tpr-cufe2o3.pdf

ChemiSoft TPx V1.02 Unit 1 (2720) Serial # 112

Sample: TPR-Rohit-CuFe2O3 18-06-12Operator: Tarun

Submitter:File: D:\ALL\TPX\DATA\SANCHIT\000-275.SMP

Started: 6/18/2012 6:27:04PM Sample Mass: 0.6690 gCompleted: Report Time: 6/18/2012 7:52:07PM

Summary Report

Experiment 1: TPR Ce Zr Support Tarun

Analysis Type: Temperature Programmed ReductionCalibration: (CHM_0005) sushil new caliberation file

Measured Flow Rate: 30.00 mL STP/minSignal Offset: -0.58381

Signal Inverted: No

PeakNumber

Temperatureat Maximum

(°C)

Volume(mL/g STP)

Peak Height

1 360.7 0.55870 0.032542 519.1 1.34454 0.054573 626.7 0.00601 0.002214 640.0 0.00277 0.00152





Tabular Report

Experiment 1: TPR Ce Zr Support Tarun

Sampling Interval: 1.0 sAnalysis Type: Temperature Programmed Reduction

Time(minutes)

Temperature(°C)

TCD Signal FurnaceTemp. (°C)

Auxiliary 2

0.00 31.7 0.00000 33.07 0.02 31.7 -0.00003 32.95 0.03 31.7 -0.00001 32.82 0.05 31.7 -0.00002 32.44 0.07 31.7 -0.00003 32.39 0.08 31.7 -0.00002 32.50 0.10 31.7 -0.00001 32.42 0.12 31.7 0.00000 32.45 0.13 31.7 -0.00003 32.38 0.15 31.7 -0.00002 32.59 0.17 31.7 -0.00001 32.65 0.18 31.7 -0.00001 32.56 0.20 31.7 -0.00001 32.58 0.22 31.7 0.00001 32.61 0.23 31.7 -0.00001 32.57 0.25 31.7 0.00001 32.50 0.27 31.7 -0.00001 32.58 0.28 31.7 -0.00002 32.52 0.30 31.7 -0.00001 32.55 0.32 31.7 0.00001 32.62 0.33 31.7 0.00002 32.62 0.35 31.7 0.00000 32.61 0.37 31.8 -0.00002 32.66 0.38 31.7 -0.00002 32.71 0.40 31.7 -0.00001 32.66 0.42 31.7 0.00001 32.71 0.43 31.8 0.00001 32.77 0.45 31.8 -0.00001 32.89 0.47 31.8 0.00000 32.87 0.48 31.8 0.00002 32.88 0.50 31.8 -0.00001 32.96 0.52 31.8 -0.00001 33.01 0.53 31.9 -0.00001 33.08 0.55 31.9 -0.00004 33.08 0.57 31.9 -0.00004 33.13 0.58 31.8 -0.00002 33.17 0.60 31.9 -0.00002 33.25 0.62 31.9 -0.00003 33.39 0.63 32.0 -0.00001 33.50 0.65 32.0 -0.00002 33.60 0.67 32.0 -0.00002 33.71 0.68 32.1 -0.00002 33.81 0.70 32.1 -0.00002 33.90 0.72 32.2 -0.00002 33.94 0.73 32.2 -0.00001 34.06 0.75 32.2 -0.00004 34.16 0.77 32.2 -0.00002 34.31 0.78 32.3 -0.00002 34.40





Time(minutes)

Temperature(°C)


Auxiliary 2

0.80 32.3 -0.00001 34.47 0.82 32.4 -0.00003 34.66 0.83 32.4 -0.00004 34.86 0.85 32.5 -0.00002 35.04 0.87 32.6 0.00000 35.17 0.88 32.6 -0.00004 35.39 0.90 32.7 -0.00002 35.57 0.92 32.7 -0.00002 35.70 0.93 32.8 -0.00001 35.93 0.95 32.9 -0.00001 36.09 0.97 32.9 -0.00004 36.29 0.98 32.9 -0.00002 36.43 1.00 33.1 -0.00003 36.63 1.02 33.1 -0.00004 36.63 1.03 33.1 -0.00002 36.95 1.05 33.2 -0.00005 37.20 1.07 33.3 -0.00002 37.44 1.08 33.4 -0.00003 37.71 1.10 33.4 -0.00004 38.09 1.12 33.5 -0.00005 38.26 1.13 33.6 -0.00006 38.48 1.15 33.7 -0.00004 38.74 1.17 33.8 -0.00004 39.00 1.18 33.9 -0.00005 39.11 1.20 34.0 -0.00004 39.38 1.22 34.0 -0.00003 39.70 1.23 34.1 -0.00005 39.85 1.25 34.2 -0.00003 40.02 1.27 34.3 -0.00004 40.32 1.28 34.4 -0.00005 40.61 1.30 34.5 -0.00004 40.78 1.32 34.5 -0.00004 40.67 1.33 34.5 -0.00008 40.92 1.35 34.6 -0.00007 41.11 1.37 34.6 -0.00007 41.21 1.38 34.7 -0.00009 41.42 1.40 34.7 -0.00009 42.06 1.42 34.8 -0.00004 42.23 1.43 34.9 -0.00008 42.53 1.45 35.0 -0.00008 42.73 1.47 35.1 -0.00007 43.06 1.48 35.2 -0.00007 43.32 1.50 35.3 -0.00008 43.50 1.52 35.4 -0.00009 43.79 1.53 35.5 -0.00009 43.89 1.55 35.6 -0.00006 44.01 1.57 35.7 -0.00007 44.21 1.58 35.7 -0.00008 44.48 1.60 35.8 -0.00011 44.75 1.62 35.9 -0.00009 44.99 1.63 36.0 -0.00010 45.24 1.65 36.2 -0.00009 45.61 1.67 36.3 -0.00011 45.87 1.68 36.4 -0.00012 46.13





Time(minutes)

Temperature(°C)


Auxiliary 2

1.70 36.5 -0.00009 46.38 1.72 36.5 -0.00013 46.54 1.73 36.6 -0.00011 46.66 1.75 36.8 -0.00011 46.69 1.77 36.9 -0.00012 46.97 1.78 37.0 -0.00013 47.17 1.80 37.1 -0.00014 47.35 1.82 37.1 -0.00013 47.57 1.83 37.2 -0.00013 47.60 1.85 37.2 -0.00016 48.10 1.87 37.3 -0.00015 48.21 1.88 37.5 -0.00015 48.43 1.90 37.6 -0.00015 48.70 1.92 37.7 -0.00016 48.79 1.93 37.9 -0.00017 49.09 1.95 37.9 -0.00017 48.99 1.97 38.1 -0.00016 49.23 1.98 38.2 -0.00017 49.63 2.00 38.3 -0.00016 49.64 2.02 38.5 -0.00018 49.93 2.03 38.6 -0.00019 50.27 2.05 38.7 -0.00016 50.48 2.07 38.8 -0.00017 50.54 2.08 38.9 -0.00021 50.74 2.10 39.1 -0.00019 50.93 2.12 39.1 -0.00018 51.03 2.13 39.3 -0.00020 50.99 2.15 39.4 -0.00018 51.35 2.17 39.5 -0.00018 51.36 2.18 39.6 -0.00020 51.64 2.20 39.7 -0.00021 51.75 2.22 39.7 -0.00020 51.85 2.23 39.8 -0.00019 52.00 2.25 39.8 -0.00020 52.13 2.27 40.0 -0.00021 52.22 2.28 40.1 -0.00022 52.13 2.30 40.2 -0.00021 52.38 2.32 40.3 -0.00020 52.60 2.33 40.4 -0.00021 52.64 2.35 40.6 -0.00020 52.87 2.37 40.7 -0.00022 53.05 2.38 40.9 -0.00021 53.20 2.40 40.9 -0.00023 53.28 2.42 41.0 -0.00023 53.41 2.43 41.2 -0.00023 53.56 2.45 41.2 -0.00024 53.58 2.47 41.4 -0.00023 53.92 2.48 41.5 -0.00021 54.03 2.50 41.6 -0.00023 54.16 2.52 41.7 -0.00021 54.20 2.53 41.8 -0.00022 54.41 2.55 41.9 -0.00023 54.59 2.57 42.0 -0.00021 54.72 2.58 42.1 -0.00022 54.79





Time(minutes)

Temperature(°C)


Auxiliary 2

2.60 42.3 -0.00021 54.98 2.62 42.4 -0.00022 54.95 2.63 42.4 -0.00023 55.17 2.65 42.5 -0.00023 55.22 2.67 42.6 -0.00023 55.10 2.68 42.7 -0.00021 55.33 2.70 42.7 -0.00025 55.32 2.72 42.9 -0.00025 55.60 2.73 42.9 -0.00021 55.66 2.75 43.0 -0.00023 55.83 2.77 43.1 -0.00025 55.89 2.78 43.2 -0.00020 55.96 2.80 43.2 -0.00021 56.07 2.82 43.4 -0.00023 56.23 2.83 43.5 -0.00021 56.38 2.85 43.6 -0.00025 56.60 2.87 43.7 -0.00023 56.73 2.88 43.9 -0.00022 56.92 2.90 44.0 -0.00020 56.96 2.92 44.2 -0.00021 57.10 2.93 44.3 -0.00021 57.33 2.95 44.4 -0.00023 57.36 2.97 44.5 -0.00022 57.54 2.98 44.7 -0.00018 57.86 3.00 44.8 -0.00020 58.03 3.02 44.9 -0.00022 58.21 3.03 45.0 -0.00021 58.39 3.05 45.2 -0.00021 58.65 3.07 45.3 -0.00021 58.76 3.08 45.4 -0.00018 58.97 3.10 45.6 -0.00020 59.14 3.12 45.7 -0.00020 59.34 3.13 45.8 -0.00017 59.52 3.15 45.9 -0.00020 59.65 3.17 46.1 -0.00021 59.87 3.18 46.2 -0.00022 60.10 3.20 46.4 -0.00019 60.31 3.22 46.5 -0.00020 60.49 3.23 46.6 -0.00020 60.66 3.25 46.7 -0.00019 60.75 3.27 46.8 -0.00021 60.86 3.28 47.0 -0.00021 60.85 3.30 47.1 -0.00022 61.12 3.32 47.2 -0.00020 61.28 3.33 47.3 -0.00020 61.46 3.35 47.5 -0.00019 61.64 3.37 47.5 -0.00020 61.88 3.38 47.6 -0.00021 62.02 3.40 47.6 -0.00019 62.13 3.42 47.6 -0.00020 62.14 3.43 47.6 -0.00020 62.23 3.45 47.7 -0.00018 62.36 3.47 47.8 -0.00016 62.51 3.48 48.0 -0.00018 62.84





Time(minutes)

Temperature(°C)


Auxiliary 2

3.50 48.1 -0.00019 63.00 3.52 48.3 -0.00016 63.26 3.53 48.5 -0.00018 63.46 3.55 48.6 -0.00015 63.63 3.57 48.8 -0.00015 63.87 3.58 49.0 -0.00016 64.03 3.60 49.1 -0.00015 64.22 3.62 49.3 -0.00016 64.42 3.63 49.4 -0.00016 64.64 3.65 49.6 -0.00016 64.93 3.67 49.8 -0.00015 65.21 3.68 49.9 -0.00015 65.41 3.70 50.0 -0.00015 65.56 3.72 50.2 -0.00015 65.81 3.73 50.3 -0.00017 65.96 3.75 50.5 -0.00016 66.17 3.77 50.6 -0.00016 66.37 3.78 50.8 -0.00017 66.62 3.80 50.9 -0.00017 66.55 3.82 50.9 -0.00015 66.49 3.83 50.8 -0.00016 66.34 3.85 50.9 -0.00018 66.48 3.87 51.0 -0.00019 66.61 3.88 51.1 -0.00019 66.85 3.90 51.3 -0.00016 67.03 3.92 51.5 -0.00017 67.26 3.93 51.6 -0.00017 67.44 3.95 51.8 -0.00016 67.53 3.97 51.9 -0.00015 67.85 3.98 52.0 -0.00016 68.09 4.00 52.1 -0.00016 68.27 4.02 52.2 -0.00018 68.41 4.03 52.3 -0.00018 68.62 4.05 52.4 -0.00015 68.75 4.07 52.6 -0.00014 69.00 4.08 52.8 -0.00016 69.23 4.10 52.9 -0.00014 69.51 4.12 53.1 -0.00015 69.70 4.13 53.3 -0.00017 69.77 4.15 53.4 -0.00015 69.90 4.17 53.6 -0.00015 70.12 4.18 53.8 -0.00016 70.35 4.20 53.9 -0.00015 70.53 4.22 54.1 -0.00013 70.50 4.23 54.2 -0.00016 70.65 4.25 54.4 -0.00014 70.75 4.27 54.4 -0.00015 70.84 4.28 54.6 -0.00012 71.08 4.30 54.6 -0.00013 71.04 4.32 54.7 -0.00014 71.16 4.33 54.8 -0.00012 71.21 4.35 54.9 -0.00012 71.68 4.37 55.1 -0.00014 71.93 4.38 55.3 -0.00013 72.17





Time(minutes)

Temperature(°C)


Auxiliary 2

4.40 55.4 -0.00016 72.37 4.42 55.6 -0.00017 72.51 4.43 55.8 -0.00015 72.76 4.45 55.9 -0.00017 72.97 4.47 56.1 -0.00016 73.23 4.48 56.3 -0.00017 73.44 4.50 56.4 -0.00018 73.63 4.52 56.6 -0.00017 73.68 4.53 56.8 -0.00020 73.83 4.55 57.0 -0.00016 73.92 4.57 57.2 -0.00016 74.19 4.58 57.4 -0.00016 74.43 4.60 57.5 -0.00017 74.71 4.62 57.7 -0.00017 74.92 4.63 57.9 -0.00014 75.14 4.65 58.2 -0.00015 75.56 4.67 58.3 -0.00012 75.87 4.68 58.5 -0.00013 76.06 4.70 58.7 -0.00012 76.22 4.72 58.9 -0.00012 76.48 4.73 59.1 -0.00011 76.60 4.75 59.2 -0.00011 76.54 4.77 59.4 -0.00009 76.70 4.78 59.5 -0.00013 76.85 4.80 59.6 -0.00013 77.05 4.82 59.7 -0.00012 77.21 4.83 59.8 -0.00011 77.30 4.85 60.0 -0.00010 77.62 4.87 60.1 -0.00010 77.95 4.88 60.3 -0.00011 78.15 4.90 60.5 -0.00010 78.27 4.92 60.6 -0.00010 78.44 4.93 60.8 -0.00012 78.52 4.95 60.9 -0.00013 78.65 4.97 61.1 -0.00013 78.69 4.98 61.3 -0.00012 78.90 5.00 61.4 -0.00013 78.99 5.02 61.5 -0.00012 79.20 5.03 61.7 -0.00013 79.37 5.05 61.9 -0.00012 79.61 5.07 62.0 -0.00013 79.76 5.08 62.2 -0.00015 80.06 5.10 62.4 -0.00014 80.19 5.12 62.6 -0.00008 80.34 5.13 62.6 -0.00010 80.30 5.15 62.6 -0.00010 80.21 5.17 62.6 -0.00009 80.33 5.18 62.6 -0.00012 80.29 5.20 62.8 -0.00011 80.46 5.22 63.0 -0.00010 80.58 5.23 63.1 -0.00010 80.78 5.25 63.3 -0.00007 80.76 5.27 63.4 -0.00007 80.94 5.28 63.6 -0.00009 81.16





Time(minutes)

Temperature(°C)


Auxiliary 2

5.30 63.8 -0.00009 81.29 5.32 63.9 -0.00007 81.50 5.33 64.1 -0.00008 81.58 5.35 64.3 -0.00009 81.95 5.37 64.4 -0.00008 82.03 5.38 64.5 -0.00009 82.15 5.40 64.7 -0.00009 82.32 5.42 64.8 -0.00009 82.41 5.43 64.9 -0.00009 82.55 5.45 65.0 -0.00010 82.60 5.47 65.1 -0.00009 82.74 5.48 65.3 -0.00013 82.87 5.50 65.4 -0.00011 83.01 5.52 65.6 -0.00013 83.22 5.53 65.8 -0.00012 83.45 5.55 65.9 -0.00013 83.54 5.57 66.1 -0.00013 83.78 5.58 66.3 -0.00010 83.95 5.60 66.5 -0.00011 84.07 5.62 66.7 -0.00010 84.30 5.63 66.9 -0.00011 84.50 5.65 67.0 -0.00009 84.72 5.67 67.2 -0.00009 84.92 5.68 67.4 -0.00010 85.08 5.70 67.5 -0.00009 85.25 5.72 67.6 -0.00009 85.42 5.73 67.8 -0.00010 85.57 5.75 67.9 -0.00008 85.77 5.77 68.1 -0.00010 85.99 5.78 68.2 -0.00007 86.17 5.80 68.4 -0.00005 86.34 5.82 68.5 -0.00005 86.53 5.83 68.7 -0.00007 86.66 5.85 68.9 -0.00007 86.90 5.87 69.1 -0.00007 87.03 5.88 69.2 -0.00007 87.22 5.90 69.4 -0.00007 87.41 5.92 69.6 -0.00007 87.62 5.93 69.8 -0.00003 87.82 5.95 70.0 -0.00006 88.02 5.97 70.2 -0.00004 88.22 5.98 70.3 -0.00005 88.37 6.00 70.5 -0.00004 88.65 6.02 70.7 -0.00004 88.82 6.03 70.9 -0.00001 89.03 6.05 71.1 -0.00002 89.21 6.07 71.2 0.00000 89.38 6.08 71.4 -0.00001 89.57 6.10 71.6 0.00001 89.74 6.12 71.7 0.00001 89.87 6.13 71.9 0.00000 90.05 6.15 72.1 0.00001 90.23 6.17 72.2 -0.00001 90.46 6.18 72.4 -0.00001 90.65





Time(minutes)

Temperature(°C)


Auxiliary 2

6.20 72.6 0.00000 90.77 6.22 72.8 0.00001 90.95 6.23 73.0 0.00001 91.12 6.25 73.2 -0.00001 91.28 6.27 73.3 0.00000 91.46 6.28 73.5 0.00001 91.67 6.30 73.7 -0.00001 91.97 6.32 73.9 0.00003 92.16 6.33 74.1 0.00002 92.36 6.35 74.2 0.00003 92.51 6.37 74.5 0.00002 92.75 6.38 74.6 0.00002 92.82 6.40 74.7 0.00002 93.03 6.42 74.8 0.00001 93.13 6.43 75.0 0.00001 93.26 6.45 75.2 0.00001 93.45 6.47 75.4 0.00002 93.66 6.48 75.5 0.00001 93.81 6.50 75.7 0.00002 93.96 6.52 75.9 0.00004 94.12 6.53 76.1 0.00004 94.24 6.55 76.2 0.00003 94.41 6.57 76.4 0.00005 94.54 6.58 76.6 0.00004 94.77 6.60 76.8 0.00005 94.99 6.62 76.9 0.00005 95.18 6.63 77.1 0.00005 95.37 6.65 77.2 0.00005 95.57 6.67 77.4 0.00004 95.68 6.68 77.6 0.00004 95.84 6.70 77.8 0.00007 95.99 6.72 77.9 0.00005 96.11 6.73 78.0 0.00003 96.30 6.75 78.2 0.00005 96.43 6.77 78.4 0.00005 96.58 6.78 78.5 0.00005 96.60 6.80 78.6 0.00002 96.73 6.82 78.7 0.00003 96.79 6.83 78.9 0.00004 96.97 6.85 79.1 0.00003 97.12 6.87 79.2 0.00005 97.33 6.88 79.4 0.00003 97.47 6.90 79.6 0.00004 97.63 6.92 79.8 0.00004 97.82 6.93 79.9 0.00004 97.98 6.95 80.1 0.00005 98.19 6.97 80.3 0.00005 98.32 6.98 80.4 0.00004 98.49 7.00 80.6 0.00005 98.67 7.02 80.8 0.00007 98.83 7.03 81.0 0.00007 99.01 7.05 81.1 0.00004 99.13 7.07 81.3 0.00005 99.30 7.08 81.5 0.00005 99.43





Time(minutes)

Temperature(°C)


Auxiliary 2

7.10 81.6 0.00002 99.54 7.12 81.8 0.00002 99.65 7.13 81.9 0.00002 99.93 7.15 82.1 0.00002 100.01 7.17 82.3 0.00002 100.18 7.18 82.4 0.00002 100.33 7.20 82.6 0.00003 100.44 7.22 82.7 0.00005 100.68 7.23 82.9 0.00007 100.84 7.25 83.1 0.00006 100.94 7.27 83.2 0.00005 101.07 7.28 83.5 0.00007 101.28 7.30 83.6 0.00009 101.46 7.32 83.8 0.00009 101.60 7.33 83.9 0.00008 101.76 7.35 84.1 0.00005 102.00 7.37 84.2 0.00009 102.14 7.38 84.4 0.00007 102.26 7.40 84.5 0.00007 102.40 7.42 84.7 0.00006 102.60 7.43 84.9 0.00007 102.70 7.45 85.0 0.00005 102.90 7.47 85.2 0.00006 103.00 7.48 85.4 0.00005 103.16 7.50 85.6 0.00006 103.38 7.52 85.7 0.00007 103.39 7.53 85.8 0.00005 103.61 7.55 86.0 0.00007 103.76 7.57 86.0 0.00008 103.83 7.58 86.2 0.00008 104.05 7.60 86.2 0.00009 104.15 7.62 86.3 0.00010 104.24 7.63 86.5 0.00011 104.41 7.65 86.7 0.00013 104.61 7.67 86.8 0.00011 104.80 7.68 87.0 0.00013 105.05 7.70 87.3 0.00013 105.18 7.72 87.4 0.00012 105.31 7.73 87.6 0.00014 105.45 7.75 87.7 0.00012 105.60 7.77 87.9 0.00012 105.75 7.78 88.1 0.00011 105.88 7.80 88.3 0.00010 106.14 7.82 88.5 0.00010 106.33 7.83 88.7 0.00011 106.51 7.85 88.9 0.00011 106.70 7.87 89.0 0.00012 106.90 7.88 89.2 0.00013 107.06 7.90 89.4 0.00012 107.37 7.92 89.6 0.00013 107.55 7.93 89.9 0.00015 107.75 7.95 90.0 0.00012 107.94 7.97 90.2 0.00012 108.14 7.98 90.4 0.00015 108.33





Time(minutes)

Temperature(°C)


Auxiliary 2

8.00 90.5 0.00015 108.44 8.02 90.7 0.00016 108.67 8.03 90.9 0.00016 108.82 8.05 91.1 0.00017 109.06 8.07 91.3 0.00018 108.94 8.08 91.4 0.00018 109.21 8.10 91.6 0.00016 109.39 8.12 91.8 0.00018 109.62 8.13 92.0 0.00019 109.91 8.15 92.2 0.00017 110.08 8.17 92.4 0.00020 110.32 8.18 92.6 0.00020 110.52 8.20 92.8 0.00017 110.83 8.22 92.9 0.00018 110.99 8.23 93.1 0.00019 111.22 8.25 93.3 0.00020 111.40 8.27 93.5 0.00019 111.15 8.28 93.6 0.00020 111.71 8.30 93.8 0.00019 111.83 8.32 94.0 0.00020 111.96

The table has been truncated to 500 entries. Consider using a larger sampling interval.





Temperature (°C)5050 100 150 200 250 300 350 400 450 500 550 600 650 700

TC

D S

ign

al (a

.u.)

0.000.00

0.01

0.02

0.03

0.04

0.05

0.06

TCD Signal (a.u.) vs. Temperature

TCD Signal (a.u.) - TPR Ce Zr Support Tarun





4227- The data requested on this report are not available.

tpr-cufe2o3.pdf

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