viacom inc. epa region 5 records ctr. · viacom inc. epa region 5 records ctr. 253775 dorothy m....

Viacom Inc. EPA Region 5 Records Ctr.

253775Dorothy M. Alke412.642.2562

VIACOMOctober 5, 2005

To: DISTRIBUTION

Re: Surface Water, Flow and Water Level MonitoringFourth Quarter 2004Lemon Lane Landfill, Bloomington, Monroe County, Indiana

1.0 BACKGROUND

This report summarizes the results of groundwater, surface water and water level monitoring workcompleted by Viacom Inc. during the fourth quarter of 2004 at the Lemon Lane Landfill site.

Monthly and quarterly groundwater and surface water monitoring was performed at a total of sixlocations (springs and streams) in accordance with monitoring requirements outlined in the April2003 Long-Term Groundwater Monitoring Plan for Lemon Lane Landfill, QAPjP Volume XXXIII.Continuous monitoring of water levels was also performed at six locations.

2.0 SURFACE WATER MONITORING

The monitoring work described in this report was performed on November 18 and December 16,2004 and January 28, 2005. This three month time period constitutes the fourth reporting quarterfor Lemon Lane Landfill for 2004.

Scope of Work

The scope of surface water sampling for this monitoring period comprised monthly and quarterlysampling stipulated in the Long-Term Groundwater Monitoring Plan, as summarized in Table 1.

Surface water sampling was performed at the following locations:

Quarry Springs (monthly)Illinois Central Spring (monthly)Slaughterhouse Spring (quarterly)Quarry A SpringQuarry A +C Springs, andQuarry B Spring

The approximate locations of these stations are shown on Figure 1, Monitoring and SamplingLocations.

October 5, 2005

Quarry Springs Observation and Sampling

There are several spring emergences that are collectively known as the Quarry Springs.Historically, the three main ones have been referred to as Quarry A, Quarry B and Quarry CSprings. The monthly monitoring samples have been samples of the combined discharges of all ofthe Quarry springs flowing at the time of sample collection. Since January 2004, observations offlow conditions in the Illinois Central swallowhole area and the Quarry Springs area have been aroutine part of the monthly non-storm monitoring and sampling routine.

Beginning with the September 2004 monthly sampling event, separate samples from Quarry BSpring and from the Quarry A+C Springs combined flow were collected when adequate flowconditions were observed. In November 2004, Quarry A Spring was added to the list of springs tobe sampled monthly, adequate flow permitting.

Sample Collection and Handling

Samples at the spring locations were collected by carefully filling a new disposable beaker. Thewater was transferred from the beaker into pre-cleaned amber glass 1-liter bottles supplied by theanalytical laboratory. Routine sampling parameters including temperature and conductivity weremeasured and recorded. Spring flow was also estimated and recorded.

Samples were analyzed by Heritage Lab of Indianapolis, Indiana. The samples were analyzed to adetection limit of 0.1 parts per billion (ppb) for all PCB parameters (except Aroclor 1221; detectionlimit 0.2 ppb) by EPA SW-846 method 8082. Samples were also analyzed for total suspendedsolids (TSS) by EPA method 160.2.

Quality Assurance

For quality assurance purposes a duplicate sample and a field blank were collected during eachsampling event. All environmental and blank samples were labeled and logged onto a chain ofcustody form. The samples were stored and transported on ice in insulated coolers. Custody of thewater samples was maintained by Viacom until shipment to the analytical laboratory. SamplesLL12190, LL12233 and LL12370 were the field blanks for the sampling events reported herein. NoPCBs were detected in any of these blank samples.

Analytical Results for Surface Water Samples

Field parameter measurements, PCB analytical results, and QA/QC results for water samplescollected during this reporting period are reported in Table 2 - Quarry Springs (combined flow),Table 3 - Quarry Springs (individual springs), Table 4 - Illinois Central Spring, and Table 5 -Slaughterhouse Spring (attached). Historical (post-remediation) results are also provided in thesetables. Copies of the chain-of-custody forms are provided in Appendix A. Copies of thecertificates of analysis are provided in Appendix B. A validation summary for these samples

October 5, 2005

appears in Appendix C. Copies of the field sampling data sheets are on file at PSARA'sBloomington Branch Office.

3.0 CONTINUOUS FLOW AND WATER LEVEL MONITORING

The purpose of flow and water level monitoring is to evaluate site-specific data characterizing sitehydrologic response under storm and non-storm conditions, and to evaluate correlations betweenPCB concentrations, spring flow and groundwater elevations.

Scope of Work

The scope of groundwater level and flow monitoring during this reporting period involved the useof dedicated instrumentation to record water level and other parameters as summarized in Table 6.Water lever transducers, water level data logging equipment, and piezometer crest gauges wereoperated during all or part of the period from November 2004 through January 2005. Theapproximate locations of the stations in which these instruments were used are shown on Figure 1,Monitoring and Sampling Locations.

Flow and Water Level Plots

The following plots of the monitored stations for this reporting period are attached:

water elevation and temperature at MW-6, PZ-H and PZ-Iwater elevation, temperature and specific conductance at MW-20water temperature and specific conductance at Illinois Central Spring Emergence

Quality Assurance

As a quality assurance check, rainfall records for this time period were obtained from the PurdueUniversity State Climatologist's web site (http://shadow.agry.purdue.edu/sc.index.htnil) for the raingauge station at the Monroe County Airport. This record was obtained for comparison to the siterain gauge data, which is located outside the PSARA office. Raw rainfall data from the web siteappears in Appendix D. Monroe County Airport rain events of approximately 0.25" or more areindicated on the attached data plots.

As a further data quality check, manual water level measurements were made after significant stormevents and specific conductance was spot checked at four locations. The purpose of the manualchecks was to verify instrument readings. Manual field check data collected during this reportingquarter are shown on the data plots.

A complete instrument maintenance log for all of the Lemon Lane Landfill installations is attachedas Appendix E. This log details the installation, re-indexing, and maintenance histories of eachtransducer and data logger present at Lemon Lane Landfill during the third quarter.

October 5, 2005

Discussion

The subsequent plots are annotated with details of when the instrumentation was installed orremoved, or other field activities of interest.

Crest Gauges

Crest gauges in landfill cap piezometers PZ-AD, PZ-AS, PZ-BD, and PZ-BS were monitoredduring the fourth quarter of 2004. Results presented in Table 7 indicate no apparent movement ofthe gauges in PZ-AS and PZ-BS during this quarter, which means that no significant amount ofwater was observed in these piezometers during this monitoring period. The gauges in PZ-AD andPZ-BD indicated that a slight amount of water was in the bottom of those piezometers during atleast a portion of this monitoring period.

If you have questions regarding the sampling and flow/water level monitoring activities or findingsfor this reporting quarter, please call Mike McCann at (812) 335-0424.

Sincerely,

M. AlkeProject DirectorBP:05-0060

Attachments

TABLES

Table 1. Scope of Groundwater, Surface Water and Other Monitoring Activitiesfor the Lemon Lane Landfill

Monitoring Station Parameter3 Frequency Other Requirements/ Comment

Routine Monitoring

Illinois Central Spring

Quarry Spring

Slaughterhouse Spring

PCB, T, C Monthly non-storm Measure conductivity and flow bycontinuous monitoring; by hand duringsampling.

PCB, TSS Quarterly non-storm Install small weir or flume; measureconductivity by hand and estimate flowusing staff gauge.

Storm Sampling

Illinois Central Spring PCB, Flow,T, C, TSS

At least two (2)events per year

At least 1,200 gpm flow from ICS

Slaughterhouse Spring PCB, Flow, Two (2) storm events 1) at least 1,200 gpm flow at ICST C TSS51 2) peak flow < 230 gpm at ICS

Piezometer Monitoring

PZ-AS, AD, BS, BD W Quarterly Crest gauges or continuous levelrecorder if significant water develops

Well Monitoring

MW-6 W Continuous Continuous level recorder

Fish / Sediment Sampling

Clear Creek and ICS/QSBranch of Clear Creek

PCB, TSS Second half of 2005 Scope comparable to 1996 event;sampling plan to be developed.

Parameters: PCB=polychlorinated biphenyl; W=water level; T=temperature; C=conductivity; TSS= Total Suspended Solids.

Table 2. Post-Remediation PCB ResultsQuarry Springs, Combined

Lemon Lane Landfill, Bloomington, Indiana

Sample ID

LL12369

LL12229

LLI2I87

LL.I2I50

LLI2144

LL12116

LL 12081

LLI 1996

LLII771

LL1I738

LLII554

LLI 1550

Ll.11546

LL1154I

LL1I378

LLI 1256

LI. II 203

LLI 11 72

LLIII25

LLI1120

LLI1I16

LL11099

LL11077

LLII072

LLI 1065

LL 10970

LLI0965

LLI 09 60

LL10943

LL10914

LL10896

LL10883

LLI0861

LL10788

LLI0764

LLI 0745

LLI 0724

LLI0719

LLI0465

LLI0456

LLI 0451

LLI 03 79

LL10351

LLI 0204

LL10I43

LLI0078

LLI 0063

LLI 0042

Sampling Date

28-Jan-05

!6-Dec-04

18-Nov-04

06-Oct-04

09-Sep-04

06-Aug-04

!6-Jul-04

14-Jun-04

05-May-04

!9-Apr-04

09-Mar-04

13-Feb-04

14-Jan-04

09-Dec-03

05-Nov-03

08-Oct-03

09-Sep-03

05-Aug-03

09-Jul-03

02-Jun-03

14-May-03

10-Apr-03

17-Mar-03

07-Feb-03

10-Jan-03

03-Dec-02

!2-Nov-02

ll-Oct-02

04-Sep-02

08-Aug-02

!7-Jul-02

IO-Jun-02

2l-May-02

ll-Apr-02

14-Mar-02

13-Feb-02

22-Jan-02

<B-Jan-02

19-Oct-Ol

13-Sep-OI

17-Aug-OI

27-Jul-OI

14-Jun-Ol

15-May-Ol

ll-Apr-OI

20-Mar-Ol

27-Feb-OI

17-Nov-OO

PCB",ppb

1.8

0.6

0.7

0.7

1.0

0.5

0.7

0.8

0.8

0.8

0.7

0.8

2.0

0.92

0.66

0.9

1

1.1

0.81

1.0

0.98

0.38

0.64

1.2

0.96

0.42

0.69

1.1

1.7

1.5

1.7

0.95

1.3

0.70

0.85

1.0

1.1

0.95

0.88

1.3

1.7

0.78

1.8

0.89

1.1

1.3

0.37

1.3

DataValidated?

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

TSS,

mg/L

77

30

35

29

55

25

14

18

27

24

16

29

50

35

27

25

44

27

9

37

I I

43

36

34

39

38

32

66

39

44

56

8

22

10

15

13

6

9

8

14

9

MR

60

46

30

4

7

13

Conductivity,uS/cm

665

661

700

746

726

727

612

685

713

691

639

733

611

645

728

734

671

678

719

708

544

689

643

784

660

710

622

704

729

695

683

482

576

604

467

604

724

680

642

646

620

768

580

723

628

692

599

725

Temperature,degC

10.8

12.1

15.2

16.0

17.0

18.3

15.9

17.5

15.2

14.8

12.0

10.4

10.9

12.6

13.8

16.0

17.2

16.5

20.1

14.0

14.2

13.6

13.0

9.3

10.0

8.8

13.5

16.0

19.3

21.5

17.9

19.6

13.3

14.0

13.5

12.3

11.4

12.6

14.8

17.1

20.9

20.8

17.0

23.2

15.4

12.3

11.4

10.2

Flowb,gal/min

I35C

150

70

15

40

30

300

60

50

70

400

200

200

150

120

50

60

150

30

150

800

200

200

40

50

20

90

70

25

20

50

140

NR"125

300

100

15

10

80

50

12

15

100

NR"

225

NR"NRJ

NR""Samples were analyzed to a detection l imit of 0.1 parts per billion (ppb) for all PCB parameters except Aroclor 1221 (detection

limit 0.2 ppb or 0.5 ppb). Other detection limits may occasionally result from non-normal sample volumes, dilutions, etc.bFlow estimated visual ly .

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Table 4. Post-Remediation PCB ResultsI l l inois Central Spring


Sample ID

LLI2373

LLI2374(DUP)

LL12234

LL12235(DUP)

LL12192

LLI2I93(DUP)

LLI2153

LL12I54(DUP)

LL12148

LLI2I49(DUP)

LL12113

LL12I14(DUP)

LL 12083

l.L12084(DUP)

LLII998

LL11999(DUP)

L L I I 7 7 3

LL1I774(DUP)

LL11740

LL1I741(DUP)

LL 11555

LLI!556(DUP)

LL11552

L,L11553(DUP)

LL11548

LL11549(DUP)

LLI1543

1,LI1544(DUP)

LLI1380

LLI1381(DUP)

LL1I258

I.L1 I259(1XJP)

LL1 1205

LL1 1206(DUP)LL1M74

L L I I I 7 5 ( D U P )

L L 1 I I 2 7

LL11I28(DUP)

L L 1 I 1 2 1

LLM122(DUP)

L L 1 1 1 1 8

LL11119(DUP)

L L U I O O

L L I H O I ( D U P )

LL1I078

LLI1079(DUP)

LL11073

LL1 1074(DUP)

LL1I066

LL11067(DUP)

LL10971LL10972(DUP)

SamplingDate

28-Jan-05

28-Jan-05

16-Dec-04

16-Dec-04

lS-Nov-04

l8-Nov-04

6-Oct-04

6-Oct-04

9-Sep-04

9-Sep-04

6-Aug-04

6-AUR-04

!6-Jul-04

16-Jul-04

U-Jun-04

14-Jun-04

5-May-04

5-May-04

19-Apr-04

19-Apr-04

9-Mar-04

9-Mar-04

13-Feb-04

13-Feb-04

14-Jan-04

14-Jan-04

9-Dec-03

9-Dec-03

5-Nov-03

5-Nov-03

8-Oet-03

8-Oct-03

9-Sep-03

9-Sep-03

5-Aug-03

5-Aug-03

9-Jul-03

9-Jul-03

2-Jun-03

2-Jun-03

l4-May-03

14-May-03

IO-Apr-03

IO-Apr-03

1 7-Mar-03

!7-Mar-03

7-Feb-03

7-Feb-03

10-Jan-03

10-Jan-03

3-Dec-023-Dec-02

PCBa.

ppb

17

16

6.4

6.5

15

18

20

19

16

17

11

10

5.1

10

17

14

9.1

12

19

20

6.4

5.7

6.1

5.5

15

16

7.8

7.8

10

9.7

10

10

9.7

9.8

7.9

8.2

16

12

15

16

4.7

4.1

4.9

4.9

3.8

2.5

1 1

1 1

8.9

7.4

14

14

Data

Validated?

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

YY

TSS,mg/L

< 1< i< i< i

2

4

< 1

< 1

< l

< 1

< 1

< 1

< 1

< \

3

< 1

< 1

< 1

< 1

NR

< 1

< 1

< 1

< 1

< 1

< 1

< 1

2

< 1

< 1

< 1

< 1

< |

< I

< 1

< 1

5

5

< 1

< 1

2

3

3

< 1

< 1

2

< 1

< 1

<1

<1

<1

7

Conductivity,uS/cm

679

679

664

664

730

730

791

791

733

733

732

732

616

616

695

695

738

738

693

693

627

627

696

696

612

612

642

642

726

726

760

760

659

659

688

688

743

743

720

720

574

574

703

703

617

617

793

793

639

639

727727

Temperature,degC

12.7

12.7

13.1

13.1

13.3

13.3

13.1

13.1

13.2

13.2

13.1

13.1

13.5

13.5

13.0

13.0

12.7

12.7

13.0

13.0

12.6

12.6

12.7

12.7

12.6

12.6

13.1

13.1

13.1

13.1

13.5

13.5

14.0

14.0

13.5

13.5

13.2

13.2

13.0

13.0

12.8

12.8

12.8

12.8

12.6

12.6

12.8

12.8

13.0

13.0

13.113.1

Flow,gal/min

120"

120C

150C

150C

110C

110°

20"

20"

50"

50"

40"

40"

150b

!50h

60"

60"

90"

90"

120b

120b

250h

250h

290'

290C

250h

250b

180C

180C

70C

70'

80C

80C

110C

HO"

100C

100C

50b

50"

63C

63C

325C

325C

I35C

135C

300h

300h

60"

60"

I50b

150h

35"35"

continued

Table 4. Post-Remediation PCB ResultsIllinois Central Spring


Sample ID

LL 10966

LL10967(DUP)

LL1096I

LL 10962 (DUP)

LL 10945

LL 10946 (DUP)

LL10916

LL10917(DUP)

LL 10898

LL10899 (DUP)

LL10885

LL 10886 (DUP)

LL 10863

LL 10864 (DUP)

LL 10790

LL10791 (DUP)

LL 10766

LL 10767 (DUP)

LL 10746

LL 10747 (DUP)

LL 10725

LL 10726 (DUP)

LL 10720

LL 10723 (DUP)

LL 10466

LL 10467 (DUP)

LL 10457

LL 10458 (DUP)

LL10452

LL10453 (DUP)

LLI0380

LL10381 (DUP)

LL10352

LL10353(DUP)

LL 10205

LL 10206 (DUP)

LL10144

LL 10 145 (DUP)

LL 10079

LL 10080 (DUP)

LL 10061

LL 10062 (DUP)

LLI0057

LL10058(DUP)

LL 10049

LL 10050 (DUP)

LL 10043

LL10044

SamplingDate

12-Nov-02

12-Nov-02

ll-Oct-02

ll-Oct-02

4-Sep-02

4-Sep-02

8-Aug-02

8-Aug-02

17-Jul-02

17-Jul-02

10-Jun-02

10-Jun-02

21-May-02

21-May-02

ll-Apr-02

ll-Apr-02

14-Mar-02

14-Mar-02

13-Feb-02

13-Feb-02

22-Jan-02

22-Jan-02

3-Jan-02

3-Jan-02

19-Oct-OI

19-Oct-Ol

13-Sep-Ol

13-Sep-Ol

17-Aug-Ol

17-Aug-Ol

27-Jul-Ol

27-Jul-Ol

14-Jun-Ol

14-Jun-Ol

15-May-Ol

15-May-Ol

ll-Apr-01

11-Apr-OI

20-Mar-Ol

20-Mar-Ol

27-Feb-Ol

27-Feb-Ol

31-Jan-Ol

31-Jan-Ol

20-Dec-OO

20-Dec-OO

17-Nov-OO

17-Nov-OO

PCBa,ppb

4.7

4.9

12

13 .

22

22

21

20

19

19

8.5

9.2

7.9

7.2

3.6

3.8

4.8

4.6

10

9.3

21

14

9.5

14

5.7

5.6

8.9

8.8

11

13

9.3

8.8

13

14

20

1714

14

14

15

2.9

4.3

4.9

5.6

5.3

5.2

8.38.5

DataValidated?

YY

YY

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

YY

Y

Y

Y

Y

Y

Y

Y

Y

Y

YY

TSS,mg/L

<1<1<1<1<13

<1

<1

<1

4

<1

<1

<1

<1

<1

<1

<1

<1

<1

<1

<1

2

<1

<1

<\

2

<1

<1

<1

<1

NR

MR

2

4

12

127

2<1

<1

3

3

4

<1

<1

<1

<1

<1

Conductivity,uS/cm

598

598

723

723

775

775

745

745

705

705

565

565

567

567

583

583

525

525

585585

723

723

677

677

601

601

653

653

645

645

762

762

588588

718

718632

632

700700

584

584

520

520

852

852

685685

Temperature,degC

13.6

13.6

13.8

13.8

13.4

13.4

13.5

13.5

13.3

13.3

13.4

13.4

12.9

12.9

12.8

12.8

12.9

12.9

13.0

13.0

13.1

13.1

13.1

13.1

14.0

14.0

14.1

14.1

13.5

13.5

13.7

13.7

13.4

13.4

I3.I

13.1

13.1

13.1

12.7

12.7

12.7

12.7

12.8

12.8

13.2

13.2

13.5

13.5

Flow,gal/min

80b

80b

60"60"

30C

30C

25b

25b

50"

50b

190C

190C

280°

280C

225C

225C

300b

300b

150b

150b

20b

20b

130b

130b

139b

139b

100b

100b

15b

15"

15b

15b

125b

125b

40b

40"240b

240"

93"

93"

280b

280b

830b

830b

360b

360b

160b

160"

"Samples were analyzed to a detection limit of 0.1 parts per billion (ppb) for all PCB parameters except Aroclor 1221 (detectionlimit 0.2 ppb or 0.5 ppb). Other detection limits may occasionally result from non-normal sample volumes, dilutions, etc.

bFlow estimated visually."Flow estimate from 1CS Treatment Facility instrumentation.NR = Not reported.

Table 5. Post-Remediation PCB ResultsSlaughterhouse Spring


Sample ID

LLI2236

--

--

--

LL 12000

LLI1558

LLI1545

LL11260

LL11124

LL11103

LL11081

LL11076

LL11069

LL10974

LL 10969

LL 10964

LL 10947

LL 10920

LL 10904

LL10891

LL 10869

LL 10796

LL 10769

LL 10749

LL10728

LL10722

LL 10469

LL 10460

LL 10455

LL 10383

LLI0355

LL 10208

LL10I47

LL 10076

LL 10064

LL 10059

LL 10051

LL 10045

SamplingDate

!6-Dec-04

1 8-Nov-04

06-Oct-04

09-Sep-04

14-Jun-04

09-Mar-04

09-Dec-03

08-Oct-03

02-Jun-03

10-Apr-03

1 7-Mar-03

07-Feb-03

IO-Jan-03

03-Dec-02

12-Nov-02

ll-Oct-02

04-Sep-02

08-Aug-02

17-Jul-02

]0-Jun-02

2l-May-02

ll-Apr-02

14-Mar-02

13-Feb-02

22-Jan-02

03-Jan-02

19-Oct-OI

13-Sep-OI

17-Aug-Ol

27-Jul-Ol

14-Jun-OI

15-May-Ol

l l -Apr-01

20-Mar-Ol

27-Feb-Ol

31-Jan-Ol

20-Dec-OO

1 7-Nov-OO

PCBa,ppb

< O . I O

~"--

<0.1

<0.1

<0 . l

<0.1

<0. l

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.1

<0.l

<0.l

<0.1

<0.1

<0.1

<0.1

<0.1

<0.l

<0.l

<0.1

<0.1

<0.1

0.11

<0.1

<0.1

<0.1

<0.1

0.13 J

0.14J

DataValidated?

Y

--

--

--

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

TSS,mg/L

3

-

-

-

68

3

1 1

9

29

51

20

14

27

16

27

< 1

10

33

21

55

23

14

13

13

14

15

18

20

60

NR

46

45

29

9

19

17

67

22

Conductivity,uS/cm

902

--

-

-

980

816

909

990

954

968

891

1440

916

911

845

928

868

886

898

835

832

833

756

796

907

877

890

904

929

1046

841

952

882

936

726

788

828

957

Temperature,degC

10.3

--

--

-

16.3

11.5

13.1

15.3

14.2

14.0

14.0

5.7

8.5

6.7

12.9

16.7

21.9

19.9

18.6

14.4

13.0

12.8

12.5

12.0

11.6

12.2

14.5

16.0

17.6

16.2

14.5

14.8

13.0

11.6

10.1

11.2

12.5

13.4

Flowb,gal/min

15

DRY

DRY

DRY

2°

23C

13C

3.51

25

20

50

15

20

5

8

8

2

2

5

15

50

20

10

10

4

5

12

2

3

3

8

2

5

2

25

20

15

5

Samples were analyzed to a detection l imi t of O.I parts per billion (ppb) foil imi t 0.2 ppb or 0.5 ppb). Other detection limits may occasionally resu

Flow estimated visually.cFlow measured by V-notch weir.NR = Not reported.

J = Estimated value. The QA/QC data indicated an analytical bias.

>r all PCB parameters except Aroclor 1221 (detection

from non-normal sample volumes, dilutions, etc.

Table 6. Continuous Flow and Water Level MonitoringViacom Inc.

Lemon Lane Landfill, Bloomington, Monroe County, Indiana

Monitoring Station Parameter Reported Monitoring Period Instrument

Illinois Central Sp

MW-6

MW-20

Piezometer AD

Piezometer AS

Piezometer BD

Piezometer BS

Piezometer H

Piezometer I

Conductivity

Temp

Water level/ temp

Water level/ temp/ conductivity

Water level

Water crest

Water crest

Water crest

Water crest

Water level/ temp

Water level/ temp

All Quarter

11/1-12/25 and 1/14- 1/31

All Quarter

11/1-11/3

11/3 - 1/7

All Quarter

All Quarter

All Quarter

All Quarter

11/17-1/31

11/1-11/17

EZLogger9000

Troll 4000

Troll 8000

Mini-Troll

Crest Gauge

Crest Gauge

Crest Gauge

Crest Gauge

Troll 4000

Troll 4000

Table?. Crest Gauge DataViacom Inc.


Piezometer AD

Date ApparentMovement (ft)

11/14/02

12/2/02

12/13/02

12/30/02

1/13/03

1/28/03

2/11/03

2/20/2003

3/5/2003

3/21/2003

4/7/2003

4/23/2003

5/8/2003

5/19/2003

6/5/2003

6/20/2003

7/2/2003

7/16/2003

7/31/2003

8/14/2003

9/3/2003

9/1 1/2003

9/29/2003

10/9/2003

10/23/2003

None

None

None

None

None

None

None

None

None

None

None

None

None

0.45'

None

0.35'

None

1.35'

None

None

None

None

None

None

None

Piezometer AS

ApparentMovement (ft)

None

None

None

None

None

1

i

None

None

None

None

None

None

None

None

None

None

None

None

None

None

None

None

None

None

Piezometer BS

ApparentMovement (ft)

None

None

None

None

None

None

None

None

None

None

None

None

None

None

None

None

None

None

None

None

None

None

None

None

None

continued

Table 7. Crest Gauge Data - continuedViacom Inc.


Piezometer ADDate Apparent

Movement (ft)11/7/200311/26/200312/8/2003

12/31/20031/15/20042/4/20042/13/20043/2/2004

3/12/20044/9/2004

4/23/20045/10/20045/21/20046/10/20046/24/20047/12/20047/29/20048/10/20048/30/20049/9/200410/6/2004

10/21/200412/7/2004

NoneNoneNoneNone0.46

NoneNoneNoneNoneNoneNoneNoneNoneNoneNoneNoneNoneNoneNoneNoneNoneNone0.2

Piezometer ASApparent

Movement (ft)NoneNoneNoneNoneNoneNoneNoneNoneNoneNoneNoneNoneNoneNoneNoneNoneNoneNoneNoneNoneNoneNoneNone

Piezometer BDApparent

Movement (ft)2

2

2

2

2

2

2

2

NoneNoneNone0.28NoneNoneNoneNoneNoneNoneNoneNoneNoneNone0.24

Piezometer BSApparent

Movement (ft)NoneNoneNoneNoneNoneNoneNoneNoneNoneNoneNoneNoneNoneNoneNoneNoneNoneNoneNoneNoneNoneNoneNone

1 Crest gauge could not be removed from Piezometer AS on this date, possibly due to abuild-up of ice in the PVC casing.2Crest gauge was installed in PZ-BD on 3/8/2004; no readings are available prior to that date.

FIGURES

SlaughterhouseSpring

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\

TECHNOLOGIES INC.

A^S sP"°g©M/r-5 Monitoring Well

Piezometer"®'Z»3

U] DB-389

(S) Rain Gauge

>—•— Landfill Perimeter Fence

*—*— Chain Link Fence

Survey ControlPoint

VIACOM, Inc.

Figure 1.Monitoring and Sampling Locations

Lemon Lane LandfillBloomington, Indiana

Drawn By:RLR

Date:

3/2/04Scale:

l'=450'

CONTINUOUS MONITORING WATER LEVEL PLOTS

Illinois Central Spring Emergence11/1/2004 0:00 to 11/30/2004 23:00

1600

1-Nov 6-Nov 11-Nov 16-Nov

2004

21-Nov 26-Nov

oc3

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1-Dec

•Specific Conductance * Airport Rain Events Airport Cumulative Rainfall


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21-Nov 26-Nov 1-Dec

•Water Temperature * Airport Rain Events Airport Cumulative Rainfall


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CO

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T3COoo

1600

1400

1200

1000

800

600

Q.CO

400

200

0-P

12/21 data gap caused by a delay inthe start of a logging program.

A large mass of algae was removed from the conductivity sensor on 12/10,resulting in a 12% drop in conductivity readings from the EZLogger.

1-Dec 6-Dec 11-Dec 16-Dec

2004

21-Dec

12/29-31 responsecaused by snow melt.

8

6 OC3

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, CD

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26-Dec 31-Dec

•Specific Conductance A Hand Measurements * Airport Rain Events Airport Cumulative Rainfall


O

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13.75

13.5

12.5

12.25

1-Dec

EZLogger stopped recording accurate temperature readingson 12/25 when a wire became disconnected.

12/21 data gap caused by a delayin the start of a logging program.

6-Dec 11-Dec 16-Dec

2004

21-Dec 26-Dec

8

7

5 5.

Oc

c_Q)

(D

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I

31-Dec

•Water Temperature A Hand Measurements * Airport Rain Events Airport Cumulative Rainfall


1600

31-Jan

•Specific Conductance A Hand Measurements » Airport Rain Events Airport Cumulative Rainfall


o0)

14

13.75

13.5

0) 13.25

•+-•to

EZLogger began recording temperature readings again on 1/14 after repairswere made following the 12/25 wire disconnection incident.

6 Oc3

5 £

31-Jan

•Water Temperature A Hand Measurements * Airport Rain Events Airport Cumulative Rainfall

Lemon Lane Landfill MW-611/1/2004 0:00 to 11/30/2004 23:00

840

835

coI_0)LLJ

I

830

825

820

815


2004

21-Nov 26-Nov

O

1-Dec

•Water Elevation A Hand Measurements * Airport Rain Events Water Temperature


840

835

Co

£LJJ

I

830

825

820


2004

21-Dec

Response on 12/29-31caused by snow melt.

- 12.50)

12 3:- 11.5

Q.(D(Q

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10.5

26-Dec 31-Dec

•Water Elevation A Hand Measurements » Airport Rain Events Water Temperature


840

815

1-Jan 6-Jan 11-Jan 16-Jan

2004

21-Jan 26-Jan 31-Jan



OO~J

830 -

£*

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CO

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M-*

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The Troll 8000 unit was removed and a mini-_ Troll was installed at this station on 11/3. :

f\ „I * — - — . , - /^ ;-

Jov 6-Nov 11-Nov 16-Nov 21-Nov 26-Nov 1-C

2004

Water Elevation A Hand Measurements * Airport Rain Events Water Temperature

- IH

- 13.9

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13.7 ft

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l[\_ _ ^_:

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Water Elevation A Hand Measurements » Airport Rain Events Specific Conductance

- oof

- 866.5

- 866

- 865.5

- 865

864.5

- 864

- 863.5

- 863

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(uS

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835


830

825

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re820

12/7 elevation dip caused by storm pumping test.

Response on 12/29-31caused by snow melt.

815


2004

21-Dec 26-Dec 31-Dec

Water Elevation * Airport Rain Events A Hand Measurements

835


830

825

Transducer was removed on 1/7 for use at another location.

CO>wu.0)

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820

815

810


2005

21-Jan 26-Jan 31-Jan

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Lemon Lane Landfill Piezometer H11/1/2004 0:00 to 11/30/2004 23:00

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o*tt

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HERITAGEJO ENSURE PROPER HANDLING OF SAMPLES PLEASE COMPLETE THE SHADED AREAS OF THIS FORM

HERITAGE ENVIRONMENTAL SERVICES, LLC. iCOMMERCIAL LABORATORY OPERATIONS 1-18913

7901 West Morris Street Indianapolis IN 46231www.heritage-enviro.com (800)827-4374 Fax: (317)486-5095

Customer name/number: \///r £ O/^ Submitter #

Project Name: L~^.v^^\ l_7tt-i*_

Z Quote No: (Given to you by your contact)

PO No. or Project/ Activity ID: /f L- $ / 7 7' * c F — ' — ' —

PRINT HERITAGE TSR NAME:

CUSTOMER STATUS: New / Existing

If no previous credit has been established with Heritage,

prepayment (check,VISA,etc) is required at thetime of sample submittal to the laboratory.

Sampled By: . , / i/I/. Vc^>4q\^f(V(

DateSampled

IHW

~« .

Timesampled

/ 7 '<//"! AM

/5JST"pM/ $QO PM/Y:/5^PM/ / ^ i o <-— AM

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LL/ZI87LUZ./86LL/Z,/d9Lt-IZ,lWLLf2.IVLLlZ-ltfZ-LLI2.113

ReltRQUshed by: {Signature/ Dale/Time

Relinquished by: (jflgnature ) Date/Time

Relinquished by: (Signature ) Data/Time

Received for Lab by (Signature) / / /

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(Note special detection limits or methods )

£Yv£

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DislrlbulloiY^Vhlle original and YeJ^w cspjes-tCLacccfnpany sample to the laboratory.Pink copy to be retained bv^hexdtent. / ^^^

Laboratory use onlyCustody seals present/intact?

Broken containers?

COC agree with sample labels?

Correct containers for testing?

Headspace issues acceptable?

Holding time(s) acceptable?

Preservative pH's acceptable?

Was pH left unadjusted?

Yes No

^

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Fax: ( )E-mail:

Sample Turn Around TimeStandard: Rush Date / /

Mo Day Yr

(Accelerated TAT subject to Additional Charge)( Date must be Accepted and Approved bv Lab )

Remarks:

Lab use onlySample No.

1{J£L\D$(D(p(03-IDS'irtno

>/ Ui^i- • •* —

Comments:

HERITAGE

1-040 ^ ^v y

TO ENSURE PROPER HANDLING OF SAIvirLES PLEASE COMPLETE THE SHADED AREAS OF THIS FORM

HERITAGE ENVIRONMENTAL SERVICES, LLC.COMMERCIAL LABORATORY OPERATIONS ' 1-189237901 West Morris Street Indianapolis IN 46231

www.heritage-enviro.com (800)827-4374 Fax: (317)486-5095Customer name/number: V/ / /4-CO^ Submitter # "

Project Name: L-C-i o^ £-*.*$_

Z Quote No: (Given to you by your contact)

PO No. or Project/Activity ID: 8L<f>(77



If no previous credit has been established with Heritage,

prepayment (check,VISA,etc) is required at thetime of sample submittal to the laboratory.

Sampled By: , / / / /'/V . l/cu*£t\£n.

DateSampled

fl-f^'O4/

^-*-»

IZ-IT-O"!

R^nou

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( 5<O 0 PM

' 3 '. ($ PMi _ % _ AM

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l/^sf it ,-• // //il/#~ffak*^ /L"I7~OT'I / ' -DO

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Relinquished by: (Signature ) Dale/Time

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type

(M

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Distribution: While original and Yellow copies to accompany sample to the laboratory. ^-^Pink copy to be retained by the cllen .

Laboratory use onlyCustody seals present/intact?

Broken containers?







Yes No

^

,/S^

^

s^

^/^

/

Send Report To:

Go: l/r^COH^-f-MZ ,

Add : 2JO 2. tt/> l/<>s*« *J fflC<

-%O^K^ 3QV 7^o^-fAttn: MiKt- /McJLfrfvA.Phone: (//i- ) "3j<r-b^2- *f YesFax: ( )E-mail:

Sample Turn Around TimeStandard: Rush Date / /

Mo Day Yr

(Accelerated TAT subject to Additional Charge)( Date must be Accepted and Approved bv Lab 1

Remarks:

T)//) /serf <>£-*! 0

Comments:


/Us?1-15

•£1 k

t\7vi?\?~Zif>

^•L.\7-7X

4- 3-2-J.

®

TO ENSURE PROPER HANDLING OF SAMPLES PLEASE COMPLETE THE SHADED AREAS OF THIS FORM

HERITAGE ENVIRONMENTAL SERVICES, LLC. \COMMERCIAL LABORATORY OPERATIONS 1-33072

7901 West Morris Street 4ndianapolis IN 46231wvtf!jA?.heritage-enviro.corn (800)8^7-4374 Fax: (317)486-5095

Analyses Requested(Note special detection limits or methods 1

Send Report To

Project Name: L<a **. w La.* A



If no previous credit has been established with Heritage,prepayment (check,VISA,etc) is required at the

time of sample submittal to the laboratory.



Received by: (Signature) Laboratory use onlyCustody seals present/intact?

Broken containers?







Relinquished by; (Signature) Received by: (Signature)

Relinquished by: (Signature Received by: (Signature

Received for Lab by: (Signature)~ Temp. 3-J0N °C

Rot /Yes j NoDistribution: White original and Yellow copies to accompany sample to the laboratory.Pink copy to be retained by the client.

APPENDIX B

Certificates of Analysis

CERTIFICATE OF ANALYSISService Location

HERITAGE ENVIRONMENTAL SERVICES, LLCCOMMERCIAL LABORATORY OPERATIONS7901 W.MORRIS ST.INDIANAPOLIS, IN 46231(317)243-8304

Received

22-NOV-04

Completed

02-DEC-04

Printed

03-DEC-04

Project

4602

Lab ID

A682105

PO Number

BL0177

Sampled

18-NOV-04 13:40

Report To

MIKE MCCANNVIACOM, INC.2002 WEST VERNAL PIKEBLOOMINGTON, IN 47404

Bill To

BETH STEIGERWALDVIACOM, INC.11 STANWIX STREETPITTSBURGH. PA 15222

CLIENT ID: LL12187

MATRIX TYPE: NON-SPECIFIC WATER

SUBMITTER CODE: 2226

MATRIX: WS

LOCATION: LEMON LANE

BLANKET ORDER RELEASE: BL0177

Sample Description

PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW&

.Analyst M WRIGHT * * - " -1 / •?$, "''-•', Analysis

Parameter

INITIAL WEIGHT OR VOLUME

FINAL VOLUME

t isioc /^^L<j^|^£ffr/*i>V '".uV -Date- 23-NOV^M • " nltrufnefit PREP '^fa " *"^^st P230.1 .0

Result

1000

5.0

Det. Limit Units

mL

mL

PCB AROCLORS BY GAS CHROMATOGRAPHY/ECD SW846-8082 ^ „ 'V _ - _VL 1%J >" AJ ~* ^-^ JjNELAC'X r *

Analysts WOOD ^ * -J ' ' r^? ' Ans^s'lfPate 24-NOV-04 J5;43 Srui fe^ECD^ ^ &L^Soi pPrep PCB SEPARATORY FUNNEL UQUID-LIQUIDEXmAVflON*SW846^3510CP2301 0 " ''f' *^?"-»'?B?; ^-'^T'^t^^V^-

Parameter

PCB AROCLOR 1016

PCB AROCLOR 1221

PCB AROCLOR 1232

PCB AROCLOR 1242

PCB AROCLOR 1248

PCB AROCLOR 1254

PCB AROCLOR 1260

PCB AROCLOR 1262

SURROGATE RECOVERY

DECACHLOROBIPHENYL (DCB)

SUMMATION OF AROCLORS

Result

BDL

BDL

BDL

0.67

BDL

BDL

BDL

BDL

132.0

0.67

Det. Limit

0.10

0.20

0.10

0.10

0.10

0.10

0.10

0.10

0.20

Units

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

% Rec

ug/L

Page 1 of 2

uKSMWF]> I I/

HERITAGE ENVIRONMENTAL SERVICES, LLC Sample ID: A682105 LL12187

Degraded Aroclor 1242 with Aroclor 1248 characteristics.

TOTAL SUSPENDED SOLIDS EPA 160.2

Analyst M. GROTE Analysis Date: 24-NOV-04 00:15

'NELAC:Y , -" „ ,

TestG403.7.0

Parameter

SUSPENDED SOLIDS

Result

35

Det. Limit Units

mg/L

Sample Comments

BDL Below Detection Limit

Sample was received on ice at temperature 4 C.Sample chain of custody number 18913.

Heritage Environmental Services, LLC certifies that the test results

indicated as NELAC (National Environmental Laboratory Accreditation

Conference) accredited (Yes for NELAC) meet all requirements of NELAC and

Illinois EPA Part 186 unless otherwise explained or justified as to the

the exact nature of the deviations.

Heritage Environmental Services, LLC is accredited under Illinois NELAC

accreditation number 100401.

Additional copies of this report sent to:

RUSS CEPKO, VIACOM, INC11 STANWIX STREET. PITTSBURG, PA 15222-1384

Approved by: PAULINE SPENCE 03-DEC-04

Page 2 of 2


HERITAGE ENVIRONMENTAL SERVICES, LLCCOMMERCIAL LABORATORY OPERATIONS7901 W. MORRIS ST.INDIANAPOLIS, IN 46231(317)243-8304

Received

22-NOV-04

Completed

02-DEC-04

Printed

03-DEC-04

Project

4602

Lab ID

A682106

PO Number

BL0177

Sampled

18-NOV-04 13:55

Report To


Bill To

BETH STEIGERWALDVIACOM, INC.11 STANWIX STREETPITTSBURGH, PA 15222

CLIENT ID: LL12188



MATRIX: WS



Sample Description

PCB SEPARATORY.';;•• ' ••• . \<r&fZ! M^:iy'iW&: ml'f&^Analyst: M. WRIGHT ? a-t^sg-J^^-a^-^ej^ffift^

"S^rffc&sE'"^ sfiiT-i :,i,-:>Ks.l<3N.:S}rt ^3510g|

J^3sjy«!! ?.vl'*&«*«*,?£=«.•.&!

Parameter


FINAL VOLUME

Result

1000

5.0

Del. Limit Units

mL

niL

;B'

3>fep:>PCB SEPARAtORY FWNEl!||Qpro|;i| jff llj

Parameter

PCB AROCLOR 1016

PCB AROCLOR 1221

PCB AROCLOR 1232

PCB AROCLOR 1242

PCB AROCLOR 1248

PCB AROCLOR 1254

PCB AROCLOR 1260

PCB AROCLOR 1262

SURROGATE RECOVERY



Result

BDL

BDL

BDL

0.86

BDL

BDL

BDL

BDL

156.0

0.86

Det. Limit

0.10

0.20

0.10

0.10

0.10

0.10

0.10

0.10

0.20

Units

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

% Rec

ug/L

Page 1 of 2

{m/mHERITAGE ENVIRONMENTAL SERVICES, LLC Sample ID: A682106 LL12188



Analyst U. GROTE"- - -1 Analysis Date:24-NOV-04 00:15

• *"],,NELAC:Y

*

Test G403.7 0

Parameter

SUSPENDED SOLIDS

Result

51

Det. Limit Units

mg/L

Sample Comments











RUSS CEPKO, VIACOM, INC11 STANWIX STREET, PITTSBURG, PA 15222-1384


Page 2 of 2



Received

22-NOV-04

Completed

02-DEC-04

Printed

03-DEC-04

Project

4602

Lab ID

A682107

PO Number

BL0177

Sampled

18-NOV-04 14:00

Report To

MIKE MCCANNVIACOM, INC.2002 WEST VERNAL PIKEBLOOMINGTON. IN 47404

Bill To


CLIENT ID: LL12189



MATRIX: WS



Sample Description

PCB SEP ARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW846-3510C V ,r 4'4 V» * \'i4fej-* M~''-- A>H <' • : ' • • : ? • ' • -i ^ ; ^ ,-- • •'• v f- •;;. - ^A^-v * w* :-,;'i'V,^ <W^;yf<' rv-J-,;Analyst:B.WOOD , . Analyas Date- ,23-NOV4J4 '• Instrument- PREP - V;^£f Test- P230.1 .0

Parameter


FINAL VOLUME

Result

980

5.0

Det. Limit Units

mL

ml

PCB AROCLORS BY GAS CHROMATOGRAPHY/ECD SW846-8082 **; ?J(f, % ,-„ ' ^ / 'fxV^ds l1

Analyst B WOOD * ,"-. . ~ ~ 5 ^ ".'"JplV Analyses Date-24-NOV-04 15^43 InstrurjfenL^ D -!. "Prep- PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION BW846-3510C P230.1.0 " \ M ' ^ « \?|f7f ^ f

Parameter

PCB AROCLOR 1016

PCB AROCLOR 1221

PCB AROCLOR 1232

PCB AROCLOR 1242

PCB AROCLOR 1248

PCB AROCLOR 1254

PCB AROCLOR 1260

PCB AROCLOR 1262

SURROGATE RECOVERY



Result

BDL

BDL

BDL

0.61

BDL

BDL

BDL

BDL

128.0

0.61

Det. Limit

0.10

0.20

0.10

0.10

0.10

0.10

0.10

0.10

0.20

^esto301 \&

Units

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

% Rec

ug/L

Page 1 of 2

uBSMKF]>i < x



TOTAL SUSPENDED SOLIDS EPA 160,2

Analyst- M. GROTE Analysis Date: 24-NOV-04 00 15

NELAC:Y ,,:

Test: G403.7:0

Parameter

SUSPENDED SOLIDS

Result

14

Det. Limit Units

mg/L

Sample Comments











RUSS CEPKO. VIACOM, INC11 STANWIX STREET, PITTSBURG, PA 15222-1384

P-lC.Approved by: PAULINE SPENCE 03-DEC-04

Page 2 of 2



Received

22-NOV-04

Completed

02-DEC-04

Printed

03-DEC-04

Project

4602

Lab 10

A682108

PO Number

BL0177

Sampled

18-NOV-04 14:15

Report To


Bill To


CLIENT ID: LL12190



MATRIX: WS



Sample Description

PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW846-3510C **&. *&> ,' w j* #<*• ... • : - . - • ' -A-,'- - * -w. -*>*»•?»• -* T *T ' \ ' •' t'w^KfeaP^^--- ~*Analyst: B. WOOD } , --- '* - * ~ ^Analysts Date°23-NOV-Q4 % ^ rlnstrumentjPREP fjf-jf- Test P230 1 0

Parameter


FINAL VOLUME ; :-"'. : • ; -

Result

980

'5.0,V. . •.::>- "• .^ ' .'...

Del. Limit

."• : . ! : :-

Units

mL

mL

PCB AROCLORS BY GAS CHROMATOGRAPHY/ECD SW846-8082 VI - j '* ' ' ,-y , - t•' ' ' - • ' • ' % "^^ ^**fc V 1. t — «* * ~"f£ -i 4 ^"if-tf * *£ "*" rCL -"): *'"~-f4^3il-H r /V ^= fe -j ffi ^^^^^-^^^E

r -Analyst: B WOOD *- - ' ^- f-JHSfts ' .* «! *J'4C^nalys1slDate-'244lOV4)4!15:43":/- •'.- • -r ^ * ' •* "' - tf^- i 1 <- &*. - ' - , *??; f s «>Prep: PCB SEPARATORY FUNNEL.UQU1D11QUID EXTRACTION SW846-3510C P230 J.O 'T>w''

Parameter

PCB AROCLOR 1016

PCB AROCLOR 1221 :

PCB AROCLOR 1232

PCB AROCLOR 1242 ;

PCB AROCLOR 1248

PCB AROCLOR 1254

PCB AROCLOR 1260

PCB AROCLOR 1262

SURROGATE RECOVERY



Result

BDL

BDL

BDL

BDL

BDL

BDL

BDL

BDL

86.0

BDL

Det. Limit

0.10

0.20

0.10

0.10

0.10

0.10

0.10

0.10

0.20

-&NELAC:Y •§?|gjj||JL- - j

Units

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

% Rec

ug/L

Page 1 of 2



Analyst M GROTE "" * AnaJysjs~Date-24-NOV-4M 00 15 Test B403.7 0

Parameter

SUSPENDED SOLIDS

Result

BDL

Del. Limit Units

mg/L

Sample Comments











RUSS CEPKO, VIACOM, INC11 STANWIX STREET, PITTSBURG. PA 15222-1384


Page 2 of 2



Received

22-NOV-04

Completed

02-DEC-04

Printed

03-DEC-04

Project

4602

Lab ID

A682109

PO Number

BL0177

Sampled

18-NOV-04 14:25

Report To


Bill To


CLIENT ID: LL12191



MATRIX: WS



Sample Description

PCB SEPARATORY FUNNEL LIQUID-LIQUID BgRACTION 5^6^35,1

^Analyst: B. WOOD • ' •- '"^'^^"L' ' ft ' ;_ H< Analysis DatK TesfP2301u

Parameter


FINAL VOLUME

Result

970

50

Det. Limit Units

mL

mL

t ,. -J > - ' -PCB AROCLORS BY GAS CHROMATOGRAPHY/ECD SW846-3B0{

'" : : - ' : . ' * ,?$"* •Jti&fr"' "$!$$' » f^gfagfJZf"" ' jiiiji,

Prep: PCB SEPARATORY FUNNEL UQUID-LlQUItfeXTRACTioNSVW^

Parameter

PCB AROCLOR 1016

PCB AROCLOR 1221

PCB AROCLOR 1232

PCB AROCLOR 1242

PCB AROCLOR 1248

PCB AROCLOR 1254

PCB AROCLOR 1260

PCB AROCLOR 1262

SURROGATE RECOVERY



*»*a?^ "~"*5S-Jrj£§;i?-''1'?j3?i* *~i if i ~ "i, '* *' '

Result

BDL

BDL

BDL

0-85

BDL

BDL

BDL

BDL

118.0

0.85

*§ffiriS(tjsfcfe*S;it

Det. Limit

0.10

0.20

0.10

0.10

0.10

0.10

0.10

0.10

0.20

f<, * =>• '

ffii&fr.Z *•grest ,03017.0

Units

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

% Rec

ug/L

Page 1 of 2


TOTAL SUSPENDED SOLIDS EPA J60.2s,r p. ^'.vf-OfrflPfcN--,Analyst M GROTE ' * • Oate:24-NOV-040015 Test- G403 7.0

Parameter

SUSPENDED SOLIDS

Result

15

Det. Limit Units

mg/L

Sample Comments











RUSS CEPKO, VIACOM, INC11 STANWIX STREET. PITTSBURG. PA 15222-1384


Page 2 of 2



Received

22-NOV-04

Completed

02-DEC-04

Printed

03-DEC-04

Project

4602Lab 10

A682110

PO Number

BL0177

Sampled

18-NOV-04 16:15

Report To


Bill To


CLIENT ID: LL12192



MATRIX: WS



Sample Description

PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW846-3510C^ j,l ^ * *i* - *j| % ]| Jf^fC

FAnalyst B. WOOD ^""'t'"" %-"-'\ * *~*'l/ * ' « /Analysis Date" 23TNOV-04~" * Instrument PREP f^T ^J|fTest P230 1 0

Parameter


FINAL VOLUME : '. '•( :'f. '"' : :?V ::!

Result

1000

i"-::-:. • • " " .;'"'- '

Del. Limit Units

mL

mL

PCB AROCLORS

lAnalyst: G.v - ' .-Prep: PCB SEPARATORY FUNNEL€lQUIDaQUlDtXTRAeTIONSW846^5tOC^30:W3fei0ia

_. ' - • •'-•:--:'"/:'vi*V!:M;iMWK3fi;-;'iffis,M;::^

Parameter Result

PCB AROCLOR 1016 BDL

PCB AROCLOR 1221 ; BDL


PCB AROCLOR 1242 : BDL

PCB AROCLOR 1248 15

PCB AROCLOR 1254 X BDL



SURROGATE RECOVERY

DECACHLOROBIPHENYL (DCB) 120.0

SUMMATION OF AROCLORS 15

Det. Limit

1.0

2.0

1.0

1.0

1.0

1.0

1.0

1.0

2.0

Units

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

% Rec

ug/L

Page 1 of 2


1:10 Dilution.

Sample has some Aroclor 1242 characteristics. Aroclor is degraded.


Analyst: M. GROTE.

Analysis Date: 24-NOV-04 00 15

"' NELAC:Y*; VP - •• •Test: G403,7.0

Parameter

SUSPENDED SOLIDS

Result Del. Limit Units

mg/L

Sample Comments













Page 2 of 2



Received

22-NOV-04

Completed

02-DEC-04

Printed

03-DEC-04

Project

4602

Lab ID

A682111

PO Number

BL0177

Sampled

18-NOV-04 16:15

Report To


Bill To


CLIENT ID: LL12193MATRIX TYPE: NON-SPECIFIC WATERSUBMITTER CODE: 2226MATRIX: WS



Sample Description

PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW|46-3510C"<:A ' *t ^ * f I fc|ljf?tr oL ;• - » " ' • • • • • • • • • •> vV$v •" :-MF*>*. w^Si ' ' >• jESc 'i VAnalyst: B. WOOD ' -m< * ' ' .l- /^Analysis Date' 23;NOV-04 >, ^nstrument.PRE^^^ -fc*T€st P230.1 0

Parameter


FINAL VOLUME ;: ""( ,. .,?':"•

Result

1000

5 •••;••" ' ' " • • " " :-!

Det. Limit

' • ' " : • % ; * • - ' •

Units

mL

ml.

prep:

Parameter

PCBAROCLOR1016

PCB AROCLOR 1221

PCB AROCLOR 1232

PCB AROCLOR 1242

PCB AROCLOR 1248

PCB AROCLOR 1254

PCB AROCLOR 1260

PCB AROCLOR 1262

SURROGATE RECOVERY



Result

BDL

BDL

BDL

BDL

18

BDL

BDL

BDL

120.0

18

Det. Limit

1.0

2.0

1.0

1.0

1.0

1.0

1.0

1.0

2.0

Units

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

% Rec

ug/L

Page 1 of 2


1:10 Dilution.

Sample has some Aroclor 1242 characteristics. Aroclor is degraded.

TOTAL SUSPENDED SOLIDS EPA 160.2A.'-'. •- . '* ,•#<

Analyst: M. GROTE 'Analysis Date: 24-NOV-04 00.15 J^Test G403.7.0

Parameter

SUSPENDED SOLIDS


mg/L

Sample Comments













Page 2 of 2



Received

17-DEC-04

Completed

04-JAN-05

Printed

06-JAN-05

Project

4602

Lab ID

A685215

PO Number

BL0177

Sampled

16-DEC-04 13:00

Report To


Bill To


CLIENT ID: LL12229



MATRIX: WS



Sample Description

PCB SEPARATORY FUNNEL LIQUID-LIQUID ExffVVCTION SW846-35^0C»^, -1^ - ',- . ^ f -'-*?«£* *^

Analyst: J. HESS * ' -*"* "V'V'W'i* „'-' C>ina1ys[s Date l EC-to "* Instrument PREP < ^""'i/ffesVroaO 1 6

Parameter


FINAL VOLUME ' ' ' " ' . . • ' . ' % ' .v :- : ', ' :. , :' ' ' 1 ' '•• ^ '' •

Result

990

5.0'"V -"^ : ;- ' ' :::

Det. Limit Units

mL

inL

Prep:

Parameter

PCB AROCLOR 1016

PCB AROCLOR 1221

PCB AROCLOR 1232

PCB AROCLOR 1242

PCB AROCLOR 1248

PCB AROCLOR 1254

PCB AROCLOR 1260

PCB AROCLOR 1262

SURROGATE RECOVERY



fe«wasa*:::-iiffl

Result

BDL

BDL

BDL

BDL

0.58

BDL

BDL

BDL

112.0

0.58

Det. Limit

0.10

0.20

0.10

0.10

0.10

0.10

0.10

0.10

0.20

Units

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

% Rec

ug/L

Page 1 of 2

HERITAGE ENVIRONMENTAL SERVICES, LLC Sample ID: A68S215 LL12229

Sample reported as Aroclor 1248 but has some Aroclor 1242 characteristics.

TOTAL SUSPENDED SOLIDS EPA 160.2 *' - " * NELAC:Y ^

Analyst: J. SMITH ' ~ ' Analysis Date: 21-DEC-04 14:00 ' Test: G403.7.0

Parameter

SUSPENDED SOLIDS

Result

30

Det. Limit

1

Units

mg/L

Sample Comments


Sample was received on ice at temperature 3.2 C.Sample chain of custody number 18923.










Approved by: PAULINE SPENCE 06-JAN-05

Page 2 of 2



Received

17-DEC-04

Completed

04-JAN-05

Printed

06-JAN-05

Project

4602

Lab ID

A685216

PO Number

BL0177

Sampled

16-DEC-04 13:15

Report To


Bill To


CLIENT ID: LL12230



MATRIX: WS



Sample Description

PCB SEPARATORS FUNNEL LIQUID-LIQUID EXTRACTION SW846-3510C - i. •$-* . t, *. <-* - I , * s -o: , • - • • '. ' „_ •*- - ;*^i'^ *. .*.&'»'*:"• ,,- - /-,t^

Analyst: J. HESS , - t " < . "^ - -;n^ Analysis Date; 21-DEC-04* Instrument- PREP "• , Jest P230 1.0

Parameter


FINAL VOLUME

Result

970

5.0

Del. Limit Units

mL

mL

PCBAROCLORSBYGASCHROMAT6GRAP^/ECD,§WM6-lM82^p'?_ 4 ;_ J J.;'

Prep: PCB SEPARATORY FUNNELfUQUTD-1.IQl)lD,EXTRAtTIOJ4 S$W?p35 ifoc P"230.1 O7*- * '* ">', '

Parameter

PCB AROCLOR 1016

PCB AROCLOR 1221 :

PCB AROCLOR 1232

PCB AROCLOR 1242 :

PCB AROCLOR 1248

PCB AROCLOR 1254

PCB AROCLOR 1260

PCB AROCLOR 1262

SURROGATE RECOVERY



Result

BDL

BDL

BDL

BDL

0.66

BDL

BDL

BDL

112.0

0.66

_ >-' ' ^ |;ffy>> "-•- '

Det. Limit

0.10

0.20

0.10

0.10

0.10

0.10

0.10

0.10

0.20

Units

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

% Rec

ug/L

Page 1 of 2

\HEUm}HERITAGE ENVIRONMENTAL SERVICES, LLC Sample ID: A68S216 LL12230



Analyst: J. SMITH - ' Analysis Date: 21-DEC-04 14:00

NELAC:Y ,

Test' G403.7.0

Parameter

SUSPENDED SOLIDS

Result

35

Del. Limit Units

mg/L

Sample Comments













Page 2 of 2



Received

17-DEC-04

Completed

04-JAN-05

Printed

06-JAN-05

Project

4602

Lab ID

A685217

PO Number

BL0177

Sampled

16-DEC-04 13:20

Report To


Bill To


CLIENT ID: LL12231



MATRIX: WS



Sample Description

PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW846-3510C t' ,—4 . , 4 -*:j, ' ,*- \ ^ s

- • : • : • • • :;. I' At ,.n" *'-** ;**- _*\J -"-•"' 1.*it -f f -K* "* •>:.Analyst: J. HESS ' , ^ Analysis Date- 21 -DEC-04 ~ instrument PREP ~j- •*„, *- Test P2301.O

Parameter


FINAL VOLUME : :

Result

1000

5.0 :,.'.'."

Det. Limit Units

mL

mL :

PCB AROCLORS BY GAS CHROMATOGRAPHY/ECD SW846-8082 ,_ , \ ^ ~;£ i -^ _^ " .-. ^ »'A^NELAC:Y t *

Analyst G, CLOUSE ^ ,- =, -"*! **«&, 4'j ?%^na'rysis'Oate- 27-DEC^04 16:56~jnshur t GCVEC . ^^^est., 301^Prep- PCB SEPARATORY FUNNEL UQUIDilQUID^ctRACTl6NSW3w-3510CP2 .4.0'' ,' f' ^?'^ *-^jff's 'f$^*'' **'"•**

Parameter

PCB AROCLOR 1016

PCB AROCLOR 1221

PCB AROCLOR 1232

PCB AROCLOR 1242

PCB AROCLOR 1248

PCB AROCLOR 1254

PCB AROCLOR 1260

PCB AROCLOR 1262

SURROGATE RECOVERY



Result

BDL

BDL

BDL

BDL

0.53

BDL

BDL

BDL

120.0

0.53

Det. Limit

0.10

0.20

0.10

0.10

0.10

0.10

0.10

0.10

0.20

Units

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

% Rec

ug/L

Page 1 of 2




Analyst: J. SMITH Analysis Date: 21-DEC-04 14:00 *

NELAC:Y

Test- G403.7.0

Parameter

SUSPENDED SOLIDS

Result

21

Det. Limit Units

mg/L

Sample Comments













Page 2 of 2



Received

17-DEC-04

Completed

04-JAN-05

Printed

06-JAN-05

Project

4602

Lab ID

A685218

PO Number

BL0177

Sampled

16-DEC-04 13:45

Report To


Bill To


CLIENT ID: LL12232



MATRIX: WS



Sample Description

PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION ISW846-3510C ~< - , , * * fe^C"* '" ' =C - T~ " ",!'. . ^ -~ .„,$ v^4^r^ , '\, \ .;?§; *J V- - $ > • * . ' • ? ' .

Analyst: J. HESS rV - 'L*' ,, i\ Jtaafysis Gate: 21-DEC-04 Instrument- PREP * «g *.f* Test P230 1.0

Parameter


FINAL VOLUME

Result

1000

5.0

Del. Limit Units

mL

mL

•pCBAROCLORSBYGASCHROMATpGJ^PHY/EOT£wM6ijB8V^C't- - X , JT^ 'V^H-'i ^ .JNEL^C:Y ,_

' ^Analyst:' G CLOUSE ^ "" ' A" c 1 56 "jnsbument; OC^CD ^ f<esl''o301 .Tjfl

Prep: PCB SEPARATORY FUNNELifCWlD-O(KlB£XTRACTIC»J^W846-3510C P230.1.0 r '' "'"^^J^ , '**• * A-^« t, * -=,• _ » , , . » Jtdr -«4 'IP' vi^vit i « " i *i •• •

Parameter

PCB AROCLOR 1016

PCB AROCLOR 1221

PCB AROCLOR 1232

PCB AROCLOR 1242

PCB AROCLOR 1248

PCB AROCLOR 1254

PCB AROCLOR 1260

PCB AROCLOR 1262

SURROGATE RECOVERY



Result

BDL

BDL

BDL

BDL

0.52

BDL

BDL

BDL

114.0

0.52

Det. Limit

0.10

0.20

0.10

0.10

0.10

0.10

0.10

0.10

0.20

Units

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

% Rec

ug/L

Page 1 of 2

\HER1WE}



TOTAL SUSPENDED SOLIDS EPA 160.2 , ' . NELAC'.Y

Analyst: J. SMITH " -'Analysis Date: 21-DEC-04 14:00 Test G403.7.0

Parameter

SUSPENDED SOLIDS

Result

12

Det. Limit

1

Units

mg/L

Sample Comments












P-IC.Approved by: PAULINE SPENCE 06-JAN-05

Page 2 of 2


HERITAGE ENVIRONMENTAL SERVICES, LLCCOMMERCIAL LABORATORY OPERATIONS7901 W. MORRIS ST.

INDIANAPOLIS, IN 46231(317)243-8304

Received

17-DEC-04

Completed

04-JAN-05

Printed

06-JAN-05

Project

4602

Lab ID

A685219

PO Number

BL0177

Sampled

16-DEC-04 13:55

Report To

MIKE MCCANNVIACOM, INC.

2002 WEST VERNAL PIKEBLOOMINGTON, IN 47404

Bill To

BETH STEIGERWALD

VIACOM, INC.11 STANWIX STREETPITTSBURGH, PA 15222

CLIENT ID: LL12233



MATRIX: WS



Sample Description

PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW846-3510C ,, V* * \ < -t -v.'• ; - ^ iv "v^^*u'''.f. 8fc ';,-•• : . • -.-IE" v-?7}Mi

Analyst B.OILLWORTH •* ' - , - Analysis Date: 21 -DEC-04 - Instrument PREP V- v ; ,t- Test- P230. 1.0

Parameter


FINAL VOLUME :: : . : . . :}

Result

1000

5.0 -f- • • ' . " . ,•* .,

Del. Limit Units

mL

mL

PCB AROCLORS BY GAS^ CHROMATOGRAPHY/ECD^W8 t]W)82^ «/,,;>*'* ,v/~ ^&^&. :*''<NHJPY

.-.Analyst G CLOUSE " ' ^^^---^ £j$£> * | 1ysisDa>tej27Ê&<)4^6-56 1nstrumentt3CfcCD'| j fgesl *O301 t.O

PrepiPCBSEPARATORYFUNNEL'UQUID-LlQUlbÊXTRACTIONSWe^SIOCPÔlo' *! i '•fe*W^^-¥ " 5 '' *

Parameter

PCB AROCLOR 101 6

PCB AROCLOR 1221

PCB AROCLOR 1232

PCB AROCLOR 1242

PCB AROCLOR 1248

PCB AROCLOR 1254

PCB AROCLOR 1260

PCB AROCLOR 1262

SURROGATE RECOVERY



Result

BDL

BDL

BDL

BDL

BDL

BDL

BDL

BDL

78.0

BDL

Det. Limit

0.10

0.20

0.10

0.10

0.10

0.10

0.10

0.10

0.20

Units

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

% Rec

ug/L

Page 1 of 2


TOTAL SUSPENDED SOLIDS EPA 160.2 ~ -„ -- -, *«; *? - . *• • ,r:2^vV * - , v-'<*-., *.' •.Analyst-J SMITH Analysis Date: 21-DEC-041400 " Test: G403 7.0

Parameter

SUSPENDED SOLIDS

Result

BDL

Del. Limit

1

Units

mg/L

Sample Comments













Page 2 of 2


HERITAGE ENVIRONMENTAL SERVICES, LLC

COMMERCIAL LABORATORY OPERATIONS

7901 W. MORRIS ST.

INDIANAPOLIS, IN 46231

(317)243-8304

Received

17-DEC-04

Completed

04-JAN-05

Printed

06-JAN-05

Project

4602

Lab 10

A685220

PO Number

BL0177

Sampled

16-DEC-04 14:20

Report To

MIKE MCCANN

VIACOM, INC.

2002 WEST VERNAL PIKE

BLOOMINGTON, IN 47404

Bill To

BETH STEIGERWALD

VIACOM, INC.

11 STANWIX STREET

PITTSBURGH. PA 15222

CLIENT ID: LL12234



MATRIX: WS



Sample Description

PCB SEPARATORY FUNNEL LIQUID-LIQUID, EXTRACTION SW846-3510C - £ ? i -* ^J^K^ * "i' " - ' " • . ' *&£*• V V^-v •<• :**• ~v- '* *v*$&$jjj&ijj^±~z~-<'*-

Analyst: B. DILLWORTH ',- * ~\, Analysis Date: 21-DEC-04 , Instrument: PREP fd^^ lTest- P230 1 .0

Parameter


FINAL VOLUME .' • V-: V

Result

980

•:5.o.'-:,:':"--" ... . " " ,:. :

Det. Limit Units

mL

mL ,

QUID EXTRACTION SWg4€p510ertSWfh J':.•?. niKtSjSSiffifKS; j,!tf isBsSifcfSSAKfi

Parameter

PCBAROCLOR1016

PCB AROCLOR 1221

PCB AROCLOR 1232

PCB AROCLOR 1242

PCB AROCLOR 1248

PCB AROCLOR 1254

PCB AROCLOR 1260

PCB AROCLOR 1262

SURROGATE RECOVERY



BDL

BDL

BDL

BDL

6.4

BDL

BDL

BDL

120.0

6.4

Det. Limit

0.50

1.0

0.50

0.50

0.50

0.50

0.50

0.50

1.0

Units

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

% Rec

ug/L

Page 1 of 2

\HERimyHERITAGE ENVIRONMENTAL SERVICES, LLC Sample 10: A685220 LL12234

1:5 Dilution.



Analyst: J. SMITH 'Analysis Date!21-DEC-04 14:00

NELAC:Y

test: G403 7.0

Parameter

SUSPENDED SOLIDS

Result

BDL

Del. Limit Units

mg/L

Sample Comments













Page 2 of 2



Received

17-DEC-04

Completed

04-JAN-05

Printed

06-JAN-05

Project

4602

Lab ID

A685221

PO Number

BL0177

Sampled

16-DEC-04 14:20

Report To


Bill To

BETH STEIGERWALDVIACOM, INC.

11 STANWIX STREETPITTSBURGH. PA 15222

CLIENT ID: LL12235



MATRIX: WS



Sample Description

PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW846-3510C ', , * -j! ' A^X-ftl*' '' z : ,

Analyst: B DILLWORTH , -$ < % ,2 • 'Wia is

Parameter


FINAL VOLUME . . . . - ' ' ' J?- ."V'. s&'V • : - • ' • • . . :^!.: ' :;

Oate-21-dEC-04 i Instrument REP ?«5f ^Tesl-P2301.0

Result

1000

5.0. ., • .f' : ' ,:i.;::- :

Det. Limit Units

mL

mL

••'•'• ' ' • • " ' : • - ' • • •'-.• .;: ; :t! *;5^^4«iFsaP*f;P«;s?ft,ii!.v<!«ir ..;';»: ' iKVuBs iPCB AROCLORSBYGASCHROJMATOGRARHY/ECDSW846|308

Prep PCB SEPARATORY FONNCT ID tloSffRAGTlOKI ^Pa_ .(...••.• • .im^c^ tS^^Vs i ^A^SS^m^y^^^^V^m^

Parameter

PCBAROCLOR1016

PCB AROCLOR 1221

PCB AROCLOR 1232

PCB AROCLOR 1242

PCB AROCLOR 1248

PCB AROCLOR 1254

PCB AROCLOR 1260

PCB AROCLOR 1262

SURROGATE RECOVERY



3ate:p7JD.EG<)4 & 6:56;3nstrume

e£gM!ismfi*m .s -i.j.-is&s.r. •'.• «;•*«

Result

BDL

BDL

BDL

BDL

6.5

BDL

BDL

BDL

130.0

6.5

i'l?Del. Limit

0.50

1.0

0.50

0.50

0.50

0.50

0.50

0.50

1.0

.' feOsJi..-'-* "- :

Units

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

% Rec

ug/L

Page 1 of 2


1:5 Dilution.



Analyst: J. SMITH

NELAC:Y

Analysis Date: 21-DEC-04 14:00

Parameter

SUSPENDED SOLIDS

Result

BDL

Det. Limit Units

mg/L

Sample Comments












. J&ivuct


Page 2 of 2



Received

17-DEC-04

Completed

04-JAN-05

Printed

06-JAN-05

Project

4602

Lab ID

A685222

PO Number

BL0177

Sampled

16-DEC-04 14:45

Report To


Bill To


CLIENT ID: LL12236



MATRIX: WS



Sample Description

PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW846-3510C . , ; •- <$ k\' ..•:' • • • ' •' - -' :*, »; ' L- iM"-*"^ ',l ' « . * ' ' • • ' • , " "1-.'sf«-=C; Analyst: B.DILLWORTH , ' ~ , _'"•» 1, i" Analysis' Oate:"21-OEC-04 , •* Instalment PREP >' V ; Test: P230. 1.0

Parameter


FINAL VOLUME ? > : +' \ - "..,,

Result

1000

5.0

Det. Limit Units

mL

rhL

: . . . . . . . . .

PCB ARQCLORS BY GAS CHROM ATQGi

:. -Prep: PCB SEPARATORY FUNNEll_i^. • • : : ' • . ' •:- :- ' :L; '.••'.'•'.. i ta

Parameter

PCBAROCLOR1016

PCB AROCLOR 1221

PCB AROCLOR 1232

PCB AROCLOR 1242

PCB AROCLOR 1248

PCB AROCLOR 1254

PCB AROCLOR 1260

PCB AROCLOR 1262

SURROGATE RECOVERY



Result

BDL

BDL

BDL

BDL

BDL

BDL

BDL

BDL

112.0

BDL

Det. Limit

0.10

0.20

0.10

0.10

0.10

0^10

0.10

0.10

0.20

Units

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

% Rec

ug/L

Page 1 of 2



Analyst: J. SMITH Analysis Date: 21-DEC-04 14:00

NELAC.-Y „--- f „--, -_«(,•"TestfG403.7.0

Parameter

SUSPENDED SOLIDS


mg/L

Sample Comments













Page 2 of 2



Received

01-FEB-05

Completed

09-FEB-05

Printed

09-FEB-05

Project

4602

Lab ID

A688828

PO Number

BL0177

Sampled

28-JAN-05 14:30

Report To


Bill To


CLIENT ID: LL12369 (MS/MSD)MATRIX TYPE: NON-SPECIFIC WATERSUBMITTER CODE: 2226

MATRIX: WS



Sample Description

PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW846-3510C , • J- *, *., -, .v^iS*" ,: • - . : • ' : • . : . . • • : : • ' . • - . , , — - , • -»•;• , * - , ';el.-' .'.AT* ?

Analyst: M. -WRIGHT : Analysis Date- 03-FEB-05 Instrument- PREP •*' "?' 'JeslfP230.1.0. ' i: . ; . . . . . . .•-•, ..'.-•* 1.

Parameter


FINAL VOLUME

Result

850

5 : ' ' . - '

Dei. Limit Units

mL

mL

PCB AROCLORS BY GAS CHROMATOGRAPHY/ECD SW846-8082 - ^ „ - *V-IV" * 'l I'J^gJJE&CfytC-: ' : ' • ' • • - / , - , , » JlJ. ^H^^ff f , > > ! J j"/4 "'fe'-' rfrB^^^^S^rf' ^

;. Analyst M WRIGHT - ^ , Analysis Date- 05-FEB-05 00 45 Instrument'cc/E^D rejf ^S^MPI .X),-

; Prep: PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW846^3510CP230 *l'o j"' - l """f"5*' "'*? ^- V -" >

Parameter

PCB AROCLOR 1016

PCB AROCLOR 1221

PCB AROCLOR 1232

PCB AROCLOR 1242

PCB AROCLOR 1248

PCB AROCLOR 1254

PCB AROCLOR 1260

PCB AROCLOR 1262

SURROGATE RECOVERY



Result

BDL

BDL

BDL

BDL

1.8

BDL

BDL

BDL

112.0

1.8

Det. Limit

0.10

0.20

0.10

0.10

0.10

0.10

0.10

0.10

0.20

Units

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

% Rec

ug/L

Page 1 of 2

\hEsimyHERITAGE ENVIRONMENTAL SERVICES, LLC Sample ID: A688828 LL12369 (MS/MSD)

Aroclor \s degraded.


Analyst: J. SMITH Analysis Date- 02-FEB-05 10:00

NELAC:Y ;:;

Test: G403.?:o

Parameter

SUSPENDED SOLIDS

Result

77

Det. Limit Units

mg/L

Sample Comments












Y - K . . .

Approved by: PAULINE SPENCE 09-FEB-05

Page 2 of 2



Received

01-FEB-05

Completed

08-FEB-05

Printed

09-FEB-05

Project

4602

Lab ID

A688829

PO Number

BL0177

Sampled

28-JAN-05 14:45

Report To


Bill To


CLIENT ID: LL12370



MATRIX: WS



Sample Description

PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW846-3510C . ~ „ , -V'- -Vt^&i *"" "'• - - i ' ''- • ' " • ' , • '«-• t - ..*•'',, -.V J-v '

Analyst M WRIGHT - , <-,, *f« ' - , -/Analysis Date: 03-FEB-05 Instrument: PREP * ~ -Test: P.230 1,0

Parameter


FINAL VOLUME ; : ; •'...

Result

980

5

Det. Limit Units

mL

mL

PCB AROCLORS BY GAS CHROMATOGRAPHY/ECD SW846-8082 v ~ *- , •* ^WELA<%U

Analyst- M WRIGHT "' - ^ ^ *^ fc^v .<JK Jjfe^. Wialysis Date- 05-FEB-05 00 45 Instrument GC/ECD ^ *^* STjSfc^D1l7t)

Prep PCB SEPARATORY FUNNEL LIQUID-LIQUID EXfRACTJONSW846-351 DC P230*1.0 *"' '- * ' ' 'J ' i^^^'^V

Parameter

PCB AROCLOR 101 6

PCB AROCLOR 1221

PCB AROCLOR 1232

PCB AROCLOR 1242

PCB AROCLOR 1248

PCB AROCLOR 1254

PCB AROCLOR 1260

PCB AROCLOR 1262

SURROGATE RECOVERY



Result

BDL

BDL

BDL

BDL

BDL

BDL

BDL

BDL

84.0

BDL

Det. Limit

0.10

0.20

0.10

0.10

0.10

0.10

0.10

0.10

0.20

Units

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

% Rec

ug/L

Page 1 of 2


NELAC:yT

Test. G403 7,0

TOTAL SUSPENDED SOLIDS EPA 160.2v j. * J *.

Analyst J. SMITH ' Analysis Date- 02-FEB-05 10 00

Parameter

SUSPENDED SOLIDS

Result

BDL

Det. Limit Units

mg/L

Sample Comments













Page 2 of 2



Received

01-FEB-05

Completed

08-FEB-05

Printed

09-FEB-05

Project

4602

Lab ID

A688831

PO Number

BL0177

Sampled

28-JAN-05 14:00

Report To


Bill To


CLIENT ID: LL12371MATRIX TYPE: NON-SPECIFIC WATERSUBMITTER CODE: 2226MATRIX: WS



Sample Description

PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW846-3510C:. . : ^ < *,'"""•• -'-ij, t'S~~ - '

Analyst: M. WRIGHT , * "": vX'Ariaiysis Date" 03-FEB-05 ^ Instrument: PREP - Test:P230.1.0

Parameter


FINAL VOLUME :: ;

Result

960

:5 "' . •' • •

Del. Limit Units

mL

mL

PCBAROCLORSBYGASCHROMATOGRAPHY/ECDSW846:8082 ,, ,„ ,• v NELAC:Y

Analyst M. BRIGHT/ * / r,,~'f*~' fr' f^^f^^^K^^e:^fBB^5WA5ninsinjmeniGCfECD

Prep- PCB SEPAF^TORY FUNNEL LIQUID-LICWIDWRACTlbrlsW84>35l6cP230.1,0'' '; r ' '

Parameter

PCB AROCLOR 1016

PCB AROCLOR 1221

PCB AROCLOR 1232

PCB AROCLOR 1242

PCB AROCLOR 1248

PCB AROCLOR 1254

PCB AROCLOR 1260

PCB AROCLOR 1262

SURROGATE RECOVERY



Result

BDL

BDL

BDL

BDL

1.5

BDL

BDL

BDL

104.0

1.5

Del. Limit

0.10

0.20

0.10

0.10

0.10

0.10

0.10

0.10

0.20

Test- O301J.O

Units

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

% Rec

ug/L

Page 1 of 2


Aroclor is degraded.


Analyst: J. SMITH ^ Analysis Date'. 02-FE8-Q5 10:00

NELACrY "

Test G403.T.O

Parameter

SUSPENDED SOLIDS


mg/L

Sample Comments












.


Page 2 of 2



Received

01-FEB-05

Completed

08-FEB-05

Printed

09-FEB-05

Project

4602

Lab ID

A688832

PO Number

BL0177

Sampled

28-JAN-05 14:10

Report To


Bill To


CLIENT ID: LL12372



MATRIX: WS



Sample Description

PCBSEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW846-3510C; , v. - . . ;_

Analyst: M WRIGHT J " Analysis Date- 03-FEB-05 " Instrument: PREP , >/•' ' Test: P230. 1.0

Parameter


FINAL VOLUME

Result

910

5 : : .•

Del. Limit Units

mL

mL

PCB AROCLORS BY GAS CHROMATOGRAPHY/ECD SW846:8082 - , - \«4^t;/ K ;3_ > . NELAC:Y~ t

Analyst: M. WRIGHT _ ^ j, , ,'1 ' /' Analysis Date- 05-F£B-05 00 45 Instmment GC/ECD tp f |est OSCJJU.O

Prep: PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW846-35 10C P230 Co ^' "'"" "'* ".-~ir " ' ~" ^ ""'''I'^

Parameter

PCB AROCLOR 1016

PCB AROCLOR 1221

PCB AROCLOR 1232

PCB AROCLOR 1242

PCB AROCLOR 1248

PCB AROCLOR 1254

PCB AROCLOR 1260

PCB AROCLOR 1262

SURROGATE RECOVERY



Result

BDL

BDL

BDL

BDL

1.2

BDL

BDL

BDL

96.0

1.2

Det. Limit

0.10

0.20

0.10

0.10

0.10

0.10

0.10

0.10

0.20

Units

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

% Rec

ug/L

Page 1 of 2




Analyst: J. SMITH * /Analysis Date: 02-FEB-05 10:00

NELAC:Y v;

Test: G403.?:o

Parameter

SUSPENDED SOLIDS

Result

18

Del. Limit Units

mg/L

Sample Comments













Page 2 of 2



Received

01-FEB-05

Completed

08-FEB-05

Printed

09-FEB-05

Project

4602

Lab ID

A688833

PO Number

BL0177

Sampled

28-JAN-05 16:15

Report To


Bill To


CLIENT ID: LL12373



MATRIX: WS



Sample Description

PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW846-3510C ,-- , - - , . ' - - , * ' . a < $ *--.•&*,- - - ' • ' . * • - ' • - • , - " , . • '

Analyst: M. WRIGHT \ " ~ '; ,=.:"'/ Analysis Date" 03-FEB-05 - Instrument PREP \" ' Test- P230. 1.0

Parameter


FINAL VOLUME : " :

Result

970

1

Det. Limit Units

mL

mL

PCB AROCLORS BY GAS CHROMATOGRAPHY/ECD SVV846-8082 , -- ~ * , : NELAC.Y. • • - . - . - „ T :<r-^, • . . • . . . - - *iit .rf*<v -' ""f^'i - . 4 ' • "i'-c , 'Analyst: M WRIGHT , ^ -' " '? k > ?- - ^ f*> /. Analysis Date' 05-FEB-05 00:45 Instrument GC/ECD x V jTest O301"7.0

Prep: PCB SEPARATORY FUNNEL UQUID-LIQUID EXTRACTION SWi46-3510C'P23o"l 0* ' tV ' * *- , ' 1

Parameter

PCBAROCLOR1016

PCB AROCLOR 1221 :

PCB AROCLOR 1232

PCB AROCLOR 1242

PCB AROCLOR 1248

PCB AROCLOR 1254

PCB AROCLOR 1260

PCB AROCLOR 1262

SURROGATE RECOVERY



Result

BDL

BDL

BDL

17

BDL

BDL

BDL

BDL

120.0

17

Det. Limit

0.50

1.0

0.50

0.50

0.50

0.50

0.50

0.50

1.0

Units

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

% Rec

ug/L

Page 1 of 2

vsHERITAGE ENVIRONMENTAL SERVICES, LLC Sample ID: A688833 LL12373

1:5 Dilution.



Analyst: J. SMITH V : Analysis Date: 02-FEB-05 10:00

NELACrY

Test: G403.7.0

Parameter

SUSPENDED SOLIDS

Result

BDL

Det. Limit Units

mg/L

Sample Comments













Page 2 of 2



Received

01-FEB-05

Completed

08-FEB-05

Printed

09-FEB-05

Project

4602

Lab ID

A688834

PO Number

BL0177

Sampled

28-JAN-05 16:15

Report To


Bill To


CLIENT ID: LL12374



MATRIX: WS



Sample Description

PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW846-3510C , - ' - <4 J 1 "~£ ' £f i.£ 1, - is flfis. * • • > • » L _ *

Analyst: M. WRIGHT , *t * V*f Analysis Date: 03-FEB-05 Instrument- PREP ' s" -Test P230.1 .0

Parameter


FINAL VOLUME : ' • . . ' " ;

Result

980

5

Det. Limit Units

mL

mL

PCB AROCLORS BY GAS CHROMATOGRAPHY/ECD SW846-8082 ^ "f^'X" fF' ELAP:Y-

Analyst M WRIGHT \ "' ' ~$* <?-i g1. ', \. ' * ~,v '-Analysis Date: 05-FEB-05 00.45 Instrument GC/ECD *5?'A^ ^Test C)301, 7^0•- L x ^ ^u _^ , f a-\* ^jZt, ^t***t r/^ a 1 *^ ^ * *• -S^* j~ ^* -*

Prep: PCB SEPARATORY FUNNEL UQUID-LIQUID EXTRACTION SW846-3510C P230 1 0

Parameter

PCB AROCLOR 101 6

PCB AROCLOR 1221

PCB AROCLOR 1232

PCB AROCLOR 1242

PCB AROCLOR 1248

PCB AROCLOR 1254

PCB AROCLOR 1260

PCB AROCLOR 1262

SURROGATE RECOVERY



Result

BDL

BDL

BDL

16

BDL

BDL

BDL

BDL

100

16

* «i

Det. Limit

0.50

1.0

0.50

0.50

0.50

0.50

0.50

0.50

1.0

'' "; "•_

Units

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

% Rec

ug/L

Page 1 of 2


1:5 Dilution.



Analyst:J. SMITH- V : ; i ' . ' Analysis Date: 02-FEB-05 10:00

NELAC:Y

TestG40370

Parameter

SUSPENDED SOLIDS

Result

BDL

Del. Limit Units

mg/L

Sample Comments













Page 2 of 2



Received

01-FEB-05

Completed

08-FEB-05

Printed

09-FEB-05

Project

4602

Lab ID

A688835

PO Number

BL0177

Sampled

28-JAN-0511:15

Report To

MIKE MCCANN

VIACOM, INC.2002 WEST VERNAL PIKEBLOOMINGTON. IN 47404

Bill To


CLIENT ID: LL12375



MATRIX: WS



Sample Description

PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW846-3510C >. _, ' «.; VsS^&kfe1 '""-"" - *• • ' „„ i-r't-^ .?. „»„ . I'* V,Lr . , &r Vi '

Analyst: M.WRIGHT ' ' "* "* Analysis Date 03-FEB-05 - Instrument PREP, j ^^Jea.P2301.0

Parameter


FINAL VOLUME

Result

970

.5 •' " ' ' • • •"

Del. Limit Units

mL

imL

PCB AROCLORS BY GAS CHROMATOGRAPHY/ECD SW846-8082 % ?;> ^ ^ «

^Analyst M WRIGHT '- x/ti' vsi'"-" I%t,?%i('Analysis Date; OS-FEe'-OS 00-45 * Instrumeiw* ' 1(T!'\f*ii.i# .-^s fs* •-;%f \ • " , • - " -,"•-&•? ' j,

Prep: PCB SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW8463510C P230.1.0 - ~

Parameter

PCB AROCLOR 101 6

PCB AROCLOR 1221

PCB AROCLOR 1232

PCB AROCLOR 1242

PCB AROCLOR 1248

PCB AROCLOR 1254

PCB AROCLOR 1260

PCB AROCLOR 1262

SURROGATE RECOVERY



Result

BDL

BDL

BDL

BDL

2.9

BDL

BDL

BDL

100

2.9

'f*-**^

Det. Limit

0.50

1-0;

0.50

0.50

0.50

0.50

0.50

0.50

1.0

tew,trY~4

Units

ug/L

ug/L

ug/L;ug/L

ug/L

ug/L

ug/L

ug/L

% Rec

ug/L

Page 1 of 2

JIEBlWElv i vf


1:5 Dilution.



Analyst: J. SMITH ." Analysis Date: 02-FEB-0510:00

; NELAC:Y :

: " Test: G403.7.0

Parameter

SUSPENDED SOLIDS

Result

19

Del. Limit Units

mg/L

Sample Comments











RUSS CEPKO, VIACOM. INC11 STANWIX STREET, PITTSBURG, PA 15222-1384


Page 2 of 2

APPENDIX C

Data Validation

Validation Results for the November 2004 Lemon Lane Spring Water Samples

1. Validation of the following samples has been completed:

• LL 12187-LL12193

2. Validation was performed per the requirements for level 4 data in the project QAPjP. This includes acheck for; Holding Time, Calibration, Blank Contamination, Precision, Accuracy, and Accuracy ofNominal Reporting Limits against method requirements. Based on this review, no data qualificationsare recommended.

3. The QAPjP requires an assessment of the overall data quality with respect to Precision, Accuracy,Representativeness, Completeness and Comparability (PARCC).

o Precision and accuracy: Precision and accuracy were accessed by reviewing the labperformance on lab spiked samples, lab spike duplicates and field duplicates. Allrequirements were met.

o Representativeness: The representativeness requirement involves an assessment of thefield sampling and lab analytical techniques. The field sampling locations andtechniques as well as lab procedures were in accordance with the approved samplingplan and QAPjP. Therefore the representativeness requirements were met.

o Completeness: The completeness goal for the project was for all project data to be 90%accepted. Completeness is calculated by dividing the total number of acceptableanalyses by the total performed. An acceptable analysis is defined as one that conformedto QC protocols and is not rejected. All these analyses were accepted. The projectcompleteness goal has been met to date.

o Comparability: All the samples taken, analyzed and validated by Viacom were taken byViacom or it's contractors sampling crews using the same procedures as previoussamples at this location. These samples were analyzed by Heritage Labs. Care shouldbe taken when attempting to trend Heritage sample results with other labs using slightlydifferent procedures. Overall these results should be directly comparable to otherHeritage lab results from these locations.

Overall, the main objective of the sampling event was to determine if PCBs are present at a concentrationof .1 ppb or more. This data is of sufficient quality to satisfy this goal.

Validation Results for the December 2004 Lemon Lane Spring Water Samples


LL 12229-LL12237







Overall, the main objective of the sampling event was to determine if PCBs are present at a concentrationof. 1 ppb or more. This data is of sufficient quality to satisfy this goal.

Validation Results for the January 2005 Lemon Lane Spring Water Samples


• LL 12369-LL12375







Overall, the main objective of the sampling event was to determine if PCBs are present at a concentrationof .1 ppb or more. This data is of sufficient quality to satisfy this goal.

APPENDIX D

Monroe County Airport Rainfall Records

Official station hourly observations: 1 November 2004 to January 31 2005

Time Precip Beginning EndingStation Date (EST) (in.) Time Time Qualifier

BMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMG

11/1/200411/1/200411/1/200411/1/200411/1/200411/1/200411/1/200411/1/200411/1/200411/1/200411/2/200411/2/200411/2/200411/2/200411/2/200411/2/200411/2/200411/2/200411/2/200411/2/200411/2/200411/2/200411/2/200411/2/200411/2/200411/2/200411/2/200411/2/200411/2/200411/2/200411/3/200411/3/200411/3/200411/4/200411/4/200411/4/200411/4/200411/4/200411/4/2004

11/11/200411/11/200411/11/200411/11/200411/11/200411/11/2004

553653753853105311531253195320532153

5315925335345355365375385395310531133125313531453155316531753185319531653175318531532533535539531053453553653753853953

0.010.010.01

00.040.220.01

00.020.070.040.050.240.060.070.040.050.080.02

0.020.010.10.080.010.01

00.01

0000

0.0100

0.010.01

00000

0.120.260.06

537

8131003

19171954

1002

152816071741

19291645

1810135214300

950

413534

658

707825

12111936

2146

854

141315491626

17551939

17071836146238305

1053423

617

$= Equipment may need calibration or replacement.


BMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMG

11/11/200411/11/200411/11/200411/11/200411/11/200411/11/200411/11/200411/11/200411/11/200411/11/200411/11/200411/11/200411/11/200411/16/200411/16/200411/16/200411/16/200411/16/200411/18/200411/18/200411/18/200411/18/200411/18/200411/18/200411/18/200411/18/200411/18/200411/18/200411/18/200411/19/200411/19/200411/19/200411/19/200411/19/200411/19/200411/19/200411/19/200411/19/200411/19/200411/22/200411/22/20041 1/22/200411/22/200411/22/200411/22/200411/23/200411/23/200411/23/200411/24/2004

1053115312531353145315531653175318531953205321532253153253353553753853953155316531753185319532053215322532316

531532533534535536531053205322535536537538539531053125321532253253

0.020.040.050.030.040.040.040.05

00.010.010.01

000

0.010000000

0.060.120.070.040.020.010.020.10.030.040.02

000

0.0100

0.010.01

00.010.02

00.01

00.01

1917

120224

5097318379001552

1747

10062013

2238531601

813902

12042152

227

1845

2202153

324550741848909

1631

61210182021

2249553

74783191110411213

2202




11/24/200411/24/200411/24/200411/24/200411/24/200411/24/200411/24/200411/24/200411/24/200411/24/200411/24/200411/24/200411/24/200411/24/200411/24/200411/24/200411/24/200411/24/200411/24/200411/24/200411/25/200411/25/200411/27/200411/27/200411/27/200411/27/200411/27/200411/27/200411/27/200411/27/200411/27/200411/27/200411/27/200411/27/200411/27/200411/27/200411/27/200411/27/200411/27/200411/27/200411/27/200411/29/200411/29/200411/29/200411/29/200411/29/200411/29/200411/30/200411/30/2004

3534535536537538539531053115912531353145316531753185319532053215322532344

536531533534536537538539531053115312571353145315531653175318531953205321531753185319532053215322533531053

0.030.010.020.010.010.050.030.07

00.03

00.01

0

0.010.01

00.010.02

0000

0.01

00

0.010

0.030.070.010.020.090.080.090.090.040.040.01

00.010.030.030.010.01

000

819

1352

1626

1820

2049

2322

625104338

652

1705

22413391019

721

1235

1657

2052

232529

653117

354

2104

3481034




11/30/200411/30/200411/30/200411/30/200411/30/200411/30/200411/30/200411/30/200412/1/200412/1/200412/1/200412/1/200412/1/200412/1/200412/3/200412/3/200412/3/200412/3/200412/3/200412/5/200412/5/200412/5/200412/6/200412/6/200412/6/200412/6/200412/6/200412/6/200412/7/200412/7/200412/7/200412/7/200412/7/200412/7/200412/7/200412/7/200412/7/200412/7/200412/7/200412/7/200412/7/200412/7/200412/7/200412/7/200412/9/200412/9/200412/9/200412/9/200412/9/2004

1153125313531453155316531753185353153253353453553756853115313551453205321532253

5315325335345355353153353453553653753853953115312531453155316531753185312531353145317531853

0.120.020.030.010.030.060.030.010.070.050.060.03

00

0.010.020.010.120.020.010.01

0.070.03

00.140.070.010.090.020.050.01

00.020.040.01

00

0.030.02

0

1109

7557551120135413542023

237

14

335

1110

1433

1557

1213

1710

213

509756756112113551355

150

306

133

943

1231

1553

1758

14011711

$$$$$




12/9/200412/10/200412/10/200412/10/200412/10/200412/10/200412/10/200412/10/200412/10/200412/11/200412/11/200412/11/200412/11/200412/11/200412/11/200412/11/200412/11/200412/11/200412/11/200412/13/200412/13/200412/13/200412/13/200412/13/200412/13/200412/13/200412/13/200412/13/200412/13/200412/13/200412/13/200412/13/200412/13/200412/13/200412/13/200412/17/200412/18/200412/19/200412/19/200412/19/200412/19/200412/19/200412/19/200412/22/200412/22/200412/22/200412/22/200412/22/200412/22/2004

1953538539531053155316531753185353153253353453553653753853135365375385395310531153125313531453155316531755185319532053215316531200353453653703853953258353453553653741

0.010.010.050.04

00.030.02

0.010.020.040.030.01

00.02

00

0.010000000000000000

0000000

0.010.060.080.070.07

1948

756

1553

458

629

1647

259

1949

1047

1754

451

212416481154




12/22/200412/22/200412/22/200412/22/200412/22/200412/22/200412/22/200412/22/200412/22/200412/22/200412/22/200412/22/200412/23/200412/23/200412/23/200412/23/200412/23/200412/23/200412/23/200412/23/200412/26/200412/26/200412/26/200412/26/200412/30/200412/30/200412/31/200412/31/200412/31/200412/31/2004

1/1/20051/1/20051/1/20051/1/20051/1/20051/1/20051/1/20051/1/20051/1/20051/1/20051/1/20051/1/20051/2/20051/2/20051/2/20051/2/20051/2/20051/2/20051/3/2005

827953105311571253155316531753183620532153235315325345355361175384494653

4335536531353145315325335345353

2538539531053115312531353145316531853191975385392210532253231324

0.020.020.01

00000

0.010.040.030.080.040.060.01

0000000

0.01000

0.01000

0.010.01

00.010.01

00.01

0

0.010.01

00.010.030.03

00.010.020.31

1553

209

9162355423

1349

129

309427

806948

1124

13411401164018001918714800

23007

1250

917

605

1400

215320436

816

1130

13521402

1830

IT!

$$$$$$$$$


Time Precip Beginning EndingStation Date (EST) (in.) Time Time QualifierBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMG

1/3/20051/3/20051/3/20051/3/20051/3/20051/3/20051/3/20051/3/20051/3/20051/3/20051/3/20051/3/20051/3/20051/3/20051/3/20051/3/20051/3/20051/3/20051/3/20051/3/20051/3/20051/3/20051/3/20051/4/20051/4/20051/4/20051/4/20051/4/20051/4/20051/4/20051/4/20051/4/20051/5/20051/5/20051/5/20051/5/20051/5/20051/5/20051/5/20051/5/20051/5/20051/5/20051/5/20051/5/20051/5/20051/5/20051/5/20051/5/20051/5/2005

15324135345355365375385391610531153123313531453155316531753185319532053215322532325

5316431753185319532053215322222313

5315334245350965375385395310531118125313531453155316531753

0.020.140.090.040.050.140.250.130.030.10.110.070.02

00.010.01

00.040.020.040.040.090.040.030.050.110.080.1

0.070.150.01

00.140.240.120.130.020.070.150.180.080.11

00.020.060.180.140.110.18

142

459

1404

1735

12

11561334

445

13411426

1637

232538

2211

1336




1/5/20051/5/20051/5/20051/6/20051/6/20051/6/20051/6/20051/6/20051/6/20051/6/20051/6/20051/7/20051/7/20051/7/20051/7/20051/7/20051/8/20051/8/20051/8/20051/8/20051/8/20051/8/20051/8/20051/10/20051/11/20051/11/20051/11/20051/11/20051/11/20051/11/20051/11/20051/11/20051/11/20051/11/20051/11/20051/11/20051/11/20051/12/20051/12/20051/12/20051/12/20051/12/20051/13/20051/13/20051/13/20051/13/20051/13/20051/13/20051/13/2005

195320532153

531532533534535531056115319532053215322532317

5315325335345355365319531535536537538531053115312531353145315531653195321555365375385335365375385395310531153

0.140.080.170.060.060.040.040.010.01

000

0.030.050.10.060.080.080.060.01

000

0.010.010.010.040.210.03

00.010.03

00.01

00.01

0

0.01000

0.130.30.290.060.020.06

11151949

553639

1050

1207

14101551

157

620724825

607

1127

629

852

1427

1907

629734835

$




1/13/20051/13/20051/13/20051/13/20051/13/20051/13/20051/13/20051/13/20051/13/20051/13/20051/16/20051/16/20051/16/20051/16/20051/16/20051/16/20051/16/20051/16/20051/16/20051/16/20051/16/20051/19/20051/20/20051/20/20051/20/20051/20/20051/20/20051/20/20051/21/20051/21/20051/21/20051/21/20051/21/20051/22/20051/22/20051/22/20051/22/20051/22/20051/22/20051/22/20051/22/20051/22/20051/22/20051/23/20051/23/20051/23/20051/23/20051/23/20051/23/2005

1253135314531553162617531853195320532100353453553653731853953105311531253135345375311531253215322532339531532533534539531053115312531353145315531653175318535536537538539531053

0.070.120.210.08

00.020.02

00000

0.01000000000000

0.030.01

0000000

0.010.01

0000000

16581826

315

703113012132057

949

1827

1348

72811421249

1844$$$$$$



BMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMGBMG

1/23/20051/23/20051/23/20051/23/20051/23/20051/23/20051/23/20051/23/20051/23/20051/23/20051/23/20051/23/20051/24/20051/24/20051/24/20051/24/20051/24/20051/24/20051/24/20051/24/20051/25/20051/25/20051/25/20051/25/20051/29/20051/29/20051/29/20051/29/20051/29/20051/29/20051/29/20051/29/20051/29/20051/29/20051/29/20051/29/20051/29/20051/29/20051/29/20051/30/2005

115312531353145315531653175318531953205321532253

53153253353453553653753553653953105335345355365375385395310531153125317531853205321532253

53

00

0.010.010.030.020.020.01

00

0.010.010.010.01

00

350

826

1139

2010

616

831

1043

1219

2202

$$$$$$$$$$$$$$$$$$$$$$$$


APPENDIX E

Transducer Maintenance Log

Lemon Lane Landfill Q4 2004 instrument Maintenance Log

Illinois Central SInstrument

EZLogger

MW-6:Instrument

Troll 4000 #13566

MW-20:Instrument

Troll 8000 #40527mini-Troll #4634

PZ-H:Instrument

mini-Troll #591 6

Troll 4000 #13510

PZ-I:Instrument

Troll 4000 #135 10

jr/ng EmergDate

12/10/2004

1/14/2005

Date11/18/2004

Date11/3/200411/3/200411/18/2004

1/7/2005

Date11/5/2004

11/17/200411/18/2004

Date11/17/2004

ence:Action

Conductivity probe submerged, not buried in sed, but embeddedin a mass of algae near the orifice; reading 65 units higher thanOrion meter. Removed some algae & cleaned probe.Temp sensor wire was disconnected on 12/25, resulting in poordata quality. Cause of disconnection unknown. Repairs weremade on 1/14.

ActionRe-indexed by 0.02'

ActionOff by 0.15'. T8 now in shop for new batteriesInstalledRe-indexed by 0.02'Removed from station for use elsewhere.

and cond calib.

ActionOff by 0.55'. Cause of difference unknown, but this mT startedcollecting erratic data on 1 1/1/04. mT was moved elsewhere.InstalledRe-indexed by 0.16'

ActionRemoved from station for use elsewhere.

viacom inc. epa region 5 records ctr. · viacom inc. epa region 5 records ctr. 253775 dorothy m....

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