7405 sw tech center dr ste a160 tigard, or 97223 (855) 800 ... · orelap id: 4077 7405 sw tech...

ORELAP ID: 4077

7405 SW Tech Center Dr Ste A160Tigard, OR 97223(855) 800-6890

18000857

3/21/2018

1A401030000697B000002753Distillate

Cannabinoids by JCB 2009 Units:

Sample IDSample Type

Receipt ConditionReceipt DateSampled DateReport Date

Sample Batch #Sample Name

500 S. Danebo Ave.

Eugene, OR 97402

3/28/2018

Extract

CBD = (CBD + 0.877 x CBDA)

THC = (THC + 0.877 x THCA)

Total Cannabinoids (Calculated)

Sublime Solutions, LLC

<LOQ

68.3

°C12.0

03/22/2018 RunID: 180322eq08

Analysis LOQ Notes Analysis Date

3/21/2018 1:14

Result

% Prep:

Result

Report Number C003965Original Batch # 1A401030000697B000002731

Cannabichromene (CBC) 1.33 0.19 N1 3/23/2018

Cannabidiol (CBD) <LOQ 0.19 3/23/2018

Cannabidiolic Acid (CBDA) <LOQ 0.19 3/23/2018

Cannabidivarin (CBDV) <LOQ 0.19 N1 3/23/2018

Cannabidivarinic Acid (CBDVA) <LOQ 0.19 N1 3/23/2018

Cannabigerol (CBG) 1.92 0.19 N1 3/23/2018

Cannabinol (CBN) 0.31 0.19 N1 3/23/2018

d-8-Tetrahydrocannabinol (d-8-THC) <LOQ 0.75 3/23/2018

d-9-Tetrahydrocannabinol (THC) 68.3 0.19 3/23/2018

d-9-Tetrahydrocannabinolic Acid (THCA) <LOQ 0.19 3/23/2018

Tetrahydrocannabivarin (THCV) <LOQ 0.19 N1 3/23/2018

Comments

A Control Study is in place. This sample is the PRIMARY sample. The Average Total THC of sample 18000857 and 18000858 = 68.35 The Relative Percent Difference (RPD) of the Total THC between sample 18000857 and 18000858 = 0.1 - PASS. Cannabinoid Analysis on 3/23/2018 under RunID 180322eq08.

1 of 3C003965 3/28/2018 3:59:01PM18000857 Final

ORELAP ID: 4077


Quality Control Summary

Laboratory Controls

LSe1L180005P36 Recovery Limit% Notesd-9-THC 86% 70-130THCA 111% 70-130

Method: JCB 2009 RunID: 180322eq08 Units: % Analysis Date: 3/23/2018

DuplicatesSD18000845 Result mg/g Original RPD NotesLimitCBDA <LOQ <LOQ 0 20<

CBDV <LOQ <LOQ 0 20<

CBDVA <LOQ <LOQ 0 20<

CBG 7.16 7.18 0 20<

CBN <LOQ <LOQ 0 20<

d-8-THC <LOQ <LOQ 0 20<

d-9-THC 119 120 0 20<

THCA 849 848 0 20<

THCV <LOQ <LOQ 0 20<

CBC <LOQ <LOQ 0 20<

CBD <LOQ <LOQ 0 20<

Method Blanks

MBeL180005P36 NotesResult Limit

CBC <LOQ 0.17CBD <LOQ 0.17CBDA <LOQ 0.17CBDV <LOQ 0.17CBDVA <LOQ 0.17CBG <LOQ 0.17CBN <LOQ 0.17d-8-THC <LOQ 0.68d-9-THC <LOQ 0.17THCA <LOQ 0.17THCV <LOQ 0.17

2 of 3C003965 3/28/2018 3:59:01PM18000857 Final

ORELAP ID: 4077


Full NoteFlag

Notes Glossary

B1 Analyte in blank, not samples.B2 Sample more than 5x blank.B3 Sample less than 5x blank.C1 QC result high, non-detects reported.C2 QC outside limits, data estimate reported.C3 QC outside limits, data acceptable based on additional QC.C4 Spike result above calibration.C5 Estimated, concentration above the calibration curve.C6 Estimated, concentration below the LOQ.C7 LOQ raised due to limited sample and/or dilution.C8 LOQ raised due to matrix interferences.LOQ Limit of QuantificationM1 Matrix effecting spike recovery.M2 Sample contains more than 4x spike.M3 Non-homogenous sample matrix effecting RPD and/or %Recovery.N See case narrative.N1 This Analyte is Not ORELAP AcredditedO Not ORELAP accredited.P1 RPD outside limits.P2 RPD non-calculable, result less than 5x LOQ.P3 RPD non-calculable, one result out of rangeT Tentatively Identified Compound (TIC) by library search.

AuthorizationReport Issued ByJulie AustinCommunications Coordinator

This report is intended to comply with Current Oregon Administrative Rules:Chapter 333 Division 7; Chapter 333 Division 8; Chapter 333 Division 64. These methods areaccredited by ORELAP, unless otherwise noted.

The results contained in this report apply only to the items tested, and are for the exclusive use of the above named person or entity.Requests for information regarding these results must be referred to that person or entity. This report must not be reproduced,except in full, without the written approval of Cascadia Labs.

3 of 3C003965 3/28/2018 3:59:01PM18000857 Final

ORELAP ID: 4077

Cascadia Labs 7405 SW Tech Center Dr Ste A160Tigard, OR 97223(855) 800-6890

18000857

3/21/2018

1A401030000697B000002753Distillate

Residual Solvents by USP 467 GCMS Units:PPM Prep:

Sample IDSample Type

Receipt ConditionReceipt DateSampled DateReport Date

Batch #Sample Name

500 S. Danebo Ave.

Eugene, OR 97402

3/28/2018

Extract

Sublime Solutions, LLC

°C12.0

RunIDs:03/27/2018

3/21/2018 1:14

Report Number C003965

180323eq05,180323eq75

Original Batch # 1A401030000697B000002731

LOQ Analyte Analyte ppm LOQ ActionNotes NotesAction Statusppm Status94<LOQ1,4-Dioxane < LOQ380 Pass

55<LOQ2,2-Dimethylbutane < LOQ290 Pass

120<LOQ2,3-Dimethylbutane 2 < LOQ290 Pass

1200<LOQ2-Butanol < LOQ5000 Pass

60<LOQ2-Ethoxyethanol < LOQ160 Pass

1100<LOQ2-Methylbutane < LOQ5000 Pass

1200<LOQ2-Propanol < LOQ5000 Pass

59<LOQ3-Methylpentane < LOQ290 Pass

1100<LOQ AAcetone < LOQ5000 Pass

73<LOQ AAcetonitrile < LOQ410 Pass

1<LOQBenzene < LOQ2 Pass

790<LOQButanes < LOQ5000 Pass

34<LOQCumene < LOQ70 Pass

890<LOQCyclohexane < LOQ3880 Pass

120<LOQDichloromethane < LOQ5000 Pass

1200<LOQEthanol < LOQ5000 Pass

1100<LOQEthyl Acetate < LOQ5000 Pass

1100<LOQEthyl Ether < LOQ5000 Pass

520<LOQEthylbenzene < LOQ2170 Pass

280<LOQEthylene Glycol 620 Pass

47<LOQEthylene Oxide < LOQ50 Pass

900<LOQHeptane < LOQ5000 Pass

290<LOQHexanes < LOQ290 Pass

390<LOQIsobutane < LOQ5000 Pass

1200<LOQIsopropyl Acetate < LOQ5000 Pass

1000<LOQm,p-Xylene < LOQ2170 Pass

680<LOQMethanol < LOQ3000 Pass

390<LOQn-Butane < LOQ5000 Pass

390<LOQNeopentane < LOQ5000 Pass

56<LOQn-Hexane < LOQ290 Pass

1100<LOQn-Pentane < LOQ5000 Pass

500<LOQo-Xylene < LOQ2170 Pass

3900<LOQPentanes < LOQ5000 Pass

160<LOQPropane < LOQ5000 Pass

160<LOQ TTetrahydrofuran < LOQ720 Pass

170<LOQ TToluene < LOQ890 Pass

1500<LOQ XXylenes < LOQ2170 Pass

1 of 5C003965 3/28/2018 4:04:21PM18000857

ORELAP ID: 4077


Comments

Tentatively Identified Compounds (TICs) not found.

A Control Study is in place. This sample is the PRIMARY sample.

Analysis on 3/27/2018 under RunID 180323eq05. Analysis on 3/27/2018 under RunID 180323eq75.

The results contained in this report apply only to the items tested, and are for the exclusive use of the above namedperson or entity. Requests for information regarding these results must be referred to that person or entity. Thisreport must not be reproduced, except in full, without the written approval of Cascadia Labs.

Authorization

Report Issued By This report is intended to comply with Current Oregon Administrative Rules:Chapter 333 Division 7; Chapter 333 Division 8; Chapter 333 Division 64. These methods areaccredited by ORELAP.Julie Austin

Communications Coordinator

2 of 5C003965 3/28/2018 4:04:21PM18000857

ORELAP ID: 4077


Quality Control Summary

LSe1L170036P38 Recovery% Limit% Run IDLaboratory ControlsLSe1L170036P38 Recovery% Limit% Run ID Notes Notes1,4-Dioxane 96 180323eq0550-150 2,2-Dimethylbutane 93 180323eq0550-150

2,3-Dimethylbutane 94 180323eq0550-150 2-Butanol 98 180323eq0550-150

2-Ethoxyethanol 94 180323eq0550-150 2-Methylbutane 92 180323eq0550-150

2-Propanol 97 180323eq0550-150 3-Methylpentane 94 180323eq0550-150

Acetone 96 180323eq0550-150 Acetonitrile 96 180323eq0550-150

Benzene 97 180323eq0550-150 Cumene 95 180323eq0550-150

Cyclohexane 96 180323eq0550-150 Dichloromethane 96 180323eq0550-150

Ethanol 96 180323eq0550-150 Ethyl Acetate 96 180323eq0550-150

Ethyl Ether 94 180323eq0550-150 Ethylbenzene 97 180323eq0550-150

Ethylene Glycol 90 180323eq7550-150 Heptane 96 180323eq0550-150

Isopropyl Acetate 97 180323eq0550-150 m,p-Xylene 97 180323eq0550-150

Methanol 97 180323eq0550-150 n-Hexane 94 180323eq0550-150

n-Pentane 92 180323eq0550-150 o-Xylene 97 180323eq0550-150

Tetrahydrofuran 99 180323eq0550-150 Toluene 97 180323eq0550-150

Matrix SpikesMS18000845 Limits% NotesMS18000845 Limits% RunID Notes RunIDRecovery% Recovery%

1,4-Dioxane 180323eq0550-15096 2,2-Dimethylbutane 180323eq0550-15097

2,3-Dimethylbutane 180323eq0550-15098 2-Butanol 180323eq0550-15097

2-Ethoxyethanol 180323eq0550-150101 2-Methylbutane 180323eq0550-15098

2-Propanol 180323eq0550-15097 3-Methylpentane 180323eq0550-15097

Acetone 180323eq0550-15098 Acetonitrile 180323eq0550-15099

Benzene 180323eq0550-15096 Cumene 180323eq0550-150113

Cyclohexane 180323eq0550-15097 Dichloromethane 180323eq0550-15098

Ethanol 180323eq0550-15095 Ethyl Acetate 180323eq0550-150115

Ethyl Ether 180323eq0550-15097 Ethylbenzene 180323eq0550-15098

Ethylene Glycol 180323eq7550-15071 Heptane 180323eq0550-15098

Isopropyl Acetate 180323eq0550-15099 m,p-Xylene 180323eq0550-15098

Methanol 180323eq0550-15096 n-Hexane 180323eq0550-15098

o-Xylene 180323eq0550-15098 Tetrahydrofuran 180323eq0550-15098

Toluene 180323eq0550-15098

3 of 5C003965 3/28/2018 4:04:21PM18000857

ORELAP ID: 4077


Duplicates

SD18000845 Result mg/kg Original RPD Limit Notes SD18000845 Result mg/kg Original RPD Limit NotesEthylene Glycol 0 20<<LOQ <LOQ 1,4-Dioxane 0 20 < LOQ<<LOQ <LOQ

2,2-Dimethylbutan 0 20 < LOQ<<LOQ <LOQ 2,3-Dimethylbutan 0 20 < LOQ<<LOQ <LOQ

2-Butanol 0 20 < LOQ<<LOQ <LOQ 2-Ethoxyethanol 0 20 < LOQ<<LOQ <LOQ

2-Methylbutane 0 20 < LOQ<<LOQ <LOQ 2-Propanol 0 20 < LOQ<<LOQ <LOQ

3-Methylpentane 0 20 < LOQ<<LOQ <LOQ Acetone 0 20 < LOQ<<LOQ <LOQ

Acetonitrile 0 20 < LOQ<<LOQ <LOQ Benzene 0 20 < LOQ<<LOQ <LOQ

Butanes 0 20 < LOQ<<LOQ <LOQ Cumene 0 20 < LOQ<<LOQ <LOQ

Cyclohexane 0 20 < LOQ<<LOQ <LOQ Dichloromethane 0 20 < LOQ<<LOQ <LOQ

Ethanol 0 20 < LOQ<<LOQ <LOQ Ethyl Acetate 0 20 < LOQ<<LOQ <LOQ

Ethyl Ether 0 20 < LOQ<<LOQ <LOQ Ethylbenzene 0 20 < LOQ<<LOQ <LOQ

Ethylene Oxide 0 20 < LOQ<<LOQ <LOQ Heptane 0 20 < LOQ<<LOQ <LOQ

Hexanes 0 20 < LOQ<<LOQ <LOQ Isobutane 0 20 < LOQ<<LOQ <LOQ

Isopropyl Acetate 0 20 < LOQ<<LOQ <LOQ m,p-Xylene 0 20 < LOQ<<LOQ <LOQ

Methanol 0 20 < LOQ<<LOQ <LOQ n-Butane 0 20 < LOQ<<LOQ <LOQ

Neopentane 0 20 < LOQ<<LOQ <LOQ n-Hexane 0 20 < LOQ<<LOQ <LOQ

n-Pentane 9 20 < LOQ<1450 1570 o-Xylene 0 20 < LOQ<<LOQ <LOQ

Pentanes 0 20 < LOQ<<LOQ <LOQ Propane 0 20 < LOQ<<LOQ <LOQ

Tetrahydrofuran 0 20 < LOQ<<LOQ <LOQ Toluene 0 20 < LOQ<<LOQ <LOQ

Xylenes 0 20 < LOQ<<LOQ <LOQ

MBeL170036P38 NotesResult Limit

Method Blanks

MBeL170036P38 Result Limit NotesRunID RunID

Units = mg/kg

1,4-Dioxane <LOQ 180323eq0592 2,2-Dimethylbutane <LOQ 180323eq0554

2,3-Dimethylbutaneh l

<LOQ 180323eq05120 2-Butanol <LOQ 180323eq051200

2-Ethoxyethanol <LOQ 180323eq0558 2-Methylbutane <LOQ 180323eq051100

2-Propanol <LOQ 180323eq051100 3-Methylpentane <LOQ 180323eq0558

Acetone <LOQ 180323eq051100 Acetonitrile <LOQ 180323eq0571

Benzene <LOQ 180323eq051 Cumene <LOQ 180323eq0534

Cyclohexane <LOQ 180323eq05870 Dichloromethane <LOQ 180323eq05120

Ethanol <LOQ 180323eq051100 Ethyl Acetate <LOQ 180323eq051100

Ethyl Ether <LOQ 180323eq051100 Ethylbenzene <LOQ 180323eq05500

Ethylene Glycol <LOQ 180323eq75290 Ethylene Oxide <LOQ 180323eq0546

Heptane <LOQ 180323eq05880 Isobutane <LOQ 180323eq05380

Isopropyl Acetate <LOQ 180323eq051100 m,p-Xylene <LOQ 180323eq05990

Methanol <LOQ 180323eq05670 n-Butane <LOQ 180323eq05380

n-Hexane <LOQ 180323eq0555 n-Pentane <LOQ 180323eq051100

Neopentane <LOQ 180323eq05380 o-Xylene <LOQ 180323eq05490

Propane <LOQ 180323eq05150 Tetrahydrofuran <LOQ 180323eq05160

Toluene <LOQ 180323eq05170

4 of 5C003965 3/28/2018 4:04:21PM18000857

ORELAP ID: 4077


Full NoteFlag

Notes Glossary

* 2,3-dimethylbutane = 2,3-dimethylbutane + 2-methylpentaneB1 Analyte in blank, not samples.B2 Sample more than 5x blank.B3 Sample less than 5x blank.C1 QC result high, non-detects reported.C2 QC outside limits, data estimate reported.C3 QC outside limits, data acceptable based on additional QC.C4 Spike result above calibration.C5 Estimated, concentration above the calibration curve.C6 Estimated, concentration below the LOQ.C7 LOQ raised due to limited sample and/or dilution.C8 LOQ raised due to matrix interferences.L1 The LOQs of the compounds in 'Hexanes' are each below the action level.LOQ Limit of QuantificationM1 Matrix effecting spike recovery.M2 Sample contains more than 4x spike.M3 Non-homogenous sample matrix effecting RPD and/or %Recovery.N See case narrative.N1 This Analyte is Not ORELAP AcredditedO Not ORELAP accredited.P1 RPD outside limits.P2 RPD non-calculable, result less than 5x LOQ.P3 RPD non-calculable, one result out of rangeT Tentatively Identified Compound (TIC) by library search.

5 of 5C003965 3/28/2018 4:04:21PM18000857

12423 NE Whitaker WayPortland, OR 97230

503-254-1794

Job Number:

Report Date:

ORELAP#:

03/27/2018

OR100028

16:11Received: 03/22/18

18-001589

Report#: 037364-00

Purchase Order:

Product identity:

Customer:

18000857 - Distillate

Sample Date:

18-001589-0005Laboratory ID:

Client/Metrc ID: 1A4010300003585000000465

Cascadia Labs7405 SW Tech Center Dr. Suite A160

Brianna LopezRelinquished by:

21 °CTemp:

1 gWeight Received:

Sample Results

Pesticides Batch 1801375Method AOAC 2007.01 & EN 15662 (mod) Units mg/kg Analyze 3/26/18 12:00:00

LOQAnalyte Result Limits Status Notes LOQAnalyte Result Limits Status Notes

Abamectin < LOQ 0.50 0.30 pass Acephate < LOQ 0.40 0.20 pass

Acequinocyl < LOQ 2.0 1.0 pass Acetamiprid < LOQ 0.20 0.10 pass

Aldicarb < LOQ 0.40 0.20 pass Azoxystrobin < LOQ 0.20 0.10 pass

Bifenazate < LOQ 0.20 0.10 pass Bifenthrin < LOQ 0.20 0.10 pass

Boscalid < LOQ 0.40 0.10 pass Carbaryl < LOQ 0.20 0.10 pass

Carbofuran < LOQ 0.20 0.10 pass Chlorantraniliprol < LOQ 0.20 0.10 pass

Chlorfenapyr < LOQ 1.0 1.0 pass Chlorpyrifos < LOQ 0.20 0.10 pass

Clofentezine < LOQ 0.20 0.10 pass Cyfluthrin (incl. Beta-Cyfl < LOQ 1.0 1.0 pass

Cypermethrin < LOQ 1.0 1.0 pass Daminozide < LOQ 1.0 1.0 pass

Diazinon < LOQ 0.20 0.10 pass Dichlorvos < LOQ 1.0 0.50 pass

Dimethoate < LOQ 0.20 0.10 pass Ethoprophos < LOQ 0.20 0.10 pass

Etofenprox < LOQ 0.40 0.10 pass Etoxazole < LOQ 0.20 0.10 pass

Fenoxycarb < LOQ 0.20 0.10 pass Fenpyroximate < LOQ 0.40 0.10 pass

Fipronil < LOQ 0.40 0.10 pass Flonicamid < LOQ 1.0 0.40 pass

Fludioxonil < LOQ 0.40 0.10 pass Hexythiazox < LOQ 1.0 0.40 pass

Imazalil < LOQ 0.20 0.10 pass Imidacloprid < LOQ 0.40 0.20 pass

Kresoxim-methyl < LOQ 0.40 0.10 pass Malathion < LOQ 0.20 0.10 pass

Metalaxyl < LOQ 0.20 0.10 pass Methiocarb < LOQ 0.20 0.10 pass

Methomyl < LOQ 0.40 0.20 pass MGK-264 < LOQ 0.20 0.10 pass

Myclobutanil < LOQ 0.20 0.10 pass Naled < LOQ 0.50 0.20 pass

Oxamyl < LOQ 1.0 0.40 pass Paclobutrazole < LOQ 0.40 0.20 pass

Parathion-Methyl < LOQ 0.20 0.20 pass Permethrin < LOQ 0.20 0.10 pass

Phosmet < LOQ 0.20 0.10 pass Piperonyl butoxide < LOQ 2.0 1.0 pass

Prallethrin < LOQ 0.20 0.20 pass Propiconazole < LOQ 0.40 0.20 pass

Page 1 of 10Test results relate only to the parameters tested and to the samples as received by the laboratory. Test results meet all requirements of NELAP and the Pixis quality assurance plan unlessotherwise noted. This report shall not be reproduced, except in full, without the written consent of this laboratory. Samples will be kept a maximum of 15 days from the report date unless priorarrangements have been made.

Testing in accordance with: OAR 333-007-0400


503-254-1794

Job Number:

Report Date:

ORELAP#:

03/27/2018

OR100028

16:11Received: 03/22/18

18-001589

Report#: 037364-00

Purchase Order:

Pesticides Batch 1801375Method AOAC 2007.01 & EN 15662 (mod) Units mg/kg Analyze 3/26/18 12:00:00

LOQAnalyte Result Limits Status Notes LOQAnalyte Result Limits Status Notes

Propoxur < LOQ 0.20 0.10 pass Pyrethrins < LOQ 1.0 0.50 pass

Pyridaben < LOQ 0.20 0.10 pass Spinosad < LOQ 0.20 0.10 pass

Spiromesifen < LOQ 0.20 0.10 pass Spirotetramat < LOQ 0.20 0.10 pass

Spiroxamine < LOQ 0.40 0.10 pass Tebuconazole < LOQ 0.40 0.20 pass

Thiacloprid < LOQ 0.20 0.10 pass Thiamethoxam < LOQ 0.20 0.10 pass

Trifloxystrobin < LOQ 0.20 0.10 pass




503-254-1794

Job Number:

Report Date:

ORELAP#:

03/27/2018

OR100028

16:11Received: 03/22/18

18-001589

Report#: 037364-00

Purchase Order:

AbbreviationsLimits: Action Levels per OAR-333-007-0400, OAR-333-007-0210, OAR-333-007-0220Limit(s) of Quantitation (LOQ): The minimum levels, concentrations, or quantities of a target variable (e.g., target analyte) that can be

reported with a specified degree of confidence.

Units of Measure

g = Gram

mg/kg = Milligram per kilogram

% wt = µg/g divided by 10,000

Derrick TannerGeneral Manager

Approved Signatory




503-254-1794

Job Number:

Report Date:

ORELAP#:

03/27/2018

OR100028

16:11Received: 03/22/18

18-001589

Report#: 037364-00

Purchase Order:




503-254-1794

Job Number:

Report Date:

ORELAP#:

03/27/2018

OR100028

16:11Received: 03/22/18

18-001589

Report#: 037364-00

Purchase Order:

Code Explanation

Q Matrix interferences affecting spike or surrogate recoveries.

Q1 Quality control result biased high. Only non-detect samples reported.

Q2 Quality control outside QC limits. Data considered estimate.

Q3 Sample concentration greater than four times the amount spiked.

Q4 Non-homogenous sample matrix, affecting RPD result and/or % recoveries.

Q5 Spike results above calibration curve.

Q6 Quality control outside QC limits. Data acceptable based on remaining QC.

R Relative percent difference (RPD) outside control limit.

R1 RPD non-calculable, as sample or duplicate results are less than five times the LOQ.

R2 Sample replicates RPD non-calculable, as only one replicate is within the analytical range.

LOQ1 Quantitation level raised due to low sample volume and/or dilution.

LOQ2 Quantitaion level raised due to matrix interference.

B Analyte detected in method blank, but not in associated samples.

B1 The sample concentration is greater than 5 times the blank concentration.

B2 The sample concentration is less than 5 times the blank concentration.

Explanation of QC Flag Comments:



7405 sw tech center dr ste a160 tigard, or 97223 (855) 800 ... · orelap id: 4077 7405 sw tech...

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