improved planar resonant rf sensor for retrieval of...

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1558-1748 (c) 2017 IEEE. Personal use is permitted, but republication/redistribution requires IEEE permission. See http://www.ieee.org/publications_standards/publications/rights/index.html for more information. This article has been accepted for publication in a future issue of this journal, but has not been fully edited. Content may change prior to final publication. Citation information: DOI 10.1109/JSEN.2017.2724942, IEEE Sensors Journal > REPLACE THIS LINE WITH YOUR PAPER IDENTIFICATION NUMBER (DOUBLE-CLICK HERE TO EDIT) < 1 AbstractIn this work, the improved planar resonant sensors based on the generalized SRR configuration are proposed for the permittivity and the permeability testing of magneto-dielectric samples. It is observed that the proposed inter-digital capacitor based split ring resonator (IDC-SRR) and the meandered line based split ring resonator (ML-SRR) provide better sensitivity for dielectric and magnetic measurement, respectively, when compared with the standard SRR based microwave sensors. Both the sensors are first modeled under unloaded condition, using the full wave electromagnetic solver, the CST Microwave Studio, in order to ensure their operating frequency range near 2.45 GHz of ISM band. In the next step, the numerical simulation of these sensors is carried out by loading them with a number of reference materials in order to develop empirical model for the determination of permittivity and permeability of test samples. Additionally, the equivalent circuit models of these sensors are obtained using the ADS circuit simulator and results are compared with the numerical simulation. All the sensors are designed and fabricated on 1.27 mm thick RT/Duroid 6006 substrate, and testing is carried out using the network analyzer. A number of standard dielectric and magneto-dielectric samples are tested using the proposed scheme in order to retrieve their permittivity and permeability values. The measured data of each sample are in good match with the corresponding reference values available in literature having a typical error of less than 6%. Index TermsCharacterization, Inter digital capacitor, Permeability, Permittivity, Split ring resonator, Magneto- dielectric. Md. Shafi K T was with the Department of Electrical Engineering, Indian Institute of Technology Kanpur, Uttar Pradesh - 208016, India. He is now with the Department of Electrical and Computer Engineering, Khalifa University of Science and Technology-The Petroleum Institute, Abu Dhabi, UAE (e-mail: [email protected]). A. K. Jha was with the Department of Electrical Engineering, Indian Institute of Technology Kanpur, Uttar Pradesh-208016, India. He is now with the Institute of Photonics and Electronics, Czech Academy of Sciences, Prague - 18251, Czech Republic ([email protected]). M. J. Akhtar is with the Department of Electrical Engineering, Indian Institute of Technology Kanpur, Uttar Pradesh - 208016, India (e-mail: [email protected]). This work was partially supported by the DST under Grant DST/TSG/ME/2015/97. I. INTRODUCTION HERE are various microwave material characterization techniques available for determination of permittivity and permeability. Among different characterization techniques, the resonant methods usually provide quite accurate parameter extraction, especially for low loss samples, provided that the material parameters are required only over a very narrow frequency band [1]. However, since most of the resonators, antennas, couplers and filters are specifically designed to work in narrow band of frequencies, the resonant methods appear to be adequate to accurately estimate the electromagnetic properties of materials in the desired frequency band. The cavity perturbation technique is one of the most preferred characterization methods for narrow band application [2]-[5]. This technique requires sample placement at the maximum magnetic or electric field position for the magnetic or dielectric characterization. However, it requires bulky and costly metal cavities for performing the characterization. In recent years, the planar resonant RF sensors have been used to replace the bulky cavities, since they have advantages such as low cost, ease of fabrication and easy integration with other monolithic integrated devices [6]-[8]. The planar microwave sensors for material characterization are currently being explored by several groups. Recently, a number of planar RF resonant sensors using various configurations such as the substrate integrated waveguide (SIW) [9], the complimentary split ring resonator (CSRR) [10]-[13], the split ring resonator (SRR) [14]-[17], and the inter digital capacitor (IDC) [6],[18],[19] have been proposed. Among various configurations listed above, the CSRR and SRR based resonant sensors are used more often due to their simple fabrication process and more compactness in design. From the early works done in this domain, it is also observed that the metamaterial inspired structures based on SRR and CSRR can provide better sensitivity as compared to other planar resonant sensors. Conventionally, the CSRR based RF sensors have been used in the past for testing of dielectric materials, while the SRR based RF sensors appear to be good choice for testing of magnetic materials due to the field configuration of the microstrip geometry [20]. However, the CSRR based sensor may not be compatible with the multilayer technology where Improved Planar Resonant RF Sensor for Retrieval of Permittivity and Permeability of Materials Muhammed Shafi K T, Abhishek Kumar Jha, Member, IEEE and M Jaleel Akhtar, Senior Member, IEEE T

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  • 1558-1748 (c) 2017 IEEE. Personal use is permitted, but republication/redistribution requires IEEE permission. See http://www.ieee.org/publications_standards/publications/rights/index.html for more information.

    This article has been accepted for publication in a future issue of this journal, but has not been fully edited. Content may change prior to final publication. Citation information: DOI 10.1109/JSEN.2017.2724942, IEEE SensorsJournal

    > REPLACE THIS LINE WITH YOUR PAPER IDENTIFICATION NUMBER (DOUBLE-CLICK HERE TO EDIT) <

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    Abstract— In this work, the improved planar resonant sensors

    based on the generalized SRR configuration are proposed for the

    permittivity and the permeability testing of magneto-dielectric

    samples. It is observed that the proposed inter-digital capacitor

    based split ring resonator (IDC-SRR) and the meandered line

    based split ring resonator (ML-SRR) provide better sensitivity

    for dielectric and magnetic measurement, respectively, when

    compared with the standard SRR based microwave sensors. Both

    the sensors are first modeled under unloaded condition, using the

    full wave electromagnetic solver, the CST Microwave Studio, in

    order to ensure their operating frequency range near 2.45 GHz of

    ISM band. In the next step, the numerical simulation of these

    sensors is carried out by loading them with a number of

    reference materials in order to develop empirical model for the

    determination of permittivity and permeability of test samples.

    Additionally, the equivalent circuit models of these sensors are

    obtained using the ADS circuit simulator and results are

    compared with the numerical simulation. All the sensors are

    designed and fabricated on 1.27 mm thick RT/Duroid 6006

    substrate, and testing is carried out using the network analyzer.

    A number of standard dielectric and magneto-dielectric samples

    are tested using the proposed scheme in order to retrieve their

    permittivity and permeability values. The measured data of each

    sample are in good match with the corresponding reference

    values available in literature having a typical error of less than

    6%.

    Index Terms— Characterization, Inter digital capacitor,

    Permeability, Permittivity, Split ring resonator, Magneto-

    dielectric.

    Md. Shafi K T was with the Department of Electrical Engineering, Indian

    Institute of Technology Kanpur, Uttar Pradesh - 208016, India. He is now

    with the Department of Electrical and Computer Engineering, Khalifa

    University of Science and Technology-The Petroleum Institute, Abu Dhabi, UAE (e-mail: [email protected]).

    A. K. Jha was with the Department of Electrical Engineering, Indian

    Institute of Technology Kanpur, Uttar Pradesh-208016, India. He is now with the Institute of Photonics and Electronics, Czech Academy of Sciences,

    Prague - 18251, Czech Republic ([email protected]).

    M. J. Akhtar is with the Department of Electrical Engineering, Indian Institute of Technology Kanpur, Uttar Pradesh - 208016, India (e-mail:

    [email protected]).

    This work was partially supported by the DST under Grant DST/TSG/ME/2015/97.

    I. INTRODUCTION

    HERE are various microwave material characterization

    techniques available for determination of permittivity and

    permeability. Among different characterization techniques, the

    resonant methods usually provide quite accurate parameter

    extraction, especially for low loss samples, provided that the

    material parameters are required only over a very narrow

    frequency band [1]. However, since most of the resonators,

    antennas, couplers and filters are specifically designed to work

    in narrow band of frequencies, the resonant methods appear to

    be adequate to accurately estimate the electromagnetic

    properties of materials in the desired frequency band. The

    cavity perturbation technique is one of the most preferred

    characterization methods for narrow band application [2]-[5].

    This technique requires sample placement at the maximum

    magnetic or electric field position for the magnetic or

    dielectric characterization. However, it requires bulky and

    costly metal cavities for performing the characterization. In

    recent years, the planar resonant RF sensors have been used to

    replace the bulky cavities, since they have advantages such as

    low cost, ease of fabrication and easy integration with other

    monolithic integrated devices [6]-[8].

    The planar microwave sensors for material characterization

    are currently being explored by several groups. Recently, a

    number of planar RF resonant sensors using various

    configurations such as the substrate integrated waveguide

    (SIW) [9], the complimentary split ring resonator (CSRR)

    [10]-[13], the split ring resonator (SRR) [14]-[17], and the

    inter digital capacitor (IDC) [6],[18],[19] have been proposed.

    Among various configurations listed above, the CSRR and

    SRR based resonant sensors are used more often due to their

    simple fabrication process and more compactness in design.

    From the early works done in this domain, it is also observed

    that the metamaterial inspired structures based on SRR and

    CSRR can provide better sensitivity as compared to other

    planar resonant sensors.

    Conventionally, the CSRR based RF sensors have been

    used in the past for testing of dielectric materials, while the

    SRR based RF sensors appear to be good choice for testing of

    magnetic materials due to the field configuration of the

    microstrip geometry [20]. However, the CSRR based sensor

    may not be compatible with the multilayer technology where

    Improved Planar Resonant RF Sensor for

    Retrieval of Permittivity and Permeability of

    Materials

    Muhammed Shafi K T, Abhishek Kumar Jha, Member, IEEE and M Jaleel Akhtar, Senior Member,

    IEEE

    T

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    the access of the ground plane is restricted to minimize the

    possible fringing effect. In order to integrate the microwave

    sensors with other compact systems having multi-layer

    structures, the SRR based sensors would provide more degree

    of freedom in system design as compared to the CSRR based

    sensor.

    Now, the recent trend in RF design is to use the magneto-

    dielectric substrates to achieve miniaturization of microwave

    circuits and systems [21]-[27]. The magneto-dielectric

    substrates introduce the magnetic properties to the substrate

    material, which provide an extra parameter in terms of the

    relative permeability for optimizing several parameters of

    microwave devices. Since the magneto-dielectric substrates

    possess the permeability and the permittivity values greater

    than unity, the devices fabricated using these substrates would

    be smaller in size compared to the devices made on pure

    dielectric substrates. However, the dielectric and magnetic

    properties of these magneto-dielectric substrates need to be

    accurately measured before using them to design a RF device.

    From above discussion, it can be inferred that the accurate

    electromagnetic characterization of magneto-dielectric

    substrates is quite important in today’s scenario and it should

    preferably be carried out using the SRR based approach in

    order to conform to the modern microstrip multilayer

    technology. It is mainly due to this reason that the generalized

    SRR based approach is proposed in this work for the RF

    characterization of magneto-dielectric samples at 2.45 GHz of

    ISM band. To this end, a novel IDC based SRR (IDC-SRR)

    RF sensor for dielectric testing, and a new type of meandered

    line based split ring resonator (ML-SRR) RF sensor for

    magnetic testing, of magneto-dielectric samples are proposed.

    The newly designed sensors are compared with other

    equivalent configurations in terms of sensitivity, which shows

    the potential advantage of the proposed sensors. The proposed

    sensors are modeled using the standard equivalent circuit

    approach, and the scattering parameters of the equivalent

    circuit model are compared with those of the numerical

    simulation results. In the next step, the numerical method

    based on the finite integration technique is used to develop an

    empirical formula for calculating the relative permittivity and

    permeability of the magneto-dielectric samples in terms of the

    measured resonant frequency and the transmission coefficient

    of the loaded sensor. The prototype is fabricated on the 1.27

    mm thick RT/Duroid 6006 substrate (εr = 6.15). Lastly, the

    measurements of various standard materials are performed

    using the fabricated prototype of the proposed sensors with the

    help of Keysight’s vector network analyzer N5230C.

    The overall paper is organized as follows. First of all, the

    design procedure of the planar RF sensor for dielectric

    material testing is explained in section II. Section III contains

    the detailed information of the microwave sensor design for

    calculating relative permeability of material under test (MUT).

    The numerical modeling of each proposed sensor using the

    electromagnetic simulation tool, the CST Microwave Studio is

    included in section IV. Section V presents the measurement

    results for different magneto-dielectric materials using

    proposed sensors. The values of relative permittivity and

    permeability of different materials are tabulated with their

    reference values available in literature. Section VI deals with

    the details of error analysis and finally, the conclusion is

    provided in section VII.

    II. DESIGN OF DIELECTRIC MATERIAL SENSOR

    Measurement of dielectric and magnetic properties of

    material requires different RF sensing spots since the

    permittivity measurement is primarily carried out by placing

    the sample in the maximum electric field region while the

    permeability determination usually requires the maximum

    magnetic field region. Here, first of all, the design of RF

    sensor for dielectric material characterization is considered.

    All the RF sensor structures presented in this paper are

    simulated using the full wave electromagnetic solver, the CST

    Microwave Studio [28]

    A. Theory

    Microwave resonant method for characterization of

    materials using planar technology is based on the field

    perturbation theory. When the resonance occurs, the total

    electric field will be confined to a smaller region of split ring

    resonator, where the sample is usually placed. This confined

    electric field is capable of sensing even a smaller change in the

    dielectric constant of the test sample. The response of the

    microwave sensor to the change in the effective dielectric

    constant of the surrounding can be noticed in terms of the

    change in resonant frequency and the quality factor of the

    loaded structure.

    Fig. 1. (a) Structure of SRR based dielectric material sensor with enlarged

    view of coupled SRR structure. The dimensions of the design are, L = 50 mm,

    W = 30 mm, L1 = 6.45 mm, L2 = 10 mm, g = 0.3 mm, wd = 0.3 mm. (b)

    Electric field configuration near SRR at 2.45 GHz.

    Fig. 2. (a) Structure of capacitive loaded SRR based dielectric material sensor

    with dimensions, L1 = 5 mm, L2 = 9 mm, g = 0.3 mm, wd = 0.3 mm. b = 0.9

    mm, La = 1.8 mm. (b) Electric field configuration near capacitive loaded SRR

    at 2.45 GHz.

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    Fig. 3. (a) Structure of IDC - SRR based dielectric sensor with dimensions, L1

    = 4 mm, L2 = 7 mm, g = 0.3 mm, wd = 0.3 mm. b = 1.5 mm. (b) Electric field

    configuration near IDC based SRR at 2.45 GHz.

    For the planar microwave sensor based on the rectangular

    shaped SRR, the maximum electric field is limited to the

    dielectric gap of the SRR at resonance, thereby giving a

    sensing spot for dielectric material characterization. Fig. 1 (a)

    shows the structure of a rectangular shaped SRR based planar

    microwave sensor. Fig. 1(b) shows the electric field confined

    to dielectric gap of the SRR at resonance condition. The SRR

    structure is excited by the magnetic field of the microstrip line

    [29]. Since it is magnetically coupled, the spacing between the

    microstrip line and the SRR should be minimum to get

    maximum energy transfer from the microstrip to the SRR

    structure. Now, as one of the major goals of the sensor design

    is to improve the sensitivity, the SRR based dielectric sensor

    should accordingly be modified. The confinement of electric

    field in the gap of the SRR can be improved by increasing the

    effective capacitance of this gap, which can be achieved by

    maximizing the local area of the ring on both sides of the gap

    resulting into a capacitive loaded SRR structure as shown in

    Fig. 2(a). Fig. 2(b) shows the electric field of the proposed

    capacitive loaded SRR structure magnetically coupled to the

    microstrip line. After comparing the electric field of the

    capacitive loaded SRR with that of the simple SRR shown in

    Fig. 1(b) at the resonant frequency, it can be observed that the

    modified SRR structure substantially improves the electric

    field in the gap region which is akin to increasing the

    sensitivity. The field in the gap region of the SRR is further

    improved here to obtain higher sensitivity by introducing an

    IDC in the gap of SRR as shown in Fig. 3(a). The IDC based

    structure shown in Fig. 3(a) basically provides higher effective

    capacitance as compared to the simple parallel plate like

    structure shown in Fig. 2 (a), which leads to higher electric

    field in the small sensing region leading to higher sensitivity

    as shown in Fig. 3(b).

    B. Comparison of sensitivity

    For comparing the sensitivity of various RF sensors, each

    sensor is modeled using the CST microwave studio with a test

    material placed on corresponding sensing area of each sensor.

    The substrate material for all the sensor design is chosen as

    1.27 mm thick RT/Duroid 6006 (εr = 6.15) with a rectangular

    cube shaped test sample having dimension of 5 mm × 5 mm ×5

    mm. Since the electromagnetic properties of materials are

    usually dispersive in nature, the proposed sensors are modeled

    to resonate at the ISM frequency of 2.45 GHz for getting the

    dielectric and magnetic properties at a common frequency.

    The resonant frequency of each sensor model is optimized to

    get same operating frequency by adjusting the dimensions of

    each structure in the CST simulation environment. Later the

    sensor is loaded with test specimens having different

    electromagnetic properties, and the change in resonant

    frequency (f) values are noted down. Since the sensor is

    designed for determination of dielectric permittivity, the value

    of relative permeability is taken as unity (relative permeability

    of free space) during the simulation. The parameter f,

    representing the difference in resonant frequency (fr) of the

    sensor loaded with a particular material from the resonant

    frequency of the sensor without MUT (f0), is then plotted

    versus the relative permittivity value for different sensor

    configurations as shown in Fig. 4. From this figure, it can be

    concluded that the sensitivity of the proposed IDC-SRR based

    sensor is much higher as compared to that of the simple SRR

    based sensor for extraction of relative dielectric permittivity of

    unknown samples. Hence, the proposed IDC-SRR based RF

    sensor, which appears to be suitable for integrating with multi-

    layer planar devices; is selected in this work for further study.

    Fig. 4. Sensitivity comparison of different dielectric sensor designs.

    C. Equivalent circuit for IDC – SRR based sensor

    For carrying out a detailed analysis of the proposed sensor

    structure, an equivalent circuit with lumped elements is used

    as shown in Fig. 5(a). In Fig. 5(a), since it is difficult to

    calculate the mutual coupling value, M for the microstrip

    based circuits, the proposed equivalent circuit model is

    transformed as shown in Fig. 5(b). The parameter values of

    the equivalent circuit are extracted using the standard

    procedure [30]. Table I gives the values of the lumped

    elements of the proposed equivalent circuit corresponding to

    simple SRR and IDC based SRR dielectric sensor designs. It

    can be observed from Table I that the capacitance value of the

    proposed resonator (C1a), is larger as compared to the simple

    SRR design, which clearly validates the higher sensitivity of

    IDC based sensor over the simple sensor design. The proposed

    equivalent circuit is simulated in ADS software, and the S21

    plot from the circuit simulation is compared with the

    electromagnetic simulation data obtained using the CST as

    shown in Fig. 6. A good match between the circuit simulation

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    and the EM simulation is obtained as shown in Fig. 6.

    Fig. 5. Proposed equivalent circuit for IDC-SRR based dielectric sensor

    TABLE I

    LUMPED ELEMENT VALUES OF PROPOSED EQUIVALENT CIRCUIT

    Sensor

    design C (pF) Lc (nH) C

    1a (pF) L

    1a (nH) R ( )

    Simple

    SRR 0.71 4.03 13.52 0.31 279.7

    IDC based SRR

    0.24 3.77 32.66 0.128 282.7

    Fig. 6. Comparison of S21 plot of CST Simulation and ADS Simulation

    III. DESIGN OF MAGNETIC MATERIAL SENSOR

    After designing the modified SRR based structure for the

    dielectric material characterization, the next step is to enhance

    the sensitivity of the SRR based RF sensors in order to

    characterize magnetic materials. The magnetic permeability

    estimation using the SRR employs the conductive loop of the

    SRR which confines maximum magnetic field around the

    conductor when the SRR is at resonance because of the

    inductance offered by the conductive loop. Fig. 7(a) shows the

    structure of the rectangular shaped SRR used for the

    estimation of relative permeability. From Fig. 7(b), it can be

    observed that the magnetic field is maximum at the far edge of

    the SRR from microstrip line. The orientation of the SRR

    structure with respect to the microstrip line is chosen in order

    to place the MUT on the conductive part of the SRR without

    effecting the coupling between the microstrip line and the

    SRR structure. Since the sensitivity of the magnetic material

    characterization depends on the amplitude of the magnetic

    field around the sensing region of conductive loop of the SRR,

    the conductive loop of the SRR is meandered here in order to

    confine maximum magnetic field in the test region. Fig. 8(a)

    shows the proposed meandered line magnetic material sensor.

    As it can be seen from the Fig. 8(b), the magnetic field is more

    densely concentrated in the meandered line region as

    compared to that of the simple SRR sensor shown in Fig. 7(b).

    Fig. 7. (a) Structure of SRR based magnetic sensor with the enlarged view of

    coupled SRR structure, The dimensions of the design are, L = 80 mm, W = 40 mm, L1 = 4.8 mm, L2 = 10 mm, wd = 0.3 mm, g =0.3 mm. (b) Magnetic field

    configuration at resonant frequency.

    Fig. 8. (a) Structure of meandered line SRR based magnetic sensor with

    dimensions, wd = 0.3 mm, g = 0.3 mm, L1 = 5.855 mm, L2 = 10 mm, La = 2

    mm. (b) Magnetic field at the resonant frequency

    Fig. 9. Sensitivity comparison of different magnetic sensor designs

    The dimensions of both simple SRR and the meandered line

    based SRR sensor are optimized in order to achieve the

    operating frequency of 2.45 GHz using the CST Microwave

    Studio. These sensors are then loaded with various magnetic

    materials having same dimension as previously used for the

    study of dielectric sensors, and the resonant frequencies of

    both the magnetic material sensors are recorded for each

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    relative permeability value while keeping the relative

    permittivity value equal to one. The difference in the resonant

    frequency value for each test specimen is plotted versus the

    relative permeability value for both configurations as shown in

    Fig. 9. It can be observed from this figure that the meandered

    line SRR magnetic sensor provides more sensitivity with

    respect to the change in the relative permeability values as

    compared to that of the simple rectangular SRR based sensor.

    From Fig. 9, it can also be observed that the proposed

    meandered line sensor is having quite good sensitivity for

    materials having lower values of the relative permeability,

    which is quite important from practical point of view as the

    relative permeability of most of the magnetic composite

    substrates lies between 1 and 2.

    A. Equivalent circuit for Meandered Line SRR based sensor

    The meandered line based SRR, similar to the simple SRR,

    is magnetically coupled to the microstrip line. Hence, the

    equivalent circuit model for the meandered line SRR magnetic

    sensor can also be represented using the topology shown in

    Fig. 5. The values of the lumped elements of equivalent circuit

    are extracted using the same procedure described earlier for

    the case of dielectric sensor, and the extracted values for the

    simple SRR and meandered SRR based magnetic sensors are

    tabulated in Table II. It can be concluded from Table II that

    the inductance value of the proposed resonator (L1a) is higher

    than that of the simple SRR sensor, which clearly validates the

    higher sensitivity of the meandered SRR magnetic sensor. The

    proposed equivalent circuit model is simulated using the ADS

    software, and S21 plots of the circuit simulation and that of the

    electromagnetic simulation using CST are compared in Fig.

    10. As observed from this graph, a good match between the

    two plots is obtained which authenticates the validity of the

    proposed equivalent circuit model of the meandered line SRR

    based magnetic sensor.

    TABLE II

    LUMPED ELEMENT VALUES OF PROPOSED EQUIVALENT CIRCUIT

    Sensor

    Design C (pF) Lc (nH) C

    1a(pF) L

    1a (nH) R ( )

    Simple

    SRR 2.67 1.72 234.5 0.018 97.7

    Meandered

    SRR 2.14 1.94 70.43 0.06 77.7

    Fig. 10. Comparison of S21 plot of CST Simulation and ADS Simulation.

    IV. NUMERICAL MODEL OF PROPOSED SENSORS

    A. IDC-SRR based dielectric sensor

    In order to obtain the mathematical relationship between the

    resonant frequency of the IDC based SRR dielectric material

    sensor with that of the relative permittivity of the MUT, the

    response of the IDC based SRR dielectric sensor to the various

    dielectric values of the test sample is used. The variation in

    resonant frequency difference plotted against relative

    permittivity corresponding to IDC based SRR dielectric sensor

    is already shown in Fig. 4. A curve fitting tool of Origin is

    utilized to develop the relation based on numerical simulation

    data and the fitting function is chosen based on the minimum

    chi-square value. The following expression is finally obtained

    using this procedure for estimation of real part of the

    permittivity of the MUT.

    0 0.91781ln

    0.1341 1.04966r

    rf f

    (1)

    where f0 represents the resonant frequency of the sensor

    without MUT, which helps in normalizing the results after

    fabrication.

    B. Meandered Line SRR based magnetic sensor

    The dependence of resonant frequency of the meandered

    line based SRR magnetic material sensor on the real value of

    complex permeability is analyzed by keeping a MUT on top of

    the meandered line region of the proposed sensor. The

    dimensions of rectangular cube shaped MUT are kept same as

    in the case of dielectric sensor. The relative permeability of

    the MUT is varied and the corresponding resonant frequency

    shift of the meandered line SRR based magnetic material

    sensor is already shown in Fig. 9. The same numerical

    simulation data are used to determine the relationship between

    the change in resonant frequency and the relative permeability

    value of the MUT. Since the relative permeability value of

    materials in microwave frequency is very small, more number

    of frequency points is selected between the relative

    permeability value of 1 and 2 in order to have accurate

    modeling of the proposed sensor. Finally, curve fitting tool of

    the Origin is used as discussed above to obtain a mathematical

    formula for calculation of the relative permeability of the

    MUT as shown below.

    00.225931

    ln0.66825 0.43511

    r

    rf f

    (2)

    The f0 in this case represents the resonant frequency of the

    proposed meandered line SRR sensor without MUT.

    V. MEASUREMENT AND RESULTS

    The prototype of each sensor designs is fabricated using

    standard photolithography, and the measurement is carried out

    by connecting each sensor to the vector network analyzer

    (VNA) through a set of coaxial cables and SMA adapters. The

    VNA input power level is kept at 0 dBm, and the IF

    bandwidth is set to 50 Hz for getting better resolution. The 2

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    port OSLT calibration is carried out using the modified

    settings of the VNA and all the measurements are carried out

    under same settings. The design of each sensor is validated by

    measuring permittivity and permeability of some standard

    samples.

    A. IDC-SRR based Dielectric Sensor

    The proposed single band dielectric material sensor is

    validated by measuring a number of standard dielectric and

    magneto-dielectric samples. Fig. 11 shows the fabricated

    prototype of proposed sensor and Fig. 12 shows the measured

    S21 parameter for different dielectric and magneto-dielectric

    samples.

    The fabricated prototype is having unloaded resonant

    frequency of 2.26 GHz. A shift in resonant frequency from its

    design value of 2.45 GHz is observed here due to the

    tolerances in standard fabrication process. The values of the

    permittivity for each sample are estimated using (1) and are

    compared with the reference values available in literature.

    Table III gives the measured values of the relative permittivity

    of various dielectric and magneto-dielectric materials

    measured using the IDC-SRR based dielectric sensor along

    with the percentage error.

    Fig. 11. Fabricated prototype of IDC-SRR dielectric sensor with an enlarged

    view of the resonant structure. The dotted curve represents the position of the

    sample.

    Fig. 12. Measured S21 plot for different dielectric and magneto-dielectric

    materials.

    B. Meandered Line SRR based Magnetic Sensor

    Finally, the meandered line SRR based magnetic material

    sensor is fabricated and tested using the same measurement

    setup described earlier. The relative permeability of various

    magneto-dielectric materials are measured using the proposed

    sensor and the VNA. Fig. 13 shows the fabricated prototype,

    and Fig. 14 shows the S21 plot measured using the VNA for

    different magneto-dielectric samples loaded on the designed

    sensor. The relative permeability values of various magneto-

    dielectric samples measured using the mathematical relation

    given in (2) are tabulated in Table IV, where the extracted data

    of each sample is compared with its reference value available

    in literature.

    TABLE III MEASURED PERMITTIVITY OF DIFFERENT DIELECTRIC AND MAGNETO-

    DIELECTRIC MATERIALS.

    MUT εr-Measured

    εr

    % Error

    Carbonyl Iron 5.84 5.5 [31] 6.18

    Ni0.6Co0.4Fe2O4 3.23 - -

    30% Cobalt-Polystyrene 2.74 - -

    20% Cobalt-Polystyrene 2.34 - -

    Teflon 2.09 2.1 [8] 0.48

    PVC 2.62 2.65 [8] 1.13

    Polyethylene 2.23 2.26 [8] 1.33

    Plexiglas 2.65 2.6 [8] 1.92

    Natural rubber 2.57 - -

    Epoxy resin 3.29 3.5 [33] 6.00

    Fig. 13. Fabricated prototype of meandered-SRR magnetic sensor with an enlarged view of resonant structure. The dotted curve represents the position

    of the sample.

    Fig. 14. Measured S21 data for different magneto-dielectric and dielectric

    materials.

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    TABLE IV MEASURED RELATIVE PERMEABILITY OF DIFFERENT MAGNETO-DIELECTRIC

    AND DIELECTRIC MATERIALS.

    MUT µr Measured µr % Error

    Carbonyl Iron 1.37 1.4 [31] 2.14

    Ni0.6Co0.4Fe2O4 1.02 - -

    30% Cobalt-Polystyrene 1.34 1.36 [32] 1.47

    20% Cobalt-Polystyrene 1.11 1.15 [32] 3.47

    Teflon 1 1 0

    PVC 1 1 0

    VI. ERROR ANALYSIS

    Fig. 15. Shift in the resonant frequency corresponding to change in the

    permittivity (permeability) at a constant permeability (permittivity) using

    magnetic (dielectric) sensor.

    One of the main objectives of this work is to characterize

    magneto-dielectric materials, which have non-unity value for

    both relative permittivity and relative permeability. However,

    for simplifying the analysis, the dielectric (magnetic) material

    testing using the proposed IDC (MLSRR) based senor is

    performed after considering the value of relative permeability

    (permittivity) to be one as explained in Fig 4 (Fig 9). Here, a

    detailed analysis is carried out to observe the change in

    resonant frequency, while changing the relative permeability

    (permittivity) of the sample from unity in case of the dielectric

    (magnetic) material testing as shown in Fig. 15. From this

    figure, it can be observed that the change in resonant

    frequency corresponding to the value of relative permeability

    (permittivity) other than unity in case of the dielectric

    (magnetic) material testing is nearly less than 1/10th of the

    change shown in Figs. 4 and 9 under similar conditions.

    Hence, it can be concluded that accuracy of the measurement

    of dielectric (magnetic) MUT would not be significantly

    affected if the relative permeability (relative permittivity) of

    the actual test sample is other than unity.

    VII. CONCLUSION

    The modified SRR based RF planar sensors have been

    designed fabricated and tested for the characterization of

    dielectric and magneto-dielectric materials at 2.45 GHz of the

    ISM band. The IDC based SRR structure shows enhanced

    sensitivity as compared to that of the simple SRR

    configuration. The proposed IDC based SRR sensor appears to

    be better suited for integration with the multilayer planar

    configuration as compared to the conventional CSRR based

    sensors due to the fact that the ground is not disturbed in this

    case. The inclusion of IDC structure on the SRR significantly

    increases the sensitivity of the sensor for dielectric testing

    which is not possible otherwise. Similarly, the meandered line

    based SRR has higher sensitivity as compared to the simple

    rectangular SRR for the characterization of magnetic

    materials. A basic equivalent circuit model is used to explain

    the microwave sensor theoretically, and a close match between

    the circuit model and the numerical model results has been

    achieved in each case. The empirical models of the proposed

    sensors obtained using the numerical approach and the curve

    fitting tools have been experimentally verified. The prototypes

    of both the sensors have been fabricated, and a number of

    standard dielectric and magneto-dielectric samples have been

    tested using these sensors. The measured relative permittivity

    and relative permeability values are in good match with

    reference values available in literature having a typical

    accuracy of more than 94%.

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    Muhammed Shafi K. T received the B.Tech. degree in electronics and communication

    engineering from Calicut University, Calicut,

    India, in 2013, and the M.Tech degree in electrical engineering from the Indian Institute of

    Technology (IIT) Kanpur, India, in 2016.

    Currently, he is a research assistant in Robotics and Advanced Sensing Laboratory of Department

    of Electrical and Computer Engineering, Khalifa

    University of Science and technology-The Petroleum Institute, Abu Dhabi, UAE. His research interests include design

    and development of microwave sensors for characterization of dielectric and

    magneto-dielectric materials, Non-destructive testing of composite materials and near field microwave imaging of multi-layer dielectric materials.

    He was associated with the Microwave Imaging and Material Testing

    Laboratory, Department of Electrical Engineering, IIT Kanpur. There he was involved in design and development of compact microwave sensors for

    various applications.

    Abhishek Kumar Jha (S’14–M’17) received the

    B.E (Hons.) and M.Tech. (Hons.) degrees in

    electronics and communication engineering from the University of Burdwan, West Bengal, India,

    and the Ph.D. degree in Electrical Engineering

    from the Indian Institute of Technology Kanpur (IITK), India.

    He is currently a postdoctoral research fellow with Bioelectrodynamics research group at the

    Institute of Photonics and Electronics, The Czech Academy of Sciences,

    Prague, Czech Republic. His research interests encompass the design and development of high-frequency planar sensors and biochips for

    electromagnetic analysis and label-free sensing of biomolecules and cells,

    numerical analysis of microwave circuits and waveguide components, advanced RF sensors, frequency selective surfaces and techniques for

    nondestructive testing of materials, printed RF electronics etc. He has

    authored/coauthored more than 30 scientific articles published in peer-reviewed international journals and conference proceedings.

    He founded and chaired the IEEE MTT-S SBC IITK, Uttar Pradesh Section, India, and served the IEEE APS SBC IITK, Uttar Pradesh Section, India, as

    the secretary. He was associated with the MTRDC, DRDO Bangalore, India,

    where he was involved in medium power injection locked magnetron. He was an Assistant Professor with the Electronics & Communication Engineering

    Department, Seacom Engineering College, Howrah, India.

    Dr. Jha is a winner of various competitive and prestigious awards including the BIRAC-GYTI award under the technological edge category, the

    Microwave Graduate Fellowship in recognition of his academic achievement

    and excellence, the IEEE SIGHT design competition award etc. He is also the recipient of the University Gold Medals for being first in the first class of B.E

    and M.Tech degrees in 2009 and 2011, respectively. He is also a member of

    International Association of Engineers, Hong Kong. He is serving as one of

    the potential reviewers of IEEE Sensor Journal, IEEE Transactions on

    Instrumentation and Measurement and IEEE Transactions on Microwave

    Theory and Techniques.

    Mohammad Jaleel Akhtar (S’99–M’03–SM’09) received the Ph.D. and Dr.

    Ing. degrees in electrical engineering from the Otto-von-Guericke University of Magdeburg, Magdeburg, Germany, in 2003.

    He was a Scientist with the Central Electronics Engineering Research Institute, Pilani, India, from

    1994 to 1997, where he was involved in the design

    and development of high power microwave tubes. From 2003 to 2009, he was a Post-Doctoral

    Research Scientist and a Project Leader with the

    Institute for Pulsed Power and Microwave Technology, Karlsruhe Institute of Technology,

    Karlsruhe, Germany, where he was involved in a

    number of projects in the field of microwave material processing. In 2009, he joined the Department of Electrical Engineering, IIT Kanpur, Kanpur, India,

    where he is currently an Associate Professor. He has authored two books, two

    book chapters, and has authored or co-authored over 150 papers in various peer-reviewed international journals and conference proceedings. He holds

    two patent on RF sensors for material testing. His current research interests

    include RF, microwave and THz imaging, microwave nondestructive testing, RF sensors, functional materials, wideband electromagnetic absorbers, UWB

    antennas for imaging, RF energy harvesting and design of RF filters and

    components using the electromagnetic inverse scattering.

    Dr. Akhtar is a fellow of the Institution of Electronics and Telecommunication

    Engineers, New Delhi, India, and a Life Member of the Indian Physics Association and the Indo-French Technical Association. He is a recipient of

    the CST University Publication Award in 2009 from the CST AG, Darmstadt,

    Germany. He served as a Chair of the IEEE Microwave Theory and Techniques Society-S Uttar Pradesh Chapter from 2013 to 2015, and the Vice-

    Chair of the IEEE Uttar Pradesh Section in 2015.