




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:


Units LevelSpike

ResultSource

%REC%RECLimits RPD


Total Recoverable Metals - Quality Control

MDL



Aluminum ug/lND 50.0 24.5

Boron "ND 50.0 0.8

Titanium "ND 50.0 1.2

Antimony "ND 10.0 1.3

Arsenic "ND 10.0 1.0

Barium "ND 5.0 1.2

Beryllium "ND 5.0 0.09

Cadmium "ND 5.0 0.1

Calcium "ND 100 79.0

Chromium "ND 5.0 0.3

Copper "1.20 5.0 Ja0.8

Iron "ND 20.0 11.5

Lead "ND 5.0 0.9

Magnesium "ND 50.0 15.6

Manganese "2.40 10.0 Ja0.6

Nickel "ND 5.0 0.6

Selenium "ND 20.0 1.3

Silver "ND 5.0 0.4

Sodium "ND 200 120

Thallium "ND 20.0 2.2

Zinc "ND 10.0 0.3


Titanium ug/l947 50.0 1000 85-11594.71.2

Aluminum "914 50.0 1000 85-11591.424.5

Boron "961 50.0 1000 85-11596.10.8

Antimony "998 10.0 1000 85-11599.81.3

Arsenic "1040 10.0 1000 85-1151041.0

Barium "943 5.0 1000 85-11594.31.2

Beryllium "1000 5.0 1000 85-1151000.09

Cadmium "988 5.0 1000 85-11598.80.1

Calcium "990 100 1000 85-11599.079.0

Chromium "958 5.0 1000 85-11595.80.3

Copper "981 5.0 1000 85-11598.10.8

Iron "1010 20.0 1000 85-11510111.5

Lead "987 5.0 1000 85-11598.70.9

Magnesium "933 50.0 1000 85-11593.315.6

Manganese "974 10.0 1000 85-11597.40.6

Nickel "1050 5.0 1000 85-1151050.6




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:


Units LevelSpike

ResultSource

%REC%RECLimits RPD



MDL



Selenium ug/l1030 20.0 1000 85-1151031.3

Silver "966 5.0 1000 85-11596.60.4

Sodium "973 200 1000 85-11597.3120

Thallium "1010 20.0 1000 85-1151012.2

Zinc "948 10.0 1000 85-11594.80.3


Aluminum ug/l918 50.0 1000 2085-11591.8 0.41524.5

Boron "962 50.0 1000 2085-11596.2 0.1660.8

Antimony "1000 10.0 1000 2085-115100 0.7391.3

Titanium "954 50.0 1000 2085-11595.4 0.6521.2

Arsenic "1040 10.0 1000 2085-115104 0.6721.0

Barium "943 5.0 1000 2085-11594.3 0.02121.2

Beryllium "1010 5.0 1000 2085-115101 0.5960.09

Cadmium "995 5.0 1000 2085-11599.5 0.6660.1

Calcium "997 100 1000 2085-11599.7 0.63479.0

Chromium "964 5.0 1000 2085-11596.4 0.6450.3

Copper "977 5.0 1000 2085-11597.7 0.4190.8

Iron "1020 20.0 1000 2085-115102 1.3811.5

Lead "992 5.0 1000 2085-11599.2 0.5360.9

Magnesium "917 50.0 1000 2085-11591.7 1.7215.6

Manganese "982 10.0 1000 2085-11598.2 0.8590.6

Nickel "1060 5.0 1000 2085-115106 0.7560.6

Selenium "1030 20.0 1000 2085-115103 0.7771.3

Silver "958 5.0 1000 2085-11595.8 0.9050.4

Sodium "967 200 1000 2085-11596.7 0.660120

Thallium "1010 20.0 1000 2085-115101 0.7922.2

Zinc "953 10.0 1000 2085-11595.3 0.4520.3




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:


Units LevelSpike

ResultSource

%REC%RECLimits RPD



MDL



Boron ug/l959 50.0 1000 ND 75-12595.90.8

Titanium "957 50.0 1000 ND 75-12595.71.2

Aluminum "927 50.0 1000 ND 75-12592.724.5

Antimony "1000 10.0 1000 ND 75-1251001.3

Arsenic "1050 10.0 1000 1.00 75-1251051.0

Barium "943 5.0 1000 ND 75-12594.31.2

Beryllium "1010 5.0 1000 ND 75-1251010.09

Cadmium "996 5.0 1000 0.100 75-12599.60.1

Calcium "1010 100 1000 ND 75-12510179.0

Chromium "965 5.0 1000 0.300 75-12596.40.3

Copper "985 5.0 1000 1.10 75-12598.40.8

Iron "1020 20.0 1000 ND 75-12510211.5

Lead "994 5.0 1000 ND 75-12599.40.9

Magnesium "941 50.0 1000 ND 75-12594.115.6

Manganese "986 10.0 1000 6.50 75-12597.90.6

Nickel "1060 5.0 1000 ND 75-1251060.6

Selenium "1040 20.0 1000 ND 75-1251041.3

Silver "964 5.0 1000 ND 75-12596.40.4

Sodium "974 200 1000 ND 75-12597.4120

Thallium "1020 20.0 1000 2.50 75-1251012.2

Zinc "957 10.0 1000 0.600 75-12595.60.3


Aluminum ug/l900 50.0 1000 ND 2575-12590.0 2.9724.5

Antimony "1000 10.0 1000 ND 2575-125100 0.2991.3

Boron "957 50.0 1000 ND 2575-12595.7 0.1770.8

Titanium "958 50.0 1000 ND 2575-12595.8 0.08361.2

Arsenic "1050 10.0 1000 1.00 2575-125105 0.09551.0

Barium "941 5.0 1000 ND 2575-12594.1 0.1801.2

Beryllium "1010 5.0 1000 ND 2575-125101 0.2960.09

Cadmium "991 5.0 1000 0.100 2575-12599.1 0.4630.1

Calcium "1010 100 1000 ND 2575-125101 0.79279.0

Chromium "961 5.0 1000 0.300 2575-12596.1 0.3640.3

Copper "981 5.0 1000 1.10 2575-12598.0 0.4370.8

Iron "1020 20.0 1000 ND 2575-125102 0.098111.5

Lead "990 5.0 1000 ND 2575-12599.0 0.4030.9

Magnesium "928 50.0 1000 ND 2575-12592.8 1.3315.6

Manganese "982 10.0 1000 6.50 2575-12597.6 0.3760.6

Nickel "1060 5.0 1000 ND 2575-125106 0.2820.6




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:


Units LevelSpike

ResultSource

%REC%RECLimits RPD



MDL



Selenium ug/l1030 20.0 1000 ND 2575-125103 0.3871.3

Silver "960 5.0 1000 ND 2575-12596.0 0.4570.4

Sodium "970 200 1000 ND 2575-12597.0 0.463120

Thallium "1010 20.0 1000 2.50 2575-125101 0.1972.2

Zinc "953 10.0 1000 0.600 2575-12595.3 0.3980.3



Aluminum ug/lND 50.0 24.5

Titanium "ND 50.0 1.2

Barium "ND 5.0 1.2

Iron "ND 20.0 11.5

Manganese "ND 10.0 0.6


Aluminum ug/l944 50.0 1000 85-11594.424.5

Titanium "1040 50.0 1000 85-1151041.2

Barium "1100 5.0 1000 85-1151101.2

Iron "990 20.0 1000 85-11599.011.5

Manganese "981 10.0 1000 85-11598.10.6


Titanium ug/l1040 50.0 1000 2085-115104 0.2891.2

Aluminum "960 50.0 1000 2085-11596.0 1.6924.5

Barium "1100 5.0 1000 2085-115110 0.6371.2

Iron "990 20.0 1000 2085-11599.0 0.010111.5

Manganese "982 10.0 1000 2085-11598.2 0.05090.6




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:


Units LevelSpike

ResultSource

%REC%RECLimits RPD



MDL



Aluminum ug/l2160 50.0 1000 1070 75-12510924.5

Titanium "1110 50.0 1000 61.6 75-1251051.2

Barium "1160 5.0 1000 62.1 75-1251091.2

Iron "2060 20.0 1000 1030 75-12510311.5

Manganese "1100 10.0 1000 123 75-12597.90.6


Aluminum ug/l2200 100 1000 1070 2575-125113 1.8849.0

Titanium "1120 100 1000 61.6 2575-125106 1.082.3

Barium "1180 10.0 1000 62.1 2575-125112 1.972.4

Iron "2100 40.0 1000 1030 2575-125107 1.9222.9

Manganese "1140 20.0 1000 123 2575-125101 3.041.2




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:


Units LevelSpike

ResultSource

%REC%RECLimits RPD


Dissolved Metals - Quality Control

MDL



Dissolved Aluminum ug/l44.4 50.0 Ja24.5

Dissolved Lead "ND 5.0 0.9

Dissolved Arsenic "ND 10.0 1.0

Dissolved Iron "ND 20.0 11.5


Dissolved Aluminum ug/l904 50.0 1000 85-11590.424.5

Dissolved Lead "998 5.0 1000 85-11599.80.9

Dissolved Arsenic "1060 10.0 1000 85-1151061.0

Dissolved Iron "1020 20.0 1000 85-11510211.5


Dissolved Aluminum ug/l932 50.0 1000 2085-11593.2 3.1624.5

Dissolved Arsenic "1060 10.0 1000 2085-115106 0.8491.0

Dissolved Lead "1010 5.0 1000 2085-115101 0.9480.9

Dissolved Iron "1030 20.0 1000 2085-115103 0.97611.5


Dissolved Aluminum ug/l918 50.0 1000 ND 75-12591.824.5

Dissolved Lead "1010 5.0 1000 ND 75-1251010.9

Dissolved Arsenic "1060 10.0 1000 1.10 75-1251061.0

Dissolved Iron "1110 20.0 1000 ND 75-12511111.5


Dissolved Aluminum ug/l953 50.0 1000 ND 2575-12595.3 3.7424.5

Dissolved Lead "1070 5.0 1000 ND 2575-125107 6.170.9

Dissolved Arsenic "1060 10.0 1000 1.10 2575-125106 0.4711.0

Dissolved Iron "1120 20.0 1000 ND 2575-125112 1.3511.5




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:


Units LevelSpike

ResultSource

%REC%RECLimits RPD


Dissolved Metals - Quality Control

MDL



Dissolved Iron ug/lND 20.0 11.5


Dissolved Iron ug/l1030 20.0 1000 85-11510311.5


Dissolved Iron ug/l1020 20.0 1000 2085-115102 0.39111.5


Dissolved Iron ug/l1030 20.0 1000 21.9 75-12510111.5


Dissolved Iron ug/l1020 20.0 1000 21.9 2575-125100 0.77811.5




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:


Units LevelSpike

ResultSource

%REC%RECLimits RPD


1613B - Quality Control

MDL

Batch 0001215 - 1613B

Blank (0001215-Blank) Prepared: 07/13/14 Analyzed: 07/15/14

Surrogate: 13C-1,2,3,6,7,8-HxCDF % 100 26-123105105

Surrogate: 13C-1,2,3,7,8-PeCDF " 100 24-185111111

Surrogate: 13C-2,3,4,6,7,8-HxCDF " 100 28-136103103

Surrogate: 13C-1,2,3,7,8,9-HxCDF " 100 29-14794.594.5

Surrogate: 13C-1,2,3,6,7,8-HxCDD " 100 28-13093.093.0

Surrogate: 13C-1,2,3,4,7,8-HxCDD " 100 32-14197.797.7

Surrogate: 13C-1,2,3,4,7,8,9-HpCDF " 100 26-138106106

Surrogate: 13C-1,2,3,4,6,7,8-HpCDD " 100 23-14096.296.2

Surrogate: 13C-1,2,3,4,6,7,8-HpCDF " 100 28-143108108

Surrogate: 13C-1,2,3,7,8-PeCDD " 100 25-18197.297.2

Surrogate: 13C-2,3,4,7,8-PeCDF " 100 21-178114114

Surrogate: 13C-1,2,3,4,7,8-HxCDF " 100 26-152103103

Surrogate: 37CL-2,3,7,8-TCDD " 100 35-19794.794.7

Surrogate: 13C-OCDD " 100 17-15795.595.5

Surrogate: 13C-2,3,7,8-TCDF " 100 24-16997.997.9

Surrogate: 13C-2,3,7,8-TCDD " 100 25-16485.485.4

2,3,7,8-TCDF pg/LND 10 -1.12

1,2,3,6,7,8-HxCDD "ND 50 -2.23

1,2,3,4,7,8-HxCDF "ND 50 -1.47

1,2,3,4,7,8-HxCDD "ND 50 -2.02

1,2,3,4,7,8,9-HpCDF "ND 50 -2.11

1,2,3,4,6,7,8-HpCDF "ND 50 -1.51

OCDF "ND 100 -6.10

1,2,3,6,7,8-HxCDF "ND 50 -1.47

OCDD "ND 100 -4.32

1,2,3,4,6,7,8-HpCDD "ND 50 -3.06

1,2,3,7,8-PeCDF "ND 50 -1.28

2,3,4,7,8-PeCDF "ND 50 -1.28

2,3,4,6,7,8-HxCDF "ND 50 -1.64

1,2,3,7,8,9-HxCDD "ND 50 -2.17

1,2,3,7,8-PeCDD "ND 50 -2.32

2,3,7,8-TCDD "ND 10 -1.65

1,2,3,7,8,9-HxCDF "ND 50 -2.35




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:


Units LevelSpike

ResultSource

%REC%RECLimits RPD


1613B - Quality Control

MDL

Batch 0001215 - 1613B

LCS (0001215-LCS) Prepared: 07/13/14 Analyzed: 07/15/14

Surrogate: 13C-1,2,3,7,8,9-HxCDF % 100 -98.698.6

Surrogate: 13C-1,2,3,6,7,8-HxCDF " 100 -101101

Surrogate: 13C-1,2,3,6,7,8-HxCDD " 100 -83.983.9

Surrogate: 13C-2,3,7,8-TCDD " 100 -88.588.5


Surrogate: 13C-OCDD " 100 -190190

Surrogate: 13C-1,2,3,4,7,8-HxCDD " 100 -114114

Surrogate: 13C-1,2,3,7,8-PeCDD " 100 -97.797.7

Surrogate: 13C-1,2,3,4,6,7,8-HpCDF " 100 -110110

Surrogate: 13C-1,2,3,4,6,7,8-HpCDD " 100 -97.097.0

Surrogate: 13C-2,3,4,7,8-PeCDF " 100 -116116

Surrogate: 37CL-2,3,7,8-TCDD " 100 -9.689.68


Surrogate: 13C-2,3,7,8-TCDF " 100 -100100

Surrogate: 13C-1,2,3,7,8-PeCDF " 100 -111111

Surrogate: 13C-1,2,3,4,7,8,9-HpCDF " 100 -107107

1,2,3,6,7,8-HxCDD ng/mL53.3 38-67107

1,2,3,4,7,8-HxCDF "56.1 36-67112

1,2,3,4,7,8-HxCDD "53.2 35-82106

1,2,3,4,7,8,9-HpCDF "51.1 39-69102

1,2,3,4,6,7,8-HpCDF "51.9 41-61104

1,2,3,4,6,7,8-HpCDD "51.7 35-70103

1,2,3,6,7,8-HxCDF "53.6 42-65107

1,2,3,7,8-PeCDF "58.6 40-67119

1,2,3,7,8,9-HxCDF "55.9 39-65112

OCDF "112 63-170112

1,2,3,7,8-PeCDD "52.8 35-71106

2,3,4,6,7,8-HxCDF "54.4 35-78109

2,3,4,7,8-PeCDF "57.8 34-80116

2,3,7,8-TCDD "11.2 6.7-15.8112

2,3,7,8-TCDF "11.0 7.5-15.8110

OCDD "107 78-144107

1,2,3,7,8,9-HxCDD "51.8 32-81104




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:

Notes and Definitions

Z-03 CCV for anayte is 4.6% outside of QA/QC parameters. Analyte may be biased high.

Z-02 Data may be biased high, CCV is 4.6% high.

Z-01c Samples were analyzed within hold using EPA 8260B. Samples re-analyzed outside of EPA recommended hold times

using EPA method 524 parameters.

Z-01b Sample is non detect for this analyteand/or the Analyte is a different structure from those analytes that are found to be

present in sample that data was not affected by high percent recovery. QA/QC is acceptepted based on these

parameters.

Z-01a No surrogate recovery due to matrix interference

Z-01 Low surrogate recovery due to matrix interfernce.

QR-07 Recoveries are outside acceptable QA/QC parameters due to matrix interferences.

QR-02 The RPD result exceeded the QC control limits; however, both percent recoveries were acceptable. Sample results for

the QC batch were accepted based on percent recoveries and completeness of QC data.

Ja Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).

J Concentration found below the lower quantitation limit but greater than zero.

Field This analyte was analyzed outside of the EPA recommended hold time of ASAP and should be analyzed in the field.

ND Analyte not detected at reporting limit.

NR Not reported

EPA 8260, EPA 8021/8015M EPA 5030B

EPA 8270, EPA 8081, EPA 8082, EPA 8141, EPA 8015M (extractable) Water - EPA 3510C, Soil- EPA 3550B

Metals Water- 3005A, Soil- 3050B

TCLP EPA 1311

Not Specified Same as Analysis Method

Analysis Method Prep Method




Project:

Project Number:

Project Manager:


11020 Sun Center Dr. #200 13-051-150



Date Reported:




excelchem environmental labs - california · 2017. 10. 26. · excelchem environmental lab. the...

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