page 1 of 44 · accreditations:iepa elap 100445;orelap il300001;aiha-lap, llc 101160;nvlap labcode...
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Page 1 of 44
April 16, 2020Date:STAT Analysis Corporation
Project: RH-SET-Chicago, SET Generating Station, 3501 S. Pul
Client: Carnow, Conibear, & Associates
Work Order: 20040320Work Order Sample Summary
Lab Sample ID Client Sample ID Collection DateTag Number Date Received
Revision 0
20040320-001A RH-413-001 4/13/2020 12:00:00 PM 4/13/2020
20040320-002A RH-413-002 4/13/2020 12:10:00 PM 4/13/2020
20040320-003A RH-413-003 4/13/2020 12:20:00 PM 4/13/2020
20040320-004A RH-413-004 4/13/2020 12:25:00 PM 4/13/2020
20040320-005A RH-413-005 4/13/2020 12:35:00 PM 4/13/2020
20040320-006A RH-413-006 4/13/2020 12:45:00 PM 4/13/2020
20040320-007A RH-413-007 4/13/2020 12:55:00 PM 4/13/2020
20040320-008A RH-413-008 4/13/2020 1:00:00 PM 4/13/2020
20040320-009A RH-413-009 4/13/2020 1:10:00 PM 4/13/2020
20040320-010A RH-413-010 4/13/2020 1:15:00 PM 4/13/2020
20040320-011A #60322 4/13/2020 2:00:00 PM 4/13/2020
20040320-012A #60277 4/13/2020 2:15:00 PM 4/13/2020
20040320-013A #60259 4/13/2020 2:40:00 PM 4/13/2020
20040320-014A #60300 4/13/2020 2:50:00 PM 4/13/2020
Page 2 of 44
Project: RH-SET-Chicago, SET Generating Station, 3501 S.
Client Sample ID: RH-413-001
Collection Date: 4/13/2020 12:00:00 PM
Matrix: Soil
Analyses Result Qualifier Units Date AnalyzedRL
Client: Carnow, Conibear, & Associates
Work Order: 20040320
DF
Lab ID: 20040320-001
Date Printed: April 16, 2020
STAT Analysis Corporation2242 West Harrison St., Suite 200, Chicago, IL 60612-3766Tel: (312) 733-0551 Fax: (312) 733-2386 [email protected]
Date Reported: April 16, 2020
Accreditations:IEPA ELAP 100445;ORELAP IL300001;AIHA-LAP, LLC 101160;NVLAP LabCode 101202-0
ANALYTICAL RESULTS
Revision 0
Semivolatile Organic Compounds by GC/MS SW8270C (SW3550B) Analyst: DMPrep Date: 4/14/2020Acenaphthene 4/14/20200.036 mg/Kg-dry 10.039
Acenaphthylene 4/14/20200.036 mg/Kg-dry 1ND
Aniline 4/14/20200.36 mg/Kg-dry 1ND
Anthracene 4/14/20200.036 mg/Kg-dry 10.13
Benz(a)anthracene 4/14/20200.036 mg/Kg-dry 10.42
Benzidine 4/14/20200.36 mg/Kg-dry 1ND
Benzo(a)pyrene 4/14/20200.036 mg/Kg-dry 10.36
Benzo(b)fluoranthene 4/14/20200.036 mg/Kg-dry 10.37
Benzo(g,h,i)perylene 4/14/20200.036 mg/Kg-dry 10.21
Benzo(k)fluoranthene 4/14/20200.036 mg/Kg-dry 10.31
Benzoic acid 4/14/20200.91 mg/Kg-dry 1ND
Benzyl alcohol 4/14/20200.19 mg/Kg-dry 1ND
Bis(2-chloroethoxy)methane 4/14/20200.19 mg/Kg-dry 1ND
Bis(2-chloroethyl)ether 4/14/20200.19 mg/Kg-dry 1ND
Bis(2-ethylhexyl)phthalate 4/14/20200.91 mg/Kg-dry 1ND
4-Bromophenyl phenyl ether 4/14/20200.19 mg/Kg-dry 1ND
Butyl benzyl phthalate 4/14/20200.19 mg/Kg-dry 1ND
Carbazole 4/14/20200.19 mg/Kg-dry 1ND
4-Chloroaniline 4/14/20200.19 mg/Kg-dry 1ND
4-Chloro-3-methylphenol 4/14/20200.36 mg/Kg-dry 1ND
2-Chloronaphthalene 4/14/20200.19 mg/Kg-dry 1ND
2-Chlorophenol 4/14/20200.19 mg/Kg-dry 1ND
4-Chlorophenyl phenyl ether 4/14/20200.19 mg/Kg-dry 1ND
Chrysene 4/14/20200.036 mg/Kg-dry 10.44
Dibenz(a,h)anthracene 4/14/20200.036 mg/Kg-dry 10.10
Dibenzofuran 4/14/20200.19 mg/Kg-dry 1ND
1,2-Dichlorobenzene 4/14/20200.19 mg/Kg-dry 1ND
1,3-Dichlorobenzene 4/14/20200.19 mg/Kg-dry 1ND
1,4-Dichlorobenzene 4/14/20200.19 mg/Kg-dry 1ND
3,3´-Dichlorobenzidine 4/14/20200.19 mg/Kg-dry 1ND
2,4-Dichlorophenol 4/14/20200.19 mg/Kg-dry 1ND
Diethyl phthalate 4/14/20200.19 mg/Kg-dry 1ND
2,4-Dimethylphenol 4/14/20200.19 mg/Kg-dry 1ND
Dimethyl phthalate 4/14/20200.19 mg/Kg-dry 1ND
4,6-Dinitro-2-methylphenol 4/14/20200.36 mg/Kg-dry 1ND
2,4-Dinitrophenol 4/14/20200.91 mg/Kg-dry 1ND
2,4-Dinitrotoluene 4/14/20200.036 mg/Kg-dry 1ND
2,6-Dinitrotoluene 4/14/20200.036 mg/Kg-dry 1ND
Qualifiers: J - Analyte detected below quantitation limits
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted recovery limits
ND - Not Detected at the Reporting Limit
E - Value above quantitation range
* - Non-accredited parameter
HT - Sample received past holding time
H - Holding time exceeded
RL - Reporting / Quantitation Limit for the analysis
Page 3 of 44
Project: RH-SET-Chicago, SET Generating Station, 3501 S.
Client Sample ID: RH-413-001
Collection Date: 4/13/2020 12:00:00 PM
Matrix: Soil
Analyses Result Qualifier Units Date AnalyzedRL
Client: Carnow, Conibear, & Associates
Work Order: 20040320
DF
Lab ID: 20040320-001
Date Printed: April 16, 2020
STAT Analysis Corporation2242 West Harrison St., Suite 200, Chicago, IL 60612-3766Tel: (312) 733-0551 Fax: (312) 733-2386 [email protected]
Date Reported: April 16, 2020
Accreditations:IEPA ELAP 100445;ORELAP IL300001;AIHA-LAP, LLC 101160;NVLAP LabCode 101202-0
ANALYTICAL RESULTS
Revision 0
Semivolatile Organic Compounds by GC/MS SW8270C (SW3550B) Analyst: DMPrep Date: 4/14/2020Di-n-butyl phthalate 4/14/20200.19 mg/Kg-dry 1ND
Di-n-octyl phthalate 4/14/20200.19 mg/Kg-dry 1ND
Fluoranthene 4/14/20200.036 mg/Kg-dry 10.86
Fluorene 4/14/20200.036 mg/Kg-dry 10.051
Hexachlorobenzene 4/14/20200.19 mg/Kg-dry 1ND
Hexachlorobutadiene 4/14/20200.19 mg/Kg-dry 1ND
Hexachlorocyclopentadiene 4/14/20200.19 mg/Kg-dry 1ND
Hexachloroethane 4/14/20200.19 mg/Kg-dry 1ND
Indeno(1,2,3-cd)pyrene 4/14/20200.036 mg/Kg-dry 10.19
Isophorone 4/14/20200.19 mg/Kg-dry 1ND
2-Methylnaphthalene 4/14/20200.19 mg/Kg-dry 1ND
2-Methylphenol 4/14/20200.19 mg/Kg-dry 1ND
4-Methylphenol 4/14/20200.19 mg/Kg-dry 1ND
Naphthalene 4/14/20200.036 mg/Kg-dry 1ND
2-Nitroaniline 4/14/20200.19 mg/Kg-dry 1ND
3-Nitroaniline 4/14/20200.19 mg/Kg-dry 1ND
4-Nitroaniline 4/14/20200.19 mg/Kg-dry 1ND
2-Nitrophenol 4/14/20200.19 mg/Kg-dry 1ND
4-Nitrophenol 4/14/20200.36 mg/Kg-dry 1ND
Nitrobenzene 4/14/20200.036 mg/Kg-dry 1ND
N-Nitrosodi-n-propylamine 4/14/20200.036 mg/Kg-dry 1ND
N-Nitrosodimethylamine 4/14/20200.19 mg/Kg-dry 1ND
N-Nitrosodiphenylamine 4/14/20200.19 mg/Kg-dry 1ND
2, 2'-oxybis(1-Chloropropane) 4/14/20200.19 mg/Kg-dry 1ND
Pentachlorophenol 4/14/20200.073 mg/Kg-dry 1ND
Phenanthrene 4/14/20200.036 mg/Kg-dry 10.51
Phenol 4/14/20200.19 mg/Kg-dry 1ND
Pyrene 4/14/20200.036 mg/Kg-dry 10.69
Pyridine 4/14/20200.73 mg/Kg-dry 1ND
1,2,4-Trichlorobenzene 4/14/20200.19 mg/Kg-dry 1ND
2,4,5-Trichlorophenol 4/14/20200.19 mg/Kg-dry 1ND
2,4,6-Trichlorophenol 4/14/20200.19 mg/Kg-dry 1ND
PCBs SW8082A (SW3550B) Analyst: GVCPrep Date: 4/13/2020Aroclor 1016 4/14/20200.088 mg/Kg-dry 1ND
Aroclor 1221 4/14/20200.088 mg/Kg-dry 1ND
Aroclor 1232 4/14/20200.088 mg/Kg-dry 1ND
Aroclor 1242 4/14/20200.088 mg/Kg-dry 1ND
Aroclor 1248 4/14/20200.088 mg/Kg-dry 1ND
Qualifiers: J - Analyte detected below quantitation limits
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted recovery limits
ND - Not Detected at the Reporting Limit
E - Value above quantitation range
* - Non-accredited parameter
HT - Sample received past holding time
H - Holding time exceeded
RL - Reporting / Quantitation Limit for the analysis
Page 4 of 44
Project: RH-SET-Chicago, SET Generating Station, 3501 S.
Client Sample ID: RH-413-001
Collection Date: 4/13/2020 12:00:00 PM
Matrix: Soil
Analyses Result Qualifier Units Date AnalyzedRL
Client: Carnow, Conibear, & Associates
Work Order: 20040320
DF
Lab ID: 20040320-001
Date Printed: April 16, 2020
STAT Analysis Corporation2242 West Harrison St., Suite 200, Chicago, IL 60612-3766Tel: (312) 733-0551 Fax: (312) 733-2386 [email protected]
Date Reported: April 16, 2020
Accreditations:IEPA ELAP 100445;ORELAP IL300001;AIHA-LAP, LLC 101160;NVLAP LabCode 101202-0
ANALYTICAL RESULTS
Revision 0
PCBs SW8082A (SW3550B) Analyst: GVCPrep Date: 4/13/2020Aroclor 1254 4/14/20200.088 mg/Kg-dry 10.18
Aroclor 1260 4/14/20200.088 mg/Kg-dry 10.11
Pesticides SW8081B (SW3550B) Analyst: GVCPrep Date: 4/13/20204,4´-DDD 4/14/20200.0018 mg/Kg-dry 1ND
4,4´-DDE 4/14/20200.0018 mg/Kg-dry 1ND
4,4´-DDT 4/14/20200.0018 mg/Kg-dry 1ND
Aldrin 4/14/20200.0018 mg/Kg-dry 1ND
alpha-BHC 4/14/20200.0018 mg/Kg-dry 1ND
alpha-Chlordane 4/14/20200.0018 mg/Kg-dry 1ND
beta-BHC 4/14/20200.0018 mg/Kg-dry 1ND
Chlordane 4/14/20200.018 mg/Kg-dry 1ND
delta-BHC 4/14/20200.0018 mg/Kg-dry 1ND
Dieldrin 4/14/20200.0018 mg/Kg-dry 1ND
Endosulfan I 4/14/20200.0018 mg/Kg-dry 1ND
Endosulfan II 4/14/20200.0018 mg/Kg-dry 1ND
Endosulfan sulfate 4/14/20200.0018 mg/Kg-dry 1ND
Endrin 4/14/20200.0018 mg/Kg-dry 1ND
Endrin aldehyde 4/14/20200.0018 mg/Kg-dry 1ND
Endrin ketone 4/14/20200.0018 mg/Kg-dry 1ND
gamma-BHC 4/14/20200.0018 mg/Kg-dry 1ND
gamma-Chlordane 4/14/20200.0018 mg/Kg-dry 1ND
Heptachlor 4/14/20200.0018 mg/Kg-dry 1ND
Heptachlor epoxide 4/14/20200.0018 mg/Kg-dry 1ND
Methoxychlor 4/14/20200.0018 mg/Kg-dry 1ND
Toxaphene 4/14/20200.036 mg/Kg-dry 1ND
Metals by ICP/MS SW6020A (SW3050B) Analyst: MDTPrep Date: 4/14/2020Aluminum 4/14/202037 mg/Kg-dry 204500
Antimony 4/14/20203.7 mg/Kg-dry 204.1
Arsenic 4/14/20201.9 mg/Kg-dry 2073
Barium 4/14/20201.9 mg/Kg-dry 20290
Beryllium 4/14/20200.93 mg/Kg-dry 20ND
Cadmium 4/14/20200.93 mg/Kg-dry 205.9
Calcium 4/14/2020110 mg/Kg-dry 2062000
Chromium 4/14/20201.9 mg/Kg-dry 2072
Cobalt 4/14/20201.9 mg/Kg-dry 2022
Copper 4/14/20204.6 mg/Kg-dry 20350
Iron 4/14/202056 mg/Kg-dry 20180000
Qualifiers: J - Analyte detected below quantitation limits
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted recovery limits
ND - Not Detected at the Reporting Limit
E - Value above quantitation range
* - Non-accredited parameter
HT - Sample received past holding time
H - Holding time exceeded
RL - Reporting / Quantitation Limit for the analysis
Page 5 of 44
Project: RH-SET-Chicago, SET Generating Station, 3501 S.
Client Sample ID: RH-413-001
Collection Date: 4/13/2020 12:00:00 PM
Matrix: Soil
Analyses Result Qualifier Units Date AnalyzedRL
Client: Carnow, Conibear, & Associates
Work Order: 20040320
DF
Lab ID: 20040320-001
Date Printed: April 16, 2020
STAT Analysis Corporation2242 West Harrison St., Suite 200, Chicago, IL 60612-3766Tel: (312) 733-0551 Fax: (312) 733-2386 [email protected]
Date Reported: April 16, 2020
Accreditations:IEPA ELAP 100445;ORELAP IL300001;AIHA-LAP, LLC 101160;NVLAP LabCode 101202-0
ANALYTICAL RESULTS
Revision 0
Metals by ICP/MS SW6020A (SW3050B) Analyst: MDTPrep Date: 4/14/2020Lead 4/14/20200.93 mg/Kg-dry 201800
Magnesium 4/14/202056 mg/Kg-dry 2022000
Manganese 4/14/20201.9 mg/Kg-dry 201100
Nickel 4/14/20201.9 mg/Kg-dry 2099
Potassium 4/14/202056 mg/Kg-dry 20830
Selenium 4/14/20201.9 mg/Kg-dry 20ND
Silver 4/14/20201.9 mg/Kg-dry 20ND
Sodium 4/14/2020110 mg/Kg-dry 20820
Thallium 4/14/20201.9 mg/Kg-dry 202.0
Vanadium 4/14/20201.9 mg/Kg-dry 2011
Zinc 4/14/20209.3 mg/Kg-dry 20580
Mercury SW7471B Analyst: LBPrep Date: 4/14/2020Mercury 4/14/20200.021 mg/Kg-dry 10.28
Cyanide, Total SW9012A Analyst: CABPrep Date: 4/14/2020Cyanide 4/14/20200.27 mg/Kg-dry 1ND
pH (25 °C) SW9045C Analyst: JARPrep Date: 4/13/2020pH 4/13/2020pH Units 18.59
Percent Moisture D2974 Analyst: FNPrep Date: 4/14/2020Percent Moisture * 4/14/20200.2 wt% 18.6
Asbestos Analysis by TEM EPA600/R-93/116 Analyst: RJSPrep Date:Chrysotile 7/13/2020% 1<1
Qualifiers: J - Analyte detected below quantitation limits
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted recovery limits
ND - Not Detected at the Reporting Limit
E - Value above quantitation range
* - Non-accredited parameter
HT - Sample received past holding time
H - Holding time exceeded
RL - Reporting / Quantitation Limit for the analysis
Page 6 of 44
Project: RH-SET-Chicago, SET Generating Station, 3501 S.
Client Sample ID: RH-413-002
Collection Date: 4/13/2020 12:10:00 PM
Matrix: Soil
Analyses Result Qualifier Units Date AnalyzedRL
Client: Carnow, Conibear, & Associates
Work Order: 20040320
DF
Lab ID: 20040320-002
Date Printed: April 16, 2020
STAT Analysis Corporation2242 West Harrison St., Suite 200, Chicago, IL 60612-3766Tel: (312) 733-0551 Fax: (312) 733-2386 [email protected]
Date Reported: April 16, 2020
Accreditations:IEPA ELAP 100445;ORELAP IL300001;AIHA-LAP, LLC 101160;NVLAP LabCode 101202-0
ANALYTICAL RESULTS
Revision 0
Semivolatile Organic Compounds by GC/MS SW8270C (SW3550B) Analyst: DMPrep Date: 4/14/2020Acenaphthene 4/14/20200.039 mg/Kg-dry 10.057
Acenaphthylene 4/14/20200.039 mg/Kg-dry 1ND
Aniline 4/14/20200.39 mg/Kg-dry 1ND
Anthracene 4/14/20200.039 mg/Kg-dry 10.18
Benz(a)anthracene 4/14/20200.039 mg/Kg-dry 10.71
Benzidine 4/14/20200.39 mg/Kg-dry 1ND
Benzo(a)pyrene 4/14/20200.039 mg/Kg-dry 10.55
Benzo(b)fluoranthene 4/14/20200.039 mg/Kg-dry 10.57
Benzo(g,h,i)perylene 4/14/20200.039 mg/Kg-dry 10.31
Benzo(k)fluoranthene 4/14/20200.039 mg/Kg-dry 10.46
Benzoic acid 4/14/20200.97 mg/Kg-dry 1ND
Benzyl alcohol 4/14/20200.20 mg/Kg-dry 1ND
Bis(2-chloroethoxy)methane 4/14/20200.20 mg/Kg-dry 1ND
Bis(2-chloroethyl)ether 4/14/20200.20 mg/Kg-dry 1ND
Bis(2-ethylhexyl)phthalate 4/14/20200.97 mg/Kg-dry 1ND
4-Bromophenyl phenyl ether 4/14/20200.20 mg/Kg-dry 1ND
Butyl benzyl phthalate 4/14/20200.20 mg/Kg-dry 1ND
Carbazole 4/14/20200.20 mg/Kg-dry 1ND
4-Chloroaniline 4/14/20200.20 mg/Kg-dry 1ND
4-Chloro-3-methylphenol 4/14/20200.39 mg/Kg-dry 1ND
2-Chloronaphthalene 4/14/20200.20 mg/Kg-dry 1ND
2-Chlorophenol 4/14/20200.20 mg/Kg-dry 1ND
4-Chlorophenyl phenyl ether 4/14/20200.20 mg/Kg-dry 1ND
Chrysene 4/14/20200.039 mg/Kg-dry 10.75
Dibenz(a,h)anthracene 4/14/20200.039 mg/Kg-dry 10.16
Dibenzofuran 4/14/20200.20 mg/Kg-dry 1ND
1,2-Dichlorobenzene 4/14/20200.20 mg/Kg-dry 1ND
1,3-Dichlorobenzene 4/14/20200.20 mg/Kg-dry 1ND
1,4-Dichlorobenzene 4/14/20200.20 mg/Kg-dry 1ND
3,3´-Dichlorobenzidine 4/14/20200.20 mg/Kg-dry 1ND
2,4-Dichlorophenol 4/14/20200.20 mg/Kg-dry 1ND
Diethyl phthalate 4/14/20200.20 mg/Kg-dry 1ND
2,4-Dimethylphenol 4/14/20200.20 mg/Kg-dry 1ND
Dimethyl phthalate 4/14/20200.20 mg/Kg-dry 1ND
4,6-Dinitro-2-methylphenol 4/14/20200.39 mg/Kg-dry 1ND
2,4-Dinitrophenol 4/14/20200.97 mg/Kg-dry 1ND
2,4-Dinitrotoluene 4/14/20200.039 mg/Kg-dry 1ND
2,6-Dinitrotoluene 4/14/20200.039 mg/Kg-dry 1ND
Qualifiers: J - Analyte detected below quantitation limits
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted recovery limits
ND - Not Detected at the Reporting Limit
E - Value above quantitation range
* - Non-accredited parameter
HT - Sample received past holding time
H - Holding time exceeded
RL - Reporting / Quantitation Limit for the analysis
Page 7 of 44
Project: RH-SET-Chicago, SET Generating Station, 3501 S.
Client Sample ID: RH-413-002
Collection Date: 4/13/2020 12:10:00 PM
Matrix: Soil
Analyses Result Qualifier Units Date AnalyzedRL
Client: Carnow, Conibear, & Associates
Work Order: 20040320
DF
Lab ID: 20040320-002
Date Printed: April 16, 2020
STAT Analysis Corporation2242 West Harrison St., Suite 200, Chicago, IL 60612-3766Tel: (312) 733-0551 Fax: (312) 733-2386 [email protected]
Date Reported: April 16, 2020
Accreditations:IEPA ELAP 100445;ORELAP IL300001;AIHA-LAP, LLC 101160;NVLAP LabCode 101202-0
ANALYTICAL RESULTS
Revision 0
Semivolatile Organic Compounds by GC/MS SW8270C (SW3550B) Analyst: DMPrep Date: 4/14/2020Di-n-butyl phthalate 4/14/20200.20 mg/Kg-dry 1ND
Di-n-octyl phthalate 4/14/20200.20 mg/Kg-dry 1ND
Fluoranthene 4/14/20200.039 mg/Kg-dry 11.3
Fluorene 4/14/20200.039 mg/Kg-dry 10.071
Hexachlorobenzene 4/14/20200.20 mg/Kg-dry 1ND
Hexachlorobutadiene 4/14/20200.20 mg/Kg-dry 1ND
Hexachlorocyclopentadiene 4/14/20200.20 mg/Kg-dry 1ND
Hexachloroethane 4/14/20200.20 mg/Kg-dry 1ND
Indeno(1,2,3-cd)pyrene 4/14/20200.039 mg/Kg-dry 10.30
Isophorone 4/14/20200.20 mg/Kg-dry 1ND
2-Methylnaphthalene 4/14/20200.20 mg/Kg-dry 1ND
2-Methylphenol 4/14/20200.20 mg/Kg-dry 1ND
4-Methylphenol 4/14/20200.20 mg/Kg-dry 1ND
Naphthalene 4/14/20200.039 mg/Kg-dry 1ND
2-Nitroaniline 4/14/20200.20 mg/Kg-dry 1ND
3-Nitroaniline 4/14/20200.20 mg/Kg-dry 1ND
4-Nitroaniline 4/14/20200.20 mg/Kg-dry 1ND
2-Nitrophenol 4/14/20200.20 mg/Kg-dry 1ND
4-Nitrophenol 4/14/20200.39 mg/Kg-dry 1ND
Nitrobenzene 4/14/20200.039 mg/Kg-dry 1ND
N-Nitrosodi-n-propylamine 4/14/20200.039 mg/Kg-dry 1ND
N-Nitrosodimethylamine 4/14/20200.20 mg/Kg-dry 1ND
N-Nitrosodiphenylamine 4/14/20200.20 mg/Kg-dry 1ND
2, 2'-oxybis(1-Chloropropane) 4/14/20200.20 mg/Kg-dry 1ND
Pentachlorophenol 4/14/20200.078 mg/Kg-dry 1ND
Phenanthrene 4/14/20200.039 mg/Kg-dry 10.69
Phenol 4/14/20200.20 mg/Kg-dry 1ND
Pyrene 4/14/20200.039 mg/Kg-dry 11.1
Pyridine 4/14/20200.78 mg/Kg-dry 1ND
1,2,4-Trichlorobenzene 4/14/20200.20 mg/Kg-dry 1ND
2,4,5-Trichlorophenol 4/14/20200.20 mg/Kg-dry 1ND
2,4,6-Trichlorophenol 4/14/20200.20 mg/Kg-dry 1ND
PCBs SW8082A (SW3550B) Analyst: GVCPrep Date: 4/13/2020Aroclor 1016 4/14/20200.094 mg/Kg-dry 1ND
Aroclor 1221 4/14/20200.094 mg/Kg-dry 1ND
Aroclor 1232 4/14/20200.094 mg/Kg-dry 1ND
Aroclor 1242 4/14/20200.094 mg/Kg-dry 10.19
Aroclor 1248 4/14/20200.094 mg/Kg-dry 1ND
Qualifiers: J - Analyte detected below quantitation limits
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted recovery limits
ND - Not Detected at the Reporting Limit
E - Value above quantitation range
* - Non-accredited parameter
HT - Sample received past holding time
H - Holding time exceeded
RL - Reporting / Quantitation Limit for the analysis
Page 8 of 44
Project: RH-SET-Chicago, SET Generating Station, 3501 S.
Client Sample ID: RH-413-002
Collection Date: 4/13/2020 12:10:00 PM
Matrix: Soil
Analyses Result Qualifier Units Date AnalyzedRL
Client: Carnow, Conibear, & Associates
Work Order: 20040320
DF
Lab ID: 20040320-002
Date Printed: April 16, 2020
STAT Analysis Corporation2242 West Harrison St., Suite 200, Chicago, IL 60612-3766Tel: (312) 733-0551 Fax: (312) 733-2386 [email protected]
Date Reported: April 16, 2020
Accreditations:IEPA ELAP 100445;ORELAP IL300001;AIHA-LAP, LLC 101160;NVLAP LabCode 101202-0
ANALYTICAL RESULTS
Revision 0
PCBs SW8082A (SW3550B) Analyst: GVCPrep Date: 4/13/2020Aroclor 1254 4/14/20200.094 mg/Kg-dry 10.34
Aroclor 1260 4/14/20200.094 mg/Kg-dry 10.20
Pesticides SW8081B (SW3550B) Analyst: GVCPrep Date: 4/13/20204,4´-DDD 4/14/20200.0019 mg/Kg-dry 1ND
4,4´-DDE 4/14/20200.0019 mg/Kg-dry 1ND
4,4´-DDT 4/14/20200.0019 mg/Kg-dry 1ND
Aldrin 4/14/20200.0019 mg/Kg-dry 1ND
alpha-BHC 4/14/20200.0019 mg/Kg-dry 1ND
alpha-Chlordane 4/14/20200.0019 mg/Kg-dry 1ND
beta-BHC 4/14/20200.0019 mg/Kg-dry 1ND
Chlordane 4/14/20200.019 mg/Kg-dry 1ND
delta-BHC 4/14/20200.0019 mg/Kg-dry 1ND
Dieldrin 4/14/20200.0019 mg/Kg-dry 1ND
Endosulfan I 4/14/20200.0019 mg/Kg-dry 1ND
Endosulfan II 4/14/20200.0019 mg/Kg-dry 1ND
Endosulfan sulfate 4/14/20200.0019 mg/Kg-dry 1ND
Endrin 4/14/20200.0019 mg/Kg-dry 1ND
Endrin aldehyde 4/14/20200.0019 mg/Kg-dry 1ND
Endrin ketone 4/14/20200.0019 mg/Kg-dry 1ND
gamma-BHC 4/14/20200.0019 mg/Kg-dry 1ND
gamma-Chlordane 4/14/20200.0019 mg/Kg-dry 1ND
Heptachlor 4/14/20200.0019 mg/Kg-dry 1ND
Heptachlor epoxide 4/14/20200.0019 mg/Kg-dry 1ND
Methoxychlor 4/14/20200.0019 mg/Kg-dry 1ND
Toxaphene 4/14/20200.039 mg/Kg-dry 1ND
Metals by ICP/MS SW6020A (SW3050B) Analyst: MDTPrep Date: 4/14/2020Aluminum 4/14/202041 mg/Kg-dry 206000
Antimony 4/14/20204.1 mg/Kg-dry 20ND
Arsenic 4/14/20202.0 mg/Kg-dry 20170
Barium 4/14/20202.0 mg/Kg-dry 20300
Beryllium 4/14/20201.0 mg/Kg-dry 20ND
Cadmium 4/14/20201.0 mg/Kg-dry 204.6
Calcium 4/14/2020120 mg/Kg-dry 2081000
Chromium 4/14/20202.0 mg/Kg-dry 2050
Cobalt 4/14/20202.0 mg/Kg-dry 2017
Copper 4/14/20205.1 mg/Kg-dry 20320
Iron 4/14/202061 mg/Kg-dry 20140000
Qualifiers: J - Analyte detected below quantitation limits
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted recovery limits
ND - Not Detected at the Reporting Limit
E - Value above quantitation range
* - Non-accredited parameter
HT - Sample received past holding time
H - Holding time exceeded
RL - Reporting / Quantitation Limit for the analysis
Page 9 of 44
Project: RH-SET-Chicago, SET Generating Station, 3501 S.
Client Sample ID: RH-413-002
Collection Date: 4/13/2020 12:10:00 PM
Matrix: Soil
Analyses Result Qualifier Units Date AnalyzedRL
Client: Carnow, Conibear, & Associates
Work Order: 20040320
DF
Lab ID: 20040320-002
Date Printed: April 16, 2020
STAT Analysis Corporation2242 West Harrison St., Suite 200, Chicago, IL 60612-3766Tel: (312) 733-0551 Fax: (312) 733-2386 [email protected]
Date Reported: April 16, 2020
Accreditations:IEPA ELAP 100445;ORELAP IL300001;AIHA-LAP, LLC 101160;NVLAP LabCode 101202-0
ANALYTICAL RESULTS
Revision 0
Metals by ICP/MS SW6020A (SW3050B) Analyst: MDTPrep Date: 4/14/2020Lead 4/14/20201.0 mg/Kg-dry 201300
Magnesium 4/14/202061 mg/Kg-dry 2034000
Manganese 4/14/20202.0 mg/Kg-dry 20930
Nickel 4/14/20202.0 mg/Kg-dry 2074
Potassium 4/14/202061 mg/Kg-dry 20970
Selenium 4/14/20202.0 mg/Kg-dry 20ND
Silver 4/14/20202.0 mg/Kg-dry 20ND
Sodium 4/14/2020120 mg/Kg-dry 201000
Thallium 4/14/20202.0 mg/Kg-dry 20ND
Vanadium 4/14/20202.0 mg/Kg-dry 2013
Zinc 4/14/202010 mg/Kg-dry 20440
Mercury SW7471B Analyst: LBPrep Date: 4/14/2020Mercury 4/14/20200.020 mg/Kg-dry 10.18
Cyanide, Total SW9012A Analyst: CABPrep Date: 4/14/2020Cyanide 4/14/20200.29 mg/Kg-dry 1ND
pH (25 °C) SW9045C Analyst: JARPrep Date: 4/13/2020pH 4/13/2020pH Units 18.97
Percent Moisture D2974 Analyst: FNPrep Date: 4/14/2020Percent Moisture * 4/14/20200.2 wt% 115.0
Asbestos Analysis by TEM EPA600/R-93/116 Analyst: RJSPrep Date:Chrysotile 7/13/2020% 1<1
Qualifiers: J - Analyte detected below quantitation limits
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted recovery limits
ND - Not Detected at the Reporting Limit
E - Value above quantitation range
* - Non-accredited parameter
HT - Sample received past holding time
H - Holding time exceeded
RL - Reporting / Quantitation Limit for the analysis
Page 10 of 44
Project: RH-SET-Chicago, SET Generating Station, 3501 S.
Client Sample ID: RH-413-003
Collection Date: 4/13/2020 12:20:00 PM
Matrix: Soil
Analyses Result Qualifier Units Date AnalyzedRL
Client: Carnow, Conibear, & Associates
Work Order: 20040320
DF
Lab ID: 20040320-003
Date Printed: April 16, 2020
STAT Analysis Corporation2242 West Harrison St., Suite 200, Chicago, IL 60612-3766Tel: (312) 733-0551 Fax: (312) 733-2386 [email protected]
Date Reported: April 16, 2020
Accreditations:IEPA ELAP 100445;ORELAP IL300001;AIHA-LAP, LLC 101160;NVLAP LabCode 101202-0
ANALYTICAL RESULTS
Revision 0
Semivolatile Organic Compounds by GC/MS SW8270C (SW3550B) Analyst: DMPrep Date: 4/14/2020Acenaphthene 4/14/20200.036 mg/Kg-dry 10.036
Acenaphthylene 4/14/20200.036 mg/Kg-dry 1ND
Aniline 4/14/20200.36 mg/Kg-dry 1ND
Anthracene 4/14/20200.036 mg/Kg-dry 10.13
Benz(a)anthracene 4/14/20200.036 mg/Kg-dry 10.46
Benzidine 4/14/20200.36 mg/Kg-dry 1ND
Benzo(a)pyrene 4/14/20200.036 mg/Kg-dry 10.37
Benzo(b)fluoranthene 4/14/20200.036 mg/Kg-dry 10.41
Benzo(g,h,i)perylene 4/14/20200.036 mg/Kg-dry 10.25
Benzo(k)fluoranthene 4/14/20200.036 mg/Kg-dry 10.36
Benzoic acid 4/14/20200.91 mg/Kg-dry 1ND
Benzyl alcohol 4/14/20200.19 mg/Kg-dry 1ND
Bis(2-chloroethoxy)methane 4/14/20200.19 mg/Kg-dry 1ND
Bis(2-chloroethyl)ether 4/14/20200.19 mg/Kg-dry 1ND
Bis(2-ethylhexyl)phthalate 4/14/20200.91 mg/Kg-dry 1ND
4-Bromophenyl phenyl ether 4/14/20200.19 mg/Kg-dry 1ND
Butyl benzyl phthalate 4/14/20200.19 mg/Kg-dry 1ND
Carbazole 4/14/20200.19 mg/Kg-dry 1ND
4-Chloroaniline 4/14/20200.19 mg/Kg-dry 1ND
4-Chloro-3-methylphenol 4/14/20200.36 mg/Kg-dry 1ND
2-Chloronaphthalene 4/14/20200.19 mg/Kg-dry 1ND
2-Chlorophenol 4/14/20200.19 mg/Kg-dry 1ND
4-Chlorophenyl phenyl ether 4/14/20200.19 mg/Kg-dry 1ND
Chrysene 4/14/20200.036 mg/Kg-dry 10.51
Dibenz(a,h)anthracene 4/14/20200.036 mg/Kg-dry 10.12
Dibenzofuran 4/14/20200.19 mg/Kg-dry 1ND
1,2-Dichlorobenzene 4/14/20200.19 mg/Kg-dry 1ND
1,3-Dichlorobenzene 4/14/20200.19 mg/Kg-dry 1ND
1,4-Dichlorobenzene 4/14/20200.19 mg/Kg-dry 1ND
3,3´-Dichlorobenzidine 4/14/20200.19 mg/Kg-dry 1ND
2,4-Dichlorophenol 4/14/20200.19 mg/Kg-dry 1ND
Diethyl phthalate 4/14/20200.19 mg/Kg-dry 1ND
2,4-Dimethylphenol 4/14/20200.19 mg/Kg-dry 1ND
Dimethyl phthalate 4/14/20200.19 mg/Kg-dry 1ND
4,6-Dinitro-2-methylphenol 4/14/20200.36 mg/Kg-dry 1ND
2,4-Dinitrophenol 4/14/20200.91 mg/Kg-dry 1ND
2,4-Dinitrotoluene 4/14/20200.036 mg/Kg-dry 1ND
2,6-Dinitrotoluene 4/14/20200.036 mg/Kg-dry 1ND
Qualifiers: J - Analyte detected below quantitation limits
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted recovery limits
ND - Not Detected at the Reporting Limit
E - Value above quantitation range
* - Non-accredited parameter
HT - Sample received past holding time
H - Holding time exceeded
RL - Reporting / Quantitation Limit for the analysis
Page 11 of 44
Project: RH-SET-Chicago, SET Generating Station, 3501 S.
Client Sample ID: RH-413-003
Collection Date: 4/13/2020 12:20:00 PM
Matrix: Soil
Analyses Result Qualifier Units Date AnalyzedRL
Client: Carnow, Conibear, & Associates
Work Order: 20040320
DF
Lab ID: 20040320-003
Date Printed: April 16, 2020
STAT Analysis Corporation2242 West Harrison St., Suite 200, Chicago, IL 60612-3766Tel: (312) 733-0551 Fax: (312) 733-2386 [email protected]
Date Reported: April 16, 2020
Accreditations:IEPA ELAP 100445;ORELAP IL300001;AIHA-LAP, LLC 101160;NVLAP LabCode 101202-0
ANALYTICAL RESULTS
Revision 0
Semivolatile Organic Compounds by GC/MS SW8270C (SW3550B) Analyst: DMPrep Date: 4/14/2020Di-n-butyl phthalate 4/14/20200.19 mg/Kg-dry 1ND
Di-n-octyl phthalate 4/14/20200.19 mg/Kg-dry 1ND
Fluoranthene 4/14/20200.036 mg/Kg-dry 10.89
Fluorene 4/14/20200.036 mg/Kg-dry 10.042
Hexachlorobenzene 4/14/20200.19 mg/Kg-dry 1ND
Hexachlorobutadiene 4/14/20200.19 mg/Kg-dry 1ND
Hexachlorocyclopentadiene 4/14/20200.19 mg/Kg-dry 1ND
Hexachloroethane 4/14/20200.19 mg/Kg-dry 1ND
Indeno(1,2,3-cd)pyrene 4/14/20200.036 mg/Kg-dry 10.21
Isophorone 4/14/20200.19 mg/Kg-dry 1ND
2-Methylnaphthalene 4/14/20200.19 mg/Kg-dry 1ND
2-Methylphenol 4/14/20200.19 mg/Kg-dry 1ND
4-Methylphenol 4/14/20200.19 mg/Kg-dry 1ND
Naphthalene 4/14/20200.036 mg/Kg-dry 1ND
2-Nitroaniline 4/14/20200.19 mg/Kg-dry 1ND
3-Nitroaniline 4/14/20200.19 mg/Kg-dry 1ND
4-Nitroaniline 4/14/20200.19 mg/Kg-dry 1ND
2-Nitrophenol 4/14/20200.19 mg/Kg-dry 1ND
4-Nitrophenol 4/14/20200.36 mg/Kg-dry 1ND
Nitrobenzene 4/14/20200.036 mg/Kg-dry 1ND
N-Nitrosodi-n-propylamine 4/14/20200.036 mg/Kg-dry 1ND
N-Nitrosodimethylamine 4/14/20200.19 mg/Kg-dry 1ND
N-Nitrosodiphenylamine 4/14/20200.19 mg/Kg-dry 1ND
2, 2'-oxybis(1-Chloropropane) 4/14/20200.19 mg/Kg-dry 1ND
Pentachlorophenol 4/14/20200.073 mg/Kg-dry 1ND
Phenanthrene 4/14/20200.036 mg/Kg-dry 10.49
Phenol 4/14/20200.19 mg/Kg-dry 1ND
Pyrene 4/14/20200.036 mg/Kg-dry 10.75
Pyridine 4/14/20200.73 mg/Kg-dry 1ND
1,2,4-Trichlorobenzene 4/14/20200.19 mg/Kg-dry 1ND
2,4,5-Trichlorophenol 4/14/20200.19 mg/Kg-dry 1ND
2,4,6-Trichlorophenol 4/14/20200.19 mg/Kg-dry 1ND
PCBs SW8082A (SW3550B) Analyst: GVCPrep Date: 4/13/2020Aroclor 1016 4/14/20200.088 mg/Kg-dry 1ND
Aroclor 1221 4/14/20200.088 mg/Kg-dry 1ND
Aroclor 1232 4/14/20200.088 mg/Kg-dry 1ND
Aroclor 1242 4/14/20200.088 mg/Kg-dry 10.19
Aroclor 1248 4/14/20200.088 mg/Kg-dry 1ND
Qualifiers: J - Analyte detected below quantitation limits
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted recovery limits
ND - Not Detected at the Reporting Limit
E - Value above quantitation range
* - Non-accredited parameter
HT - Sample received past holding time
H - Holding time exceeded
RL - Reporting / Quantitation Limit for the analysis
Page 12 of 44
Project: RH-SET-Chicago, SET Generating Station, 3501 S.
Client Sample ID: RH-413-003
Collection Date: 4/13/2020 12:20:00 PM
Matrix: Soil
Analyses Result Qualifier Units Date AnalyzedRL
Client: Carnow, Conibear, & Associates
Work Order: 20040320
DF
Lab ID: 20040320-003
Date Printed: April 16, 2020
STAT Analysis Corporation2242 West Harrison St., Suite 200, Chicago, IL 60612-3766Tel: (312) 733-0551 Fax: (312) 733-2386 [email protected]
Date Reported: April 16, 2020
Accreditations:IEPA ELAP 100445;ORELAP IL300001;AIHA-LAP, LLC 101160;NVLAP LabCode 101202-0
ANALYTICAL RESULTS
Revision 0
PCBs SW8082A (SW3550B) Analyst: GVCPrep Date: 4/13/2020Aroclor 1254 4/14/20200.088 mg/Kg-dry 10.33
Aroclor 1260 4/14/20200.088 mg/Kg-dry 10.21
Pesticides SW8081B (SW3550B) Analyst: GVCPrep Date: 4/13/20204,4´-DDD 4/14/20200.0018 mg/Kg-dry 1ND
4,4´-DDE 4/14/20200.0018 mg/Kg-dry 1ND
4,4´-DDT 4/14/20200.0018 mg/Kg-dry 1ND
Aldrin 4/14/20200.0018 mg/Kg-dry 1ND
alpha-BHC 4/14/20200.0018 mg/Kg-dry 1ND
alpha-Chlordane 4/14/20200.0018 mg/Kg-dry 1ND
beta-BHC 4/14/20200.0018 mg/Kg-dry 1ND
Chlordane 4/14/20200.018 mg/Kg-dry 1ND
delta-BHC 4/14/20200.0018 mg/Kg-dry 1ND
Dieldrin 4/14/20200.0018 mg/Kg-dry 1ND
Endosulfan I 4/14/20200.0018 mg/Kg-dry 1ND
Endosulfan II 4/14/20200.0018 mg/Kg-dry 1ND
Endosulfan sulfate 4/14/20200.0018 mg/Kg-dry 1ND
Endrin 4/14/20200.0018 mg/Kg-dry 1ND
Endrin aldehyde 4/14/20200.0018 mg/Kg-dry 1ND
Endrin ketone 4/14/20200.0018 mg/Kg-dry 1ND
gamma-BHC 4/14/20200.0018 mg/Kg-dry 1ND
gamma-Chlordane 4/14/20200.0018 mg/Kg-dry 1ND
Heptachlor 4/14/20200.0018 mg/Kg-dry 1ND
Heptachlor epoxide 4/14/20200.0018 mg/Kg-dry 1ND
Methoxychlor 4/14/20200.0018 mg/Kg-dry 1ND
Toxaphene 4/14/20200.036 mg/Kg-dry 1ND
Metals by ICP/MS SW6020A (SW3050B) Analyst: MDTPrep Date: 4/14/2020Aluminum 4/14/202037 mg/Kg-dry 204900
Antimony 4/14/20203.7 mg/Kg-dry 20ND
Arsenic 4/14/20201.8 mg/Kg-dry 2066
Barium 4/14/20201.8 mg/Kg-dry 20370
Beryllium 4/14/20200.92 mg/Kg-dry 20ND
Cadmium 4/14/20200.92 mg/Kg-dry 208.5
Calcium 4/14/2020110 mg/Kg-dry 2040000
Chromium 4/14/20201.8 mg/Kg-dry 20130
Cobalt 4/14/20201.8 mg/Kg-dry 2020
Copper 4/14/20204.6 mg/Kg-dry 20300
Iron 4/14/202055 mg/Kg-dry 20210000
Qualifiers: J - Analyte detected below quantitation limits
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted recovery limits
ND - Not Detected at the Reporting Limit
E - Value above quantitation range
* - Non-accredited parameter
HT - Sample received past holding time
H - Holding time exceeded
RL - Reporting / Quantitation Limit for the analysis
Page 13 of 44
Project: RH-SET-Chicago, SET Generating Station, 3501 S.
Client Sample ID: RH-413-003
Collection Date: 4/13/2020 12:20:00 PM
Matrix: Soil
Analyses Result Qualifier Units Date AnalyzedRL
Client: Carnow, Conibear, & Associates
Work Order: 20040320
DF
Lab ID: 20040320-003
Date Printed: April 16, 2020
STAT Analysis Corporation2242 West Harrison St., Suite 200, Chicago, IL 60612-3766Tel: (312) 733-0551 Fax: (312) 733-2386 [email protected]
Date Reported: April 16, 2020
Accreditations:IEPA ELAP 100445;ORELAP IL300001;AIHA-LAP, LLC 101160;NVLAP LabCode 101202-0
ANALYTICAL RESULTS
Revision 0
Metals by ICP/MS SW6020A (SW3050B) Analyst: MDTPrep Date: 4/14/2020Lead 4/14/20200.92 mg/Kg-dry 203500
Magnesium 4/14/202055 mg/Kg-dry 2014000
Manganese 4/14/20201.8 mg/Kg-dry 201100
Nickel 4/14/20201.8 mg/Kg-dry 20110
Potassium 4/14/202055 mg/Kg-dry 201100
Selenium 4/14/20201.8 mg/Kg-dry 20ND
Silver 4/14/20201.8 mg/Kg-dry 20ND
Sodium 4/14/2020110 mg/Kg-dry 20610
Thallium 4/14/20201.8 mg/Kg-dry 202.3
Vanadium 4/14/20201.8 mg/Kg-dry 2012
Zinc 4/14/20209.2 mg/Kg-dry 20770
Mercury SW7471B Analyst: LBPrep Date: 4/14/2020Mercury 4/14/20200.021 mg/Kg-dry 10.26
Cyanide, Total SW9012A Analyst: CABPrep Date: 4/14/2020Cyanide 4/14/20200.27 mg/Kg-dry 1ND
pH (25 °C) SW9045C Analyst: JARPrep Date: 4/13/2020pH 4/13/2020pH Units 18.95
Percent Moisture D2974 Analyst: FNPrep Date: 4/14/2020Percent Moisture * 4/14/20200.2 wt% 19.5
Asbestos Analysis by TEM EPA600/R-93/116 Analyst: RJSPrep Date:Chrysotile 7/13/2020% 1<1
Qualifiers: J - Analyte detected below quantitation limits
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted recovery limits
ND - Not Detected at the Reporting Limit
E - Value above quantitation range
* - Non-accredited parameter
HT - Sample received past holding time
H - Holding time exceeded
RL - Reporting / Quantitation Limit for the analysis
Page 14 of 44
Project: RH-SET-Chicago, SET Generating Station, 3501 S.
Client Sample ID: RH-413-004
Collection Date: 4/13/2020 12:25:00 PM
Matrix: Soil
Analyses Result Qualifier Units Date AnalyzedRL
Client: Carnow, Conibear, & Associates
Work Order: 20040320
DF
Lab ID: 20040320-004
Date Printed: April 16, 2020
STAT Analysis Corporation2242 West Harrison St., Suite 200, Chicago, IL 60612-3766Tel: (312) 733-0551 Fax: (312) 733-2386 [email protected]
Date Reported: April 16, 2020
Accreditations:IEPA ELAP 100445;ORELAP IL300001;AIHA-LAP, LLC 101160;NVLAP LabCode 101202-0
ANALYTICAL RESULTS
Revision 0
Semivolatile Organic Compounds by GC/MS SW8270C (SW3550B) Analyst: DMPrep Date: 4/14/2020Acenaphthene 4/14/20200.036 mg/Kg-dry 10.067
Acenaphthylene 4/14/20200.036 mg/Kg-dry 1ND
Aniline 4/14/20200.36 mg/Kg-dry 1ND
Anthracene 4/14/20200.036 mg/Kg-dry 10.12
Benz(a)anthracene 4/14/20200.036 mg/Kg-dry 10.25
Benzidine 4/14/20200.36 mg/Kg-dry 1ND
Benzo(a)pyrene 4/14/20200.036 mg/Kg-dry 10.25
Benzo(b)fluoranthene 4/14/20200.036 mg/Kg-dry 10.24
Benzo(g,h,i)perylene 4/14/20200.036 mg/Kg-dry 10.19
Benzo(k)fluoranthene 4/14/20200.036 mg/Kg-dry 10.24
Benzoic acid 4/14/20200.90 mg/Kg-dry 1ND
Benzyl alcohol 4/14/20200.19 mg/Kg-dry 1ND
Bis(2-chloroethoxy)methane 4/14/20200.19 mg/Kg-dry 1ND
Bis(2-chloroethyl)ether 4/14/20200.19 mg/Kg-dry 1ND
Bis(2-ethylhexyl)phthalate 4/14/20200.90 mg/Kg-dry 1ND
4-Bromophenyl phenyl ether 4/14/20200.19 mg/Kg-dry 1ND
Butyl benzyl phthalate 4/14/20200.19 mg/Kg-dry 1ND
Carbazole 4/14/20200.19 mg/Kg-dry 1ND
4-Chloroaniline 4/14/20200.19 mg/Kg-dry 1ND
4-Chloro-3-methylphenol 4/14/20200.36 mg/Kg-dry 1ND
2-Chloronaphthalene 4/14/20200.19 mg/Kg-dry 1ND
2-Chlorophenol 4/14/20200.19 mg/Kg-dry 1ND
4-Chlorophenyl phenyl ether 4/14/20200.19 mg/Kg-dry 1ND
Chrysene 4/14/20200.036 mg/Kg-dry 10.30
Dibenz(a,h)anthracene 4/14/20200.036 mg/Kg-dry 10.11
Dibenzofuran 4/14/20200.19 mg/Kg-dry 1ND
1,2-Dichlorobenzene 4/14/20200.19 mg/Kg-dry 1ND
1,3-Dichlorobenzene 4/14/20200.19 mg/Kg-dry 1ND
1,4-Dichlorobenzene 4/14/20200.19 mg/Kg-dry 1ND
3,3´-Dichlorobenzidine 4/14/20200.19 mg/Kg-dry 1ND
2,4-Dichlorophenol 4/14/20200.19 mg/Kg-dry 1ND
Diethyl phthalate 4/14/20200.19 mg/Kg-dry 1ND
2,4-Dimethylphenol 4/14/20200.19 mg/Kg-dry 1ND
Dimethyl phthalate 4/14/20200.19 mg/Kg-dry 1ND
4,6-Dinitro-2-methylphenol 4/14/20200.36 mg/Kg-dry 1ND
2,4-Dinitrophenol 4/14/20200.90 mg/Kg-dry 1ND
2,4-Dinitrotoluene 4/14/20200.036 mg/Kg-dry 1ND
2,6-Dinitrotoluene 4/14/20200.036 mg/Kg-dry 1ND
Qualifiers: J - Analyte detected below quantitation limits
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted recovery limits
ND - Not Detected at the Reporting Limit
E - Value above quantitation range
* - Non-accredited parameter
HT - Sample received past holding time
H - Holding time exceeded
RL - Reporting / Quantitation Limit for the analysis
Page 15 of 44
Project: RH-SET-Chicago, SET Generating Station, 3501 S.
Client Sample ID: RH-413-004
Collection Date: 4/13/2020 12:25:00 PM
Matrix: Soil
Analyses Result Qualifier Units Date AnalyzedRL
Client: Carnow, Conibear, & Associates
Work Order: 20040320
DF
Lab ID: 20040320-004
Date Printed: April 16, 2020
STAT Analysis Corporation2242 West Harrison St., Suite 200, Chicago, IL 60612-3766Tel: (312) 733-0551 Fax: (312) 733-2386 [email protected]
Date Reported: April 16, 2020
Accreditations:IEPA ELAP 100445;ORELAP IL300001;AIHA-LAP, LLC 101160;NVLAP LabCode 101202-0
ANALYTICAL RESULTS
Revision 0
Semivolatile Organic Compounds by GC/MS SW8270C (SW3550B) Analyst: DMPrep Date: 4/14/2020Di-n-butyl phthalate 4/14/20200.19 mg/Kg-dry 1ND
Di-n-octyl phthalate 4/14/20200.19 mg/Kg-dry 1ND
Fluoranthene 4/14/20200.036 mg/Kg-dry 10.70
Fluorene 4/14/20200.036 mg/Kg-dry 10.060
Hexachlorobenzene 4/14/20200.19 mg/Kg-dry 1ND
Hexachlorobutadiene 4/14/20200.19 mg/Kg-dry 1ND
Hexachlorocyclopentadiene 4/14/20200.19 mg/Kg-dry 1ND
Hexachloroethane 4/14/20200.19 mg/Kg-dry 1ND
Indeno(1,2,3-cd)pyrene 4/14/20200.036 mg/Kg-dry 10.15
Isophorone 4/14/20200.19 mg/Kg-dry 1ND
2-Methylnaphthalene 4/14/20200.19 mg/Kg-dry 1ND
2-Methylphenol 4/14/20200.19 mg/Kg-dry 1ND
4-Methylphenol 4/14/20200.19 mg/Kg-dry 1ND
Naphthalene 4/14/20200.036 mg/Kg-dry 1ND
2-Nitroaniline 4/14/20200.19 mg/Kg-dry 1ND
3-Nitroaniline 4/14/20200.19 mg/Kg-dry 1ND
4-Nitroaniline 4/14/20200.19 mg/Kg-dry 1ND
2-Nitrophenol 4/14/20200.19 mg/Kg-dry 1ND
4-Nitrophenol 4/14/20200.36 mg/Kg-dry 1ND
Nitrobenzene 4/14/20200.036 mg/Kg-dry 1ND
N-Nitrosodi-n-propylamine 4/14/20200.036 mg/Kg-dry 1ND
N-Nitrosodimethylamine 4/14/20200.19 mg/Kg-dry 1ND
N-Nitrosodiphenylamine 4/14/20200.19 mg/Kg-dry 1ND
2, 2'-oxybis(1-Chloropropane) 4/14/20200.19 mg/Kg-dry 1ND
Pentachlorophenol 4/14/20200.073 mg/Kg-dry 1ND
Phenanthrene 4/14/20200.036 mg/Kg-dry 10.66
Phenol 4/14/20200.19 mg/Kg-dry 1ND
Pyrene 4/14/20200.036 mg/Kg-dry 10.55
Pyridine 4/14/20200.73 mg/Kg-dry 1ND
1,2,4-Trichlorobenzene 4/14/20200.19 mg/Kg-dry 1ND
2,4,5-Trichlorophenol 4/14/20200.19 mg/Kg-dry 1ND
2,4,6-Trichlorophenol 4/14/20200.19 mg/Kg-dry 1ND
PCBs SW8082A (SW3550B) Analyst: GVCPrep Date: 4/14/2020Aroclor 1016 4/14/20200.088 mg/Kg-dry 1ND
Aroclor 1221 4/14/20200.088 mg/Kg-dry 1ND
Aroclor 1232 4/14/20200.088 mg/Kg-dry 1ND
Aroclor 1242 4/14/20200.088 mg/Kg-dry 10.22
Aroclor 1248 4/14/20200.088 mg/Kg-dry 1ND
Qualifiers: J - Analyte detected below quantitation limits
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted recovery limits
ND - Not Detected at the Reporting Limit
E - Value above quantitation range
* - Non-accredited parameter
HT - Sample received past holding time
H - Holding time exceeded
RL - Reporting / Quantitation Limit for the analysis
Page 16 of 44
Project: RH-SET-Chicago, SET Generating Station, 3501 S.
Client Sample ID: RH-413-004
Collection Date: 4/13/2020 12:25:00 PM
Matrix: Soil
Analyses Result Qualifier Units Date AnalyzedRL
Client: Carnow, Conibear, & Associates
Work Order: 20040320
DF
Lab ID: 20040320-004
Date Printed: April 16, 2020
STAT Analysis Corporation2242 West Harrison St., Suite 200, Chicago, IL 60612-3766Tel: (312) 733-0551 Fax: (312) 733-2386 [email protected]
Date Reported: April 16, 2020
Accreditations:IEPA ELAP 100445;ORELAP IL300001;AIHA-LAP, LLC 101160;NVLAP LabCode 101202-0
ANALYTICAL RESULTS
Revision 0
PCBs SW8082A (SW3550B) Analyst: GVCPrep Date: 4/14/2020Aroclor 1254 4/14/20200.088 mg/Kg-dry 10.13
Aroclor 1260 4/14/20200.088 mg/Kg-dry 1ND
Pesticides SW8081B (SW3550B) Analyst: GVCPrep Date: 4/14/20204,4´-DDD 4/14/20200.0018 mg/Kg-dry 1ND
4,4´-DDE 4/14/20200.0018 mg/Kg-dry 1ND
4,4´-DDT 4/14/20200.0018 mg/Kg-dry 1ND
Aldrin 4/14/20200.0018 mg/Kg-dry 1ND
alpha-BHC 4/14/20200.0018 mg/Kg-dry 1ND
alpha-Chlordane 4/14/20200.0018 mg/Kg-dry 1ND
beta-BHC 4/14/20200.0018 mg/Kg-dry 1ND
Chlordane 4/14/20200.018 mg/Kg-dry 1ND
delta-BHC 4/14/20200.0018 mg/Kg-dry 1ND
Dieldrin 4/14/20200.0018 mg/Kg-dry 1ND
Endosulfan I 4/14/20200.0018 mg/Kg-dry 1ND
Endosulfan II 4/14/20200.0018 mg/Kg-dry 1ND
Endosulfan sulfate 4/14/20200.0018 mg/Kg-dry 1ND
Endrin 4/14/20200.0018 mg/Kg-dry 1ND
Endrin aldehyde 4/14/20200.0018 mg/Kg-dry 1ND
Endrin ketone 4/14/20200.0018 mg/Kg-dry 1ND
gamma-BHC 4/14/20200.0018 mg/Kg-dry 1ND
gamma-Chlordane 4/14/20200.0018 mg/Kg-dry 1ND
Heptachlor 4/14/20200.0018 mg/Kg-dry 1ND
Heptachlor epoxide 4/14/20200.0018 mg/Kg-dry 1ND
Methoxychlor 4/14/20200.0018 mg/Kg-dry 1ND
Toxaphene 4/14/20200.036 mg/Kg-dry 1ND
Metals by ICP/MS SW6020A (SW3050B) Analyst: MDTPrep Date: 4/14/2020Aluminum 4/14/202038 mg/Kg-dry 205800
Antimony 4/14/20203.8 mg/Kg-dry 20ND
Arsenic 4/14/20201.9 mg/Kg-dry 203.6
Barium 4/14/20201.9 mg/Kg-dry 20230
Beryllium 4/14/20200.94 mg/Kg-dry 20ND
Cadmium 4/14/20200.94 mg/Kg-dry 204.5
Calcium 4/14/2020560 mg/Kg-dry 100220000
Chromium 4/14/20201.9 mg/Kg-dry 2099
Cobalt 4/14/20201.9 mg/Kg-dry 203.7
Copper 4/14/20204.7 mg/Kg-dry 2023
Iron 4/14/202056 mg/Kg-dry 2012000
Qualifiers: J - Analyte detected below quantitation limits
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted recovery limits
ND - Not Detected at the Reporting Limit
E - Value above quantitation range
* - Non-accredited parameter
HT - Sample received past holding time
H - Holding time exceeded
RL - Reporting / Quantitation Limit for the analysis
Page 17 of 44
Project: RH-SET-Chicago, SET Generating Station, 3501 S.
Client Sample ID: RH-413-004
Collection Date: 4/13/2020 12:25:00 PM
Matrix: Soil
Analyses Result Qualifier Units Date AnalyzedRL
Client: Carnow, Conibear, & Associates
Work Order: 20040320
DF
Lab ID: 20040320-004
Date Printed: April 16, 2020
STAT Analysis Corporation2242 West Harrison St., Suite 200, Chicago, IL 60612-3766Tel: (312) 733-0551 Fax: (312) 733-2386 [email protected]
Date Reported: April 16, 2020
Accreditations:IEPA ELAP 100445;ORELAP IL300001;AIHA-LAP, LLC 101160;NVLAP LabCode 101202-0
ANALYTICAL RESULTS
Revision 0
Metals by ICP/MS SW6020A (SW3050B) Analyst: MDTPrep Date: 4/14/2020Lead 4/14/20200.94 mg/Kg-dry 2097
Magnesium 4/14/202056 mg/Kg-dry 20120000
Manganese 4/14/20201.9 mg/Kg-dry 20470
Nickel 4/14/20201.9 mg/Kg-dry 2012
Potassium 4/14/202056 mg/Kg-dry 20880
Selenium 4/14/20201.9 mg/Kg-dry 20ND
Silver 4/14/20201.9 mg/Kg-dry 20ND
Sodium 4/14/2020110 mg/Kg-dry 201000
Thallium 4/14/20201.9 mg/Kg-dry 20ND
Vanadium 4/14/20201.9 mg/Kg-dry 2015
Zinc 4/14/20209.4 mg/Kg-dry 20200
Mercury SW7471B Analyst: LBPrep Date: 4/14/2020Mercury 4/14/20200.020 mg/Kg-dry 10.076
Cyanide, Total SW9012A Analyst: CABPrep Date: 4/14/2020Cyanide 4/14/20200.28 mg/Kg-dry 1ND
pH (25 °C) SW9045C Analyst: JARPrep Date: 4/13/2020pH 4/13/2020pH Units 111.3
Percent Moisture D2974 Analyst: FNPrep Date: 4/14/2020Percent Moisture * 4/14/20200.2 wt% 19.4
Asbestos Analysis by TEM EPA600/R-93/116 Analyst: RJSPrep Date:Chrysotile 7/13/2020% 11-2
Qualifiers: J - Analyte detected below quantitation limits
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted recovery limits
ND - Not Detected at the Reporting Limit
E - Value above quantitation range
* - Non-accredited parameter
HT - Sample received past holding time
H - Holding time exceeded
RL - Reporting / Quantitation Limit for the analysis
Page 18 of 44
Project: RH-SET-Chicago, SET Generating Station, 3501 S.
Client Sample ID: RH-413-005
Collection Date: 4/13/2020 12:35:00 PM
Matrix: Soil
Analyses Result Qualifier Units Date AnalyzedRL
Client: Carnow, Conibear, & Associates
Work Order: 20040320
DF
Lab ID: 20040320-005
Date Printed: April 16, 2020
STAT Analysis Corporation2242 West Harrison St., Suite 200, Chicago, IL 60612-3766Tel: (312) 733-0551 Fax: (312) 733-2386 [email protected]
Date Reported: April 16, 2020
Accreditations:IEPA ELAP 100445;ORELAP IL300001;AIHA-LAP, LLC 101160;NVLAP LabCode 101202-0
ANALYTICAL RESULTS
Revision 0
Semivolatile Organic Compounds by GC/MS SW8270C (SW3550B) Analyst: DMPrep Date: 4/14/2020Acenaphthene 4/14/20200.036 mg/Kg-dry 1ND
Acenaphthylene 4/14/20200.036 mg/Kg-dry 1ND
Aniline 4/14/20200.36 mg/Kg-dry 1ND
Anthracene 4/14/20200.036 mg/Kg-dry 10.041
Benz(a)anthracene 4/14/20200.036 mg/Kg-dry 10.091
Benzidine 4/14/20200.36 mg/Kg-dry 1ND
Benzo(a)pyrene 4/14/20200.036 mg/Kg-dry 10.071
Benzo(b)fluoranthene 4/14/20200.036 mg/Kg-dry 10.099
Benzo(g,h,i)perylene 4/14/20200.036 mg/Kg-dry 10.051
Benzo(k)fluoranthene 4/14/20200.036 mg/Kg-dry 10.061
Benzoic acid 4/14/20200.89 mg/Kg-dry 1ND
Benzyl alcohol 4/14/20200.18 mg/Kg-dry 1ND
Bis(2-chloroethoxy)methane 4/14/20200.18 mg/Kg-dry 1ND
Bis(2-chloroethyl)ether 4/14/20200.18 mg/Kg-dry 1ND
Bis(2-ethylhexyl)phthalate 4/14/20200.89 mg/Kg-dry 1ND
4-Bromophenyl phenyl ether 4/14/20200.18 mg/Kg-dry 1ND
Butyl benzyl phthalate 4/14/20200.18 mg/Kg-dry 1ND
Carbazole 4/14/20200.18 mg/Kg-dry 1ND
4-Chloroaniline 4/14/20200.18 mg/Kg-dry 1ND
4-Chloro-3-methylphenol 4/14/20200.36 mg/Kg-dry 1ND
2-Chloronaphthalene 4/14/20200.18 mg/Kg-dry 1ND
2-Chlorophenol 4/14/20200.18 mg/Kg-dry 1ND
4-Chlorophenyl phenyl ether 4/14/20200.18 mg/Kg-dry 1ND
Chrysene 4/14/20200.036 mg/Kg-dry 10.14
Dibenz(a,h)anthracene 4/14/20200.036 mg/Kg-dry 1ND
Dibenzofuran 4/14/20200.18 mg/Kg-dry 1ND
1,2-Dichlorobenzene 4/14/20200.18 mg/Kg-dry 1ND
1,3-Dichlorobenzene 4/14/20200.18 mg/Kg-dry 1ND
1,4-Dichlorobenzene 4/14/20200.18 mg/Kg-dry 1ND
3,3´-Dichlorobenzidine 4/14/20200.18 mg/Kg-dry 1ND
2,4-Dichlorophenol 4/14/20200.18 mg/Kg-dry 1ND
Diethyl phthalate 4/14/20200.18 mg/Kg-dry 1ND
2,4-Dimethylphenol 4/14/20200.18 mg/Kg-dry 1ND
Dimethyl phthalate 4/14/20200.18 mg/Kg-dry 1ND
4,6-Dinitro-2-methylphenol 4/14/20200.36 mg/Kg-dry 1ND
2,4-Dinitrophenol 4/14/20200.89 mg/Kg-dry 1ND
2,4-Dinitrotoluene 4/14/20200.036 mg/Kg-dry 1ND
2,6-Dinitrotoluene 4/14/20200.036 mg/Kg-dry 1ND
Qualifiers: J - Analyte detected below quantitation limits
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted recovery limits
ND - Not Detected at the Reporting Limit
E - Value above quantitation range
* - Non-accredited parameter
HT - Sample received past holding time
H - Holding time exceeded
RL - Reporting / Quantitation Limit for the analysis
Page 19 of 44
Project: RH-SET-Chicago, SET Generating Station, 3501 S.
Client Sample ID: RH-413-005
Collection Date: 4/13/2020 12:35:00 PM
Matrix: Soil
Analyses Result Qualifier Units Date AnalyzedRL
Client: Carnow, Conibear, & Associates
Work Order: 20040320
DF
Lab ID: 20040320-005
Date Printed: April 16, 2020
STAT Analysis Corporation2242 West Harrison St., Suite 200, Chicago, IL 60612-3766Tel: (312) 733-0551 Fax: (312) 733-2386 [email protected]
Date Reported: April 16, 2020
Accreditations:IEPA ELAP 100445;ORELAP IL300001;AIHA-LAP, LLC 101160;NVLAP LabCode 101202-0
ANALYTICAL RESULTS
Revision 0
Semivolatile Organic Compounds by GC/MS SW8270C (SW3550B) Analyst: DMPrep Date: 4/14/2020Di-n-butyl phthalate 4/14/20200.18 mg/Kg-dry 1ND
Di-n-octyl phthalate 4/14/20200.18 mg/Kg-dry 1ND
Fluoranthene 4/14/20200.036 mg/Kg-dry 10.26
Fluorene 4/14/20200.036 mg/Kg-dry 1ND
Hexachlorobenzene 4/14/20200.18 mg/Kg-dry 1ND
Hexachlorobutadiene 4/14/20200.18 mg/Kg-dry 1ND
Hexachlorocyclopentadiene 4/14/20200.18 mg/Kg-dry 1ND
Hexachloroethane 4/14/20200.18 mg/Kg-dry 1ND
Indeno(1,2,3-cd)pyrene 4/14/20200.036 mg/Kg-dry 10.045
Isophorone 4/14/20200.18 mg/Kg-dry 1ND
2-Methylnaphthalene 4/14/20200.18 mg/Kg-dry 1ND
2-Methylphenol 4/14/20200.18 mg/Kg-dry 1ND
4-Methylphenol 4/14/20200.18 mg/Kg-dry 1ND
Naphthalene 4/14/20200.036 mg/Kg-dry 1ND
2-Nitroaniline 4/14/20200.18 mg/Kg-dry 1ND
3-Nitroaniline 4/14/20200.18 mg/Kg-dry 1ND
4-Nitroaniline 4/14/20200.18 mg/Kg-dry 1ND
2-Nitrophenol 4/14/20200.18 mg/Kg-dry 1ND
4-Nitrophenol 4/14/20200.36 mg/Kg-dry 1ND
Nitrobenzene 4/14/20200.036 mg/Kg-dry 1ND
N-Nitrosodi-n-propylamine 4/14/20200.036 mg/Kg-dry 1ND
N-Nitrosodimethylamine 4/14/20200.18 mg/Kg-dry 1ND
N-Nitrosodiphenylamine 4/14/20200.18 mg/Kg-dry 1ND
2, 2'-oxybis(1-Chloropropane) 4/14/20200.18 mg/Kg-dry 1ND
Pentachlorophenol 4/14/20200.072 mg/Kg-dry 1ND
Phenanthrene 4/14/20200.036 mg/Kg-dry 10.27
Phenol 4/14/20200.18 mg/Kg-dry 1ND
Pyrene 4/14/20200.036 mg/Kg-dry 10.17
Pyridine 4/14/20200.72 mg/Kg-dry 1ND
1,2,4-Trichlorobenzene 4/14/20200.18 mg/Kg-dry 1ND
2,4,5-Trichlorophenol 4/14/20200.18 mg/Kg-dry 1ND
2,4,6-Trichlorophenol 4/14/20200.18 mg/Kg-dry 1ND
PCBs SW8082A (SW3550B) Analyst: GVCPrep Date: 4/14/2020Aroclor 1016 4/14/20200.085 mg/Kg-dry 1ND
Aroclor 1221 4/14/20200.085 mg/Kg-dry 1ND
Aroclor 1232 4/14/20200.085 mg/Kg-dry 1ND
Aroclor 1242 4/14/20200.085 mg/Kg-dry 1ND
Aroclor 1248 4/14/20200.085 mg/Kg-dry 1ND
Qualifiers: J - Analyte detected below quantitation limits
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted recovery limits
ND - Not Detected at the Reporting Limit
E - Value above quantitation range
* - Non-accredited parameter
HT - Sample received past holding time
H - Holding time exceeded
RL - Reporting / Quantitation Limit for the analysis
Page 20 of 44
Project: RH-SET-Chicago, SET Generating Station, 3501 S.
Client Sample ID: RH-413-005
Collection Date: 4/13/2020 12:35:00 PM
Matrix: Soil
Analyses Result Qualifier Units Date AnalyzedRL
Client: Carnow, Conibear, & Associates
Work Order: 20040320
DF
Lab ID: 20040320-005
Date Printed: April 16, 2020
STAT Analysis Corporation2242 West Harrison St., Suite 200, Chicago, IL 60612-3766Tel: (312) 733-0551 Fax: (312) 733-2386 [email protected]
Date Reported: April 16, 2020
Accreditations:IEPA ELAP 100445;ORELAP IL300001;AIHA-LAP, LLC 101160;NVLAP LabCode 101202-0
ANALYTICAL RESULTS
Revision 0
PCBs SW8082A (SW3550B) Analyst: GVCPrep Date: 4/14/2020Aroclor 1254 4/14/20200.085 mg/Kg-dry 1ND
Aroclor 1260 4/14/20200.085 mg/Kg-dry 1ND
Pesticides SW8081B (SW3550B) Analyst: GVCPrep Date: 4/14/20204,4´-DDD 4/14/20200.0017 mg/Kg-dry 1ND
4,4´-DDE 4/14/20200.0017 mg/Kg-dry 1ND
4,4´-DDT 4/14/20200.0017 mg/Kg-dry 1ND
Aldrin 4/14/20200.0017 mg/Kg-dry 1ND
alpha-BHC 4/14/20200.0017 mg/Kg-dry 1ND
alpha-Chlordane 4/14/20200.0017 mg/Kg-dry 1ND
beta-BHC 4/14/20200.0017 mg/Kg-dry 1ND
Chlordane 4/14/20200.017 mg/Kg-dry 1ND
delta-BHC 4/14/20200.0017 mg/Kg-dry 1ND
Dieldrin 4/14/20200.0017 mg/Kg-dry 1ND
Endosulfan I 4/14/20200.0017 mg/Kg-dry 1ND
Endosulfan II 4/14/20200.0017 mg/Kg-dry 1ND
Endosulfan sulfate 4/14/20200.0017 mg/Kg-dry 1ND
Endrin 4/14/20200.0017 mg/Kg-dry 1ND
Endrin aldehyde 4/14/20200.0017 mg/Kg-dry 1ND
Endrin ketone 4/14/20200.0017 mg/Kg-dry 1ND
gamma-BHC 4/14/20200.0017 mg/Kg-dry 1ND
gamma-Chlordane 4/14/20200.0017 mg/Kg-dry 1ND
Heptachlor 4/14/20200.0017 mg/Kg-dry 1ND
Heptachlor epoxide 4/14/20200.0017 mg/Kg-dry 1ND
Methoxychlor 4/14/20200.0017 mg/Kg-dry 1ND
Toxaphene 4/14/20200.035 mg/Kg-dry 1ND
Metals by ICP/MS SW6020A (SW3050B) Analyst: MDTPrep Date: 4/14/2020Aluminum 4/14/202039 mg/Kg-dry 2010000
Antimony 4/14/20203.9 mg/Kg-dry 20ND
Arsenic 4/14/20201.9 mg/Kg-dry 206.5
Barium 4/14/20201.9 mg/Kg-dry 20250
Beryllium 4/14/20200.97 mg/Kg-dry 201.2
Cadmium 4/14/20200.97 mg/Kg-dry 202.9
Calcium 4/14/2020120 mg/Kg-dry 20200000
Chromium 4/14/20201.9 mg/Kg-dry 2027
Cobalt 4/14/20201.9 mg/Kg-dry 204.3
Copper 4/14/20204.8 mg/Kg-dry 2042
Iron 4/14/202058 mg/Kg-dry 2026000
Qualifiers: J - Analyte detected below quantitation limits
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted recovery limits
ND - Not Detected at the Reporting Limit
E - Value above quantitation range
* - Non-accredited parameter
HT - Sample received past holding time
H - Holding time exceeded
RL - Reporting / Quantitation Limit for the analysis
Page 21 of 44
Project: RH-SET-Chicago, SET Generating Station, 3501 S.
Client Sample ID: RH-413-005
Collection Date: 4/13/2020 12:35:00 PM
Matrix: Soil
Analyses Result Qualifier Units Date AnalyzedRL
Client: Carnow, Conibear, & Associates
Work Order: 20040320
DF
Lab ID: 20040320-005
Date Printed: April 16, 2020
STAT Analysis Corporation2242 West Harrison St., Suite 200, Chicago, IL 60612-3766Tel: (312) 733-0551 Fax: (312) 733-2386 [email protected]
Date Reported: April 16, 2020
Accreditations:IEPA ELAP 100445;ORELAP IL300001;AIHA-LAP, LLC 101160;NVLAP LabCode 101202-0
ANALYTICAL RESULTS
Revision 0
Metals by ICP/MS SW6020A (SW3050B) Analyst: MDTPrep Date: 4/14/2020Lead 4/14/20200.97 mg/Kg-dry 20510
Magnesium 4/14/202058 mg/Kg-dry 2055000
Manganese 4/14/20201.9 mg/Kg-dry 201200
Nickel 4/14/20201.9 mg/Kg-dry 2017
Potassium 4/14/202058 mg/Kg-dry 201100
Selenium 4/14/20201.9 mg/Kg-dry 20ND
Silver 4/14/20201.9 mg/Kg-dry 20ND
Sodium 4/14/2020120 mg/Kg-dry 20800
Thallium 4/14/20201.9 mg/Kg-dry 20ND
Vanadium 4/14/20201.9 mg/Kg-dry 2013
Zinc 4/14/20209.7 mg/Kg-dry 20410
Mercury SW7471B Analyst: LBPrep Date: 4/14/2020Mercury 4/14/20200.018 mg/Kg-dry 10.095
Cyanide, Total SW9012A Analyst: CABPrep Date: 4/14/2020Cyanide 4/14/20200.27 mg/Kg-dry 10.43
pH (25 °C) SW9045C Analyst: JARPrep Date: 4/13/2020pH 4/13/2020pH Units 111.6
Percent Moisture D2974 Analyst: FNPrep Date: 4/14/2020Percent Moisture * 4/14/20200.2 wt% 18.6
Asbestos Analysis by TEM EPA600/R-93/116 Analyst: RJSPrep Date:Chrysotile 7/13/2020% 11-2
Qualifiers: J - Analyte detected below quantitation limits
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted recovery limits
ND - Not Detected at the Reporting Limit
E - Value above quantitation range
* - Non-accredited parameter
HT - Sample received past holding time
H - Holding time exceeded
RL - Reporting / Quantitation Limit for the analysis
Page 22 of 44
Project: RH-SET-Chicago, SET Generating Station, 3501 S.
Client Sample ID: RH-413-006
Collection Date: 4/13/2020 12:45:00 PM
Matrix: Soil
Analyses Result Qualifier Units Date AnalyzedRL
Client: Carnow, Conibear, & Associates
Work Order: 20040320
DF
Lab ID: 20040320-006
Date Printed: April 16, 2020
STAT Analysis Corporation2242 West Harrison St., Suite 200, Chicago, IL 60612-3766Tel: (312) 733-0551 Fax: (312) 733-2386 [email protected]
Date Reported: April 16, 2020
Accreditations:IEPA ELAP 100445;ORELAP IL300001;AIHA-LAP, LLC 101160;NVLAP LabCode 101202-0
ANALYTICAL RESULTS
Revision 0
Semivolatile Organic Compounds by GC/MS SW8270C (SW3550B) Analyst: TEMPrep Date: 4/14/2020Acenaphthene 4/14/20200.18 mg/Kg-dry 1ND
Acenaphthylene 4/14/20200.18 mg/Kg-dry 1ND
Aniline 4/14/20201.8 mg/Kg-dry 1ND
Anthracene 4/14/20200.18 mg/Kg-dry 10.30
Benz(a)anthracene 4/14/20200.18 mg/Kg-dry 10.62
Benzidine 4/14/20201.8 mg/Kg-dry 1ND
Benzo(a)pyrene 4/14/20200.18 mg/Kg-dry 10.51
Benzo(b)fluoranthene 4/14/20200.18 mg/Kg-dry 10.54
Benzo(g,h,i)perylene 4/14/20200.18 mg/Kg-dry 10.34
Benzo(k)fluoranthene 4/14/20200.18 mg/Kg-dry 10.45
Benzoic acid 4/14/20204.5 mg/Kg-dry 1ND
Benzyl alcohol 4/14/20200.93 mg/Kg-dry 1ND
Bis(2-chloroethoxy)methane 4/14/20200.93 mg/Kg-dry 1ND
Bis(2-chloroethyl)ether 4/14/20200.93 mg/Kg-dry 1ND
Bis(2-ethylhexyl)phthalate 4/14/20204.5 mg/Kg-dry 1ND
4-Bromophenyl phenyl ether 4/14/20200.93 mg/Kg-dry 1ND
Butyl benzyl phthalate 4/14/20200.93 mg/Kg-dry 1ND
Carbazole 4/14/20200.93 mg/Kg-dry 1ND
4-Chloroaniline 4/14/20200.93 mg/Kg-dry 1ND
4-Chloro-3-methylphenol 4/14/20201.8 mg/Kg-dry 1ND
2-Chloronaphthalene 4/14/20200.93 mg/Kg-dry 1ND
2-Chlorophenol 4/14/20200.93 mg/Kg-dry 1ND
4-Chlorophenyl phenyl ether 4/14/20200.93 mg/Kg-dry 1ND
Chrysene 4/14/20200.18 mg/Kg-dry 10.74
Dibenz(a,h)anthracene 4/14/20200.18 mg/Kg-dry 1ND
Dibenzofuran 4/14/20200.93 mg/Kg-dry 1ND
1,2-Dichlorobenzene 4/14/20200.93 mg/Kg-dry 1ND
1,3-Dichlorobenzene 4/14/20200.93 mg/Kg-dry 1ND
1,4-Dichlorobenzene 4/14/20200.93 mg/Kg-dry 1ND
3,3´-Dichlorobenzidine 4/14/20200.93 mg/Kg-dry 1ND
2,4-Dichlorophenol 4/14/20200.93 mg/Kg-dry 1ND
Diethyl phthalate 4/14/20200.93 mg/Kg-dry 1ND
2,4-Dimethylphenol 4/14/20200.93 mg/Kg-dry 1ND
Dimethyl phthalate 4/14/20200.93 mg/Kg-dry 1ND
4,6-Dinitro-2-methylphenol 4/14/20201.8 mg/Kg-dry 1ND
2,4-Dinitrophenol 4/14/20204.5 mg/Kg-dry 1ND
2,4-Dinitrotoluene 4/14/20200.18 mg/Kg-dry 1ND
2,6-Dinitrotoluene 4/14/20200.18 mg/Kg-dry 1ND
Qualifiers: J - Analyte detected below quantitation limits
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted recovery limits
ND - Not Detected at the Reporting Limit
E - Value above quantitation range
* - Non-accredited parameter
HT - Sample received past holding time
H - Holding time exceeded
RL - Reporting / Quantitation Limit for the analysis
Page 23 of 44
Project: RH-SET-Chicago, SET Generating Station, 3501 S.
Client Sample ID: RH-413-006
Collection Date: 4/13/2020 12:45:00 PM
Matrix: Soil
Analyses Result Qualifier Units Date AnalyzedRL
Client: Carnow, Conibear, & Associates
Work Order: 20040320
DF
Lab ID: 20040320-006
Date Printed: April 16, 2020
STAT Analysis Corporation2242 West Harrison St., Suite 200, Chicago, IL 60612-3766Tel: (312) 733-0551 Fax: (312) 733-2386 [email protected]
Date Reported: April 16, 2020
Accreditations:IEPA ELAP 100445;ORELAP IL300001;AIHA-LAP, LLC 101160;NVLAP LabCode 101202-0
ANALYTICAL RESULTS
Revision 0
Semivolatile Organic Compounds by GC/MS SW8270C (SW3550B) Analyst: TEMPrep Date: 4/14/2020Di-n-butyl phthalate 4/14/20200.93 mg/Kg-dry 1ND
Di-n-octyl phthalate 4/14/20200.93 mg/Kg-dry 1ND
Fluoranthene 4/14/20200.18 mg/Kg-dry 11.5
Fluorene 4/14/20200.18 mg/Kg-dry 1ND
Hexachlorobenzene 4/14/20200.93 mg/Kg-dry 1ND
Hexachlorobutadiene 4/14/20200.93 mg/Kg-dry 1ND
Hexachlorocyclopentadiene 4/14/20200.93 mg/Kg-dry 1ND
Hexachloroethane 4/14/20200.93 mg/Kg-dry 1ND
Indeno(1,2,3-cd)pyrene 4/14/20200.18 mg/Kg-dry 10.26
Isophorone 4/14/20200.93 mg/Kg-dry 1ND
2-Methylnaphthalene 4/14/20200.93 mg/Kg-dry 1ND
2-Methylphenol 4/14/20200.93 mg/Kg-dry 1ND
4-Methylphenol 4/14/20200.93 mg/Kg-dry 1ND
Naphthalene 4/14/20200.18 mg/Kg-dry 1ND
2-Nitroaniline 4/14/20200.93 mg/Kg-dry 1ND
3-Nitroaniline 4/14/20200.93 mg/Kg-dry 1ND
4-Nitroaniline 4/14/20200.93 mg/Kg-dry 1ND
2-Nitrophenol 4/14/20200.93 mg/Kg-dry 1ND
4-Nitrophenol 4/14/20201.8 mg/Kg-dry 1ND
Nitrobenzene 4/14/20200.18 mg/Kg-dry 1ND
N-Nitrosodi-n-propylamine 4/14/20200.18 mg/Kg-dry 1ND
N-Nitrosodimethylamine 4/14/20200.93 mg/Kg-dry 1ND
N-Nitrosodiphenylamine 4/14/20200.93 mg/Kg-dry 1ND
2, 2'-oxybis(1-Chloropropane) 4/14/20200.93 mg/Kg-dry 1ND
Pentachlorophenol 4/14/20200.37 mg/Kg-dry 1ND
Phenanthrene 4/14/20200.18 mg/Kg-dry 11.3
Phenol 4/14/20200.93 mg/Kg-dry 1ND
Pyrene 4/14/20200.18 mg/Kg-dry 11.2
Pyridine 4/14/20203.7 mg/Kg-dry 1ND
1,2,4-Trichlorobenzene 4/14/20200.93 mg/Kg-dry 1ND
2,4,5-Trichlorophenol 4/14/20200.93 mg/Kg-dry 1ND
2,4,6-Trichlorophenol 4/14/20200.93 mg/Kg-dry 1ND
PCBs SW8082A (SW3550B) Analyst: GVCPrep Date: 4/14/2020Aroclor 1016 4/14/20200.088 mg/Kg-dry 1ND
Aroclor 1221 4/14/20200.088 mg/Kg-dry 1ND
Aroclor 1232 4/14/20200.088 mg/Kg-dry 1ND
Aroclor 1242 4/14/20200.088 mg/Kg-dry 1ND
Aroclor 1248 4/14/20200.088 mg/Kg-dry 1ND
Qualifiers: J - Analyte detected below quantitation limits
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted recovery limits
ND - Not Detected at the Reporting Limit
E - Value above quantitation range
* - Non-accredited parameter
HT - Sample received past holding time
H - Holding time exceeded
RL - Reporting / Quantitation Limit for the analysis
Page 24 of 44
Project: RH-SET-Chicago, SET Generating Station, 3501 S.
Client Sample ID: RH-413-006
Collection Date: 4/13/2020 12:45:00 PM
Matrix: Soil
Analyses Result Qualifier Units Date AnalyzedRL
Client: Carnow, Conibear, & Associates
Work Order: 20040320
DF
Lab ID: 20040320-006
Date Printed: April 16, 2020
STAT Analysis Corporation2242 West Harrison St., Suite 200, Chicago, IL 60612-3766Tel: (312) 733-0551 Fax: (312) 733-2386 [email protected]
Date Reported: April 16, 2020
Accreditations:IEPA ELAP 100445;ORELAP IL300001;AIHA-LAP, LLC 101160;NVLAP LabCode 101202-0
ANALYTICAL RESULTS
Revision 0
PCBs SW8082A (SW3550B) Analyst: GVCPrep Date: 4/14/2020Aroclor 1254 4/14/20200.088 mg/Kg-dry 1ND
Aroclor 1260 4/14/20200.088 mg/Kg-dry 1ND
Pesticides SW8081B (SW3550B) Analyst: GVCPrep Date: 4/14/20204,4´-DDD 4/14/20200.0018 mg/Kg-dry 1ND
4,4´-DDE 4/14/20200.0018 mg/Kg-dry 1ND
4,4´-DDT 4/14/20200.0018 mg/Kg-dry 1ND
Aldrin 4/14/20200.0018 mg/Kg-dry 1ND
alpha-BHC 4/14/20200.0018 mg/Kg-dry 1ND
alpha-Chlordane 4/14/20200.0018 mg/Kg-dry 1ND
beta-BHC 4/14/20200.0018 mg/Kg-dry 1ND
Chlordane 4/14/20200.018 mg/Kg-dry 1ND
delta-BHC 4/14/20200.0018 mg/Kg-dry 1ND
Dieldrin 4/14/20200.0018 mg/Kg-dry 1ND
Endosulfan I 4/14/20200.0018 mg/Kg-dry 1ND
Endosulfan II 4/14/20200.0018 mg/Kg-dry 1ND
Endosulfan sulfate 4/14/20200.0018 mg/Kg-dry 1ND
Endrin 4/14/20200.0018 mg/Kg-dry 1ND
Endrin aldehyde 4/14/20200.0018 mg/Kg-dry 1ND
Endrin ketone 4/14/20200.0018 mg/Kg-dry 1ND
gamma-BHC 4/14/20200.0018 mg/Kg-dry 1ND
gamma-Chlordane 4/14/20200.0018 mg/Kg-dry 1ND
Heptachlor 4/14/20200.0018 mg/Kg-dry 1ND
Heptachlor epoxide 4/14/20200.0018 mg/Kg-dry 1ND
Methoxychlor 4/14/20200.0018 mg/Kg-dry 1ND
Toxaphene 4/14/20200.036 mg/Kg-dry 1ND
Metals by ICP/MS SW6020A (SW3050B) Analyst: MDTPrep Date: 4/14/2020Aluminum 4/14/202040 mg/Kg-dry 2013000
Antimony 4/14/20204.0 mg/Kg-dry 20ND
Arsenic 4/14/20202.0 mg/Kg-dry 208.3
Barium 4/14/20202.0 mg/Kg-dry 20240
Beryllium 4/14/20200.99 mg/Kg-dry 201.1
Cadmium 4/14/20200.99 mg/Kg-dry 202.3
Calcium 4/14/2020120 mg/Kg-dry 20160000
Chromium 4/14/20202.0 mg/Kg-dry 2028
Cobalt 4/14/20202.0 mg/Kg-dry 205.2
Copper 4/14/20205.0 mg/Kg-dry 2076
Iron 4/14/202059 mg/Kg-dry 2029000
Qualifiers: J - Analyte detected below quantitation limits
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted recovery limits
ND - Not Detected at the Reporting Limit
E - Value above quantitation range
* - Non-accredited parameter
HT - Sample received past holding time
H - Holding time exceeded
RL - Reporting / Quantitation Limit for the analysis
Page 25 of 44
Project: RH-SET-Chicago, SET Generating Station, 3501 S.
Client Sample ID: RH-413-006
Collection Date: 4/13/2020 12:45:00 PM
Matrix: Soil
Analyses Result Qualifier Units Date AnalyzedRL
Client: Carnow, Conibear, & Associates
Work Order: 20040320
DF
Lab ID: 20040320-006
Date Printed: April 16, 2020
STAT Analysis Corporation2242 West Harrison St., Suite 200, Chicago, IL 60612-3766Tel: (312) 733-0551 Fax: (312) 733-2386 [email protected]
Date Reported: April 16, 2020
Accreditations:IEPA ELAP 100445;ORELAP IL300001;AIHA-LAP, LLC 101160;NVLAP LabCode 101202-0
ANALYTICAL RESULTS
Revision 0
Metals by ICP/MS SW6020A (SW3050B) Analyst: MDTPrep Date: 4/14/2020Lead 4/14/20200.99 mg/Kg-dry 20180
Magnesium 4/14/202059 mg/Kg-dry 2042000
Manganese 4/14/20202.0 mg/Kg-dry 201000
Nickel 4/14/20202.0 mg/Kg-dry 2021
Potassium 4/14/202059 mg/Kg-dry 201600
Selenium 4/14/20202.0 mg/Kg-dry 20ND
Silver 4/14/20202.0 mg/Kg-dry 20ND
Sodium 4/14/2020120 mg/Kg-dry 201100
Thallium 4/14/20202.0 mg/Kg-dry 20ND
Vanadium 4/14/20202.0 mg/Kg-dry 2019
Zinc 4/14/20209.9 mg/Kg-dry 20800
Mercury SW7471B Analyst: LBPrep Date: 4/14/2020Mercury 4/14/20200.019 mg/Kg-dry 10.11
Cyanide, Total SW9012A Analyst: CABPrep Date: 4/14/2020Cyanide 4/14/20200.28 mg/Kg-dry 1ND
pH (25 °C) SW9045C Analyst: JARPrep Date: 4/13/2020pH 4/13/2020pH Units 111.0
Percent Moisture D2974 Analyst: FNPrep Date: 4/14/2020Percent Moisture * 4/14/20200.2 wt% 19.7
Asbestos Analysis by TEM EPA600/R-93/116 Analyst: RJSPrep Date:Chrysotile 7/13/2020% 1<1
Qualifiers: J - Analyte detected below quantitation limits
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted recovery limits
ND - Not Detected at the Reporting Limit
E - Value above quantitation range
* - Non-accredited parameter
HT - Sample received past holding time
H - Holding time exceeded
RL - Reporting / Quantitation Limit for the analysis
Page 26 of 44
Project: RH-SET-Chicago, SET Generating Station, 3501 S.
Client Sample ID: RH-413-007
Collection Date: 4/13/2020 12:55:00 PM
Matrix: Soil
Analyses Result Qualifier Units Date AnalyzedRL
Client: Carnow, Conibear, & Associates
Work Order: 20040320
DF
Lab ID: 20040320-007
Date Printed: April 16, 2020
STAT Analysis Corporation2242 West Harrison St., Suite 200, Chicago, IL 60612-3766Tel: (312) 733-0551 Fax: (312) 733-2386 [email protected]
Date Reported: April 16, 2020
Accreditations:IEPA ELAP 100445;ORELAP IL300001;AIHA-LAP, LLC 101160;NVLAP LabCode 101202-0
ANALYTICAL RESULTS
Revision 0
Semivolatile Organic Compounds by GC/MS SW8270C (SW3550B) Analyst: TEMPrep Date: 4/14/2020Acenaphthene 4/14/20200.039 mg/Kg-dry 10.16
Acenaphthylene 4/14/20200.039 mg/Kg-dry 1ND
Aniline 4/14/20200.40 mg/Kg-dry 1ND
Anthracene 4/14/20200.039 mg/Kg-dry 10.26
Benz(a)anthracene 4/14/20200.039 mg/Kg-dry 10.48
Benzidine 4/14/20200.39 mg/Kg-dry 1ND
Benzo(a)pyrene 4/14/20200.039 mg/Kg-dry 10.36
Benzo(b)fluoranthene 4/14/20200.039 mg/Kg-dry 10.34
Benzo(g,h,i)perylene 4/14/20200.039 mg/Kg-dry 10.24
Benzo(k)fluoranthene 4/14/20200.039 mg/Kg-dry 10.34
Benzoic acid 4/14/20200.99 mg/Kg-dry 1ND
Benzyl alcohol 4/14/20200.20 mg/Kg-dry 1ND
Bis(2-chloroethoxy)methane 4/14/20200.20 mg/Kg-dry 1ND
Bis(2-chloroethyl)ether 4/14/20200.20 mg/Kg-dry 1ND
Bis(2-ethylhexyl)phthalate 4/14/20200.99 mg/Kg-dry 1ND
4-Bromophenyl phenyl ether 4/14/20200.20 mg/Kg-dry 1ND
Butyl benzyl phthalate 4/14/20200.20 mg/Kg-dry 1ND
Carbazole 4/14/20200.20 mg/Kg-dry 1ND
4-Chloroaniline 4/14/20200.20 mg/Kg-dry 1ND
4-Chloro-3-methylphenol 4/14/20200.39 mg/Kg-dry 1ND
2-Chloronaphthalene 4/14/20200.20 mg/Kg-dry 1ND
2-Chlorophenol 4/14/20200.20 mg/Kg-dry 1ND
4-Chlorophenyl phenyl ether 4/14/20200.20 mg/Kg-dry 1ND
Chrysene 4/14/20200.039 mg/Kg-dry 10.53
Dibenz(a,h)anthracene 4/14/20200.039 mg/Kg-dry 10.13
Dibenzofuran 4/14/20200.20 mg/Kg-dry 1ND
1,2-Dichlorobenzene 4/14/20200.20 mg/Kg-dry 1ND
1,3-Dichlorobenzene 4/14/20200.20 mg/Kg-dry 1ND
1,4-Dichlorobenzene 4/14/20200.20 mg/Kg-dry 1ND
3,3´-Dichlorobenzidine 4/14/20200.20 mg/Kg-dry 1ND
2,4-Dichlorophenol 4/14/20200.20 mg/Kg-dry 1ND
Diethyl phthalate 4/14/20200.20 mg/Kg-dry 1ND
2,4-Dimethylphenol 4/14/20200.20 mg/Kg-dry 1ND
Dimethyl phthalate 4/14/20200.20 mg/Kg-dry 1ND
4,6-Dinitro-2-methylphenol 4/14/20200.39 mg/Kg-dry 1ND
2,4-Dinitrophenol 4/14/20200.99 mg/Kg-dry 1ND
2,4-Dinitrotoluene 4/14/20200.039 mg/Kg-dry 1ND
2,6-Dinitrotoluene 4/14/20200.039 mg/Kg-dry 1ND
Qualifiers: J - Analyte detected below quantitation limits
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted recovery limits
ND - Not Detected at the Reporting Limit
E - Value above quantitation range
* - Non-accredited parameter
HT - Sample received past holding time
H - Holding time exceeded
RL - Reporting / Quantitation Limit for the analysis
Page 27 of 44
Project: RH-SET-Chicago, SET Generating Station, 3501 S.
Client Sample ID: RH-413-007
Collection Date: 4/13/2020 12:55:00 PM
Matrix: Soil
Analyses Result Qualifier Units Date AnalyzedRL
Client: Carnow, Conibear, & Associates
Work Order: 20040320
DF
Lab ID: 20040320-007
Date Printed: April 16, 2020
STAT Analysis Corporation2242 West Harrison St., Suite 200, Chicago, IL 60612-3766Tel: (312) 733-0551 Fax: (312) 733-2386 [email protected]
Date Reported: April 16, 2020
Accreditations:IEPA ELAP 100445;ORELAP IL300001;AIHA-LAP, LLC 101160;NVLAP LabCode 101202-0
ANALYTICAL RESULTS
Revision 0
Semivolatile Organic Compounds by GC/MS SW8270C (SW3550B) Analyst: TEMPrep Date: 4/14/2020Di-n-butyl phthalate 4/14/20200.20 mg/Kg-dry 1ND
Di-n-octyl phthalate 4/14/20200.20 mg/Kg-dry 1ND
Fluoranthene 4/14/20200.039 mg/Kg-dry 11.2
Fluorene 4/14/20200.039 mg/Kg-dry 10.14
Hexachlorobenzene 4/14/20200.20 mg/Kg-dry 1ND
Hexachlorobutadiene 4/14/20200.20 mg/Kg-dry 1ND
Hexachlorocyclopentadiene 4/14/20200.20 mg/Kg-dry 1ND
Hexachloroethane 4/14/20200.20 mg/Kg-dry 1ND
Indeno(1,2,3-cd)pyrene 4/14/20200.039 mg/Kg-dry 10.19
Isophorone 4/14/20200.20 mg/Kg-dry 1ND
2-Methylnaphthalene 4/14/20200.20 mg/Kg-dry 1ND
2-Methylphenol 4/14/20200.20 mg/Kg-dry 1ND
4-Methylphenol 4/14/20200.20 mg/Kg-dry 1ND
Naphthalene 4/14/20200.039 mg/Kg-dry 10.045
2-Nitroaniline 4/14/20200.20 mg/Kg-dry 1ND
3-Nitroaniline 4/14/20200.20 mg/Kg-dry 1ND
4-Nitroaniline 4/14/20200.20 mg/Kg-dry 1ND
2-Nitrophenol 4/14/20200.20 mg/Kg-dry 1ND
4-Nitrophenol 4/14/20200.39 mg/Kg-dry 1ND
Nitrobenzene 4/14/20200.039 mg/Kg-dry 1ND
N-Nitrosodi-n-propylamine 4/14/20200.039 mg/Kg-dry 1ND
N-Nitrosodimethylamine 4/14/20200.20 mg/Kg-dry 1ND
N-Nitrosodiphenylamine 4/14/20200.20 mg/Kg-dry 1ND
2, 2'-oxybis(1-Chloropropane) 4/14/20200.20 mg/Kg-dry 1ND
Pentachlorophenol 4/14/20200.080 mg/Kg-dry 1ND
Phenanthrene 4/14/20200.039 mg/Kg-dry 11.2
Phenol 4/14/20200.20 mg/Kg-dry 1ND
Pyrene 4/14/20200.039 mg/Kg-dry 10.98
Pyridine 4/14/20200.80 mg/Kg-dry 1ND
1,2,4-Trichlorobenzene 4/14/20200.20 mg/Kg-dry 1ND
2,4,5-Trichlorophenol 4/14/20200.20 mg/Kg-dry 1ND
2,4,6-Trichlorophenol 4/14/20200.20 mg/Kg-dry 1ND
PCBs SW8082A (SW3550B) Analyst: GVCPrep Date: 4/14/2020Aroclor 1016 4/14/20200.094 mg/Kg-dry 1ND
Aroclor 1221 4/14/20200.094 mg/Kg-dry 1ND
Aroclor 1232 4/14/20200.094 mg/Kg-dry 1ND
Aroclor 1242 4/14/20200.094 mg/Kg-dry 1ND
Aroclor 1248 4/14/20200.094 mg/Kg-dry 1ND
Qualifiers: J - Analyte detected below quantitation limits
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted recovery limits
ND - Not Detected at the Reporting Limit
E - Value above quantitation range
* - Non-accredited parameter
HT - Sample received past holding time
H - Holding time exceeded
RL - Reporting / Quantitation Limit for the analysis
Page 28 of 44
Project: RH-SET-Chicago, SET Generating Station, 3501 S.
Client Sample ID: RH-413-007
Collection Date: 4/13/2020 12:55:00 PM
Matrix: Soil
Analyses Result Qualifier Units Date AnalyzedRL
Client: Carnow, Conibear, & Associates
Work Order: 20040320
DF
Lab ID: 20040320-007
Date Printed: April 16, 2020
STAT Analysis Corporation2242 West Harrison St., Suite 200, Chicago, IL 60612-3766Tel: (312) 733-0551 Fax: (312) 733-2386 [email protected]
Date Reported: April 16, 2020
Accreditations:IEPA ELAP 100445;ORELAP IL300001;AIHA-LAP, LLC 101160;NVLAP LabCode 101202-0
ANALYTICAL RESULTS
Revision 0
PCBs SW8082A (SW3550B) Analyst: GVCPrep Date: 4/14/2020Aroclor 1254 4/14/20200.094 mg/Kg-dry 1ND
Aroclor 1260 4/14/20200.094 mg/Kg-dry 1ND
Pesticides SW8081B (SW3550B) Analyst: GVCPrep Date: 4/14/20204,4´-DDD 4/14/20200.0019 mg/Kg-dry 1ND
4,4´-DDE 4/14/20200.0019 mg/Kg-dry 1ND
4,4´-DDT 4/14/20200.0019 mg/Kg-dry 1ND
Aldrin 4/14/20200.0019 mg/Kg-dry 1ND
alpha-BHC 4/14/20200.0019 mg/Kg-dry 1ND
alpha-Chlordane 4/14/20200.0019 mg/Kg-dry 1ND
beta-BHC 4/14/20200.0019 mg/Kg-dry 1ND
Chlordane 4/14/20200.019 mg/Kg-dry 1ND
delta-BHC 4/14/20200.0019 mg/Kg-dry 1ND
Dieldrin 4/14/20200.0019 mg/Kg-dry 1ND
Endosulfan I 4/14/20200.0019 mg/Kg-dry 1ND
Endosulfan II 4/14/20200.0019 mg/Kg-dry 1ND
Endosulfan sulfate 4/14/20200.0019 mg/Kg-dry 1ND
Endrin 4/14/20200.0019 mg/Kg-dry 1ND
Endrin aldehyde 4/14/20200.0019 mg/Kg-dry 1ND
Endrin ketone 4/14/20200.0019 mg/Kg-dry 1ND
gamma-BHC 4/14/20200.0019 mg/Kg-dry 1ND
gamma-Chlordane 4/14/20200.0019 mg/Kg-dry 1ND
Heptachlor 4/14/20200.0019 mg/Kg-dry 1ND
Heptachlor epoxide 4/14/20200.0019 mg/Kg-dry 1ND
Methoxychlor 4/14/20200.0019 mg/Kg-dry 1ND
Toxaphene 4/14/20200.039 mg/Kg-dry 1ND
Metals by ICP/MS SW6020A (SW3050B) Analyst: MDTPrep Date: 4/14/2020Aluminum 4/14/202043 mg/Kg-dry 2011000
Antimony 4/14/20204.3 mg/Kg-dry 20ND
Arsenic 4/14/20202.2 mg/Kg-dry 207.1
Barium 4/14/20202.2 mg/Kg-dry 20340
Beryllium 4/14/20201.1 mg/Kg-dry 20ND
Cadmium 4/14/20201.1 mg/Kg-dry 202.6
Calcium 4/14/2020130 mg/Kg-dry 20180000
Chromium 4/14/20202.2 mg/Kg-dry 2029
Cobalt 4/14/20202.2 mg/Kg-dry 204.5
Copper 4/14/20205.4 mg/Kg-dry 2070
Iron 4/14/202065 mg/Kg-dry 2020000
Qualifiers: J - Analyte detected below quantitation limits
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted recovery limits
ND - Not Detected at the Reporting Limit
E - Value above quantitation range
* - Non-accredited parameter
HT - Sample received past holding time
H - Holding time exceeded
RL - Reporting / Quantitation Limit for the analysis
Page 29 of 44
Project: RH-SET-Chicago, SET Generating Station, 3501 S.
Client Sample ID: RH-413-007
Collection Date: 4/13/2020 12:55:00 PM
Matrix: Soil
Analyses Result Qualifier Units Date AnalyzedRL
Client: Carnow, Conibear, & Associates
Work Order: 20040320
DF
Lab ID: 20040320-007
Date Printed: April 16, 2020
STAT Analysis Corporation2242 West Harrison St., Suite 200, Chicago, IL 60612-3766Tel: (312) 733-0551 Fax: (312) 733-2386 [email protected]
Date Reported: April 16, 2020
Accreditations:IEPA ELAP 100445;ORELAP IL300001;AIHA-LAP, LLC 101160;NVLAP LabCode 101202-0
ANALYTICAL RESULTS
Revision 0
Metals by ICP/MS SW6020A (SW3050B) Analyst: MDTPrep Date: 4/14/2020Lead 4/14/20201.1 mg/Kg-dry 20250
Magnesium 4/14/202065 mg/Kg-dry 2072000
Manganese 4/14/20202.2 mg/Kg-dry 20750
Nickel 4/14/20202.2 mg/Kg-dry 2018
Potassium 4/14/202065 mg/Kg-dry 201400
Selenium 4/14/20202.2 mg/Kg-dry 20ND
Silver 4/14/20202.2 mg/Kg-dry 20ND
Sodium 4/14/2020130 mg/Kg-dry 201400
Thallium 4/14/20202.2 mg/Kg-dry 20ND
Vanadium 4/14/20202.2 mg/Kg-dry 2020
Zinc 4/14/202011 mg/Kg-dry 20310
Mercury SW7471B Analyst: LBPrep Date: 4/14/2020Mercury 4/14/20200.023 mg/Kg-dry 10.16
Cyanide, Total SW9012A Analyst: CABPrep Date: 4/14/2020Cyanide 4/14/20200.29 mg/Kg-dry 10.38
pH (25 °C) SW9045C Analyst: JARPrep Date: 4/13/2020pH 4/13/2020pH Units 110.8
Percent Moisture D2974 Analyst: FNPrep Date: 4/14/2020Percent Moisture * 4/14/20200.2 wt% 116.3
Asbestos Analysis by TEM EPA600/R-93/116 Analyst: RJSPrep Date:Chrysotile 7/13/2020% 1<1
Qualifiers: J - Analyte detected below quantitation limits
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted recovery limits
ND - Not Detected at the Reporting Limit
E - Value above quantitation range
* - Non-accredited parameter
HT - Sample received past holding time
H - Holding time exceeded
RL - Reporting / Quantitation Limit for the analysis
Page 30 of 44
Project: RH-SET-Chicago, SET Generating Station, 3501 S.
Client Sample ID: RH-413-008
Collection Date: 4/13/2020 1:00:00 PM
Matrix: Soil
Analyses Result Qualifier Units Date AnalyzedRL
Client: Carnow, Conibear, & Associates
Work Order: 20040320
DF
Lab ID: 20040320-008
Date Printed: April 16, 2020
STAT Analysis Corporation2242 West Harrison St., Suite 200, Chicago, IL 60612-3766Tel: (312) 733-0551 Fax: (312) 733-2386 [email protected]
Date Reported: April 16, 2020
Accreditations:IEPA ELAP 100445;ORELAP IL300001;AIHA-LAP, LLC 101160;NVLAP LabCode 101202-0
ANALYTICAL RESULTS
Revision 0
Semivolatile Organic Compounds by GC/MS SW8270C (SW3550B) Analyst: TEMPrep Date: 4/14/2020Acenaphthene 4/14/20200.043 mg/Kg-dry 10.25
Acenaphthylene 4/14/20200.043 mg/Kg-dry 1ND
Aniline 4/14/20200.43 mg/Kg-dry 1ND
Anthracene 4/14/20200.043 mg/Kg-dry 10.50
Benz(a)anthracene 4/14/20200.043 mg/Kg-dry 10.99
Benzidine 4/14/20200.43 mg/Kg-dry 1ND
Benzo(a)pyrene 4/14/20200.043 mg/Kg-dry 10.70
Benzo(b)fluoranthene 4/14/20200.043 mg/Kg-dry 10.84
Benzo(g,h,i)perylene 4/14/20200.043 mg/Kg-dry 10.48
Benzo(k)fluoranthene 4/14/20200.043 mg/Kg-dry 10.59
Benzoic acid 4/14/20201.1 mg/Kg-dry 1ND
Benzyl alcohol 4/14/20200.22 mg/Kg-dry 1ND
Bis(2-chloroethoxy)methane 4/14/20200.22 mg/Kg-dry 1ND
Bis(2-chloroethyl)ether 4/14/20200.22 mg/Kg-dry 1ND
Bis(2-ethylhexyl)phthalate 4/14/20201.1 mg/Kg-dry 1ND
4-Bromophenyl phenyl ether 4/14/20200.22 mg/Kg-dry 1ND
Butyl benzyl phthalate 4/14/20200.22 mg/Kg-dry 1ND
Carbazole 4/14/20200.22 mg/Kg-dry 10.28
4-Chloroaniline 4/14/20200.22 mg/Kg-dry 1ND
4-Chloro-3-methylphenol 4/14/20200.43 mg/Kg-dry 1ND
2-Chloronaphthalene 4/14/20200.22 mg/Kg-dry 1ND
2-Chlorophenol 4/14/20200.22 mg/Kg-dry 1ND
4-Chlorophenyl phenyl ether 4/14/20200.22 mg/Kg-dry 1ND
Chrysene 4/14/20200.043 mg/Kg-dry 11.1
Dibenz(a,h)anthracene 4/14/20200.043 mg/Kg-dry 10.27
Dibenzofuran 4/14/20200.22 mg/Kg-dry 1ND
1,2-Dichlorobenzene 4/14/20200.22 mg/Kg-dry 1ND
1,3-Dichlorobenzene 4/14/20200.22 mg/Kg-dry 1ND
1,4-Dichlorobenzene 4/14/20200.22 mg/Kg-dry 1ND
3,3´-Dichlorobenzidine 4/14/20200.22 mg/Kg-dry 1ND
2,4-Dichlorophenol 4/14/20200.22 mg/Kg-dry 1ND
Diethyl phthalate 4/14/20200.22 mg/Kg-dry 1ND
2,4-Dimethylphenol 4/14/20200.22 mg/Kg-dry 1ND
Dimethyl phthalate 4/14/20200.22 mg/Kg-dry 1ND
4,6-Dinitro-2-methylphenol 4/14/20200.43 mg/Kg-dry 1ND
2,4-Dinitrophenol 4/14/20201.1 mg/Kg-dry 1ND
2,4-Dinitrotoluene 4/14/20200.043 mg/Kg-dry 1ND
2,6-Dinitrotoluene 4/14/20200.043 mg/Kg-dry 1ND
Qualifiers: J - Analyte detected below quantitation limits
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted recovery limits
ND - Not Detected at the Reporting Limit
E - Value above quantitation range
* - Non-accredited parameter
HT - Sample received past holding time
H - Holding time exceeded
RL - Reporting / Quantitation Limit for the analysis
Page 31 of 44
Project: RH-SET-Chicago, SET Generating Station, 3501 S.
Client Sample ID: RH-413-008
Collection Date: 4/13/2020 1:00:00 PM
Matrix: Soil
Analyses Result Qualifier Units Date AnalyzedRL
Client: Carnow, Conibear, & Associates
Work Order: 20040320
DF
Lab ID: 20040320-008
Date Printed: April 16, 2020
STAT Analysis Corporation2242 West Harrison St., Suite 200, Chicago, IL 60612-3766Tel: (312) 733-0551 Fax: (312) 733-2386 [email protected]
Date Reported: April 16, 2020
Accreditations:IEPA ELAP 100445;ORELAP IL300001;AIHA-LAP, LLC 101160;NVLAP LabCode 101202-0
ANALYTICAL RESULTS
Revision 0
Semivolatile Organic Compounds by GC/MS SW8270C (SW3550B) Analyst: TEMPrep Date: 4/14/2020Di-n-butyl phthalate 4/14/20200.22 mg/Kg-dry 1ND
Di-n-octyl phthalate 4/14/20200.22 mg/Kg-dry 1ND
Fluoranthene 4/14/20200.043 mg/Kg-dry 12.5
Fluorene 4/14/20200.043 mg/Kg-dry 10.24
Hexachlorobenzene 4/14/20200.22 mg/Kg-dry 1ND
Hexachlorobutadiene 4/14/20200.22 mg/Kg-dry 1ND
Hexachlorocyclopentadiene 4/14/20200.22 mg/Kg-dry 1ND
Hexachloroethane 4/14/20200.22 mg/Kg-dry 1ND
Indeno(1,2,3-cd)pyrene 4/14/20200.043 mg/Kg-dry 10.43
Isophorone 4/14/20200.22 mg/Kg-dry 1ND
2-Methylnaphthalene 4/14/20200.22 mg/Kg-dry 1ND
2-Methylphenol 4/14/20200.22 mg/Kg-dry 1ND
4-Methylphenol 4/14/20200.22 mg/Kg-dry 1ND
Naphthalene 4/14/20200.043 mg/Kg-dry 10.081
2-Nitroaniline 4/14/20200.22 mg/Kg-dry 1ND
3-Nitroaniline 4/14/20200.22 mg/Kg-dry 1ND
4-Nitroaniline 4/14/20200.22 mg/Kg-dry 1ND
2-Nitrophenol 4/14/20200.22 mg/Kg-dry 1ND
4-Nitrophenol 4/14/20200.43 mg/Kg-dry 1ND
Nitrobenzene 4/14/20200.043 mg/Kg-dry 1ND
N-Nitrosodi-n-propylamine 4/14/20200.043 mg/Kg-dry 1ND
N-Nitrosodimethylamine 4/14/20200.22 mg/Kg-dry 1ND
N-Nitrosodiphenylamine 4/14/20200.22 mg/Kg-dry 1ND
2, 2'-oxybis(1-Chloropropane) 4/14/20200.22 mg/Kg-dry 1ND
Pentachlorophenol 4/14/20200.087 mg/Kg-dry 1ND
Phenanthrene 4/14/20200.043 mg/Kg-dry 13.1
Phenol 4/14/20200.22 mg/Kg-dry 1ND
Pyrene 4/14/20200.043 mg/Kg-dry 12.0
Pyridine 4/14/20200.87 mg/Kg-dry 1ND
1,2,4-Trichlorobenzene 4/14/20200.22 mg/Kg-dry 1ND
2,4,5-Trichlorophenol 4/14/20200.22 mg/Kg-dry 1ND
2,4,6-Trichlorophenol 4/14/20200.22 mg/Kg-dry 1ND
PCBs SW8082A (SW3550B) Analyst: GVCPrep Date: 4/14/2020Aroclor 1016 4/14/20200.10 mg/Kg-dry 1ND
Aroclor 1221 4/14/20200.10 mg/Kg-dry 1ND
Aroclor 1232 4/14/20200.10 mg/Kg-dry 1ND
Aroclor 1242 4/14/20200.10 mg/Kg-dry 1ND
Aroclor 1248 4/14/20200.10 mg/Kg-dry 1ND
Qualifiers: J - Analyte detected below quantitation limits
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted recovery limits
ND - Not Detected at the Reporting Limit
E - Value above quantitation range
* - Non-accredited parameter
HT - Sample received past holding time
H - Holding time exceeded
RL - Reporting / Quantitation Limit for the analysis
Page 32 of 44
Project: RH-SET-Chicago, SET Generating Station, 3501 S.
Client Sample ID: RH-413-008
Collection Date: 4/13/2020 1:00:00 PM
Matrix: Soil
Analyses Result Qualifier Units Date AnalyzedRL
Client: Carnow, Conibear, & Associates
Work Order: 20040320
DF
Lab ID: 20040320-008
Date Printed: April 16, 2020
STAT Analysis Corporation2242 West Harrison St., Suite 200, Chicago, IL 60612-3766Tel: (312) 733-0551 Fax: (312) 733-2386 [email protected]
Date Reported: April 16, 2020
Accreditations:IEPA ELAP 100445;ORELAP IL300001;AIHA-LAP, LLC 101160;NVLAP LabCode 101202-0
ANALYTICAL RESULTS
Revision 0
PCBs SW8082A (SW3550B) Analyst: GVCPrep Date: 4/14/2020Aroclor 1254 4/14/20200.10 mg/Kg-dry 1ND
Aroclor 1260 4/14/20200.10 mg/Kg-dry 1ND
Pesticides SW8081B (SW3550B) Analyst: GVCPrep Date: 4/14/20204,4´-DDD 4/14/20200.0021 mg/Kg-dry 1ND
4,4´-DDE 4/14/20200.0021 mg/Kg-dry 1ND
4,4´-DDT 4/14/20200.0021 mg/Kg-dry 1ND
Aldrin 4/14/20200.0021 mg/Kg-dry 1ND
alpha-BHC 4/14/20200.0021 mg/Kg-dry 1ND
alpha-Chlordane 4/14/20200.0021 mg/Kg-dry 1ND
beta-BHC 4/14/20200.0021 mg/Kg-dry 1ND
Chlordane 4/14/20200.021 mg/Kg-dry 1ND
delta-BHC 4/14/20200.0021 mg/Kg-dry 1ND
Dieldrin 4/14/20200.0021 mg/Kg-dry 1ND
Endosulfan I 4/14/20200.0021 mg/Kg-dry 1ND
Endosulfan II 4/14/20200.0021 mg/Kg-dry 1ND
Endosulfan sulfate 4/14/20200.0021 mg/Kg-dry 1ND
Endrin 4/14/20200.0021 mg/Kg-dry 1ND
Endrin aldehyde 4/14/20200.0021 mg/Kg-dry 1ND
Endrin ketone 4/14/20200.0021 mg/Kg-dry 1ND
gamma-BHC 4/14/20200.0021 mg/Kg-dry 1ND
gamma-Chlordane 4/14/20200.0021 mg/Kg-dry 1ND
Heptachlor 4/14/20200.0021 mg/Kg-dry 1ND
Heptachlor epoxide 4/14/20200.0021 mg/Kg-dry 1ND
Methoxychlor 4/14/20200.0021 mg/Kg-dry 1ND
Toxaphene 4/14/20200.043 mg/Kg-dry 1ND
Metals by ICP/MS SW6020A (SW3050B) Analyst: MDTPrep Date: 4/14/2020Aluminum 4/14/202046 mg/Kg-dry 2011000
Antimony 4/14/20204.6 mg/Kg-dry 20ND
Arsenic 4/14/20202.3 mg/Kg-dry 205.8
Barium 4/14/20202.3 mg/Kg-dry 20390
Beryllium 4/14/20201.2 mg/Kg-dry 20ND
Cadmium 4/14/20201.2 mg/Kg-dry 202.8
Calcium 4/14/2020140 mg/Kg-dry 20210000
Chromium 4/14/20202.3 mg/Kg-dry 2032
Cobalt 4/14/20202.3 mg/Kg-dry 204.7
Copper 4/14/20205.8 mg/Kg-dry 2068
Iron 4/14/202069 mg/Kg-dry 2021000
Qualifiers: J - Analyte detected below quantitation limits
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted recovery limits
ND - Not Detected at the Reporting Limit
E - Value above quantitation range
* - Non-accredited parameter
HT - Sample received past holding time
H - Holding time exceeded
RL - Reporting / Quantitation Limit for the analysis
Page 33 of 44
Project: RH-SET-Chicago, SET Generating Station, 3501 S.
Client Sample ID: RH-413-008
Collection Date: 4/13/2020 1:00:00 PM
Matrix: Soil
Analyses Result Qualifier Units Date AnalyzedRL
Client: Carnow, Conibear, & Associates
Work Order: 20040320
DF
Lab ID: 20040320-008
Date Printed: April 16, 2020
STAT Analysis Corporation2242 West Harrison St., Suite 200, Chicago, IL 60612-3766Tel: (312) 733-0551 Fax: (312) 733-2386 [email protected]
Date Reported: April 16, 2020
Accreditations:IEPA ELAP 100445;ORELAP IL300001;AIHA-LAP, LLC 101160;NVLAP LabCode 101202-0
ANALYTICAL RESULTS
Revision 0
Metals by ICP/MS SW6020A (SW3050B) Analyst: MDTPrep Date: 4/14/2020Lead 4/14/20201.2 mg/Kg-dry 20180
Magnesium 4/14/202069 mg/Kg-dry 2066000
Manganese 4/14/20202.3 mg/Kg-dry 20940
Nickel 4/14/20202.3 mg/Kg-dry 2018
Potassium 4/14/202069 mg/Kg-dry 201300
Selenium 4/14/20202.3 mg/Kg-dry 203.5
Silver 4/14/20202.3 mg/Kg-dry 20ND
Sodium 4/14/2020140 mg/Kg-dry 201600
Thallium 4/14/20202.3 mg/Kg-dry 20ND
Vanadium 4/14/20202.3 mg/Kg-dry 2021
Zinc 4/14/202012 mg/Kg-dry 20300
Mercury SW7471B Analyst: LBPrep Date: 4/14/2020Mercury 4/14/20200.022 mg/Kg-dry 10.16
Cyanide, Total SW9012A Analyst: CABPrep Date: 4/14/2020Cyanide 4/14/20200.33 mg/Kg-dry 1ND
pH (25 °C) SW9045C Analyst: JARPrep Date: 4/13/2020pH 4/13/2020pH Units 110.9
Percent Moisture D2974 Analyst: FNPrep Date: 4/14/2020Percent Moisture * 4/14/20200.2 wt% 123.1
Asbestos Analysis by TEM EPA600/R-93/116 Analyst: RJSPrep Date:Chrysotile 7/13/2020% 1<1
Qualifiers: J - Analyte detected below quantitation limits
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted recovery limits
ND - Not Detected at the Reporting Limit
E - Value above quantitation range
* - Non-accredited parameter
HT - Sample received past holding time
H - Holding time exceeded
RL - Reporting / Quantitation Limit for the analysis
Page 34 of 44
Project: RH-SET-Chicago, SET Generating Station, 3501 S.
Client Sample ID: RH-413-009
Collection Date: 4/13/2020 1:10:00 PM
Matrix: Soil
Analyses Result Qualifier Units Date AnalyzedRL
Client: Carnow, Conibear, & Associates
Work Order: 20040320
DF
Lab ID: 20040320-009
Date Printed: April 16, 2020
STAT Analysis Corporation2242 West Harrison St., Suite 200, Chicago, IL 60612-3766Tel: (312) 733-0551 Fax: (312) 733-2386 [email protected]
Date Reported: April 16, 2020
Accreditations:IEPA ELAP 100445;ORELAP IL300001;AIHA-LAP, LLC 101160;NVLAP LabCode 101202-0
ANALYTICAL RESULTS
Revision 0
Semivolatile Organic Compounds by GC/MS SW8270C (SW3550B) Analyst: TEMPrep Date: 4/14/2020Acenaphthene 4/14/20200.038 mg/Kg-dry 10.26
Acenaphthylene 4/14/20200.038 mg/Kg-dry 1ND
Aniline 4/14/20200.39 mg/Kg-dry 1ND
Anthracene 4/14/20200.038 mg/Kg-dry 10.55
Benz(a)anthracene 4/14/20200.038 mg/Kg-dry 11.7
Benzidine 4/14/20200.38 mg/Kg-dry 1ND
Benzo(a)pyrene 4/14/20200.038 mg/Kg-dry 11.5
Benzo(b)fluoranthene 4/14/20200.038 mg/Kg-dry 11.8
Benzo(g,h,i)perylene 4/14/20200.038 mg/Kg-dry 11.1
Benzo(k)fluoranthene 4/14/20200.038 mg/Kg-dry 11.3
Benzoic acid 4/14/20200.96 mg/Kg-dry 1ND
Benzyl alcohol 4/14/20200.20 mg/Kg-dry 1ND
Bis(2-chloroethoxy)methane 4/14/20200.20 mg/Kg-dry 1ND
Bis(2-chloroethyl)ether 4/14/20200.20 mg/Kg-dry 1ND
Bis(2-ethylhexyl)phthalate 4/14/20200.96 mg/Kg-dry 1ND
4-Bromophenyl phenyl ether 4/14/20200.20 mg/Kg-dry 1ND
Butyl benzyl phthalate 4/14/20200.20 mg/Kg-dry 1ND
Carbazole 4/14/20200.20 mg/Kg-dry 10.36
4-Chloroaniline 4/14/20200.20 mg/Kg-dry 1ND
4-Chloro-3-methylphenol 4/14/20200.38 mg/Kg-dry 1ND
2-Chloronaphthalene 4/14/20200.20 mg/Kg-dry 1ND
2-Chlorophenol 4/14/20200.20 mg/Kg-dry 1ND
4-Chlorophenyl phenyl ether 4/14/20200.20 mg/Kg-dry 1ND
Chrysene 4/14/20200.038 mg/Kg-dry 12.0
Dibenz(a,h)anthracene 4/14/20200.038 mg/Kg-dry 10.60
Dibenzofuran 4/14/20200.20 mg/Kg-dry 1ND
1,2-Dichlorobenzene 4/14/20200.20 mg/Kg-dry 1ND
1,3-Dichlorobenzene 4/14/20200.20 mg/Kg-dry 1ND
1,4-Dichlorobenzene 4/14/20200.20 mg/Kg-dry 1ND
3,3´-Dichlorobenzidine 4/14/20200.20 mg/Kg-dry 1ND
2,4-Dichlorophenol 4/14/20200.20 mg/Kg-dry 1ND
Diethyl phthalate 4/14/20200.20 mg/Kg-dry 1ND
2,4-Dimethylphenol 4/14/20200.20 mg/Kg-dry 1ND
Dimethyl phthalate 4/14/20200.20 mg/Kg-dry 1ND
4,6-Dinitro-2-methylphenol 4/14/20200.38 mg/Kg-dry 1ND
2,4-Dinitrophenol 4/14/20200.96 mg/Kg-dry 1ND
2,4-Dinitrotoluene 4/14/20200.038 mg/Kg-dry 1ND
2,6-Dinitrotoluene 4/14/20200.038 mg/Kg-dry 1ND
Qualifiers: J - Analyte detected below quantitation limits
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted recovery limits
ND - Not Detected at the Reporting Limit
E - Value above quantitation range
* - Non-accredited parameter
HT - Sample received past holding time
H - Holding time exceeded
RL - Reporting / Quantitation Limit for the analysis
Page 35 of 44
Project: RH-SET-Chicago, SET Generating Station, 3501 S.
Client Sample ID: RH-413-009
Collection Date: 4/13/2020 1:10:00 PM
Matrix: Soil
Analyses Result Qualifier Units Date AnalyzedRL
Client: Carnow, Conibear, & Associates
Work Order: 20040320
DF
Lab ID: 20040320-009
Date Printed: April 16, 2020
STAT Analysis Corporation2242 West Harrison St., Suite 200, Chicago, IL 60612-3766Tel: (312) 733-0551 Fax: (312) 733-2386 [email protected]
Date Reported: April 16, 2020
Accreditations:IEPA ELAP 100445;ORELAP IL300001;AIHA-LAP, LLC 101160;NVLAP LabCode 101202-0
ANALYTICAL RESULTS
Revision 0
Semivolatile Organic Compounds by GC/MS SW8270C (SW3550B) Analyst: TEMPrep Date: 4/14/2020Di-n-butyl phthalate 4/14/20200.20 mg/Kg-dry 1ND
Di-n-octyl phthalate 4/14/20200.20 mg/Kg-dry 1ND
Fluoranthene 4/14/20200.038 mg/Kg-dry 13.2
Fluorene 4/14/20200.038 mg/Kg-dry 10.24
Hexachlorobenzene 4/14/20200.20 mg/Kg-dry 1ND
Hexachlorobutadiene 4/14/20200.20 mg/Kg-dry 1ND
Hexachlorocyclopentadiene 4/14/20200.20 mg/Kg-dry 1ND
Hexachloroethane 4/14/20200.20 mg/Kg-dry 1ND
Indeno(1,2,3-cd)pyrene 4/14/20200.038 mg/Kg-dry 10.99
Isophorone 4/14/20200.20 mg/Kg-dry 1ND
2-Methylnaphthalene 4/14/20200.20 mg/Kg-dry 1ND
2-Methylphenol 4/14/20200.20 mg/Kg-dry 1ND
4-Methylphenol 4/14/20200.20 mg/Kg-dry 1ND
Naphthalene 4/14/20200.038 mg/Kg-dry 10.085
2-Nitroaniline 4/14/20200.20 mg/Kg-dry 1ND
3-Nitroaniline 4/14/20200.20 mg/Kg-dry 1ND
4-Nitroaniline 4/14/20200.20 mg/Kg-dry 1ND
2-Nitrophenol 4/14/20200.20 mg/Kg-dry 1ND
4-Nitrophenol 4/14/20200.38 mg/Kg-dry 1ND
Nitrobenzene 4/14/20200.038 mg/Kg-dry 1ND
N-Nitrosodi-n-propylamine 4/14/20200.038 mg/Kg-dry 1ND
N-Nitrosodimethylamine 4/14/20200.20 mg/Kg-dry 1ND
N-Nitrosodiphenylamine 4/14/20200.20 mg/Kg-dry 1ND
2, 2'-oxybis(1-Chloropropane) 4/14/20200.20 mg/Kg-dry 1ND
Pentachlorophenol 4/14/20200.078 mg/Kg-dry 1ND
Phenanthrene 4/14/20200.038 mg/Kg-dry 12.5
Phenol 4/14/20200.20 mg/Kg-dry 1ND
Pyrene 4/14/20200.038 mg/Kg-dry 12.6
Pyridine 4/14/20200.78 mg/Kg-dry 1ND
1,2,4-Trichlorobenzene 4/14/20200.20 mg/Kg-dry 1ND
2,4,5-Trichlorophenol 4/14/20200.20 mg/Kg-dry 1ND
2,4,6-Trichlorophenol 4/14/20200.20 mg/Kg-dry 1ND
PCBs SW8082A (SW3550B) Analyst: GVCPrep Date: 4/14/2020Aroclor 1016 4/14/20200.091 mg/Kg-dry 1ND
Aroclor 1221 4/14/20200.091 mg/Kg-dry 1ND
Aroclor 1232 4/14/20200.091 mg/Kg-dry 1ND
Aroclor 1242 4/14/20200.091 mg/Kg-dry 1ND
Aroclor 1248 4/14/20200.091 mg/Kg-dry 1ND
Qualifiers: J - Analyte detected below quantitation limits
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted recovery limits
ND - Not Detected at the Reporting Limit
E - Value above quantitation range
* - Non-accredited parameter
HT - Sample received past holding time
H - Holding time exceeded
RL - Reporting / Quantitation Limit for the analysis
Page 36 of 44
Project: RH-SET-Chicago, SET Generating Station, 3501 S.
Client Sample ID: RH-413-009
Collection Date: 4/13/2020 1:10:00 PM
Matrix: Soil
Analyses Result Qualifier Units Date AnalyzedRL
Client: Carnow, Conibear, & Associates
Work Order: 20040320
DF
Lab ID: 20040320-009
Date Printed: April 16, 2020
STAT Analysis Corporation2242 West Harrison St., Suite 200, Chicago, IL 60612-3766Tel: (312) 733-0551 Fax: (312) 733-2386 [email protected]
Date Reported: April 16, 2020
Accreditations:IEPA ELAP 100445;ORELAP IL300001;AIHA-LAP, LLC 101160;NVLAP LabCode 101202-0
ANALYTICAL RESULTS
Revision 0
PCBs SW8082A (SW3550B) Analyst: GVCPrep Date: 4/14/2020Aroclor 1254 4/14/20200.091 mg/Kg-dry 1ND
Aroclor 1260 4/14/20200.091 mg/Kg-dry 1ND
Pesticides SW8081B (SW3550B) Analyst: GVCPrep Date: 4/14/20204,4´-DDD 4/14/20200.0018 mg/Kg-dry 1ND
4,4´-DDE 4/14/20200.0018 mg/Kg-dry 1ND
4,4´-DDT 4/14/20200.0018 mg/Kg-dry 1ND
Aldrin 4/14/20200.0018 mg/Kg-dry 1ND
alpha-BHC 4/14/20200.0018 mg/Kg-dry 1ND
alpha-Chlordane 4/14/20200.0018 mg/Kg-dry 1ND
beta-BHC 4/14/20200.0018 mg/Kg-dry 1ND
Chlordane 4/14/20200.018 mg/Kg-dry 1ND
delta-BHC 4/14/20200.0018 mg/Kg-dry 1ND
Dieldrin 4/14/20200.0018 mg/Kg-dry 1ND
Endosulfan I 4/14/20200.0018 mg/Kg-dry 1ND
Endosulfan II 4/14/20200.0018 mg/Kg-dry 1ND
Endosulfan sulfate 4/14/20200.0018 mg/Kg-dry 1ND
Endrin 4/14/20200.0018 mg/Kg-dry 1ND
Endrin aldehyde 4/14/20200.0018 mg/Kg-dry 1ND
Endrin ketone 4/14/20200.0018 mg/Kg-dry 1ND
gamma-BHC 4/14/20200.0018 mg/Kg-dry 1ND
gamma-Chlordane 4/14/20200.0018 mg/Kg-dry 1ND
Heptachlor 4/14/20200.0018 mg/Kg-dry 1ND
Heptachlor epoxide 4/14/20200.0018 mg/Kg-dry 1ND
Methoxychlor 4/14/20200.0018 mg/Kg-dry 1ND
Toxaphene 4/14/20200.038 mg/Kg-dry 1ND
Metals by ICP/MS SW6020A (SW3050B) Analyst: MDTPrep Date: 4/14/2020Aluminum 4/14/202042 mg/Kg-dry 2011000
Antimony 4/14/20204.2 mg/Kg-dry 20ND
Arsenic 4/14/20202.1 mg/Kg-dry 209.9
Barium 4/14/20202.1 mg/Kg-dry 20420
Beryllium 4/14/20201.0 mg/Kg-dry 201.1
Cadmium 4/14/20201.0 mg/Kg-dry 203.8
Calcium 4/14/2020130 mg/Kg-dry 20150000
Chromium 4/14/20202.1 mg/Kg-dry 2043
Cobalt 4/14/20202.1 mg/Kg-dry 205.6
Copper 4/14/20205.2 mg/Kg-dry 2072
Iron 4/14/202063 mg/Kg-dry 2049000
Qualifiers: J - Analyte detected below quantitation limits
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted recovery limits
ND - Not Detected at the Reporting Limit
E - Value above quantitation range
* - Non-accredited parameter
HT - Sample received past holding time
H - Holding time exceeded
RL - Reporting / Quantitation Limit for the analysis
Page 37 of 44
Project: RH-SET-Chicago, SET Generating Station, 3501 S.
Client Sample ID: RH-413-009
Collection Date: 4/13/2020 1:10:00 PM
Matrix: Soil
Analyses Result Qualifier Units Date AnalyzedRL
Client: Carnow, Conibear, & Associates
Work Order: 20040320
DF
Lab ID: 20040320-009
Date Printed: April 16, 2020
STAT Analysis Corporation2242 West Harrison St., Suite 200, Chicago, IL 60612-3766Tel: (312) 733-0551 Fax: (312) 733-2386 [email protected]
Date Reported: April 16, 2020
Accreditations:IEPA ELAP 100445;ORELAP IL300001;AIHA-LAP, LLC 101160;NVLAP LabCode 101202-0
ANALYTICAL RESULTS
Revision 0
Metals by ICP/MS SW6020A (SW3050B) Analyst: MDTPrep Date: 4/14/2020Lead 4/14/20201.0 mg/Kg-dry 20190
Magnesium 4/14/202063 mg/Kg-dry 2058000
Manganese 4/14/20202.1 mg/Kg-dry 20880
Nickel 4/14/20202.1 mg/Kg-dry 2025
Potassium 4/14/202063 mg/Kg-dry 201100
Selenium 4/14/20202.1 mg/Kg-dry 203.1
Silver 4/14/20202.1 mg/Kg-dry 20ND
Sodium 4/14/2020130 mg/Kg-dry 202100
Thallium 4/14/20202.1 mg/Kg-dry 20ND
Vanadium 4/14/20202.1 mg/Kg-dry 2030
Zinc 4/14/202010 mg/Kg-dry 20390
Mercury SW7471B Analyst: LBPrep Date: 4/14/2020Mercury 4/14/20200.019 mg/Kg-dry 10.11
Cyanide, Total SW9012A Analyst: CABPrep Date: 4/14/2020Cyanide 4/14/20200.29 mg/Kg-dry 1ND
pH (25 °C) SW9045C Analyst: JARPrep Date: 4/13/2020pH 4/13/2020pH Units 19.56
Percent Moisture D2974 Analyst: FNPrep Date: 4/14/2020Percent Moisture * 4/14/20200.2 wt% 114.2
Asbestos Analysis by TEM EPA600/R-93/116 Analyst: RJSPrep Date:Asbestos Components 7/13/2020% 1ND
Qualifiers: J - Analyte detected below quantitation limits
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted recovery limits
ND - Not Detected at the Reporting Limit
E - Value above quantitation range
* - Non-accredited parameter
HT - Sample received past holding time
H - Holding time exceeded
RL - Reporting / Quantitation Limit for the analysis
Page 38 of 44
Project: RH-SET-Chicago, SET Generating Station, 3501 S.
Client Sample ID: RH-413-010
Collection Date: 4/13/2020 1:15:00 PM
Matrix: Soil
Analyses Result Qualifier Units Date AnalyzedRL
Client: Carnow, Conibear, & Associates
Work Order: 20040320
DF
Lab ID: 20040320-010
Date Printed: April 16, 2020
STAT Analysis Corporation2242 West Harrison St., Suite 200, Chicago, IL 60612-3766Tel: (312) 733-0551 Fax: (312) 733-2386 [email protected]
Date Reported: April 16, 2020
Accreditations:IEPA ELAP 100445;ORELAP IL300001;AIHA-LAP, LLC 101160;NVLAP LabCode 101202-0
ANALYTICAL RESULTS
Revision 0
Semivolatile Organic Compounds by GC/MS SW8270C (SW3550B) Analyst: TEMPrep Date: 4/14/2020Acenaphthene 4/14/20200.040 mg/Kg-dry 10.21
Acenaphthylene 4/14/20200.040 mg/Kg-dry 1ND
Aniline 4/14/20200.40 mg/Kg-dry 1ND
Anthracene 4/14/20200.040 mg/Kg-dry 10.39
Benz(a)anthracene 4/14/20200.040 mg/Kg-dry 11.2
Benzidine 4/14/20200.40 mg/Kg-dry 1ND
Benzo(a)pyrene 4/14/20200.040 mg/Kg-dry 11.2
Benzo(b)fluoranthene 4/14/20200.040 mg/Kg-dry 11.2
Benzo(g,h,i)perylene 4/14/20200.040 mg/Kg-dry 10.82
Benzo(k)fluoranthene 4/14/20200.040 mg/Kg-dry 10.97
Benzoic acid 4/14/20201.0 mg/Kg-dry 1ND
Benzyl alcohol 4/14/20200.20 mg/Kg-dry 1ND
Bis(2-chloroethoxy)methane 4/14/20200.20 mg/Kg-dry 1ND
Bis(2-chloroethyl)ether 4/14/20200.20 mg/Kg-dry 1ND
Bis(2-ethylhexyl)phthalate 4/14/20201.0 mg/Kg-dry 1ND
4-Bromophenyl phenyl ether 4/14/20200.20 mg/Kg-dry 1ND
Butyl benzyl phthalate 4/14/20200.20 mg/Kg-dry 1ND
Carbazole 4/14/20200.20 mg/Kg-dry 10.23
4-Chloroaniline 4/14/20200.20 mg/Kg-dry 1ND
4-Chloro-3-methylphenol 4/14/20200.40 mg/Kg-dry 1ND
2-Chloronaphthalene 4/14/20200.20 mg/Kg-dry 1ND
2-Chlorophenol 4/14/20200.20 mg/Kg-dry 1ND
4-Chlorophenyl phenyl ether 4/14/20200.20 mg/Kg-dry 1ND
Chrysene 4/14/20200.040 mg/Kg-dry 11.4
Dibenz(a,h)anthracene 4/14/20200.040 mg/Kg-dry 10.41
Dibenzofuran 4/14/20200.20 mg/Kg-dry 1ND
1,2-Dichlorobenzene 4/14/20200.20 mg/Kg-dry 1ND
1,3-Dichlorobenzene 4/14/20200.20 mg/Kg-dry 1ND
1,4-Dichlorobenzene 4/14/20200.20 mg/Kg-dry 1ND
3,3´-Dichlorobenzidine 4/14/20200.20 mg/Kg-dry 1ND
2,4-Dichlorophenol 4/14/20200.20 mg/Kg-dry 1ND
Diethyl phthalate 4/14/20200.20 mg/Kg-dry 1ND
2,4-Dimethylphenol 4/14/20200.20 mg/Kg-dry 1ND
Dimethyl phthalate 4/14/20200.20 mg/Kg-dry 1ND
4,6-Dinitro-2-methylphenol 4/14/20200.40 mg/Kg-dry 1ND
2,4-Dinitrophenol 4/14/20201.0 mg/Kg-dry 1ND
2,4-Dinitrotoluene 4/14/20200.040 mg/Kg-dry 1ND
2,6-Dinitrotoluene 4/14/20200.040 mg/Kg-dry 1ND
Qualifiers: J - Analyte detected below quantitation limits
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted recovery limits
ND - Not Detected at the Reporting Limit
E - Value above quantitation range
* - Non-accredited parameter
HT - Sample received past holding time
H - Holding time exceeded
RL - Reporting / Quantitation Limit for the analysis
Page 39 of 44
Project: RH-SET-Chicago, SET Generating Station, 3501 S.
Client Sample ID: RH-413-010
Collection Date: 4/13/2020 1:15:00 PM
Matrix: Soil
Analyses Result Qualifier Units Date AnalyzedRL
Client: Carnow, Conibear, & Associates
Work Order: 20040320
DF
Lab ID: 20040320-010
Date Printed: April 16, 2020
STAT Analysis Corporation2242 West Harrison St., Suite 200, Chicago, IL 60612-3766Tel: (312) 733-0551 Fax: (312) 733-2386 [email protected]
Date Reported: April 16, 2020
Accreditations:IEPA ELAP 100445;ORELAP IL300001;AIHA-LAP, LLC 101160;NVLAP LabCode 101202-0
ANALYTICAL RESULTS
Revision 0
Semivolatile Organic Compounds by GC/MS SW8270C (SW3550B) Analyst: TEMPrep Date: 4/14/2020Di-n-butyl phthalate 4/14/20200.20 mg/Kg-dry 1ND
Di-n-octyl phthalate 4/14/20200.20 mg/Kg-dry 1ND
Fluoranthene 4/14/20200.040 mg/Kg-dry 12.9
Fluorene 4/14/20200.040 mg/Kg-dry 10.20
Hexachlorobenzene 4/14/20200.20 mg/Kg-dry 1ND
Hexachlorobutadiene 4/14/20200.20 mg/Kg-dry 1ND
Hexachlorocyclopentadiene 4/14/20200.20 mg/Kg-dry 1ND
Hexachloroethane 4/14/20200.20 mg/Kg-dry 1ND
Indeno(1,2,3-cd)pyrene 4/14/20200.040 mg/Kg-dry 10.75
Isophorone 4/14/20200.20 mg/Kg-dry 1ND
2-Methylnaphthalene 4/14/20200.20 mg/Kg-dry 1ND
2-Methylphenol 4/14/20200.20 mg/Kg-dry 1ND
4-Methylphenol 4/14/20200.20 mg/Kg-dry 1ND
Naphthalene 4/14/20200.040 mg/Kg-dry 10.044
2-Nitroaniline 4/14/20200.20 mg/Kg-dry 1ND
3-Nitroaniline 4/14/20200.20 mg/Kg-dry 1ND
4-Nitroaniline 4/14/20200.20 mg/Kg-dry 1ND
2-Nitrophenol 4/14/20200.20 mg/Kg-dry 1ND
4-Nitrophenol 4/14/20200.40 mg/Kg-dry 1ND
Nitrobenzene 4/14/20200.040 mg/Kg-dry 1ND
N-Nitrosodi-n-propylamine 4/14/20200.040 mg/Kg-dry 1ND
N-Nitrosodimethylamine 4/14/20200.20 mg/Kg-dry 1ND
N-Nitrosodiphenylamine 4/14/20200.20 mg/Kg-dry 1ND
2, 2'-oxybis(1-Chloropropane) 4/14/20200.20 mg/Kg-dry 1ND
Pentachlorophenol 4/14/20200.080 mg/Kg-dry 1ND
Phenanthrene 4/14/20200.040 mg/Kg-dry 12.3
Phenol 4/14/20200.20 mg/Kg-dry 1ND
Pyrene 4/14/20200.040 mg/Kg-dry 12.3
Pyridine 4/14/20200.80 mg/Kg-dry 1ND
1,2,4-Trichlorobenzene 4/14/20200.20 mg/Kg-dry 1ND
2,4,5-Trichlorophenol 4/14/20200.20 mg/Kg-dry 1ND
2,4,6-Trichlorophenol 4/14/20200.20 mg/Kg-dry 1ND
PCBs SW8082A (SW3550B) Analyst: GVCPrep Date: 4/14/2020Aroclor 1016 4/14/20200.096 mg/Kg-dry 1ND
Aroclor 1221 4/14/20200.096 mg/Kg-dry 1ND
Aroclor 1232 4/14/20200.096 mg/Kg-dry 1ND
Aroclor 1242 4/14/20200.096 mg/Kg-dry 1ND
Aroclor 1248 4/14/20200.096 mg/Kg-dry 1ND
Qualifiers: J - Analyte detected below quantitation limits
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted recovery limits
ND - Not Detected at the Reporting Limit
E - Value above quantitation range
* - Non-accredited parameter
HT - Sample received past holding time
H - Holding time exceeded
RL - Reporting / Quantitation Limit for the analysis
Page 40 of 44
Project: RH-SET-Chicago, SET Generating Station, 3501 S.
Client Sample ID: RH-413-010
Collection Date: 4/13/2020 1:15:00 PM
Matrix: Soil
Analyses Result Qualifier Units Date AnalyzedRL
Client: Carnow, Conibear, & Associates
Work Order: 20040320
DF
Lab ID: 20040320-010
Date Printed: April 16, 2020
STAT Analysis Corporation2242 West Harrison St., Suite 200, Chicago, IL 60612-3766Tel: (312) 733-0551 Fax: (312) 733-2386 [email protected]
Date Reported: April 16, 2020
Accreditations:IEPA ELAP 100445;ORELAP IL300001;AIHA-LAP, LLC 101160;NVLAP LabCode 101202-0
ANALYTICAL RESULTS
Revision 0
PCBs SW8082A (SW3550B) Analyst: GVCPrep Date: 4/14/2020Aroclor 1254 4/14/20200.096 mg/Kg-dry 1ND
Aroclor 1260 4/14/20200.096 mg/Kg-dry 1ND
Pesticides SW8081B (SW3550B) Analyst: GVCPrep Date: 4/14/20204,4´-DDD 4/14/20200.0019 mg/Kg-dry 1ND
4,4´-DDE 4/14/20200.0019 mg/Kg-dry 1ND
4,4´-DDT 4/14/20200.0019 mg/Kg-dry 1ND
Aldrin 4/14/20200.0019 mg/Kg-dry 1ND
alpha-BHC 4/14/20200.0019 mg/Kg-dry 1ND
alpha-Chlordane 4/14/20200.0019 mg/Kg-dry 1ND
beta-BHC 4/14/20200.0019 mg/Kg-dry 1ND
Chlordane 4/14/20200.019 mg/Kg-dry 1ND
delta-BHC 4/14/20200.0019 mg/Kg-dry 1ND
Dieldrin 4/14/20200.0019 mg/Kg-dry 1ND
Endosulfan I 4/14/20200.0019 mg/Kg-dry 1ND
Endosulfan II 4/14/20200.0019 mg/Kg-dry 1ND
Endosulfan sulfate 4/14/20200.0019 mg/Kg-dry 1ND
Endrin 4/14/20200.0019 mg/Kg-dry 1ND
Endrin aldehyde 4/14/20200.0019 mg/Kg-dry 1ND
Endrin ketone 4/14/20200.0019 mg/Kg-dry 1ND
gamma-BHC 4/14/20200.0019 mg/Kg-dry 1ND
gamma-Chlordane 4/14/20200.0019 mg/Kg-dry 1ND
Heptachlor 4/14/20200.0019 mg/Kg-dry 1ND
Heptachlor epoxide 4/14/20200.0019 mg/Kg-dry 1ND
Methoxychlor 4/14/20200.0019 mg/Kg-dry 1ND
Toxaphene 4/14/20200.040 mg/Kg-dry 1ND
Metals by ICP/MS SW6020A (SW3050B) Analyst: MDTPrep Date: 4/14/2020Aluminum 4/14/202043 mg/Kg-dry 2012000
Antimony 4/14/20204.3 mg/Kg-dry 20ND
Arsenic 4/14/20202.1 mg/Kg-dry 209.8
Barium 4/14/20202.1 mg/Kg-dry 20240
Beryllium 4/14/20201.1 mg/Kg-dry 20ND
Cadmium 4/14/20201.1 mg/Kg-dry 20ND
Calcium 4/14/2020130 mg/Kg-dry 2023000
Chromium 4/14/20202.1 mg/Kg-dry 2023
Cobalt 4/14/20202.1 mg/Kg-dry 209.2
Copper 4/14/20205.4 mg/Kg-dry 2041
Iron 4/14/202064 mg/Kg-dry 2024000
Qualifiers: J - Analyte detected below quantitation limits
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted recovery limits
ND - Not Detected at the Reporting Limit
E - Value above quantitation range
* - Non-accredited parameter
HT - Sample received past holding time
H - Holding time exceeded
RL - Reporting / Quantitation Limit for the analysis
Page 41 of 44
Project: RH-SET-Chicago, SET Generating Station, 3501 S.
Client Sample ID: RH-413-010
Collection Date: 4/13/2020 1:15:00 PM
Matrix: Soil
Analyses Result Qualifier Units Date AnalyzedRL
Client: Carnow, Conibear, & Associates
Work Order: 20040320
DF
Lab ID: 20040320-010
Date Printed: April 16, 2020
STAT Analysis Corporation2242 West Harrison St., Suite 200, Chicago, IL 60612-3766Tel: (312) 733-0551 Fax: (312) 733-2386 [email protected]
Date Reported: April 16, 2020
Accreditations:IEPA ELAP 100445;ORELAP IL300001;AIHA-LAP, LLC 101160;NVLAP LabCode 101202-0
ANALYTICAL RESULTS
Revision 0
Metals by ICP/MS SW6020A (SW3050B) Analyst: MDTPrep Date: 4/14/2020Lead 4/14/20201.1 mg/Kg-dry 2090
Magnesium 4/14/202064 mg/Kg-dry 2012000
Manganese 4/14/20202.1 mg/Kg-dry 20530
Nickel 4/14/20202.1 mg/Kg-dry 2021
Potassium 4/14/202064 mg/Kg-dry 201900
Selenium 4/14/20202.1 mg/Kg-dry 20ND
Silver 4/14/20202.1 mg/Kg-dry 20ND
Sodium 4/14/2020130 mg/Kg-dry 20280
Thallium 4/14/20202.1 mg/Kg-dry 20ND
Vanadium 4/14/20202.1 mg/Kg-dry 2025
Zinc 4/14/202011 mg/Kg-dry 20170
Mercury SW7471B Analyst: LBPrep Date: 4/14/2020Mercury 4/14/20200.024 mg/Kg-dry 10.096
Cyanide, Total SW9012A Analyst: CABPrep Date: 4/14/2020Cyanide 4/14/20200.30 mg/Kg-dry 1ND
pH (25 °C) SW9045C Analyst: JARPrep Date: 4/13/2020pH 4/13/2020pH Units 19.29
Percent Moisture D2974 Analyst: FNPrep Date: 4/14/2020Percent Moisture * 4/14/20200.2 wt% 117.4
Asbestos Analysis by TEM EPA600/R-93/116 Analyst: RJSPrep Date:Chrysotile 7/13/2020% 1<1
Qualifiers: J - Analyte detected below quantitation limits
B - Analyte detected in the associated Method Blank
S - Spike Recovery outside accepted recovery limits
R - RPD outside accepted recovery limits
ND - Not Detected at the Reporting Limit
E - Value above quantitation range
* - Non-accredited parameter
HT - Sample received past holding time
H - Holding time exceeded
RL - Reporting / Quantitation Limit for the analysis
Page 42 of 44
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